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ADULTEKATIONS  DETECTED; 

5;7/::"j-;3  i:;;;;::?3iTit 

OR,      PLAIN      IKSTEircTIONa      POB     THE  ^    _.    i/.'Ji'QJI^    OhlVE 

\fjj  ALVO,  UUF. 


FOOD    AND    MEDICINE. 


BY 


s-n 


.it*/ 


ARTHUR   HILL[HASSALL,  M.D.,   Lond. 

ANALTST  OP  *'  THE  LANCET  BANITABT  C03f  UIS3I0X  :  " 


AUTHOH  or 

lllft:    RKI'OBTH  or  THAT  COMMISKIUN,   NOW   prBMSIIKI>   t'NDKR  TIIK  TITLE   OF 
**  ruO»   AND    ITS  AUULTEKATION'})  ;" 

ALSO  or 

**  A    HI!«TURT  or  THE   BRITISH    yRKSIIWATKR   ALG.Kj" 


"the    MICROHCOPIC    ANATOMY    Or    THE    HL'MAN     BO  I>V  ; " 
AMD  OTHER  VOBXS. 


LAWl   Ubi\ru*l-    iJi....»^..L>    Oii 


i^VERSilY 


LONDON: 
LONGMAN.  BROWN,  GREEN.  LONGMANS,  AND  ROBERTS. 

1857. 


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ADULTEKATIONS  DETECTED; 

sv;-;-:.7j  i:  ;:-.-i:^3iTX 

OB,      PtllN      INBTEUCTIONS     POB     THE  ^  .^    j  /.jjrj,^    ''luiVE 


FOOD    AND    MEDICINE. 


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vn 


'*•>*/ 


ARTHUR  HILL[HASSALL,   M.D.,   Lond. 

ASALTBT  OP  "  THE  LANCET  SANITARY  C0MMIS3I0X  :  " 


i.UTROK  Of 

THE   RErORTS  OF  THAT  COMMIMIUN,   NOW   rUBI.ISHKIl   UNDKR  TIIR  TITLE  OF 
"  FOOD  AND   ITS  ADKLTKHATIU.NH  ;  " 

ALSO  OF 
**  A   HISTORY  OF  THE   BRITISH    FRRKHWATRR   ALO.K  ; '* 


THR    MICROSCOPIC    AKATOMY    OF    THR    HUMAN     BODY;" 
ASD  OTHSB  WOBKH. 

LANE  Liuun..V.  o. j-u  oiiiVERSlTY 


LONDON: 
LONGMAN,  BROWN,  GREEN,  LONGMANS,  AND  ROBERTS. 

1857. 


Tk&  Hf/U  qf  traiulatioH  U  rwMmif . 


BRTXRU>  AT   6TAT10NXKS    !(ALI. 


A 


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PREFACE, 


TaE  present  work  is  not  intended  to  supcrsedo  my  previous 
book,  entitled  "  Food  and  its  Adulterations  ; "  the  plans  and 
objects  of  the  two  works  being  distinct. 

The  principal  objects  of  the  Jirst  and  larger  work  were,  and 
•till  are,  to  demonstrate  the  exist4>nce  of  extensive  adulteration, 
in  all  the  more  important  articles  of  daily  consumption,  as 
actually  supplied  by  mtirchants  and  traders  to  the  public ;  to 
show  that  adulteration  largely  affected  the  pecuniary  interests 
of  the  consumer  and  the  revenue ;  and  that  it  was  a  question  most 
seriously  affecting  the  public  health.  These  objects  tlie  work 
in  question  lias  fully  accoraplished. 

Aaooe  of  the  results  of  my  former  investigations,  the  import- 
ance of  the  subject  of  aduUeration  has  been  recently  officially 
■cknowledged  by  the  ftppr>ihlment  by  the  House  of  Commons  of  a 
Select  Committee  to  inquire  into  tbe  matter.  This  Committee, 
Wider  the  able  presidency  of  Mr.  Sclioleneld,  M.P.  for  Birming- 
huOf  xealously  prosecuted  its  inquiries  ibr  two  sessions  of 
Parliament,  and  the  result  has  been  to  confirm,  to  the  fall 
extent,  the  accuracy  and  fidelity  of  the  investigations,  in  the 
intMecution  of  which,  mainly  through  the  medium  of  **  The 
lAncet**  I  have  been  engaged  for  so  many  years.  The  Report 
of  this  Committee  lias  been  laid  before  the  House.  It  ac- 
kAOwiedges  that   adulteration    widely  prevails;   that   the  evil 

k   '2 


VI 


PKEFACE. 


requires  to  be  dealt  wiih  by  the  Legislature  ;  and  it  containfl 
suggestions  and  recommendations  for  the  euppression  of  adulte- 
ration. 

The  Committee  state  that  they  "cannot  avoid  the  conclusion 
that  ndulteration  widely  prcvaiW  "Not  only  is  the  public 
health  thus  exposed  to  danger,  and  pecuniary  fraud  coinmiltcd 
on  the  whole  commnniry,  but  the  public  morality  is  tainted,  and 
the  high  commercial  cliaructer  of  the  country  seriously  lowered 
both  at  home  and  in  the  eyes  of  foreign  countries." 

Thesti  are  ^rave  statements  and  admiasions,  made  on  the  very 
highest  authority. 

The  chief  purpose  of  M#  present  work  is  to  furnish  plain  in- 
structions, microscopical  and  chemical,  embodying  the  results  of 
extended  practice  and  experience,  for  the  discovery  of  adulte- 
rations in  Food  and  Medicine. 

To  accomplish  this  object  effectually,  it  will  be  necessary 
that  the  adulterations  to  which  each  particular  Jiriicle  of  con- 
sumption or  drug  is  subjected,  should  be  described  in  as  concise 
yet  clear  ii  manner  as  possible-  The  treatise  will  tberefore  not 
he  limiteii  to  a  mere  description  of  the  methods  by  which  adul- 
teration may  be  discovered,  but  will  contain  much  infurmalion 
in  relation  to  adulteration  in  general. 

The  best  method  of  putting  a  stop  to  adulteration  is  undoubt- 
edly to  destroy  the  security  attending  the  practice  of  it. 

The  first  step  necessary  for  the  accomplishmenl  nf  this  object 
is  to  supply  the  means  requisite  for  the  discovery  of  adulteration. 

The  happy  application  of  the  microscope  to  the  subject  of 
adulteration,  lias  furnished  tht*.  means  of  detecting  u  host  of 
ndulterntioQS,  the  discovery  of  which  had  before,  for  the  most 
part,  been  considered  to  be  impossible  ;  but  still  practical  expla- 
nations and  details  are  required  to  enable  others  to  employ  the< 
instrument  with  advantage  for  that  purpose;  and  the  same 
remark  applies  to  chemistry.    Such  necessary  details  and  e\pla- 


PUEFACE. 


Vll 


Tintionp,  accompanied  by  a  large  number  of  microscopical 
illustrations,  it  is  hoped  will  be  found  in  the  pages  of  this 
work,  and  that,  through  ita  inBtrumentality^  the  many  huudreda 
of  microseopists  and  chenaists  scattered  over  all  parts  of  the 
country,  will  be  induced  to  upply  themselves  to  the  discovery  of 
adulterations  in  articles  of  food  und  medicine,  in  the  resiipective 
neighbourhoods  and  localities  in  which  they  reside.  Should 
this  anticipation  be  realised,  "a  heavy  blow  and  grcAt  discour- 
agement **  will  be  inflicted  upon  all  adulterators,  for  the  se- 
cuiity  in  which  their  proceedings  were  formerly  conducted 
will  bo  for  ever  destroyed. 

The  more  frequent  discovery  of  adulteration  will  doubtless 
lead,  in  many  cases,  to  the  publication  of  the  names  and  addreftses 
of  the  parties  perpetrating  it.  It  was  this  publication  which 
contributed  so  essentially  to  the  success  of  my  reports  in  "  The 
Lancet."  By  it  direct  responsibility  was  secured,  the  honest 
tradesmaa  was  distinguished  from  his  unscrupulous  com- 
petitor, and  in  many  instances  the  olfence  of  adulteration  was 
brought  home  to  the  parties  actually  guilty  of  it. 

This  unparalleled  proceeding  was  in  the  first  instance,  and 
when  science  hud  been  but  imperfectly  opplied  to  the  detection 
of  adulteration,  attended  with  the  utmost  hazard,  not  only  to 
Mr.  Wakley,  who  suggested  the  publication  of  the  names,  and 
who  incurred  the  legal  risk  attendant  thereon,  hut  also  to 
myself,  staking  as  I  did  reputation  and  prospects  alike  upon  the 
issue  of  a  most  arduous  and  responsible  undertaking. 

Id  publishing  the  present  treatise,  and  in  thus  supplying  a 
public  want,  I  am  realising  a  suggestion  for  the  suppression  of 
adulteration  which  I  made  in  evidence  before  the  Select  Com- 
mittee on  Adulteration,  in  July  18o5,  namely,  that  a  cheap 
treatise  on  adulteration  should  be  published,  which  *' should  be 
illustrated  with  wood-cuts  showing  the  microscopicol  appear- 
ances and  structure  of  the  diiferent  articles,  both  genuine  and 

X4 


vni 


PREFACE. 


adulterated^  and  cont^ning  plain  directions  f^r  the  discovery 
of  adaltpraiion." 

The  work  to  which  I  have  given  the  title  **  Food  and  its 
Adulterations,^  comprista  the  R<*port8,  carefully  revispil^  of  the 
Analytical  Sanitary  Commission  of  "  Tlie  Lanuet."  These 
reports  were  publiethod  a.t  short  intervals  in  that  periodical  for 
a  term  of  four  years,  commencing  January  1851,  and  ending 
December  1854,  and  they  contained  2387  analyses,  of  which 
2063  were  of  articles  of  food,  and  324  of  drugs. 

Of  these  analyses,  which  were  for  the  most  part  both  micro- 
scopicftl  and  chemical,  2222  were  made  by  myself;  and  the 
reports  being  all  written  by  me,  I  retain  the  copyright  of  them 
under  a  special  agreement. 

In  the  present  work,  the  analyses  above  referred  to  are  not 
given,  but  merely  the  general  conclusions  or  results  derived 
from  those  analyses :  in  addition  to  which,  this  work  contains 
the  results  of  the  analyses  of  several  hundreds  of  samples  of 
articles  of  food  and  drugs  which  have  never  been  published 
in  "  Tlie  Lancet,"  and  the  whole  of  which  have  been  made 
by  myself  during  the  years  1855  and  lHo6. 

Availing  himself  of  a  temporary  misunderstanding  betnrcen 
myself  and  Mr.  Wakley,  Dr.  Letheby  put  forward,  some  time 
back,  a  claim  of  so  exaggerated  and  incorrect  a  character  for  par- 
ticipation in  the  work  of '*  The  Lancet "  Commission,  which 
claim  heattemptedto  support  by  the  publication  in  "The  Times" 
newspaper  of  extracts  from  my  private  and  confidential  letters 
addressed  to  him,  that  I,  in  justice  to  myself,  consider  it  neces- 
sary to  define  once  more  in  this  plac*)  the  extent  and  nature  of 
the  assistance  rendered  by  Dr.  Letheby. 

Having  been  on  terms  of  intimacy  with  him  for  some  years, 
I  employed  liim  occasionally  to  make  certain  analyses  both 
for  myself  and  for  "The  Lancet,"  I  sending  him  the  samples, 
and  indicating  the  particulars  required.     Tlie  results  were  in 


I 


PUEFACE. 


IX 


all  cases  returned  direct  to  me,  the  analyses  charged  for  and  the 
accounts  made  out  by  Dr.  Letheby  in  my  name,  be  not  holding, 
during  the  whole  time  op  in  a  single  instance,  tlie  slightest 
communication  either  with  Mr.  Wukley  or  with  any  person 
connected  with  "The  Lancet." 

The  accounts  and  other  documents  furnished  by  Dr.  Lctheby 
Jiving  been  fortunately  preserved,  they  were  submitted  to  the 
tiny  of  Mr.  George  Bolton,  the  Rev.  R.  S.  Daniell,  5LA., 
and  others.  The  gentlemen  whose  names  are  given  above 
drew  up  a  Report,  embodying  the  results  derived  from  an 
examination  of  the  accounts,  &eM  from  which  the  following 
is  extracted  ;  — • 

'•  The  accounts  rendered  by  Dr.  Leiheby,  Ijeing  so  clear  and 
in  his  own  handwriting,  furnirih  indi^^putable  and  conclusive 
evidence  of  the  actual  number  of  analyses  performed  by  him, 
some  of  them  being  partial  analyses  only.  Tl»ua  it  is  dislinctly 
shown  that  the  entire  number  of  chemical  analyses  performed 
by  Dr.  Lctheby,  viz.  16o«  bears  but  a  very  small  proportion  to 
the  number  of  the  analyses,  as  well  microscopical  as  chemical, 
j>eriormed  by  Dr.  Ha^sall,  viz.  24S1. 

*' Of  these  samples  63  were  of  tobacco  and  snutT,  and  53  of 
opium;  thur*  leaving  48  samples  of  all  other  khids;  but  it  is 
to  be  especially  noted  tbat  the  analyses  of  these  53  samples  of 
opium  are  not  recorded  in  Dr.  Hassall's  work  on  *  Food  and  its 
Adulterations.' 

"As  witness  our  hands  this  first  day  of  August,  One  thou- 
sand eight  hundred  and  fifty-five. 

•*  Ratmond  S.  Damiell,  M.  A.,  Oxon. 
"Gkoroe  Bolton. 

•*  9.  Qaocn  Street,  Bronipton." 


It  is  perhaps  necessary  to  state  that  in   the  new  analyses, 
amounting  to  some  hundreds,  the  results  of  which  arc  recorded 


PREFACE. 


in  this  work,  ovpr  anil  above  the  2481  before  alluded  to^  Dr. 
Letheby  has  hnd  no  piirt  whatever.* 

For  the  informntion  contained  in  this  work  respecting  the 
duties  ujiuii,  and  consumption  of  the  vnrioua  articles  treated  o{\ 
we  are  indebted  to  Mr.  T.  C.  Kent,  of  Upton-on-Severn,  and 
A,  W.  Fonblanque,  Esq.,  of  the  Statistical  Department  of  the 
Board  of  Trade,  to  both  of  whom  we  tender  our  sincere  and 
cordial  thnnka  for  the  aid  thus  afforded. 

The  author  baa  spared  no  pains  or  expense  to  insure  the 
fidelity  and  cnrefu!  execution  of  the  wood  engravings.  Of  tliese 
about  two-thirds  were  drawn  on  vrtyod  by  Mr.  Henry  Miller,  un- 
der the  direct  superintendence  of  the  author,  and  the  others  by 
Mr.  Tuffen  West,  with  the  exception  of  the  figures  of  liquorice, 
which  were  drawn  by  Mr.  Searson  :  they  were  all  engnived  by 
Mr.  Hart  of  Gloucester  Street,  Bloomsbury  Square.  Nothing 
could  exceed  the  care  bestowed  by  each  of  I  he  artists  named  upon 
the  execution  of  the  (igures,  and  the  author  believes  that  no 
engravings  of  microscopic  objects  have  Mtherto  been  produced 
on  wood  superior,  and  but  few  equal,  to  those  wfiich  will  bo 
found  dispersed  through  tlie  pages  of  the  present  work. 

It  is  not  a  little  singtiliir  that  Mr,  Miller  and  Mr.  West,  two  of 
the  beat  microscopic  artists  we  have  had,  bulh  commenced  thtnr 
careers  as  artists  with  the  author.  The  first  drawings  from  the 
microscope  made  by  Mr.  Miliur,  were  for  "  The  Microscopic  Ana- 
tomy of  the  Human  Body*'  about  ten  years  since,  from  wliich 
time  until  his  death,  which  occurred  recently,  he  continued,  ex- 
cept for  a  few  short  intervals,  in  tlie  autiior's  service.  Mr.  West 
aUo  resided  with  the  author  for  a  time,  and  his  first  microsco- 
pical drawings  were  also  for  the  work  above  mentioned. 

Bennett  Street,  St.  James's  Street, 
Jaiioaiy  12tli,  1857. 

•  For  a  fullrr  rpfulntton  of  Dr.  l*thrbr'i  claim  and  irsnwurt  of  bll  ronduci,  tbc  rraclrr 
la  rplvrrnt  lo  ii  P-»niuhlci  bjr  JKmet  Cnur  UuniruJ,  K»q..  BarrlMer.  Juliii  A.  Power. 
L.  M..  M.  A..  Cnntab.  nn.l  Karrnund  8.  Danlall.  M.  A,  Uson. ;  publlihed  by  WUIIam 
'i'rgjtand  Co.,  S5.  Quf«n  Strcai,  Chwpttdv. 


CONTENTS. 


Pago 
Iktroditctobt  RsacA&xfl    -  .  .  -  -      1 

On  the  MEiLNS  bt  which  Adclteration  hat  be  detected       -    43 
Food    -  -  -  -  -  -  -63 

Tea      -  -  -  -  -  -  -     65 

Coffee  ......  ]05 

CmooBT  ......  130 

Cocoa  ......  155 

Chocolate  -  -  -  -  -  -  171 

SUOAS  -  -  -  -  .  -  181 

HONET  ......    198 

UiLK    -  -  -  -  .  .  -  205 

FlOUB  A2TD   BeBAD  .....    237 

BimBK  ......  295 

Labd    .......  301 

Oatheal  ......  306 

Abbowboot         -  -  -  -  -  -312 

Saoo    •  -  •  •  -  -  -  323 

Tapioca  -  -  -  -  .  -  327 

PBOPBIETABT    AUHEKTABY   FbEPABATIONS  ...    330 

AjfCHOTIES  ......   335 

Potted  Meats  akd  Fish  -  -  -  -  -  341 

MCBTABD  ......   344 

Pbpfek  -  -  -  -  -  -  356 

CATEmne  ......  368 

CoKBT  Powder  -  -  -  -  -  -  378 

Tubmbbio  -  -  -  -  -  -  387 


3U1  CONTKNT8. 

Page 
ViNEOAS  ......  390 

PiCKLBS  ......  405 

Oh  PoisoNOtTB  Bottled  Froits  ahd  Veqetables  -  -  409 

PB£8BRVB8  and  JbLLIES     .....   414 

Sauces  ......  419 

Spices  ......  422 

Isiholass  ...  ...  456 

Gbi^tike  .....  .  462 

Annatto  ......  465 

Cheese  .  .  .  .  .  -477 

Coloured  Sugab  Coneectiohert    ...  -  484 

Porter  _....-  499 

Alb      ....  ...  516 

GiH       -  .  .  -  -  -  -  524 

Rum     -  -  -  ...  .  .539 

Brandt  ......  540 

WiNB   -.--.-,  544 
Drugs  -  -  .....  5^9 

Tobacco  ....  -  -  556 

Skuff  ---.---  605 
Ofiux  .  .  .  .  -  -  .624 

scaxmont  ......  647 

Jalap  .......  656 

Ipecacuanha       ......  668 

coloctnth  .---..  675 

compouitd  scamhont  powder         ....  678 

Aromatic  Contection       .....  679 

Liquorice  ......  679 

List  op  Drugs   -  -  -  -  -  -691 

Concludino  Bekarks        .....  692 


LIST  OF  ENGRAVINGS. 


tber 
.  ami  13.    Sfvtifin  or  llfiroartvd  Cnflte  Brrrjr  -  « 

3.     Frajcmrat  of  Koutrd  Oiicrirf  Koot  ... 

St«rch  Grsaiilet  nf  Haranta  Arrowroot        ... 
Tbe  iane  of  Curruina  or  Fait  India  arrnwroot 
The  Hiao  of  Ttnuo  or  BrUUb  ArrowrooC 
L«aru  of  thr  Tn  Ptaut  .... 

Atum  Tartpljr  of  the  tnTno  .... 

Upptr  larface  of  L^af  of  Tea        .  -  -  - 

I'odcr  »urfftCf  of  Mire    .  -  -  -  . 

Upptr  fturfoce  of  CullT-develffip**!  1*'^  ... 

ftrudure  of  foreign  LeaffnuiMl  In  Lie  Te« 
The  Mine  of  another  foreipi  Leaf  found  la  Uc  Tr« 
Uppvr  and  Undnr  Surfaces  of  Leaf  of  Camellia  Soaanqua      *- 
'I'fie  umc  or  riuni  -  •  .  •  '. 

Leavet  o(  rhlor.iti>hii*  Inconipiciiui  and  C*an)eUU  SitMnqua  • 
Imitjultm  C'jinar,  Gunpowder,  or  Lie  Tea  .  -  • 

Leave*  of  Willow  nod  Poplar         .... 
Tbe  umeof  Pliuip  aitd  Oak  .  -  .  . 

The  ume  of  lUitthom,  Sloe  or  Wild  Pl.im,  Bewh,  KIdor,  and  Elm 
L*  Veno  Beno  ■..•-• 
Tbr  Oilopte  BoUnlcal  Powder      .... 
Porilon  of  the  liueatlnK  Meinbrtni!  of  the  CoRiK  Berry 
Fraftment  of  RoaiCed  Coffee  _  .  _  _ 

Structure  and  Ctiatactert  of  Geimlnn  Ground  Coffee  . 

B'uiMrd  fcroutid  Lupin  Seed,  called  Colllna 
Coffiy.  «iluUrr»t(xl  Willi  t'hicory     .... 
Celli  or  MufrttliJ-Wiirirl  Koot     -  .  .  - 

CmAW  adutirraled  with  Manfffjltl-Wuniel    .  .  • 

Tbe  aoini-  uiih  Chirory  and  Fliiatled  Wlirat 
The  tatae  witli  Chicorr  and  Roftited  Bean* 
The  tame  Willi  flririinil  Arum       *  .  .  . 


Fraffmrot  of  Hoattnl  Chicory  Root,  ahowlni  tU  CcHl 
Frafrmeiir  of  (he  ume,  •howltif  Ita  l>otted  Duct 


ltn;tlOn  of  Clurorjr  Kcxtt,  ihowltifi  the  Vaui  lactlcenMa 
Chicorr  adullcrued  wltn  Itoaited  Wheat  Farina 

Tbe  fiime  adiiltrrated  with  a  veg/Lable  Subataace  rviembUng  Groand  Acorn 
Structurrs  d«-tec:).'<(l  m  Oak  Bark  Povder    -  • 

Tan  known  u  Croiti       .  -  .  ■ 

Tubular  Fibrei  un  lurlace  of  Cocoa  Seed    - 

Th«>  two  outer  Tunics,  wfih  the  Muctlajtc-bearlne  Cetli  of  the  lluak  of  mom 
«1.    Cella,  Woody  Fltire,  and  Sftiral  Vpatela  nf  H<-cnnd  Membraiir  of  aame 

43.  1'Mit  Membrane  cuvcrlng  tbe  Surface  ai>d  hotet  of  the  Cocoa  Seed      - 
41     Cell*  which  form  the  kernel  of  the  Cocoa  Seed 
41.    Cenutce  Trinidad  Cocoa  ... 

46.  Unadulteraud  FUked  Cocoa 

47.  Soluble  Ctiroa,  iire(uireil  by  Steane.  Da«U,  artd  O.  • 

44.  Homieopalhic  Cocoa,  prepared  hf  Mr.  G.  B-  White 
49.  Bolable  CxKoa.  nrrpared  bf  i.  S,  Frr  and  S<ini 
to,  HnmtropAtbir  Cutfu.  firefuml  hy  Taylor,  Brother* 
ftl.  Uuiiu'i  GonuiDQ  Vnadulterated  Chocolate 
U.  I'rir>t4l*  of  C!ane  l^uitar  ... 
W.  A  FraKmvnt  of  Suiar  Cane  .  .  • 
&«.     Frafmrnta  of  the  sugar  Caue        ... 


PDIte 
and  I  IS 

-  47 

-  49 
49 
AO 

m 

C7 
71 

U 

n 

7« 
77 
78 

n 
n 
w 

vt 

m 


IIS 

114 
IIA 
lift 
IM 
VJ& 
\K 

\r 

i-a 

IM 
lU 
IM 
137 
141 
142 

la 

144 
139 
■•W 

161 

ir.8 
l«l 

Ift4 
16ft 
171 
174 
I7A 
1711 
177 
IM 
IM 
1*7 


XIT 


LIST  OF    ENGUAVINGb. 


N  amber 

bi.    A  Portion  of  the  Bpldnrmli  afthv  C4ne     ... 
M,     Ov«  and  Younjt  nftho  Acjinia  S.ir(^))&r(        .  .  _ 

07.    A  Sugar  liitcct  -  .  .  .  . 

M.    The  lame         ...... 

n.    Sporulei  of  the  Fnngvu  limnd  in  browTi  Sugar 

W.     A  Fragmfm  of  Woodj  Hbre  of  the  Fit       • 

01.     CrjttMU  o(  Hnxipy  •  -  .  .  . 

n.    HoMj  colliiclctl  princtpallf  From  a  H«aih  .  -  . 

63.  Boa«]t  aduUetdlvd  wltb  C«ne  Suyv  ... 

64.  Good  Mlik         ...... 

e\    Poor  Mllk- 

6A.    Cr«un  ...... 

67.    Curd  of  Milk     ...... 

M,    Coimtrum         ...... 

CB.     Common  HvdrnniHrr    ..... 

70.  The  Ontcsimal  Galartornvter       .  .  .  - 

71,  Lactomctpr  am)  Siitnd    •  •  •  .  . 

75.  The  l.»oi' »c<>iK!  .  -  -  .  . 

73.  Milk  iwiutt< TAird  wilh  Slu^'i  Braiiii  ... 

74.  Tmu  and  SifbaUnce  of  Seed  of  NVbntI       ... 

76.  8tfticturt-  and  Appearance  oflbe  Surcli  Graaulri  of  Wheat  Flour 
7R.    Tola  aod  Surtare  of  Seed  of  Barley  ... 

77.  Stnidura  nnd  Chimct^rt  of  Burlo;  Siuch 

78.  Structure  of  TMta  of  Hjre  .  .  -  _ 
70.    Structure  and  Characteri  of  tlie  Stare))  Grauulci  of  Rjre  Flour 
80.     TriU  uf  Oal      .--.._ 
Ml.    Struciure  and  Chamctpri  cf  the  Starch  Cnrpiitrlr*  uf  Oat  FInur 
^2.    The  lame  of  the  Siarrh  Oninul«of  Indlaa  Cvrn  Hour 

B3.    Traiurorie  8ecliuo  u[  Tetta  of  Indian  C'urn 

84.    Hu*k  of  Hire    ...... 

hi.    Surch  C^rpiiKrlPi  and  Crl]>of  Rire  ■  .  . 

n6.     SUrch  Oranulei  of  Raw  Wheat  Flour  -  -  . 

fl7.    Trantvertr  Scctinii  or  Krgot  of  Rye  ... 

89.     Spurn  of  I'rrdo  t^rict  .... 

Vd.    The  umo  of  L'redu  Srcplum        .... 

yO.    Wheat  FInur  infMtrd  wllli  Tuccliita  Cramitill 

91.    Fuctinla  Gramliiii  ..... 

M.    Fungus,  commoDly  found  in  iCnle  tMvad     ... 
9$.    Btiuctiite  i<f  the  Grain  of  LuUucb  TcmuleiituTu,  «r  Darnel 
94.     Kumcroui  Vibilorci  TrtUd         -  -  -  - 

9J(,    AcArut  KAriuiD,  or  Meal  Milo         .... 

9B.     Acjuiii  fioiii  Flour  ..... 

97,  The  Yewt  Funs""  -  .  -  .  - 

98,  Adulteraird  Coiiri  Flour  .... 
Sit.    QcAD  Flour         ■...-. 

100.  Wheat  Fluur,  adultemted  with  Beau  Flour 

101.  The  ftam«,  ndultera'ed  with  Rii-e  ... 
lOJl.    The  aat»«.  aduliarated  wiih  Indian  Cora  Flour 

103.  Wneat  Bread  adult»rat<>d  wilh  I'otato         ... 

104.  Structure  nf  Seed  of  Durra  .... 

105.  Lard,  adulteratKl  with  Potato  Starch  ... 
Oanoeal.  adullcrntrd  with  Uartry  Meal      -  .  . 
Starch  Graniilet  u(  KlArnnla  Arrowroot      -               -               . 
Canna,  or  Tout  Ira  Muu  Arrowfoot             ... 
Curcuma  Arrowroot        ..... 

Taoca  Arrowrout  ..... 

Potato  Armwroot  ---•-. 

Arum  Arrowroot  ..... 

Sajto  Surr^i       ...... 

Starch  iiranulei  of  Sfigo  -  .  -  . 


106. 
107. 
108. 

I«t. 

no. 
lu. 

112. 
IIS. 
J 14. 

ll». 

116. 
1)7. 
118. 
ltd. 
ISO. 

111. 

in.    Fracnrat  of  outer  mnr.bnine  ors««l  of  Wbitt  Muitard 


Factltiout  Safo  ...... 

SUrch  Graoulei  of  Minibot  llt(lli>ima.  or  Tapioca 

«Urch  Graoiile*  of  Tapioca,  altered  tiy  lb«  b«at  employed  tn  tu  (weparatloti 

Sample  of  Wtiarl'in'i  hrvtlrnta    •  .  .  _  . 

The  »ame  ol  L)u  Barry '»  Revalenta  Arabica  ... 

LMab'i  AJImenlary  Karhia,  ur  HomtBopathlc  Farlnactout  Food 

The  True  AochoTy 


■  IM) 
191 
IM 

-     194 

■  19.t 
300 

■  Wl 

ata 

917 

Sl» 

219 

.    220 

sal 

.    328 


2S6 
U4-2 

•ua 

344 

tih 
247 
244 
UAH 
SM 
Shi 

s&a 

SA4 
3U 
S»S 
861 
Ml 
36S 
364 
a6ft 
SOS 
967 


270 
271 
-JtU) 
a87 
288 
289 
'J90 

■j$i 

aoft 

311 

au 
ai6 

317 

ai8 

830 

asi 

325 

as6 

327 
338 
329 
.132 
.133 
334 
336 


LIST   OF  ENOUAVINGS. 


XV 


Number  Pic« 

1 9.    FrRgmeuto  of  middle  and  liinvr  tunln  of  Wbils  MiutATd  Si^l  .  .    sir 

Sftmpl«  of  (reniilne  Ground  Wblitt  Miutanl  ....    349 

llu«k  of  IllAck  Miiftt^nt  Sr«l  ......     849 

Samttle  of  "Double  i>u[>\'r{)ne  Miut^rd"-  ....    3^ 

MuiiatdadultvratNl  wttli  wbMt  flour,  tiiriniftlc,  and  CajeniM  •  -    391 

Hukkof  ClivlockSMd  ---....    it! 

The  tain*  of  Hup*  Sflad  --..-..    3(9 
The  tautr  uf  East  lodiui  lUpr  8e«d  reiriubUnr  ■  ipecin  ofMitttAnl    •  -    SM 

Tratuv«rtc  aod  Vvrllcal  ftccUooi  of  Huik  of  MiuUrd  S««d  tntit  witli  In  adutw. 
mlvd  r«M        ........    yn 

111.    SvciiMi  uf  repp«r  B^rrj-  •  •  •  •  .  -    UO 

ISS.     Portion  of  cortex  or  I'vppvr  &«rrr,  ttiowiag  the  »!!•  which  rorm  iu  flrit  and 

i0c><nd  Ujm  ...-.•..    3^0 
Furtlon  of  (uurth  Umlna  of  cortra  of  Pepper  Berry,  ihowiDC  .the  qU  contained 

In  ih«ca>lilc»  iifitir  crIU  ...*•.    3gt 

Section  of  rentral  ptjrtioo  of  Pepper  Berry,  ibowlQf  th«  two  klndi  of  cetlft,  and 
tu  JUQCtloD  »l(h  tne  corieK         ......    gg 

Ground  and  un«dulter«led  Ulacfc  Pepper    .....    jq 

Structure  of  Ltnoeed       --.....    ggg 

Epidennn  of  Captinim  ..-..-.    370 
Fracmcnt  of  KpidrrmU  uf  Cnpsicum  Berry,  rlewedoo  Ita  outer  lurCice  .    X7| 

The  iimv,  vlowed  on  it>  iniipr  •urbco         .....    373 

P^renchjr ni*  of  L'apiicuni  Berry  •  •  •  •  .  .     373 

TniiUTerfe  Hectioo  ol  Cap«icura  Iterrf       .....    374 

Verucal  !»«ctlon  of  SUmd  uf  CaMlcum  .....    37^ 

Cmjeiina  adulteralrd  wlUi  red  lead,  uround  rice,  and  tumeric  -  .    375 

Tran«Teri*  r'ectiuD  of  Mcricnrp  of  lorlantter  ....    379 

Outer  meiubruteand  TtaoirerM  Sdfkm  of  a  Cardaraom  Seed  -  .    ail 

1-17.    Trani>«r>e  SectlcA  of  9jcricar]t  at  Cumin  .  -  .  .  .    ^g 

IW.    Outer  Coat  or  1>tta  of  a  Fenugreek  Serd  .....    3^4 

rr«iu«ert«*  St-rtkio  of  L/itte  of  fenugreek  Seed         ....    33^, 

i»ectlon  o(  Tuber  of  rurntrric      .--...    ggg 
Ciriiutnc  Oiouiid  TurmCTic  •-..._    j|^ 

AcrliQer  Model  -----..    jt)) 

Uraiigv  Marntalod*,  adulterated  with  Apple  or  TUrolp  •  .  117 

flrru  Ibxit         •  -  -  -  -  •  -  -41ft 

A  pvrlinn  nfche  EptdencU  of  tlie  Rlilxotnp  of  Gloger  ...    ^^ 

Spvt^r^l  TUiur*  uli*rr«Ml  rntfff  ing  intu  the  foroiuiun  of  the  Gtn|er  IlhlKoiae, 

deprived  of  m  I-lpldcnitla  •.-...     |23 

fjenulnr  Grouml  (Jiri^fr  ......    |]g 

Howilerrd  (imger  ndultrniteil  with  SBf{0  Powdrr       •  -  .  .     43^ 

The  iiimt- nitiilct-nitM  with  Potato  and  Sbwo  SUrrliea  ...    ^^ 

The  (All  '  'I  with  (\iyttiic  and  Tapioca      -  -  .  .     ^^ 

Luiigltii  I  I  (:^nnamon  carried  Ir«ii»*er»ely  through  the  tmrk  .    431 

ti<m(iliii    I  .\»dtT  -  -  •  -  -  _    I3S 

ST- r*^     '  I   ■■  HuJ  ttkk  of  Ca*tU  of  the  fiAlural  kixe  andappftarauce  .    434 

I  <'(Jon  of  Cftiila      .... 

I  jxjndof  .... 

bt.  ;. .■..:i;]et  -  .  .  -  - 

Triim»fr»e  >«ctlon  of  Maoe  _  -  -  - 

Prtjd  uf  Clu«(^•bud  .  .  .  -  - 

Transierte  section  ■>[  Flower -Halk  of  tha  Clora 

IfongUiidinal  Sft-tion  of  Fliiufr>»lalk  (>rthe  Cluve   > 

Vertirai  St'Ciion  n(  Hu»k  of  Pmientu  L^rry 

I'xTrioi)  Di  t|j.<  Mi-_inlir«D««  on  .Siirf«:i!  n(  the  Seetl  Proper 

\  .  .11  ul  the  Seed  Proprr,  of  Ptmcolu  Derry 

I  ■<>,  or  Alliptce         .... 

«..  II      .  -I  >fivr       .  .  -  -  - 

S«^ti>>ni  of  hhrcd*  of  Ut-latlne  and  Iiinglast 

itvcuon  of  Send  01  Atinalt'»  .... 

Annattoadiillrrnt'^l  with  Turmeric  .  -  - 

Til  ,  '-       !     Kir  .... 

ji  'ii(<oMd  entirely  nfAcaruk  Slro  M  Omom  Mite 

^  liewi  of  Cheete  Mite 

I  i.ui  ajui  K'»"d«or Hop  ... 

I  u«  of  Leaf  of  Totucco  ... 

L^.-..i  ^iirbce  of  tainv    .  .  .  •  - 


in. 
in. 

I«6. 

117. 

\tn. 

1X1. 

lao. 

131. 


116. 

IM. 
137. 

im. 

IK>. 
140. 

HI. 
142. 
143. 
144. 
l*\ 


iKt. 

liQ. 
Iftl. 
Iftl. 

153. 
|IU. 
IM. 
IM. 

|A7. 
1^ 

1*1. 
)0<l. 

ir,i. 

IQS. 

1(3. 
IM. 
I(>V 
IWL 
HS7. 
)(M. 
It». 
170. 
171. 
I7i 
173. 
174. 
17*. 
I7& 
177. 

in. 

|k| 

I-  - 


^^^mtAT 


^^/OM 


Al 


^^Tn 


otfr 


^t'/i 


Gi-a/ 


suh 


OZ)t;, 


yeet 


or 


^-«ior'''^-»rC7^:'s-.^---^.r 


'*ft. 


aw 


0'/86 


cr/OA^. 


'-^^r:^?::-?Si?::; 


•"otAe, 


'^>Ve 


lot 


'•'«/»  „.::  "'•''■we. 


to 


'M 


In 


ters 


sfoi'dp..  -  ""  "o'  <v.-'":  *""■'/ 


"*'i."?:sr-.^ 


''•Ijj 


"Oil. 


or 


*"'^^, 


•'•«« 


^u 


•"^■^ene^^'^^or 


'«t4e 


^*'<«i 


arfo;. 


""^ijt. 


«er. 


'^'«-«^ 


OQ, 


tA 


i//tej, 


«a: 


<f/o, 


'"''*'^.„:"^""-":> 


^^'cA 


•^/br 


ttfl 


^•"^o,        I 


mn 


LIST  OF    ENOUAVINGS. 


Kutobvr  'l^ 

IB6.    Trantvarfc  SecUoo  of  Mid-rib  of  LMf  Of  Tobueo  ...    47$ 

m.    Portion  of  Tnin»»fne  S«TUan  uf  M14>ribaf  liMf  nf  Tobacco  -  -    W7 

lis.    Longitudinal  Srcllon  of  Nld-rlb  of  Luf  of  Tobacco .  -  .  -    B7S 

INB.    <;imulni'  Cut  TuImcco     ..-..--    VT9 

190.  Pivtlnncif  rndcr  KuKacs  of  thfl  l^Afrif  th«  Dock     .  .  -  .601 

191,  Trftnifn*'' tcctlonof  Mld-rfbof  L«af  of  Dnck  •  -  -  -  Ktt 
li».  I'ortiuii  of  Trmuvvrte  Section  of  M-d-ribof  Uaf  of  Dock  .  .  -  iOt 
190.  LongttiKlinal  M-rtiona(Mtd-ribof LeafofDock  •  -  •  •  8M 
194.    rortioii  of  I'lidiM*  Surrac*  of  Rhubarb  L#ar              ....    3M 

196.  TranivcrM  Section  of  MUl-rlb  of  IUiub4rb  I.«af  *  •  •  -  (W 
1<|6.     I'ortloa  of  U|ipt<r  Sur tnc?  of  Leaf  of  CoUsfool           -               -               •  .    A67 

197.  Poillon  of  t'lidrrStirf^ce  of  the  Mm«.  .....    9M 

IWi.    TraniTtT»«  SetUon  ol  one  o(  the  VVlni  of  L«if  of  Coltsfoot  -  -  -    M» 

lUO.     Tliv  wine  of  tbe  Exlorn-il  Sarf«c<«  of  the  Pof^pf  C«(>iula         -  -    Oft 

300.    Tlir  iMme  of  Inner  Surface  of  thr  Poppy  Cjq»u1p     .  .  *  ■    ^^6 

tOI.     PorUon  of  Surfac«  of  out  of  the  Piar«nla  or  DiM<T'lnt^t4  of  Porpjr  rapftiU      •    (17 
KH     Tfanivmc  Sortlun  through  tlir  Tlilckrir^ •  nf  a  DUappimrmt  of  Poppy  C«|ttuln  -     f^l^ 
SOB.     1'TaulTc^ft(^  Section  of  Uliseplmrot  of  Poppjr  Cap>ulc  -  -  -     VfJ 

tMt    Fragment  nf  Poppy  Swsd  ......    (00 

aOk     S4Up)(!  nf  Opium  aJ<ilU>rAt(Ml  with  Poppr  CApiule    •  •  •  .614 

30ft.    Th«  tame  AdultoraCMl  wttb  Poppy  CApinle  and  Whrnt  Flnur  •  •  •    M(k 

yi7.     Kityplinn  Oplntn.  iitliiltrrKtixl  vliti  fiiini,  Woody  Fibre,  and  Wheat  Flour  •    (M 

SOfL     Fureor  ViriEin  .Srammon)  In  Powdvr         ....  *    flill 

Ml.    Scammony.  largt'ly  adulimtod  vHu  WhMt  •  •  .  .    OAI 

StO*    Tniii*«rr»e  SMtlun  nl  Jal-<p  Tubrr,  diowlDitlhe  apr^^ranre  and  diilrib«(llon  Of 

the  dark,  and  probably  Ur«ln  CrlU  -  -  -  -  •    Oa? 

Sll.     Tbp  Miiio,  «lH><rlii«  th^  SlATch  t^-lla,  and  iiltn  the  Ili^in  CrIU  •  •     fiM 

319.    All  the  Struciiirri  and  tloincnt*  found  In  ti^nulne  powdered  JaUp      •  -    AS 

111.  Powd*red  Jalap,  Ijrgcly  Artiiltrrat^  uith  wudl  ....  CBT 
!I14<     Ipfcacuanha  Hoof,  tranavrrivc  Section  ofthf  Cortex  ...    &9 

IIA.    Tbe  utni>,  Aactlnni  of  tb«  rcntral  pait  or  Mc<lituUlum  -  .  .    670 

)i^     Oroutne  urounct  Ippou-uaiihA       -  .  •  •  •  -    fiTl 

317.    TnnavcfM  Section  of  Gourd  of  Colocjrnth  •  -  -  .671 

aia.    Portion  of  Surfacu  of  Gourd  ..-.-.    674 

))0.    KvcUon  of  Sc«d  of  Colircyntli        '-  -  -  •  •  •    0T4 

^10.    Rhubarb  ftdultetal«d  with  wlieat  flour        -  .  •  •  -    6T7 

ni.    Powdered  Squilli  adnltirnt'-ii  nith  wh«U  (lour  •  >  -  .    67t 

Tit.     TranaTrrii*  Mollcm  of  Koiit  of  Ll<)iioric«    ...  -  -    IM 

3X1.     LAnKUiMllna)  S*-i.-(ton  of  LiquorKc  Hoot    ,-  .  -  -  -    AM 

SM.     Irnntvrrtc  Srclioii  u(  I.Kiniirire  Ilntit  .  .  .  -  ■     1914 

2Xa.    Lti|tiortca  Powder  adulterated  wttli  iurni«rlci  ai^<l  Eut  tadlui  arrowroot  .    OW 


ADUl/i'ERATIONS   DETECTED, 


r;ENERAL  INTRODUCTION. 


I 


In  this  Introduction  the  subject  of  adulteration  will  be  considered  in 
some  of  iti  more  general  and  imporunt  iis{H?eL<i  and  rolations  :  thus, 
uniongsl  olbur  [)oints,  wbat  constitutes  uflulleration  will  1>e  defined,  ita 
prevalence  sbowu,  a  clatisitication  of  articlef*  employed  for  ndulterntion 
;j;iTCn,  the  importance  of  the  subject  explained,  and,  lutly,  the  means 
or  remedies  by  which  adulteration  may  be  discovered  and  obviated 
cODnidered. 

Definition  of  AduUeration. 

It  may  facilitate  the  clearer  understanding;  of  the  subject  to  define 
nt  the  outstitwhutconstitute^  adulteration;  but,  before  doing  so,  it  may 
btf  well  to  cJlplttin  what  is  not  Hdulteratitm.  This  is  the  inure  neces- 
sary, since  this  part  of  the  subject  is  involved  in  some  degree  of  un- 
certainty and  confusion. 

llie  sale  of  one  article  in  place  of  another  is  not  an  adulteration, 
but  a  substitution. 

Again  the  presence  of  substances  in  articles  in  consequence  of  im- 
purities contained  in  the  materials  out  of  which  they  were  prepared, 
,iu^  for  ejtample,  of  arsenic  in  the  liydrochloric  seid  used  in  the  prepa- 
ntion  oi  unfertnent«d  bread  does  not  constitute  adulteration  :  they 
ore  simply  impurities. 

I^asUy,  the  accidental  presence  of  subitancea  in  any  commodity  does 
not  constitute  adulteration. 

Excluding  then  from  the  class  of  adulterations  all  cases  of  tuBstitutiony 
of  impurities^  and  accidental  coritamiiuttiofu,  adulteration  may  be  thus 
di'fiiiud. 

it  consists  ia  the  intentloniil  addition  tu  an  article,  for  ptnposes  of 

n 


GENERAL   INTRODUCTION. 


gain  or  deception,  of  any  substAnpe  nr  .lubfltanccs  the  presence  of 
which  is  not  ao-knowleilged  in  ihv  nnme  umler  wliiclj  lite  article  is  t^old. 

It  ifl  not  easy  so  to  frame  n  definilion  as  tliot  it  sbdl  aiiply  to  every 
case:  that  now  given  ilcies,  Iiowtvcr, must  t-ertninly  embrai-c  tbe  grcjil 
majority  of  adultcratiDtia  practised,  and  it  excludes  subxtitutlons,  iiu- 
puritiea,  and  accidcntnl  i*nntaminations,  because  it  ppeciBes  tliat  the 
addition  niimt  be  iatentional, 

ALH:ording  to  tliia  definition  the  sale  of  cofTcc  containing  chicory 
for  and  as  coffee,  of  cocoa  into  which  sugfar  and  starcU  have  been 
purposely  introduced,  and  of  mustard  containing  flour  rmd  tumuTic, 
as  cocoa  and  mustard,  constitutes  bo  many  adulterations^  and  as  such 
they  oughr  undoubtedly  to  be  coniiidered. 

llie  consumer  entering  a  ftbnp,  and  unking  for  any  article,  has  a  right 
to  ex[)ect  that  he  will  be  .lupfdiod  with  that  which  he  demandn,  and 
for  which  he  pays,  and  be  ought  not  to  be  furnished  with  a  mixtureof 
iirtictcs  not  acknowlcdj^ed  in  the  name  under  whii-h  the  mixture  is 
sold,  and  the  nature  and  prnpfirtions  of  ihe  ingredients  entering  into 
which  arc  often  unkimwn  tn  him.  This  rlj/ht  undeniably  belongs  to 
the  purchaser,  and  any  wilful  violation  of  it  conRtituies  adulteration. 

The  words  coffee,  cocoa,  and  mustard  convey  distiuct  ide.is  :  these 
names  have  been  bestowed  upon  certain  vegetable  productions, —  coffee 
upon  the  berries  of  the  coffee  plant,  cocoa  and  mustiinl  upon  the  seeds 
bruised  and  reduceil  to  powder  of  tbe  cocoa  and  mustard  plants:  any 
application,  therefore,  of  these  words  to  mixtures  and  compnunib  is  oh- 
viuuply  improper,  and  in  many  coses  is  in  a  liigb  degree  deceptive. 

The  plea  that  the  addition  of  chicory  to  coffee,  of  flour  and  su^iar 
to  cocoa,  (if  turmeric  and  flour  to  mustard,  a.s  well  as  that  numerous 
other  additions,  constitute  improvementft,  ought  not  to  avail.  In 
nineteen  cases  out  of  twenty,  these  whlitions  are  no  improvements  at 
all ;  and  where  they  really  arc  so,  the  mixtures  ought  to  be  acknow- 
ledged, wherever  practicable,  in  the  names  under  which  «uch  mixed 
articles  are  sold  ;  and  not  only  ought  this  to  be  done,  but  the  propor- 
tions uf  the  several  ingredients  should  be  stated. 

Even  with  such  regulations  it  is  questionable  how  far  the  sale  of 
Euch  mixtures  ought  to  be  permitted,  except  in  cases  where  distinct 
advantages  can  be  shown  to  result  from  them,  because,  in  the  present 
Btat«  of  science,  it  is  fref[uently  impossible  to  determine  the  truth  or 
falsehood  of  any  statements  which  might  be  put  forth  respecting 
prcKKirtions  of  the  several  ingredients  contained  in  any  mixture. 


GENERAL  IJJTUODUCTION.  & 

Prervdence  of  Adnlteration, 

TTic  following  particulars  will  serve  to  convey  some  idea  of  the  great 
prevalence  of  ndulteration. 

During  the  course  of  the  last  six  years  the  author  has  examined  mi- 
nute]^ and  scrupulously,  microscopically  and  chemically,  over  3000  sam- 
pler uf  the  principal  articles  of  consumption,  oa  well  as  many  drugs ;  and 
lis  theonegreat  result  of  this  somewhat  extended  experience,  he  alTirraa 
that  some  inhorL  time  back  there  were  few  articles  of  cnnsumption  the 
odulterutiun  of  which  was  practicable,  and  which,  at  the  same  time, 
could  be  rendered  profitable,  which  were  not  extensively  subjected 
to  adulteration. 

True  it  is  that  adulteration  does  not  now  prevail  to  anything  like 
the  extent  it  did  when  his  investigations  first  coniuiented,  —  this 
highly  important  and  gratifying  result  being  attributable*,  in  the  first 
instance,  to  the  exposure?  of  adulteration  made  for  so  long  a  period  in 
"  The  Lancet,"  and  subsequently  in  tlie  evidence  given  before  the 
Select  Parliamentary  Committee  on  Adulteration. 

The  GTidence  of  ibe  cxtcaaivc  prevalence  of  adulteration  does  not, 
however,  rest  upon  the  testimony,  undeniable  as  that  evidence  has  l>cen 
shown  to  be,  of  a  single  inquirer  ;  but  many  scientific  observers  of  un- 
doubte<]  capabilities,  and  in  every  respect  trustworthy^  have  testified 
to  the  same  effect :  as  in  this  country,  Accum,  Allichcll,  Normandy, 
Gray,  O'Shaughnesay,  Pereira,  Thomson,  Wartngton,  Taylor,  Calvert, 
Quekett,  Bustick,  Gay,  Phillips  of  the  Kxcisc,  and  ntany  others ;  and 
nbroaii,  MM.  Garnicr  and  Harel,  and  M.  Cbevallier. 

The  numerous  witnesses  examined  before  the  Committee  on 
Adulteration,  with  one  or  two  unimportant  exceptions,  concur  in  their 
statements  respecting  the  gcncrnl  prevalence  of  adulteration.  Imleed, 
so  conclusive  is  the  evidence  deemed,  thai  the  Cnnimittcc  stale  that 
ibey  have  been  constrained  to  acknowledge,  as  shown  in  tbe  IVefaoe 
to  this  work,  that  tlie  statements  made  as  to  the  extensive  practice  to 
adulteration  have  been  fully  confirmed  by  the  in({uiry,  and  that  legis- 
lation hfta  been  rendered  imperative. 

Of  course  no  evidence  can  be  more  satisfactory  or  conclusive  than 
that  of  witnesses  who  speak  to  what  they  themselves  have  ascertained 
in  the  course  of  their  investigations:  there  is,  however,  evidence  of  the 
existence  of  adulteration  of  another  kind,  nnd  that  is  the  occasionid 
supply  of  ortidca  of  consumption  to  workhouses  and  other  public 

a  2 


i 


&EN'EltAL    INTRODUCTIOX. 

establialiracnls  under  market  price.  IVc  are  acquainteJ  witb  more  than 
*me  instance  of  tbw  kind,  especially  in  tlic  articles  arrowroot  and  oat- 
ineu! :  tlie  iliirLTuncc  in  price  being  ascertained  to  have  been  made  up 
hy  udultii^ration. 

Dr.  Noriimiidy  concludes  bis  evidence  l^eiore  tlie  Parliamentary 
Comuiittce  wiib  this  remark  :  — 

"  Adulteration  is  a  wide-spread  evil,  which  has  inrailcd  every  branch 
of  commerce  :  everything  which  can  be  mixed  or  uduUeruted  or  de- 
bosed  in  any  way  is  debased."  To  the  general  accuracy  of  this  decla- 
raiion  our  own  experience  compels  ub  to  subscribe. 

It  may  in  the  next  place  be  considereti  how  it  hupptnus  that  adultera- 
tion i$  tv  prevalent. 

Various  rco^onti  have  been  assigned  to  account  fur  this  prevalence: 
the  majority  of  these  have  been  gu^;^esLed  by  parties  more  or  le^s 
interested  iu  adulteration,  either  directly  (*r  indirectly  :  the  principal 
i.f  them  we  shall  proceed  to  notice,  and  first  tliose  reaaona,  or  rather 
excuses,  which  have  been  urged  in  defence  of  adulteration. 

Excuses  urged  in  Kztemtation  of  Adulteration, 

One  reason  ossified  in  defeuce  of  nmny  adulterutiona  is  that  they 
are  practised  in  ubcdieaee  to  the  wishes  and  tastes  of  thu  public. 

Another  rea«)n  is  that  the  additions  made  to  several  articles  con- 
stitute improvements. 

It  is  on  the  first  of  these  plea<4  that  the  practice  of  colouring  the  red 
sauces,  potted  meats,  and  fish  with  bole  armenian  ;  chee.se  with  annatto; 
])iokle&,  bottled  fruits,  and  vegetables,  with  copper;  and  sugar  con- 
fectionor)'  with  various  pi;;menls  consisting  of  suits  of  arsenic,  copper, 
zinc,  and  antimony,  is  excused. 

Kow,  aUh{]u;;h  it  may  be  true  that  the  public,  in  some  instances, 
prefer  the  more  highly  coloured  article,  yet  they  do  bo  tu  a  mere  ques- 
tion of  appearance,  and  in  total  ignorance  of  the  means  by  which  these 
colours  are  obtained:  these  means  explained,  and  the  jiublie  made 
aware  of  the  fact  that  ibey  are  produced  by  some  of  the  most 
]H)i8onous  substances  known,  it  is  not  correct  to  say  that  they  would 
knowingly  sanction  the  use  of  these  poisons,  and  would  prefer,  merely 
for  the  sake  of  colour,  articles  which  were  known  to  contain  injurious 
substances  to  those  which  are  pure  and  wholesome. 

It  is  on  the  second  of  thesie  pleas,  viz.,  that  the  additions  made  to 
several  articles  constitute  so  many  improvements,  that  the  addition  of 


GENERAL   INTRODDCTION. 


chicory  to  coffee  U  defended ;  wLeat-flour  and  tarmcrio  to  mustard ; 
Hupu"  and  starch  to  cocoa ;  sulphuric  acid  to  vinegar.  We  shall  have 
hereafter  to  speak  of  the  addition  of  chicory  to  cofTee,  and  of  sugar 
and  starch  to  cocoa  :  we  shall  show  ihat  it  is  very  questionable  whether 
chicory  U  an  improvement  to  cofl*ee,  and  whether  it  is  not  positively 
hurtful;  if  it  l>e  an  improvement, still  it  is  proper  that  each  of  the 
articles  called  chicory  and  cofTee  should  be  sold  by  itself,  and  usiid 
by  the  public  or  not  as  it  might  wish.  In  the  case  of  cocoa  it  will  be 
shown  that  the  au^r  ami  starch  are  employed  in  many  cases  Ut  such 
an  extent  that  the  compound  of  starch,  Bus?ar,  and  cocoa,  scarcely 
retains  the  flavour  or  smell  of  the  letter  substance,  while  its  colour 
is  so  altered  and  reduced,  that  it  becomes  necessary  to  hare  recourse 
to  coloured  earths  to  bring  it  up  to  its  proper  standard. 

The  manufacturer  telU  us  that  mustard  by  itself  is  so  disagree* 
able  that  we  could  not  eat  it,  and  hence  the  use  of  wheat-flour  and 
turmeric.  Uut  the  answer  to  this  st^itemcnt  is,  that  in  some  of  the 
so-called  mustards,  the  tunneric  and  wbeat-llour  are  so  out  of  pro- 
portion  that  the  compound  scarcely  retains  the  flavour  of  miutord. 
Again,  that  genuine  mustard  cannot  be  so  unpalatcahle  a  thing  is 
rikown  by  the  fact  that  there  are  now  a  few  mttnufacturers  who 
profess  to  sell  nothing  but  the  {renuine  article. 

Another  plea  urged  in  extenuation  of  certain  additions  is  that  they 
are  necessary  in  order  to  make  the  articles  keep.  It  was  on  this 
ground  that  the  legislature  was  brought  to  fianction  the  addition  of 
sulphuric  acid  to  vinegar ;  but  that  it  has  no  real  foundation  in 
this  case  is  proved  by  the  fact  that  there  are  now  manufacturers  con- 
ducting extensive  establishments  who  do  not  add  even  the  smallest 
proportion  of  sulphuric  acid  to  their  vinegar. 

Wlion,  therefore,  the  manufacturer  or  «;eller  defends  any  particular 
admixture,  or  adulteration,  on  any  of  the  pleas  referred  to,  namely, 
that  it  is  practised  to  suit  th«f  public  taste,  that  it  is  an  improvement, 
or  that  it  is  necessary  in  order  to  make  the  article  keep,  we  would 
advise  our  readers  to  look  well  into  the  matter  for  themselves;  they 
will  be  almost  sure  to  find  something  wrong,  some  fallacy  at  the 
bottom  of  these  statements, — they  will  too  often  find  that  this  pre- 
tended rq;ard  for  the  wishes  and  tastes  of  the  public  resolves  itself 
into  a  question  of  gain  to  the  manufacturer  or  trader. 

Another  plea  sometimes  urged  in  extenuation  of  adulteration,  ami 

perhaps  there  is  sometbing  in  it*  but  not  much,  is  that  it  is  impossible 

u  .1 


GENERAL   INTRODUCTIOK. 


to  supply  genuine  articles  at  tbc  prices  the  pabUc  is  wiiliug  to  ipikj 
for  tbem. 

No  doubt  tUe  public  likes  to  obtain  wbat  It  requires  at  as  cbeap  a 
rate  as  pott^iblc, — but  it  is  for  the  trailer  to  fix  llic  prices  at  which 
he  can  afford  to  »ct[  his  goods,  and  not  the  public :  further,  if  it  ivere 
explained  to  tl^e  public  hj  the  dealer  thut  he  i>r)uld  not  answer  for  the 
quality  or  puriiy  of  the  very  cheap  articles  sold,  there  are,  we  believe, 
very  few  persons  who  would  be  so  silly  as  to  prefer  the  adulterated 
to  the  genuine  article,  although  the  former  might  be  apparently 
the  cheaper. 

We  say  apparently  cheaper^  because  in  many  cases  these  so-called 
cheap  articles  tire  really  the  dearest  In  the  end,  for,  owin^  to  the  extent 
it}  which  they  are  adulterated,  (hoy  do  not  go  nearly  so  far  as  j^enuine 
nrtielra  would  do.  The  public,  then,  we  ctmsider  u  but  little  at  fnult : 
it  merely  requires  to  be  made  acquainted  with  the  true  and  actual  state 
of  thinfFS,  and  there  is  no  doubt  but  that  in  ninety-nine  out  of  every 
hundred  case*  it  wduld  prefer  the  genuine  to  the  adulleratcfl  com- 
uuxlity,  even  allhou;.'!)  for  this  a  somewhat  higher  price  had  to  be  paid. 

A  further  excuse  sometimes  urged  in  defence  of  certain  adultera> 
lions  is,  that  they  do  no  harm,  fiy  this  plea  wo  suppose  is  meunt, 
lliftt  they  are  not  hurtful  to  the  health,  but  only  to  the  pocket  On 
this  ground  the  adulteration  of  milk  with  water  is  sometimes  de- 
fended :  now  we  are  of  opinion  tliat  there  are  few  more  scandalous 
and  indirectly  injurious  adulterations  than  tliis.  Milk  is  an  important 
and  prime  article  of  diet,  full  of  ^ou^i^hraent,  and  in  proportion  as 
water  is  added,  so  urc  those  who  partake  of  the  diluted  compound 
robbed  of  their  proper  nourishment. 

Such  arc  some  of  the  excuses  employed  in  defence  of  odulterntinn. 
That  they  should  be  urged  by  certain  manufacturers  and  traders, 
whose  profits  in  some  cases  are  so  largely  dependent  upon  adulteration, 
is  not  so  surprising :  but  whiit  really  is  astonishing  Is,  that  there  should 
be  found  some  few  men,  very  few  we  arc  hiij>py  to  state,  of  mi»re 
or  less  scientific  repute,  who,  influenced  by  certain  considerations  of 
interest,  lend  the  weight  of  their  names  and  use  (heir  ycientific  attain- 
ments in  defence  of  adulteration, 

Science  is  never  so  ri<;htly  or  so  nobly  employei:!  as  when  tt  ministers 
to  the  wants  and  welUticing  of  mankind,  and  especially  when  it  is 
nsed  for  the  protection  of  the  public  health.  On  the  other  hand,  is 
it  not  an  unworthy  and  an  ignoble  use  to  make  of  sciencv,  to  employ 


GKNEKAI.    INTKODUCTlOJf, 


^ 


it  in  defence  of  practices  whtcli  i*vcn  those  wbo  defend  Uietii  moat  in 
ihcir  own  consciences  must  comJema? — and  ytt  there  ore  men  who 
thus  deiotian  liieinsolves. 

That  it  would  be*  right  to  make  public  the  names  of  those  who  thus 
disgrace  themselves,  to  refute  their  argunientA  and  reasonings,  &ud 
CO  expose  the  motives  in  which  tbeir  conduct  originat4;8,  few  will 
deny :  we  fccl^  however,  that  this  is  »cnrce1_v  a  fitting^  place  so  to  do, 
and  shall  therefore  rcfruin  from  pursuing  this  course  :  wc  shall  merely 
refer,  in  a  general  way,  and  as  briefly  :is  possible,  to  the  kind  of  ar- 
guments reported  to  by  the  per:tons  to  wliam  we  liave  alluded.  Of 
course  they  employ  the  tlilTerent  reasons,  or  rather  picas,  to  which 
we  have  referred,  anfl  the  fallacy  of  muBt  of  which  we  have  exposed; 
but  in  addition  to  which  they  resort  to  other  proceedings. 

Thus  ihcy  endeavour,  if  possible,  to  get  up  a  cry  of  exajfperation, 
this  in  the  face  of  evidence  of  ihe  most  conclusive  and  demon- 
strative character. 

Another  course  pursued  ia  t^)  cite  some  of  the  leds  important  in- 
stances of  adultcnttion,  as,  for  example,  the  addition  of  alum  to  bread, 
of  water  to  gin,  and  to  argue  from  them  as  though  they  were  not, 
oa  they  really  are,  parts  uf  a  system,  but  as  though  they  were  the  worst 
imtanoes  of  adulteration,  and  as  though  the  entire  case  rt^'sted  upon  them. 

Another  favourite  plea  used  in  extenuation  of  adultcratiun  is 
that  the  quantilicii  in  which  souie  of  the  substances  arc  employed,  as 
those  used  for  the  sake  of  colour,  nre  too  inconsidenible  to  be  pro- 
ductive of  hurtful  results. 

This  is  so  sometimes,  but  it  ceiHaiuly  is  not  the  case  in  the  ma- 
jority of  instances:  in  many  coses  injurious  consequences  have  been 
a«Ttually  proved  to  euitue:  thus  mai^y  persons  have  been  poisoned 
outright,  nnri  have  lost  their  lives,  from  the  use  of  r(dnure<l  sugar 
confectionary;  others  have  been  rendered  seriously  ill.  Cases  of 
lead  paralysis  hove  been  produced  by  the  lead  pur^MWidy  introduced 
into  snuff,  and  the  same,  it  has  been  asserted,  has  occurred  from  the 
uite  of  cayenne  coloured  or  adulterated  wiili  red  lead.  A)in.\u, 
illness  of  a  senous,  and  even  fatal,  character  bos  been  produce<l  by 
the  use  of  poisonous  adulterants  not  pijrments,  as  from  lend  in  wine, 
ci*ccu1us  indicus  in  beer  and  spirits.  ]ndce<l,  instances  might  be  mul- 
tiplied to  a  large  extent  of  disease  ori;:inating  in  the  use  of  substances 
rmployed  for  adulteration.  WTio  can  tell  how  many  invalid.^  and  tender 
rhildren  have  fallen  victims  to  the  dangerous  adulterations  practised 

n  A 


%  GENERAL   INTBODUCTIOK. 

Upon  fxHid,  drinka  and  drugs,  if  the  true  causes  nf  premature  death 
could  be  traced  out  in  all  sucli  cases?  That-  dyapeplie  ailments  often 
owe  tbeir  origin  to  the  acliiUerfttionof  nrticles  ol"  (bod  is  unquestionable. 

Besides,  if  the  etni^loynient  of  jKiifuinons  pigments  and  oilier 
substances  arc  to  be  penuitted  at  all,  what  guarnntee  or  security  have 
we  against  accidents  resulting  from  the  careless  and  ignorant  use  of 
such  poisonous  or  injurious  articles  ?  Theonly  right  and  narc  principle 
upon  which  to  act  we  maintain  is  to  discard  the  use  of  all  additions 
to  articles  of  consumption  that  are  unnecit'iisary,  and  which  may 
|»os8ibly  become  a  source  of  danger.  Again,  it  must  l)c  remembered 
that  the  ill  eiTects  of  adulteration  cannot  be  estimated  by  the  quantity 
of  any  particular  ingredient  contained  in  any  one  article  ;  so  prevalent 
is  adulteration,  that  in  the  course  of  a  singli;  day  it  often  happens 
that  several  injurious  ingredients  are  partaken  of,  and  in  onler  to 
arrive  at  any  correct  conclusion  wo  um:?t  therefore  take  the  sum 
of  the  whole  of  these  injjredients.     See  p.  21. 

Lastly,  in  endeavouring  to  estimate  the  eOects  of  odalteration  on 
health,  the  fact  must  bu  borne  in  mind  that  some  of  the  metallio 
poisons  used  are  what  are  called  cumulatire.     See  p.  20. 

)Ve  have  been  induced  to  enter  into  an  examinution  of  the  various 
pleas  on  which  tlie  practice  of  adultvriition  is  wuK'times  defended,  in 
Tjrder  that  when  the  readers  of  this  work  hear  theui  urged,  as  some 
ot'  them  doubtless  will,  they  nuy  know  wliat  they  are  really  worth, 
and  how  they  may  be  refuted. 

Having  noticed  ihe  various  pleas  on  which  adulteration  is  defended, 
we  have  still  to  consider  to  what  cause  or  causes  ita  prevalence  is  due. 


Seal  Catue*  of  Oa  Prevalence  of  Adulteration. 
The  great  cause  which  accounts  for  the  larger  part  of  the  adul 
tcration  which  prevaiU  is  the  desire  of  increased  profit;  a  second 
cause  is  excessive  and  unfair  competition.  A  trader,  perceiving  that 
his  neighbour  in  the  same  bu.*iines»  is  selling  his  gt>odB  at  prices  at  which, 
if  genuine,  it  would  be  impossible  to  realise  a  proGt,  knov^s  that  this 
can  only  be  done  by  having  recourse  to  adulteration,  and  finding  that  he 
cannotcompetewith  his  unscrupulous  fellow  truiler,  at  longthhe  himself 
too  ol\en  has  recourse  to  the  same  practice.  We  thus  perceive  how 
dilUcult  it  is  fur  many  tradesmen  who  desire  to  do  so  to  conduct  their 
bosinetaet  in  a  honourable  way,  and  to  resist  the  temptation  to  adul- 


GENERAL    INTRODUCTION.  9 

terat«.     The  main  cau»>s  of  the  prevalence  of  adulteration  are,  then, 
the  dctire  of  increased  profit  and  cxccsmvc  and  unfair  competition. 


Who  are  the  Parties  guilty  of  Adulteration  f 

The  next  question  for  wmsideration  is,  who  are  the  parties  guilty  of 
»lultcrAtion. 

The  answer  is,  in  some  cases,  the  manufacturers,  and  in  others  the 
retail  dealers.  This  dislinelion  is  of  the  utmo:it  importance,  especially 
with  reference  to  the  means  to  be  adopted  for  the  discOTcry  and  sup- 
pression of  adulteration. 

Some  of  the  adulterations  practised  require  to  be  so  on  the  large 
scale,  and  involve  the  use  of  extensive  machinery,  which  the  trades* 
man  does  not  possess  ;  and  in  consequence  certain  adulterations,  aa  of 
.  dour,  of  chicory,  of  cocoa,  ot'nipices,  and  of  many  ilrugn,  are  practised  by 
the  grinderti  and  roasters  of  those  articles :  there  it«  a  claits  of  persona 
known  OB  Sptce  and  Dru>;  Grinders,  with  whom  lies  much  of  the  fault 
of  the  adulteration  of  spices  and  drugs. 

in  the  drug  trwle  the  practice  at  one  time  was  very  general,  and 
<t  still  prevails  to  some  extent,  of  adding  sawdust  of  <Iidcrent  kinds,  as 
well  aa  other  articles,  in  order,  it  wa<4  urged  in  excuse,  to  make  up  for 
the  varying  and  avcrai^e  Iub»  sustained  by  diflerent  drugs  in  the 
cour*e  of  drying  and  grinding  to  a  uniform  toss  of  4  per  cent.  This 
is  called  the  4  per  cent,  sytitcm ;  however,  the  practice  does  not  stop 
here,  but  Iead.i  to  every  species  and  degree  of  abuiie. 

The  adulterations  of  mustard,  vinegar,  annatto,  snufT,  coloured 
sugar  confectionary,  and  some  other  articles,  ore  also  usually  prac- 
tised by  the  manufacturers. 

There  are  good  reasons  why,  in  many  caws,  the  manufacturer  should 
be  the  adulterator;  not  only  has  he  the  necessary  machinery  and  the 
means  of  performing  the  requlsjite  operations  iyn  a  large  scale,  but  the 
responsibility  of  adulteration  is  thus  taken  ofi'thc  shoulders  of  the  tens 
of  thousands  of  traders  by  whom  the  public  is  immediately  supplie<l, 
and  is  confined  in  s<mie  degree  to  the  comparatively  small  body 
of  manufacturers,  whose  proceedings  are  coiulucted  in  rL-tiremcnt  and 
•ecrecy,  and  whose  premises  are  not  accessible  to  the  public. 

The  retail  trader,  however,  takes  in  many  coses  his  share  in  the 
•work  of  adulteration ;  as  one  example,  we  may  mention  that  much 
of  the  adulteration  of  beer  and  spirits  is  perpetrated  by  the  pub- 
lican.    Kven  in  those  cases  in  which  the  retailer  does  not  himself 


10 


GENERAL   INTRODUCTION, 


adulterate,  be  often  purchases  of  nduUcruting  mcrclinnts  with  gtiiltj 
knowledge  ;  thus,  in  many  cascs^  he  is  swareof  the  fact  that  the  article 
he  purchases  is  adulterated,  from  the  price  paid  for  it  being  less  than 
that  at  which  the  genuine  article  can  be  procured.  In  such  eases 
the  tradesman  i^  a  party  to  the  fraud,  aud  is  as  guilty  as  the  actual 
perpetrator  of  the  adulteration. 

It  should  be  known  thtUcvcn  the  purchnsin^^of  articles  of  consump- 
tion in  the  raw  state  b^  the  trader  nffurds  no  guarantee  for  the  genu* 
ineness  of  those  articles,  provided  they  are  afterwards  sent  to  the 
grinder  or  manufacturer  to  be  ground  or  manufactured.  We  have 
known  tradeHuitfu  who,  witihing  to  pretext  themselves  as  fur  as  possible 
against  adulteration,  have  purchased  the  best  cocoa  beans  and  chicory 
nibs,  and  have  then  sent  them  to  the  grinder  to  be  prepared,  bui^ 
upon  being  returned  to  them,  tliey  were  found  to  be  adulterated. 
Messrs.  Ridgwuy  and  Co.,  of  Kin;;  William  Street,  forwarded  to  the 
author,  some  time  §ince,  some  fliike  fot-oa  for  oxaminntion  :  tins  was 
found  to  be  adulteruteil  with  wbefll-flour.  Measrs.  Rid^'way  then 
stated  that  tliey  purohnxed  the  best  cocoa  beans  they  could  procure, 
and  sent  them  tn  the  munnfacturer  to  be  nude  \nto  Jiitke  cot*oa,  which 
should  consist  of  nothing  but  cocoa.  The  miuiufacturer,  in  this  case, 
had  subtracted  some  of  the  cocoa,  and  had  replaced  it  with  wheat- 
flour.  Since  this  occurred  Messrs.  Uidgway  have  had  a  mill  erected 
on  their  premises,  and  now  make  tlieir  own  flake  cocoa. 

Now  it  must  031  be  inferred  from  these  remarks,  that  there  are 
not  many  honest  maiiufacLurcrs  and  traders  connected  with  the  manu- 
facture and  sale  of  articles  of  consumption.  We  ktiow  that  there  nre 
many  such,  and  on  In-half  of  some  of  those  who  either  lire  really 
(:nilty  of^  or  who  lend  themselves  to  adulteration,  the  uxcusi^h  may  be 
urged  that  utitil  very  rwently  the  legislature  has  been  indiflerent  to 
this  subject,  that  it  dm*!*  not  protect  t)ie  honest  trader,  and  (bat  in 
self-defence,  and  for  very  livelIh(K)d*8  sake,  be  is  often  driven  to 
adutternle. 

CLASSiriCATIOK   OF   AdULTBKATIOX. 

Not  only  is  adulteration  prevulent,  but  the  substances  employed  are 
very  nnmerous;  different  kinds  of  substances  being  used  for  diflerent 
purposes.  The  majority  of  substances  used  are  so  for  one  of  three 
purposes:  either  for  the  sake  of  hulk  or  weight,  the  articles  used  of 
coarse  being  cheaper  than  tbusc  to  which  they  are  added ;  for  the  sake 


QENEEAL   INTRODUCTION. 


11 


oCcohur,  that  is,  to  heighten  and  imprtive  the  appearance  of  articles  &s 
it  is  consi<iere<I,  often  erroneously,  the  natural  colour  of  such  artinlcs 
bv'ing  frequently  altered  and  reduced  by  dilution  with  other  uUultcr- 
itiag  substances  added  for  bulk  and  weight ;  or,  lastly,  to  increase  the 

agency  of  articles,  and  to  heighten  their  ^ro^rftw  and^immr. 

The  first  kind  of  adulteration  is  the  more  usual  fDrni,  und  is  that 
hy  which  the  practice  is  rendered  so  prufiiabte  ;  the  second,  that  which 
consists  in  the  addition  of  colouring  matters  of  various  kinds,  is  often 
necessitated  by  the  first  kind,  so  that  these  two  descriptions  of  adul- 
teration frcfiuontly  go  logetber. 

An  example  of  the  first  kind  uf  adulteration  is  furni&hed  by  the 
addition  of  roosted  corn  to  chicory  or  coffee  jKjwdens  and  of  water  to 
milk. 

Of  the  second,  in  the  addition  of  red  lead  t<>  cayenne,  Venetian  red, 
umber,  &c.,  to  chicory  and  cocoa;  while  an  example  of  tlie  third  form 
of  adulteration  is  met  with  in  tlie  addition  of  nlkalicji,  as  nl^o  the 
chromnles  of  |)otash,  hellobure.  uud  powdered  glass  to  snulf. 

Now  it  is  in  the  second  class,  viz.,  that  whiuti  consi^la  in  the  em- 
ployment iii  colouring  mattersi  of  various  kinds,  that  the  mdjority  of 
tho«ic  adulterations  are  included  which  are  prejudicial  to  health  :  this 
will  be  8*?en  more  clearly  hereafter. 

So  numerous  and  various  arc  the  substances  employed  for  adultera- 
tion that  a  classification  of  them  according  to  the  articles  in  which 
tbey  are  encountered,  an<l  the  purposes  to  which  they  are ajiplied,  be- 
comes uaeful.     Such  a  i-liusifi cation  is  j;!;iven  in  the  fidlowing  tables. 

The  annexed  Table  contains  only  the  names  of  thoso  substances 
which  we  have  ourselves  ascertained,  by  original  ub$er>-ati(tns  and 
Analyses,  to  be  actually  employed  for  the  adulteration  of  Articles  of 
Food;  it  does  not  include  Drugs. 


Clauijied  List  of  the  varimu  Suhstancea  ascertained  hy  Ourtelres  to  be 
employed  for  the  differeut  Purpo»rs  nf  Adulteration  :  eix.  /or  Sulk 
ami  Weight,  for  Colour^  atulfor  Smelly  7'aste^  and  other  Prpperliea. 


Amiuttd. 

VM  BMlk  and  WetRbt. 

rvCrfnv. 

Rt«.    WhPikt     anil     Bnrley 
Floart,  Tumicrlc.  C«rbo- 

nau    and    Sulphate    uf 
LlilM^    Had    fornigiiiout 

Tumwrie,  Red  fernjirf- 
nou«      Karlht,     SoJL 
Allull. 

Sutphatc  of  Cop- 
per. 

^v 

C^^^^^l 

^H 

•       GENEEAL   INTEODUCTION. 

^^ 

PvTmc.  Knitll, 

1 

r«  Bulk  and  wcgmt. 

For  Cotmir. 

m4«tkrrVto. 

Aknow-Root  . 

l«m*«. 

Srito,  Potato,  nnd  Tuploai 

Srjucbet,     and     vHrt<iu« 

niixrum   and    comhiriA- 

Elciii*  of  t\\r*t  with  the  lii- 

Fi^rtor  Arroik-ri-nU. 

ANOMVItt 

Dutch,  Freurh.and  Slelllaii 

Bole  Armpnton,   Wnc- 
tloJi  Kfd. 

IM*miT  - 

Wabpr          .        -        -        - 

Burnt  Snjtar. 

Mmhrtl      Potnlix^,      nice, 

- 

A(unn.  Hardiftivd 

Hun*,        fijrr,        Iiidiin 
Corn 
W«er. 

Stuff. 

Bvmmrmvm 

SaUa  of  CV>pppr,uiiiAll:r 

Salt. 

AKD    ThiTA- 

[h»    Acetate   or  Sul- 

BUtt. 

phate. 

Cn»iii      . 

-          -          -           - 

A'tnatto,    Bole    Armr- 
olan.  Vcuvtian  H«d. 

ClNKAHnN 

CftMlii.  ami  moit  orUie  ar- 
iicl0«    m»n(lone«l  under 

Sptcri. 

But      tndu      Arrow-mot, 

CoehlDPAl.  Lik»,  Tndl- 

rftCnOHABY. 

WbMl  WKl  Potato  Fl«MJr, 
Hjilrftted      Sulfihate    of 

LtlDt. 

)(■>,     Pimi«Imix     Hliif, 

Antwerp   Blttu.  Artl. 

flclfll        rii;r.imjiriiir, 

C«rli<>n>Tp  oi  Cii^ijifT 

or    Vi-rditrr,   ('srbo- 

natpof  LiaitorWhliP 
Lead,  It.HlUad.Vrr 
millon  .Chroinp  Yel- 
low or  Cbrnin'itp*  of 
LcHd.I.fmoii.DranMC' 
anil  lit'ep;  (iamliDxtr; 
Xap  CirHciniJm  th?ief 

BrunRwkk,      Crpen*, 

Eintrrald      flrern    i>r 

Arvpnlf*    iif    4;of»ppr, 

Indian     R«^;    bri>Hn 
rernminrMi*     farrhs, 
cblvllj  l^mbor,  jlleii- 
na,      and       Vniidykp 
Brawn,  and  v«ri(>iii 
cnmblnatiiui*    ■)(   the 
abovt'  pigmenlM. 

Comx     . 

Chicory.    Rout»d    Wheal. 
Ity4>  and     I'oiata  Floiirft, 

wiinel,  Aninii 

Burnt  Suanr,  or  Blaclt 
Jark. 

CiiieoiT  - 

Riwtnl    WhMt    and    Kfe 
Flmira,  Burnl  Boaitt  ami 
Ai-urna,  ttewduit,  M«h(v< 
g*)'Y      ^awiliut.    Carrot 
Al4iiKi*l.wurs«). 

Frrnigliioui  rnrThi,  nit 
X'cnt'llMii       Ued    and 
Vmi^fi,  Burnt  Sugar 
or  Black  Jack. 

t 

COOttAANOCHO- 

Maraiil«,    Kott   IndU,  and 

VfiiPtian      Bed,      Red 

COL41B. 

Taroi  orTaittti    Arrow- 
moU  ;Ti>u»  Wt  Mda;  Iha 
Flourt  of   WliMt,  IndUn 
Com.  S«go,   PnUtn.   Jiml 
TAnioca,arulTar|t>u*Mi\- 
tiirci    of    thfw:     SuKd'', 
Ciiilcunr,  Ccx'cia  Htuki. 
Ground  nice.  Muitardliiuk, 

Oclirp.  and  ullwr  f»"r- 
ruglnou*  carthi. 

Catimni     Tbp- 

nv6  I>«d.    VmnlKriQ 

mu 

tUlL. 

or     RUulpfvtirpt     nt 
Mercury.      Venelian 
Red.  Tumaark. 

^^^^^^^^^^^^^^^^^^^^^^B 

~^^M 

^^^^^                       OENER^VL   INTRODUCTION.                                              ^^H 

F«r  Tarta,  fn»itt 

CotTAKn       *»n 

rwBalkMMlWrfffal. 

rorCalMU. 

•ailMhnrn.- 

WVirar,  Poraln,   aod    Rice 

Ohrofn^      Yellow       or 

EOO  PoWtlMD 

Flour*. 

Chromate    of    Lead, 

Turmeric, 

CUIKT    rOWDU 

Cmuod  Uice,  PoUlD-fariEia. 
Sail. 

Ked  iMd 

Salt. 

Flovk 

Hlcf,  Bf-ani,   Rrv.    Iiiiliui- 
Coro.  Pouto  VVur.           i 

-          «           -          . 

Alum. 

GlMOM      - 

Whnut,    Sua,   iDd    PnUto ! 
Flours,      around     Ulce, 
MuMard  HtuU. 

Turmeric  Povdvr. 

flin   .       •       . 

W»ler,  Sugar    -        -        • 

Cayenne,   Taula 
nr       Cinnamon, 
Su(n»r.  and    fla- 
vourlufurdlFRr- 
eot  hlndi.     hor 
fining.        Alum, 
B«lt  of  Tartar. 

HOMIY 

Flour,  C«iiP  Sugar. 

|MX<1L4U  • 

GcUUne. 

L««*        -       . 

Pouto-flour,  Waier 

•          •          "          • 

Salt.Carbonntfl  of 
Soda.     Caustic 
Line. 

LiQunict 

Whral-anur.l'otxto  SUrrti. 
tiDiM    Starrh     pnihnl.t) 
'  Rk*r .Chalk,  uml  GcHutiv. 

MUlTjIlltl   - 

WI>CAi<flour,  Turnif>rlc 

Tunnerk. 

MtLK            ■         - 

W«CT 

Annalto. 

MUL«AL4D>         - 

Pulp  of  Apple  tir  Titr  nl  p. 
Barlpj'Bour,   ajid  ili*  Inir- 

'  Oatmui  - 

gummu  of  Bulrr  cAlled 
Hubble. 

ruHBK           AND 

Water 

Sujtw,  Trrula  ■ 

Sugar,    TrMcle, 

Stoi'T. 

bait. 

1 

PicftLa    • 

-         -         -         - 

Salt*  o' Copper.  UAU ally 
(he  Arcutv  of  Copper. 

1 

PorT«o    MUT« 

Flour,     iirobjU>lr    VlTiMt- 

Duir     ArtneuUii.     ami 

4«ii»  Kim. 

flnur  boiled. 

•  'tnetliuei    VonutUu 

r 

Puntivui 

Salit  of  Cu|ffi«r,  Including 
the  Acetate. 

Hed. 

rtrrcB      . 

Wbeit    afttl     Pm    Flour, 
OriMind      Hire,     C.touml 
MutUril  Seedt,    LlnHvU 
Me«I.   P.  l>..or   Peppcr- 
D.ut. 

&400          -        - 

Pouio-flour. 

S»nrr 

Th?  CbroniAlet  of  Po- 
luh,    C'ltrocniite     of 
I**d.         fetruginou* 
Cdrtba,    ehiclly     litn- 
l>erf,  Ked  and  Yellow 
OCbre.  Ked  Lead,  or 
Oxide  of  LMd. 

The     Chrnmatet 
of  Potash,  Car. 
boiule   of  Am- 
monia.      Ltme. 
Pondered  Glass 
or    Sile«,  Pnw. 
deredOrrli-root. 

BlM           -        . 

Water 

-           -          -          . 

Carrnne,    Burnt 
Sugar. 

KtOAB 

Wheal-flnur  lo    two    CUM 

only,    Poiato-flour.    and 

Tai'iocA-tUrcli,  each   in 
"  oQtfumplr. 

" 

ftnetm : 

CuiYU  -       - 

PDwAiDNl    CloTe-«Ullu    In 

1 

Ct%HAUoii     - 

CoMU,  WbcAt-dnur.  Sago- 
mtoi,    wild    minture*    of 
(hr»e  :  KaK  India  Arrow- 
root. Poialo-Aour. 

. 

16 


OENEKAl,   IN  TKODUCTION. 


List  of  Articles  utttted  hy  Oikerx  to  hf  employed  fitr  the  different 
Piir/Hfitea  of  Adulterutum^  but  of  the  Use  of  which  iio  Pogitive 
Erideme  hoA  been  adduced^  idthough  it  i>  extremely  pj-i)Lable  that 
many  of  them  haoe  beeny  or  are  occasinRnllyy  had  recourse  to. 


For  Taiite.  Smelk 

FoBuUtmiWactii. 

F«  Colwif. 

ud  oLlwr  Pn^ 

Aebow-Root    . 

pmin. 

Ground  Rlc«. 

ANCHOnSS 

Hrrats. 

Bmuu 

Burlpy,    Onl.      Pf*    Flmir, 
IMt.e     Cfliiy,    Pl*»t«r    of 

CoLOHBRD  Con. 

WbltP    Potti-r'i  rlay.    Pi[n- 

Ciihall,   Smilt,  UHr«. 

rMrrio))A.ay. 

Cliijr.    or    Cornith   <Uy  ; 

mariiif,  Litmua,  (■*«• 

Ch^lk.  Flmtt-f  or    Parli. 

pies  Yellcm. 

S«rd 

Corrii     -      - 

Ri>Ait<H)        P«M,       Co(fce 
Grtiuodi,  Parmiv- 

ladder  Rwt. 

CmooRY    - 

Torreli«d      Gnmnd     Rier, 

B«k«^   HorM-i    Lirer, 

Roftited  BiH-ult.  Oak  Hnrk 

Durai  Blood. 

1'an.     EKiiAiutod.    T«o, 

called  Crmui. 

Cocoa  akd  Cbo- 

OH    ScR    HlKMilB,     Co«r*r 

R«<)  r.«Rd,  Vermllloii, 

COLATR- 

BrAnnvFlour.AnimAlKoti, 

KMf       RDd      Yvticiw 

Rt  TaIIow.  Ijird,  Tri-arlP, 

Ochre. 

Siilphatrof  t.lmc,  Thalk. 

Flove 

L"h*lli,  IIon(?  Earth,  PIn«tfr 
of  I'arU,  Po«der«l  t  HrU. 

ftta     .         .         * 

AcPtatr  of  l>f»H. 
Oil   of   Turpen- 

UIM      •          ■          • 

"''"•** 

line. 

Commnn  ArtPtilc 
■nd  Prn<xld«  u[ 

l^lTMcra 

Mercuor. 

MURTABO   - 

ppA-  flour,       I,tn»«d-tD«il, 

Milk 

Shcrp  »  Hralfu.  ChRlk. 

l»KrMii      - 

Ground  Oil  C^kp.  CUy 

RkllfllllRRT  Jel-Llr 

Cumiiit  JHly      - 

Orri»-root 

StOAt 

Smid,  hUiiT  of  P»rl», 

Sauchi       • 

riiRlk,  |-U*(<-ro(Pari*. 

RM  I^aJ. 

ToMACCO    • 

Thr     lpfl%ir«    of    CRbb^iRP, 

Llqiiortctf,      Beet-root 

Sr]     AnmonUc, 

Sw^werd.    Rr««»rt     Chi. 

Drpei.  Crtrchii,  Ful- 

Curboasta    of 

cocj'fDot,  B»D,  OAliuni, 

ler'*  Kuth. 

Ammonia,    NU 
triit«  of  Ammo. 
nt...  &alt,  Alka. 
Ilfi.  aa  PolAih 
and  hixUi  CatP- 
chuirTerrAja- 
[lonlca.  Opium. 

VlNBOAl      - 

Ai-Hlr,    Pvriillpi. 
iiroui,    Hrdm- 
rhloric.  Sltrlc. 
Rod     Tarurk, 
Acidly  Cayenoe, 

Salt. 

I 


GENEBAL  INTRODUCTIOK. 


\7 


List  of  Article*  stated  to  be  used^  but  scarcely  likelij  to  be  emploj/ed^ 
for  the  Purpose  of  Adulteration. 


AMHonn  .          .         - 
Brrrn        -           •          • 
Cumi 
CmcviT 

CAYIflhl       - 

Milk 

PiMTIK  Alio  ALS       - 
VlftlOAH         ... 

For  Bulk  and  W«l^. 

r«»  c«io«. 

PluUiT  or  Parb. 
Uud. 

Mad*ter-root            .          .           - 
nrirh-dit*!    .           •           .           • 
Brlck-tluil    .           -           .           ■ 
Mitk  at  Almonds,  Gum,  Oum  Tra- 

gucaiilb. 
Opium.            , 
Usalic  Acid. 

Mjuldfrmot. 

Hrlrkdutt. 
Brtck  -duiU 

Another  nrrangemcnt  or  cloMificatioti  of  subslancM  used  for  adul- 
tcration  is  into  those  thnt  arc  not  injurious,  but  the  use  of  which  is 
simply  fraudulent,  and  into  those  which  are  hurtful  to  licalth.  A  list 
of  alt  the  liiibfitjinces  employer!  for  adultf^rution,  which  are  more  or 
leas  prejudicial  to  health,  will  be  gtrcn  hereafter. 


Importakce  of  tub  Subject  or  Auultkbatiopt. 

The  subject  of  odultomtion  is  undoubtedly  one  of  bij^h  impnrlflncr, 
and  in  ita  conseijuences  it  utlbrds  much  material  which  may  fairly 
engage  the  earnest  thoughts  of  the  financier,  the  aanitarian,  and  the 
moralist. 

The  financier,  Iwcause  it  involves  to  a  large  extent  considerations 
iff  profit  and  toss;  profit  to  the  majiufacturer  iind  seller  of  adulterated 
articles,  and  huts  to  the  consumer  and  the  revenue. 

The  saniturian,  IxK'&use  some  of  (he  articles  employed  in  adulter- 
stioa  are  of  an  exceediuj;ly  injurious  character,  and  calculated  to 
aflect  niiilerially  the  public  health. 

And  the  momlist,  since  the  practice  of  adulteration  involves  decep' 
tion,  and  even  frnml. 

Adulteration  U  iherefore  u  great  national  question,  closely  affecting 
the  pocket  of  the  consumer,  the  revenue,  and  the  health  and  moral:* 
of  the  people.  We  sball  nun-  proceed  to  enlarge  upon  each  of  these 
bends. 

The  pecuniary  BeariugM  of  Adultemtiotu 

Xbe  pecuniary  bearings  of  the  subject  of  adulteration  arc  of  very 

c 


J« 


GENERAL   IKTKODUCTJON. 


great  importance,  and  thcj  relate  to  the  consumer,  ibc  manufac- 
turer, merchant,  or  tradesman,  aiti]  the  revenue. 

The  great  profit  of  adulteration  arises  from  the  sale  of  articles  so 
adulterated  as  to  be  greatly  inferior  in  value  to  genuine  commoditieft, 
a  price  being  denianOed  for  these  mixetl  floods  }-ieIding  a  larjj^er  profit 
than  could  be  obtained  by  the  sale  of  uDmlullerated  goods;  in  fact, 
ihey  are  often  sold  at  the  rate  of  the  pure  arlii'le?.  This  increase<l 
profit  to  the  seller  is  just  e>o  much  loss  to  the  conHumer.  This  ma^ 
be  illustrated  bj  the  sale  of  mixed  chicory  and  coffee  as  ^nuinc 
coffee:  chicory  may  be  purchased  for  about  30^.  the  fwt.,  or  about 
3d,  per  lb. ;  coffee  for  80#^  or  nearly  9c/,  per  lb.  Now  coffee,  as  fre- 
quently S4.>ld,  often  contains  50  per  cent,,  and  in  many  cases  much  morv 
than  ihiA,  of  chicory ;  and  for  the  mixture,  half  chicory  and  half  coffee, 
worth  about  Qd.  or  7d,  per  lb.,  from  Is.  to  1«.  Cff.  is  charged. 

So  great  ia  the  loss  of  IhecoiiHumer  arising  out  of  the  practice  of 
adulteration  that  it  is  questionable  whether  it  does  not  amount  in 
most  cases  to  more  than  the  sum  of  the  whole  of  his  taxes.  The 
greatest  lusers  by  adulteration  are  the  humbler  classes,  the  labourer 
and  the  artisan,  who  are  compelled  to  purchase  the  nrlicles  they  use 
at  the  cheapest  shops,  where  adulteralinn  prevails  to  the  greatest 
extent.  This  practice  therefore  presses  with  peculiar  hardship  upon 
the  labouring  portion  of  the  population. 

It  is  clear  that  the  sellers  of  adulterated  articles  of  consumption,  be 
they  mnnufaciurers  or  retail  dealers  nre  in  a  position  to  enhance 
their  profits  by  the  practice  of  adulteration^  and  are  enabled  to  under- 
sell, and  too  often  to  ruin,  their  more  scrupulous  and  honest  compe- 
titors. 

The  question  of  the  adulteration  of  food  is  therefore  one  which 
vitally  affects  the  interests  of  thf  tturrt  honest  avfl  respectable  portion  of 
ike  trading  eommmxity^  who  dt-'pend  upon  the  manufacture  and  sale  of 
articles  of  consumption,  and  it  bvlxoves  them  strenuously  to  exert 
themselves  to  put  an  end  to  the  prevailing  system  of  adulteration 
which  is  undermining  the  very  foundation  of  trade,  namely,  Faitu  im 
CoMMKaciAi.  iMTEoarrr. 

The  peeuniiiry  interests  of  the  State  in  (he  question  of  adulteration 
will  become  apparent  when  we  remember  thiit  a  large  pnrt  of  the 
revenue  is  derived  from  duties  on  articles  of  consumption.  The  more 
ibe&e  articles  are  adulteiated,  the  more  is  the  revenue  defrauded. 


GENERAJ.   INTRODUCTION. 


19 


lib  not  possible  tocatiuute  witlian/  degree  of  cerUinty  tho  precise 
loss  to  the  State  arising  out  of  adulteratioD  ;  but  it  is  evident  from  the 
millioDs  of  money  derived  from  dudes  on  articles  of  consumption,  and 
from  tbe  extent  to  wbich  adulteration  has  prevailed  and  still  ])revails, 
tbat  tbe  loss  must  amount  annually  to  many  hundreds  of  thousands 
of  pODmU.  A  calculation  has  been  mado,  whereby  the  loss  to  the 
revenue  from  adulteratioD  is  cstimateii  at  two  uiillions  annually.  The 
author  of  the  *' Food  of  London,*'*  [».  1 38.,  stales  that  half  the  national 
revenue  is  derived  from  articles  of  consumption.  These  few  facts  are 
sufficient  to  show  the  paramount  importance  of  adulteration  to  tho 
national  Excheijuer. 

If  the  State  loses  so  much,  it  is  pretty  certain  that  the  public  suiTera 
a  much  greater  loss. 

The  Sanitary  Bearings  of  Adulteration. 
We  DOW  come  to  consider  the  question  of  adulteration  at  it  affects 
tkepuhiit  health.  No  doubt  can  possibly  be  entertained  on  this  sub- 
ject: no  one  who  examines  with  sufficient  care  the  facts,  but  mu&t 
acknowledge  that  the  subject  of  adulteration  is  of  the  liighusl  import- 
ance in  a  sanitary  point  of  view^  and  as  a  question  of  public  health. 

In  the  Jirti  piaect  the  adulteration  of  articles  with  substances, 
oltkougU  harmless  in  themselves,  ia  frequently  prejudicial,  by  reducing 
nnd  weakening  tho  natural  pro[>erties  of  those  articles.  This  is  the 
case  when  roasted  corn  or  carrot  is  added  in  cofToe,  and  water  to  milk : 
but  the  remark  applies  especially  to  medicines ;  for  in  this  case  to 
reduce  tbe  strengLh  of  a  medicine  by  adulteration  is  to  destroy  or 
modify  the  proper  action  of  that  medicine.  The  proper  doses  of  dlf* 
ferent  remedial  agents  have  been  dotennined,  in  must  cases,  by  coi'eful 
observation  and  experiment ;  and  in  diOcrcnt  doses  the  same  medi- 
cine is  known  to  produce  very  different  effects.  To  adulterate  medi- 
cines, even  with  banuless  substances,  b  to  destroy  the  very  foundation 
of  the  healing  art,  and  so  to  render  nugatory  the  wisest  and  best 
directed  efforts  of  the  physician. 

/»  the  iecontl  place,  adulteration  acta  prejudicially  to  the  public 
health  when  substances  are  employed  possessing  injurious  properties. 
Now  a  itreat  variety  of  such  substances  are  used  for  the  purpose  of 
Iteration.    We  have  ourselves  detected,  amongst  others,  the  follow- 

*  Bjr  George  Dodd.    LongnuLQ  &  Co. 
C  2 


GENERAL    INTUOUUCTION. 

ing :  —  the  three  chromates  of  lead,  the  !hree  Bninswick  greens,  which 
areiuixturus  of  the  cUroiuatvs  of  lead  aird  judigu  or  Pruesiaii  blue*  rM 
oxide  of  lead  or  red  lead,  arsenite  of  copiicr,  sulfthale  of  cop(>er,  car- 
bonate of  copper  or  verditer,  carbonate  of  lead  or  white  lead,  biaul- 
phuret  of  mercur)'  cinnabar  or  vermilion,  acetate  of  copper,  enlphuLe 
of  iron,  gamboge,  cayenne  in  spirits.,  bronze  powders,  which  are  allovs 
of  copper  and  zinc,  sulphate  of  lime,  carbonate  of  1  ime,  red  fcmiginntii^ 
carth5,  and  other  subatoncea  more  or  less  injurious.  This  list,  it  will 
be  observed,  eontaiiiK  Oie  name!)  of  some  of  the  most  virulent  poisong. 
Sometimes  the  rjiiantiiies  of  these  substances  used  is  so  uousiderablo 
that  immediate  ill  efT'ccts  are  produced :  thus,  as  has  alreailj  been  staled, 
not  a  year  passes  but  that  serious,  and  even  fatal*  accidents  arise  out 
of  the  practice  90  recklessly  pursued  of  colourin'?  sugar  confeetionavy 
witli  poisonous  pij^menta.  More  frcipicntly  the  ctleota  are  more  slowly 
developed:  the  substances,  although  taken  perhaps  in  but  minute 
quantity,  gradually  and  insidiously  deteriorate  the  tteallh,  giving  rise 
frequently,  amongst  other  maladies  to  rarious  f(triiis  of  4lys|)ep5ia  or 
indigestion  :  sometimes,  as  in  the  case  of  lead,  copper,  mercurj*,  and 
•rvenic,  they  accumulate  in  the  system  until  at  Icngtlj  serious  con* 
sequences  arc  produced;  thus  coses  of  paralysis  have  been  recently 
traced  in  the  clearest  manner  to  the  use  of  snuiT  adulterated  with 
preparations  of  lead ;  some  of  these  cases  will  be  fouml  recorded  in 
*•  Food  and  its  Adulterations:"  other  cases  of  lead  paralysis,  it  has 
been  slated,  have  been  produced  by  the  use  uf  cayenne  adulterated 
with  red  lead. 

The  subji»ined  Table  contains  not  only  the  names  of  the  sulwtnnceg 
used  In  ailulleruLlun  possessing  more  or  lees  injurious  properties,  but 
also  the  names  of  the  articles  in  which  they  have  been  discovered :  it 
wilt  be  perceived  that  the  number  of  injurious  substances  thus  em- 
ployed ia  very  great. 

Injurious  Subskmee*  aeltinUy  detected  in  adulterated  Articles  of 

Consumption. 


Sttbttancet. 

Cocculus  Indicua. 
ArsenitecfcopiM!r,  emerald  green, 

or  Seheelc's  green. 
Sulphate  of  copf>er  or  blue  vitriol, 

and  acetate  of  copper  or  verdi- 

grin. 


Articles. 
Beer,  rum. 
Coloured  sugar  confectionary. 


FIckles;  bottled  fruits  and  vege- 
tables; preserves;  dried  und 
crystallised  fruits. 


^^^^^^^^^^^^^P"^^^^^^^^B 

^ 

^^^^P                          QKNEllAL   INTRODUCTION.                               31           ^^^ 

^^K  »                   Substance t. 

Articles,                                 ^^^| 

^^^^ta^xmite  of  copper  or  verditer. 

Coloured  sugar  confectionary  and          ^^^B 
Custard  powders,   sugar    confcc-                 H 

The  three  chrotnaics  of  lead. 

tionary,  tea,  and  snutK                               H 

Ued  oxide  of  lead. 

Cayenne,  curry  powder.                                 H 

lied  ferru^inou-H  earths,  05  Vene- 
tian red,   bole  Ariuenian^    red 

Ked   suuces,    as  i^hrimp,  lobster,                 H 

anchovy    and    tomata   sauces ;                  ^M 

and  yellow  ochres,  umber,  &c. 

and   in'  potted  meats  and  6sh,                ^M 
cocoa,  chicory^  anchovies,  an-           ^^^H 

natto,  cheese,  tea,  and  sntiff,  &c.          ^^^H 

Carbonate  of  lead. 

Sugar  con  foe  tionary.                               ^^^^ 

Plumbago  or  black  lead. 

In  certain  black  and  Lie  teas.                 ^^^H 

BUuIphurct  of  mercury  or   cin- 
nabar. . 
1         Sulphate  of  iron. 

Cayenne,  sugar  confectionary.               ^^^H 

Re-dried  tea,  and  in  beer.                       ^^^| 

^H  Sulphate  of  copper. 

Bread,  rarely  ;  annatto.                           ^^^H 

^^  Cayenne. 

Gin,  rum,  ginj^er,  mustard.                     ^^^H 

^^    Gamboge. 

Sugar  confectionary.                               ^^^^| 

Chromatfis  of  potash. 

Tea  and  snuff.                                          ^^^B 

The  three  false  Brunswick  greens 

Sugar  confectionary.                    ^^^| 

being  mixtures  of  thechroraates 

^^^H 

ofleodaad  indigo,  or  Prussian 

^^^H 

blue. 

^^^H 

Oxychlorides   of  copper   or  true 

^^H 

Brunswick  greens. 

^^^H 

Orpiment  or  sulphuret  of  arscni- 

^^H 

cum. 

^^^^1 

Ferrocyanide  of  iron  or  Prussian 

^^H 

blue. 

^^^H 

Antwerp  blue  or  FruaiMaQ  blue 
and  clialk. 

Ditto.                                 ^^H 

^^^H 

Indigo. 

Ditto.                              ^^M 

U  Itraooarine. 

Ditto.                                .^^H 

Artificial  ditto. 

^^H 

Hyrtrated  sulphate  of  limp,  mine- 

Flour, bread,  sugar  confectionary.          ^^^| 

ral  white,  or  plaster  of  Paris. 

^^^^1 

Alunu 

Bread  and  flour.                                       ^^^| 

Sulphuric  acid. 

Vinegar,  gin.                                            ^^^H 

^H  itronze  powders  or  alloys  ofcopper 

Sugar  confectionary.                                ^^^H 

^^P     aod  zinc. 

^^H 

r            Now  with  eridence  such  oa  the  above,  it  is  impossible  to  contend          ^^^| 

^^K  that  the  use  of  such  a  variety  of  injurious,  and  cvou  poisonous,  sub-          ^^^H 

^^Bttances   is   unattended  with  danger,  and  tliat  a<lulteration  does  not          ^^^H 

^H                                ^  ^                                     ^^1 

tfl  GENERAL   INTRODUCTION. 

affect  the  public  health.  It  may  so  happen^  and  it  doubtl^'RS  docs 
Fuinctimes  occur,  that  the  sutnc  person,  in  the  course  of  a  gingle  day, 
receives  into  his  stomach  some  eight  or  ten  of  the  articles  above  enume- 
rated. Thus,  with  the  potted  meats  and  fish,  anchovies,  red  sauces, 
or  cayenne,  taken  at  breakfast,  he  would  consume  more  or  less  bole 
Armenian,  Venetian  red,  red  lead,  or  even  bisulphuret  of  mercury.  At 
dinner,  with  his  curry  or  cayenne,  he  would  run  the  chances  of  a 
eeconJ  dose  of  lead  or  mercury  ;  with  the  pickles,  bottled  fruits  and 
veftetablcs,  be  would  be  nearly  sure  to  have  copper  administered  to 
him  ;  while  if  he  partook  of  bon  Son*  at  dessert,  there  is  no  tellings  what 
nuuiber  of  poisonous  pigments  he  might  consume.  Again,  in  his  ten,  of 
mixed  or  green,  he  would  certainly  not  escape  without  the  adminis- 
tration of  a  little  Prussian  bhic,  and  it  might  be  worse  things :  if  he 
were  a  snulT-taker,  be  would  be  pretty  sure  to  1>c  putting  up  him  nostrils, 
from  time  to  time,  small  quantities  of  either  some  ferruginous  earth, 
bichromate  of  potash,  chromatc  of  leadj  or  red  lead  r  finally,  if  he  in- 
dulged himself  with  a  glass  or  so  of  grog  before  going  to  bed,  he  would 
incur  the  risk  of  having  the  coats  of  his  stomach  burned  and  irri- 
tated with  tincture  of  capsicum  or  essence  of  cayenne.  If  an  invalid, 
his  condition  would  be  still  worse ;  for  then,  in  all  probability,  he  would 
be  deprived  of  much  of  the  benefit  of  the  skill  of  bis  physician  through 
the  dilution  and  sophistication  to  which  the  remedies  administered 
for  bis  relief  were  subjected.  This  is  no  fanciful  or  exaggerated 
picture,  but  one  based  upon  the  results  derived  from  the  repeated 
analysis  of  diiTerent  articles  as  furnished  to  the  consumer. 


Moral  Bearings  of  Adulteration. 

The  third  and  last  aspect  in  which  adultemlion  is  to  be  considered 
is  the  mural. 

It  is  impossible  for  a  man  to  be  guilty  of  adulteration  and  yet  be  an 
honest  and  a  moral  man.  Can  it  even  be  said  of  the  adulterator,  be  he  a 
manufacturer  or  a  roaster  and  grinder  of  chicory  and  coffee,  or  be  he  a 
retail  tradesman  who  sophisticates  the  goods  wbich  be  sells  and  mixes 
them  with  roasted  com  or  beans,  Venetian  red,  &c.,  that  he  is  guilty  of  a 
less  oflenee  than  the  common  thief?  The  last  takes  but  our  property, 
while  the  former  not  only  robs  us  of  our  substance  but  sometimes 
destroys  our  health  as  well. 


GENERAL   INTBODUCTION. 


23 


Rat  BtluIUratioD  not  only  nukes  those  who  practise  it  dishonest, 
but  other  very  wrious  evils  oft«n  ensue '.  thus  it  begets  a  loss  of 
eonfidence  on  the  part  of  the  buyer  in  those  with  whom  be  deals. 
In  this  way  sometimes  not  only  doea  the  honest  trader  come  to  be 
looked  upon  with  the  same  suspicion  as  the  adulterating  merchant 
or  tradesman,  but  the  itatug  of  the  whole  of  that  portion  of  the 
-trading  community  engaged  in  the  sale  of  articles  of  consumption 
is  lowered^  and  it  is  looked  upon  with  misgiving  in  all  its  transactions; 
lastly,  the  character  of  the  whole  nation  for  integrity  in  it«  dealings 
■uffers  tn  consequence  of  adulteration. 

There  is,  then,  scarcely  an  individual  whose  interests  are  not  deeply 
enneemed  in  the  subject  of  adulteration.  The  interests  of  large 
public  institutions  of  alt  kinds  are  vitally  affected  by  adulteration,  as 
our  hospitalsand  other  charitable  establishments,  workhouses,  barracks, 
shipping,  lunatic  asylums,  public  schools,  and  simitar  institutions. 
Many  of  these  establishments  are  supplied  by  contract  with  diHercnt 
articles  of  consumption,  as  tea,  sugar,  coffee,  cocoa,  arrowroot,  oatmeal, 
tptoet,  &c.  Now  it  often  happens  that  the  articles,  and  especially 
oatmeal  and  arrowroot,  supplied  under  these  contracts,  arc  adulte- 
rated, and  this  is  frequently  to  be  explained  by  the  fact  that  these  and 
Other  articles  are  sometimes  purchased  under  market  price,  and 
conaequontly  cannot  possibly  be  genuine. 

Taking  into  consideration,  therefore,  all  the  circumstances  of  the 
case,  we  believe  it  to  be  almost  impossible  to  orer-cstimate  the  im- 
portance of  the  subject  of  adulteration,  viewed  either  as  a  question 
of  public  health,  of  pecuniary  loss  to  the  consumer  and  the  revenue, 
or  aa  one  of  morality.  To  sum  up,  it  is  not  too  much  to  say  that  the 
question  of  adulteration  is  one  which  affects  the  health  of  thousands, 
and  even  the  lives  of  many  ;  that  hundreds  of  thousands  of  pounds 
are  annually  lost  to  the  consumer  and  the  revenue  by  the  practice 
of  adulteration ;  and  that  by  its  prevalence  the  moral  ttatut  of  the 
eODUoerciat  portion  of  the  community  of  this  country  is  lowered  in 
the  eyes  of  the  world. 


Tub  Remedies  fob  Adulteration. 
The  means  to  be  employed  for  the  suppression  of  adulteration  are 
of  two  kinds,  viz.,  those  which    are  required  for  the  ducove/y  of 
adulteration,  and  those  for  its  //umxhtat'iU* 

c  4 


lU 


GENERAL    INTRODUCTION. 


The  prindpttl  incnns  to  be  adoptei]  for  the  detection  of  nduttornt'ion 
are,  First, — The  appointment  in  the  priiicijwii  towns  and  di&cricts  of 
the  United  Kingdom  of  inspectors  and  anal_f&t«.  The  duty  of  the 
inspectors  would  be,  to  procure  articles  of  food  and  medicine,  to 
forward  them  to  the  analyst  of  his  district  for  his  analysis  and  report, 
nnd  to  bring  cases  of  mlulteration  before  the  pn)pt!r  authorities  fur 
a<ljudication.  In  our  impr>rt  towns  a  principal  udditionol  duty  of  the. 
inspector  would  be,  to  watch  over  articles  of  food  and  medicine 
brought  to  this  country,  and,  in  doubtful  cases,  to  forward  them  to 
the  analyst  for  his  npinion.  Lastly,  the  inspector,  like  the  present 
Excise  officers,  should,  in  certain  coses,  have  the  power  of  entry  on 
suspected  premises ;  in  general,  however,  the  samples  collected  for 
analysis  shouhl  be  procured,  in  the  presence  of  a  witness,  in  the 
ordinary  way,  by  purchase,  and  the  power  of  entry  would  rarely 
require  to  be  enforced.  The  Excise  obtains  its  evidence  of  adultera- 
tion  chiefly  by  the  seizure  of  articles  in  the  warehouses,  &c.,  forcibly 
entered,  of  the  adulterator ;  in  this  respect  a  very  great  difference 
would  exist  between  the  proceedinr^  of  the  Excise  and  that  of  the 
authorities  now  proposed  to  be  called  into  operation. 

While  it  would  l>c  requisite  that  every  i:hier  lown  and  district 
should  be  provided  with  its  inspector,  it  woulJ  not  be  necessary  to 
appoint  an  e<|ual  number  of  analysts,  as  the  same  analyst  could,  in 
many  eases,  act  for  several  towns.  In  the  appointment  of  analysts, 
special  regard  should  be  had  to  their  qualifications,  and  none  should 
be  appointed  who  were  not  conversant  with  the  application  of  the 
microscope  to  the  detection  of  adulteration. 

The  appointment  of  the  inspectors  and  aiudysts  to  be  vested  in  the 
municipal  or  other  local  authorlLios. 

Second, — That  a  Metropolitan  Board  of  Insjjcctors  and  Analysts 
be  appointed,  its  sppointment  to  be  in  the  hands  of  the  Government. 
To  this  hoard  should  be  confided  the  charge  (if  dealing  with  the 
subject  of  the  aduUerutioii  td'  the  food  and  medicine  of  the  metro- 
polis and  its  suburbs.  The  board  should  publi<;h  periodical  reports  of 
its  proceedings,  these  reports  containing  the  particulars  of  the  articles 
WuUysed,  including  tlm  names  and  atldressus  of  the  parties  of  whom 
they  were  procured,  and  this  whether  they  proved  to  be  genuine  or 
adulterated.  Further,  the  local  inspectors  and  analysts  should  be 
required   to   make   periodical   returns   of  their    proceedings  to  the 


GENERAL   INTItODUCTlON, 


25 


Metropolitan  Board.  Bj  this  means  a  rast  amount  of  u»eful  in- 
formation in  regard  to  adulteration  would  bo  accumulated^  and  the 
several  local  authorities  would  bu  k<!pt  up  to  thti  full  measure  o( 
their  duties.  Lastly,  in  the  Central  Board  the  local  analysts 
would  poAseos  an  authority  on  adulteration  of  the  highest  ohu- 
racier,  which  they  might  consult  at  ail  times  in  cases  of  doubt  and 
difficulty.  We  consider  the  institution  of  this  Board  absolutely 
indispensable  to  the  successful  working  of  any  scbeme  designed  fur 
the  repression  of  adulteration.  Without  it,  although  local  inspectors 
and  analysts  might  be  appointed,  but  little  good  would  be  effected, 
because  there  would  be  no  sufficient  authority  over  thorn  to  ascertain 
whether  they  discharged  their  duties  properly  and  efEciently. 

Further,  the  services  of  the  dilTerenc  Boards  of  Health,  the  various 
sfpitary  officers,  and  inspectors  of  nuisances,  might  be  made  avail- 
able to  some  extent  in  procuring  articles  of  food  and  medicine  sus- 
pected to  be  adulterated. 

Fo^Uie  prevention  and  punishment  of  adalteration,  the  following 
are^flphasures  which  appear  requisite. 

'  That  all  cases  of  adulteration  should  be  disposed  of  aumuiarily 
before  the  Justices  of  the  Peace,  but  with  a  right  of  appeal  to  the 
Court  of  Quarter  Sessions. 

That  a  system  of  publication  of  the  names  and  addresses  of  all 
persons  whose  goods  hare  been  analysed  should  be  adopted,  and  this 
whether  the  articles  on  examination  proved  to  be  adullcruledorgenuine. 

That  the  sellers  of  adulterated  articles  should  be  punished  by  the 
infliction  of  fines,  and  the  actual  adulterator  by  fine  or  imprisonment, 
especially  in  the  cose  of  second  oflTences. 

That  it  should  be  rendered  imperative  on  persons  convicted  of 
selling  adulterated  articles  that  they  should  keep  a  placard  con- 
taining the  text  of  the  judgment  condemning  them  posted  up  in  the 
most  prominent  part  of  their  windows  for  three,  six,  nine,  or  twelve 
months  at  a  time. 

Few  methods  of  punishing  fraudulent  tradesmen  could  be  devised 
more  effectual  than  this,  and  which,  we  have  been  given  to  understand, 
has  been  enforced  in  France. 

The  above  is  a  short  outline  of  the  chief  measures  which  appear  to 
bft  necessary  for  the  discovery  and  prevention  of  adulteration.  The 
iMinisbmeuta  proposed  should  extend  to  all   kimls  of  adultvrationi 


2C 


GENEKAL    INTEODDCTJOK, 


n 


wheiber  injurious  t^  healthy  involving  pecuniiiry  loUf  or  whether 
simply  deceptive  ;  in  fact,  tbo  tleHnition  ofmlultcraCion  alreail^r  given, 
«nd  which  ni»y  here  be  repealed,  should  be  adhered  to. 

*' AdultemtioD  consists  in  the  intentionid  addition  to  an  article, 
for  purposes  of  gain  or  deception,  of  any  substance  or  substances  the 
presence  of  which  is  not  ucknoirledgcd  In  the  name  under  which  the 
article  is  sold," 

According  to  this  definition,  the  fltle  of  mixed  artielct  tinder  the 
name  of  one  only  of  the  ingredients  entering  into  the  composilion  of 
the  mixture  would  be  punishable.  We  regret  exceedingly  to  find 
tliat  the  Parliamentary  Committee  on  Adulteration  propose  to  attach 
punishments  to  certain  adulterations  only, — those  involving  pecuniary 
loss  to  the  purchaser,  or  which  arc  injurious,  either  directly  or  in- 
directly, to  health. 

It  is  not  pmposed  to  afEx  any  punishment  to  adulterations  with 
substances  of  a  cheap  and  innocuous  ehnracter ;  provided  "the  public 
derive  the  full  benefit  of  this  cheapness  in  a  lower  price.**  It  is  not 
even  recommended  that  such  mixed  articles  should  be  sold  as  mixturesi 
the  label  aOUcd  to  them  s|)ecirying  the  cotnptwiition  of  the  mixture. 

That  is  to  say,  supposing  tlie  recommendations  of  the  Cimimiltce  to 
be  acted  upon,  it  will  aiill  be  lawful  to  sell  a  variety  of  mixed  articles, 
as  tea,  coffee,  chicory,  arrowroot,  &c.,  wliieh  are  not  what,  by  the 
name  under  which  Ihey  are  sold,  they  prwfess  to  be,  and  what  as- 
suredly they  ought  to  l>o.  Thus  for  a  very  largo  proportion  of  the 
adulterations  actually  proctised,  not  only  wuuld  no  remedy  be  pro- 
vided, but  a  positive  legal  licence  would  be  given  for  their  perpetration. 

The  Committee  acknowl<*ge  that  "  the  public  morality  is  tainted, 
and  the  high  oommcrciat  character  of  this  country  seriously  lowered, 
both  at  home  and  iu  the  eyes  of  foreign  countries,"  through  adulw- 
raiion.  We  very  much  fear  ibat  the  recommendation  of  the  C<»m- 
milte«  respecting  "innocuous"  adulterations  is  by  no  means  calcu- 
latcd  to  take  nwuy  ibis  national  n*pronch. 

Besides,  this  distinction  of  adulteration  into  harmless  and  hurtful 
opens  the  door  to  perpetual  oonllictfl  of  itj»inion  and  litigation  aa  W 
what  constitute  innoeuou*  and  what  injurious  adulterations;  wbereaa 
there  is  no  commercial  adultcrnliim  which  can  l>e  practise*!  tb»l  w 
not  ii^jurious  in  some  sense  or  other,  either  to  public  morality,  to  the 
pocket,  or  to  health. 


I 


GENERAL  INTRODUCTION. 


27 


■ 


To  make  rach  a  distinction  as  this  is  to  leave  untoucbtxl  tbc  dh- 
lionesty  necessarily  inTolved  in  !h«  practice  of  adulteration  of  every 
kbd.  According  to  our  views,  all  adulteration  ia  to  be  condemned, 
because  it  involves  at  least  intentional  and  designed  deception;  bul 
the  Committee  would  indirectly  sanction,  and  altnuat  legalise,  a  large 
class  of  deceptive  adulterations,  and  thus,  in  some  respects,  matters 
woald  be  rendered  worse  than  they  even  are  at  present  There  are 
few  persons  who  do  not  feel  that  in  practising  adulteralion  of  any  kind 
ibey  are  guilty  of  that  which  is  wrong,  and  which  they  wimld  hi' 
ashamed  to  avow  openly ;  but  the  Committee  would  take  away  thifi 
Mnse  of  shame,  aud  tell  us  that  uiauy  sdulteratioiis  are  not  reprehen- 
wble,  aikd  ought  to  1>e  connivcil  at  by  tltc  Legi<ilaturc. 

It  is  true  the  Committee  throw  in  a  kind  of  saving  clause,  and 
state,  **  provided  the  public  derive  the  full  benefit  of  this  eheopiiess  in 
a  lower  price."  It  is  well  known  that  most  articles  are  sold  in  the  mixed 
state  chiefly  to  enhance  profits,  and  that  almost  consUuilIy  the  public 
are  loaert  by  such  mixtures  ;  but  the  great  difficulty  will  be  to  pro- 
duce satisfactory  proof  of  the  i>ecuniary  loss  sustained.  Inmany  cases 
it  is  not  possible  to  determine  the  proportions  of  the  several  ingredi- 
ents in  a  mixture,  and  these  being  undetermined,  it  is  imi>ossible  to 
ascertain  the  value  of  the  mixture. 

We  are  decidedly  of  opinion,  therefore,  that  under  the  bead  of  "in- 
nocuous '*  adulterations,  the  public  would  be  defrauded  to  an  enor- 
mous extent. 

A  single  good  purpose  served  by  this  distinction  of  adulteration 
into  innocuous  and  hurtful  we  cannot  perceive.  It  appejirs  to  us 
that  Qo  real  difficulty  exlstd  either  in  de6ning  what  constitutes  adul- 
teration, or  in  determining  how  to  deal  with  it.  The  course  dictated 
by  common  sense  should  be  followed — viz.,  that  of  re(|uinng  that  every 
article  should  be  what  it  professes  to  be,  and  what  ihc  public  under- 
stand it  to  be  by  the  name  under  which  it  is  sold.  Ou  this  point,  thure- 
fure,  we  consider  that  the  Committee  have  fiiUen  into  a  grave  niistiikc. 

Wc  much  regret  that  the  Committee  should  have  involved  tbem- 
aelves  in  this  difficulty,  seeing  that  the  right  course  to  pursue  is  so 
plain  and  obvious, — namely,  to  require  that  every  article  should  be 
what  it  professes  to  be  by  the  name  under  which  it  b  vended.  If  it 
be  told  u  muatcrd,  arrowroot,  or  cocoa,  it  should  be  one  or  the  other 
of  tlMMC  articleii  «nd  nolhijig  else. 


18 


GENERAL   INTRODUCTION. 


If  it  be  rijiht  to  allow  the  sale  of  mixed  articlea,  it  is  dnubtleas 
only  commonly  honest  and  just  that  tbesc  articles  shouM  be  soM  u 
mtjctures,  fimJ  tUeir  L'om[)09ttion  sjiecified. 

In  aJopling  this  course,  no  real  difficulty  whatever  exists,  as  it 
would  be  ens/  to  devise  names  auflieiently  appropriate  by  wlucli 
these  mixtures  might  be  distingnisbpd,  aa  —  "mixed  mustard,  cousist- 
iiiff  of  muslarj,  wheat-flour,  and  turmeric ;"  "  mixed  cocoa,  consisting 
of  cocoa,  sago,  and  sugar." 

But  we  would  go  further  than  this,  and  require  that  the  proportions 
of  the  several  ingTLMlients  should  be  specified  thus  :  '■'Mixed  Mustard^ 
containing  mustard  50,  wheat-flour  40,  and  turmeric  10  parts ;  and  the 
same  with  coffee  and  some  other  mixtures.  Now  tlie  labelling  of 
articles  in  this  way  has  already  been  sanctioned  by  the  legislature, 
which  re((uire8  that  mixed  coffee  and  chicory  should  be  sold  only  as 
thus  labelletl  :  "This  is  sold  as  a  mixture  of  cliicory  and  cofFcc."  All 
that  is  needed,  therefore,  is  an  extension  of  the  some  syitem. 

With  regard  to  tlie  punishmi'nts  for  adulteration,  we  perceive  that 
the  only  punisbnjent  which  the  Committee  recommend  to  be  iuBioled 
is  that  by  fine. 

The  Report  of  the  Committee  states:  "  A  summons  shall  be  issued, 
and  the  case  be  investigated  before  the  justices,  who  shall  have 
power  to  inflict  summary  punishment,  by  fine  or  imprisonment,  in 
every  case  where  pecuniary  fraud  or  danger  to  hcaith  shall  have  been 
proved," 

We  fear  that  it  must  be  concluded,  from  the  wording  of  the  ibore 
jmragraph,  that  the  punishment  of  imprisonment  is  only  proposed  t-o 
be  iiiUicted  in  default  of  payment  of  the  fine.  If  this  be  so,  then  our 
conviction  is,  that  pecuniary  fines  ore  a  most  inadequate  punishment; 
they  neither  are  adequate  to  the  serious  nature  of  the  offence  com- 
mitted, nor  will  they  scnre  to  check  adulteration  to  any  extent.  The 
system  of  fines  has  been  repeatedly  tried,  and  hoft  hitlierto  failc<l.  Of 
what  moment  is  a  fine  of  a  few  |K>unds  to  an  adulterating  merchant, 
spice  or  drug  grinder,  who,  probably,  before  the  discovery  of  his  guilt, 
has  been  engaged  for  years  in  adulteration,  whereby  he  has  realised 
hundreds  and  thousands  of  pounds?  Besides,  to  adulterate  is  to  com- 
mit fraud,  and  surely  it  cannot  be  right  to  compound  with  fraud  by  a 
money  payment.  What  ia  required  is,  that  adulteration  should  be 
braniled  as  a  crime,  and  this  can  only  be  done  by  affixing  to  it  some 


QfeNBKAL   INTHODUCTION. 


29 


punishment  which  shall  entail  personal  discredit  and  disgrace,  such  as 
that  of  imprisonment.  Wo  are  therefore  decidedly  of  opinion  ihat 
impriDonuienl  ought  to  furni  one  of  the  puui^ihuii^iits  for  adulteratioiii 
it  being  reserred  fop  the  worst  oases,  and  for  second  offences.  The 
pumsbmeut  by  fines  only  will  effect  little  or  nothing  for  the  suppres- 
sion of  adulteration.  On  referring  to  thu  laws  in  force  against  adul- 
teration in  France,  Belgium,  Prussia,  lloUand,  Uamburgh,  and  even 
New  York,  we  find  that  imprisonment  is  onct  of  the  punishments  en- 
forced against  adulteration.  Why  then,  we  ask,  are  adulterators 
in  EngUud  —  a  country  formerly  presumed  to  set  a  pattern  of  coiu- 
meroiol  inte^^rity  to  the  world  —  to  be  dealt  with  so  gently  ?  The 
Cnmtailtee,  who  have  taken  great  pains  to  collect  the  laws  in  force  iu 
other  countriesi  could,  we  should  supjKJse,  scarcely  have  failed  to 
notice  the  efficient  character  of  those  laws,  as  contrasted  with  their 
own  feeble  recommendations.  Amongst  other  penalties  intlicted  iu 
most  countries,  are  the  confisi'iatiou  of  the  adulterated  goods,  and  the 
prohibition  of  confirmed  adulteraturs  from  following  their  trades  or 
callings.     The  Report  of  the  Committee  is  silent  on  both  these  points. 

The  parties  whom  the  Committee  recommend  to  be  punished  are 
ike  actual  adtdterator  anil,  with  certain  restrictions^  the  teller.  It  is 
not  pro|josed  thst  tlie  seller  should  be  held  responsible  when  "he 
can  afford  satisfiictory  proof  that  he  has  himself  been  deceived,  and 
was  not  conscious  of  the  adulteration  practised,  unless  he  has  evinced 
A  culpable  knowledge  of  the  trade  which  he  professes  to  follow.'* 

In  legislating  upon  the  subject  of  adulteration,  it  should  be  remem- 
bered that  the  seller  is  frecpiently  as  much  a  party  to  adulteration  as 
the  actual  adulterator.  This  is  shown  by  the  fact  that  he  often  buys 
articles  at  prices  ai  which  be  knows  it  is  impossible  that  they  can  be 
genuine.  Again,  it  should  lie  recollected  that  it  is  often  the  interest 
of  the  seller  to  screen  the  iidulterating  wholesale  merchant  or  manu- 
facturer, he,  in  many  case?,  being  largely  in  his  debt.  In  the  course  of 
the  publication  of  the  reports  of  "  The  Lancet "  Sanitary  Commission 
we  met  with  many  cases  in  wliich  the  seller  preferred  to  incur  the 
risk  consequent  upon  the  publication  of  his  name,  rather  than  divulj^e 
the  names  of  the  parties  by  whom  he  was  supplied.  Tlie  seller, 
therefore,  must  not  be  let  off  too  easily,  especially  when  he  attcm]>(s 
to  screen  the  perpetrator  of  adulteration. 


aa 


GENERAL   IIH'RODUCTIOK. 


The  fttlhwing  are  the  ttept  recommended  by  the  Commiitee/or  the 
JJiiCQvery  and  Suppression  of  Adulteration, 

"  Tt  will  be  desimblc,"  states  the  Report, "  therefore  to  empower  mu- 
nicipal or  other  local  or  district  autliorities,  to  appoint  an  ofBcer  or 
officers,  who,  on  complaint  mude,  nr  in  cases  of  resaonable  su^^picion, 
shall  pnx'uro  ponions  of  any  articles  supposed  to  be  adulterated,  with 
A  view  lo  their  exaiuination  or  amily^iis  by  some  duly  qualified  person 
appointed  for  that  purpose.  On  the  report  of  Buch  person,  if  h 
confirm  the  suspicion  of  adulteration,  a  suniinona  i^hall  }fc  issued 
and  the  case  be  investigated  before  the  justices,  who  shall  have  power 
to  inflict  summary  punishment,  by  fine  or  imprisonment,  in  every  case 
where  pecuniary  fraud  or  danger  to  health  shall  have  been  proved. 
It  ia  essential  that  a  right  of  HppeM  should  lie  lo  the  Court  of  Quarter 
Sessions. 

"  With  regard  to  coloured  confeclionary,  your  Committee  recom- 
mend that  authority  should  be  given  to  local  boards  of  bealtli  op 
other  governing  bodiea  to  forbid  the  use  for  colouring  of  all  mineral 
matter,  and  all  poi(ioning  vegetable  matter. 

"But  although  your  Comtiiitlee  desire  to  leave  the  execution  of  the 
law  against  adultemtion  in  the  hands  of  the  local  authorities,  they 
are  of  opinion  that  very  valuable  assistance  would  be  afforded  to 
such  bodies  in  ascertaining  the  fact  of  adulteration,  if  one  or  more 
K'ientific  analysers  were  to  be  appointed  under  the  anthority  of  the 
Generttl  Boar<l  of  Health,  to  whom  the  local  authorities  might  refer 
whenever  they  thonghl  fit.'* 

The  Committee  do  not  moke  any  special  recomraenda lions  inr^anl 
to  the  adulteration  of  drugs. 

**  Your  Committee  are  of  opinion  that  no  inspection  at  the  outporia 
would  guarantee  to  the  consumer  the  purity  of  commodities  pasiting 
through  the  hands  of  intermediate  particH  ;  and  the  exclusion  of  im- 
pure drugs  would  operate  injuriously,  by  interfering  with  the  supply 
obtained  by  scientific  processes,  calculated  to  extract  valuable  matter, 
even  from  products  seemingly  almost  worthless." 

On  this  point  also  we  differ  from  the  Committee,  bccaasc  we  believe 
that  a  system  of  inspection  would  be  found  to  opei-ate  most  benefi- 
cially.    Jt  hao  already  been  tried  in  America,  and  the  jdan  has  worke«l 

U.     Supposing  that,  in  accordance  with  the  opinion  of  the  Com- 


GENERAL   INTRODUCTION. 


31 


mittee,  no  inspection  at  the  chief  places  of  import  is  established,  what 
will  bap[K.'i)  ?  Adulterated  drugs  will  be  iin|>ortcd  as  heretofore,  and 
will  find  purchuers ;  they  will  pass  into  the  handi)  of  the  wholeaala 
drngf^ists.  from  them,  again,  into  those  of  the  retail  chemist,  and  thus 
they  will  reach  the  consumer,  who,  finding  that  be  has  been  supplied 
with  an  vlulterated  drug,  will  have  no  rt.'niedy ;  for,  according  to  the 
report,  the  seller  is  not  to  be  held  rcfiponsible  for  adulterations  of 
which  he  hiu  no  knowle<lge.  Theitc  remarks  apply,  not  only  to  drugs, 
but  to  mmny  articles  of  food  occasiimiUly  imported  in  an  adulterated 
condition. 

The  suggestions  of  the  Committee  doubtless  contain  much  that  is 
good,  as  far  as  they  go ;  but  they  do  not  go  far  enough,  and  hence 
I  bey  will  not  prove  effectual.  ITieir  great  defect  is  that  they  do  not 
include  any  provision  for  a  central  board  or  authority  such  as  we 
conceive  to  be  essential.  The  urganisation  proposed  in  connection 
with  the  General  Board  of  Health  is,  considering  the  magnitude  of 
the  evil,  of  too  limited  a  character  to  effect  much  good.  It  is  essen- 
tially ncces»ary  tlial  there  should  be  some  well  organitted  central 
authority,  having  a  competent  head :  the  construction  and  duties  of 
this  body  have  already  been  indicated.  SuppoM?,  in  accordance  with 
the  recommendations  of  the  Committee,  the  various  local  oiTieers  to  be 
.appointed  ;  who  is  to  determine  whether  they  do  their  duty  or  not  ? 
Who  is  to  advise  and  guide  them  in  the  discbarge  of  that  duty  P  And, 
finally,  in  what  way  arc  the  facts  in  regard  to  adulteration,  brought 
to  light  through  their  labour?*,  to  be  made  available  for  the  general 
gOO<l  ?  Now  the  formation  of  a  board  such  as  is  indicated  does  not 
necessarily  imply  the  institution  of  a  new  authority :  the  Auuly- 
ticftl'Board  of  the  Excisei  if  remodelled  and  placed  on  a  broa<lcr 
basis,  might  be  made  to  answer  the  puri>osc  fully.  The  reorganisa- 
tion of  this  board  is  imperatively  deroandeil ;  in  its  present  state  it  is  a 
diagrace  to  the  country.  The  correctness  of  this  sutemcnt  we  shall 
proceed  to  prove. 

The  question  may  next  be  considered  to  what  extent  the  new  mtiehi' 
nery  proposed  to  be  called  into  operation  for  the  attppregsian  of  adidtf 
ration  trill  cIobH  with  the  duties  uud  jMtsition  of  the  Eiciae  in  regard  to 
aduJirrutitm. 

One  of  the  chief  dutiea  entrusted  to  the  Excise  is  the  protection  of 
the  revenue  (of  which  no  uiconsidcrable  portion  is  derived  from  du- 
tiea on  exciseable  articles  ol' consumption)  from  loss  arising  out  of 


GENERAL   INTRODUCTION. 


flduhoration  of  those  articles.  Amongst  the  articles  bearing  ui  Ekciso 
duty,  niid  for  the  aduUeratioa  of  which  the  Excise  are  respobsiblef  aro 
tea,  coffV*,  cocoa,  pepper,  spirila,  and  tobacco,  including  snuC  Now, 
It  maj  be  inquired,  do  the  Committee  propose  that  the  purchasers  and 
analysts  whom  they  desire  to  be  appotntud  should  occupy  themselves 
with  the  adutterntion  of  the  several  articles  enumerated  !*  If  so,  they 
would  be  actually  discharging  the  duties  for  which  the  Excise  are  paid 
and  rvsponsible,  and  thus  that  body  would  be,  to  a  great  extent,  supcr- 
»oded.  On  the  other  hand,  Riipposing  that  these  articles  nre  still 
rcsenred  for  the  Excise  to  deal  with,  what  would  then  be  the  state  of 
the  case?  Just  this,  tlial  the  revenue  would  still  continue  to  be  de- 
frauded to  a  Unje  extent,  and  the  public  health  injured,  as  they  have 
iHwn  for  years  past,  by  the  prevalence  of  an  enormous  amount  of 
aduUoriitiou  in  exciseable  articles,  and  nearly  all  of  which  adulter- 
ations, under  a  thoroughly  cfrecltve  system  of  management,  might  be 
prevented.  This  brings  us  to  consider  the  question,  hma  far  the 
£xcis«  has  hitherlo  protected  the  revenue  from  loss  throtigh  adtdter* 
ation. 

The  articles  under  Excise  supervision  have  already  been  enumerated- 
Of  these  articles,  tea  is  still  subject  to  considerable  ailulteration, 
while  the  extent  to  which  the  public  are  defrauded  in  coffee  and 
cocon  is  notorious;  they  are  also  lai^ely  defrauded  in  pepper,  spirits, 
and  tobacco,  as  is  proved  by  the  following  results  of  analyses  of  those 
(uiirles  as  supplied  to  tl»e  public,  and  as  rejiorted  in  "  The  Lancet." 

Of  nnnicroiis  Bomples  of  black  and  white  pepper  analysed,  fully  one- 
half  were  adulterated  with  ground  rice,  pea-dour,  wheat-flour,  UnscL-il 
meal,  nml  mu.>>ttuM  husk. 

Of  thirty-eight  samples  of  ^'k  examined,  a  very  large  proportion 
were  adulterated,  some  of  them  being  reduced  in  strength  une-holr, 
whik' »even  uf  them  cnntaineU  caycunc  pepper.  The  same  was  thu 
caao  with  rttm  and  braiut^. 

Of  forty-three  different  Mti^jtexnmined,  nearly  all  were  adulterated, 
the  adulterating  in<:rodients  used  being,  for  the  most  part,  salt,  alka- 
lies, silica,  red  and  yellow  ochre,  red  lead,  chromate  of  leod,  and 
t.>hroniHtL'  uf  pularh. 

'n>0  Excise,  then,  hns  most  signally  failed  in  its  principal  duty  — 
namely,  the  protcolion  of  the  revenue  against  adulteration. 

The  pnnif  tbut  it  has  thus  foiled  is  furniBhcd  in  the  fact  ihat,at  the 
iUuc  of  ihe  pttblicatiou  of  the  author's  reports  in  "  The  Lancet,'*  adul- 


GENERAL   INTRODUCTION, 


>n  was  ascertained,  on  evMence  the  nio»t  incontrov^rliblu,  ioprc- 
every  one  of  the  articles  subject  to  the  supervision  of  the  Excise. 
Now  this  stale  of  things  ought  not  to  bo,  and  it  ia  one  which  i^  di^ 
creditable  to  the  Government  of  thi»  country. 

The  causes  of  the  failure  of  the  Excise  may  next  be  considered :  they 
arc  several;  but  we  do  not  pro]H)9e  to  do  more  at  present  than  just, 
in  the  briefest  possible  manner,  refer  to  one  or  two  of  tho«e  causes. 

One  reuiion  is  the  want  of  sutfieient  activity  and  vigour  in  enforcing 
the  powers  with  which  they  arc  intrusted.  Compared  with  the  prc- 
[Yolencc  of  odutteration,  how  selilom  do  they  moke  exposures  of  aduU 
[teratiun,  and  institutii  prosecutions  ! 

Another  reuson  is  thut  they  do  not  »ufficiently  employ  the  resource* 
of  science  for  the  discovery  of  adulteration.  They  rely  too  much 
upon  the  information  of  Excise  ini^pectors,  and  too  little  ujKin  science, 
upon  the  resources  of  chemistry-,  but  more  ctspccittlly  u)>on  a  know- 
ledge of  vegetable  structure  as  ruvcoled  lo  the  competent  ob- 
server by  menus  of  the  microscopu. 

From  not  eni]duying  science  enough*  the  Excise  has,  for  the  most 
pnrt,  in  order  lo  discover  evidence  of  adulteration,  been  driven 
to  adopt  A  system  of  eifpionn^e,  and  to  tlie  rude  and  inquisitorial 
proceeding  of  entering  forcibly  ui>on  susiMJCtvd  premises,  and  of 
seizing  on  any  adulterated  articles  or  sulistances  employed  in  adul- 
teration, and  which,  pcrcliance,  they  might  find  in  the  course  of  their 
search.  The  method  adopted  by  **The  Lancet"  Commission  was  in 
sli'iking  contrast  to  this.  It  simply  purcliased  the  dilTerent  articles 
as  sold  in  ilie  ordinary  way  of  business,  and  applied  to  their  analyses 
all  the  resources  of  science,  especially  the  microscope  and  chemistry. 
iJy  this  proceeding  it  was  not  necessary,  as  in  the  case  of  the  Excise, 
^)  maintain  un  army  of  '*  4000  "  Excise  inspectors,  neither  was  it  requi- 
site to  violate  the  sanctity  of  men's  private  dwellings. 

That  the  P^Ixcise  hml  not  employed  science,  either  sulBciently  or 
eS^ctively,  for  the  detection  of  adulteration,  at  the  period  of  the 
Commenceujent  of  our  investigations,  is  proved  by  many  circum- 
^Itances. 

Thus  we  found  a  variety  of  chemical  adulterations  to  prevail,  of 
which  the  Excise  possessed  no  knowledge ;  but  it  was  in  respect  to  the 
nsc  of  the  microscope,  as  an  instrument  for  the  discovery  of  adultera- 
tioo,  that  its  knowledge  was  the  roost  defective.    Of  this  ignorance 


34 


GENEEAL   INTEODUCTIOy. 


it  has  itself  furnished  a  memorable  and  striking  proof.     In  ]$50 

repeated  remonstrances  were  addressed  to  the  Government  to  prohibit 
the  iiduUnration  of  coflVe  with  chicorj.  The  Government  cxcutcd 
itself  from  Interfering*  on  the  pleu,  publicly  urged  by  the  then 
Chancellor  of  the  Kxchequer,  Sir  Churles  Woodj  in  the  House  of 
Coromnns,  that,  neither  by  chemistry,  nor  by  any  other  means,  was 
the  adulteration  of  coiTcc  wiih  chicory  to  be  detected.  This  statement 
was  maile  on  the  strength  of  a  report,  jirocured  at  the  instance  of  the 
Excise,  from  three  of  the  most  distinguished  chcmiitts  of  the  thiy ;  the 
real  (act  at  the  aame  time  being,  that  nothing  h  more  easy  or  certain 
than  the  discovery  of  the  ailulteration  in  question,  by  means  of  the 
microscope.  Further,  we  have  within  tl>e  last  few  years  brought  to 
light,  with  the  aid  of  the  microscope,  huiidreila  of  Hdulterations,  the 
existence  of  which  was  utterly  unknown  to  tlic  Kxcise,  Even  now, 
although  we  have  done  so  much  to  teach  thiit  h(»\y  the  use  of  the 
microscope,  it  has  as  yet  failed  to  afford  the  public  any  evidence 
to  show  that  it  is  capable  of  em]>Inying  that  instrument  nri;;!)!  for  the 
discovery  of  adulteration.  It  not  unreasojiubly  nn^ht  have  been 
expected,  that  a  numerous  ami  public  body  like  the  Excise,  instituted 
and  paid  for  the  special  work  of  discovering  adult  emtio  n,  with  the 
most  innple  opportunities  and  facilities,  would  not  have  required  to 
be  tttu^lit  ita  business  by  those  engaged  in  prosecuting  the  subject  of 
adulteration  in  a  private  und  unolTicial  capacity. 

It  might  also  have  been  reusoriably  expected  not  only  that  it  woald 
not  require  to  be  taught  itself,  but  that  it  would  have  published  from 
time  to  lime,  for  the  information  and  guidance  of  the  public,  some  in- 
stmctions  calculated  lo  put  it  on  its  guard  against  adulterations,  and 
to  teach  it,  to  some  extent,  how  tn  detect  them. 

We  learn  from  the  Report  of  the  Select  Committee  on  Adulteration, 
that,  "  in  addition  to  about  4000  officers  scattered  over  the  country,  the 
Board  (of  Excise)  employs  about  sixty  to  seventy  analytical  chemists, 
whose  numbers  arc  recruited  by  students  educated  for  the  purfMJse  at 
University  College,  lo  the  number  of  lourteen  in  every  year."  AVhji 
here  is  a  whole  army  nf  inspectors  and  analysts!  With  such  huge 
machinery  as  this,  the  wonder  Is  that  adulteration  should  exist  in  any 
degree,  much  less  that  it  should  be  all-prevulent  1  Had  we  the 
organisation  and  control  of  such  an  enormous  staff,  we  would  under- 
take to  all  but  eradicate  adulteration  from  the  land. 


GENERAL   INTRODUCTION. 


as 


Now,  it  mu9t  be  remembered  tbKt  the  chief  dutj  of  th'ia  large  force  is 
timply  to  protect  tbe  revenue  agfiirijit  fraud  in  some  halfdozcn  articles  of 
eon»uiuption.  Willi  uduUeration,  as  Buub — with  the  great  mass  of  adul- 
.terfttioriR,  whether  they  are  injurious  to  health,  or  wliether  detrimental 
to  the  revenue — the  Excise  concerns  itself  not.  Sinf^ular  to  relate, 
thi:re  are  a  variety  of  articles  of  eoneuniptiou  which  pay  duty  to  the 
8tat«%  which  help  to  augment  the  revenue,  and  which  are  nolorii>nsly 
adulterated,  and  yet  the  Excise  docs  not  talcc  cognisance  of  the  adul- 
Icralion  of  Euch  articles. 

It  thus  appears  that  the  Excise  has  the  smallest  possible  amount  of 
idutj  to  perform  in  connection  with  aduUeraiinnf  and  yet  thi^  small 
ts  it  i«,  is  most  inefBciently  performed,  llicre  is  no  reason  whatever 
why  this  discrcditjiblv  state  of  things  should  exist.  The  present 
machinery  of  the  Excise,  remodelled,  might  be  made  to  act  against 
iduheration  with  enormous  eflfect. 

Annther  reason  is  ihnt  it  does  not  avail  itself  eufliciently  of 
llie  advanloties  to  be  derived  from  free  publicity.  We  are  dis- 
pOKd  to  rely  more  upon  the  regular  publication  of  the  namr's  and 
iddreaaes  of  those  whose  goods  have  been  analysed,  for  the  sup- 
pression of  adulteration,  than  upon  any  other  means,  in  conse- 
i^aence  of  the  excellrnt  effects  which  have  undoubtedly  resultetl  from 
the  publication  in  "The  Lancet,"  for  a  period  of  four  years,  of  the 
auBOB  of  upwards  of  2000  merchunts  and  iradesmen.  So  great  has 
Wen  the  effect  of  this  publication,  combined  with  the  recent  exposures 
Wfore  the  Parliamentary  Cunuuittee,  that  we  are  of  opinion  that  not 
•twentieth  part  of  the  adulteration  now  prevjiils^  in  the  metropolis  at 
that  did  at  the  time  when  the  reports  of  *'The  Analytical  Sanitary 
Commisiion "  first  ap|>eared.  In  some  articles  the  improvement  is 
■ktaifcet  to  the  eye  alone,  as  in  the  red  sauces,  pickles,  bottled  fruits 
■od  Ttgetables,  and  coloured  sugar  confectionary. 

TIm  foHowing  remarks,  in  reference  to  the  publication  of  tbe  names 
of  traders  in  "  The  Lancet "  ami  the  effect  j>ro<luccd  by  the  micio- 
Mofie,  occur  in  tlic"  Qunrierly  Review  "for  March,  1855,  in  a  review  of 
ibr  autiior's  work  entitled  "  Fo<.pd  und  its  Adulterations." 

"A  gun  suddenly  fired  into  a  rookery  coulil  not  cause  a  greater 
eomnotion  than  did  this  publication  of  the  names  of  dishntiest  mules- 
■CD;  DOT  docs  tiie  daylight,  when  you  lid  a  stone,startle  n^\y  and  loath- 
things  more  quickly  than  the  pencil  of  light,  streaming  through  a 
D  3 


as 


GENERAL   INTKODUCTIOX. 


1 


quarter-inch  lens,  8uq>riscd  in  tbeir  native  ugliness  the  lliousftnil 
andone  illegal  sul»tnnt-e»wlii('h  enter  more  or  less  into  Dvcry  ck'scrip- 
tion  of  food  which  it  will  piiy  to  adulterate.  Niiy  to  sucli  a  pitch  of 
refinement  has  the  art  of  f»bric.iLion  of  alinientary  substances  reaclii.*il, 
that  the  very  nrtiolus  used  (n  adulterate  ore  Uieriiaelves  adultenited; 
and  while  one  trn(k*sman  is  plckinjj  the  pockets  of  his  cnstomeri 
a  still  more  cunnin<^  rogue  is,  unknown  to  himself,  deep  in  his  own." 

No  objection,  we  believe,  exists  to  the  suheiue  which  we  bave  briefly 
set  forth  for  the  discovery  and  prevention  of  adulteration,  on  tbe 
score  of  expense;  on  the  contrary,  wbile  nn  imnieniic  saving  would 
ensue  to  the  consumer,  the  revenue  would  be  greatly  benefited  and 
the  public  health  i)roIci*ted.  The  reijuisitc  machinery  is  in  existence 
at  the  present  lime:  as  has  bofore  been  -ilatod.  there  Is  an  enormous 
and  costly  maohinery  at  work  for  the  prevention  of  the  adultera- 
tion of  some  half  dczcn  exciseable  articles, — that  nf  the  Excise, — con- 
aiatin^  of  some  70  ehcuiists  and  4000  inspectors.  The  Excise  however, 
has  failed  to  accum[jlish,  to  a  frreat  extent,  this  single  object:  further, 
it  takes  no  LOgnisauce  of  the  ndulterntion  of  many  duty-pMyiiig 
articles,  as  spicea,  on*owroot,  &c.,  nithounh  this  immediately  airecls  the 
revenue;  uor  does  it  notice  those  adulterations  whieh  are  simply 
frauds  upon  the  consumer,  or  which  are  delrimental  U>  thu  pubtic 
health:  thus  it  does  not  interfere  with  the  adulterations  of  drugs, 
nor  does  it  inlertUct  the  u.se  of  poisonous  pipncnts  in  the  crtloiiring 
of  sugar  confectionary,  &c.  Nearly  all.  therefore,  that  appeiint  to  be 
requisite  in  order  to  insure,  to  a  very  great  extent,  (he  suppression  of 
adulteration,  m  to  remodel  the  ileteetice  and  wudytical  dcpartmeuUt  nftht; 
Excise^  ami  to  enlarge  the  sphere  of  its  operntiowi.  The  atialycical 
department  should  be  made  to  take  copiisance  of  all  adultenitions, 
whether  in  duty-paying  articles  or  in  ariitl«-s  free  of  duty.  The  best 
way  would  he  either  to  plnce  the  remodelled  amdyLiral  department 
of  the  very  unpopular  Excise  under  the  Hoard  of  lleiihh,  (he  vnrious 
Customs  and  Excise  detective  inspectors  coramnnicaliiii;  with  the 
reconstituted  Board,  or  else  to  render  it  indepemlent  and  distimt. 

Some  such  change  as  that  here  recommended  is  tinperiitively  de- 
manded, and  must  ere  Inng  Uike  place.  It  is  impossible  to  allo'nr  the 
Analytical  Hoard  of  the  Excise  to  remain  much  hmgiT  in  its  present 
anomalous  and  most  iuetBcient  condition.  Xliia  change  cfTected,  the 
Board  would  lose  its  arbitrary  and  objectionable  character;  it  would 


ccasti'to  be  reg'arded  as  an  engine  for  tbe  extortion  of  money;  but 
wliile  it  really  and  eflectually  protected  the  revenue,  it  would  at  the 
some  lime  protect  the  interests  of  the  bonest  trader,  of  tbe  consumer, 
and  al«o  become  a  guardian  of  the  public  heattb. 

We  are  sorry  that  our  views  difier  so  much  from  those  expressed 
by  the  Select  Committee  of  the  House  of  Commons  on  Adulteration; 
but  we  have  felt  ourselves  constrnined  to  give  tree  expression  to 
our  opinions  on  this  ({ueatiou  which  so  closely  concerns  the  interests 
of  the  public,  and  which  are  paramount  to  nil  other  con,-iiderationfl. 
With  abundant  evidence  of  a  most  conclusive  character,  wiili  a  cose 
which  the  Committee  themnelves  acknowledge  to  be  fully  proved,  it 
must  be  confessed  that  the  Report  is  a  very  weak  and  timid  one, 
when  the  gigantic  character  of  the  evil  to  be  remedied  is  considered. 
It  would  appear  na  tliDUgh  the  Committee,  from  the  universality 
of  the  practice  'of  adulteration,  and  from  its  extensive  ramifications 
throughout  the  highest  and  the  Inwei^t  branches  of  trade,  had  become 
alarmed,  and  shrank  from  grappling  with  it  in  a  bold  and  compre- 
hensive manner.  Notwithstanding,  however,  that  the  Report  falb 
short  uf  what  is  required,  it  is  yet  a  highly  important  document,  and 
one  which  must  be  folhtwed  by  legislation.  The  grateful  thanks,  there- 
fore, of  the  public  are  fully  due  to  the  able  chairman  of  th'it  Com- 
mittee, Mr-  Scholefieid,  M.  P.,  and  bis  colleagues,  namely.  Viscount 
Ebrington,  Viscount  Goodench.  Lord  Claude  Hamilton,  Hon.  C.  P.  Vil- 
liers,  Hon.  W.  Cowper,  Mr.  Alderman  Cubitt,  Mr.  Gregson,  Mr.  Kin- 
naird,  Mr.  Knight,  Mr.  Peacocke,  Mr.  Otway,  Mr.  SwifV,  Mr.  Sheridan, 
and  Mr.  Wise.  Mr.  MofTut,  we  suppose,  was  placed  upon  the  Committee 
to  represent  the  case  of  the  adulterators.  For  two  sessions  these  mem- 
bers of  (he  Jlouse  of  Commons— uU  volunteers  for  the  duty — were 
unremitting  in  their  attendance  at  the  meetings  of  the  Committee, 
and  tbey  elicited  from  the  various  witnesses,  by  their  well-directed 
inquiries,  a  mass  uf  most  valuable  evidence,  which  cannot  but  result 
ere  long  in  a  great  public  benefit. 

Various  grounds  exist,  which  render  it  imperative  that  some 
elTective  legislation  should  promptly  be  carried  into  effect  fur  the 
suppression  of  adulteration. 

Legislation  on  the  subject  is  required — 

First.  —  For  the  Frutectiun  of  the  Public  IleuUh. — The  evidence  given 
before  the  Parliamentary  Committee  on  Adulteration  proves  that  the 

l>  3 


GENERAL   INTRODUCTION. 


deadliest  poLions  Are  daily  resorted  to  for  purposes  of  adulteration,  to 
the  injury  of  the  health,  and  the  dcstnicrion  of  the  lived,  of  thuuitandB. 
There  U  scarruly  a  paitjiiiiuuci  pig-iuyiit  kiiuwii  in  these  islaadtt  vrhich 
is  not  thus  employed. 

Second.  —  For  the  Protection  of  the  Rnenw. — Thl*  will  be  readily 
acknowledged  when  it  id  known  that  nearly  half  the  natioiml  re- 
venue is  derived  from  taxes  on  food  and  bevera;;c3.  It  has  alrendy 
been  shown  that  not  long  since  ad u Iteration  was  rife,  and  it  still  exists 
to  a  large  extent  in  nearly  all  articles  of  consumption,  both  solid  and 
fluid,  and  including  even  those  under  the  enpervisJon  of  the  Excise. 

Third.  —  In  the  Interests  nj"  the  Iloii^xt  Mcrvhaut  atul  Trader. — The 
upright  trader  is  ])lui:ed  in  a  most  trying  and  unfair  position  in  con- 
se<jiuence  of  adult(;rati«>n.  lie  is  exposed  to  the  most  ruinous  and 
unfl^'mpulous  competition;  too  often  he  is  undersold,  and  his  business 
thus  taken  from  him.  It  is  therefore  to  the  interest  of  the  honest 
trader  that  eO'eetive  legislation  should  tuko  place,  and  not  only  is  it  to 
his  interest,  but  we  can  state  that  tt  is  his  must  anxious  desire  tlmt 
adulteratii>n  should  be  aboli»hc<l.  In  advocating  the  suppression  of 
adulteraticfn,  we  arc  therefore  advocating  the  rights  and  interests  of 
all  honourable  traders. 

Fourlh. — For  the  sake  of  the  Consumer — lliat  the  consumer  U 
extensively  robbed  through  adulteration,  sometimes  of  his  hcidth,  but 
always  of  bis  money,  is  unquestionable.  It  ii>,  however,  the  poor  man, 
the  labourer,  nnd  the  artisan,  who  is  the  most  extensively  defrauded  ; 
for,  occupied  early  and  late  with  his  daily  labour,  often  in  debt  with 
those  with  whom  he  deals,  he  has  no  time  or  jjower  to  help  himself  in 
the  matter,  and  if  he  had  the  tin»e  he  still  would  require  the  requisite 
knowledge.  The  subject  of  adulteration,  therefore,  while  it  coucernfl 
all  L'lasses,  is  eminently  a  pour  nian's  {)ue&'tion ;  the  extent  to  whicli 
be  is  cheated  through  adulteration  is  re»llj  enormous. 

Fifth.  —  Oh  the  Grourul  of  PnMic  Morality.  —  Adulteration  in» 
volves  deception,  ^lishonesty,  fraud,  and  robbery,  and  since  adultera- 
tion is  so  previilent,  so  equally  must  these  vices  prevail,  to  the 
•crinna  detriment  of  public  miirality,  and  to  the  injury  of  the  cha- 
racter of  the  whole  nation,  for  probity,  in  the  eyes  of  the  world. 
Under  this  head  we  cannot  do  better  than  quote  the  langu^e  of  the 
Parliamentary  Committee  on  Adulteration.  *'Not  only,"  states  the 
Report,  "is  the  public  health  thus  exposed  to  danger*  and  pecuniary 
fraud  committed  on  tlie  whole  couimuuityt  but  the  public  morality  is 


GENERAL    INTRODUCTION.  39 

tainted,  and  <be  high  commercial  cbarncter  of  this  country  seriously 
lowerc<i,  both  at  home  and  in  the  eyes  of  foreign  countries."  We 
repeat^  then,  that  some  prompt^  active,  and  efficient  legislative 
interference  is  demanded,  for  the  snke  of  public  morality,  and  the 
character  of  this  country  amongst  the  nations  of  the  world. 


But  there  arc  yet  other  reasons  for  legislation.  It  cannot  he 
doubted  but  that,  in  makin;;  known  the  imtiue  of  the  adulterations 
practised  upon  a  variety  of  articlest  although  we  have  doterrt'd  some, 
yet  have  we  also  taught  many  the  way  to  adulterate,  and  nf  this 
knowle<ige  they  will  not  be  slow  to  avail  themselves,  especially  in  the 
absence  of  any  aulfirient  check.  The  recent  startling  and  frightful 
exposures,  although  they  have  done  good  for  a  time,  will,  if  unsup- 
ported, serre  but  to  increase  the  evil  at  some  future  day. 

A  reluctance  is  expressed  in  some  quarters  to  grapple  with  the 
giant  evil  of  adulteradon  from  the  fear  lest  it  should  interfere  with, 
ond  impose  restrictions  on,  trade.  This  fear  we  believe  to  be  ground- 
less ;  and  even  if  there  were  some  foundation  for  it,  yet  it  ought  not 
to  be  allowed  to  prevail  against  what  our  consciences  tell  us  to  be 
right.  Trade  is  one  thing,  poisoning  our  food  another.  Surely  there 
is  no  necessary  connection  between  the  two;  and  if  conne<!ted,  the 
sooner  the  connection  is  severcil  the  better  —  the  better  on  all  grounds, 
and  especially  it  will  be  to  the  advantage  of  trade  itself.  We  main- 
tain, however,  that  the  connection  which  now  exists  is  entirely  un- 
natural, that  it  has  sprung  up  under  a  careless  and  loose  state  of 
things,  and  that  it  is  the  duty  of  the  State  to  interpose  its  authority 
fur  the  prevention  of  adulteration. 

Now  it  should  be  clearly  understood  that  it  is  not  necessary  for  the 
suppression  of  adulteration  that  restrictive  measures  should  be 
resorted  to,  calculateil  to  interfere  with  trade,  or  to  impede  the 
liberty  of  the  subject,  beyond  those  already  in  existence  ;  indeed 
some  of  the  restrictions  now  in  force,  and  interference  at  present  in 
uperationt  might,  under  a  better  organisation,  be  discontinued. 

Let  us  recall  to  mind  the  powers  already  conferred  for  the  suppres- 
sion of  adulteration.  The  Excise  is  at  liberty  to  enter,  by  force,  upon 
any  premises,  where  the  adulteration  of  an  exciseable  article  is 
suspected  to  be  carried  on,  or  where  adulterated  goods  are  supposed 
to  be  deposited;  the   adulterators  or  sellers  of  adulterated  articles 

D  4 


40 


GENERAL   INTRODUCTION^ 


may  be  apprehended,  punished  by  fines,  which  are  sometimes  Tery 
heavy,  or  imprisonment ;  uU  the  aUuUernled  artltles  may  be  confis- 
cated, as  well  as  the  im[)leme«ta  emph)ycd  in  their  preparation.  The 
fioard  may  lock  up  a  manufacturer's  premises  taking  the  keys  away, 
even  when  be  in  not  practicing  adulteration,  and  it  may  control  the 
processes  of  luanufacture  therein  pursued.  Here  ia  interference 
•with  the  freedom  of  trade  and  the  liberty  of  the  subject,  with  a 
vengeance ! 

Again,  magifttrates  or  peace  officers,  by  warrant,  under  the  Rread 
Act,  may  search  any  premises  and  seize  any  ndultcratcd  Hour  or 
bread,  search  for  any  forbidden  ingredient,  inflict  the  penakios  of  tine 
and  imprisonment ;  and  lastly,  they  may  publish  the  namey  of  the 
olTonders. 

To  prevent  smuggling, — an  ofl*encB  which,  in  it&  effects  u|>on  the 
revenue,  is  allied  lo  adu!tera:ion, —  a  large  force,  armed  to  the  teeth,  Is 
stationed  all  around  the  coasts  of  these  islands:  it  may  seize  the 
smuggler,  and,  if  he  resist,  kill  him ;  or  it  may  take  his  contraband 
goods  from  him,  and,  on  cunviclion,  cast  him  into  prison.  Here, 
again,  is  interference  wJtli  the  liberty  of  the  subjert ;  and,  remember, 
in  smuggling,  the  revenue  only  is  defrauded,  and  but  little  is  thought 
of  public  health  or  morality. 

Lastly,  recall  lo  mind  the  powers  exercised,  nnd  properly  so,  in  the 
oofles  of  bad  or  diseased  meat,  and  of  short  weights  and  measures, 
which,  be  it  known,  often  go  along  with  adulteration.  In  such  cases 
there  is  the  power  of  entering  upon  suspected  premises,  of  seizing  and 
oonfiscAting  the  articles,  and  of  punishing  the  wrongdoers  by  fine  or 
imprisonment. 

It  may  be  inquired,  how  comes  it  that,  with  such  powers  of  re- 
pression, adulteration  so  prevails  ?  The  answer  is,  that  the  laws  in 
force  respecting  adulteration  are  partirU  only  in  their  operation;  that 
they  relate  only  to  certain  articles;  that  they  are  for  the  most  part 
but  seldom  enforced;  and  that  some  of  them  have  even  fallen  into 
desuetude.  AVhut  concerns  everybody,  what  is  evorybtxly's  business, 
becomes,  in  fact,  according  to  the  old  adage,  nobody's  business. 

The  cries  of  "freedom  of  trade"  and  *'  the  liberty  of  the  subject,*' 
in  connection  with  adulteration,  are  in  reality  unmeaning  termi',  used 
OS  bugbears  to  frigbten  the  timid  and  to  throw  the  public  off  their 


GENERAL   INTRODCCTlON. 


41 


^nard*     Wc  repeat,    then,   ftESTRicTtrK  m£A6URE1«   betoetd   tdobg 

Ai'READT  ISV  EXISTSHCB,  CALCULATED  EITHEB  TO  IMrSDE  TMB 
TKZEDOK  OZ  TBAD£  OE  TO  CtBTAlL  THE  J-t&liBTy  HT  TUt  TKAUES 
Ott  TUS  SCBJECTf  A&E  MOT  RE<4t[lRGE>  TOR  THE  gUPFKESSlOR  OF 
ADULT£BATION.  WlIAT  IS  DEEDED  18  AN  EFFECTIVE  SCLEHTIFIC 
OROA!fl3ATiON  FOR  THK  rUflCOVEHT  Of  ADBI,TEKAT10N,  AVU  THE 
ADEQUATE    fCTflBlIHEAT    OF   TU£    OFf&NCS. 


f 


ON    THE    31EANS     BY     WHICH     ADULTERATION 
MAY  BE  DETECTED. 


W 


Thsbb  are  two  principal  means  by  whit'li  the  discovery  of  adultera- 
tion is  efTc'Cied,  chemistry  and  tIil*  rnicrmcope. 

Cht'tiiititry  lias  betn  long  employed  for  the  detection  of  adulteration, 
and  it  was  upon  tbis  means  of  iuvestij^tiun  thut  the  earlier  observers 
almost  exclusively  relied. 

The  application  of  the  microscope  to  the  detection  of  adulteration 
is  campurativcly  new,  and  dates  chiefly  fr<im  the  penml  at  which  my 
pa{>er  on  the  Adulteration  of  Coffee  was  communicated  to  the  Hota- 
nical  Sfjciety  of  London,  that  is  from  August,  I8i0.*  This  is  certainly 
the  most  practical  and  important  use  which  has  ever  beiu  made  of 
that  imifriimeiit ;  for  by  its  means  hundreds  of  adulterations  have  beea 
discovered,  the  detection  of  which  wiis  beyond  the  power  of  L-hemiatry, 
And  which  had  previously  eluded  all  the  efforts  of  science.  The  author 
believes  that  be  may  claim  to  have  been  the  Hrst  to  employ  on  a  large 
•Cftle  the  microscope  for  the  discovery  of  lulidlersitian  ;  on  tbiis  point, 
however,  the  lanfftiage  of  others  may  be  employeil. 

"  The  Lancet/  in  reviewing  the  author's  work  on  the  AduUcmtian  of 
Food,  writes,  January,  1855  :  "  It  is  now  unnecessary  to  say  how  com- 
pletely Dr.  Uassall  dispelled  the  delusion  as  to  the  circumscription  of 
science,  and  how  he  demonstrated  that  the  microscope,  wieliled  by  the 
skilful  naturalist  and  chemist,  was  able  to  unravel  and  to  analyse  the 
coni|>onent  structures  of  substances  thnt  bid  defiance  to  the  blow- 
nipe  and  the  lest-tubc  alone.  U  is  the  jrrcat  and  orij^'inal  merit  of  Dr. 
llussall  to  hare  applied  the  microscope  to  important  uses  tn  inquiries 
of  this  nature,  and  to  have  i<hown,  by  it^  uses^  not  only  many  things 
previously  L*onsidered  impossible  to  ^luw,  but  many  things  uut  pre- 
viously suspected  to  exist." 

The  "  Quarterly  Review,"  in  an  article  on  the  same  subjeet,  remarks  : 
"  It  is  in  the  application  of  the  mioroseope  that  consists  Dr.  Hassall's 
advftotagc  over  all  previous  investigators  in  the  same  field.  The 
precision  with  which  he  is  enabled  to  state  the  results  of  his  labours 
lemves  no  appeal." — March  1855. 

The  "  Dublin  Ueview  "  remarks :  "  The  secret  of  his  succew  has 
been  that,  in  otldition  to  chemical  analysis,  he  has  used  the  microscope 
in  his  intpiiries;  and  his  merit  not  only  consists  in  the  able  manner 
in  which  he  has  employed  the  instrument,  but  in  his  being  the  first  to 
use  it  practically  and  to  such  an  extent  for  this  purpose.** 

"The  microscope,'*  writes  "The  Timca,"  t  rclerrmg  to  our  labours, 

•  Sm  "  Timrs."   Auput  8. 18&a  t  Juljr  M.  lfiS&. 


41      MEAKS    FOE  THE   DETECTIOX  OF  ADULTERATION. 


"  seems  to  have  been  the  more  cfTeclive  instrument  in  the  work.  Less 
ihun  five  years  ago  it  woulti,  we  are  told,  have  VMit'ti  inj|K)ssible  to 
detect  the  presence  of  chicory  in  t'offec.  In  iUct,  tlie  opinion  of  three 
clistin-iuisheU  ithemiiits  Wiis  actually  f|Uoletl  in  the  House  (>f  Commons 
to  that  effect ;  whereas  by  the  use  uf  th^j  niicroEiCu|ie  the  dtderencee  of 
Btructure  in  these  two  substances  can  be  promptly  disoerneti." 

Lastly,  the  following  remarks  from  the  pen  of  a  very  able  writer. 
Dr.  Robert  Barnes,  may  be  fpioted:  *' The  scientific  originulily  of 
Dr.  Hassolfs  labours  in  laying  bnrc  the  health-destroying  anrl  fraud- 
ulent adulterationa  of  fooil  and  drug»,  is,  if  {>fl89ible,  stiU  more 
inerituriuu»  ;  and  it  would  be  difficult  to  over-estimntu  the  public  im- 
]Kjrtance  of  tlie  results  obtained.  The  means  previously  relied  upon 
to  check  these  adulterations  were,  the  cumbrous  and  coiiitly  uiacluiiery 
of  the  Excise,  and  the  subsidiary  aid  which  cheiubtry  could  aOV^nl, 
The  officers  of  the  Excise  were,  for  the  most  part,  *iriven  to  seek  for 
evidence  by  forcible  entry  and  the  seizure  of  articles  found  on  sus- 
pected premises.  When  the  art  of  the  chemtat  failed,  science  was 
practically  e.thiiustcd.  So  late  aa  1851,  the  then  Chuiicellor  of  the 
£xche<[uer  was  able  to  <piote  in  the  House  of  Comtnniis,  us  the  de- 
liberate opinion  of  three  of  the  most  distin^uiif^hed  chemisUa  of  the  day, 
who  had  oeen  B[>ociaUy  recjue-sted  to  report  upon  the  subject,  'WW 
neither  by  chemistry  nor  by  any  other  meaits  amUi  the  admisture  of  chi' 
cory  with  cofffic  he  detected.'^  How  completely  lliis  foregoue  conclu-^ion 
has  been  exploded  by  the  labours  of  Or.  Hassallj  as  Analyst  of  the 
Sanitary  Commission  of  "  The  Lancet,"  is  notorious.  There  is  now 
nothing  in  Bcicncc  more  certain  and  precise  than  the  discrimination, 
by  meaus  ol'  the  microscope,  of  the  various  forms  of  vegetable  tissues,  no 
matter  to  what  extent  they  may  be  pulverised^  mixed,  or  even  roastu<i. 

"  The  interest  of  Dr.  llassairs  researches  is  universal.  They  have 
benefited  tlie  public  revenue,  every  man  in  lieaUh  or  in  sickn(!S3,  and 
the  physician  who  trusts  in  the  properties  of  the  a>;entj(,  wheth<^r  me- 
dicinal or  dietetic,  which  he  prctoribes ;  and  Ptirliamcnt  has  been  in- 
formed thn>ugh  them  of  new  grounds  ond  new  principles  of  legislation. 
The  jrreat  importance  of  the  subject  of  the  adulteration  of  food»  drink, 
and  droits,  has  already  been  recoj^nised  by  ParUament,  and  this  nminly 
tliruugb  tlie  labours  of  Dr.  Uassalt." 

Ok  tob  ApruciTiOH  or  thb  MicRoscors  to  tub  Djbtsction  of 
Adultkratiok. 

The  microscope  is  dpecially  suited  to  the  detection  of  orgnnised 
structures  or  substances,  as  the  several  part^  of  animals  and  plants :  it 
is  with  the  latter  that  we  shall  chiefly  have  to  do  In  the  course  of  the 
present  work. 

When  we  surrey  with  our  unaided  vision  any  animal  or  plant,  we 
detect  a  variety  of  evidences  of  organisation  or  structure  ;  but  there  is 
in  every  part  of  every  animal  or  vejietable  production  an  extra- 
ordiuary   amount  of  organisation,   wholly  invisible  to  the  unarmed 


BT   THE   MICROSCOPE. 


49 


xu 


»ic:hl,  and  which  19  revcnied  only  to  the  powers  of  the  mtcrofcope. 
Nuw  this  ininuto  »n*l  microKopieal  or^uuisation  is  diifL'rcnt  in  dii- 
f^rent  ]Mirts  of  the  same  animal  or  plant,  ami  different  in  iHHerent 
animals  and  plants,  so  that  by  means  of  these  tlifi'eriMices,  rightly 
understood^  the  ex[)urit'nced  microscopic  id  observer  is  enabled  to 
identify  in  many  castas  infinitely  minute  portions  of  iininiid  or  vi^yetable 
tiruiues,  and  to  rvft*r  them  to  the  pjirt.i  »ir  snet-ies  to  which  they  belong. 

Thus,  by  raeaiH  of  the  nuo-rosco|>e,  one  Icinil  of  root,  stem,  or  leaf 
may  trcnerally  be  di:§tingui<^hed  from  another,  one  kind  of  starch  or 
Hour  troni  unother,  one  seed  from  unuiher,  und  so  on.  In  thid  wuy^ 
the  microscope  becomes  an  iuvaluable  and  indispcuttuble  aid  in  the 
discovery  of  adulteration. 

Applying  the  microscope  to  food,  it  appears  that  there  ia  scarcely  a 
vegetable  nrticle  of  consumption,  not  a  liquid,  which  may  not  be 
distin^^iished  by  means  of  that  instrument.  Further,  thnt  all  thtwe 
adultiTutions  of  these  articles  wliich  consist  in  the  addition  of  other 
vegetable  substjinees,  and  which  ciKistitutc  by  fur  the  muiority 
of  udulteratioas  practiaed,  may  likewise  be  discovered  and  discri- 
mirmted  by  the  same  means. 

Tlio  same  remarks  applv  to  all  the  vegetable  drugs,  wliether  roots, 
barks  »et?d«,  or  leaves.     \Ve  are  not  acquainted  with  one  such  drug 
iuch  may  not  be  thus  di<|(i^i.'^ui^)K'tl. 

JTbe  seeds  even  hclonf;inji  to  dilferent  species  of  the  same  genus 
*iBty  fn-quently  be  distinirui^ticd  fmrn  each  other  by  the  mii'r<isrope, 
ajKiint  in  some  cases  of  very  great  importance.  A  remarkable  instance 
of  this  has  fallen  under  our  observation.  The  SGe<ls  of  the  dilferent 
8|)eciL^  of  mustjinl,  rape,  &c.  may  all  be  diijtinguiahed  under  the  nii- 
crtiecojM}  by  difi'ercnces  in  their  organisation.  To  hhuw  the  im- 
fHtrtance  of  the  discrimination  in  »ome  cases,  the  following  instance 
may  be  cited.  Some  cattle  were  fe<l  with  rape  cake,  and  died  with 
symptoms  of  inllammati4in  of  the  stomach  and  bowels.  Nothing 
of  u  poisonous  nature  could  be  detected  on  anal  vsls ;  but  it  was  sus- 
pected that  the  cake  might  be  adulterated  with  mustard  husk, 
altliough  even  this  point  could  not  be  clearly  established  by  chemical 
research.  Under  tiiese  circumstances  the  cake  w:ih  sent  to  the  author 
ibr  examination,  wito  had  but  little  dilTicully  in  a^*ertaining  that  it 
was  adulterated  with  mustard  seed,  which,  from  tbe  large  quiintity 
consumed,  was  doubtless  the  cause  of  the  fatal  inflammation.  Not 
only  can  the  seeds  of  different  plants  of  the  same  genus  l>e  frcnnentlj 
discriminated  by  the  microscope,  but  in  some  cases  those  belonging 
even  to  mere  mhetiet  of  species. 

The  microscope  in  some  cHBes  can  even  inform  us  of  the  processes  or 
affente  to  which  certain  vegetable  Mibalances  have  been  sulyected. 
llIu.^trations  of  this  are  aflorded  by  the  starches  of  wheat  and  barley  : 
it  can  be  determineil  by  the  microscope  whether  these  are  ruu\  btiked^ 
nr  hitUed^  or  whether  uuilted  or  nnmuUefl.  Illustrative  figures  will  be 
found  in  the  articles  on  Urb\d  and  Bbkb. 

Again  it  is  not  only  when  the  articles  are  in  a  separate  state  that 


46      MEANS  FOE  THE   DETECTION   OF   ADULTERATION. 


they  can  be  thus  distinjruishetl  i  but  even  when  ;nixed  tngelher  in 
difforent  proportions.  We  have  8ucc*;e»led  in  det-cetiniy  in  certain 
TegelAblc  powders  no  loss  than  nine  different  vegetable  prwluciions. 

So  great  and  mnniloitt  itre  the  difTerenoes  ri^vealed  by  ihc  micro- 
scope in  different  vegetable  substances,  tbaU  with  ordinary  care  and 
some  uinuiint «}!' preliminary  knowledge,  the  discriniinution  become!  a 
mutter  ut'die  ;;reutesi  enise  and  the  mo^t  abaulute  cerluinty. 

This  will  appear  even  from  an  examination  of  the  fivefoUowingfigures. 

Fig.  1. 


^^-S-" 

^^^^/i:? 


Scebon  of  tTtrioiircp  Corrn  BmKr,  •howEng  the  aUr  *oA  form  or  thi  ctUi,  u  viTl 
u  tlir  drop*  (if  oil  contained  wIlhlD  llieir  <»vUm«.  Ormvii  vUh  the  Cuoer*  LueklA, 
and  fRBcnlfled  14ll  diameten. 

The  abovefigure  represents  a  section  or  fragment  of  the  unroasted  coffee 
berry:  if  the  reader  will  contrast  this  with  the  next  figure,  which  repre- 
sents a  small  fragment  of  chicory  root,  he  will  perceive  how  great  is  the 
difference ;  so  with  the  starch  granules  of  the  difiercnt  arrowroots  ;  of 
wheat,  rye,  rice  and  Indian  corn  Hours ;  with  jiitap  and  rhubarb ;  and 
with  a  variety,  we  might  say  ahost,ofotherfnjb3tanees.  Now  chemistry 
could  not  fiirni.thuswith  the  nameof  even  one  of  these  different  starches. 
Further,  wonderful  to  relate,  the  grinding  and  pulverisation,  and 
even  the  charring,  of  many  vegetable  siibstanceB,  does  not  so  destroy 
their  structure  as  to  render  their  identification  by  the  microscope  im- 
possible. Chicory  and  coffee  may  be  thus  roneti'd  niul  pulverised,  and 
vet  each  may  be  subsequently  identified  with  the  grreateat  case,  they 
being  in  fact  but  little  changed,  except  in  colour,  and  in  the  case  of 
coffee  by  the  dispersion  of  the  droplets  of  oil  visible  in  the  cells  of  the 
unroosled  berry. 


BY   THE   MICROSCOPE. 


47 


Again,  lubsUnces  may  be  discoTcred  bj  meana  of  the  microfioopc, 

rhen  introduced  into  arliclcii  for  the  purpose  of  adulteration  in 

Ltremeljr  minute  qnantities  :  the  case  of  soine  njustard  forwarrled  by  n 

lufiu^turer  to  "The  Lancet'*  «ome  time  since  furniebed  a  remarkable 

lastrftlion  in  point. 

Fig.  2. 


% 


Ttwtmmmt  of  Kaamo  Cnicort  Root,  Ukvn  from  ■  Mmple  of  ftdiiltcnUd 
mSm»,  ilMwIiic  Uifl    or/J«   vt   whkh   It  li   prindpsltr   convlltutcd. 
Dr»vii  vtth  the  C«aiCTm  Lucldi,  uid  ina<iilfic«l  l«l  dkmoUrn. 

TVe  nrastAfd  was  atnteil  tobe  j^enuine  ;  hut  on  examination  with  the 
inier«KOpe»  it  was  found  to  contain  a  small  (luanlity  of  turraeric.  The 
manufacturer,  when  informed  of  the  fact,  Tcry  candidly  and  properly 
■cknnwledged  that  thia  was  the  case,  and  stntcd  that  he  had  added  '^  tjcif 
KnatttMi^  (vrmeric  tt>  Jifty-six  pouiuh  of  seeds,  not  for  the  purpnse  of 
;.'.iin  or  adulteration^  but  simjdy  to  enliven  the  colour  and  mnke  its 
^['pcarance  more  acceptable;  "  that  is,  the  (piantity  of  tuniiuric  present, 
am)  discovered  by  the  microscope,  consisted  of  only  one  part  in  448  of 
thcquantity  examined.* 

Tbe  Ust  illustration — and  a  very  sfrikin;;  and  beautiful  one  it  is^  al- 
tJxMi^  not  immediatelr  coaneeled  wiih  the  subject  of  adulteration, — 
vhicn  we  shall  adduce  m  order  to  show  the  oxtruonlinary  character  of 
liic  information  furnished  in  somu  cases  by  tbe  microscope  is  supplied 
by  honey. 

*  Food  1114  111  AUultvraUooi.  p.  IX). 


48     MEANS   FOR  THE   DETECTION  OF   ADULTEKATION* 


Honey  is  the  saccharine  exudation  from  the  nectaries  of  flowers :  the 
bees  in  collecting  iL  carry  away  some  of  the  pollen  of  the  flowers 
visited  by  them.    Now  tliis  pollen  consists  of  cells  or  vesicles,  difTering 

Fif.  X 


Slarvh  franulM  nr  MkR^KTA,  cmll«d  commonly  W«^  Indltn  ftrromoot. 


I>r«vn  «hh  llw  Ostnuk  LwciiU,  wmI  i 


iW  lUuiietcr*.  , 


in  size,  form,  and  slruclure,  nccordinp  ti>  ihe  plaiita  from  which  it  is 
derived,  rcrtuiii  plants  being  chanicterisud  by  polJeii  [•nitiulL'?  of  a  cer- 
tiiin  eunfigiirttiinn  and  organisation.  Hy  the  pnlteii  jiresent  in  honey, 
therefore,  ihc  scientific  microscopist  acquainted  wiili  thv  fhuracter- 
istics  of  the  pollen  of  different  plants  Is  enabled  to  decide  In  many  in- 
stances upon  the  nature  of  the  plants  from  whirli  the  honey  has  beoQ 
procured,  and  whether  it  has  been  collected  from  the  llowersof  the  field, 
the  garden,  the  beathf  or  the  mountain.  See  article  Honet  for  figure 
inilluBtrutiim. 

There  is  still  another  use  to  which  the  microscope  may  be  applied 
in  the  detection  of  a<)ulteration  ;  it  may  frequently  be  made  to  serve 
8fl  an  auxiliary  to  ehemiciil  researches  :  tbu!*,  for  example,  when 
we  want  to  owertain  whether  any  (tubstance  contains  starch,  carbo- 
nates, phosphuti'S  &c^  it  is  often  the  quickest  and  most  c»»rtnin  way  to 
apply  the  reit^icnts  to  a  small  quautity  of  the  substance  while  this 
is  under  the  field  of  vision  of  the  microscope. 

Wh&t  the  microscope  is  capable  of  cO'ccting  in  the  discovery  of 


d 


BT   THE   MICHOSCOrE. 


49 


lulturation  having  been  thus  explained,  the  mode  of  the  applica* 
~  vf  thai  instmmenl  to  the  subject  may  next  be  considered. 


•nuwroPti  oofiunnDly  ib-tinnilnBt4>l  Rut  rndlKO  ftrrovTOoL 
Qunafa  I.uclJa,  uid  nu4[uilSwJ  'IM)  dlamclen. 

ll  wAold  be  out  of  place  to  ^ve  any  description  in  this  work  of  the 
npon  which  ihe  microscope  lias  been  constructed;  the  most 
nopk' details  on  thiii  subject  are  to  be  found  in  the  Bevertil  works 
which  treat  of  the  tncchuuiitm  of  the  mifToscope.  It  will  he  suOioient 
thit  tiiv  titles  »f  Booie  of  these  works  should  be  indicated,  as  thoso 
gitefi  Inflow. 

"The  Microscope,    its  Ilistory,   Construction,  and  Appllpationa." 
Bj  J>»-*7  Ho^ir.  I.:,(i.,  M.  U.  C.  S.      Price  7«.  6^/.    Uoutledge  &  Co. 
"  Tl       '  -pe;'     By  Dr.  Beale.     John  Chnrohill. 

**A  i  1  rtiatise  on  the  Microscope."  By  Prof,  tiuekctt.  Price 

31#.     ii  ,  Rcjient  Street. 

Ic  i-  however,  that  a  few  remarks  should  be  nmde  upon 

Tpry  iiin>"r  uiiit  subject  of  tite  cost  of  amicroscu[>e  suitable  for  the 
fury  ol  ftdidteranon. 
The  co*t  of  a  microscope  suitable  for  the  purpose  varies  much  ac- 


50  MEANS  FOB  THE  DETECTION  OF  ADDLTEEATION. 


cording  to  the  makers  tlic  charncter  nf  the  stant],  antl  the  nnturfi  nnd 
number  of  the  object- glasses  or  powers  with  which  it  is  furnished. 


Fit.b. 


I 


Potato  Mnomro&L.  oommflnly  eancrf  BrItUh  mmmmol.     Drawn  with 
the  Cuncrm  Liidda.  mnd  in*ctilfled  9fO  dUoMten. 

If  supplied  with  French  or  German  achromatic  object-glasses,  it  may 
be  put  down  at  about  I  Of. 

M.  Pillischcr,  of  New  Bond  Street,  supplies  a  Stud^jiU^  or  Medical 
miertarope^  suiBcient  for  oriliaary  purposes,  for  7/.  7».  It  consists 
of  microsoopG  stand  complete^  but  wiihuut  etage  movcmenta,  quarter 
and  inch  object-plasseB,  one  eye-piece,  and  mahogftny  case. 

Mr.  Maker,  of  lligh  llolborn.  stifipliea  Studentji  microscopes  suitable 
for  nhyHiulo^icnl  purposes,  and  furnitihed  with  cuac*  and  three  achro- 
matic powers,  1-inch,  I*, and  ^-incb,  for 4/.  Ijx.and  5i.  \5x.  each.  The 
objcct-glawcs  may  als«>  be  purehiised  separately  of  Mr  Baker. 

The  Sticiety  of  Arts  prize  microscojH',  manufacluri'd  by  R.  Field 
and  Son,  of  113.  New  Street,  Birniingbara,  is  furni.shcd  with  case, 
two  cjc-pieces,  and  two  object-glasses,  at  a  cost  of  Si,  ^.  This  in- 
stnimciit  we  have  not  seen. 

Binilh  and  Beck's  Educational  microscope  consists  of  two  object- 
fflasses^the  l-inch  and  J-iucU;  two  eyc-piecws;  a  firm  stand,  with  a  joint 
for  varying  the  position,  quick  and  slow  motions  to  the  body ;  a  stage 


1 


Br   THE  MICROSCOPE. 


51 


^ 


with  springs  that  allow  any  motion  to  he  p^ven  to  the  object ;  concaTe 
mirror  ;  a  aide  condensing  tens ;  forceps,  glass  plutcis  ph'ers  :  all  packed 
in  mahogany  cose.    Its  coeit  is  lU/,    Address,  6.  Coleman  Street,  City. 

Messrs.  Powell  and  Lealand  turniffh,  for  13/.  IJji.,  an  instrument  of 
the  followin<j:  description.  It  has  n  very  firm  triptHi  »tun<],  willi  euarse 
adjiistment  by  rack  and  pinion  ;  two  eye-pieces  ;  two  object-jxlussea, 
naiuelr,  J- and  1-inch  ;  iliapliragm  nnd  gtnps  :  the  whole  packed  in  ma- 
hogany case.  For  2/.  2j?.  more  tlie  jj-inch  object-glass  may  be  sutjsti- 
tuted  for  the  inch.  Addres.s,  4.  Seymour  iMuce,  New  Knad.  The 
fflas?^  supplied  by  Messrs.  Smith  and  Beck,  and  Muisrs.  FowcU  and 
Lealand,  arc  English  made. 

It  does  not  appear  that  Mr.  Ross  manufactures  any  cheap  microscope 
suitable  fur  Xhv  purpose. 

A  very  excellent  and  cheap  microscope  stand,  which  we  are  much  in 
the  habit  of  recommending,  is  made  by  \Ir.  Byle^  of  9G.  St.  John 
Street  Uoarl.  It  has  tbe  double  stage  movemcnLs,  the  advantage  of 
which  is  very  great,  a  fine  adjustmcnc,  and  an  excellent  mirror,  and  is 
remarkably  cheap  at  61.  3s.  For  2/.  7jr.  miire,  two  verj  good  German 
achromstic  glasses  may  be  procured  of  Air.  linker,  namely,  tbe  ^ 
and  |-inch.  This  microscope  is  very  well  suited  for  the  detectiou 
of  adulteration. 

It  is  desiruble,  although  not  nbsoltitely  necessary,  that  wlmtever 
microscope  may  be  purchafleil  shouli)  be  furnishtKi  with  a  polari.vope, 
as  this  will  be  found  extremely  useful  in  the  discriniinatioii  of  some  of 
the  starches. 

The  object-glasses  most  useful  for  tlie  detection  of  aduUeralion  arc 
the  |-  and  |-inch  glasses ;  it  is  not  very  often  that  the  ^-iiich  gla.^  is 
require<i,  oJthough  it  is  necessary  in  some  cases,  as  in  the  exa* 
mination  of  the  smaller  sfarcb  granules,  as  those  of  rice,  liquorice,  &c. 

For  different  objects  different  magnifying  powers  are  requisite. 
What  these  should  be  may  l>e  ascertaintd  in  gL-neral  by  reference  to 
ihc  descriptions  attached  to  the  various  cngrarings  scattered  through- 
out the  work.  It  is  well  to  accustom  oneself  as  far  as  possible  t4>  the 
examination  of  objects  with  tbe  same  glasses,  as  in  this  way  different 
objects  may  be  more  readily  eompared  the  one  with  the  other. 

The  examination  of  objects  is  in  some  ca^es  facilitated  by  employing 
in  the  first  instance  an  object-glass  of  low  magnifying  power,  as  the 
)-incb  or  ^-incli,  and  subsequently  having  recourse  to  a  higher 
power  to  nmke  out  the  details. 

It  is  desirable  oUaq  thnt  tbe  microscope  used  should  be  provided 
with  two  or  three  eye-pieces,  as  by  this  means  we  are  furnished  with 
intermediate  ranges  of  niaj;nirying  powers. 

The  maker  supplying  tlie  instrument  should  always  furnish  a  printed 
table  fltatinc  the  nnmlwrof  diameters  which  each  object-glass  and  eye- 
piece mngnifies.  The  following  table  shows  the  extent  to  which  the 
different  object- glasses  and  eye-pieces  are  usually  made  to  magnify.  It 
Applies  more  particularly  to  the  glasses  manufactured  by  Mr.  Koss. 

K  3 


52      MEANS  FOR   THE   DETECTION  OF   ADULTERATION. 


Bfc-flauM. 

ObI«t.gI»*i«. 

Un. 

l-in. 

i-lB. 

Kn. 

l-to. 

*-ln 

A. 

B. 
C. 

Value     or 
each  Kpac« 
in  the  mi- 
crOBJetcr 
cye-glflfia 
with       the 
Tfthoasofa- 
ject-ghiM.. 

\ 

60 
80 

too 

■IHHU31 

100 
130 
160 

■0005303 

230 

350 
SOO 

■0002325 

-I20 

670 
900 

•oooiiu 

In  mlditinu  to  ihe  niicroscope,  it  Is  Dccessor^  thnt  the  observer 
filiouhl  bf  furnidbeil  willi  ^lass  slides,  celU,  and  thin^luAs  covers,  with 
mouiituU  iieeillLfsi,  and  also,  it"  be  dt.'«>irc8  to  preserve  p-erm;im:)iUy  any 
of  ibe  objtTts  ht>  moeLs  with,  with  a  preserving  fluid,  ami  with  a 
cement  Ui  secure  the  ctlla  and  covers.  The  cells,  slides,  and  covers, 
may  be  ohtuined  of  most  inicroscftpe  niakci-s,  of  Air.  Bilker,  Itullxtrn, 
or  of  Mr.  Bender,  0.  Brunswick  Places  Ciiy  Koad. 

Several  Jiuids  are  used  for  the  «xLibitiou  and  prcserv'ntion  of 
microseupic  objects. 

One  ot  these  is  Canada  1}a1snm,  diluted  wJth  turpentine  to  sucb  a 
consistency  as  to  allow  of  its  droppio;;  readily  from  a  pencil. 

Mr.  Deane  rei-ommends  the  ffiUowing  conipoKitinn  for  preaerving 
dry  or  moist  animal  or  vegetable  Bubstonces :— Of  White's  patent  sixe 
or  gelatine  6  ounces  by  weight,  boiiejr  9  ounces,  n  little  spirits  of  wine, 
and  a  few  drops  of  creosote  ;  mix  and  fdli^r  whilst  hot, 

Another  composition  Is  thus  nnule  :  — Pure  glycerine  4  iluldounces, 
distilled  water  2  ounces,  j^elutlne  1  ounce  by  weight ;  dissolve  the 
gelatine  in  the  water  made  hot,  then  add  the  glycerine  and  uze. 

Or  pure  glycerine  only  may  be  used. 

The  glycerine  may  alao  be  used  with  the  addition,  when  desirable, 
of  salt,  corrosive  sublimate,  creosote,  or  i?pirit. 

Other  preserving  Uuids  are  weak  spirits  and  wator;  creosote  and 
water,  in  the  proportion  of  a  drop  or  two  of  the  former  to  6  oz.  of 
water  ;  or  creosote,  a  little  spirit  and  water. 

A  very  useful  iluid  fi>r  mounting  cryytals  of  salts  ts  castor  oil, 
first  recommeniled  by  Mr.  Waringlon. 

The  following  are  the  receipts  for  the  well-known  snlutions  of 
Goadby.    No.  1.  Hay  salt  4  oz.,  alum  2  oz.,  corrosive  sublimate  *2  grs., 


BT  THE  MICBOSCOFE. 


53 


^ 


boiling  wntcr,  I  quart;  mix.  No.  2.  The  proportionH  of  salt  and 
alum  are  the  same,  but  the  quantities  of  corrosive  sublimate  and  water 
art!  doubled. 

Professor Queketfe  preservative  fluid  j»  nimle  ol'creosote  1  ^drachms, 
wood  naphtha  2  oz^  distilled  water  32  oz.,  chalk  hs  much  as  h  required 
to  make  the  creosote  and  naphtha  into  apuste  ;  before  arlding  llie  water 
the  solution  is  allowed  to  i^tjind  tor  a  day  or  two,  and  h  then  fdtcred  ; 
two  small  lumps  of  camnbur  are  ihon  added,  and  oAcr  the  lapse  of  a 
week  the  solution  is  aurain  filtore<],  when  it  is  ready  fur  use. 

Of  the  several  sulutiuns  rmtntfdi,  none  are  so  ^<>*^  f(>r  the  preservation 
of  most  vegetable  preparatiuiis  nn  those  containing  glycerine  or  gelutine, 
either  separately  or  combined.  One  advantage  of  p;lycerine  is  that  it 
is  not  so  hi^fhly  refractive  as  Canada  biilsam,  and  another  that  moist 
objects  may  be  put  up  in  it  without  any  previous  drying. 

The  next  best  is  perhapa  Quekett's  preservative  fluid. 

There  are  aUo  several  cemejiti  employed  for  closing  the  cells :  one  of 
these  is  shelMac  varniRh  ;  this  is  usually  made  by  (iissolvinr>  black 
sealing-wax  in  rcctiticd  npirit:  it  is  best  prepared,  however,  from  the 
shelldoc  itself.  Two  or  tliree  coatings  or  layers  of  this  varnish  should 
be  used,  applied  in  succession  as  the  previous  coating  bos  become 
dry.    It  is  not  acted  upon  by  weak  spirit. 

Another  cement  is  ^nld  sire. 

Gum-copal  disjiolved  in  nil  of  lavender  also  furnishes  a  useful  cement. 

Marine  glue,  much  used  for  cementing  the  cells  to  the  glass  slideSf 
coDsisis  of  equal  parts  of  shcU-lac  antl  India-rubber,  dissolved  in  coal  or 
mineral  napuiho,  the  solution  b\.'iii;jr  irurefully  mixed  aflerwiirdi  by 
means  of  best.  It  may  bu  rendered  thinner  by  the  addition  of  more 
uaphlhu,  snd  when  bard  it  is  readily  disserved  by  naphtha  or  ether. 
This  is  the  cement  used  by  Goadby. 

The  cement  employed  hv  Mr.  Quekett  for  deep  ce\U  U  made  by 
melting  together  2  ok.  of  black  resin,  I  oz.  of  bees-wax,  and  1  oz.  of 
vermilion. 

Mr.  C  Brooke's  cement  consists  of  Brunswick  black,  to  which  a  little 
lodia-rubber  dissolved  in  mineral  naphtha  has  been  added. 

Mr.  llelt  makcH  usv  of  dark-coloured  and  old  jupanners*  size,  for 
•ecuring  the  upper  thin  gla.-'s  covers,  and  marine  glue  for  the  cells. 

In  using  the  cements  care  should  be  Utkvn  to  select  tliose  which  do 
not  exhibit  any  atHnity  for  the  preserving  fluid  c<mtaine<l  in  thecfUs : 
tlius  no  resinous  cement  should  be  employed  when  the  contained  fluid 
is  spirituous. 

For  securing  the  gloss  cells  to  the  slides  marine  glue  is  a  good 
cement,  and  shell-lac  varnish  for  closing  tlie  edges  of  the  covers,  where 
glycerine  or  casUir  oil  is  used. 

For  more  det.ailcd  practical  instructions  in  the  mounting  and  pre- 
scn'aiion  of  niicroscopic  object,s,  the  reader  is  referred  to  the  excelleut 
work  by  Mr.  Hogg,  the  title  of  which  is  given  on  page  49. 

The  various  vegetable  articles  employed  cither  as  food  or  medicines, 

Z  3 


34      MEAKS  FOK   THE  DETECTION  OP  ADULTEBATIOK. 


as  well  ail  the  iubstanccs  used  for  their  adulteration,  are  moatly  put 
up  in  some  jircscrving  fluid ;  and  in  general,  as  tbey  consist  citticr  of 
thin  sections  or  6ne  powdeni,  celU  are  not  required.  All  thnt  is  in 
generui  re<.iui»ite  lA  to  deposit  tbe  section  or  a  luinute  portion  of  tbe 
powder,  taking  care  to  dilTu^e  it  cquoJly,  in  a  drop  of  tbe  li<{uid 
placed  in  tbe  middle  of  tbe  glass  slide ;  to  cover  tbis  with  a  square 
or  circle  of  ibin  f^lass,  observing;  tbat  no  air  lies  beneath  it ;  to  remove 
tbe  superMuoua  moisture  around  the  edge«  of  tbe  glass  with  blotting 
paper,  and  when  quite  dry  to  apply  the  cement  by  means  of  a  iine- 
pointud  brusb. 

The  inmle  orprcpariti<x  the  objects  for  examination  with  the  micro- 
8C(y:>e  may  next  be  considered. 

Before  proceeding  to  the  examination  of  any  article  with  a  view  to 
discover  wbetber  it  is  ndulterated  or  not,  it  is  necessary  to  acquaint 
ourselveii  thf)rougbly  with  the  appearance  and  structure  of  the  article 
itself.  If  thl8  be  in  tbe  state  of  powder,  a^  tbe  different  kinds  of  flour 
and  arrowroot,  notbing  more  is  necessary  than  to  place  a  very  minute 
portion  of  it  upon  Jhe  gbk*s  slide,  to  add  a  drop  or  two  of  water,  dif- 
fusing the  powder  evenly  through  it  in  u  layer  so  tbin  that  tbe  light 
easily  passes  Llirougli  it,  to  \;ovcr  the  object  witli  one  of  tbe  thin  glass 
covers,  and  to  place  it  in  u  proper  position  under  tbe  micro^cupe  for 
observHtioQ,  If  tbe  vegetable  substance  be  a  solid  one.  aa  a  root,  stem, 
or  seed,  tlien  it  is  necessary  to  make  some  thin  secrinns  of  it,  deter- 
mining the  structure  from  these.  These  Fcctions  are  best  prepared  by 
means  of  a  sharp  and  thin-backed  razor  :  of  these  sections  some  should 
be  longitudinal,  others  transveriie,  and  others  should  embrace  tbe  sur- 
faces of  tbe  object,  both  external  and  internal,  where  tbe  latter 
exists.  The  exatuinutiou  is  fucilitiited  in  sinne  cases  by  tearing  some 
of  tbe  sections  in  pieces  with  neeiUes  and  also  by  examining  them 
in  glycerine  in  place  of  water,  this  renderinjr  the  structure  more 
distinct.  Lastly,  where  the  article  is  one  employed  in  the  form  of 
powder,  it  is  necessary  to  prepare  sonic  of  the  genuine  powder,  and 
to  moke  ourselves  familiar  with  its  structural  churucterislics. 

Having  progressed  thus  far  in  the  examination  of  the  article.,  we  are 
in  apoeiiion  to  strrutinise  samples  ofii,  with  a  view  to  the  detection  of 
adulteration.  Knowing  well  the  structures  wbiuh  ore  met  with  in  the 
genuine  article,  we  shall  exjjtiriencc  but  little  difhculty  in  determining 
whether  the  sample  contains  any  foreign  or  extraneous  vegetable  sub- 
stance, or  consists  entirely  of  the  one  article. 

Having  determined  thnt  it  docs  contain  such  foreign  substance, 
the  next  thing  is  to  endeavour  to  ascertain  the  nature  of  this,  an<l  to 
refer  it  to  the  jilant  or  substance  to  which  it  belongs.  The  faciliij 
with  which  this  is  done  depends  upun  the  extent  of  our  acquaintance 
with  other  vegetable  substances.  If  this  be  considerable,  a  glance  is 
oilen  sullicient  to  determine  this  point. 

However,  it  is  not  requisite  in  oM  cases  that  we  should  posseu 
a  knowledge  of  the  structure  and  appearances  presented  by  any  very 


I 


BY  CHEMISXaY- 


&6 


I 


great  number  of  vegetable  prMluctions,  since  a  few  articles  are  con* 
stantly  emploveil  for  adullerauon  in  the  oaac  of  very  many  and  widely 
dlficrent  artides,  such  as  wheat  flour,  (wtato  starcb,  sapo  powder,  rice, 
&C. ;  and  all  that  is  necessary  in  such  cases  is  that  we  should  be  ablo  to 
recognise  these  substances  when  we  meet  with  tbem. 

Most  Tegetiible  substances  are  made  up  of  certain  structures  and 
element?,  as  cellular  tissue,  woody  rthre,  vessels,  statx-h  ij^anides,  &c. 
In  leaves  we  liAve  stomata  and  often  hair-like  appDndage<<,  and  in  needs 
there  are  two  or  more  membranes.  In  endeavouring  to  discriminiite 
between  difTcrcnt  vegetable  substances,  wo  must  examine  and  com- 
pare mnst  carefully  these  several  tistfues  and  structure^!  the  one  with 
the  other.  We  must  compare,  UmIx  for  size  and  structure^  the  cellular 
tissue  of  one  vegetable  substance  with  that  of  anotheri  and  the  same 
with  the  woody  fibre,  the  vessels,  tbe  starch,  &c. 

Before  proceeding  to  determine  the  minute  structure  of  any  vej^e- 
tablc  substance  by  means  of  the  microscoi)c,  we  would  Ktron^ly  re- 
commcni]  the  observer  to  look  over  some  work  on  Structural  Botany, 
and  thus  to  become  acquainted  with  the  cbarnuteri sties  of  the  principal 
tissues  and  elements  which  enter  intu  tbe  orgtinisution  of  ihu  several 
component  parts  of  ve*;etabie».  He  uliouM  iiutiuoint  hiuHt'll  with  the 
characters  and  structure  of  cellular  tissue,  woody  tibre,  va&oulur  tissue, 
sclerous  tissue,  of  starch  granules,  with  the  general  structure  of 
roots  and  stems,  leaves,  Itowers  iiu'ludinr;  the  pollen,  and  particu- 
larly with  seeds.  He  will  finil  a  liille  preliminary  study  of  vegetable 
anatomy  facilitate  ^^reatly  his  sub^erjuent  and  more  special  inquiries. 

Any  of  the  following  works  will  be  found  suitable  for  this  purpose. 

"Outlines  of  Structural  and  Physiological  Botany/*  I'rice  10«.  6d, 
By  A.  Henfrey.    Van  VoorsL 

"Descriptive  and  Physiological  Botany."  Lardner's  " CyclupiBdia." 
By  Prof.  Henslow.     Longmans  &  On,. 

Scbleiden's  "  Principles  of  Scienlitic  Botany.**  By  Lancaster.  Long- 
mans &  Co, 

Balfour's  "  Structural  and  Physiological  Botany.'*  Price  U,  lis.  6J. 
Loogmons  &  Co. 


Ok  the  Afpucatiok  or  Chemistbt  to  thb  Dbtectiok  or 

Adultebatioit. 

Chemistry  is  adapted  particularly  for  the  <letection  of  tbe  various 
chemical  substances  and  salts  used  for  adulteration  :  the  microscope, 
on  the  other  hand,  as  has  been  already  state<l,  is  specially  suited  to  the 
detection  of  all  organised  structures  and  substances,  whether  animal 
or  Tcgctabie.  Xow  it  is  precisely  in  this  branch  of  investigation  that 
chemistry  fails  to  afford  us  any  considerable  aid. 

Chemistry  can  tell  us  whether  starch  is  present  in  any  substance, 
but  it  is  very  seldom  indeed  that  it  can  furnish  us,  as  the  microscope 
90  constantly  does,  with  the  name  of  tbe  plant  from  which  tbe  starch 

E   4 


56      MEA>-8   FOR   THE   DETECTION  OF   ADULTERATION. 

was  derived  :  it  pan  indeed  olfto  moke  ii<  arqiiflinted  with  the  fact  that 
womly  fibre  is  contnined  in  any  porticulariirtide,  but  it  cannot  furnish 
Ufl  with  the  name  of  the  tree  or  plant  of  which  it  forme*!  a  constituent. 

Another  great  advantage  of  the  niicroscope  over  chemistry  is  the 
greater  ppee'l  with  whicli  results  may  be  arrived  at.  JIany  chemicftl 
analyses  occupy  days^  while  most  microscopical  examinations  may  be 
made  by  the  practise*!  observer  in  the  course  of  a  few  minutes.  With 
the  author's  present  knowledge,  there  are  but  few  articles  of  which  ho 
could  not  examine  readily  100  samples  per  week. 

Nevertheless,  the  information  supJ^lied  by  chemistry  in  connection 
with  adulteration  is  of  the  hi;;he»t  miportance,  and  it  is  impossible 
ncoeasfully  to  study  the  subject  of  adulteration  without  having  re- 
course const&ntly  both  to  the  microscope  and  chemistry. 

The  importance  of  chemistry »  as  npplied  to  the  discovery  of  adul* 
terAtion.  is  shown  by  the  fnrt  that  the  majority  of  the  substances  in- 
jurious to  health  employed  for  adulteration  can  be  detected  with 
certainty  only  by  chemical  methods  of  research. 

It  will  perhaps  save  los>s  of  time  hereafter,  prevent  disappointment, 
find  remove  soinediflicultiett  which  muy  lie  in  the  wiiy  of  the  beginner, 
if  we  now  make  a  few  observations  on  the  chemical  apnaratus  re<iuired 
iur  the  detection  of  adulteration,  aud  on  certain  chemical  operations  or 
prooeMea  constantly  employed. 

On  the  Chemical  Apparatus  required. 

It  is  not  necessary  that  the  manner  in  which  the  laboratorj'  should 
be  fitted  up  should  be  described  ;  this  of  coursemust  be  suppfied  with 
both  gas  nnd  water,  with  benches  and  tables,  the  gas  must  be  Liid  on 
At  difl'erent  points,  and  the  jeta  provided  with  burners  of  different 
kinds. 

Chemical  analysis  is  of  two  kinds,  qualitative  and  quantitative ;  the 
object  of  tlie  iir^t,  as  the  name  implies,  is  to  ascertain  the  nature  of 
the  several  comjMment  parts  of  any  given  compound  ;  that  of  tfaesecond 
ia  to  determine  the  prufiortions  or  quantities  of  such  comjwnents. 

The  operations  of  quallt.'itive  chenneal  analysis  are  easier  and  oc- 
onny  leas  time  than  thoHC  of  quantitative  analysis;  and  in  many  cases 
it  18  aufficicmt  for  our  pur[)OHe  to  determine  the  nature  of  thi?  cltemical 
substance  use<i  for  atlidteration,  arvd  wc  need  not  go  on  to  ascertain 
the  qunntily  present  in  any  article;  although,  when  wc  di'sire  to  go 
thoHMiglily  into  the  subject  of  adulteration,  this  also  will  in  some 
instances  be  necessary. 

The  apparatus  enumerated  below  includes  the  greater  part  of  that 
which  is  required  for  both  purposes. 

For  drying  and  evaporating. — A  water,  a  sand,  an  air,  and  an  <^I 
bath,  evaporating  dlsoea  of  various  sizes,  and  watch  glasses. 

For  weighing  and  meaxuring — A  pood  bnlanee(if  for  weighing  very 
accurately  fractions  of  a  grain,  Ocrtltng's  is  the  best);  weights  of  brass 


\jK\it  LlL»ui»»U  *>iru;iu>xU  u»i»»u 


iOl 


iY 


BT  CHEMISTRY. 


57 


and  pintinum ;  a  specific  gravity  bottle,  graduated  pipettes,  flatktt  ffl 
of  various  sizes  and  measures;  densimeters,  as  a  saccharometer,  galHcto- 
meter  anrl  urinomoter. 

for  titration. — Funnel  stands,  funnels,  and  filtering  paper. 

For  pulverisatioH.-^-Mitrtars  ;  a  mill. 

For  distiUation. — A  still,  retorts,  and  condensers. 

For  Incineration. — JVlutHes,  jwrccluiii  and  platinum  crucibles  and 
dishes. 

In  addition  to  the  above  apparatus,  test  tubes,  a  lactometer,  iher- 
inomcter  (one  not  mounted,  and  bavin/r  a  Inng  range  of  degrees),  a 
vnsh  bottle,  and  a  drop  tube,  will  be  required. 

When  it  is  probable  that  a  large  number  of  samples  of  the  same 
article  will  have  to  be  examined,  and  many  similor  operations  con- 
ducted at  the  same  time,  it  is  desirable  that  ifpfcinl  arrangements 
should  be  made  with  this  view,  and  that  we  should  be  furnished  with 
aeries  of  crucibles,  glasses,  diKhen,  &c.  of  the  same  size. 

Any  information  which  may  be  re(]uired  respecting  the  apparatus 
employed  may  be  readily  obtained  from  the  manufacturers  and  sellers 
of  chemical  apparatus. 

On  the  Chief  Prelimifiary  Chemical  Operatioiu. 

The  chief  preliminary  chemical  operations  are  those  of  weighing, 
I'measuring,  desiccation,  cvaporntion,  nitration,  decantation,  distillation, 
»nd  incineration.  A  few  observations  may  now  be  madc^upon  each  of 
theje  proteases. 

Weighittg. — The  precautions  to  be  observed  in  weighing  are,  for 
'the  most  part,  of  a  tolerably  obvious  character  and  require  no  fipL'cinl 
description.  The  substance,  especially  if  it  be  in  a  dish  or  capsule, 
should  not  be  weighed  while  warm  ;  if  it  l>e  one  likelj  to  absorb  water 
It  should  be  weighed  enclosed  in  watch  glasnes  {  and  if  its  weight  is 
not  determined  immedioUdy  after  being  dried,  it  shoidd  be  kept  under 
a  bell  gliws  near  to  a  dish  of  sulphuric  acid.  These  prernutions  of 
course  need  not  be  observed  in  cases  where  the  exact  weight  is  not  of 
ittatcriul  consequence,  or  where  the  quantity  of  the  substance  weighed 
M  considerable  ond  where  it  is  not  hygroscopic. 

Mettmhng, —  This  jirocess  is  hnif  recourse  to  in  the  case  of  fluids, 
MA  it  is  more  expeditious  than  weighing.  'l*be  instruments  used  for 
this  purpose  are  the  graduated  pif>ette,  the  graduated  burette  or 
dropping  glass,  the  grailualed  c}-liiider  or  measure,  and  the  graduated 

In  measuring  lir^uids  in  glass  vessels,  the  dark  zone  formed  by  the 
adhc«ion  of  ihc  Huid  to  the  inner  walls  of  the  glass  should  be  tuken 
into  account.  The  measuring  is  most  occurote  when  the  mark-lino 
of  the  measure  coincides  with  the  lower  border  of  the  dark  rone. 

Dtnccation, —  Most  substances  contain  more  or  less  superfluous 
water,   that  is,  water  which  is  simply  in  a  state  of  mechanical  ad- 


56      MEANS   FOR  THE  DETECTION   OF   ADCLTERATION. 


mbiture,  and  not  chemically  combined  with  the  substance;  most  solid 
bodies,  tberefore,  require  to  be  deprived  of  this  non-e^-scntiid  water 
befiare  tber  can  be  quantitatively  analysed;  and  this  is  e0bcted  by  the 
upwution  of  drying.  With  the  constitutional  water  we  of  course  must 
BOC,  ill  genottl,  interfere. 

To  acDompliah  this  object  satisfactorily,  it  is  requisite  that  we  should 
be  acqaainted  with  the  pro^icrtie:!  of  the  substance  operated  upon, 
wkelber  it  loses  water  simply  in  contact  with  the  atmosphere,  in  air 
dried  to  312°,  or  at  a  red  beat  These  data  will  »erve  to  guide  us  in 
tW  sdectJotn  of  the  process  of  desiccation  best  suited  to  the  substance 
VB^er  ezanunation. 

Sntlaaoea  are  dried  by  means  of  blotting  paper,  under  a  bdl  jar 
m  f—tf  t  witfa  sulphuric  acid,  in  the  exhaosted  receiver  of  an  air 
in  tbc  valer,  air,  and  oil  baths. 

B^ority  of  substances  with  which  we  shall  hare  to  deal  being 
loK  water  at  21:2"  F.  and  are  decomposed  at  a  re^  btat ;  eon- 
flBfaottlj  ^hey  require  to  be  dried  in  a  water  bath.     When  higher 

iwialiiii  i  are  needed,  as  in  rendering  certain  salts  anhydrous,  the 

r  or  ofl  ha»k»  must  he  had  recotirse  to. 

TW  aad  bub,  although  useful  in  many  cases,  rcqiHres  to  be  em* 


as  it  is  not  ea^y  to  regulate  its  teMperaciure,  and 
placed  upon  it  are  rvadity  charred  aM  desirored. 
or  dish  contaioing  the  substance  to  be  dried  aaoold 
Snedj  npoa  tbe  sbelf  of  the  water  cr  oil  b«tb,  bat  a 
recuin  dasb  sbould  be  interposed. 
EraporataoB  mav  be  elTected  eitbcr  n  the  water 
or  orer  the  flame  of  a  gas  or  spirit 
fron  boiltng  or  spurting.     Aa 


mtm  <■■»  m  tm  mly  tbe  beat  by  mean$  of  a  Hamw 


care  being 
way  in 

tbe  erapotaiing  dish  ftam  caaUaimaAmmj  dost 
meBetmrj  to  protect  tbe  disb  ai  mam  way;  tUs 
bf  covcnof  it  vitb  a  dieet  ofilwii^  VV  tvnied 


;  or  a  glaas  rod  twisted  iato  a  traimidar  abate 
and  Be  paper  Mnead  over  it  aad  bcfft  n  poailion  ay 
mi  lad  acnea;  bvt  a  atill  beUcr  way  is  to  secare  tlie 
tmm  mmM  baapa  fitting  desely  tbe  «m  orer  tbe  otber. 
nsoMMto  are  aqiaiaied  oaos  wnv  bv  aaa  ai  tvo 
y  by  ilB^Maardecaatarioa     Iba  immms  of  a  goad 

to JBM  tbroi^gb  rt;  tbera  ii  a  yaat  d»r- 

«!■»  VaaMr  ■paved,  mmiiii  wmmmnKimmAmhat^ 
If  ■  uifTailli  ifMi    r    m  -  ^^"T   i  r  -^  -    -  i 


IVk  ia 


'mmi 


BT  CHEMISTRY. 


S9 


wirm  distillod  water  previous  to  drying.    These  operations  arc  best 
conilactetl  by  placing  a  number  of  SUcrs  in  a  glass  funnel. 

It  will  be  fuund  convenient  to  prepare  a  number  of  filters  in  this 
way  and  to  ke^p  theiD  of  <]il]'tfrent  sizes,  regictertng  the  weights  of  the 
asltes,  corrcspomliui;  to  the  several  sizetf.  Tbia  may  be  readily  done 
by  preparing  some  circular  pieces  of  cord-board  to  serve  aa  patterns 
tor  the  iHrveral  sises. 

Before  prooeedinj;  to  filter  any  liquid  for  the  purpose  of  separating 
a  precipitate  from  it,  it  is  in  general  advisable  to  allow  the  precipi> 
tate  to  subside  to  a  great  extent :  in  this  way  it  is  less  liable  to  pass 
tlirouffh  the  filter  or  tbe  filter  to  become  clogged. 

It  la  in  some  cases  necessary  to  promote  and  assist  the  speedy 
Md  complete  subsidence  of  the  precipitate.  Heating  the  precipi- 
tate with  its  menstruum  will  of^en  produce  tbe  desired  effect ;  in 
othrr  casciff  as  with  chloride  of  silver,  agitation  may  be  hurl  recourse 
to  with  advantage ;  lastly,  in  some  ini^tanccs  reagent;^  may  be  added,  as 
alcohol  added  to  water  to  imlucc  complete  precipitation  uf  clil(»ri(le  of 
pUtinun  and  ammonium,  chloride  of  Iea<l,  and  sulplmte  of  lime, 
or  anuBOoia,  to  ensure  tbe  precipitation  of  phospLaie  of  ina<;^ne9ia 
and  aaamonia.  Again,  a  precipitate  may  somettmea  be  prevented 
tnm  pMsing  throu^h  a  filter  by  modifying  the  menstruum :  thus,  the 
teadeDcy  of  sulphate  of  harytii,  when  filtered  from  an  aijueous  solution, 
to  pwa  throuffn  the  Biter,  mny  be  prevented  in  a  great  measure  by 
tbe  addition  of  chluride  of  ammonium. 

Substances  which  have  been  precipitated  from  hot  solutions  arc 
OMally  best  filtered  while  hot,  since  hot  duids  run  through  the  filter 
more  rjuickly  than  cold  ones. 

Lajily,  tlie  precipitate  should  be  repeatedly  washed  with  fresh  quan- 
of  tlie  proper  menstruum, — usually  distilled  water, — until  there 
txace  uf  a  dissoWed  substance  to  Ite  detected  in  the  last  rinsings. 
J^cantaHun, — The  second  method  by  which  precipilates  may  be 
ktrd  is  by  dceanlation :  this  will  be  found  in  many  cases  a  very 
itious  and  accurate  method  of  soparaiion.  The  precipitate 
be  allowed  to  subside  completely  bcl'ure  pouring  off  tbe  supcr- 
lik^uid,  and  should  subsetpieully  lie  washed  repeatedly. 
^  larger  amount  of  water  buMng  required  for  washing  precipitates 
ed  by  decantatioo  than  is  the  cose  with  pi-ecipitates  washed  upon 
1%  it  li  Deoeaaory,  where  the  former  pnxress  is  adopted,  that 
precipitates  sbould  be  insoluble.  For  the  same  reason  decanta- 
tion  o  not  ordinarily  resorted  to  in  cases  where,  besides  the  amount 
i  ti  the  prrdpitaled  substance,  we  have  to  dctermiue  the  amount  of 
I  oClbff  ooostatneota  contained  in  the  decanted  fluids. 
\  DitittUdiotL. — Tbere  are  three  iwrticulars  which  require  to  be  care- 
^■hOy  attended  to  in  the  distillation  of  alcoholic  liquids,  including 

^^^  One  of  these  i^  to  close  completely  tbe  opening  between  tbe  beolc  of 
the  retort  and  tbe  neck  uf  the  receiver  ;  this  is  well  effected  by  mcsng 


60      MEANS   FOB   THE  DETECTION   OF   ADOLTERATION, 


of  ft  perforated  cork,  by  which  the  two  vessels  arc  Joined,  the  junction 
bein^'  well  secured  by  a  lule  of  Unseed  meal  made  into  a  paste. 

Another  purttcuiar  is  to  take  eure  that  all  the  ulcohol  hns  really 
passed  over  before  suspending  the  diaulliition.  Before  thiti  is  fully 
accomplished  it  is  ffenerally  necessary  that  three-fourths  of  the  spi- 
rituous liquid  should  be  distilled  o\'or;  and  even  then  it  is  advisable, 
where  the  strictest  accuracy  is  desired,  to  distil  over  a  fresh  but 
email  quantity  of  the  liquid,— that  which  first  passed  orer  having 
been  reinoveil, — and  to  take  its  Bpecific  gravity. 

The  third  point  h  to  re;njlatecxa<;tly  the  temperature  of  the  Bpirit 
to  a  fixed  standard  before  proceeding  tu  the  determination  of  its 
specific  gravity,  by  means  of  the  specific  gravity  bottle. 

Incineration.— ~'V\\vre  are  two  objectji  to  be  kept  in  view  in  the 
incineration  of  organic  atihstanccs,  the  ashes  of  which  are  intended  for 
analysis  or  the  weight  of  which  is  required  to  be  determined  with 
accuracy. 

These  are,  the  complete  destruction  of  tlie  carbon,  without  alteration 
or  decomjHWttton  of  the  wdta  composing  the  ash, 

The  combustion,  therefore,  while  it  is  eomjilete,  must  be  effected  at 
the  lowest  practicable  temperature,  that  ia^  at  a  dull  red  heat.  There 
are  several  waTS  in  which  these  objects  may  be  aocompUshed.  It  will 
be  necessary  only  to  notice  one  or  two  of  the  best  and  most  con- 
renient  methods.     One  method  ia  aa  fallows :  — 

The  organic  Bubstance.  beingproperty  dried  at  212'* F.  and  weighed, 
is  to  be  charred  in  a  platinum  or  Hessian  crucible  at  a  gentle  red 
heat.  The  charred  mass  ia  then  to  be  transferred  to  a  shallow  pla- 
tinum ilish ;  over  this  is  to  be  placed  a  glairs  chimney  supported  on  ft 
triangular  piece  of  platinum  wire  ;  the  tlame  of  a  gas  or  spirit  lamp 
is  to  be  applied  tfl  the  dish.  The  increased  current  of  air  caused  by 
the  chimney  suffices  to  eflect  the  complete  incineration  of  most  or- 
ganic substftnt'es. 

In  a  second  method  the  muffle  is  employed. 

The  Huhstanee  to  be  incinerated  Is  placed  on  a  plutinum  ur  porcelain 
dish  or  capsule;  this  ia  introduced  into  the  muflle,  which  in  gruduu-lly 
heated  in  the  furnace.  When  the  evolution  of  the  empyreumatic  pro* 
ducts  of  combustion  ceases,  the  beat  ithould  be  Increased,  but  not  be- 
yond a  ▼ery  faint  redness,  visible  only  in  the  dark.  At  this  tempera- 
ture, no  salts  except  the  carbonates  —  the  carbonic  acid  being  partially 
dissipated — are  decomposed,  and  the  cnrbon,  which  burns  with  a  feeble 
incandescence,  is  destroyed  in  the  course  of  a  few  hours. 

When  great  accuracy  is  not  required,  the  incineration  may  be  con* 
ducted  in  a  porcelain  capsule,  nver  an  o|)en  fire  or  flame. 

When  the  substance  to  be  in«tnerated  is  too  large  fur  the  moflle,  it 
may  be  first  chtirred,  and  its  bulk  thus  reduced. 

That  the  careful  regulation  of  the  temperature  duriag  incineration 
is  a  matter  of  juueh  imjiortancc,  is  shown  by  the  fact  that  when  the 
beat  is  increased  much  beyond  a  dull  redness,  the  metallic  chlorides 


BY   CHEMISTRY. 


fl 


I 


«re  in  part  volatilised,  as  may  be  also  a  portion  of  the  phosphoric  and 
lulpbiiric  ocid^s  of  the  phnsnhutes  nntl  sulphates  :  besides/excessive 
heat  causes  the  metallic  cblorido^  and  the  phosphates  of  the  aikaliefl  to 
l\itie :  and  the  fused  mass  encU>sing  the  carbon,  greatly  impedes  iM 
ooDibiution. 

MoHt  of  the  salts  and  substances  present  in  the  ashes  of  plants  were 
unquestionably  constiluenis  of  (lie  plants  from  which  the  iisbes  were 
procured.  In  regard  to  some  others,  it  is  uncertain  whether  they 
were  originally  present  in  the  plant,  or  owe  their  formation  to  the 
incineration ;  while,  with  respect  to  otliers,  it  is  certain  that  they  owe 
ibeir  oripn  entirely  to  that  process. 

Thus  the  sulphates,  and  even  the  carbonates,  may  have  been  original 
consiilucnUiof  the  plants;  or  they  may  have  been  forme*),  and  this  they 
no  duubt  are  to  some  extent,  iii  the  process  M'  iiicineriiiion  by  tlie  de- 
struction of  Bolts  With  organic  acids,  and  by  the  oxidation  of  the 
sulphur  present  in  all  plants. 

The  metallic  sulphides  are  certainly  forme<l  by  the  action  of  the 
charcoal  u(>on  the  sulphates,  the  supply  of  oxygen  bein^  limited. 

It  was  formerly  considered  that  the  presence  of  carbonates  in  the 
ash  of  n  plant  not  coiituining  carbonates  might  invariably  be  regarded 
as  a  proof  of  the  presence  of  h&Ud  with  organic  acids  in  the  liuiiiierated 
pliiot.  It  bos  been  abowu,  however,  that  ulkuline  carb^^iatos  and  lyyro' 
phosphates  are  formed  when  tribasic  alkaline  phosphates  are  ignited 
with  a  large  excess  of  sugar,  or  with  the  corbou  of  sugar. 


Bf  agents  required  for  the  Detection  of  Adulteration. 
It  had  occurred  f-o  us  to  enumerate  the  rea;;ent9  reijuired  for  the 
detection  of  adulteration.  These  mi;/ht  htive  been  arranjred  either  under 
the  names  of  the  articles  subjected  to  cxaminiition,  the  several  pur- 
for  which  the  reagents  are  etnployed  being  at  the  same  time 
ery  briefly  indicated ;  or  they  might  have  been  clasMlied  under  the 
eaxU  t'f  (be  dilforent  chemical  substances  employed  in  ailulteration. 
^On  full  consideration,  however,  it  does  not  appear  that  any  suHiuiont 
or  treat  advantages  would  result  from  either  of  the  propoieddaasifi- 
cationi  of  the  reagents  rcquireil ;  these  will  of  course  be  specified  in 
conmx'tion  with  the  description  of  the  means  to  be  adoptedlor  the  dis- 
covery of  the  adulterations  practised  upon  the  various  articles  of  food 
and  me<licine  described  in  the  course  ot  the  work. 

The  preceding  observations  relatin;?  to  the  chemical  apparatus,  pre- 
liminary  chemical   processeri,    and   the    reagents    emphiyed    for   the 
;overy  of  adulteration,  are  of  course  iiitcniletl   not  for  professed 
lists,  hut  rather  for  thf  infuniiEition  of  students  and  beginners, 
■iesire  to  become  acquainted  only  with  as  much  chemistry  as  will 
ibic  them  to  detect  adulteration  in  arlielea  of  food  and  ntt-Ulcine. 
ho|H.il  that  they  will  facilitate  the  labours  of  the  inquirer,  who 
object  in  view. 


62      MEANS  FOB  THE   DETECTION  OF   ADULTERATION. 

The  special  instruction!!,  inicri>scopit'al  and  rbcmicat,  necessai^  for 
the  discovery  of  the  adulteraiiohs  to  which  the  several  ariielcs  oifood 
anil  metlicine  examined  are  subject,  will  be  found  under  the  names  of 
the  articles  themselves. 

As,  however,  occasional  doubts  and  difficulties  may  arise,  nnd  par- 
ticularly M  the  student  may  desire  to  extend  bis  investigations  hL-yond 
the  limits  of  this  treatise,  it  would  be  well  tliat  he  should  provide 
himself  with  the  Rnf];lish  translations  of  Fresenius'  works  on  crncmioal 
analysis,  the  one  entitled  "  Elementary  Instruction  in  Qualitative 
Chemical  AualysiB,"  and  the  other  "A  System  of  Instruction  in  QuanU- 
taiive  Chemical  Analysis.*'  These  works  abound  in  practical  inscruc* 
tioti  of  the  first  importance,  and  therefore  are  invaluable  to  the  student 
of  chemistry. 


PAET  I. 
FOOD  AND  ITS  ADULTERATIONS, 


On  Ike  McojiM  pur  Kued  ill  procuring  Samples  for  Analyxis^and  in  arriving 
ai  the  Rendu  recorded  in  the  present  Wurk. 

BxroKx  proceeding  to  describe  the  oduUerAtions  practised  upon  each 
of  the  more  important  articles  ofconKiimptint),  whether  aoIl^Ls  UqiitdH,, 
or  medicines,  it  mty  be  premised  that  we  nhall  chiefly  describo  those 
irfnltcrationi  which,  in  thu  course  of  six  yt-'ara*  continuous  appticatiou 
to  the  vubject,  we  Iiive  ourselves  ascertained,  on  the  strictest  investi- 
gation, to  be  actually  prartiiie<I. 

We  ma^  state  also,  briefly,  the  method  pursued  in  order  to  arrive  at 
the  mnlti  about  to  be  placed  before  the  reader. 

The  method  pursued  to  detect  aiiulterution  was  as  follows.  A  con- 
■derable  number  of  samples  of  each  article  submitted  tn  examination, 
wcrv  purchased  in  the  ordinary  way  at  shops  of  ail  ilencription^,  some 
of  ibeie  being  establishments  uf  tlie  first  class,  and  others  shops  tit 
which  the  general  public  obtained  its  goods.  In  many  instances, 
all  the  dkopa  of  one  kind  in  whole  roods  and  streets  were  visited  with- 
out exception  in  succession. 

These  purchases  were  made  in  the  presence  of  witnesses, — vre  our- 
MlreSi  for  greater  socurtty,  and  knowing  well  the  fearful  rejpontiibility 
which  rested  upon  us,  accompanying  the  purchasers  on  all  occa- 
fioML.  Immediately  that  any  article  was  pun'hased,  the  names  of 
iht  porchasers  were  placed  ujHjn  it,  the  date  of  the  purchase,  and  the 
prioe  paid  for  it  Subflequentty  each  sample  wtia  subjected  to  careful 
Bucrotcopical  and  chemical  examination,  tlie  results  of  the  analysis 
being  published  from  time  lo  time  in  "The  Lancet,"  together  with 
~  addresees  of  the  merchants  or  traders  from  whum  the 
made. 


64         MEA.N8  PUESUED   FOR  PROCURING  SAMPLES. 

The  publienttoii  of  the  severul  Reports,  which  for  a  long  time  came 
out  almost  wuL'kly,  extendetl  over  k  i)eriod  of  four  years.  The  last  of 
our  reports  which  appeared  was  publieibed  in  "  The  Lancet"  in  De- 
cember^ 1H54.  Since  that  period  we  have  been  incessantly  occupied 
with  the  sul>ject,  and  httve  published  two  works  on  adulteration, 
AS  well  fia  artieles,  the  substance  of  which  will  be  found  recorded 
in  the  pages  of  this  work,  on  the  adulteration  of  Cones  tlour,  ea«o  and 
tapioca,  annatto,  cheese^  honey,  rum,  brandy,  wine,  liquorice,  coloeynth, 
compound  scummonv  powder,  and  ntlier  dru<^, 

Tne  conclusions,  then,  at  which  we  haTe  arrived,  are  based,  not  u[ion 
the  results  of  the  e^camination  of  a  single  or  even  a  few  samples  of  aiiv 
particular  artiide,  but  upon  tlie  rigorous  examination  of  an  extendetl 
neTU's  of  samjileH,  these  amounting,  in  the  a<>grc^te,  to  abe>ub  3000 
Bpeeimeiis  nf  all  kinds. 

Our  readers  will,  we  arc  osrured,  a^ee  with  us,  that  it  was  im- 
pos&ible  lu  proceed  in  a  more  business-like  or  impartial  manner 
lliau  tliis,  or  to  ofler  stronger  guarantees  of  the  accuracy  of  the  I'esuhx 
obtained. 

We  would  now  state  that  although  the  names  of  between  two  and 
three  thouannd  traders  have  been  thus  piil>li«hed:,  the  publication 
extentlingj  as  already  stated,  over  a  |>eriod  of  more  than  four  yt-ara,  in 
one  case  only  were  any  legal  procceuings  resorted  to,  and  even  in  this 
flingle  instance  the  action  was  abandoned  at  an  early  date,  without 
any  acknowledgment  being  made  of  error  having  been  coinmitted.. 
I'ursiiing  such  a  system,  and  with  such  resullA,  we  would  nsk,  is 
it  possible  that  the  conclusiuns  arrived  at  could  be  otherwise  than 
correct?  On  the  contrary,  is  it  not  certain  that,  if  mistrtke^i  hail  been 
madi^  they  would  have  Leen  quirkly  exposed,  and  Mr.  Wakloy  the 
Editor  of  "  The  Lancet"  and  ourselves  visited  with  the  consequences, 
vhich  would  have  been  nothing  short  of  utter  ruin  and  disgrace. 

Arrangement  o/Artielea  of  Food, 

Articles  of  food  are  divisible  into  snlids  and  liquids.  The  solids  may 
be  further  separated  into  those  which  are  deriveil  from  either  the 
vegetable  or  animal  kingdom,  and  the  liquids  into  natural  and  manu- 
factured drinks. 

As  no  particularly  iksefiil  purpose  would  be  served  by  following  the 
above  arrangement,  we  do  not  propose  to  confine  ourselves  to  it,  but 
will  treat  of  the  several  arlicles  rather  in  the  order  of  their  use  at  the 
breakfast  or  dinner  table.  By  adoptin;j  tbia  course,  a  tolerably  natural 
arrangcmen-  will  be  secured.  Thus  tlie  several  natural  and  manu- 
factured drinks,  the  condiments.  &c.,  will  follow  in  order. 

The  consiiJeralion  of  the  articles  consumed  at  breakf:utt  brings  us 
to  the  description  of  the  adulterations  of  tea,  cotlee,  chicory,  cocoa, 
sugar,  honey,  milk,  tlour,  bread,  butter,  lord,  o&tmeal,  imcbovies, 
potted  meats,  and  tisb. 


TEA,   AND   ITS   ADOLTEBAT10N8. 


63 


Wherever  practicAble,  the  following  course  or  order  will  be  adopted 
in  tliG  trcAtnient  of  each  artic-te. 

First.  Its  chemical  comp(>sition  and  peculiarities,  f^cneral  or  mi- 
criwcopiciU  structure,  nnd  itd  properties,  will  be  described. 

Second.      Its  adultiTutions. 

Third.'  The  muthnds,  microscopicELl  and  cbcmioal,  employed  for 
the  diacoTCry  of  its  aduHenitionB. 


TEA,   AND   ITS   ADULTERATIONS. 
Gaowm  akd  I'serARATioN  of  Tea. 


^ 


Tbb  tea-plant,  TTiea  ■Siwwww.  ami  of  which  T.  Bohea  and  T.  riri- 
ftis  ore  but  varieties,  is  a  hardy,  evergrrwn,  and  Ipafy  shrul>.  which 
att^init  the  hvipht  of  from  three  to  six  feet,  and  upwards;  it  belongs 
tfi  the  natural  family  Cuiutnniferte^  Temstromtacete  of  Liiidley,  whieh 
includes  the  Caniellius.  It  is  generally  propng.itcd  from  seed;  the 
seedling  are  pliinted  out  in  row?,  three  or  lour  feet  apart  when  n 
year  old,  and  the  plants  come  to  maturity  in  trom  three  to  four  years, 
yieldiu;*.  in  the  cour!(C  of  the  seusnn,  three,  and,  in  aome  cases,  four 
crops  of  leaves.  The  cropping  is  seldom  continued  beyond  the  tenth 
ur  twelfth  year,  when  the  old  treea  are  dug  up  and  replaced  by  seed- 
lings. 

The  first  pathering  takes  place  very  early  in  the  spring,  a  second  in 
the  beginning  of  May,  a  third  a1>out  the  middle  of  June,  and  a 
fourth  in  August.  The  leaves  of  the  first  pothering  are  the  most 
vulunbUs  anil  from  these.  Pekoe  tea,  which  consitits  of  the  young  leaf- 
buds,  as  well  as  black  teas  of  the  highest  quality,  are  prepared  : 
those  of  the  last  gathering  are  large  and  old,  and,  consequently, 
inferior  in  flavour  and  value. 

*'  It  was  after  the  year  600  that  the  use  of  tea  became  general  in 
China,  and  early  in  the  ninth  century  (I^IO)  it  was  introdueed  into 
Japan.  To  Euro[te  it  was  nut  brought  till  about  the  be'^iiiiiinj^  of  the 
seventeenth  century.  Hot  infusions  of  leaves  had  l>cen  already  long 
familiar  as  drinks  in  European  countries.  Dried  sapc-Ieaveswei-e  mueh 
in  u<«e  in  Knplund,  and  are  even  said  to  have  been  CArrit;tl  as  an  article 
of  trade  to  China  by  the  Dutch,  to  be  there  exchanjied  for  the 
Chinese  leaf,  which  has  since  idniust  entirt?lv  BUperscded  them.  A 
Kussian  embassy  to  China  also  brought  baelc  to  Mojteow  some  care- 
fully packed  green  tea,  which  tvoa  received  witli  great  acceptance. 
Awl  in  the  some  century   (]Gti4)  the  Knglish  £a»c  India  Company 


6S  TEA,  AND   ITS  ADULTERATIONS. 

OODBidered  it  lu  a  rnre  gift  to  present  the  Queen  of  Englukd  witli  two 
pounds  of  ten,*'*  —  Johnsion. 


F(g.6, 


T^AVKi   or    THE   TkA'PLAHT. 

j1  ,  jTODiii  leaf  I  fi,  iMf  of  blitck  tva  ortii«<liu(n  lite  1  t',  illtto  of  Ujjtr  growtlt  | 
/i,  leaf  of  th«  grrvn  vuioty  vf  the  tM-|iluit. 

The  leaves  vnry  considerablj?  in  size  and  form,  necordinp  to  »ge : 
the  jfoungest  leiived  are  narrow,  convoluted,  and  downy  ;  those  next 
in  Hge  mid  size  litivu  their  edges  dehcutelv  >ei*rated,  wiiii  the  venation 
acwcfly  perci.'p)ib!e ;  in  tiioee  of  nicdiuni  and  large  sizes  the  veniition 
is  well  marked,  u  series  of  characterifitic  loops  being  formed  alougeocb 


•  ThcPlui.br  SchlddMi.    Second  Edttlon,  p.l43. 


TEA,   AND   ITS  ADULTERATIONS. 


67 


raarpn  of  the  leaP,  and  the  serrations  are  atronger  and  deeper,  and 
placed  at  greater  intervals. 


FtK.J. 


LMfof  Um  AtMtm  TKrtrtj'of  th»TKA-i'L\^T  i  the  Ttnitiflii  li  theMtoe  u  tn  the 
kl>ck  uid  cr««n  T&fwtie*.  but  their  U  <k  tlicht  diOttmcc  in  tfac  •emtlotM, 
vbich  Kre  Blt«mal«ljr  Uifc  asd  md&II  —  s  ililllemia»  wliich  i*  tmbabl;  not 


The  principal  varieties  of  black  tea  are  Boheo^  which  is  the  com- 
raonest,  and  coarsest  description,  Conj»ou,  Souchonrf,  Capor,  and  Padre 
Souchong,  and  Pekuo,  which  are  of  the  highest  quality,  the  last  eon- 
aisting  of  the  very  younf;  and  uncxpanded  leav&s,  and  which,  when 
clothed  with  down,  confuilute  flowery  I'ekoe. 

The  principal  varieties  of  jrrt'en  tea  are  Twankny,  Hyson-skin, 
Young  Hyson,  Hyson,  luiperinl,  and  Gunpowder,  wliich,  in  green  tea, 
corresponds  with  flowery  Pekoe  in  black.  Inipmal,  Ilyaon,  and 
Young  Hyson,  consist  of  the  second  and  third  gatherings,  while  the 
light  and  inferior  leaves,  separated  from  Wvytn  by  a  winnowing  ma- 
chine, constitute  Hyson-skin,  a  variety  in  considerable  demand 
amongst  the  Americans. 

There  is,  according  to  most  writers,  but  one  species  of  ten-plant, 
from  which  the  whole  of  the  above,  and  many  other  varieties  of  tea, 
axe  obtained,  the  dififerences  de[woding  upon  soil,  climate,  age  of  the 
leaves,  and  mode  of  preparation. 

The  plants  from  which  black  teas  are  prepared  are  grown  chiefly 
on  the  slopes  of  hills  and  ledges  of  mountains*,  while  the  green  tea- 
shruhs  are  cullivated  in  manured  soils.  TTpon  this  circumstance 
many  of  the  diU'erences  between  the  two  vorictiM  depend. 

Other  dilfercnces  are  occasioned  by  the  processes  adopted  in  the 
preimratiun  :ind  roosting  of  the  leaves.  Thus,  while  black  tea  is  first 
roasted  in  a  shallow  iron  vessel,  called  a  Aho,  and  peeondly  in  sieves. 
over  a  bright  charcoal  fire,  green  tea  does  not  undergo  the  second 
method  of  roasting,  but  only  the  first — that  io  the  Auo. 


*  There  ii  a  range  called  Ihr  Dohes  Motintalna,  rrom  wblcb  Bohu  tM  takei  its  nune. 

w  S 


TEA,   AND  ITS   ADCLTEEATIONS. 


n 


The  leaves  of  blaek  tea  undergn  a  species  of  fermentation  before 
their  final  dryinp,  and  it  is  this  which  occaiions  them  tn  assume  so 
dark  a  colour:  those  of  frreeii  tea  do  not  undergo  this  preliminary 
fermentation,  beinp  dried  wiiile  iti  n  fresher  state :  but  the  leaves,  as 
thus  prepared,  arc  of  a  yellowish  or  olive  green  tint,  rery  unlike  the 
colour  of  the  green  leas  imfnorled  into  this  country. 

An  in)j>ortant  part  of  ihe  iimiiuracture  often  consists  in  the  roUiitg 
the  leaveflL^'^  ^  'o  iini)art  to  (hem  tlieir  cklTractenstic  twisted  shtii}e. 
'ITiis  is  eflected  by  subjecting  the  leavea  to  pressure,  and  rolling  by 
•the  bands  in  a  nartleiilnr  manner.  The  first  effect  of  the  appliralion 
of  heat  to  the  leaves  in  llie  Am«,  is  t«  render  tliem  soft,  and  flaccid; 
when  in  this  stnte,  ibcy  are  rentnved  frmn  the  vessel,  and  subniitted 
to  the  first  rolling  =^  an  operation  which,  after  the  renewed  action  of 
the  Alio  on  each  occasion,  is  three  or  four  limes  rei>ealed,  with  superior 
teas,  before  the  process  Is  considered  to  be  complete. 

SeetUitig  of  Tea. 

There  are  several  kinds  of  scented  tea:  thow  with  whieh  we  are 
best  aequajnted  in  tins  coiintry  are  scouted  Caper  or  Chulan,  and 
flCenU'd  orange  Pekoe.  The  scent  is  cnnununiiyileil  to  tliese  teas  by 
mean^  of  the  Chuhin  flower,  Chlnranihtm  iHconHpieiius.  The  flowers 
of  other  plants  are,  however,  used  for  the  purpose ;  amongst  tliesc  may 
be  niLincd  those  of  Olca  /ragraiUj  Gardenia  florida,  and  Jasminum 
Sambac. 

The  process  pursued  varies  In  dilTerent  cases.  Sometimes  the  fresh 
flowers  are  strcxvn  between  successive  layers  of  tea;  the  tea  and 
flowers  are  then  Coasted  until  the  flowers  become  crisp,  when  they  are 
sifted  out.  In  other  cases  the  flowers  arc  dried,  powdered,  and  then 
sprinkled  over  the  tea.  For  further  purticulars  retspecting  the  scenting 
of  tea,  the  render  is  referred  to  Mr.  Uull's  ^  Account  of  the  Cultivation 
and  Manufacture  of  Tea  in  China." 

Analysii  of  Tea. 

The  Infusion  mode  from  tea  contains  gum,  glucote^  or  saccharine 
matter,  a  large  quantity  of /uwrtift,  ro/o/iVf  oi/,  and  a  peculiar  nitro- 
genised  principle  called  thtine;  this  is  identical  with  caffeine^  and 
upon  its  presence  many  of  the  properties  of  tea  depeniL 

The  amounts  of  gum  and  riinnin  contained  in  a  given  sample  of  tea 
afford  data  by  which  its  qualily  may,  to  some  extent,  be  determined. 

The  percentage  of  (lu-se  substances  may  be  obtaineil  in  die  iollow- 
uig  manner:  One  hundrt^d  grains  ol  tea,  dried  by  meaits  of  a  water- 
bath,  are  to  be  boiled  for  some  time  in  about  a  ijuart  of  tlistilled 
water;  this  tlis^olves  out  the  gum  and  tannin,  but  dues  not  affect  the 
lignin,  which,  re-dried  in  the  same  way  iit  a  tt-niperiiture  of  21*2° 
Fohr.,  and  weighcnl,  gives  the  amount  of  that  substance  present  in  the 


TEA,   AND  ITS   ADULTERATtONS. 


69 


hundred  ^ains,  and  shows  by  the  loss  of  weight,  the  combinod  quan- 
tities of  t Be  pum  and  tnnitii).  The  deooction  is  now  to  be  evaporated, 
and  the  rcatduuni  treateil  with  ulrohul;  this  will  take  u[i  the  tannin 
and  colouring  matter,  but  leavt;  the  guQi>  the  weight  of  which  being 
ascertained,  af^er  drying,  gives  the  p«r>centaj£e  of  tannin. 

Should  it  be  desired  to  estimnte  the  quantity  of  tannin  separately, 
thin  moy  be  efleeted  either  by  evupomting  the  alcoholic  solution  and 
drying  the  residue  in  the  ordinary  xray,  or  eljic  by  the  preeinitation  of 
the  tannin  from  the  decfx'tion,  by  a  sulutioii  of  gelatine.  The  preci- 
pitate being  washed  aud  dried  ut  a  steoui  heat,  indicates  the  quantity 
of  tannin,  100  graiua  of  the  precipitate  being  equal  to  40  grains  of 
tannin. 

The  determination  of  the  amount  of  nitrogen  in  any  tea  should 
form  part  of  a  ri^jid  analysis;  for  this  purpose,  100  grains,  dried  in. 
a  water-batli  until  it  ceases  to  loee  weight,  ia  to  be  incinerated  with 
aoda-liuie,  and  iis  oontcnta  in  nitrogen  locn  ascertained. 

While  the  average  amount  of  nitrogen  in  tea  exceotU  five  per  eent^ 
that  in  rloe,  hawthorn,  and  elder  leaves  is  seldom  over  three  per 
cent.,  and  in  the  fl^^t  tww  is  nearly  always  much  under  this  quantity. 

The  fullowing  nre  the  methods  of  proceeding  adopted  by  dilferent 
chemi&ts  iur  obtaining  the  active  principle  of  tea,  theine^  and  fur  esti- 
mating its  amount :  — 

Mulder  obtains  it  from  tea  by  lienting  the  evaporated  extract  by 
hot  water,  with  calcined  magnesia,  tiltering  the  mixture,  evaporating 
to  dryness  the  liquor  which  passes  through,  and  digesting  the  residuum 
with  ether.  This  solution  being  distilled,  the  ether  of  course  paasea 
over,  and  the  theine  remains.  This  principle  may  be  extracted  iu 
the  same  wuy  from  raw  ground  coffee. 

Dr.  Sleiihouse  obtains  theine  by  adding  acetate  of  lead  to  a  decoc- 
tion of  (<'a,  evaporating  the  filtered  liquid  to  a  dry  extrarl,  and  ex- 
pMing  this  extract  to  a  subliming  heat  in  u  (shallow  iron  pan,  whose 
mouth  is  covered  with  porous  pnper,  luti^d  round  the  edges  aa  a 
filler  to  the  vapour,  and  surmounted  with  u  cap  of  c(mii>act  paper,  aa 
ihe  receiver.  According  to  ibis  method,  l>r.  Stenhouse  obtained  only 
1  '37  per  cent,  of  theine. 

M.  I'eligot,  remeniberiug  that  the  quantity  of  nitrogen  contained  in 
lea-leaves  frequently  amounted  tu  6  percent.,  was  hence  led  to  be- 
lieve that  much  more  theine  existed  in  them  than  had  hitherto  been 
separated,  and  he  adopted  the  following  improved  method  of  extrac- 
tion :  — 

To  the  hot  infusion  of  tea,  subacetatc  of  lead  and  then  ammonia 
were  added;  the  liquid  was  tillered,  and  the  lead  tseparated  by  means 
of  sulphuretted  hydrogen;  after  a  second  filtration,  the  clear  liquid, 
being  evaporated  ut  a  gentle  heat,  aflurded,  on  cooling,  ait  abumlant 
crop  of  crystals.  Qy  re-evaporation  of  the  mother  liquid  more 
cryatals  were  procured,  amounting  altogether  to  from  5  to  6  per  cent. 

According  to  Mulder't  atudyns,  100  partd  of  tea  conaial  of — 

r  3 


70 


TEA,  Aim   ITS   ADULTERATIONS 


Grcm. 

BU^. 

IWntial  oil  (to  wliich  the  flavoor  u 

idue) 

-     0-79 

0-60 

CMoropbylle  - 

. 

. 

.     022 

1-84 

Wax 

- 

- 

-     0-28 

— 

Resin 

•             — 

- 

-     2-22 

3-64 

Gum 

- 

- 

-     8-56 

7*28 

Tannin 

. 

. 

-  17-80 

12-88 

Tlieine 

. 

. 

.     0-43 

046 

Extractiye     - 

. 

m 

-  22-30 

19*88 

Do.,  dark- coloured 

. 

.     

1-48 

Coltmrable  matter, 

separable  by  hydrocblo- 

ric  acid 

. 

. 

-  23-60 

1912 

Albumen 

*             • 

. 

-     3-00 

2-80 

Vepetable  fibre 

- 

- 

-  17-08 

28-32 

Ash 

- 

- 

•    5-56 

5-24 

1000 


1000 


The  iketne  ta  obviously  rnucb  underrated  in  JIulder's  analyses. 
According  to  Stenhoiise,  the  teas  of  commerce  contain,  on  an  average, 
about  2  per  cent  of  theine. 

Thetne,  when  pure,  crystaHiscs  in  fine  needles,  glossy.  Ukc  white 
silk;  the  crystals  lose,  nl  -21.2'',  8  per  cent,  of  their  weight,  or  two 
utoma  of  water  of  crystallisation  ;  tiiey  are  bitter  but  have  no  smell; 
they  iiiwlt  at  550°  F.,  and  sublime  at  543*^  without  deconiposing  ;  dried 
at  350°,  they  dissolve  in  98  parts  of  cold  water,  97  vV  alenhol,  and 
194  parts  tif  ether.  Tlieine  is  a  feeble  base,  and  is  precipiiable  by 
tiuinin  alone  from  ita  .solutions. 

The  volatile  oil  is  not  prcsiMit  in  fresh  tea,  but  is  developod  \n  the 
course  of  dryin^  and  roa-stinp  ;  it  is  to  it  that  the  aromtt  and  Uuvoup 
of  tea  are  mainly  due  :  100  poundii  of  tva  distUied  with  water  yield 
about  1  pound  uf  this  oil. 


Slructwe  of  the  Tea-leaf. 

The  characters  of  tlie  tea-leaf  visible  to  the  naked  eye*  such  as  its  ve- 
nation and  the  crenution  of  the  edges,  have  already  been  described. 

Examined  with  the  microscope,  the  following  is  aeeertaiiitid  to  be 
its  {general  structure.  It  is  made  of  epidermic  cells,  sloniata,  paren- 
chyTuatous  rellfi,  and  hairs. 

The  epidermic  cclU  yary  much  in  sire,  accordinij  to  the  age  and  size 
of  the  leaf:  in  the  leaf  of  nicdtuni  age  and  size  the  cells  are  small  and 
slightly  angular  only,  while  in  the  hard  and  old  loaf  they  are  very 
much  lar};er,  more  angular,  and  the  walls  of  the  cells  arc  more 
didtiuctly  visible. 

The  utotnata  are  confined  principally  to  the  under  surface  of  tlie 
leaf,  they  are  rather  numerous,  small,  and  are  formed  of  two  reuifurm 


TEA,    AND    ITS  ADULTERATIONS. 


71 


celU,  which  leave  a  very  decided  aperture  between  them.  Theepider- 
lic  ceila  arifuml  the  atumata  are  much  elongated  and  curved  like  the 
eells  of  the  stomatA  themselves. 

The  hairs  are  abo  confined  to  the  under  surface  of  the  leaf:  in  the 
verj  joung  leaf  they  are  very  nunieruufi,  hut  in  those  of  middle  age 
»fthey  are  much  leas  abundant,  ajid  indeed  in  some  eases  are  nearly 
"Itogelher  WMntlng  ;  ihey  are  short,  and,  when  not  broken,  [minted  and 

idivided. 

The  celU  forming  the  substance  or  parenchyma  of  the  leaf  resemble 
of  most  other  leavee,  and  do  not  present  anything  remarkable* 

Fig.%. 


i»  and  the  next  figure  represent  the  tea-leaf  as  it  appears  under 
micnwcope  as  met  with  in  most  black  tens. 

J^ropertien  of  Tea. 

Lo-Ta,  a  learne<l  Chinese,  who  lived  in  the  dynasty  of  Tanff,  a.p. 
to  90G.  j?ire«  the  foUnwin;;  a^rrecable  account  of  the  (pialities  and 
fcctJ  «>f  the  infusion  of  the  leaves  of  the  tea-plant :  — 

|i'ro|>ers  the  spiriU,  :ind  harmonises  the  mind  ;  dispels  lassitude, 
plieve*  fMtiaue ;    awakens  thought,   and   prevenla   drowsiness ; 
or  refre*he.«i  the  bo<ly,  and  clcnrs  the  perceptive  faculties.** 
Tereira's  "Materia  Medica"  we  find  the  following  remarks  re- 
UlinfF  to  the  properties  of  tea:  —  "  Ita  astrinpcncy  is  proved  by  its 
"*     lical  properties.     Another  quality  possessed,  especuilly  by  areen 
b  that  of  diminishing  the  tendency  to  sleep.     Tea  appears  to 


73 


TE^i    AND  ITS   ADULTEKATIONS. 


posKM    a  sedative   influcocc  with  regard   to  the  vascular  sYfltem. 
btrong  green  teu^  taken  in  large  <[uaiit>ties,  is  capable,  id  Bomo  con- 


Vntlrrwmfact  AfTEA-iJiAr,  afaovlDi  th«  alnmAU  uwl  edit  of  UU«  porUoB  oT  Iht 
leaf,  u  veil  M  «  pan  of  oue  uf  Ibc  luUn  bj  wbioli  Uila  lurfhea  U  elotbfd. 

RtitutionSf  of  producing  most  distressing  feelings,  and  of  operating  as 
a  nareiitic  " 

Pru^e^so^  Johnston  gives  the  following  deseription  of  tbe  propcrlia 
of  lea  :  "  It  exiiilarntes  without  genaibly  intoxicating.  It  excitet  ike 
brain  to  increused  activitj^,  and  pruduces  wiLkcfuIiicss.  Hence  itt 
usefulness  to  hard  studL'uts,  to  those  who  have  vigils  to  keep,  and  to 
persons  who  labour  much  with  the  head.  It  soothes,  on  the  cnntrarj, 
and  stills  tlie  vu<iculur  system ;  nnd  hi'nce  its  use  in  inflnmniatorT 
diaeaacs,  and  as  a  cure  tor  headache.  Green  tea,  when  taken  strong,  acts 
very  powerfully  upon  some  constitutions,  prtnlucing  nervous  treiiv 
blings  and  other  distressing  Bytiiptoms,  ueting  as  a  narcotic,  and,  in 
inferior  animals,  even  pnxlucJtig  p:iridysis.  Its  exciting  effect  upon 
the  nerves  makus  it  uneful  in  cuunteracting  the  elTects  of  opium  and 
of  fermented  liquors,  and  the  stujwr  sometimes  induce<l  by  (iever.*** 

The  properties  and  cifecis  of  tea  are  due  to  the  conjoined  nciidn  of 
at  least  three  active  chemical  constituents,  nmnoly,  tbe  volatile  vil^ 
Acintr,  and  tannic  acid. 

The  special  action  of  the  volatile  oil  bos  not  yet  been  scientifically 

•  ChMDlflr;  of  ComnoD  LUb.    BUckwood. 


TEA,   AND   ITS   ADULTERATIONS. 


73 


led  ;  but  in  Professor  Johnston's  "  Chemist  ry"  we  meet  with 
tb«  following  remarks  rt'latire  to  il«  prfnit-rties  :J—  "  That  it  does  exert 
paverful,  sod  most  likely  a  narcotic,  mtlucnce  is  rendered  probable 


TtM-t.%AT. 

jt ,  m^^mmutttm  at tanf-dfvclopcd  leaf, rvpmnHDf  tht etlli of  vhleh  It  U oon- 
■MvMt  t  A,  mnitt  nirtiMx,  kboviaf  Ita  ccUt  maii  UontAta  i  V,  cltloropbyU* 


ij  known  fact*.  Amonf;  them  T  mention  (he  headaches  and 
to  which  tea-tastertt  are  Bnhj(»ct ;  thu  attax^ka  of  paralysis 
afler  a  few  years,  those  who  are  employed  in  packing  and 
««p«ckisie  chests  of  tea  arc  found  to  be  liable ;  and  the  circumstance, 
mmdf  aOudtfd  to.  that  in  China  tea  is  rarely  used  till  it  is  a  year 
old,  b^CTMC  of  the  peculiar  inloxicftting  profwrty  which  new  t£a 
fomtmm,  TTw  efletl  of  tiiis  keeping  upon  tea  must  be  chiefly  to 
aHoir  a  portion  of  the  volatile  infiredients  of  the  leaf  tx»  escape.  And 
loMlr,  toat  there  i*  a  [towcrful  virtue  in  this  oil  is  render(>d  probable 
b^  ibtt  &et  ikai  the  similur  nil  of  coffee  has  been  found  by  cxperi- 
»f^t  f*j  puwpm'f  nsrrotic  prrt|>ertie9.'* 

n  of  the  second  active  constituent  of  tea — thein^ 
:  by  direct  experiment.  In  ihe  (luantity  in  which 
ti  t»  lajly  «:<jtt-iiM(...|  liy  most  tca-drinkorp,  tlnit  if,  some  four  or  five 
|Tmin«, —  a  quantity  onlitmrily  presentin  alKmt  half  an  ounce  of  good 
tra,  —  H  haa  been  found  lo  diminish  the  waste  of  tissue,  the  ncceasity 
for  food  to  rrpair  the  waste  bein;;  lessened  in  an  etiuul  proportion  : 
«■«  of  tho  efleclf  of  tea  is,  therefore,  to  save  food. 
If  M  aach  as  eight  or  ten  grains  of  theine  be  token  doily ,^a  quan- 


74  TEA,  AKD  ITS  ADULTERATIONS. 

tity  present  in  iiboiit  one  ounce  of  loa  of  gf)uJ  (juiilil y. — it  givea  rise  to 
tbe  tulluwing  Kyiiijitiiins:  the  pulse  \»  reinlerecl  mure  rre<|uenL,  the  actioD 
of  the  heart  stron^tTi  trembling  ensues^  and  there  is  a  perpetual  in- 
clination to  micturalioii.  "At  the  sanietime»  the  imtt;riiiation  is  ex- 
cited ;  and  after  awhile  the  ihcmshts  wander,  visions  be;;iii  to  be  seen, 
and  a  peeulifu*  fitate  of  intoxication  coiueit  on.  All  these  symptoms 
are  followed  by,  and  pass  off  In,  deep  sleep."  It  is  evident,  therefore, 
that  the  ejects  of  slrong  tea  are  attributable  in  a  great  measure  to 
the  over-d(»»e  of  theine  intrfiduced  thniugli  it  into  the  stomach. 

The  third  active  principle  of  tea  is  the  tannin  or  tannic  acid:  it  is 
this  which  imparts  to  tea  its  astringent  tiute,  and  which  cause*  it  to 
exert  n  slightly  conslipating  elFect  upon  the  boweU.  It  is  the  more 
completely  extracted  the  longer  the  tea  is  infused. 

A  fourth  not  uiiim[i(>rtatit  earistituerit  of  the  tea-leaf  id  p;luten, 
which  forms  no  less  than  one-roiirlb  of  the  weight  of  the  dried  leaves. 
As  tea  is  generally  consumed  in  thi^  country,  the  benefit  of  this 
substance  is  for  the  uio.«t  part  Imt  to  the  sysLcm,  it  nut  being 
dissolved  by  the  hut  wuter^  but  remaining  behind  in  the  leaves, 
with  which  it  is  usu:illy  thrown  away.  On  this  account  the  use 
of  soda  has  been  recommended,  this  dissolving  a  larger  proportion. 
of  the  gluten.  In  some  countries  the  tea-leaves,  either  whole  or  in 
powder,  from  which  the  infusion  ha.^  bet^n  made,  are  themselves  eaten  ; 
and  in  this  way  the  whole  of  the  beneficial  pruperties  of  tea  are  secured. 

"The  wealthy  Chinese  simply  infuse  the  leaves  in  an  elegant 
porcelain  i.'iip,  which  ha^  a  cover  of  the  Eiaine  niuteriul ;  the  leaves  sink 
to  the  bottom  of  the  eiip,  and  geuerally  rennuu  there  without  incon- 
veniencet  though  oceasiunally  suine  may  float  or  rise  to  the  surface. 
To  prevent  this  jnconvenicnce,  sometimes  a  thin  piece  of  silver,  of 
filagree,  or  open  work,  is  placeil  imi]iediut<?ly  on  ihem.  AVhere 
economy  is  necessary  to  Ix*  stti<iied,  the  tt-aptyt  is  use^l.  The  wealthy 
Japinese  continue  ine  ancient  mode  of  grinding  the  leaves  to  powder; 
and  after  infusion  in  a  cup,  Mt  is  whip^wed  with  a  split  bnmboo,  or 
denticulated  instrument,  till  it  cream*,  when  they  drink  both  the  in- 
fusion and  powder,  as  coffee  is  used  in  many  parts  of  Asia.'"* 

In  China,  as  appears  from  the  following  extract,  tea  is  the  common 
bcTerage  of  the  people.  The  late  Sir  George  Staunton  informs  us 
"that  tea,  like  beer  in  England,  is  sobl  in  public -houses  in  every 
town,  and  along  ])ublic  roads,  and  the  banks  of  rivers  and  cnnid.^  nnr 
is  it  unusual  for  the  burdened  and  weary  traveller  to  lay  down  his 
load,  refresh  himself  with  a  cup  uf  warm  tea,  and  then  pursue  his 
journey."  f 

The  Atliltbratiom  or  Tea. 

Much  skill  and  ingetmity  are  displayed,  its  we  shall  shortly  perceive, 
both  at  home  and  in  China,  in  the  adulteration  of  tea. 

■  B«n.  o«i  tht  L'ultlvallcn  «M  MAnurMlurr  of  Tm,  p  15. 
t  Lord  Mscannfy'i  EmtNuij'  to  FeUn,  toI.  U.  p.  96. 


I 

I 


TEA,  AKD  ITS  ADULTEBATIONS.  75 

The  principal  adulterations  of  tea  are  the  work  of  the  Chinese 
themselves ;  but  otber  adulteratlonii  arc  performed  nearer  home,  by, 
in  fact,  Kritish  fubricalonj  of  spurimis  len,  lioiii  bliick  and  ^reen. 
Thoee  ululterationH  may  be  described  in  the  first  place  which  are  of 
Chinese  nrijiin. 

The  SouclwngB  and  Congous  which  form  the  groat  bulk  of  the  black 
tea  consumed  in  ihis  country  are  rarely  adulterated. 

There  are,  however,  vurieties  of  blLiik  tea  imported  into  this 
country  fruni  Cbinu  which  are  never  utherwi.sc  than  adulterated; 
these  are  the  black  Ounpowtlen  Capers  or  Chuian*^  and  scented  orange 
Pekoe, 

Adulterations  practised  fry  the  Chinese. 

The  flduiterationi  practiaed  with  tea  by  tht!  Chinese  are  of  three 
very  distincc  kindd  :  one  conoistsin  the  inteniiixtun^  with  genuine  tea 
of  leaves  other  than  those  of  the  tea*plant;  a  gecomi  Is  the  manufac- 
ture of  spurious  articles  denominated  Lie  tea  ;  while  the  lliird  kind 
of  adulteration  conaibtii  in  glazing,  painting,  or  artificially  colouring 
the  surface  of  the  leaves  with  various  pigmentary  substances. 

Adulteration  with  Foreign  Leaves. 

In  reference  to  the  use  of  leaves  other  lima  those  of  the  tea-plant  the 
eridence  of  Dr.  Dickson  may  be  quoted,  who  states :  "The  Chinese 
annaolly  dry  many  millions  of  pounds  of  the  leaves  of  diiTerent  pliints 
to  mingle  with  the  genuine,  as  those  of  the  ash,  plum,  &c. ;  so  that  all 
epurious  leaves  found  iu  parcels  of  bad  tea  must  not  be  su])pose<l  to 
be  introduced  into  theni  by  dealers  in  this  county.  While  the  tea- 
trade  was  entirely  iu  the  minds  of  the  East  India  Company,  few  of 
these  adulterated  teas  where  iihipped  fur  Ibis  country,  as  experienced 
and  competent  inspectors  were  kept  at  Canton  to  prevent  llie  exporta- 
lion  of  such  in  the  Company's  ships  ;  but  since  the  trade  has  been 
opened,  all  kinds  Jind  a  ready  outlet;  and  as  the  demand  oAen 
exceeds  the  supply,  a  manufactured  article  is  furnished  to  the  rival 
crews,"  • 

Notwitlistonding,  however,  the  occasional  use  of  foreign  leaves,  we 
can  state,  from  the  careful  examination  of  a  liir<,'e  number  uf  samples, 
that  the  ^reat  bulk  of  the  tea  iuii>or(ed^  especially  the  black  tea,  is 
but  little  affected  by  this  adulteration.  We  have,  however,  on  several 
occasions,  met  with  foreign  leaves  and  paddy-husk  in  some  of  the 
inferior  descriptions  of  green  tea,  an<i  in  samples  of  the  article  to  be 
described  hereafter,  manufactured  by  the  Chinese,  and  denominated 
Lie  tea. 

The  first  tea  in  which  we  discovered  foreign  leaves  was  a  sample 
of  Gunpowder  fWoping  tea).  Subse*|uently  four  different  samples  of 
of  low  (juatity,  as  imported  into  this  country  from  China,  were 
•  Aitklo  "  Tea,"  U  pMoy  C^yolopadta. 


76 


TEAj   AND   ITS  ADULTEHATI0X8. 


8ubject«J  to  micro<tcopic  examinntion,  and  were  all  found  to  be  adul- 
lorated  with  forLnj^n  leaves. 

In  a  sample  of  (iuripowder  fragments  of  two  kinds  of  foreign  leaves 
were  detwleil.  'i'lie  tea  m  question  coiisjisted  in  part  of  leaves,  and 
partly  uf  Lit;  tea.  Now  those  foruign  leaves  formed  not  only  the 
greater  portion  of  the  loose  leaves,  but  also  oiitcred  largely  into  the 
composition  <tf  the  little  masses  of  wliich  Lie  tea  is  carifltilutcd, 
pcarcely  »  particleof  tea-leaf  itself  having  W-en  observed  in  the  sample. 

The  stnicture  of  two  of  thuae  leaves  ia  show-n  in  the  two  tlfllowing 
figures. 

Fig.  1 1 . 


FoKKiOB  Liir  IV  Lib  Tea. 
a.  vpppr  toTfliot  of  Wtf  I  ^  lowtr  nirfiM.  khcvlrc  the  kHi  vlth  their  iltiititlr- 
bM<1c<l  tnftrjrlnk  tif  which  U  ia  amtiOKd  i  r.  rhlcrnrihyllc  i-clU.  to  >ll*pa«Fd  M 
to  fonii  Terj-  luge  tnolm ;  d,  «lannl«l  c*ll«  Umtui  on  iij)p«i  lurfaer  of  the 
l««f  in  Ihf  courw  Arth«T«lM  i  ',  ipIkI  vmwI  ■/,  mII  of  tiirm«Tle  i  o,  Tngmtnt 
Of  t'roMUD  Mm  t  A.  pArtieJc*  of  the  whiU  powilu,  prolMbljr  Ckimt  day. 

A  sample  of  "  Lie  (ea^*^  admixed  with  a  few  pmall  fragments  of 
leaves,  conHisting  principally  of  portions  of  the  leai",  much  broken  up, 
is  represented  xujig-  12. 

In  A  eampte  of  Ttmnhay,  in  addition  to  those  of  tea,  the  leavea  of 
three  other  plant,i  were  detected,  two  of  which  we  identified,  the  one 
was  Cnmetiin  Sajtanqita^  x\\^  other  a  kind  of  plum:  they  are  repre- 
sented in^A.  1^.  and  14. 


TEA,    AND   ITS  ADULTERATIONS.  77 

A  second  sample  of  ^  Ttranfiay'*  vrna  asceruincd  to  consist  of  tea 
mixed  with  paddv-husk,  purtioiia  of  seed-vessels,  and  other  substances: 
the  leaves  were  of  a  coarse  description,  and  wnntcd  the  peculiar  twist 
characteristic  of  the  more  cnrefully  prep:iri'<l  kini]^  of  tfta. 

The  leaves  of  Chloranthu*  iacauKpicuun^  o-s  well  as  of  CamfUia  5a. 
Ma/it/ua^  have  hecn  known  to  be  emfdnyed  in  the  adulteration  of  tea, 
and  the^  differ  from  tea-leaves  chicUy  in  their  venation      Fig,  15. 

Tlie  second  kind  nf  adulteration  consieta  in  the  luiumfaeture  of 
artjcles  m;ide  up  in  imitation  of  tea,  oa  the  different  varieties  of  Lie  tea. 


FOMIOX  LlAF  IF  Lll    TiA. 

a.  upper  lurflMt  of  iMf  I  h.  lower  luifBoe  i  r,  chlurDphvlle  aeUi :  4,  tlong*tfld 

mm,  f.  |MJrti(inn/o««arih«  t<r«ncbt«]  ftod  tiHiKPUilwIn  ritUKlH  uii  ihd  iui<lcr 

mrftn  «*  ilw  lr»f  i  /.  c«ll  af  tuimuic  j  v.  fncnwM  <rf  PrtwdMi  Uim  i  A,  i«r- 

tklM  cT  Uw  kA.jk  pMnkr.  " 


Adulteration  with  Lie  Tea. 

Now  Lie  lea  i»  so  caUed  because  it  is  a  spurious  article,  and  not  tea 
at  all :  it  consists  of  the  dust  of  tea-leuves,  sometimes  of  fcireign  leaves, 
and  sand  made  np  by  means  of  starch  or  gum  into  little  massefl. 
which  ore  afterwards  painted  and  coloured  so  as  to  resemble  either 
black  or  green  Gunpowder.  The  skill  exhibited  in  the  fiibricntion  of 
this  spurious  article  U  very  great,  and  we  have  met  with  at  least  a 


rs 


TEA,    AND    ITS   ADULTERATIONS. 

Fig.  13. 


I.EAf  or  Camkllia  8A«A)ig4iA,  found  Id  Bunpt«  of  TVraMibiy. 
><,  tipper  ■urfkc*  of  leaf,  i>Knrins  tlw  will  of  vhich  l(  la  maipOMd  i  if, 
■arhcKt  extilUUag  )U  cclu  ■d<1  flomtU  i  C.  chjorophjrik  vk\\%. 

Fig.  14. 


LaAr  or  Vunt,  ftmnd  In  Sunple  of  7VvtNi»w. 
JtiipptriurliuMof  Icafi /(,  tuidcrturfMai  C*  elUorofiiyllfl  eelb. 


TEA,   AND   ITS   ADULTERATIONS. 


rft 


dozeu  varieties  of  it,  differing  from  eacli  other  in  the  size  and  colour- 
ing^oftbe  little  masses. 

This  article,  flUhnnfjh  the  rhcits  contJiining  it  nro  bronded  with 
the  words  "  Lie  tea,"  wiis  at  a  recent  period  extensively  imported  into 
this  country,  and  of  course  found  purchasers. 

It  is  exnresslv  manufactured  for  aduUerationi  and  it  ie  largely 
employed  for  this  purpose  by  the  Chineac  tlieuiselves,  who  mix  it 
with  the  dilVerent  (jiunjMiwUer  tea.-,  black  and  jireen  ;  which  are  so  far 
genuine  that  tliey  ronlain  no  other  k-af  than  that  of  tea,  oltboujjh  they 
are  artificially  colnured.  Gunpowder  tens,  even  notL\  are  frequently 
met  with  containing  various  proportions  of  Lie  tea. 

Fig,  1», 


<4.L*af  orCnLOiAvrmrt  lACDxiricLTm  i  0,  ditto  of  Camkllu  SAiAjrqvAt  I«itm 

IM9(1  tu  MlatMr&u  Ice. 

Mr.  Warington,  in  a  communication  read  before  the  Chemical 
Society  of  London,  May,  1851,  states  :  — 

"  On  inquiry,  I  have  learnt  tliat  about  750,000  lbs.  weight  of  Uiese 
te«s  have  been  iui]>urted  into  this  country  within  the  last  eighteen 
months,  their  introduction  being  tjuitcof  modern  origin  ;  and  I  under- 
stand that  attempts  have  been  made  to  get  them  passed  through  the 


80 


TEA,   AND   ITS   ADULTERATIONS. 


customs  as  manufacbtrcd  goodg^  and  not  tu  teas;  ft  title  which  they 
certainly  richly  merit,  although  it  must  be  ovitiont,  from  a  moment's' 
consideration,  ilmt  the  revenue  would  doubtless  be  defruuded,  iuas- 
inuoh  us  the  cousunier  would  have  tt*  buy  them  as  ttjas  from  the 
dealer.  IL  is  to  be  feared,  hi>wever,  that  a  uiurket  for  them  is  found 
elsewhere.  The  Cliinese,  it  uppoars,  would  not  sell  them  except  as 
teas,  and  have  the  candour  to  upecify  them  as  Lie  teas;  and  if  they 
are  mixed  with  other  tens  of  low  quality,  the  Chinese  merchant 
f^ives  a  certificate,  stating  the  propnrtitm  of  the  Lie  tea  present  with 
the  genuine  leaf.  This  manufacture  and  mixing  is  evidently  prav* 
tiaed   to   meet  the  price  of  the  English  merchant.     In  the  case  of 

Ffc.  IB. 


\  J 


$T^ 


Tmitatiox  Cafsb  oe  OusrowDiiu 

«  A,  fraffTBenU  of  Die  tea-ln\f  or  in%fdm»t;  hh,  putlclc*  of  »«md;  ec> 
oMVMidw;  drf,  grnnp*  of  grmnulwof  Mnrir-iaMf;  r  r,  panicle*  ot  nira-lAt 
nMtttn://,  otUaoT  tmniMrie;  9  a.  rnfmenU  at  iiuUif?.    UatfulOed  310 


the  above  samples^  the  black  ii  called  by  the  Chinese,  Lie  Flotrer 
Caper i  the  green,  Lie  Gunpowder;  the  average  value  is  from  8rf.  to  U. 
per  lb.  The  brokers  have  adopted  the  curious  terms  g^um  and  dusU  as 
applied  to  tlie^e  Lie  teas  or  their  mixtures,  a  cognomen  which  at  first 
1  Dad  some  diHiculty  in  understanding:,  from  the  rapid  manner  in 
which  the  Grat  two  word*  were  run  Icigether," 


TEA,  AND  ITS  AD0T.TERATIOXS. 


61 


"Mr.  Ripley,  tea  broker,  in  evidence  before  ihe  ParltamentAry  Com- 
mittcCf  states  that  tlio  importfttion  of  Lie'Jca  in  1847  amounted  to  about 
100,000  lbs.,  after  which  it  increased  about  tbrecrold,  and  eventually 
it  became  as  lar^  as  400,000  or  200,000  lbs. 

Artificial  Colouration  and  Adttiieraiion  of  Tea. 

The  third  principal  kind  of  adultcraCton  to  which  tea  is  liable 
consists  in  the  glassing,  painting,  or  artificial  colouration  of  the  leaves. 
This  practice  is  had  recourse  to  for  the  purpose  of  improving,  as  some 
consiaer,  the  appearance  of  certain  descriptions  of  tea,  especially  the 
inferior  kind.^  and  for  the  better  concealment  of  some  of  lU  adulter- 
ations, OS  where  foreign  leaves  arc  used,  and  to  disguise  more  effec- 
tually the  nature  of  Lie  tea. 

The  substance  employerl  in  the  glazing  of  the  varieties  of  black  lea 
known  as  scentt^d  Caper  or  black  Gunpowder,  orange  Pekoe  and  the 
black  variety  of  Lie  tea,  U  one  with  which  houseniaidii  are  particularly 
familiar,  viz.  fp*uphitc,  plumbattc,  or  black>lead.  The  teas  coated  with 
this  substance  present  a  jmruliarly  smooth  and  glossy  appearance. 

OccasioDuIly  small  quantities  of  Prussian  blue  or  indigo,  turmeric, 
China  clay,  or  some  other  yellow  and  white  powders,  are  useil,  as  well 
as  the  blaok'lead,  in  order  to  impart  a  somewhat  different  appear- 
ance to  Cliulnn  and  black  Lie  tea. 

Bui  it  is  with  greeu  tea  that  the  practice  of  artificially  colouring  the 
leaves  is  carried  to  the  greatest  extent.  The  varieties  of  green 
tea  imported  into  this  country  from  China  are  Twankay,  Hyson-skin, 
voung  Hyson,  Hyson,  Imperial,  and  Gunpowder,  Now  the  colour  of 
the  whole  of  these  teas,  without  a  single  exception,  is  artifieial,  and 
caused  by  the  adherence  to  the  leaves  of  various  colouring  matters. 

The  usuitl  colouring  matters  employed  an;  fcrrocyanidc  of  iron  or 
Prussian  blue,  turmeric,  and  China  clay;  these  nrc  mixed  in  various 
proportions,  so  as  to  pruduce  different  shades  of  blue  und  green  ;  the 
surface  of  the  leaves  being  moisteneii,  they  are  then  agitated  with  the 
mixtures  until  they  become  faced  or  ghi«ed,  as  it  is  termed. 

Occasionally  other  substances  are  employed  by  the  Chinese,  aa  indigo 
and  nilpbatc  of  lime,  or  gypsum.  In  proof  timt  it  has  long  been  the 
pmctice  fref|uently  to  colour  preen  tea  arti6cia]Iy,  we  have  the  evi- 
dence of  various  travellers;  but  the  must  conclusive  and  complete  evi- 
dence, both  as  to  the  extent  of  the  practice  and  the  nature  of  the 
ingrc'liont*  used,  has  been  suppUed  by  meuns  of  the  microscope. 

Amongst  the  writers  who  have  noticed  the  subject  of  the  iirdficial 
colouration  of  tea  may  be  mentioned  Dr.  Horsfield.  Dr.  Koyle,  Mr. 
Davis,  Mr.  Bnicc,  Mr.  Ball,  Mr.  Fortune,  and  Mr.  Warington. 

In  Dr.  Horsfield's  translaticm  of  n  Dutch  work  on'tlie  subject 
of  the  cultivation  of  tea  io  Java,  tlie  following  dialogue  occurs  :  — 

^  Visitor*  —  Is  It  indeed  the  case  that  tea  is  so  much  adulterated 
in  China  y 


83 


AND  ITS  ADULTERATIONS, 


"  SuperinUndeht. — UrKiuuslinnntlyTbul  nol  in  the  interior  provinces, 
for  ihore  exist  rijrid  laws  oj^ninst  the  uduliorution  of  tea ;  and  all  tens, 
as  tliey  come  out  of  the  planlntions,  are  examined  on  the  part  of  the 
povernment,  to  determint;  whtiihor  they  are  genuine;  but  in  Canton, 
which  is  the  emporium  of  teas,  nnd  especially  at  lIoni\n,  muny  fiorts, 
indeed  most  tea.%  are  pxeatly  aditlterated,  and  that  with  injrredienta 
injurious  to  healthf  especially  if  too  much  of  these  ingredients  be 
added.  This  is  especially  the  case  with  the  ^'reeii  tea,  in  order  to 
improve  the  colour,  and  in  this  manner  to  add  to  the  vidue  of  the  teu 
in  the  eyes  of  the  common  consumers. 

"  Visiitfr. —  Are  these  ingrecJienis  known  ? 

**  Superijitrmlent.  —  Most  of  ihem  are  certainly  known;  they  have 
been  communicated  to  government  (the  Dutch  government),  while  at 
the  same  lime  the  privile^ti  has  been  requested  that  they  might  not 
be  employed  here;  ami  although  this  occasions  loss,  the  retjuest  has 
been  gnutted,  and  it  has  been  ordered  by  government,  that  not  the 
least  admixture  should  take  place,  cither  to  improve  the  colour  or 
taste  of  llie  tea,  even  in  such  coses  where  this  mijrht  be  desirable."  • 

Dr.  Royle  writes  t»  "  The  Chinese  in  the  neighbourhood  of  Canton, 
ore  able  to  prepare  u  tea  which  can  be  coloured  and  made  up  to  imitate 
various  quuUlie^  of  green  tea,  and  large  quantities  are  thus  yearly 
made  up. 

"Young  Hyson,"  states  Mr.  Davis  J,  "until  spoiled  by  the  large 
demand  of  the  Americans,  wos  a  delicate  genuine  leaf,  and  as  it  could 
not  be  fairly  prociuced  in  any  large  quantities,  the  call  for  it  on  the 
part  of  the  Amencanfl  was  answered  by  cutting  up  and  silling  other 
green  teas  through  sieves  of  a  certain  size,  and  as  the  Corapany*8 
inspectors  detected  the  imposture,  it  formed  no  portion  ot  their 
London  importation.  But  the  &buse  became  still  worse  of  late,  for 
the  coarsest  blark  tea-leaves  have  been  cut  up,  and  then  coloured  with 
a  pre]>aration  rcsemhling  the  hue  of  green  tcad." 

*'  but  (his  was  nothing,"  continues  Mr.  Davis,  "in  compariflon  with 
the  ertrontery  which  the  Chinese  displayed  in  carrying  on  an  extensive 
manufacture  of  green  teoM  from  (hinutged  hbivk  leave*^  at  ft  village  or 
suburb  called  llon&n. 

"  The  remission  of  the  tea-duties  In  the  United  States  occasioned, 
ia  the  years  1832  and  1833,  a  demand  for  green  teas  at  Canton, 
which  could  not  be  supplied  by  arrivals  frnm  the  provinces,  The 
Americans,  however,  were  obli^e<l  to  sail  with  cargoes  of  green  teas 
within  the  favourahle  season;  they  were  determined  to  have  the  teas, 
and  the  Chinese  were  determined  that  they  should  be  supplied.  Certain 
rumours  being  allout  concerning  the  manufacture  of  green  tea  from 
old  black  leaves,  the  writer  of  this  became  curious  tu  ascertain  the 
truth,  and  with  some  difficulty  |M;rsuftded  a  Hung  tiierehnut  to  conduct 
liim,  accompanied  by  one  uf  the  inspectors,  to  the  place  where  the 

•  Eiuy  rvn  th«  CuUlvaUnn  und  NaDH&ictun!>  or  Tm  Iq  Jiti.  Traoilittftt  from  the  Dutcb. 
t  Tea,  MMllclnil  aud  DietetlmL  — ^awv  CifCloMdia, 
1  Darli*  Chln«»e,  vt>l.lL  \>.  4Si. 


I 


I 


TEA,   AND   ITS   ADULTEnATIOXS. 


63 


itiorw  were  cftiried  on.  Entering  one  of  these  laborataries  of 
fictitiotiB  Hrson,  the  pnriies  were  wiinessw!  to  a  tttranjcu  scene.  I'be 
dtmaged  buck  tea-leaves,  after  being  dried,  were  trsn^ferreil  to  a 
CMt-iron  pan,  placed  over  a  furnai'(*,  and  stirred  rapidly  with  the 
huid«  a  fiinnll  quantity  of  turmeric,  in  powder,  having  been  previnusly 
'fttrwlure*!.  This  gives  the  It^avcs  n  yellowish  or  ornnge  ting*-,  hut.  they 
ren.'  9tiU  to  be  made  (rreen.  For  this  purpose  some  lumps  of  fine  blue 
producedf  together  with  a  substance  in  powder^  which  from  the 
given  to  them  by  workmen,  as  well  as  thuir  at>|>earunce,  were 
m  at  once  to  be  Prussinn  hlue  and  jiypsuni.  These  were  tri- 
irated  finely  together  with  a  suiall  [>estle,  in  such  pru[iortion:*  (is 
lid  the  djrk  colour  of  the  blue  to  a  light  shade ;  ami  a  quuntity 
lo  a  teftspoonful  of  the  powder  being  added  to  the  yellowish 
,  theM  were  stirred  as  before  over  the  fire  until  the  tea  had 
the  fine  bloom  colour  of  Hyson,  with  very  much  the  mme  xcent. 
prevent  all  positibilicy  of  error  regarding  the  substances  employed, 
»!«•  of  them  were  carried  away  from  the  place.  The  Chinese 
quite  conscious  of  the  real  character  of  the  occupation  in 
they  were  engaged;  for  on  attempting  to  enter  several  other 
where  the  came  process  was  going  or,  the  doors  were  speedily 
ti|>on  the  jtarty ;  indee<l,  had  it  not  been  for  the  iniloence  of  the 
it  who  (jr>nducted  them,  there  would  have  been  little  chance  of 
ig  as  mncb  as  they  did.** 

!r.  Bruce  stateti,  that  "  in  ihe  last  operation  of  colouring  the  green 
a  mixture  of  sulphate  of  lime  and  indigo,  very  finely  pulverised, 
lift«<<i  through  fine  muylin,  in  the  proportion  of  three  of  the 
ftrroer  to  one  of  the  latter,  is  added ;  to  a  pan  of  tea,  eontaiiiirig  seven 
p-'Un'U,  alxiut  half  a  teaspoonful  of  this  mixture  is  put,  iiod  rubbed 
«.nd  roilo^l  along  with  the  tea  in  the  piin  for  alwrnt  an  hour.  The 
aUvfe  mixture  is  merely  to  give  it  a  unifonn  colour  and  ap[K?arance. 
Tlie  indigo  gives  it  the  colour,  and  the  itulphnte  of  lime  files  it."  • 

In  Mr.  Ball**  vHluoble  work,  already  (juoted,  we  meet  with  the  fol- 
lo«in|^  ob«erraiions  relating  to  the  artificial  or  factitious  colouring  of 
cotaui  desariptions  of  erecu  tea  :  — 

**The  Utter —  vix«  The  Singlo  Hysons  and  *  Superior  Twanktiy'  — 
lunre  fi^nently  a  glazed  appearance,  vla  also  the  Singlo  Gujif>ow- 
Au%  which  I  imagine  may  formerly  have  arisen  more  from  the  (pia)ily 
of  Cbc  I{»f  than  from  any  factitious  means  emplovetl  to  produce  the 
eelaar,  Slill  in  some  casen  a  small  quantity  ol  colouring  matter  may 
ksTc  been  used.  It  has  al&o  1>ccn  snown  that  the  tea  made  from  the 
HooAb  IcATca  bod  a  glazed  appearance.  It  nevertheless  is  true,  that 
when  the  leaf  is  deficient  in  tne  requisite  colour,  the  Chinese  do  not 
beitUitc  to  employ  colouring  nuiltifr  to  improve  it. 

**  Again,  Ki  fii-r  as  the  churai'teristic  colour  of  gi'cen  tea  rs  concerned, 
die  node  of  producing  it  has  been  explained  and  e»tubli»hed.  If  fac- 
titioai  meant  ore  now  generally  or  almost  universally  adopted  to  imi- 

*  Rtfion  en  lh«  3l»ntirMture  of  Tea 
O  2 


84 


TEA,   AND  ITS  ADULTERATIONS. 


tAte  or  increase  the  eCTect  of  tlie  natural  colour,  it  may  be  considered 
tu  a  great  and  novel  obuse,  and  ought  to  be  discouraceU  hy  brokers 
and  dealers.  It  is  injurious  to  flavour.  Whether  the  Chine.st?  do  em- 
ploy oolonrinf;  matter  or  not  for  the  teas  they  use  thcinsclvt-s,  there 
can  be  no  doubt  tbtit  the  bulk  of  the  Hyson  teas  of  the  present  day, 
and  indeed  all  destTiptiona  of  green  tea,  arc  now  glazed  to  a 
dcj^ec  which  would  have  insured  their  rejcctiun  by  the  East  India 
Company/* 

Tien  Hing,  described  by  Mr.  Ball  as  a  respectable  tea  merchant 
and  factor,  in  his  account  of  the  method  of  making  Twankiiy  tea, 
writer, — 

*'  In  the  seventh  or  eijibtb  moon  (August  and  September)  each 
parcel  is  compared  together,  when  such  aa  correspond  in  quality  and 
colour  are  formed  into  one  pile,  roaated  three  cA^Aian^,  the  dust  sifted, 
and  the  tea  pai:ked  (hot)  In  chests  for  Ciinton.  The  Iciived  of  the 
Becnn<l  patherings  have  no  juices,  are  light,  thin,  and  of  no  sulistance; 
the  infusion  weak  and  tasteless,  the  colour  red,  ami  the  infuseil  leaves 
black.  If  very  coinmnn  and  old,  colonring  nuitter  is  tlien  U5ed.  ITie 
factitions  colour  is  produced  by  a  mixture  of  Ma  Ivy  Hocy,  Tien  Hoa 
(indigo),  and  She  Kno  powder  (calcined  foliated  pypsum).  Tlic 
smallest  quantity  put  into  the  kuo  at  one  time  is  one  or  two  tea- 
spoonfuls,  and  the  largest  three  or  four.  The  colour  then  changes 
to  a  light  blue.  The  fire  niust  be  mode  of  charcoal,  and  much  atten- 
tion paid  to  (be  roasting.  Now,  if  the  chest^n  be  not  in  readinesif.  it  ia 
to  be  feared  the  tea  may  be  mixed  with  falso  leaves,  the  smell  thereby 
injured,  and  the  tea  rendered  unhealthy.  But  I  must  refer  you  to  abler 
men  than  myself  for  instruction  on  that  point.  I  have  no  information 
on  Buch  practices." 

Mr.  Ball  then  goes  on  to  state  **  that  most  other  nierehanlA  or 
TactorB  ain'ee  with  the  foregoing  account  of  the  Twankay  teas,  and 
particularly  as  to  the  circumstance  of  their  being  portly  glazed  or 
coloured  by  artificial  means,  and  also  that  some  chops  arc  mixed  with 
leaves  that  are  not  tea-lenves."  • 

Another  writer,  Mr.  Fortune,  who  also  saw  the  colouring  of  tea 
performed  in  Chinri,  and  who  has  described  the  process  minutely, 
states  that  during  one  part  of  the  operation  the  hand.s  of  the  work- 
men are  ijuite  blue.  "  I  could  not  help  thinking,"  he  remarks,  "tliat 
if  any  green-tea  drinkers  had  been  present  during  the  operation,  iheir 
taste  would  have  been  corrected  and  improved. 

'*  One  day  an  English  gentleman  in  Snanhae  being  in  conversation 
with  some  Chinese  from  the  green-tea  country,  asked  them  what 
i^easons  they  had  for  dyeing  the  tea,  and  whether  it  would  not  be 
better  without  undergoing  this  process.  They  acknowledged  that 
tea  wa.**  much  better  when  prepared  without  having  any  such  ingre- 
dients mixed  with  it,  and  that  they  never  drank  dyed  teas  ihemBclvea ; 
hitt  remarked  that  as  foreigners  seemed  to  prefer  having  a  mixture  of 

*  Oo  Uir  CalUv»ti(Hi  and  Miuiufaclar«  of  Tea. 


TEA,  AND  ITS  ADULTERATIONS.  81 

Prussian  blue  and  gynsimi  with  Uieir  ten  to  mukc  it  look  uniform  ami 
prettjt  and  as  these  ingrefiients  were  cheap  enough,  the  Chinese  Imd 
no  objection  to  supply  tliem,  especially  aa  such  teas  always  fetched  a 
hieher  price."  * 

Air.  AVarint^n  communicBted  a  valuable  paper,  on  the  artificial 
colouration  of  tea,  to  the  Chemical  Society,  in  1844.     He  writes, — 

"  In  examining  lately  some  samples  of  tea  which  had  been  seixed 
froin  their  being  supposed  to  be  spurious,  my  attention  was  arrested 
by  tf»e  varied  tints  which  the  sample  of  green  tea  ejthibited,  extending; 
from  a  dull  olive  to  a  bri;;ht  ijreenishblue  colour.  On  submitting 
this  to  the  scrutini^sin;;  test  of  examination  by  the  microscoi*  with  a 
magnifying  power  of  one  hundred  timed  linear,  the  object  being  iltu- 
mioaied  bv  reflected  light,  the  cause  of  this  variation  of  colour  wo^ 
imroediatefy  rendered  apparent,  for  it  was  found  tbat  the  curled  leaves 
were  entirely  covered  with  a  wbite  powder,  haviiig  in  places  a  sliyhlly 
glistening  aspect,  and  these  were  interspersed  with  small  granules  of  a 
bright  blue  colour,  and  others  of  an  orange  tint;  in  the  folded  and 
conse<pienlly  more  protected  parts  of  the  curled  leaves  these  were 
more  distinctly  visible," 

Mr.  Warincton  subsenuently  examined  several  other  samples  of 
green  tea  as  miported,  the  whole  of  which  be  found  to  be  arliBci&lly 
col  uu  red. 

Lastly,  in  the  Museum  of  Economic  Botany  attached  to  the  Kew 
Botanical  Gardens,  tlieie  are  some  9[>ccimens  of  tea  dyes,  used  by 
the  Chinese  to  colour  their  green  teas.  These  were  procured  by 
Mr.  Berlhold  Seeman  from  one  of  the  tea  factories  at  Canton. 
They  consist  of  Prussian  blue,  turmeric,  chalk,  and  cither  China  clay 
or  gypsum-t 

It  appears,  therefore,  from  these  examinations  that  the  green  teas,  as 
imported,  are  very  frecjuently  faced  or  coloured  artificially.  Our  own 
investi^'fltions,  embracing  a  great  variety  of  samples,  show  thot  nearly 
the  tvkffc  of  the  green  feas  imported  into  this  country^  ax  retailed  in 
the  MhojiHy  are  tkwi  coloured;  and  that  when  not  thus  coloured,  there 
is  but  little  in  appearance  or  colour  to  distinguish  green  from  black 
tea  :  the  chief  difference  in  colour  being  that  the  former  is  sometimes 
inclined  to  olive. 

In  the  Museum  at  Kew  will  be  found  a  series  of  samples  of  block 
and  green  tea,  also  of  several  didercnt  varieties  of  l^ie  tea,  all  artifi* 
cially  cdoured,  being  some  of  tho<ie  met  with  by  ourselves  in  the  course 
of  our  investigations  into  the  subject  of  the  adulteration  of  tea. 

It  is  a  question  deserving  consideration,  how  far  the  colouring 
BAtten  employed  exi>lain  the  injurious  effects  which  result  in  some 
cases  from  uic  use  of  green  tea.  The  Chinese  themselves  never  make 
of  these  glazed  teas  —  a  rather  significant  fact 


•  T«  Countrir*  of  China. 

t  Sm  Food  and  lu  AdultentioDi,  p.  aSS. 

u  3 


u 


TEA,    AND   ITS    ADULTERATIONS. 


Adultcrationt  of  Tea  practised  in  Oiia  Country, 

We  now  pass  on  to  the  consideration  of  Aose  aduUerntioM  which  are 
practised  in  thin  country. 

Fig.  IT. 


^.LmToPWillov  I  R,  dllto  of  TorLAB. 

AduIterntorB  in  this  country  have  succeeded  in  imitating  with  con- 
siderable skill  the  practices  of  the  Chinese. 

Thus  they  sometimes  use  foreijzn  leaves  to  mix  with  {genuine  tea, 
and  they  face  the  fabricated  article  willi  various  colouring  matters, 
ACcnrdinjT  oa  it  is  to  resemble  bliirk  or  green  ten. 

These  leaves,  with  the  exception  of  sh»e  leaves,  arc  never  useil 
whole;  but  they  are  broken  up,  mixed  wiih  gum  and  catechu,  and 
itiadti  int-o  little  masses  like  those  of  Lie  tea;  these  are  subsequently 
coloured  either  black  or  green  as  may  be  requiretl. 

It  is  of  but  little  conscijuence  what  kind  of  leaf  is  employed  for 

i  purpose ;  any  leaves  that  are  readily  procurable  will  answer  the 

•e.     The  following  leaves  have  been  det^»cled  ut  dilTerent  times, 

Uy  by  llic  Exci:iCi  eDterin<;  Into  the  formation  of  spurioiu  teas 


TEA,  AND  IT8  ADULTERATIONS. 


87 


of  British  fabrication :— Beech,  elm,  horse-chesnut,  plane,  bastard 
plane,  fancy  oak,  willow,  poplar,  hawthorn,  and  sloe. 

Fig.  I«. 


C,  L««f  oTpLAirat  D,  ditto  of  Oak. 

Some  of  the  leaves  above  named  are  represented  in  the  accompany- 
ing engravinga. 

The  colouring  matters  employed  are  often  more  injurious  than 
those  use<l  bj  the  Chinese  :  the  fiiibstanccA  aclually  detected  are  the 
followihp  :  rose  pink»  Dutoh  pink,  catechu,  chromutcof  lend,  Bulphate 
of  iron,  Venetian  red,  soap-stone  or  French  chalk,  carbonate  of  lime, 
carbonate  of  magnesia,  carbonate  of  copper,  arsenite  of  copper,  the 
chromates  of  potash,  Prussian  blue,  and  indigo. 

Dutch  pink,  rose  pink,  catechu,  sulphate  of  iron,  carbonate  of  lime, 
carbonate  of  magnesia,  soap-^tone,  PruMian  blue,  and  indigo  have  been 
repeatedly  met  with  in  adulterated  tea,  in  some  instances  by  the 
Kxcise  authorities. 

The  following  particulars  in  reference  to  the  use  of  Boap-stone  or 
French  chalk  are  taken  from  an  article  in  the  "  Household  Words  ** 
under  the  title  of  "Death  in  the  Tea  Pot  :*' — 

•'  By  the  belp  of  Mr.  Slivers,  we  were  enabled  in  a  recent  number 
to  ex|)Ose  to  an  injured  public  some  of  the  ingre<lient«  of  metropolitan 
milk  —  *  London  Genuine  particular.*  A  correspondent  now  makes  a 
further  revelation  uf  how  our  tea-jKits  are  defiletl  when  it  is  innocently 
mppoted  thai  a  pure  bcTeragc  is  in  course  of  concoction. 

Q  4 


68  TEA,  AND   ITS   ADULTERATIONS. 

**  *A  short  time  s'moe/  he  saj?,  *a  friend  of  mine,  a  chemist  in 
Manchester,  ivoa  applied  to  for  a  quantity  of  French  chalk,  u  species 


A,  Leaf  of  the  IlAVTBni*  i  It,  dllto  of  Ike  Sloe,  or  Wild  Pum  i  T.  ditto  of  Uw 
Bum  I  />.  ditto  of  ttM  ELCiKii  :  A',  ditto  of  tb«  Eui. 

•  •  Til'  «ho1e  iir  the  IrKTM,  rievut  tbftt  uf  tlie  nunellla.  ate  flfitrM]  OB  Ibilr 
unJVr  ■urfuw*.  Ttic  dm.  pluM,  uiil  o«k  Ic&tim,  frocn  vhldi  th«  tkvtehM  wva 
prcpBKilt  wtrc  of  email  u«c. 

of  talc,  in  fine  powder;  the  party  who  purchased  it  used  regularly 
several  pounds  a  week.  Not  being  an  article  of  usual  sale  in  Mieh 
quantity,  our  frieDd  became  curious  to  know  to  what  use  it  could  be 
aM>Ued;  on  asking  the  wholesale  dealer  who  supplied  hiint  he  stated 
his  belief,  that  it  was  used  in  "^fing-"  tea  (the  last  piocess  of  con- 
verting black  tea  into^reen),  and  that  within  the  last  month  or  two, 
he  hml  sold  in  Manchester  upwards  of  a  thousand  pounds  nt'  it.  Our 
fnend  the  chemist  then  instituted  a  series  of  experiments,  and  the  re- 


TEA,  AND  ITS  ADULTERATIONS. 


89 


suit  proved  tbnt  a  great  deal,  if  not  nil  tho  common  green  tea,  used  in 
this  country,  is  coloured  artilioiully.  The  vory  first  experiment  do- 
suoDDtrjted  fraud.  The  plan  adopted  was  as  follows  :  —  A  few  sjjoon- 
iulii  of  green  tea  at  five  shillings  a  pound,  were  placed  on  a  soiult 
[SteTeii  and  held  under  a  gentle  stream  of  cold  wnter  flowing  from  a  tap 
[lor  the  space  of  four  or  five  minutes.  The  tea  quickly  changed  itj 
^eolour  from  green  to  n  dull  yellow,  and  upon  drying  with  u  very 
sentlc  heat  gradually  assumed  the  appearance  of  ordinary  black  tea. 
On  making  a  minute  microscopic  examination  of  the  colouring 
matter  washed  from  the  leaf,  and  which  was  caught  in  a  vessel  bcluw, 
it  appeared  to  be  CDui]]0sed  uf  tlirec  substances,  particles  of  yellow, 
blue,  and  white.  The  blue  was  proved  to  be  Prussian  blue  ;  the 
yellow  thought  to  be  turmeric  ;  and  the  white,  French  chalk.  If  the 
two  former  be  mixed  together  in  fine  powder,  thoy  will  give  a  green 
of  anj  required  6h»dc.  It  is  made  to  adhere  to  the  tea-leaf  by  some 
tdheaivc  matter,  nnd  then  it  is  ^*  faced  "  by  the  French  chalk,  to  give 
it  the  pearlv  appearance  so  much  like<i. 

"  '  This  simple  experiment  any  one  can  perform.  A  gentleman  »a- 
sured  me  that  a  friend  of  bis  a  short  lime  since  happened  —  though 
quite  unintentionalty  on  his  port  —  to  walk  into  a  private  room  con- 
nected with  the  establishment  of  a  wholesale  tea-denier,  and  there  be 
saw  the  people  actually  at  work  converting  the  black  tea  into  green  ; 
the  proprietor  soon  dLicnvered  his  presence  in  the  room,  and  before 
him.  in  no  measured  tenns,  severely  rcpriuiandcd  the  workmen  for 
having  permitted  a  stranger  to  enter.*  " 

Carbonate  of  cop|«fr  (X'curred  to  the  extent  of  35  per  cent,  in  some 
tea  which  was  seized  in  London  by  the  Excise  in  1843. 

The  tea  into  the  facing  of  which  the  chromatea  of  potash  entered 
wa5  seized  in  Manchester  in  1845. 

The  following  articles  were  likewise  seized  on  the  premiacs,  evidently 
intended  to  be  used  in  the  colouring  of  adulterated  tea :  — 

A  mixture  of  chromate  of  lead  and  carbonate  of  lime. 

Arsenite  of  copper. 

A  mixture  of  indigo,  chromate  of  lead,  and  carbonate  of  lime. 

A  mixture  of  arsenite  of  copper,  carbonate  of  magnesia,  and 
Venetian  red. 

In  lft48  other  soizurea  of  adulterated  green  tea  occurred. 

In  some  instances  the  colouring  matters  employed  to  face  the  tea 
have  amounted  to  7,  8,  and  even  to  9  per  cent. 

Sometimes  an  infei-iur  black  tea,  or  a  re-dried  black  tea,  ia  luiificially 
coloured,  and  so  converted  Into  a  green  tea. 


AthiUtroHon  with  Exhaustefl  Tea~Uuve». 

At  other  times  exhausted  tea-leaves  are  treated  with  sulphate  of 
iron,  catechu,  and  gum,  to  give  them  colour,  ostringency,  and  gtotf, 
and  sold  again  as  black  tea,  or,  when  coloured^  as  green  tea. 


90 


TEA,   AND  ITS   ADULTERATIONS. 


The  clicmical  composition  of  a  tea  tlvus  made  up  from  exliausted 
leaves^  t3  of  course  very  diflTfrent  from  genuine  and  unused  black  teo, 
as  appears  from  the  following  analyses :  — 

Unused  Black  Tea, 


By  Frank. 

By  Phillipa, 

Tannin 

40-6 

Lignin 

46-8 

Gum      -        -        _ 

6-3 

Gum     -         -        - 

5-9 

Woody  fibre   - 

4-1-8 

Tannin 

425 

Glutinoua  matter     - 

6-3 

Albumen    and     co- 

Volatile matter  and 

louring  matter    • 

4-8 

loss    -        -        . 

20 

]00-0 


1000 


Genuine  green  tea  contains  about  the  same  proportion  of  gum  as 
black. 

Exhausted  Slack  Tea,  re-dried  and  made  vp  tcith  Gutn, 

By  Phillips. 
Lignin  -        -        .         -        78-6        .        78*1 

Gum    -----         15-5        -        20-5 
Tannin  and  colouring  matter  5-9  ,      -  1*4 

100-0  100-0 

"When  the  re-dritMl  leave.v  in  addition  to  being  made  up  with  gum, 
are  artilioially  coated  or  coloured,  nearly  the  same  different^es  of  eom- 
poaition  exi»t. 

Contrasting  the  analyBcs  of  exhausted  tea-leaves  made  up  vr'ilh  gum« 
vith  those  of  genuine  teu,  it  will  be  seen  that  while  the  amount  of 
tannin  in  the  I'onner  ia  very  much  reduced,  the  r[uuutity  of  liguiu, 
and  also  of  gum,  is  greatly  increased. 

The  following  observations  in  reference  to  the  eroplovment  of  ex- 
hausted tea-leaves,  ore  by  Mr.  George  Phillips,  of  the  Inland  Revenue 
Office:  — 

"In  the  year  1843,  there  were  many  coses  of  re-dried  tea-lcavcs, 
which  were  prosecuted  witli  vigour  by  this  board,  and  the  result  was, 
so  far  as  we  could  ascertain  at  the  time,  the  !iuppre:$siou  of  the  trade. 
It  was  supposed,  in  1843,  that  there  were  eight  manufactories  for  the 
purpose  of  re-drying  exhausted  tea-leaves  in  London  alone,  and  several 
Desides  in  various  parts  of  the  country.  The  practice  pursued  was  iia 
follows ;  —  Persona  were  employed  to  buy  up  the  cxnnustod  leaves 
at  hotels,  cofiee-housc!*,  and  other  places,  at  '2^<I.  and  Ori.  |>er  pound. 
These  were  taken  to  the  factories,  mixed  with  a  solution  of  gum,  nu<i 
re-dried.  After  this,  the  dried  leaves,  if  for  black  tea,  were  mixed 
with  rose  pink  and  black-lead,  to  face  them,  as  it  is  termed  by  the 
tra<ie." 


TEA,   AKD   ITS  ADULTERATION^. 


91 


I 
I 


These  fahricnted  tea.s  nrc  seldoui  sold  alone  to  the  public,  but  are 
used  for  mixing  with  tlie  riKtre  genuine  teas. 

Adtd/fmtion  wUh  Foreign  Leaces. 

As  illufltmting  iLe  adulteration  of  tea  villi  foreign  leaves,  the  fol- 
lowing case»  may  be  cited  :  — 

On  ibe  18ib  of  December  1820,  a  seizure  of  spurious  tea  was  made 
by  the  Excise  in  Liverpool,  on  the  premises  of  John  Stevens,  where  a 
regular  mnnufnctory  was  carried  on.  Samples  nf  the  articles  seized 
were  presented  to  us  by  Dr.  Muspratt  and  Mr^  Phillips  of  the  Inland 
Revenue.  One  of  the  samples  consisted  of  a  mixture  of  the  entire 
dried  leaves  of  the  sycaraure,  and  hnrse-cbcsnut.  In  another  specimen 
the  leaves  were  so  broken  Ouwn  that  it  was  searculy  possible  to  iden- 
tify them  without  the  aid  of  the  niieroscoj>e.  A  third  sample  con- 
sisted of  large  tumps  of  Irregular  size  and  shape,  fnnned  of  thtf  broken 
leaves,  including  even  the  stalks,  agglutinated  by  means  of  catechu. 
In  another  specimen  these  masses  were  broken  down  into  smaller 
masses  or  fragments,  resembling  tho^e  of  gunpowder  tea.  In  this  state 
the  article  was  ready  cither  for  mixing  with  genuine  black  tofi,  or  for 
being  fflce<l,  in  imitation  of  green  gunpowder ;  lastly,  otiier  samples 
were  coloured  with  indigo.and  very  closely  resembled  the  green  gun- 
powder tea  of  the  Chinese. 

In  this  case,  then,  we  have  not  only  the  use  of  foreign  and  worthless 
leaves,  but  these  were  forraetl  into  masses  resembling  those  of  Lie  tea ; 
and  lastly  these  masses  were  artificially  coloured  after  the  manner  of  the 
Chinese. 

But  seizures  of  adulterated  tea  of  Briti.sh  fabrication  havf  been 
made  even  more  recently  than  that  above  referred  to.  The  Aillowing 
account  of  proceedings  of  the  Clerkenwell  Police  Court,  is  copied  from 
"  The  Times  "  of  May.  1 85 1 :  — 

"  Kdward  South,  and  Louisa,  his  wife,  were  placed  at  the  bar,  before 
Mr,  Combe,  charged  by  Mr.  Inspector  Brennan,  of  the  G  division, 
with  being  concerned  in  the  manufacture  of  spurious  tea. 

"  It  appeared  from  the  statement  of  the  inspector,  that  in  conse- 
quence of  information  that  the  prisoners  and  others  were  in  the 
habit  of  carrying  on  an  extensive  traffic  in  manufacturing  spurious 
tea  on  the  premises  situate  at  27^.  ClerkenwelUcIoiiie,  Cterkenwell- 
green,  on  Saturday  evening,  at  about  seven  o*c]uck,  the  witness,  io 
company  with  Sergeant  Cole,  proceeded  to  the  house,  where  they 
found  the  prisoners  in  an  apartment,  busily  engaged  in  the  manufac- 
ture of  spurious  tea.  There  was  an  extensive  furnace,  before  which 
was  suspended  an  iron  pan,  containing  sloe-leaves,  and  tea-leaves 
which  they  were  in  the  practice  of  purchasing  from  coflee-sbop  keepers, 
after  being  lued.  On  searching  the  place,  they  found  on  immense 
quantity  of  used  tea,  bay-leaves,  and  every  description  of  spurious 
ingredients*  for  the  purpose  of  manufacturing  illicit  tea,  and  they 


TEA,  AND  1TB  ADTTLTEEATIONS. 

were  nilied  with  solution  of  gum  and  a  quantity  of  copperas.    Tlie 
heal  of  the  place  was  so  excessive,  that  the  officers  could  scarcely 

F(f.  90. 


La  Vhxo  Hiiro, 
a  «.  frkcmeau  of  tlie  nmafJt  ^m  rr> ;  &  h,  MTtieka  of  gam  cai<itku  : 
c  I',  cry^ott  uiualljr  pincnt  iu  mUcUti.    MifnUlcd  3A0  dtunttm. 

remain  in  it,  but  the  prisoners  did  not  seem  at  all  oppressed  by  it. 
The  woman  was  employed  in  stirring  about  the  bay>letLves  and  other 
compositions  with  the  solution  of  gum  in  the  pan  ;  and  in  one  part  of 
the  room  there  waa  a  lar^e  quuntity  of  spurious  stuff,  the  exact 
imit-ation  of  gtfnuine  tea.  In  a  back  rw>ui  tbcy  found  nearly  100  lb?, 
weight  of  re-dried  tea-leaves,  bay-leaves,  and  sloe-Jeuves,  all  spread 
on  the  door  drying.  The  inspector  told  the  prisoners  that  he  was  a 
{}o1iceol^cer,  and  also  un  inland  revenue  ofhcer,  and  he  must  take 
them  into  custody,  together  with  the  whole  of  the  ingredients  and 
apparatus  for  makinf^  the  spurious  tea.  Mj-.  Brennan  ftiliied  that  the 
prisoners  had  pursued  their  nefarious  traflic  most  extensively,  and 
were  in  the  bal>iL  of  deattnrr  largely  with  (jrocers,  chandlers,  and 
others,  especially  in  the  counlry.  llie  various  articles  produced, 
prior  to  their  completion,  had  the  most  disgusting  appearance,  and 
were  evidently  prejudicial  t^  health.  He  had  communicated  with  the 
Excise  authorities,  who  considered  it  a  case  of  such  importance  to 


i 


TEA,    AND  ITS  ADULTERATIONS- 


93 


fhe  puWic,  tliat  they  requested  the  witbJrawal  of  the  present  char^, 
in  order  that  they  might  prosecute  the  prUonera  uuder  the  Excite 


F,K.  21. 


ToB  Cnam  Botaxical  Fuwhr. 

a  8,  tUrdnwrpo^clwef  M*ea>;^*.  ff«gn>w>t»ofcgfecAM;cg,  fryiteZ*.   Mifnllcd 

810  diuiMten  of  Mme. 


^ 


laws;  being  determined,  if  possible,  to  put  a  stop  to  such  abominable 
proceedings." 

Before  concluding  the  subject  of  the  adulteration  of  tea,  two 
articles  sometimes  employed  in  its  adulteration  have  to  be  noticed, 
viz..  La  Vena  Benoy  and  Cliinese  Botanical  Powder. 

Lit  Vmn  Beno  is  a  coarse  powder  of  a  reddish-brown  colour,  and  it 
coQsista  of  between  SO  and  90  per  cent,  of  catechu,  and  the  remainder 
of  fra^cnts  of  sumach  leaf. 

It  19  rccoiuiiiended  for  its  strengthening  properties,  especially  for 
strengthening  the  nerves  and  the  voice,  but  above  all  for  its  economy  ; 
a  threepenny  packet,  it  is  asserted,  will  go  as  far  as  a  (juarter  of  a 
pound  of  tes,  with  which  it  is  rocoommended  that  it  should  be  mixed. 

The  Chintie  Botanical  PoiLtfer^  is  a  preparation  got  up  in  imitation 
of  La  Veno   Beno,  and  is   principally  used  for  the  same  purpose* 


9i 


TEA,   AND   ITS  ADULTERATIONS. 


nDmclTt  to  mix  with  tea.  It  consists  of  catccha  and  whcut-flour.  The 
directions  for  its  use  are  aa  follows: — Take  hulf  n  teiupuouful  of  the 
]:K>wder,  1o  two  teuspKCinlTula  uf  tea,  ami  it  will  jiruduce  (dO  runs  the 
advertisement)  a  streriylh  efjiial  to  foui'  teaspoonfuis  of  tea. 

Both  these  powders  are  very  astringent,  and  (berefore  their  penornl 
use  in  highly  objectionable ;  thej  are,  in  fact,  active  medicinal  prepara- 
tions. 


RUULTS  OF  TBB   EXAMlHATIOlf     or   SaUPLBS   A8     BOLD   TO   TBK 

Pliilic,  &c. 

The  results  of  (be  inierosconical  and  chemical  exunicatton  of  Bome 
hundreds  of  »iiui|ilet<  ol'tea  tid  iiu]<ortedf  and  as  gold  to  the  consumer, 
in  Ihia  country,  briellv  summed  up,  are  iis  follows:  — 

That  the  j^eat  bufk  of  the  Slack  teas  used,  as  the  Congous  and 
Souch'mj;*,  are  genuine. 

Tbiit  the  Black  tca5,  known  as  Scented  Coper,  and  Scented  Orange 
Pekoe,  are  invariably  glazed  or  faced  with  piuiuhugot  and  soinctiiucs 
with  a  little  Prus»ian  blue  or  indigo,  turmeric,  auU  s^dphate  o/litne^  or 
China  clay. 

Further,  that  Scented  Caper  or  Chuinn  is  often  adulterated  with 
lAe  tea,  padtly^hmky  and  havei  Mher  than  those  of  tea. 

That  xeceral  varieties  of  a  spurioyu  Caper,  or  black  Gnnpt>rcder^  are 
prepared^  which  consist  of  tea-dtut,  and  »nmetimej  the  diiKt  of  other 
leapes,  and  sand.,  made  up  into  little  masses  with  ffum.,  and  f^ced  or 
glazed  with  plumbago^  Frutsian  blue,  and  turmeric- powder :  in  some 
coses  these  imitations  are  sold  separately,  but  most  frequently  they 
are  used  to  mix  with  and  adulterate  the  better  i|ualitiea  of  Caper  — 
viz.  those  which  are  made  of  tea  faced  with  plumbago  only. 

With  rc*|H?ct  to  Oreert  tea  the  principal  conclusions  tire- 
That  these  teas,  with  the  exception  of  a  few  of  British  growth  and 
manufacture,  from  Assam,  ore  invariably  adnlieratcd — -that  is  to  aay, 
■re  g;lu7ed  with  colouring  matters  of  dtfTcront  kinds. 

Thus  in  this  country  there  is  really  no  such  thing  as  a  green  tea — 
that  is,  a  tea  which  poesesses  a  natural  j^reen  hue. 

That  the  colnnritig  ttiattem  HJted  are  in  eeneral  Prusxinn  hlWy  indigo^, 
turmeric •fMwder,  snlphate  of  lime,  and  China  clay,  other  ingredients 
being  sometimes  but  not  frequently  employed. 

That  green  teas,  arul  more  e/tpecirdly  fne  Guupoialers^  in  atldition  to 
being  faced  andglazed^  are  more  subject  to  adulteration  tii  other  ways 
than  black  teas,  excepting  Caper,  <u  by  admisture  with  leaves  not  those 
ofteu^  wilh  paddy-husk,  and  particularly  icith  Lie  tea. 

That  Lie  tea  is  prejjared  mo  ax  to  rraembie  green  tea,  and  u  extemively 
used  by  the  Chinese  themselves  to  adulterate  Gunpowder  tea  ;  it  was  also, 
until  recently,  sent  over  to  this  country  in  vast  riuantities,  and  wat 
employed  for  the  same  purpose  by  our  own  tea-dealers  and  grocers. 
It  ts  still  sometimes  met  with,  especially  in  mixed  green  teas. 


TEA,    AND   ITS   ADULTERATIONS. 


US 


Tliftt  inferior  samples  of  green  lea»  especially  Twankay,  arc  not  only 
artificinlly  coloured,  but  they  also  sometimes  contain  foreign  leaves^ 
paddy 'husk^  and  other  foreign  matters. 

Thv  above  are  the  inort*  mi|X)rtaDt  conclusions  as  to  tbe  condition  of 
btark  auvt  «;rueii  teas  ut>  iiu[.>ort«d,  but  tbtse  articles  undergo  further 
deterioration  in  our  own  country.     Tbus  it  has  been  shown  — 

Thnt  exhansted  tea-leaves  are  sometimes  made  up  with  gum,  &c.,  aitd 
rfsnld  to  the  puldic  as  genuine  black  tea,  and,  when  artificially  coloured 
awl  glazeji,  even  as  green  tea. 

That  the  substances  employed  in  the  colouring  are  in  many  cases  rery 
much  more  objectionable  and  injurious  than  (hose  used  by  the  Chinese^ 
being  sometimes  highly  poisonous. 

That  it  is  no  uncommon  thing  for  tea,  both  black  and  green,  to  be  fa- 
bricatedfrom  various  British  leaves,  leaves  not  those  of  tea,  and  possessit^ 
no  properties  in  common  with  the  leaves  of  that  plant. 

That  black  Chulan  and  Lie  tea,  when  coloured,  have  been  known  to  be 
employed  by  our  own  dealers  and  grocers  for  the  adulteration  of  green 
tta. 

Of  the  adulterations  noticed,  those  practiced  by  tbe  Chinese  are  of 
course  by  far  the  most  important,  because  they  extend  to  a  very  con- 
siderable portion  of  the  tva  consumed  in  this  country;  at  the  same 
tioief  the  frauds  resorted  to  by  our  own  dealers  must  not  be  lost 
sight  of 

It  has  thus  been  shown  that  tea  is  subject  to  a  ktrge  amonnt  of 
adulterutiou. 

It  is  interesting  to  contrast  the  so-called  f^een  teas  of  China  with 
the  green  teas  somutimes  im|iorted  from  Assuiu,  but,  more  particularly, 
with  the  lea  call ed  Kumaon.  Tbe  dilTuiencc  of  appearance  is  Uitually 
Tory  great;  the  leaves  of  these  feus  are  of  a  dull  and  yellowijib-^rreen 
colour,  90  diflerent  from  tlie  Chinese  tciLs,  tlmt  they  would  sciircoly  be 
recognised  by  an  ordinary  observer  as  f;reen  tea  at  all.  This  marked 
diflercDce  arisen  from  the  fact  that  the  Kumnnn  and  Eomctiiues  (he 
Assam  teas  are  not  usually  coloured  or  gl»zed  like  the  Chinese  teas, 
althougli  the  Assam  are  so  nut  unt're<{uently  to  some  extent. 

One  beneficial  retiult  which  hus  folluwed  from  the  publication  of  our 
Report  on  the  adulteration  of  tea  in  "The  Lancet"  and  in  the 
authors  work  entitled  *'  Food  and  its  Aflultcrations"  may  now  be  re- 
ferred to;  it  is  one  which  scarcely  could  have  been  anticipated. 

ll  appears  that  the  Chinese  themselves  have  within  the  last  year  or 
90  begiin  to  give  up  the  practice  of  colouring  or  glazing  their  green 
teas.  This  is  shown,  first,  by  the  fact  that  notunfreouently  they  now 
send  to  this  country  chests  of  uncoloure<l  green  tea,  the  chestscontain- 
ing  it  even  bcine  branded  with  the  word  "  uncohniretl ; "  and  secondly, 
by  the  improve*!  appearance  projiiented  by  many  of  those  teas  which 
ore  coloured  or  glazed,  the  pro|)oriion  of  colouring  matters  now  used 
bcin^  much  less. 

Uaculuurud  gn:en  teas  arc  even  commonly  advcrtiBed  for  sale :  it 


96 


TEA,  AND   ITS   ADULTEBATIONS. 


should  be  known,  however,  that  in  many  cases  these  are  nothing  more 
than  ordinary  green  tcoa,  from  which  the  colouring  matter  has  been 
reiuovuJ  by  nieona  of  steam. 

Ok  tue  Detection  of  the  Adultsbatioks  op  Ibx. 

Tho  detection  of  the  adulterations  of  tea  may  be  considered  under 

the  four  following  heads  :  vir.  the  detection  of  forei^  leaves ;  of  the 
various  subatnncea  emploj-cd  for  the  facing  or  glazing  of  tea;  of  ex- 
hausted tea-leaves;  and  of  Lie  tea. 


I 


On  the  Detection  of  Foreign  leaves. 

The  teas  in  wbich  foreifrn  leaves  are  most  WkiAy  to  be  met  with,  are 
those  of  low  nuiUity;  as  Twaiikay,  inferior  Gunpowder,  Cliulan,  and 
Lie  tea;  also  in  teas  of  British  fabrication. 

The  leaves  may  occur  in  two  stiites,  either  more  or  less  entire,  or 
broken  up  into  Irapnents  which  may  be  found  either  loose  in  the 
(lust  of  tea,  or  che  a<;;;lutinated  by  means  of  a  solution  of  gum  or 
starch  into  mosses  artificially  coloured. 

For  the  detecti(»n  of  foreign  leaves  a  thorou^Ii  acquaintance  with 
the  tea-leaf  itself  is  necesaiiry,  its  shape  and  various  sixes,  the  vena- 
tion of  the  cJgeft,  the  dii^tribution  of  the  veins  and  lastly^  its  micro- 
scopical structure,  embracing  parliculurly  the  size  of  the  cells, 
stomato,  &c.  All  these  points  are  well  delineated  in  the  figures  of  the 
tea-leaf  already  given. 

In  order  lo  facilitate  the  identification  of  any  foreign  leaves  met 
with,  a  knowledge  is  desirable  of  the  characters  of  tbc  leaves  most 
likely  to  be  encountered.  For  this  nurpose  it  will  bo  well  to  examine 
carefully  the  engravings  of  foreign  leaves  actually  detected  in  adulte- 
rated tea  contained  Jn  ihis  work. 

To  discover  foreiv'n  leaves  in  a  more  or  less  entire  state,  the 
tea  should  be  infused  in  luit  water  for  a  few  minutes,  and  all  su.<tpiciotis 
pieces  unrolled  ant]  exaniine<l,  and  compnreil  with  the  tea-leaf  itself; 
regard  being  had  especially  to  the  distribution  of  the  veins,  and  the 
edges  of  the  leaves  or  portions  of  leaves. 

To  detect  foreign  leaves  much  broken  up^  ns  In  Lie  tea  and  in  tea- 
dustt  the  microscope  must  be  resorted  to ;  if  in  Lie  tea,  the  maai^es  must 
be  disiutegrated  by  means  of  hot  water,  and  the  fragments  torn  up 
with  needles,  and  examined  diligently  and  carefully  with  that  Instni- 
menL 


On  the  Detection  of  Substances  entering  into  the  Facing  of  Tea, 

As  has  already  been  stated,  a  rery  great  variety  of  substances  is 
employed  in  the  facing  of  tea.  Of  these,  some  occur  in  teas  of  Chinese 


:Aj  akd  IT8  Adulterations. 


97 


manuracttirc ;  bat  others  —  and  those  sometimes  of  a  more  injurious 
character  —  liuve  been  met  with  in  tea  fabricated  at  home. 

The  principal  ttubstanceit  used  by  the  Chinese  arc,  for  preen  tea, 
Prussian  blue^  indigo,  turmeric,  unci  some  white  |)ow(ler,  usuullv 
Kaolin  or  Chiim  oUv,  but  occasionally  pypsum  or  sulphate  of  linio;  and 
for  c<;rlain  black  te;ia,  black-lea*!,  as  well  as  in  some  cases  sioiUlyr  quan- 
tities of  the  pij^meiUs  previously  mentioned. 

By  the  mixture  of  blue,  yellnw,  and  white  colours,  green  pigments 
or  dyes  are  produced  of  various  tints. 

The  dcieetiun  of  all  the  substances  referred  to,  is  by  no  means  dif- 
ficult. 

The  first  thin^  necessary  is  to  ascertain  whether  the  tea  be  really 
artificially  coloured  or  not. 

For  this  purpose,  if  the  leaves  be  coated  to  any  considerable  extent, 
it  will  be  sutHcient  simply  to  view  one  or  two  of  them,  as  opnrpie  objects, 
with  a  piiiss  of  one  inch  focus,  when  tho  colourinj;^  nifitters  entering 
into  (he  comiK)5ition  of  the  facing  will  be  detected  as  minute  specks  or 
particles,  each  rcflcctin"  its  nppropriute  tint. 

Another  nicthwi  of  Ueiertitiiiinp  the  s:ime  jioint  is  to  scrape  gently 
the  surlnce  of  two  or  three  of  rhe  leiivea  with  ii  [leiikiiife,  when,  if  they 
be  faced,  the  colouring  matters  may  be  detect^fd  in  the  {wwder  thus 
separated,  viewed  as  an  upiique  object. 

A  third  method  is  to  place  five  or  six  leaves  on  a  slip  of  glass, 
moistening  them  with  a  few  drops  of  water,  and  after  the  leaves  have 
became  softened,  firtnly  fl<jueezin^  the  water  out  between  the  finj^er 
and  thumb;  thi^  will  then  be  found  to  contain  more  or  less  of  the 
ingredients  forming  the  fucinjr,  shoubl  such  Imve  been  employed. 

Or,  should  it  be  detiireU  to  obtain  the  results  on  n  Urge  scale,  half 
an  ounce  or  so  of  the  leaves  may  be  iij^itated  in  a  litde  water  for  a  few 
minutes;  this  will  <letuch  much  of  the  facing,  without  unfolding  the 
leaves,  and  after  a  time  the  facing  will  collect  as  a  sediment  at  the 
bottom  of  the  vessf^l. 

Laiitly,  the  tea-dust,  more  or  less  of  which  is  present  in  nearly  every 
sample  of  tea,  is  usually  found  to  contain  the  ingredient^}  used  in  the 
facing  in  considerable  quantity,  and  from  its  examination  satisfactory 
results  may  in  general  be  very  readily  obtained. 

Having  by  one  or  other  of  the  above  processes  determined  whether 
the  sanifHe  of  tea  be  faceil,  the  next  step  is  to  ascertain  the  nature  of 
the  iKubsfances  used  for  this  purpose. 

Ferrocjfanide  of  iron  or  PruiAiau  bluf. — The  blue  colouring  matter 
has  generally  Im^co  found  to  be  either  Pru.ssian  blue  or  indigo,  but 
most  iVixjneiuly  the  former. 

Fru.'isiaQ  blue  may  lie  recognised  under  the  microscope  by  the  an- 
gular form  of  the  fragments  and  by  their  brilliant  and  transparent 
blue  colour,  but  nioBt  deciiiedly  by  the  oclioti  of  liijuor  poLasna;,  wijich 
cjuicLly  destrovs  the  blue,  turning  the  frogiuenls  of  u  dull  reddiah- 
brown  colour,  the  original  colour  being  restored  ou  the  addition  of 


9S 


TEA,    AND   ITS   ADLLTERATIONS. 


dilute  sulphuric  aciil.  These  reagents  may  be  readily  applied  in  verjr 
minute  quaiitiiios  to  the  smallest  fractions  of  Prussian  olue  visible  in 
tht  field  uf  the  microscrpe. 

In  geiicnd,  the  iileiitiliL-nlion  of  the  Prussian  1jIu(%  hy  the  inetinsjust 
pointed  (JuL,  is  Huni(:i(.-tit,  but  In  some  cOJHfa  a  more  direct  oheiuic&l 
ftnalysis  may  bi^  required. 

For  this  purpose  the  fnllowlng  proceedinpt  must  be  adopted^  which 
applies  equidly  to  indigo  and  any  other  pigment  or  atibstance  with 
which  the  tea  may  be  glazed,  ivnd  which  is  required  to  be  procured 
in  a  gcpHmte  state  in  considerable  quantity. 

An  ounce  or  more  of  the  tea  is  u*  be  ajjitated  for  several  minutes 
with  warm  water,  the  leaves  Reparated  by  straining,  and  the  liquid  set 
aside  at  rest  fi»r  some  hours,  until  the  colouring  matters  have  com- 
pletely aub.siiled.  The^e  nmy  be  olitftini-*<l  by  decantation,  and  after 
wa.^hin<r  m:Ly  be  dried  in  reuilineiw  for  analysts. 

The  fullnwiiig  are  the  i^heniirol  projjerties  of  ferrocyanideof  iron,  or 
Pnissionbluer—U  is  insoluble  in  water,  in  alcohol,  and  in  dilute  acids. 
Concentrated  sulphuric  acid  ihrms  with  it  a  white  pasty  mans,  from 
which  wjler  u<:uiti  separates  it  unaltered  i  nitric  acid  decomposes  it ; 
concentrated  hydrochloric  acid  ultimately  abstracts  part  of  its  iron; 
sulphuretted  hydrogen,  iron  and  z'uif  fdiiig.-',  r-^nder  it  wliite,  in  conse- 
quence of  the  abstraction  of  part  of  llie  cyanogen.  It  is  not  de- 
colourised by  chlorine.  The  alkalies  discharge  its  colour.  (Jeetniipose  it 
into  soluble  ferrocyanidc»,  and  oxide  of  iron,  which  is  precipitated. 

ludiffo. — ThisBubstanceisdistiriguidbcd  undertlie  microscope  by  the 
irregular  form  of  the  particles,  their  granular  texture,  and  ^reeiiish- 
blue  tint,  but  chiefly  by  the  fact  that  the  colour  is  not  discbarged  by 
liquor  potaesflB  at  ordinary  temperatures. 

The  following  are  some  of  the  more  important  chemical  cbarncter- 
istics  and  properlies  of  indigo  : — It  exhibits  a  coppery  lustre  on  being 
rubbeil  with  the  nail ;  it  is  not  soluble  in  water,  dilute  acids,  ether,  or 
alcohol ;  it  is  not  attacke<l  by  Iifpior  potassa.'  at  ordinary  lemjieratures, 
but,  distilknl  therewith,  it  is  decompo&etl  and  converted  intoa  yellowish 
brown  biiuidy  aniline  is  formed^  as  shown  by  the  develujinjent  of  a 
beautiful  vioIet*blue  colour  on  the  addition  of  a  sohition  uf  chloride 
of  lime.  It  is  freely  di.«solvcd  by  strong  sulphuric  acid,  forming  a  deep 
blue  solution  ;  is  bleached  by  chlorine  :  heated  in  a  test  tube,  it  sub- 
limes in  rich  violet  vapours. 

Turmeric. — The  only  cert^n  meana  by  which  turmeric  powder 
when  mixed  with  other  articles  can  be  discovered,  is  furnished  by  the 
microscope.  A  description  of  (he  minute  structure  of  turmeric  will  be 
given  hereafter  :  in  the  meantime  it  will  lie  sufhcient  to  stale  that  tur- 
meric may  be  at  once  identilied  by  means  of  the  large  yellow  cells  of 
which  it  IS  mainly  cumposed,  nnd  the  form  of  the  starch  granules 
with  which  these  are  filled. 

There  are  no  chemical  test.<(  by  which  turmeric  may  be  identified  :  it 
becomes  brown  un  (he  addition  of  alkalies,  in  which  respiict  it  com- 


TKA,   AND   ITS   ADnLTEIlATlONS.  99 

porU  itself  like  moat  other  Tcttotr  vi^rr^ralile  oolonrin^  inntt«rs:  its 
decoction  lK»coincs  much  dnrkonol  by  iodine,  showing  the  presence  of 
Blarch  ;  by  this  character,  imJecil,  turmeric  niny  in  some  cases  be  dU- 
titiguishet)  from  certain  other  vegciable  yellow  pigments  which  do 
not  cnntain  Btarch. 

Bl>ick-lea(l. — Graphite,  plumbago,  or  black  lead,  the  substance  »o 
familiar  to  hniirtemaicU,  contti»l8  of  oarbon  and  ir<in,  uJiuallv  in  the 
proportion  trf  1)5  per  cent  of  the  Inrnier  to  5  ]>er  cent  of  the  hitter. 

The  jet-black  glossy  and  meiallic  apf>eariinre  oftlim  substance  is  so 
characieriritic^  as  to  serre  in  nia^r  coses  for  it.s  iilentificaiion. 

Apart  from  the  evidence  of  the  [ire^onee  of  thia  substance  afforded 
by  tfto  eye  alone,  it  may  be  detected  in  other  ways. 

If  a  thin  slice  be  removed  from  llie  surfjice  of  one  of  tlic  leaves 
faced  with  this  (*iil>slaiioe,  and  placed  under  ihu  riilera«ico[n»,  i(  will  be 
eeen  to  be  thickly  studded  with  nunieroii-*  riiimite  black  particles. 

A^in,  if  one  or  Iwo  teaspoonfuln  ol  lilmk-lcmli'd  leu  be  infused  in 
boiling  water,  the  liijuid,  after  «  time,  wil!  in  inmiy  ciises,  where  the 
quantity  of  farin;;  is  oon-*iiU'rahio,  ar-fpiire  a  hlm-ki^ih  hue,  and  on 
evanorution,  the  bitttnin  of  the  vessel  containin;:;  it  will  be  found  tu  ex- 
hibit the  dark,  nhininir.  ami  <harnctcn?tic  coating  of  hlark-lenil. 

Lastly,  if  a  small  tpiantiiy  of  it  be  weighed  and  ignited,  the  whole 
of  the  carbon  will  be  di^i^ipated,  in  or  about  the  proportion  of  95  per 
cent.,  and  the  iron  in  the  state  of  oxide  will  remain  behind. 

Chtwt  Cloy^  or  Knolin,  is  prepared  from  deciiyinir  granite,  and  ts 
the  result  of  the  disintegration  and  parllal  decomposition  of  the  feUpar 
and  mica  of  that  mineral. 

Talc  or  Mica  occurs,  as  is  well  known,  in  laminatefl  plates;  it  re- 
fractA  the  light  powerfully,  and  exhibits  a  considerable  amount  of 
iridtfM:enoe.  It  eonsisiii  of  silicate  of  alumina,  witli  («rBilicate  of 
potjissu. 

FtUpar  resembles  very  closely  mica  in  its  composition,  and  i»  com- 
poscil  of  single  equivalents  of  the  neutial  silicates  of  pota^ish  and 
aluntina. 

If  the  whlio  powder  facing  the  tea  consist  of  China  clay,  wc  must 
proceed  iw  follows  to  deierndite  its  nature  : — A  quantity  of  the  tea  dye 
having  lieen  separated  either  by  washing  or  by  shaking  some  of  the 
teaal>oui  in  the  dry  ftJite,  it  mu^t  be  heated  to  redness;  by  this  means 
the  turmeric  and  Prussian  blue  will  lie  destroye<l,  and  the  white 
powder  obtained  nearly  pare,  containing  chiefly  the  iron  derived 
from  the  Prussian  blue. 

The  powder  muH  be  acted  upon  with  very  dilute  hydrochloric 
acid;  the  silica  will  remain  undissolvi'd,  but  the  alumina  and  oxide 
of  iron  will  be  taken  up,  but  are  precipitated  on  the  addition  of  am- 
monia. Such  an  analysis  as  this  is  seMom  required,  as  the  determi- 
nation of  the  exact  composition  of  the  white  jxiwder  used  is  rarely 
necessary. 

Sulphate  of  Lime. — The  leavea  of  tea,  especially  those  from  Assam, 

u  2 


100 


TEA,  AND   ITS    AOrLTERATIONS. 


are  somelimDS  dusted  oi-er  with  sulpliate  of  lime,  and  this  in  aome 
castis  where  no  other  onhiurlnn^  substance  is  employed. 

Tills  salt  t«hon1d  he  dissolveil  in  wviik  hydrncmdHc  acid,  the  Holution 
furthfi"  diluted  with  waii?r;one  part  of  tbt:  9i>lution  must  be  lejited 
with  chloride  of  biiritiia  for  Miiphuni:aci(J,  and  the  olhiir  wiih  oxalate 
of  nmmotiia  for  hine.  It  is  not  often,  in  the  cnae  of  tea,  :h»t  this 
analysis  is  required,  any  more  thun  that  fur  China  clay  or  bluck-lead. 

It  now  remains  that  the  niethotls  by  which  the  Rcveral  gubstance* 
which  have  hen  discnvereil,  from  lime  to  tiiiit*,  entering  into  the  facing 
of  tea  of  Ilritt^ll  fahrieiition,  shouhl  be  <'(ni?»idered. 

Thf  prineinal  of  those  sulistanneHi  are  Duteh  jmik,  rose  pink,  logwood, 
tnrmene,  curlionaie  of  lime,  carljooiue  i>f  ma;;nesia,  steatite,  soap-stone 
or  silicate  of  nin^nc^ia,  chruinate  ^>1'  luai!,  ihu  cUromatea  of  potitsUf 
ferrwyanide  of  iron,  iudij^u,  carbunate  of  copjivr,  acetate  of  copper, 
artenile  of  top|»or. 

As  carbonate,  acetate,  and  arsenite  of  copper,  uhromate  of  lead,  and 
the  cKrouiates  of  potash,  nre  rarely  nsed  for  the  faoinp  of  tea,  and  as 
the  methods  of  detecting;  these  poisonous  salts  arc  given  under  the  ar- 
ticles Sii<rar  Confecttutiary  and  SitutT,  It  ia  not  neccttsary  to  introduce 
them  in  this  place. 

The  [trocesses  for  the  detection  of  Pnissinn  blue,  imlin-o,  anrl  ttir- 
nicrie,  have  nlready  been  given  ;  then'  remiiids  to  describe,  iherefore, 
those  only  for  the  detertion  of  Dutch  pink,  rose  pirik,  logwood,  the 
<;arboniUes  of  lime  and  mu-ineMji,  wnd  French  chtdk  or  nonp-slone. 

Dntch  Pink. —  Although  called  Dutch  phik^  this  ?ubstance  is  of  a 
brijjht  yfllow  colour;  it  cou'iists  of  a  vegetable  dye  in  cmnhination 
with  chalk  or  oarhnnntc  of  lime.  It  is  the  yellow  pigment  most  fre- 
quently used  in  this  country  in  the  fucinf:  of  spurious  green  tea. 

For  its  detection  the  folluwloj^  method  shauhl  be  pursued;^  An 
alkali  should  first  be  apjilied  t<i  thi:  yellow  dye,  in  order  to  determine,  in 
the  first  place,  whether  it  be  vt'^jetable  or  not:  if  it  turn  brown,  there 
is  no  doubt  about  its  Vfjfetuhle  clmrHcter  In  the  next  place,  ii  minute 
portion  of  itshould  he  ex:iiuined  under  the  microscope,  with  the  view 
of  ascertaining  whether  it  is  tunneric  or  not:  if  the  celh  of  lurmeric 
are  not  visible,  and  if  it  effervesce  with  on  acid,  there  is  no  doubt  that 
the  dye  is  vej»etable.  and  inosi  probably  Dutch  pink. 

Rote  Pitik  and  Loetcooil. —  Uose  pink  consists  of  the  colouring 
matter  of  logwood  in  cnmbination  wi(h  carhoiiate  nf  lime.  An  in- 
fusion of  the  wood  is  hrst  prepared  throuLih  which  the  liiijoi^ diffused, 
and  this  in  subaitling  carries  down  with  it  tin-  coloiirin^r  matler. 

This  pigment  is  distin^'uiihed  by  the  action  ofncidji  which  intensify  * 
its  reil  colour,  and  of  alkalies  whicli  turn  U  brown,  as  well  as  by  the 
presence  of  carl)onate  of  lime  or  ciudk. 

Kxtraet  of  logwood,  Dr.  Normandy  states,  ia  sonictimcs  used  in  the 
adulteration  of  teas  represented  jls  Souchong  and  Pekoe. 

'iliifi  luay  be  detected  by  moistuuing  a  few  uf  the  leaves  with  water, 


TEA, 


AND   ITS  ADULTERATIONS. 


101 


and  rubbing  them  uj)on  a  piece  of  white  papor,  which,  if  logwood  is 
proficitt^  will  be  stainod  bluisb-hlai*k.  Moreover,  a  Tew  drops  ot'suU 
pbuiiv  acid  added  to  a  concentrated  infusion  of  the  tea  cause  it  to 
turn  red. 

Citrbonnte  of  Zime  or  Chalk. — If  on  the  addition  of  an  acid  the 

?articli's  uf  white  jiowder  etfL-rveace,  it  most  probably  conaiots  of  chalk, 
n  order  to  reiidcr  the  detcrininntinn  ii  mutter  of  certainty,  however, 
the  powder  niubt  be  dissolved  in  weak  hydruchluric  aeid,  und  the  lime 
prveipituted  by  lueuiis  of  u^ulule  of  ammoniu  :  ibis  reairenl  does  not 
precipitate  luaguesia,  shuuM  that  ulkuliijie  earth  hjipjwn  lo  be  in 
•olulton. 

Carbonate  of  Magnesia. — T!ie  powder  must  first  be  dissolved  in 
dilute  hydrochloric  acid,  the  solution  treated  with  chloride  of  ommci- 
nium^  and  ummonia  iidded  in  sili^ht  excess ;  the  iun^nesi:i  i>j  then  pre- 
eipititted  by  means  of  phosphate  of  soda ;  the  precipitate  uiusl  bo 
collncted  and  eonvtfried  into  the  pyrophosphate  by  ignition,  from 
which  the  carbonate  of  magnesia  is  ealculnted.  Should  lime  altto  be 
present,  tliis  must  first  be  removed  by  means  of  oxahite  uf  ainuionia. 

French  Chidby  Soap'Htone^  or  Silicate  of  Magnejtia.  — The  indigo  or 
Prussian  blue  and  turmeric  having  been  destroyed  by  ignition,  the 
residuary  powder  is  to  Itc  treated  with  dilute  hydrochloric  acid  ;  the 
magncitia  will  be  diKsolved,  but  nut  the  silicic  arid.  The  magnesia 
may  tlicn  be  precipitated  us  bclbre,  care  being  taken  to  remove  ihe 
lime  should  any  be  presentf  and  the  sUicic  acid  ignited  and  weighed. 


On  the  Detection  of  Exhausted  and  lie-dried  Tea-leaves. 

KxhauHtod  tea-leaves  occur  in  two  forms.  Usually  they  are  made 
up  in  iiiiiuitiou  of  blutk  lea,  but  oceasiunully  of  •^reen  ulso :  the 
detection  is  easier  in  the  former  than  in  the  latter  ease.  In  the  ease 
of  bluck  lea  the  imitation  can  ollyn  be  detected  by  the  eye  alone,  but 
in  other  cases  a  cbt^mical  analysis  of  the  leaves  is  uecest^ary. 

One  ehiiracter  by  which  the  re-dried  leaves  nmy  be  known,  is  the  fold 
or  roll  of  tlie  leaves:  this  is  less  rtHrulnr  anil  uniform  than  that  of 
uniued  tea,  the  surfaces  being  agglutinated  together,  and  many  flat 
piece*  nf  leaves  occur. 

Another  character  is  the  glossy  appearance  presented  by  the  leaves, 
due  to  the  gum  with  which  they  are  almost  constantly  made  up.  By  the 
roUortwi*it  of  the  leaves,  and  by  ihe  glossy  appearance  presented  by 
tbeni,  re-drietl  tea  may  in  general  he  easily  recogniset! ;  but  when 
a  chemical  analysis  is  requisite,  the  following  pro<reeding  must  be 
odopted.  The  \wt  centago  of  tannin,  of  gum,  and  of  wmxlr  fibre  must 
be  lietermined  :  if  the  leaves  be  really  exhausted  there  will  be  a  great 
deficiency  of  tannin,  and  an  excess  of  woody  libreand  especially  of  gum. 

In  genuine  and  unused  tea,  according  to  the  quulity,  the  tunnin  bus 
beenuscertained  to  vary  from  30-0  to  450  |>er  cent  in  the  ease  ufsuj>erior 
teas ;  in  used  tea  to  range  I'rom  7"J  to  07  per  cent ;  or  the  tea  may  even 

H  3 


fl 


103 


TKA,   AND    ITS    ADULTERATIOK8. 


be  completely  exhausted  of  its  tannin.  Tbepum  ranges  from  6"31o  59 
per  cent,  in  the  one  0U5e,  unfl  inun  20"5  to  1 1"G  |)er  cent  in  the  other. 
LnHtiT,  the  wooiiy  fibre  in  unused  tea  varies  from  448  to  4G'y»  and  in 
exhausted  tea  from  9*2  8  to  7*2  !>  j^cr  cunt.  The  process  for  rleterniining 
the  aniuiint.s  oftnnnin,  gum,  fin<l  insoluble  residue  or  woody  tibre,  will 
be  found  deaeribed  at  p.  Q8.  Green  ten  iiaualljr'  euntams  About  the  same 
proportion  of  gum  as  black  tea,  but  leas  tunniu. 


AnalytiK  of  Oreen  Teoy  by  Mr.  Phillips. 


Ligniu 

iJiini    - 

Tannin  anJ  alhuraen    - 

Colounn>!  maiLur 


55-3 
5-4 

371 
2-2 


1000 

nut  other  matters  are  noroetituea  tnliled  to  exhausted  tea-leaves 
besides  g:uin,  as  catechu  and  sulphate  of  iron,  in  order  to  moke  up  for 
the  deficiency  of  lannin, 

Detet'tion  jtf  Cntechu.  —  Catechu  consists  in  preat  purl  of  tannin  : 
tlierc  will  be  -.'round  Uiv  behevin;!  thnt  (Ijia  Mib^tauce  has  beeuiMnpluyed 
if,  on  imulysiii,  both  tlie;;uni  and  tannin  are  in  excess  ;  for  the  one  is  not 
likely  to  be  einplnyed  without  the  other.  The  presence  of  ciileelm 
may  olito  be  iut'errcd  when,  there  being  no  excess  of  gum,  the  tauuiu 
is  itself  greatly  in  excess. 

A  certain  rourrhness  and  astringency  in  the  tea  is  likewise  indicative 
of  the  jiresenee  of  caleidiu. 

When  a  siilmii>ii  of  sulphate  of  iron  ta  broupht  into  contact  with  a 
solution  ctf  tannin  or  one  of  tea  which  contains  a  large  amount  of 
tannin,  the  liijuid  becomes  deeply  coloured  ;  and  it  is  on  Uiis  uccount 
that  the  sulphate  of  iron  is  sometimes  added  to  exhausted  tea-leaves, 
to  give  an  ajipeuronce  of  strength. 

Dftrvliun  tif  fyu([ihate  nf  Iron.  —If  the  infusion  mnde  from  the  ex- 
hausted ten  present  u  ceriiiin  darkness  of  npjicurancc,  the  presence  of 
sulphate  of  iron  niny  be  suspected ;  if  on  nddin^^  ii  little  tincture  of  gallfl 
the  colour  is  heiphtciuMl.  but  litlk'  doubt  reujsiins.  Lastly,  it"  necessary, 
whieh  is  but  bchhim  the  case,  — the  iurintiun  uf  ihc  leaves  uuiy  b€ 
analysed  J'or  Kul[>huri<;  acid,  ami  llie  ash  of  the  evaporated  infusion 
for  iron,  b<'th  of  which  must  be  determined  ijUJtntitntivcly.  The  sul- 
phuric acid  must  be  thrown  «K»wn  by  inenns  of  clilnritle  of  barium  or 
nitrate  of  baryta,  the  precipitate  wei^jhcd^  and  the  quantity  of 
sulphuric  acid  calculated  ironi  it.  It  should  be  remember^.-*!  that  tea 
naturally  t^ontains  a  ^nli1]l  quantity  of  sulphuric  acid,  uhielly  in  the 
combined  state,  derived  ]>artlv  from  the  leaves,  but  principiuly  frum 
the  water  used  in  making  the  uifusion. 

The  presence  uf  iron  may  be  determined  by  means  of  tincture  uf  galls, 
M  already  noticed,  or  uf  lerrocyanide  of  potassium,  which  gives  a  blue 


TEA,   Aia>  ITS  ADULTERATIONS. 


103 


precipitate  of  ferrocyanide  of  iron  or  Prussian  blue.  The  quantity  of 
iron  coiiUined  in  the  tea  umy  hii  (Ihib  asiigrtaiiieil : — A  (ino4  aiul 
weighed  jmh  tion  oftlie  teu  is  inciniTiiieU  :  if  iiiut'h  Iruu  is  pre&iiiit.tliu  ash 
will  be  coloured  more  or  loss  with  the  red  oxide  of  that  metal.  The  ash 
is  next  boiled  with  dilute  bydroehloric  acid  :  this  take*  up  the  iron  and 
Alumina,  and  pho^iphutos,  which  are  nguin  precifiitated  on  thi-  atlilition 
of  excess  of  ammonia:  the  precipitate  must  b«  collected,  ignited,  and 
weighed.  Iron  is  usually  dctcruiined  in  combination  with  alumina,  and 
the  phosphates  occurring  in  tea  are  in  general  not  so  large  as  lu  affect 
inateriully  the  accuiw:y  of  the  result,  Thu  phoi^phateti  may  however 
he  removed  previous  to  the  precipitntion  of  the  iron  and  alumina,  by 
digesting  the  ash  of  the  incinerated  tea  in  an  exceedingly  weak  solu- 
tion of  hyilrochloric  ncid, —  su  weak  that  it  will  not  affect  the  iron  and 
alumina.     For  further  details  refer  to  p.  I*i9. 

When  exhausted  ton-leaves  have  been  faced,  and  so  converted  into 
an  imilaiinn  of  greeci  tea,  the  deteclinn  of  the  fraud  by  the  eye  alone 
is  more  difljeult  than  in  the  ca^e  of  black  tea,  as,  ulthou^li  we  have  btill 
the  irregular  form  of  thu  leaves,  we  have  not  the  uiiuaturul  gloss  to 
guide  us.    In  this  case,  therefore,  we  must  resort  to  chemiuiil  analysis. 

Exhausted  tea-leaves  are  of  course  not  only  deficient  in  tunnin,  but 
likewise  in  iheine;  in  some  eases,  therefore,  it  may  be  desirable  to  de- 
termine the  amount  of  that  important  constituent  of  tea  present,  which 
may  be  done  by  following  one  or  other  of  the  proceobcs  described  ftl 

On  the  Detection  of  Lie   Tea. 

The  detection  of  Lie  tea  is  by  no  means  difficult :  In  some  cases 
it  may  be  diiicriminaie<l  by  the  in*cgularity  in  the  lorin  of  the  particles 
or  masses,  and  by  their  increased  weight  owing  to  the  sand  wbtch  they 
contain. 

Before  pronouncing  an  opinion  as  to  the  nature  of  any  sample,  it 
is  however  in  all  cases  necessary  to  act  on  the  masses  with  hot  w»ler. 
When  hot  water  is  applied  to  genuine  tea,  the  masses  quickly  unfold 
and  expand  into  leaves  or  portions  of  leaves;  when  to  Lie  tea,  they 
break  down  and  become  disinteLrntted ;  no  leaf  appearing,  and  the 
residue  is  heavy,  gritty,  and  dirty-h)oking.  Again,  if  one  of  the 
masses  be  placed  between  the  teeth  it  feds  gritty. 

But  since  Lie  tea  often  occurs,  us  already  stated,  mixed  with  other 
teas,  it  is  necessary  to  lrx>k  them  well  over  and  lo  pick  out  all  the 
masses  which  present  a  suspicious  appearance,  and  to  treat  them  with 
hot  water. 

Having  ascertained  that  the  tea  under  examination  consists  either 
entirely  or  in  part  of  Lie  tea,  it  becomes  necessary,  in  those  cases  in 
which  we  desire  to  carry  the  analysis  further,  lo  very  carefully 
examine  the  leaf-dust,  which  the  masses  always  contain,  with  the  nii- 
crosco{}e,  iu  order  to  determine  whether  any  foreign  leufdust  be 
present. 

n  4 


lOi 


TEA,   AND  ITS  ADULTERATIONS. 


Ash  of  Genuine  Tea. 


Gunpowder 
Kemuoii  H^son 

Scented  Caper 


5-0 

€0 

55 


Lastly,  in  some  oases  we  may  desire  to  know  the  per-centajjeof  sand 
which  niay  be  present.  For  IUjs  purpose  a  weiglied  portion  of  the 
tea  must  be  incineralcd,  and  the  ash  weighed.  Genuine  tea  fur- 
nishes oil  an  average  about  5  per  cent  of  aab,  and  Lie  tea  oa  much  in 
some  cases  as  50  per  cent 

The  following  results  were  obtained  by  Mr,  Warinf^ton  from 
the  incineration  of  a  variety  of  teas.  They  will  be  fouud  useful  for  the 
purpose  of  comparison  :  — 

Ath  of  Lie  Tea,  or  Tfa  aduUeratfd 

with  Lie  Tea. 

Lie  Guni>owder  No.  1.         -     45*5 

No.  2.  -     34*0 

Lie  flower  Caper  -         -     37"5 

Mixtures  containing  these       f  11*0 

Lie  teas        -  -  \l'15 

In  Lie  tea  of  British  fabrication  the  leaves  are  almost  always  foreign, 
and  the  mrts**fl  rarely  rnntnin  satirl. 

For  the  detemiiimtiftn  of  tlie  nature  of  the  substances  employed  in 
the  facing  of  Lie  tea  when  rhi>sc  liave  been  used,  reference  should 
be  made  to  tlie  remark:^  coininoucin^  on  p.  96. 

In  consciiucnce  of  the  war,  a  retrograde  step  in  the  duty  was 
enacte<l,  and  it  stands  at  U.  9J.  per  lb.  until  the  5th  of  AprlU  1857  ; 
after  that  day  it  will  b«  U.  W.  until  5th  April,  185S.  Xhoncefor- 
wanl  \».  per  lb. 

Home  consumption  1854,  61,970,341  lbs.  Duty  U.  6rf.  after  5th 
April  of  that  year. 

In  1855,  (>3,454,035  lbs.     Duty  1<.  Orf. 

First  9  months  of  1856,  48,0H3,784  lbs.,  which  is  a  slight  diminution, 
the  consumpiion  for  ihe  same  9  months  of  18:55  being  48J40,'}88  lbs. 

The  followiii;;  tjuestion,  and  autiwer  by  Mr.  George  Phillips,  will 
serve  as  an  illustration  of  the  gross  ignorance  of  the  Excise,  even  in 
regard  to  the  adulteration  of  tlie  few  articles  of  consumpiion  under  its 
supervision. 

Air.  Mnffatt.  "  Is  it  within  your  experience  that  no  poisonous  sub- 
stance is  ustnl  in  the  facing  nf  tea  at  the  present  lime? 

Jiephj.  "  It  is  po.^sible  there  might  be  some  samples  found  now 
coloured  with  Prussian  hluc  ;  but  /  hove  not  seen  any  ti/vfielf.''^ 

Now  let  the  reader  remeiBU;r  that  all  the  green  teas  m  this  country 
are  artificially  coloured,  and  ibut  one  of  the  sulistanct's  used  is  in 
ninety-nine  out  of  q  hundred  case.*  Prussian  blue,  and  he  will  have 
some  notion  of  the  ignorance  and  incompetence  of  the  Excise. 

Again,  it  appears  by  the  returns  jtlaced  iK'fore  the  Committee  by 
Mr.  George  Phillips,  that  in  twelve  year.f  the  Kxcitse,  with  its  70 
chemists  and  4000  inspectors,  examined  only — and  this  in  a  very 
superficial  way — 142  samples  out  of  900,000,  the  number  of  packages 
imported. 


COFFEE;  AND  ITS   ADULTERATIONS. 


105 


Ci 

h 

II       h 


^^  in  I 


COFFEE,  AND  ITS  ADULTERATIONS. 

Tub  bererage  coflTee  consuU  of  an  infusion  in  Loiliog  water  of  the 
roAsted  sc«^l9  of  a  plant  which  htm  ri'L-eivcl  tin?  Hutunical  name  of 
Coffta  Arahtcn^  find  which  is  said  to  be  indi-^f  luma  fn  certain  dislricU 
of  Southern  Abyssinia^  where  it  j;rows,  with  the  profusion  of  a  wild 
weed,  iner  the  rucky  surface  of  ihc  country. 

Id  AbyssiniJiT  coffee  has  been  in  use  from  lime  immemorial ;  in 
Persia  it  wa*  in  use  as  early  as  875  ;  it  was  iiitrnducLd  into  Arabia 
about  the  fifteenth  century;  nnd  about  the  luiUille  oT  the  sixtefnth 
Cftnturv  it  began  to  be  employed  iii  Omstantinoplo  ;  white  we  learn, 
on  the  authority  of  Professur  Johnston,  it  wiu  nnt  iintU  llie  latter 
"  alf  of  the  seventeenth  century  that  it  made  it^  way  into  Europe, 
first  iuto  London,  and  some  yciu-s  i<ubt$e(}uently  to  Marseilles. 

In  Johnston's  "Chemistry  of  Common  Life"  we  meet  with  Ibefol* 
towing  description  of  the  cofi'ee  plant  or  tree:  — 

The  coflee  tree,  when  in  good  health  and  full  grown^  attains  a 
height  in  some  countries  not  exceeding  ei^dit  or  ten  feel,  but  in  others 
averaging  from  fifteen  to  twenty  feet.  It  is  covered  with  a  daric, 
smooth,  shining,  and  evergreen  foliajje.  It  is  sown  in  nurseries, 
transplanted  when  about  six  months  ohi,  in  three  years  conies  into 
full  1>euring,  and  in  favourable  circumscunces  will  continue  to  bear 
fur  twenty  years.  It  delights  in  a  dry  S'lil  and  n  warm  situation;  its 
flowers  are  pale,  white,  fragrant,  and  rapidly  fading;  its  fruit  lilce 
that  of  the  cherry  tree,  but  it  grows  iu  clusters  ;  wiihin  the  fruit  are 
the  seeds  or  berries.  On  dry  antl  elevated  pai'ts  the  berries  are 
smuller  and  have  a  better  Bavour,  but  berries  of  all  sizes  improve  in 
flavour  or  rrptfii  by  tceeping.  The  small  berries  of  Arabia  will  ripen 
in  three  yeans;  but  the  worst  coffee  produced  in  America  will  in  from 
to  fourteen  years  become  *  as  good,  nod  acquire  us  high  a  flavour, 

the  best  we  now  luive  from  Turkey.'  " — EUi». 

The  seeds,  improperly  culled  berries,  of  Arabian  or  Mocha  colFee  are 
small,  and  of  a  dark  yellow  colour;  tliot^e  of  Java,  and  East  Indian 
arc  larger,  and  of  a  puler  yellow  ;  while  those  of  Ceylon,  West  Indian, 
and  llrazilian  coffee  possess  a  bluish  or  greenish-grey  tint. 

The  dried  fruits  or  berries  are  rarely  imported :  occasionally,  how- 
ever, the  seeds  contained  in  their  endocarp  or  husks  are  met  with  in 
comiuerce. 

Recently  the  very  important  fact  has  been  made  known  that 
the  leaves  possess,  to  a  certain  extent,  the  com|)osition  as  well  as 
many  of  the  properties  of  tlie  seeds,  and  hence  their  Inlroduc- 
liuii  into  this  country  has  been  proposed.  It  appears  that  a  beverage 
umdi!  from  roasted  cofl'ee-leaves  hoA  long  been  used  in  the  Eaateni 
Archipelago,  esncclally  iu  Sumatra. 

Mr.  Ward,  wlio  hia  been  many  years  settled  in  Sumatra,  stateftj^ 


lOfi 


COFFEE,    ANT>   ITS  ADULTKRATIONS. 


"As  a  beverage  the  natives  universally  prefer  the  leaf  to  the  berry, 
giving  as  u  reason  tliat  it  contain:^  more  of  tlie  bitter  principle^  rtkI  is 
more  nutritioua.  In  tlie  lowlands,  tolFee  Js  nuL  ptuntcd  for  llie  berrv» 
not  bein^  sufficiently  productive,  but  Ibr  tine  leuf;  the  yjeople  plant 
it  roiina  their  houses  for  their  own  use.  It  is  an  undoubted  fact, 
that  everywhere  they  prefer  the  leaf  to  the  berry."  * 

Chcpuad  Composition  and  Properties  of  the  Coffee  Seed. 

The  foUowing  quantitative  analyses  of  coffee  are  by  Schrader  and 
Pajen ;  f  — 


Rate  Coffee. 

Roasted  Coffee 

. 

Schrnder. 

Sch  roller. 

Pcouliftp  cflffeio  prin- 

CafTeic ]iriuciple     - 

12'50 

ciple 

17-58 

Extractive 

4.80 

Gununjr    and    mu- 

(jum umi  muciliLgu 

10-42 

cilaginous  extract 

364 

Oil  and  resin 

208 

ExlrMctive 

0-62 

vSulid  residue 

68-75 

Resin 

0-41 

Loss 

1-45 

Fatty  oil  - 

05t2 

Stdid  residue 

66-66 

100-00 

Loss  water 

1057 

100  00 


Payent  Analysis  of  Raw  Coffee.X 
Celiidose  ...---  34-000 

Water  hygroscopic  -----  12*000 

Fatty  substances  -  -  -  -  -  10  to  13000 

Glucose,  dextrine,  and  undetermined  vegetable  acid        -  15'J00 

Legumine,  easeine  (glutine)  P  ...  10*000 

Chiomgenate  (eaflesite)  uf  potash,  and  caffeine    -  -  35  lo  5*000 

Nitrogenous  substance    -----  3*000 

Free  caffeine     -  ....  -  0*800 

Concrete  ewential  oil      -  -  -  -  -  0  001 

Aromatic  fluid,  essential  oil  -  -  -  -  0002 

Mineral  substances  -----  6*097 

Acconling  to  Messrs.  Graliam,  Stenhouse»  and  Campbell,  raw  coffee 
contains  as  much  as  from  fi  to  7  per  cent  of  cane  sugar ;  this  is  cither 
entirely  destroyed  by  the  roasting,  or  it  rarely  exceeds  1*12  per  cent. 

According  to  the  same  authorities,  the  nitrogen  In  roasted  coffee 
lies  between  2^  and  3  per  cent. 

The  following  analyses  of  the  €uh  of  coffee  are  by  Messrs.  Graham 
and  Slenhouse :  §  — 

*  rhannarruttrfti  Journnl,  rol.  vlll.  p.m. 

f  ChemlcA!  Ouvttc.  vol  ir.  p.  U..  mi?.  X  Ibid. 

(  Chomtotl  Itqxirt  oo  tb«  mode  of  detecting  VegeUble  SulMtaocet  mixed  with  Coflbe. 


COFFEE,  A>D  ITS  ADULTEBATI0N8, 


Analytes  oftXt  AmH  of  Coffee. 


lo; 


turn 

j»^ 

Klra. 

,^ 

Umcbt. 

■fctrr,. 

PMa»b         - 

6*- 10 

&i.7U 

i4-00 

M30 

M^« 

51 -M 

U-M 

ScnU 

^ 

.. 

^ 

^ 

UlM 

4  10 

4-aii 

4  11 

4r,| 

610 

6-M7 

ft-6B 

M«tDeda    • 

i-« 

H-46 

»«0 

8-66 

frW 

RH7 

a-49 

8«fqgloxkla  ot  Iron 

0« 

0-W 

073 

0*63 

044 

U-44 

0^1 

Sulphuric  add 

S1i8 

4 '45 

S49 

a-fti 

lin 

ffMi 

a-iB 

rhii.ilne     - 

)  II 

0<IS 

O^ii 

1  (JO 

072 

0-.W 

OiSO 

CirlKMllL-  «rtd 

I7'4r 

1&93 

IHU 

16M 

IBM 

I6-9S 

M-9S 

Phoaphurk-acU      - 

lO-M 

LI13U 

1106 

I0«0 

11-13 

W-I.'i 

10-B& 

Silk» 

^n 

.,-•, 

^ 

^ 

^ 

— 

— 

&«n.t 

— 

— 

- 

— 

— 

— 

— 

lotrfis 

Kwao 

W-97 

W06 

100- w 

ViJBh 

IOO<t4 

^ 


The  chief  peculiarities  of  the  composition  of  the  aih  of  coffee,  are 
the  absence  of  soda  anil  the  itinall  i|uiinrity  of  silica  present :  thia,  in- 
deed, is  so  small  as  to  reii<lcr  it  ilouhtful  whether  it  cnntains  any  but 
that  vbich  is  sccirlenfally  ndlierent  to  ihv;  bcnrie?.  Contrastetl  with 
the  ash  of  chicory,  Bcvt-ral  other  jicc'iilinrilie>  prosont  thcinfldves,  such 
A3  the  small  quantity  of  t'hh»rine  iind  *»f  se^iiuloxide  of  iron,  and  the 
lariie  quantity  of  carbonic  acid  coniaiiicd  lit  ihc  ash  of  cufTee. 

'rhe  three  most  important  cunstiluciits  nf  tlie  cofluc-bcrry  arc,  the 
ToUUiU  oily  called  caffeotte;  the  coffric  acid,  uiiulogous  to  tlic  tannin 
of  tea ;  and  the  cafftxne^  idfuticol  with  tbc  thclne  of  tea.  AVc  &huH  make 
ft,  few  observations  on  each  of  these  constituents. 

The  properties  of  coffee  seetl  are  mucli  nllt-rcd  by  roasting :  the 
principal  products  of  torrefaciion  are  a  bniwn  bitter  principle^  de- 
rived principally  from  tlic  conversion  of  the  sugar  into  carninel,  and 
tht  arumatic  oil,  called  aiff'eane. 

The  propertica  of  the  infusion  of  the  roasted  coffe«  seeds  are  thus 
summed  up  by  Pereira:  — 

**  Rousted  coffee  posKcsses  powerfully  anti-»oporific  properties : 
hence  its  use  as  a  drink  by  thoitc  who  <le!<irc  nm*turnal  study,  and 
■8  an  antidote  to  counteract  the  effects  of  opium  and  other  naicotics, 
and  to  relieve  intoxication.  Jn  thoiie  unaccustomed  to  its  use,  it  is 
apt  lo  occasion  thirst  and  constipiition.  On  some  persons  it  acts  aa  a 
sfiffht  purgative.  It  is  occasionally  useful  in  relieving  headache,  es- 
pecially the  form  callefl  nen'ous.  It  has  also  been  employed  ^as  a 
febrifuge  in  interniittcnts,  as  n  stomftchiu  in  someformsof  dys|H'^i8ia  and 
B»  a  stimulant  to  the  cerebro-spinttl  system  in  some  nervtius  diMirdera. 
Fliiyer,  Dr.  Pcrcival,  and  others  have  used  it  in  spasmoilic  asibma ; 
and  Luenncc  !«iiy8,  '  I  have  myself  seen  ^everal  cases  in  which  coffee 
was  really  useful.  The  immoderate  use  of  coffee  is  said  to  produce 
Denrous  symptoms,  such  as  uixieCy,  tremor,  disordered  vision,  palpita- 


COFFEE,  AXB  ITS  ADULTEHATION'S. 


tian  and  feverisbness."  *     Cofie*;  is  also  supposed  to  counteract  the 
tendonrjr  to  the  rormation  ofgrarel  and  stone. 

The  propertiefl  nnd  effecta  of  coffee  are  lUud  described  by  Profesaor 
Johnitton  :  — 

*'  Ir  exhilarates,  arouses,  and  keeps  awake ;  it  counteracts  the  stupor 
occavioiied  by  fuligue,  by  disvasc,  or  by  opium  ;  it  allnys  hunjrt?r  to  a 
certain  extent,  jjives  to  the  weary  increased  slren^rth  and  vi-jnur,  and 
imparts  a  feeling  of  comtbrt  and  repose.  Its  physiological  eflects  ujxjn 
the  system,  so  far  as  tbpy  have  been  investi^'iUtf!,  njjpear  to  be.  that 
while  it  ninkes  the  brain  more  active,  it  Honthes  the  budy  gonerally, 
makes  the  t'Uan;;e  nnd  vraato  of  iuatti;r  alower,  and  the  deuiand  for 
food  in  consei[ueiiru  It-M.  All  those  elTects  it  owes  to  the  conjoined 
action  uf  three  ingredients  very  .siniihir  U)  those  containe<I  in  tea." 

WluMi  rousted  cofltje  is  di&tilled  with  water,  the  volatile  urtmuitic  oil 
or  cafffoue  pusses  over,  and  by  drinking  the  oil  and  water  together 
its  enects  may  be  ascertnined. 

When  the  quantity  of  oil  obtained  from  two  ounces  of  coffee  was 
taken  in  a  day,  it  was  found  In  protluce  an  agreeable  exeitement  mid 
ffcntle  perspiration,  to  dispell  the  sensjiiioTi  of  hunger,  and  to  imive  thu 
bowels.  **In  its  exhihiraiin-r  nclion  upon  tht?  brain,  it  affVuls  the  iuia-ji- 
nation  less  than  the  reasoning  powers."  — Johaton, 

When  the  dose  of  oil  was  doubleil,  violent  perspiration  comes  on, 
with  sleejile^sness  and  symptoms  of  eongettion. 

Lehmann,  by  a  series  of  careful  obeervationg  and  experiments  on  the 
urine,  ascertained  that  it  exercised  an  etfcct  eiiual  to  that  of  cuffeine 
in  retarding  the  waste  of  the  tissues. 

The  raw  cotfce  seeds  contain  al)out  5  per  cent,  of  an  astringent  acid, 
—  the  caffeic  or  caflcn- tannic, —  which  diflt'rs  from  ordinary  tannic  acid 
in  that  it  docs  not  blacken  a  solution  of  iron,  as  the  iril'ii.'iiun  uf  tea 
does,  but  renders  it  jjreen,  and  does  not  precipitate  j^eUiiiie  from  its 
solution.  This  acid,  although  changed  somewhat  by  the  roasting,  yet 
retains  to  some  extent  iljt  a^rringent  properties.  "  Chemists  gcneraUy 
are  disposed  to  refer  the  tlavour  and  peculiar  propt-rties  of  coffee  as  a 
beverage  more  to  its  acid  —  the  ctijfeic  acid  {particularly  after  that 
substance  is  modified  in  it.i  properties  by  roasting)  thao  any  other 
constituent." —  Gruhnm  and  St/nihouM, 

Caffeic  ncid.  like  the  acid  of  the  cinchona  barks  —  kinic  acid,  yields 
kinone  when  the  syrupy  exira'*t  of  coffee  is  mixed  in  a  retort  with 
about  four  times  its  weight  of  binoxiile  of  maniranese  and  one  pint  of 
sulphuric  acid,  diluted  with  an  equal  quantity  of  water,  and  the 
mixture  ia  subjpcteil  to  di'itillation.  The  Kinone  passes  over  into  the 
receiver  in  the  form  of  yellow  crystal;*,  which  mlhere  to  the  neck  and 
aides  of  the  retort,  as  well  as  a  bright  yellow  liquid  containing  kinone 
with  much  formic  acid.  Kinone  is  distinjruishedl  by  its  volatility  and 
acrid  oduur,  resembling  that  of  chlorine.  AVitb  mumonJa  thesoiutionof 

•  Mstoria  Medtcs.  vol  tt.  p.  tecA ,  ml  ediuon. 


COFFEE,  AND  ITS  ADULTERATIONS. 


109 


I 


kinnne  gives  a  sepia  black  ooloar,  converted  into  reddish-brown  by 
»ul|itiurf:tted  b^dro^ou.     It  is  dischar^l  br  sulphurous  acid. 

Tbc  ftxtriiigent  acid  in  coifee  is  muuh  losi<  itiun  in  tea,  and  hence  it 
docrt  not  retard,  to  the  same  extent,  tbc  uctiun  of  the  bowels,  especially 
wl«in  ill*  ofieration  i»  counteracted  by  the  volatile  urumatic  oil,  whica 
txerts  an  fl(>crient  tendency. 

Caffeine  is  a  weak  nlkuloid  of  a  white  colour,  crystflllises  in  long 
«ilky  needles,  fusible,  volatile,  and  suluble  in  water,  alcohol,  and  ether. 
llj  aqueous  wlutiun  is  precipitated  by  tannic  acid. 

The  pro[»orliun  of  caHeine  obtained  in  fivu  cxperiiueiits,  in  it  de  by 
Me^tfrv.  Grabtun  and  SteiUiouse,  upon  dilferent  samples  ofcolTeei  was 

follows  : — 


Caffeine  in  Haw  Coffee. 
Native  Ceylon 

Plantation  Ceylon 


0-80 
0-80 
101 
034 
0-83 


y 

■  Tlic  proportion  of  the  annlogons  principle  in  tea — thcine — is  usually 

H      over  *i   per  cent;  ihat  ifl,  tea  contains  (in  the  average  fully  twice  as 
H      much  of  this  alkaloid  as  coflce. 

H  •*  By  rubbing  common  roasted  coffee  in  a  mortar,  with  a  fifth  of  its 

V  weight  of  ftloked  liiue,  and  then  boiling  llie  tiiixlure  in  alcohol, 
about  J  per  cent  of  theine  may  be  readily  extracted.  Weight  for 
weijibl,  iLercfore^  tea  yields  about  twice  at  nmeh  theine  as  roa&(ed 
ei>fiee  does  to  the  water  in  which  it  is  infused.  Rut  as  we  generally 
vte  a  greater  weight  of  eoHee  than  we  do  of  t^-a  in  prcpjrin;^  our 
beTcragvs,  a  cup  of  coflee  of  ordinary  stren^rt^h  will  probal>ly  contain 
lu  much  theine  as  a  cup  of  nnlinary  Englisli  tcA.  A  cup  of  ntrong 
French  coffee  will  contain  twice  as  much  caffeine  as  a  cup  of  weak 
French  tr-a." — Johnston* 

■  The  action  of  cafll-ine  is  nearly  identical  with  that  of  theine,  the 

crperation   of   which    on   the    system    bos    already    been    described, 
rtde  p.  7fl.,  rt  srrfintiir. 

We  meet  with,  in  Pereira'a  "  Materia  M«*dicfi,'*t  th*-*  following  olwer- 

I  rations  in  relation  to  the  properties  of  cafffinc  :  — 
**  Mulder  gave  a  grain  of  it  to  a  rabbit;  the  animal  ale  but  little  the 
next  d.ny,  and  alwrted  the  day  atTer.  Liebig  has  suggested  that  it 
probably  contributes  to  the  formation  of  taurine,  the  nitrogenised 
constituent  of  bile.  Acconlingto  Lehmann{,oatreine  in  doses  of  from 
2  to  10  grains  causes  violent  excitement  of  the  vascular  and  nervous 
systems — palpitations  of  the  heart;  extraordinary  frequency,  irregu- 
larity, and  oucn  intermission,  of  pulse ;  oppression  of  the  chesty  polos 

•  Chomlitry  of  ComiDon  Lffr.  p.  MB. 
t  Vol.  li.  p.  ItWj  Ard  ittltinn. 
t  PliytivtuificBl  Cfbcmiitrr,  troniUtcd  by  D.  Dar,  red.  i  p.  136.  CavrndUh  S0CU171  ■*&!• 


i 


no 


COFFEE,   AND   ITS   ADULTEEATIOKS. 


'm  the  bend,  confusion  of  the  senses,  sinking  in  the  etra,  sninlUlations 
before  the  eyes,  sleeplessness,  fliui  delimim.  Fri  nil  cases  mn  augiuen- 
tatioii  was  found  ui  the  ani'tuiit  of  ureft  weorelod." 

Extraction  of  Caffeine. — The  follnwin;;  is  the  process  adopted  for 
the  extraction  of  caffeine  by  Messrs.  Graham  and  Sfenhousc  :  — 

The  raw  coflee  was  pround  fine,  havinjr  been  previously  well  dried 
at  212"  F.  to  I'ucililAte  thmt  operation.  A  decoction  was  then  mmleof 
1000  grains,  by  the  repeiitcil  application  of  boil  in;;  water,  so  as  to  ex* 
haust  the  rofice  of  all  Holtible  matter.  The  t'oliition  was  concentrated 
a  little  by  evaporation.  The  acid  uf  the  coffet?  and  certain  other  sub- 
stances were  now  entirely  precipitated  by  the  addition,  6r»t,  of  the 
neutral  acetate  of  lead,  and  then  of  the  subacetate  of  lead.  These  in- 
soluble nistters  were  removeti  from  thi-  liipiid  by  filtration.  The  excess 
of  lead  in  solution  was  then  thrown  down  by  means  of  hydrosulphuric 
acid.  The  lit^uid,  after  this  preparation,  was  evaporated  to  drynes*,  and 
the  drv  niatier  left  wns  exhai]<cied  by  means  of  strong  spirits  of  wina 
CSp,  Gr.  0'840).  Tlie  iilcolinlic  solution  was  concentrated  bv  evapo- 
ration, and  iillowcd  to  stand  in  ii  nearly  syrupy  state  for  about  tea 
days,  in  order  to  cry!«tnllise.  The  crystals,  which  are  caffeine,  were 
collected  upon  a  sniiiU  filter,  and  compressed  j>owi'rfully  to  remove 
the  mother  liquor.  These  crystals  were  re-dis«olved  in  a  small  quan- 
tity of  water;  the  Roliition  evaporated  and  crystallised  anew.  It?xve 
nImoHt  nothing  but  cafl'eine,  in  long  silky  white  needlcSf  witli  little  or 
no  rolour. 

"Wbc-n  it  ia  merely  desired  to  extract  cnfleine  from  raw  or  roasted 
coQce  witiioui  resanl  to  ({uantily,  the  general  pr<M'ess  for  the  extrac- 
tion of  organic  bases,  by  means  of  ether,  sutfiees.  Lime  is  adde<l  to 
the  infusion  of  coffee,  which  is  then  evaporated  to  dryness  uptm  i 
wat«r-bath.  The  extract  may  be  divi(U*d  by  means  of  clean  rood, 
and  then  agitsted  with  ether.  The  caffeine  crystallises  as  the  ether 
evanoruteSf  or  it  may  l>c  rc-dissolved  in  water,  and  crystallised  afraiit. 
"We  believe,"  write  Mosj^rs.  Graham  and  Stenhoune,  "  that  the catTeine 
fromlOpercent.  of  cofftre  in  a  uiixturc  might  bo  extracted,  in  sufficient 
quantity  for  its  identification,  bv  the  preceding  simple  proces. 
Oaffeinef  when  once  obtainefl,  is  fully  recognised  by  its  easy  sublima* 
tion,  and  also  by  its  action  with  nitric  acid,  in  which  it  resemblei 
uric  acid.  When  the  solution  of  caffeine  in  niinc  acid  is  evapfu'ated 
to  dryness,  and  exposed  to  ammoniacal  gas,  it  is  covered  by  a  pink 
blush,  likt^  murcxiile.** 

The  coffee  seed  likewise  contains  about  13  per  cent,  ofglt^en^  which, 
being  for  the  luo^t  part  in<tolub1e  in  boiling  water,  is  contained  in  ike 
coffee  grounds.  In  some  countries  the  grounds  are  drauk  as  well  as 
the  coffee. 

The  following  analyses  show  the  comparative  and  average 
position  of  the  unroasted  coffee-berry  and  the  tea4eaf,  ai  imported 
into  Europe :  — 


COFFEE,  AND  ITS  ADDLTERATIONS. 


Tea, 

Coffee 

Mulder. 

Payeu 

Water 

5 

1-2 

Gum  andflugar 

21 

15* 

Gluten 

2fi 

la 

Theine 

k 

1 

Fat  and  volatile  oil 

4 

13 

Tannic  acid   - 

13 

5 

Woody  fibre 

24 

34 

Ash 

^ 

6| 

]()0 


100 


The  quantity  of  coffee  exhraotive  oblaintnl  from  the  cofTee  seed  by 
Iter,  differ*  Tcry  much  in  differerit  sampii-s, — a  ibfferL'noe  not  ex- 
plwned  by  tlie  extent  of  roasting  of  the  »eeda.  The  addition  of  an 
alkali — ai  soda — to  the  water,  incrcoaea  the  auionnt  of  extract,  and 
a  itrongcr  inAuion. 


It 


Structure  of  the  Coffee  Seed. 
Two  parts  are  tobediseriniinated  in  tht;  coffee- berry — the  substance 
the  berrv,  and  the  testa,  or  investment  by  vrhieh  it  is  surrounded. 
The  herry^  previous  to  roasting,   and  even  after  it  hiu  been  aoaked 
a  lon^  tiroe  in  water,  t!(  hard  and  tough,  in  which  reitpect  it  dillera 
1  all  tbc>«c  substimcea  which  enter  itito  the  adullcr^lion  of  coffee, 
which  become  suftenLil  by  immersion  in  cold  water,  the  hardness 
retained  subsequently  to  tlie  cburrinrr,  and  \-a  80  great,  that  by 
ebaracter  alone  the  fra^nents  of  the  [ground  and  roasted  coffee- 
may  be  readily  distinguished  from  tnose  of  cbieury. 
cxmsisU  of  an  asftemblaze  of  vesicles  or  cells  of  an  tinffvlar  form, 
b  adhere  ao  firmly  together  tli.-it  iher  break  up  into  piWes  rather 
■eparate  into  distinct  and  jierfet-t  ceils.     The  {*avilies  of  the  cells 
ude,  in  the  form  of  liitle  diopn,  a  considerable  ipiantity  of  aromatic 
latile  oil,  on  the  presence  of  which  the  frajjrance  iind  many  of  the 
five  priociplefl  of  the  berry  mainly  depend.     Fig.  2i. 

c  Uitn^  or  investing  menibnuie,  presents  a  structure  very  distinct 
that  of  the  sulistanc>4  of  the  berry  itself,  and  when  once  seen  it 
be  confounded  with  any  other  tissue  which  has  vet  been  ob- 
entering  into  the  adulteration  of  coffee  :  it  is  made  up  princi* 
Itv  of  elongated  and  adherent  cell*,  forming  a  singii.'  layer,  and 
Ting  oblique  markings  upon  their  surfaceii ;  these  cells  rest  upon 
otl>er  thin  membrane  which  presents  an  iudidtinct  fibrous  Ktructure. 
cen  the  berry  and  its  covering  some  essential  oil  is  generally 
I.     Fi^.  23. 

The  quantity  of  this  membrane  present  in  a  broken  and  divitletl 
in  any  lample  affords,  therefore,  some  clue  to  tlie  atuouut  of 
oootained  in  it. 


ret) 


^ 


112 


COFFEE,   AND   ITS   ADULTERATIONS, 


It  has  been  proposed  to  deprive  the  berry  of  this  mcinbnine,  and  a 
patient  luis  uetually  been  taken  out  Ibr  tiiis  purpose — a  process  of 


Ar.*s>. 


I 


BeetloD  of  UxxoastU)  CorrKB  Biikt.  ahoirini  the  dH  naA  Airra  of 
Iha  cell*,  k*  wll  u  th«  drop*  at  oil  ouoUlittd  wilhin  thtir  ekvt- 
Um.    Dnwn   wiUi  tiw  C«nwra  Lucid^,    uid  nutgnUkd  140  dU- 


somewbat  doubtful  utttUy,  because  tbo  removal  of  this  tissue  cannot 
be  eflVclcil  withrmt  the  loss  of  the  greater  part  of  the  essential  oil 
Ivinff  between  it  and  (he  berrjr,  and  usually  udlicrent  to  the  former. 
In  the  act  of  roasting,  however,  more  or  less  of  ilii.H  membrane  ht- 
comes  uparated  from  the  berry,  when  it  h  termed  by  the  roasten 
••  flighu/" 

In  the  c>*'>"ve  which  runs  alonp  each  berry,  a  few  small  vessels^ each 
formed  of  n  stnglu  and  continuous  spiral  thread,  are  usually  to  be  met 
with  ;  it  is  impossible,  however,  to  eonfoHnd  these  with  the  tJuct«  here- 
after to  be  described,  and  which  occur  in  certain  other  vegetable 
tissues. 

Now  tlic  roasting  of  the  berry  does  not  tdtcr  its  structure ;  tlx 
tissiicf)  are  indeed  partially  clmrred,  but  they  fftill  pres"rve  their  chief 
characteristics.  The  eit^entiul  oil,  however,  is  no  lonjrer  visible  in  the 
cells  in  ihe  form  of  niiiuUe  drops  vr  spherules.  This  has,  in  part, 
been  dissipated  by  the  henl  einplnyed  in  the  prt>ce»»  of  roasting,  and 
in  part  is  more  gcrierully  dilfiist.'i]  thrim;:bout  the  cavities  uf  the 
cells;  that  it  i«  not  entirely  dirtsipalt'd  and  destroyed  is  evident  from 
the  fact,  that  in  ground  roasted  colTee,  dilTuaed  m  a  little  water,  tlM 


COFFEE,  AND  ITS  ADULTERATIONS. 


13 


Ai]  iDAy  b«  roadilj  detected  in  considernble  quantitjr  in  a.  partially 
l(i««d  BUtte,  in  litde  masses  uf  irregidar  size  and  form.     Fig.  24> 


/)jr-33. 


i<4lfc«Ij>T««Ti<(a  MuHBtitrEorth^cnOlM  benj.  ahovlnf  lu  •tmotnic. 


Cm  TBS  ADn.TEBATioH  oT  CorrsB. 

Tli«re  Are  few  articles  or  consumption  moro  subject  to  extenflive 
adullcnuion,  and  ilits  of  the  grostie^t  kind,  than  cofT<ie. 

At  the  time  when  we  lirst  directed  uur  Attention  to  theadultoration 
of  OptfeCi  ttbuut  aix  jcars  «ince,  it  was  Hciircclj'  |K)BAible  to  procure 
I  Miapla  ni  g^nMind  ccQ've,  no  matter  what  the  price  paid  for  ic  or 
irWrc  it  WMf  puirhiiK'tl,  that  w;is  not  hir^cly  ndultt^ruteij. 

Ad/$iiemlnfH  u'tih  Chicnry. — The  most  prcvali-nl  uilultcratton  of 
«o(b^  t*  wiib  chicorj.  lu  nearly  nil  the  sample.s  tlien  examined 
iUeory  formetl  a  large  proportion  of  the  aitii-le,  while  in  many  in- 
ttanOM  it  coosisttfl  uhnn-t  cntirelr  of  chicory.  At  the  present  time 
cotfcc  i»  still  much  adulterated  with  chicory,  while  the  eoni|H>und  ftoM 
vith  Hut  UbeU  now  pre8i-ritK.'d  by  the  law,  '^  i'his  is  a  mixture  of 
ducory  uid  culTee,**  vfieo  cousisla  of  little  cLm;  than  chicory. 

1 


114 


COFFEE,  AND   ITS   ADULTERATIONS. 


Even  the  grinding  of  coffee  in  the  presence  of  the  purchaser  affonU 
DO  certain  guarantee  for  the  genuineness  of  the  articJc,  as  not  un- 


Fig.a. 


^ir-yv 


^^^r 


A  fragment  of  Roai tbd CorvsR.    Drswn  vlih  the  CAinem  LadiU,  KOd  macnlflMl 
llOdUmctcn. 

frequently  the  grocer  ndniitly  convey*  into  the  null,  from  a  box  placet! 
close  to  it,  a»  mnny  chicory  nibs  oa  he  pleases,  and  which,  owing  to 
their  resemblance  in  size  and  colour  to  coffee  berries,  are  not  readily 
distinguiehotl  at  a  short  distance. 

Even  whole  roasted  L-uffce  has  been  ndulteratcd  with  chicory:  In 
this  ca«e  the  berrieF  [ire  cumprL'ssed  into  tht'  form  of  coffee  berries.  In 
18dOt  Messrs.  Duckworth,  tif  Liverpool,  lo<>k  out  a  patent  for  mould- 
ing chicory  into  the  ahape  of  berries  :  tliey  appear  Irt  have  been  induced 
to  do  so  in  consequence  of  the  existeiii;e  in  1650  of  a  Treasury 
minute,  wliich  allowed  of  the  sale  of  chicory  mixed  with  coffee  with- 
out any  restriction. 

It  has  been  loudly  nnd  repeatedly  urgfd  in  extenuation  of  this 
adulteration,  csi>ecially  by  grocers,  that  the  addition  of  chicory  to 
coffee  is  a  great  improvement.  Tliere  are  undoubtedly  some  few  per- 
sons who  consider  that  it  dues  iniiirove  the  Oavour  by  making  the 
infuiiion  more  bitter,  allhimgh  that  is  not  our  npiniun,  imh-  tbut  of  the 
great  majority  of  persons.  We  believe,  moreover,  tlii-t  the  taste  of 
those  persons  who  really  prefer  the  mixture,  has  been  vitiatetl,  mid  that 
had  they  the  opportunity  of  partaking  of  well  prepared  and  unu<lul- 
tcrated  coffee,  they  would  not  be  hm;;  before  tncy  acknnwledjxed  the 
infinite  superiority  of  the  genuine  beverage  even  as  a  matter  of  taste. 
When  the  relative  propt-rttes  of  cofiee  and  chicory  are  taken  into  ac- 


J 


COFFEE,  AND  ITS  ADULTERATIONS. 


115 


oountf  no  doubt  whatever  can  be  entertained  aa  to  which  U  the  supe- 
rior article.  The  composition  and  properties  of  chicory  will  be  shortly 
considered. 


TUi  ncnffaic  czhiblta  the  itraetan  ud  ckknetan  of  rfufci-  fmaid  Come 

Again,  it  has  been  asserted  that  in  France  and  other  continentAl 
countries  the  use  <»f  chicory  is  almost  universal.  We  have  taken  con- 
siderable painSf  when  abroad,  to  ascertain  how  far  this  statement  is 
correct,  and  we  will  new  state  with  what  results.  We  found  that  in 
ail  the  good  hotels  in  Frfince  and  Germany  the  coffee  served  up  was 
genoinCf  and  did  not  contain  a  particle  of  chicory  ;  also,  that  chicory 
wu  not  mixed  with  coffee  in  the  houses  of  the  wealthy,  but  that  it 
vas  largely  enipIoye<l,  either  separately  or  mixed  with  co6ee,  by  poor 
persons,  and  amongst  the  dooiestica,  not  beeauj«  it  was  considered  to 
De  an  improvement,  but  on  the  score  of  economy,  chicory  costing  about 
2d.  or  tki  per  lb.,  and  coffee  four  or  five  times  as  much.  This  is  the 
real  secret  of  the  use  of  chicory  abroad,  and  not  because  of  any 
preference,  or  that  it  improves  the  flavour  of  coffee.  Where  money 
IS  not  an  object^  and  where  the  best  coffee  is  required,  chicory  is  but 
•eldoin  had  recourse  to.  The  practice,  then,  abroad  is  the  very 
reverse  of  what  lins  been  asserted,  and  it  affords  no  countenance 
to  the  statement  that  coffee  is  improved  by  the  use  of  chicory. 

1  2 


116 


COFFEE,   AND   ITS  ADULTERATIONS. 


Afsin,  if  ri?n1ly  an  improvement,  as  some  persons  consider,  it  woiiUl 
only  be  ao  wben  uni))Ioyudin  certiiiri  pruportionn.  Now  in  the  ground 
coffee  sold  in  the  shops  in  this  country^  it  is  met  with  in  every 
proportion,  it  constituting  sometimes  over  90  |i*r  cent,  of  the  article. 
The  ftllepalion  that  chicory  improve*!  the  flavour  of  coffee^  would 
not  warrant  its  use  to  nnytliing  like  thnt  extent. 

It  cannot  therefore  be  doubted  for  a  moment  that  the  Tcnl  cause 
of  the  extensive  employment  of  chicory  in  this  country,  is  that  by 
its  means  gnwers  are  enabled  to  enhance  yresilly  their  profils. 

But  we  will  suppose,  for  sake  of  arpumentT  (hat  it  in  a  decided  im- 
provement ;  yet  thia  does  not  justify  the  sale  of  a  mixture  of  chicory 
i\n<l  coffee,  a*  nnd  under  the  name  of  coflfee,  coflee  frequently 
forminfj  but  a  smidi  per-centa<;e  of  the  article.  Such  n  mixture^  if 
permitted  at  all,  shouUt  not  only  be  sold  Itdiclled  as  u  mixture,  but  the 
projjortions  of  each  in^fredient  should  be  specified. 

We  consider  that  few  persona  will  be  tliajjused  to  question  the  rijiht 
of  the  purchaser,  when  lie  enters  a  shop  and  n»ks  for  a  particular 
article,  to  expect  that  he  will  be  supplied  with  the  article  he  de- 
mnndri ;  and  that  if  he  oj^ks  for  coffee  he  will  be  supplied  with  coffee^ 
and  not  with  a  mixture  of  two  articles  in  the  must  uncertain  and 
indr'finite  proportions. 

Let  the  two  articles,  therefore,  be  sold  separately,  nnd  let  them  be 
purchased  by  the  public  ut  their  respective  price».  This  is  the  simple 
and  Htraigbtturward  course  to  pursue,  and  is  that  which  is  adopted  on 
the  continent. 

At  length,  and  after  years  of  labour  and  argument,  the  government 
has  been  driven  tn  acknowledge  the  imprnpriety  of  permitting  chicory 
lo  be  sold  under  the  name  of  coffee,  and  frfqiieiitly  also  at  the  price  of 
that  article;  and  within  the  last  two  ycurs  or  so,  it  h&s  been  required 
that  the  mixed  article  should  be  sold  lnl>ellcd  *'  This  is  a  mixture  of 
Chicory  and  Coflee." 

But  tlii»  regulation  by  no^  means  fulliU  the  requirements  of  justice, 
because  the  mixture  is  often  pabned  off  when  coffee  only  is  asked 
for,  and  because  the  proportions  of  the  inprcdients  are  not  stated. 

There  is  one  circumsrance  which  nhtiidd  be  fiarticularly  remembered 
in  considerinj;  the  question  of  the  adulteratitm  of  ciiffee  with  chicory, 
namely,  the  difference8,Jehemieal  and  physiological,  which  exist  between 
the  two  article?. 

Coffee  and  Chicory  cnntniMed. — Coffee  Is  the  seed  of  a  plant,  and  it 
contains  essential  oil  or  catfeone,  caffeic  aciil,  and  a  peculiar  print-jple 
termed  caffeine  ;  each  of  the^e  constituents  possesses  different  nnd 
highly  impf^rtant  properties,  upon  which  the  value  of  cofft-e  mainly 
depends. 

Chicory  Is  the  root  of  a  plant  belonping  to  the  family  of  the 
dandelions.  It  contains  no  essentiid  oil,  tannic  acid,  or  alkaloid 
analogous  to  that  of  coffee.     The  chief  constituenta  of  which  it    is 


COFFEE,  AND  IT8  ADULTEBATION6, 


lt7 


N 


mude  up  when  roMtoii,  nre  a  liltle    giim,  stirrftr  partly  bume<l  and 
reduced  to  caramel,  colouring  matter,  and  insahibfe  veiietable  tissue. 

Between  the  two  artii:les,  therefore^  there  U  no  andc^  whatever; 
and  in  proportion  as  the  strength  of  coffee  19  reduced  bv  admixture 
with  chicory,  so  are  the  active  properties  of  colfce  diminished. 

It  ift  to  the  presence  of  constituents  similar  to  thu»c  of  coffee  that 
tea,  as  has  already  been  pointed  out,  und  ulso  cocoa,  owe  their  active 
propertieH,  and  which  has  led  to  the  ulmost  uuirersal  employment  of 
either  t£a,  coffee,  or  cocoa  over  nearly  the  whole  of  the  inhabited  por- 
tions of  the  globe. 

But  coffee  is  subject  to  adulteration  with  a  variety  of  other  articles 
besidcit  chicory. 

Aflulieratiun   with   RiHutetl   Grainy   RooU^   Acorns,    Suwdunt,  ^r. 
Thus  it  is  not  unlreiiuently  udult^-ruted   with  rotuted  grant,  princi- 

fally  wheats  and  also  with  scorched  peat  and  beant  ground  into  powder. 
,eM  coinmonly  roasted  carrotXy  mawfold'Wurzrl^  ry<r,  and  acorn*  have 
been  employed,  and  even  woody  fibre,  or  sawdust,  especially  mahogany 
sawdust.  We  have  ourflclvca  delected  sawdust  on  two  occasions, 
and  the  other  substances  mentioned  in  several  instances. 

Other  articles  whiuh  have  been  forwarded  to  us,  and  which  it  has 
been  stated  have  been  used  in  the  adulterution  of  coQ'ee,  are,  first,  an 
article  termed  '^coffiiuiP  oaX-bark  tatiy  exhausted  tan  termed  croatSf  and 
baked  kttrxes  lioers. 

The  article  on  which  the  name  of  coffina  was*  bestowed,  was  intro- 
duced into  this  country  in  IS^l,  and  was  expressly  made  for  the  adul- 
teration of  coffee.  It  was  ilcscribcNl  as  the  seed  of  u  Turkish  plant, 
which  was  found  to  be  highly  nutritious.  On  subjecting  it  lucxiimi- 
n»tion  with  the  microscope,  it  was  ascertained  to  consist  of  liie  roasted 
seeds  of  some  leguminous  plant,  probably  a  lentil. 

Of  this  article  we  were  infnrmed  that  no  less  than  eighty  tons  were 
oflercd  for  sale  by  a  Scotch  hou*;  at  abiiut  I  '2/.  per  ton ;  that  is,  at  about 
l^rf.  per  lb.  On  this  single  transaction  the  revenue  would  be  de- 
frauded of  no  less  u  sum  than  4480/.,  and  the  public  of  ut  least  four  times 
that  umount,  namely  18,000/. 

The  importation  of  about  one  hundi*ed  tons  of  lupin  seed  from  Kgypt 

into  GloA^ow,  has  led,  writes  a  correspondent,  to  the  conjecture  that 

this  cofUua  wns  made  from  it,  —  a  conjecture  most  probably  correct, 

since  the  structures  met  with  in  cofBna  exactly  resemble  those  of  lupin 

ed. 

The  same  firm  to  which  the  coffina  was  sent  was  offered,  at  about 
the  same  time,  five  hundred  tons  of  forei;rn  acorns  at  &L  per  ton,  or 
leas  than  three  farthinpi  per  lb.  Should  these  have  found  a  pur- 
chaser, the  revenue  would  have  been  cheated  to  the  extent  of  t28,ObO/., 
and  the  public  to  thut  of  112,000/.  The  acorns,  when  rfia.tted  and 
powdtreil,  were  intended  to  be  used  in  the  adulteration  of  coffee. 

In  a  little   work,  publishciJ  some  four  or  five  years  since,  entitled 

1  3 


113 


COFFEE,   AND  IT8  ADULTER  A  TI0N9- 


**  Coffee  as  it  U  and  as  it  on^ht  to  be,"  the  following  observations 

iK'Cur  in  reference  Ut  the  u»e  of  baked  horses'  anil  bullocks'  livers;  — 

"In  various  parts  uf  the  meLropolis,  but  more  especially  in  the  east, 

are  to  be  found  liver  bakers.    These  men  take  the  livers  of  oxen  and 


Fif.  9L 


Drkwn  with  the  C»Tncn  Luci^Ik,  bikI  tnBgnilled'14'i  dJiiiiittfn. 


horses,  bake  I  hem,  and  grind  them  into  ft  powder  which  they  sell  to 
the  low-priced  coffee-shop  keepers  at  from  4rf.  to  Gt/.  per  lb.,  horses* 
liver  coffee  beiiring  the  highest  price."  It  may  be  known,  tlie 
writer  states,  "  by  allowlnjr  the  coffee  to  stand  until  cold,  when  a 
thick  y>enicle  or  akin  will  l>e  found  upon  the  top.  It  goes  further 
than  coffl'e,  and  is  generally  mixed  with  coffee  and  other  vegetable 
imitations  of  coffee." 

The  adulteration  of  coffee  in  some  oases  alten*  and  reiluces  so  greatly 
the  colour  iind  appearance  of  the  article,  as  well  a:<  of  the  infusion  made 
from  it,  that  the  use  of  colourinp  niatter3  is  fret^uently  necessitated. 

One  of  these  is  burnt  Htigar,  familiarly  known  in  the  grocery  trade 
and  by  coffee-shop  keepers  as  BInck  JacK. 

It  is  sold  to  the  coffee-shop  keepers  usually  in  tin  canisters  at  1«. 
per  lb.:  it  is  sometimes  dtfuuniinatud  tho  coffee  refiner  { it  is,  however^ 


COFFEE,  AND   ITS  ADULTERATIONS.  119 

rather  a  coIovirJiif;  oj^cnt,  and  it  ia  employed  to  impart  colour  and  bit- 
terness to  bevunig(?6  uiude  iVoni  adultiTaUHl  conijc,  these  being  the 
qualities  wliich  in  the  ejres  of  superSoiul  observers  denote  strength 
aiid  goodness. 

Sugar  is  sometimes  added  to  coffee  berries  while  underrroiiig  the 
process  of  roasting,  and,  being  then  burned,  is  converted  into  a  cofTee 
colourer. 

Another  article  used  to  give  increased  colonr  to  adulterated  ground 
coffee  is  V'enetian  redy  or  some  other  analogous  ferruginous  earth.  Vf'a 
have  not  only  ourselves  obtained  repeated  evidence  of  the  use  of  this 
substance,  but  we  shall  presently  quote  a  passage  from  the  writings  of 
the  late  Dr.  Pereira  in  reference  to  its  employment. 

In  the  latter  part  of  IS^Othe  inithor  read  a  communication  to  the 
Botanical  Society  of  Lnndnn  on  tlio  uduUerntion  uf  cnlfee  ;  that  is 
some  months  before  the  puhlicatinn  of  the  fii*Ftof  his  Rcporuin  "The 
Lancet"  on  adulteration.  In  thh  the  auifiur  dc^crilM.'u,  tor  the  first 
time,  the  results  at  which  he  had  been  enabled  tu  arrive  by  the  ex- 
amination of  cufieu  by  means  of  the  microscope.  These  results  wer& 
as  follow  :  — 

BendU  of  the  Microacopieal  Examination  of  thirty-four  different 
Coffees  of  all  QualUie*  and  Prices^  and  avid  under  the  fuUowing  at- 
tractive Titiet : 

Coffeeg  of  High  Price, 

1.  Finest  Mocha  Cnffee,     No  adulteration. 

2.  Noted  Old  Mocha.     No  adullcraiion. 

3.  Finest  Jnmaica  Coffee.     No  adutteration. 

4.  Hich  Old  Mocha,     Of  chicory,  a  good  deal. 
6.  Beit  Ohi  Mocha.     A  little  chicory. 

6.  Fitte  Old  Turkey  Coffee.     3Iuch  chicory. 
7-   Vtry  Fine  Mocha.     Much  chicory. 

8.  Genuine  Old  Mocha.     A  little  chicory. 

9.  Finest  Turkey  Coffee.     Contains  chicory. 

10.  Celebrated  Old  Mocha.     A  good  deal  of  chicory. 

Ciffeet  of  Medium  Price. 

11.  Co0ta  Rica  Coffee.    Nearly  one-half  chicory. 

13.  Fine  Jamaica  Coffee.     Contains  a  considerable   quantity  of 
roHsted  com. 

13.  Veliriouw  Coffee.     Roasted  beans  and  chicory,  forming  about 

one-third  of  the  article. 

14.  PlaiitatinH  Coffee.     Of  roasted  corn  much,  with  some  chicory, 

both  together  forming  not  \&n  than  a  third  of  the  sample. 
16.  Finest  Turkey  Coffee.     Much  chicory,  and  some  roasted  com; 

very  little  cotlee. 
16.  Celebrated  Jamaica.     Very  little  coffee,  principally  chicory. 

I  4 


1B0< 


COFFEE,   AND  ITS  ADULTERATIONS. 


About  one-half  coiFL^c,  much  chioor/, 


17.  Finest  Berhiee  Coffee. 

and  some  wheat, 

18.  SpUndid  Turkey  Coffee,  About  one-hulf  c<  flue,  the  rest  chicory. 

19.  Fine   Plantatum    Coffee.     Oiie-tbirii   coflee,   ihe   rest  chicory, 

with  a  little  rousted  corn. 

20.  Beantiful  Jamaica  Ctffee.    Two-thirds  cofTee,  ihe  rest  clucorj, 

witJi  u  little  corn. 

21.  FiueMt  Jam  Coffee.    Half  cofiec,  much  roasted  corn,  with  a 

little  chicory. 

22.  Superior  Plantation  Coffee,  Three-fourths  coffee,  the  remainder 

chicory. 

Coffees  of  Low  Price. 

23.  Fine  Mountain  Coffee.     Fotir-tiflli§  coffee^  one-fifth  chicory. 

24.  Pantian  Coffee.     Princijmliy    cbicoiy   and   corn ;   very   little 

coffee. 

25.  Superb  Coffee.    The  principal  port  corn  and  chicory ;  very 

little  cotTce. 

26.  Rieh  drinking  Coffee.    One-third  coffee,  the  rest  chicory,  with 

some  roasted  <.'urn. 

27.  Very  excellent  Coffee.  Oue-half  coffee,  the  other  mostly  chicory, 

28.  Delicious  Fantity  Coffee,     Ouc-fuurth  Cufftie,  three-fourths  chi- 

cory. 

29.  Fine  Ceylon  Coffee.     Very  little  coffee,  a  great  deal  of  chicory, 

with  9UI11C  roa$tod  corn. 

30.  Fine  Jaca  Coffee.  AIucU  chicory  and  aome  roasted  potato  ;  very 

liillc  coffee. 

31.  Coffee  a»  in  France.     Principally  chicory. 

32.  Very  excellent  Coffee.     PriiK-ipally  cliicory. 

33.  Fine  Plantation  CeyUm.     Nearly  all  chicory  ;  very  little  coffee. 

34.  Delicious  drinking  Coffee.     A  large  quantity  of  chicory,  and 

much  roasted  corn. 

From  an  examination  of  this  Table  it  appears  — 

Iftt.  Tiiat  of  the  thirty-four  coffcca,  thirty-one  were  adulterated. 

2nd.  That  chicory  wus  present  in  thirty-one  of  the  samples. 

3rd.  Roasted  com  in  ttrelce. 

4lh.  Hcans  and  potato  llnur,  each  in  one  sample. 

5th.  That  in  sixteen  cases  the  adullornlinn  consisted  of  chicory  only. 

6tb.  That  in  the  remainiiigyr/lr^^N  sampler,  the  adulteration  conhislcd 
of  chicory,  and  either  ro:iste4l  corn,  bean.x^  or  [totatoea. 

7th.  That  in  many  instanci'S  the  quantity  of  coffee  present  was  very 
small;  while  in  others,  it  formed  not  more  than  one-fil'lu, 
fourth,  third,  half^  amtso  on  of  tlie  whole  artlile. 

We  are  satisfied  that  the  gross  ag^^ri-wat*?  of  the  adulterations 
detected  did  not  amount  to  leas  than  one-third  of  the  entire  bulk  of 
the  quantity  piu'choscd.    Now,  on  referring  to  the  Kevenue  Ketunu, 


COFFEE,  AND  ITS  ADULTEKATIONB. 


ISl 


Snd  tbat  tbe  mm  derired  from  the  duty  on  cotTee  for  1855   wna 

•IHL  1 1*.  9</.,  an  amount  wliicli  welmve  no  beHitation  in  sny)ngnii<flit 

e  been  enormously  increuscd  liy  vigilance  in  ihe  (i*.*U;i:liun  of  the 

ultoration  of  thid  important  article,  and  by  pun't«hixient  of  the  fraud 

en  detected. 

Since  Uie  da(«  referred  to,  we  have  exurniued  t^ome  liumlrotls  of 
plea  v(  ground  cofl'ee.*  Until  witliin  thu  last  year  or  two,  we  always 
found  a  very  Lu-jje  proportion  of  tbe  samplesi  to  lieaduiterat-ed.  Mure 
recently,  however,  the  cotiditioti  of  the  urticlu  has  ^'rently  iNi[)roveil ; 
the  groaaer  adulterations,  —  whatever  may  be  the  state  of  things  in  the 
vifkoea,  — M  far  as  the  metropnlis  is  concerneili  ure  now  much  less 
tlCftlly  prartifted :  the  principal  adulteration  iti  that  with  i-huory, 
is  Mill  mixed  with  eodee,  and  sohl  without  the  prescrilied  label 
soffee.  This  improved  eiato  of  thiugii  is  undonhtcdJy  due  to 
repeated  exr>u>ures  made  witliin  tbe  \asl  four  or  tive  years.  But 
it  not  perfectly  certain,  if  these  exposures  were  to  cease,  that  mailers 
iiM  ff«xin  become  even  worse  than  belbre,  and  that  t!ie  •»cnndalou8 
i  nefarious  practices  which  once  prevaded  iii  the  adulteration  of 
this  article  would  speedily  l*e  rife  again  ? 

The  adulterations  by  means  »(  roasted  com,  beans,  coffee  oolonrcr, 
snd  Venetian  red  are  altogether  indefensible,  .since  the  only  thinj:;  in 
c«nnmon  between  most  of  these  and  cofiee  is  the  colour  which  they 
II  infusion  or  decoction. 
-  !<;  rears  tiace,  roasted  corn,  principally  rye,  was  largely  sold, 
axid  employed  to  make  a  beveraijeT  which,  by  a  Bction,  was  digni&ed 
by  tbe  name  of  coffee  ;  the  chief  argument,  independent  of  price, 
Bf^ed  in  fttvour  of  it,  was  its  supposed  nutritive  properties. 

Whim  it  is  recollected  that  the  starch  of  roasted  corn  is  in  part 
rrUttCvd  to  the  condition  of  charcoal,  it  will  at  once  be  perceived  that 
it*  natritive  qualities  cannot  be  very  great,  and  chat  a  smgle  uioutblul 
le  bread  contains  more  nouribhment  than  a  dozen  cups  of 
nude  from  roasted  com. 

i  "  roaxted  com  "  is  now  no  longer  sold  openly,  yet,  as  we 

i>een.  the  grocer  has  not  failcfl  to  uviiil  himself  of  it  fur  his 

»efit,  but  to  the  great  disadvantage  of  llie  public, 

atbilteration  of  coflce  bv  subs-tances  so  chtap  and.  for  the  pur- 

U*  Hhi<-li   tht-y  are  applied,  worthlc:*s  as  these,  is  a  gross  fraud, 

iplmtie  condemniition,  and,  when  ascertained  to  be  proc- 

u)g  exposure  and  punishment. 


On  the  Deiectum  of  the  Adtdterationa  of  Coffee* 

^AtflMUks  to  be  resorted  to  fir  the  detection  of  the  adulterations 
0f«oSW,  ftre  of  three  kinds  :  namely,  certain  physical  characters  and 
ptmarnnuni    preaeute^l    by   adulterated  samples ;    the    microscope ; 

*  IW  iwtlcMtes  at  Umm  MuaOiMtioui  are  recorded  io  "  Food  sod  lU  Adullcrmtloiw.  '* 


132 


COFFEE,   AND   ITS  APCLTERATI0N9, 


and  chemistry.  By  the  first,  we  ascertain  in  ftomc  casea  the  pcncml 
fact  whether  the  sumplc  Ja  rtduPerated  or  not;  and  by  the  others, 
eiipeciiilly  by  tho  microscope,  we  leurn  the  nature  of  the  pariiculHr 
adulturalioD  or  adulteratioiiB  practised. 

The  first  means  consist  in  noticing  whether  the  esmple  in  the  mass 
cakes  or  coheres,  whether  it  floats  in  water  or  not,  ami  the  colour  of 
the  infusion. 

If  the  ground  coffee  cakes  in  the  paper  in  which  it  is  folded  or 
when  pre:tsed  between  the  fingers,  there  w  jrood  reason  (or  believing 
that  it  is  adulterated,  mt»st  probably  with  chicory. 

If,  when  a  few  pinches  uf  the  suspected  cuflee  are  placed  upon  some 
water  in  a  wine-;;la.H»,  part  tloats  and  part  liinks,  there  is  rea^n  to 
believe  that  it  is  adulterated:  it  may  be  either  with  chicory,  rr>astcd 
com,  or  Minic  other  Jinid«^(tus  subslnnces.  The  colTrc  does  not  im- 
bibe the  water,  but  floats  on  the  aurloce,  while  the  other  substances 
absorb  the  water,  and  jrT'aiiuully  subside  to  the  bottom  to  a  greater 
or  less  extent.  Ususdly,  hnwevLT,  part  «f  the  colTee  subsidw  with  the 
chicory,  and  h  jHtrtion  of  the  latter  remains  on  the  surtui:e  with  the 
coffee ;  and  atYer  the  lapse  of  a  short  time,  in  general,  both  cuffec  and 
chicory  fall  to  the  bottom. 

Again,  if  the  rnid  water  to  which  a  portion  of  ground  coffee  has 
been  adde<l,  quickly  becomes  deeply  coloured,  it  is  an  evidence  of  the 
presence  of  somo  roasted  vegetable  substance  or  burnt  sugar  ;  for 
when  coffee  is  added  to  water,  it.  becomes  scarcely  coloured  fur  some 
time. 

Lastly*  if  in  a  few  grains  of  coffee,  spread  out  on  a  piece  of  glass  and 
moistened  with  a  few  tlropa  of  water,  we  are  enabled  lo  pick  out,  by 
mean<i(>fa  nee*IIe,  minute  pieces  nf  substance  of  a  soft  cnnsistence, 
the  coffee  is  iloubtless  adulterated  ;  for  the  particles  of  the  cotlee  seed 
are  hard  and  resii^tlng,  and  do  nut  Iwcomc  soft  oven  after  prolonged 
immersion  in  water. 

AVhen,  therefore,  any  sample  cakes  into  a  mass,  quickly  furnishes  to 
cold  water  a  deep-coloured  S"lution.  or  is  found  to  contain,  when 
moistened  with  water,  sufl  particK's  like  those  of  bread-crumb,  there 
QUI  be  no  question  as  to  the  existence  of  adulteration. 

The  general  characters  of  genuine  grouinl  coflee  are,  therefore,  the 
reverse  of  the  above. 

By  these  general  means,  and  without  hnving  recourse  to  science, 
the  observer  is  ot\en  enabled  lo  state  whether  any  sample  of  coffee  is 
adulterated  or  not ;  but  in  order  to  iletermine  the  cluiructer  of  the 
adulteration  practised,  wo  must  employ  either  the  microscope  or 
chemistry.  In  the  ca^e  of  coffee,  by  far  the  most  imp''jrtant  inform- 
ation is  furni-Oied  by  the  miiroscope ;  indeed,  chemjstry  affords  no 
certain  means  for  the  iilcniiljcalion  of  the  miijnriiy  of  the  vegetable 
substances  emiiloyed  in  ibe  adukeralion  of  coliee,  and  did  it  do  so,  it 
would  hardly  be  required,  since  these  may  be  so  readily  detected  bj 
the  microscope. 


J 


COFFEE,    AND  ITS  ADO  LTE  EAT  1 0KB. 


1 33 


Grahxtn,  Stenbouse^  and  Campbell  h»ve  instituted  some 
^>ecial  cheniicul  inquiries  on  the  mode  of  detecting  vegetable  sub* 
stances  mixed  with  coffee:  these  will  be  found  rct'erred  to,  at  some 
length,  under  the  nrtifle  Chicory. 

The  result  ol'  these  invcslipations  is,  tliat  it  is  easy  enou;;b  to  ascer- 
tain by  means  of  chemistry  the  general  fact  of  adulteration,  but  that 
it  is  not  possible  by  the  same  means  to  detumiioe  tbe  nature  of  the 
adulteration  practifict),  even  that  with  chieury. 

The  general  fact  of  adulteration  may  be  determined  in  a  variety 
of  ways;  as,  in  addition  to  tlie  colour  of  the  infusion  and  by  its  specific 
Ifravity,  by  the  quantity  oi  sugar  contained  in  it,  and  the  composition 
of  the  ash. 

The  quantity  of  augar  in  roasted  coffee  rarely  exceeds  1*12  per 
cent,  white  in  tbe  saccharine  rooia  used  in  the  adulteration  of  coffee  — 
as  those  of  roasted  chicory,  carrot,  parsnip,  and  mangold-wurzel  — it 
Tarie»  from  9  to  1 8  per  cent. 

The  mont  distinctive  peculiarity  of  the  composition  of  the  ash  of 
coffee,  is  the  small  ([uantity  o( silica  contained  to  it :  "the  presence," 
state  Messm.  Gnilium  and  Stenhnuse,  **or  1  per  cent  or  upwardn  of 
silica  in  the  ashes  of  coffee  is  a  proof  of  adulteration;  that  the  adul- 
terating substances  which  increase  the  proportion  of  silica  moat 
considerably  are  oats  and  barley,  then  chicory  and  dandelion,  wbich 
are  followed  by  r)-e  and  wheat ;  but  turnips  and  carrots  would  produce 
a  small  aud  less  decisive  effect." 


W 


DftertninaHon  of  the  Sugar  in  adultmratrd  Coffee. 

The  foUnwinc  process  may  be  pursued  for  the  deicrmination  of  the 
mgar: — Two  thousand  grains  of  the  article  are  to  be  infiisod  iu  three 
separate  pints  of  water,  tbe  Grst  cold,  and  tbe  second  and  third  warm. 
To  this  infusion  udd  about  ime-eighth  part  of  brewers  yeast,  weighed 
after  being  dried  by  pressure  in  n  calico  bag.  Tbe  fermentation  is  to  be 
continued  for  fortv-eight  hours,  the  infusion  being  kept  at  a  temfierature 
of  from  80  to90°Fahr.  The  liquor  is  then  to  he  di-^tifled  twice,  the  alco- 
holic solution  weiched,  and  il^  ppecifu^  gravity  taken  at  a  temperature 
of  WO"  Fahr.  When  the  quantity  of  pu;:ar  and  the  amount  of  alcohol 
developed  is  yery  small,  recourse  oiay  be  Lad  to  tbe  fermentation 
test. 

The  articles  which  have  been  detected  entering  into  the  adul- 
teration of  ground  coffee,  have  already  been  enumerated:  they  are 
roots  of  ditierent  kinds,  parlicularly  chicory  and  mangold-wurzel ; 
vorioas  farinaceous  substances  in  the  roasted  and  puwdcretl  state,  as 
wheat  flniir,  beans,  and  acorns,  besides  woody  fibre  or  sawdust,  burnt 
sugar,  and  Venetian  red,  or  reddle. 

On  the  Detection  of  Chicory  —  Some  five  or  six  years  since,  an 
outcry  having  arisen  in  consequence  of  the  substitutinn  to  an  enormous 
extent  of  chicory  for  cofl'ce,  and  government  being  called  upou  to  in- 


1S4 


OOFFEEy  AMD  ITS   ADULTERATIONS. 


terfcre,  the  (juestion  as  to  whether  the  presence  of  chicory  in  ground 
coffee  was  iliscovcruble  or  not  by  means  of  science,  was  rcftfrred  by 
the  Chancellor  of  the  Exchequer  of  the  time  to  a  coniwission  of 
chemists. 

These  chemists  reported,  that  "  neitlier  by  chemistry  nor  by  any  other 
means  whs  the  oflmixture  of  chicory  with  coffee  to  be  detected."  This 
report  was  publicly  quoled  by  Sir  Cfiftrics  Wooil  in  the  House  of 
Common:!,  and  on  the  mrength  of  it  the  guvemment  refused  to  inter* 
fere  in  the  prevention  of  the  adulteration  of  coffee.  Now  at  the  some 
time  the  nuthur  showed,  in  the  moat  conclusive  manner,  that  nothing 
is  more  en8y  and  certain  than  the  detection  of  chicory  tu  coffee  by 
means  of  the  microscope. 

The  structure  of  cuffee  baa  already  been  fully  described ;  that  of 
chiwiry  will  shortly  lie  considered :  it  may  be  stated  now,  however, 
that  it  differs  in  every  respect  from  coffee,  in  the  rounded  form  and 
easy  scpar^tbitity  of  its  component  cells,  and  in  the  presence  of  dotted 
ducts,  and  vosa  lucticentia. 

Tlte  differences  will  be  sudJcieally  obvious  on  an  examination  of  the 
following  figure. 

ng.v. 


awvf  U« ilnictatM  In  «  Mmpli gf  Co9wn  nikttnMta  wM  CHICOU. 
<>  1.  eont !  b  ft,  cbkofy. 

Detection  of  Matigold-WurzeL^-Thh  root  differs  from  cbicor;  i« 


COFFEE,  AND  ITS  ADULTEKATIONS. 


12: 


TCfT  much  Iiipgcr  nze  of  the  cells,  and  in  the  absence  of  milk  vessels 
lacticcQtic.     J^'igt.  2b.  and  29. 


Aff.  96. 


YWb  fl(a>*  ■■hlkiV  th*  qbIU  of  vhtch  th»  rvA  of  MAVooLivmnkL  li  chfmtj 
mnme  •  11  «UI  ti  vtmmA  tliftt  ti\«y  ut  mvmuI  uni«a  iwgcr  th«n  Umm  of 


Dtdediim  of  Cnrrot  nnii  Parimip.  —  The  tuber  of  carrot  fliffers 
cfait^orv  rhiellv  in  the  absence  of  milk  vessels  ;  that  of  parsnip  in 
tbe«b«enci*  of  Ihe  »iinie  vessels,  aiul  in  the  presence  in  the  cells  of 
ftfnilftHT  formed  starch  corpuf^oles  of  sinall  f^izo. 

On  the  Defectum  vf  Wheat  Flonr^  d^'c. — It  ih  generallj  stated  thut  the 
pTf'^fnce  of  roasted  com  or  aiiy  other  substance  contiiintn;:  a  lorpe 
^^|fr|H>rl4i>n  of  starch,  niny  be  detected  bv  the  blue  coh>ur  produce<l  on 
^Hbe  addition  of  a  solution  ol'  iodine  to  the  cold  decoction.  We  have 
^ElDt  found  this  to  be  correct  in  all  coses,  for  on  adding  inline  todccoc- 
^Hpons  of  tire  ddferent  colFees  iiscertained  to  be  adulterated  with  ronsted 
^"iMix.  tiie  li(|uids  did  not  become  blue,  but  almost  blmk,  with  a  tinge 
oTbrovn  or  olive.     This  api^ears  to  ame  from  the  obscuration  of  the 


Ci^r?E£,  AKD  ITS  ADULTERATIONa. 


^-'  1  nt  to  whether  the  presence  of  chicory  in  ground 

Slit^  il'le  or  not  by  meano  of  science,  was  referred  by 

Ul«   ^ftivuwUor  uf  (he  Exchequer  of  the  time  to  a  commtMion  of 

These  chuiuiiitt  roporlod,  that  "neither  by  rhemirtry  nor  by  any  other 
tu«»H>'.*  w  lid  iht)  iidmixturo  of  chicory  with  coffee  to  be  detected."  This 
'*  UK  piiblii'ly  (pitted  by  Sir  Charles  Wood  in  the  Himse  of 
,  uitd  nn  tlio  (tirength  of  it  the  goveriiiuent  refueed  lu  inier- 
I'ls  (It  the  |iu(Vttntion  of  the  adultcrution  of  coffee.  Now  at  the  same 
liuiti  thn  uullmr  showed,  in  the  nio:(t  conclusive  manner,  that  nothing 
iH  luuro  t'i*»y  ithil  certadn  than  the  detection  of  chicory  in  coffee  by 
Uiuuuk  of  the  hticroBiutjH}. 

Thvi  ilrurltiru  of  coffee  has  already  been  fully  described  ;  that  of 
ektt:'iti7  will  ttlmrtly  be  cotisidere*! :  it  iniiy  be  stad^d  now,  however, 
thitt  it  dilVi-m  in  overy  res|»ect  from  cotlee^  in  the  rounded  form  and 
ii4iiy  •e|iui.thiliiy  of  its  component  cells,  aad  iu  the  preiieuce  of  dotted 
dut-.u,  uimI  vuia  lactiocntia. 

Thu  thlffruiiueg  will  be  sufficiently  obvious  on  an  examination  of  the 
fciiluMiiig  ligurti, 

rtg.ar. 


tium  tht  rtnictiiru  tn  b  wmpl*  t.f  Corn*  «tf«Jfcr^«f  wOA  CwroRr. 
a  u.  coOfee  ;  b  b,  eliltwry. 

Detection  of  Mangold- WurzeL— This  root  differs  from  chicory  in 


d 


COFFEE,  AND  ITS  ADULTEBATIONS. 


127 


be  ffUI«d,  generally,  that  those  of  wheat  consist  of  rounded  and  llat- 
tened  discs  of  various  sixes.   The  appearances  which  they  present  ore 


Fdf.ao. 


■—111  of  Q^«  mOiMtniiai  wM  hoA  CmcuKr  om/  roaated  WitUT. 
•  a.  MAa  1  *  1^  olikorT  l  e  c,  whe«t  fluur. 

^NK^tinct  from  the  cells  of  either  coffee  or  chicory,  as  will  be  seen 
IH^Be  annexed  engruviof;.      Fig.  30, 

dH  fil*  Drieetion  of  BtMn  Flour.  —  The  substance  of  the  seed  of  the 
bcmn  b  BUide  ap  of  cellis  each  of  which  contains  several  litArch  cor- 
piBclcs.      The   fomi   and   chorocters  of  these  nre  very  distinctive  ; 
ihe^  uv  fur  the  oiomI  part  either  ova)   or  unifurni,  with   n  central 
vity    of  an  elongated  form,  and  from  the  margin  of  which  eborC 
9»  or   pmccoM*  may  be  seen  radiating.     So  long  in  some  of  the 
aniile*  of  medium  size  is  this  cavity,  that  they  appear  to  be  com- 
pletely   bisected;    occasionally    a    few    strongly    marked    concentric 
najTB  ore  visible.     Some  uf  these  characters  arc  exhibited  inT^^'.  iM. 

Om  lAr  Pfteciion  of  RiMtxtttl  and  Ortmml  Acorn  — 'tUa  prcacnce  of 
liitj  Dubfttmnce  is  distin<;ui»hed  by  the  lorni  and  bizeti  uf  the  starch 
corfwiftde^,  which  form  so  Urge  a  part  of  the  acorn,    /i^,  32. 

On  the  Detectwn  of  Savdiul. — The  detection  of  sawdust,  especially 
mabojrany  lawilust,  U  extremely  easy;  the  presence  of  woody  fibre  of 
•umc  kind  or  other  is  sure  to  be  discovered  h  hen  the  suspected  samplefl 


in 


COFFEE,   AND   ITS  ADULTERATIONS 


come — as  they  always  ought  —  to  be  ^aminetl  with  the  microscope. 
The  presence  of  sawdust  hftving  been  thus  asceruined,  a  pound  or  bo  of 


F4r>ai. 


CVtr  B^wlte^ali^  wUk  both  CmcoiT  iMrf  roaaltj  Bt.kir%. 
astuoflkai  bk^iiUtary  t  cf.  TOMMdtaui  lour. 

the  coflee  should  be  spread  out  on  a  slip  of  glass,  and  moistened  with 
wal*r,  when  the  fra;7nii»nl:9  of  wrBwly  fibre  uiut  pynemlly  be  pick<!d 
out  bv  mean*  of  a  netMJlc ;  they  .nliould  then  be  subjected  to  a  more 
careful  microscopicjil  sorutiny. 

The  woo«ly  fibre  of  plants,  like  the  cellulose,  starch  corpnsctes,  and 
vc»9cls»  frequently  no?sosses  distinctive  chnractcrs,  viHible  un<lcr  the 
inicroBunpe,  by  whicn  tlie  plant  or  tree  furniehin^  it  may  be  identified. 

In  the  cft'^e  of  malinjt[fiiiy  sawdust  the  ideiitificution  is  easy  enouph ; 
the  eompnrlness  of  the  Utile  masses  of  fibre,  the  utrong  rross  markin{^, 
and  the  n.lour  are  sulHcicntly  charnctcrislic. 

It  should  be  remembered  that  chicory,  especially  the  older  roots,  con- 
tains a  small  proportion  of  woody  fibre,  so  that  care  roust  be  exercised 
not  to  confound  this  fibre  with  exlraneous  woody  fibre  or  sawdust  intro- 
duced for  the  purpose  of  adulterutiun.  If  the  quantity  of  fibre 
present  be  very  small,  and  it  a^n'ees  with  that  of  chieory  in  its  struc- 
ture OS  seen  under  the  micrn^enpe,  there  can  be  little  doubt  but  that  the 
fibre  beloni:s  tn  the  root  of  chicory. 

On  the  Detection  of  Caramel  or  Burnt  Sugar.  —  When  the  water 


COFFEE,   AND   ITS   ADULTERATIONS. 


129 


added  to  auv  f^ainplc  of  fjroundcoirec  becomes  deeply  and  quickly  co- 
loured, and  when  on  examination  witb  tbe  microscope  it  la  ascertained 


Fig.  XI, 


Sunrle  oC  Onf<*t  otttJumud  tHiJt  ^^und  Acoas.    a  o,  oolite  i  b  6,  eklOdlT  | 


that  no  foreign  vegetable  is  present,  there  will  be  good  reason  fur  sap- 
posing  that  it  contains  burnt  sugnr. 

Again,  wht'o  shining  black  purticles  are  perceptible  in  the  coffee,  and 
these  slowly  dissolve  in  water,  pivinjj  ri»c  ton  dark-coloured  solution, 
it  undoubtedly  contains  the  snlfslani-c  in  question.  Soinelirnes,  when 
the  particles  are  too  small  to  be  tliscerncd  by  the  naked  eye,  tbey  maybe 
seen  under  the  microscope,  and  their  solution  iu  water  watched. 

Again,  the  presence  of  burnt  su^or  may  be  dctecte<l  by  adopting 
the  loUowing  j)roce»9: — From  a  weighed  ({uantity  of  dried  coffee  an 
infuaiun  in  cold  water  is  to  be  prepared  :  this  must  be  eva|>orat«d 
in  a  woter-batb,  dried,  and  lasted.  If  the  extract  bo  dark-coloured, 
brittle,  and  possess  the  bitter  taste  of  burnt  sugar,  no  doubt  remains 
as  to  the  presence  of  that  substance. 

Wfe  are  unacquainted  witb  any  process  by  which  the  quantity  of 
burnt  suffiir  prL'sent  con  be  accurately  determined,  seeing  that  the 
extract  funiishe<l  by  pure  coffee  vai-ie3  very  greatly,  and  that  of 
■dalterated  coffee  to  a  stiU  more  considerable  ext«nt ;  while  ftUo  the 


L»0 


COICOEY,   AND   ITS  ADULTEBATIONS. 


composition  of  the  burnt  sugar  is  so  much  chonj^d,  that  its  nmoait 
cannot  be  deter tniiied  in  thv  &ume  umniiur  as  ^apc  su^or. 

On  the  Deduction  of  Vertctmn  Red.  —  .Sniuetmics  mt hen  the  Venetian 
red  haa  been  t'iireles;*ly  i(ieor[>orutetI  with  tbe  cotlVe,  particles  of  it 
maj  bti  detected  with  the  naked  eye ;  but  it  h  not  often  tbat  it  can  be 
dbcovered  in  this  way.  The  process  to  be  adopted  in  ordinary  cases 
is  as  follows :  —  A  |M>ption  of  tlie  suspecto<i  t^>ft'.fe  is  to  be  incinerated, 
and  the  colour  of  the  ash  noted :  if  this  be  deoi>ly  coloured  and  of  a  rusty 
red  or  yellovrish  hue»  then  Venetian  red,  reddle^  or  some  unologotu 
earthy  substance  baa  been  mixed  with  the  Loflce. 

If  we  desire  to  form  &ome  opinion  oa  to  the  amount  of  this  present, 
the  cofl'ee  must  be  dried  ina  wuter-bsitb,  500  'jin.  incinerated,  nnd  the 
ash  weighotl  and  analyseil ;  thy  weight  may  be  compared  with  that  of 
the  ash  of  vjenuine  coffee,  and  the  usb  tbeti  tested  i|u:Lntitativcly  for 
iron,  and,  since  the  Venetian  red  is  »(>metimt\t  ilfldf  adulternted  with 
chalk,  fnr  it  also.  The  process  for  the  quuntiiative  estimation  of  iron 
will  befonnd  detailed  at  pp.  10*2.  and  141>.,  and  that  for  chalk  at  p.  lOt. 

It  has  thus  been  shown  that  coffee  \i  liable  to  a  liirjjd  Aud  scon* 
dahius  amount  of  adulteration. 

Tbe  duty  on  coffee  is  -id.  [H^r  lb.  until  April  5th,  1657.  Thereafter 
3(/.  per  lb. 

Lbi. 

Home  consumpLion  1854  duty  3J.  37,471,014. 

,»  1855  35,87fi,-i87. 

9  months  of        1 8 JG  2<>,522,8-2  J . 

„  1S55  27,598,417. 

Duty  4d.  on  and  after  April  21dt,  1855. 


CHrCORY,  AND  ITS  ADULTERATIONS. 

CmcoRT,  succory,  or  wiM  endive,  Cychorium  Tntyhus,  belong<i  to 
the  same  natural  family  of  plants  as  the  donilelion,  a  M^ry  chorac* 
rcristic  and  familiar  cognomen  of  which  we  refrain  from  moutiouiof. 
Like  the  dan<leliun,  chicory  is  indigenous,  and  may  be  seen  {rrowlng 
in  various  pai-Ut  of  the  country,  by  llie  road  or  hed;i:e  side  \  it  uiaT 
be  recognined  by  the  cwnipound  chamcter  of  its  tlower»,  and  their 
bright  anil  1>t^autiful  blue  coloin*.  It  blossomi  in  tlie  months  of 
August  and  September ;  and  uny  person  detiiring  to  |;et  a  sight  of 
this  very  notorious  vcgcUble,  may  grntify  bis  curiosity  by  a  walk 
along  tbc  banks  cif  the  Thamc*s,  from  Kew  tor  about  u  mile  or  «o  in 
the  direction  of  Kichuiond. 

'*  Tliia  plant,"  says  M'Culloch,  "  is  found  rrrowing  wild  on  calcareous 
soils  of  Eo{:Iand,  and  in  mo6t  countries  ofKurupe.  In  its  nalund  Atate 
the  stem  riiK^s  from  one  to  three  feet  higb^  but  when  cultivated  it  shuota 


CHICORY,   AND   ITS  ADULTERATIONS. 


131 


^ 


to  the  heifi;ht  of  Ave  or  eix  feet*  Tlie  root  runs  deep  into  iho  groiiud, 
and  is  white,  und  flciihr,  undyii^ldii  a  milky  jiiicti,  It  is  cultivtitijd  to 
some  extent  in  thiii  couiitrv  as  an  herbnge  jilaiit^  its  cxeollence  in  lliis 
re!4p*!t;t  having  been  strongly  insisted  upon  by  tlielute  Arthur  Ynung. 

"  Hut  in  Gi'minny,  and  in  some  pinM^i  of  th<?  KetheHand-.  and  Kriuioe, 
it  is  extensively  eultlvuted  lor  the  6uke  of  ilb  root,  which  is  utied  as  a 
suU'-tilutc  for  coffee. 

When  prepared  on  a  hir^re  scale,  the  roots  itre  partially  dried 
find  8t)ld  lo  the  niunutiiclurers  of  the  article,  who  wii>h  ihcni,  cut  tlieiu 
in  pieces,  kiln-Jry  them,  nnd  grind  ihein  between  tluLed  rulJers  into  a 
powder. 

"  The  powder  has  a  striking  rcseniblunce  to  dark  ground  coffoe,  and 
a  strong  ndour  of  liquorice.  It  hn.s  been  exten^ively  ii9C«l  in  Prussin, 
Brunswick,  and  other  pnrt*  of  Gerinany,  for  sevenil  years;  but  as  it 
wants  the  essential  oil,  nnd  the  rich  arouiatie  tltivour  of  ctifloti,  tt  Has 
little  in  conminn  wiih  the  latter,  except  it£  ouluur,  und  bus  nulhiug 
to  reeuuiniend  it  exL-cpt  its  cheapness." 

Notwiih»>tnndin^r  ihiit  ehicory  *'  bus  nothinj;  to  recommend  it  except 
\ix  cheapness,"  iind  th.il  it  \»  us.ed  exclusively  (o  aduUerulc  coffee,  it 
bos  uf  late  yonr.f  been  raised  in  prcai  quantity  in  tliis  country,  in  the 
counties  ol'  Surrey,  Bedford,  and  York,  owing  to  the  very  iuipro[>er 
enciuiragcmcnt  given  by  Government. 

Lar>[e  crops  of  chicory  are  grown  in  Yorkshire,  in  the  neighbour- 
hood, h  is  stated,  of  pronerty  behinging  to  a  lute  Chancellor  of  the 
Exchequer ;  and  it  was  tni^  circuniKtunce  wliich  led  lo  the  assertion 
that  he  was  bini»elf  an  extensive  grower  of  the  plant. 

Thii  statement  has,  however,  been  diatinetly  contradicted  by  the 
Chancellor  in  (juestiim,  wln>,  in  luuking  knuwn  llie  denial,  refrained 
from  any  allusion  t4i  the  circiunstancc  which  explains  the  origin  of  the 
Tepf»rt,  We  are  not  surprised  thtit  the  cbarae  slionld  have  Wen  made, 
fur  it  is  only  natural^  when  an  individual  pertinaciously  follows  a 
course  opjMJsed  to  reason  and  correct  principles,  that  an  endeavour 
should  be  made  to  uccounl  for  conduct  so  lingular,  and  that  it  should 
be  tniugined  that  souie  strung  per-»nnul  interest  existed,  whereby  the 
coufse  of  pruiecding  wlupteil  might  be  explained. 

Foreign  chicory  is  considered  to  be  preatly  superior  to  that  of 
£nuli»h  growth,  and  is  consctpichtly  much  dcurer. 

The  root  h  taken  up  just  before  the  nlunt  blossoms,  and,  when 
roasted,  Urd  is  added  in  the  pio[tortion  ot  2  Ibe.  uf  lurd  to  1  cwt.  of 
the  kiln-dried  root.  A^'hen  gitiuud  and  exposed  to  the  air,  chicory 
absorbs  water  readily,  and  becomes  umist  and  clammy. 

Analytvt  of  Chicory. 
Ohi(!ury  root  has  been  subjected  tu  examination  and  analysis,  by  the 
auttiur,  and  by  Dr.  Letheby  ut  the  author's  rei^uesit,  iu  three  condi- 
tions, luunelv:  — 

"  lat.  Iu  1(8  recent,  or  rsw  state. 

K  a 


13B 


CHICORY,    AND    ITS   ADULTERATIONS. 


"2nfl.  In  the  kiln-dried  condition. 

"  Hrd.  In  the  roasted  and  powdered  form,  afl  itis  used  for  the  adul- 
teration of  coffee. 

"Tbe  raw  root  furnislies  a  milky  juice,  wlucli  owes  its  opaeity  to 
the  presence  of  an  inert  vegetable  Bubrftunce  nuuied  liiuliiie.  The 
juice  in  very  bitter,  antl,  wlieu  filti^red  and  !ieate«i,  it  shows,  by  its 
turbidity,  that  il  contnin^i  a  small  ipinntity  of  albumen. 

•*  When  macerated  in  cold  water,  it  yields  about  13  per  cent,  of  solid 
matter  or  extractive,  which  Jtivcs  to  the  solution  n  very  hitter  taste; 
nlcohnl  also  extracts  this  bitter  conBtituent,  and  on  cvnporation  it 
funiitthes  n  gummy  product,  which  is  very  similur  in  tta  properties 
to  the  bitter  material  of  the  dsitnlelion  root.  Acetate  of  lead  pro- 
duces a  copious  precipitate  in  Lhe  liquid  from  the  deposition  of  (j^uiit, 
vegetable  acid,  and  colouring  matter,  liy  means  of  Felifniij's  test,  it 
was  found  tliut  the  raw  root  contained  1*1  per  cent  of  grape  sugar  or 
glucose. 

"  The  kiln-dried  root  possesses  all  the  characters  of  the  preceding:, 
but  in  a  higher  do^n^i?,  for  water  extracts  about  50  j>er  cent  of  solitl 
uiaLtcr;  and  the  solution  furnished  to  Fchlings  test  as  much  as  10*5 
per  cent,  of  sugar. 

"Neither  of  tbesie  specimens  exhibited  the  least  trace  of  stnrclii 
but  bv  boiling  in  water,  filterinp,  and  raoling,  they  yielded  a  Hraall 
quantity  of  a  while  powder,  wliiuh  liad  all  the  ehuraeter:*  of  Inuline. 

"The  absence  of  starch  in  tlic  state  in  which  the  root  is  onlinarily 
used  is  also  cnnclusively  ?hown  by  luenns  of  the  microscope  ;  and 
we  find  that  the  tissue  contains  abundance  orcellnlo»e,  which,  by  the 
action  of  strong  sulphuric  aeld,  gives  a  product  that  renders  iodine 
blue. 

**Tlie  roasted  chicory  rout  yields  from  45  to  65  jwr  cent,  of  soluble 
extractive.  Its  solution  in  water  is  aciil,  and  it  dot^s  not  possess  the 
pecufiiir  bitter  taste  of  the  raw  root ;  but  the  taste  of  the  li(|uid  is  more 
like  that  i)f  burnt  sugar.  The  cop|)er  test  shows  the  presence  of  from 
10  to  13  (>er  cent,  of  sujjar. 

"The  followintr  analyses  represent  the  per-ccnt«ge  composition  of 
the  root  in  itit  different  conditions :  — 


I 


Hygroscopic  moisture 

Gummy  matter  (like  pcctine)    • 

Glucose,  or  grnpe  sugar 

Bitter  extractive 

Fatly  matter 

Cellulose,  inuline,  and  woody  matter 

Ash  - 


m  Knot. 

K)ln.dried 

77-0 

]5'0 

7-5 

208 

11 

10-5 

40 

li)-3 

0-6 

1-9 

90 

29-5 

0-8 

30 

100  0 


100-0 


CHICOBY,    AND   ITS  ADULTERATIONS. 
"  The  composition  of  the  roasted  root  was  ns  fullows  :  — 


133 


Hvproscopic  moisture 

Gummy  matter 

Glucose      -  -  - 

Mutter  like  burnt  sugar 

Falty  matter 

lin^wn  or  burnt  woody  matter  - 

Ash  - 


lit  S|>rclfnea.    2iiil  S|N-cimeD. 


14-5 

12-8 

9-3 

14-9 

12  2 

10-4 

291 

24-4 

20 

2-2 

28-4 

28-5 

4-3 

6-8 

1000 


100-0 


"  The  a»h  of  these  had  the  following  composition  :  — . 


Chloride  of  pDtiL<!f>ium 
Sulphnte  of  (Mtosh 
Phosphate  of  pnliuh 

Pitto      of  mu^ncdia 

Ditto      of  Jiiiio 
Cnrbonate  of  lime 
Atuiiiina  and  oxide  of  iron 
Sand  - 


\%t  Sprdmm. 

2nd  Specimen 

0  22 

0-43 

097 

0  98 

1-41 

1-37 

0-30 

0^53 

040 

0-81 

010 

0-26 

OiM) 

0-20 

0-70 

2-20 

430 


6*80 


Raw. 

H'Mtact 

23-76 

n  9fl 

30-49 

15-96 

35-23 

17-»8 

320(i 

9-86 

ktessrs.  Grahnm,  Stenhouse,  &nd  Campbell  *  found  in  four  samples  of 
chicory,  the  following  per-centugea  of  grope  sugur  :  — 


Foreign  chicory     -  -  - 
Guernsey  chicory   - 

Knglish  chii'ory      -  -  - 

Yorkahire  chicory  -  -  - 

ITie  quantities  of  sugar  in  manfjold-wurzel,  carroM,  turnips,  parsnips, 
beet  and  dandelion  roots  wcrt.*  found  to  be  nearly  as  •;reat  as  in 
chicory,  and  hence  the  sugar  present  in  it  does  not  affbitl  a  means 
by  which  it  may  be  distinguished  from  other  sweet  roots  when  mixed 
with  cofTee. 

Tbc  following  repre6ent«  the  per-cenlsffe  composition  of  the  ash  of 
four  samples  uf  chicory,  according  to  Messrs.  Graham  an<I  Sten* 
house:  — 


CKvmlcd  Hrport  on  the  mode 


of  dotvctinf  V«gc««bl«  SubcUocM  mlMd  with  CoAc, 
K  3 


'184 


CHICORY,  AND   ITS  ADULTERATIONS 


ttartm 

Exit  1Kb- 

roTMcn. 

nnerM>7. 

FotMh 

33-48 

?4-W 

»-56 

MDT 

Sndn 

H-I'i 

|.V|0 

SH4 

8-«l 

Uip« 

9W* 

SW 

5-00 

fiSI 

>fiirnMla      ... 

5  27 

7 -Si 

5-41 

a-M 

SfMt)ulu«IJf  fir  Iron 

3 -HI 

MS 

5-SS 

a-ftv 

Sul|ihunc  Aclil 

I0-J9 

loss 

S-S8 

601 

<_'hl«rlitr>       ... 

4ftl 

4tM 

sss 

4-.Sfi 

Carltoolc^iM 

17H 

a-HH 

a^p 

S-)» 

Vhotphurtcadd 

tOG« 

11^7 

T« 

6-B^ 

Sitli-a 

3H1 

'ifii 

IVJS 

10-fi3 

S«nd 

•J '38 

M-CH 

33-10 

W-19 

lOO-M 

»fl<M 

it»-6e 

VMM 

MeMn.  Grnhftm  nnd  Stcnhouse  found  the  stltca  uid  sand  insoluble 
in  ncids  to  ha,  in  four  sninples  of  roasteil  cliicory,  us  follows, — 10*69, 
13*l3t  30'7I,  find  SUiHa  per  cent,  of  the  nsh ;  the  quantities  of  this 
Hilira  f^oluhh;  in  iitknl!  wa.^,  in  tlie  s.itnc  Hiiniplcs,  808,  0'3'2,  20*19, 
and  2;rlO  purr.?.  Much  of  tlu3  pdica  was  doubtlefs  derivtfd  from  the 
sand  »iid  dirt  iirllicrinj;  to  ihe  iniperfiMlly  cleansed  roots. 

The  chief  eoiwiiluents  ofroiisteii  chicory  ure  the  gum,  plucose,  nnd 
cnmmel.  The  quantltjr  of  nitrogen  in  chicory  is  not  one-half  Omt  of 
coflee. 

Bv  nn  exnminnlton  of  the  fiirepninc  antilyscs  it  will  be  seen  thntthe 
roni  does  not  cnntiiin  nnythiii^j  whieh  can  pof^^ibly  he  rej^nrded  na  a 
Hubttitute  for  cofTee.  It  will  be  sdso  m;inife<)t  that  in  tho  nrocosa  of 
ronatinjr.  the  bitter  prinoij)lo  of  ilic  reeent  root  is  partly  ues(i*oyed, 
iind  thut  by  the  lorrefrtclton  of  the  snccharinc  and  othLT  constituents 
li  nunntity  of  caramel  is  producetl,  whieh  has  nn  virtue  beyond  tinit 
of  burnt  supar.  The  large  (['lantity  of  oil  fouml  is  dlmhtle^s  derived 
from  the  Inni  n*ed  in  rousting  the  root ;  nearly  •'i  per  cent,  of  fat  has 
Wen  obtained  (Voni  some  sani])les  of  torrefietl  chicory.  The  quantity 
of  oil  nnturnllr  presiTt  in  the  root  is  exceedinjrly  sninll.  It  is  like- 
wise evident  thiit  the  kiln-dried  root  hns  under^rone  fermentiition, 
whereby  the  amount  of  sugar  hiis  become  greatly  inereoscd. 

Stmeture  of  Chkttry  Hoot, 

In  the  raw  chicory  root  four  parts  or  itinietnrcs  mfty  be  dietin- 
fruishcd  with  facility  :  cells,  dotte<l  vessel^  vessels  of  the  latex,  and 
woody  fibre. 

When  the  ndulterntinjf  grinder  or  merchant,  in  the  secresy  of  his 
own  wiirehouse,  lirst  reduced  cincory  root,  pnriinip?,  corn,  bpuns,  &c^ 
to  chiirrod  nml  nearly  impulpable  powders,  the  idea  probably  never 
entered  hi-*  mind  that  enou;;h  of  the  diHttnctive  structural  charat'ters 
of  each  of  these  tiubsttances  still  remained  undcstroyed,  to  enable 
the  man  of  science  to  dr:ig  to  light  his  guilty  deeds,  and  to  detect 


I 


I 


CHICORY,    AND   ITS   ADULTERATIONR. 


1.15 


their  presence  in  every  parcel  of  adulterated  cofiee  sent  out  from 
his  premises. 

In  the  roasted  and  cbarreil  chicorj  root  the  same  structures  may  be 
detected  as  arc  di^tinguisbablc  in  the  raw  or  unroasted  root. 

The  ohief  part  of  the  root  h  made  up  of  Jittle  utricles  or  ceils. 
These  are  jrenernlly  of  a  rounded  form,  but  Bornelimes  they  are 
narrow  and  elongateil.  The  former  o<rcur  where  the  pressure  is 
least  and  the  root  soft ;  the  Utter  in  the  neighbourhood  of  the 
vessels. 


?■, 


^ 


Fngmtnl  oflUAKnn  Cmk-dkt  H<>ot.  ulun  from  •  Mmpk  of  wluUcratcd  eoflH. 
khuwIiiK  the  celU  <if  wbteli  li  U  |irliiiH|ia)ljr  ctui^li utcil.   Urmwti  «lili  Uic  CmmcrA 

The  dotted  txMch  are  particularly  abundant  in  the  central  and 
harder  pnrM  of  the  root,  which  they  traverse  in  bundles:  they  are 
cylindrical  unbranched  tuh(:.%  tnpcrinor  to  a  point  hL  either  extremity, 
and  elegantly  marked  on  the  nurfare  with  short  libres,  describing  an 
interrupted  spiral  course.     Fi^.  3-1. 

In  studying  the  structure  of  chicory  root,  wc  have  clearly  ma'ic  out 
the  origin  of  ibo  dotted  ve^seIp  in  narcow  elunj^ated  cells,  ta|ierin;(  to 
a  nhorii  point  at  either  end,  at  tintt  smooth,  but  subsei^uently  exhibiting 
faint  oblirpic  markings. 

The  vessels  of  the  latex,  va*a  lacticcnttay  are  preifent  in  most  plants, 

K  4 


136 


CHICORV,    AND    ITS    ADULTERATIONS. 


bnTing  a  milky  juice  or  sap;  they  form  branclicfl  and  frequently 
anttMtoinosing  tubes,  of  smaller  diameter  than  the  dotted  vessels,  and 
witii  smooth  membranous  panetes. 

Fig,  M. 


Tnignmi  of  RoASTBDCiiirovr  RimT.  Uhto  from  •  iunple  of  tdoltrnitcd  cvtht, 
thowlTic  the  tlotudor  liil«rni|>t«il  iplrftl  vcmcU,  whicli  |>bm  In  bundle*  thmufli 
thr  Ctfutral  imiXm  of  (h«  rouU  Dtk«u  wllh  the  Cuncrft  Ijucidk,  uul  mMgnitid 
11(1  dlameteri. 

These  vessels  afford  a  useful  means  hy  which  chicory  may  be  distin 
guished  from  most  other  roots  employed  in  the  adulteration  of  coflee. 

The  tofyody  fibre  of  chicory  root  does  not  present  any  markings  or 
other  peculinrities  of  structure  of  a  distinctive  character. 


Properlien  of  Chicory. 

Recent  chicory  root  is  possessed  nf  active  medicinal  properties  in  con 
sequence  of  irhii'h  it  has  Inngbeen  included  in  th(»"Mftlenvi  Modica.** 

Those  properties  resemble  closely  those  of  the  allied  pl.inf,  the  dan- 
delion, in  reference  to  which  we  find,  in  the  work  of  Dr.  Pereira,  the 
following  observations  :  — 

"  Its  obvious  effects  are  those  of  a  atnmnchic  and  tnnic.  In  large 
doses  it  acts  as  a  mild  aperient.  Its  diiirctie  operation  h  less  obvious 
and  constant.  In  various  chronic  diseases,  its  coti  tinned  use  is 
Attended  with  alterative  and  resolvent  effects;  but  where  the  digestive 


A 


I 


CHlCORTj    AND   ITS  ADULTERATIONS. 


JS7 


orcansi  are  weak,  an<l  remlily  disonlrrefl,  Iftrnxacum  19  very  apt  to  oc- 
cuion  dyspepaiu.  tlalulency,  pain,  aiid  diarrhcea.** 

Ftg.Vt. 


Thi«  ffiwTBvlng  itpnmabt  Um  narrow  tnA  brftnclii«<l  v«Meli  t  Veto  Taetiefntiai,  w 
•tNindui  In  i'mcoRT  R<k>t,  «hkh  conTcr  Uie  milkv  iaicc  of  tb«t  plant,  aitd 
alao  tlioir  llidr  rvlaliuii  to  the  onUnarjr  uUriclca  or  nlla,  of  wtilch  Ume  lutNtauca 
of  tht  itKrt  i*  principally  inad«  up. 

These  remarks  of  course  apply  to  the  recent  root.  Proressor  JMlin- 
Bton,  whose  views  appear  to  us  more  favoumble  than  the  facts  warninf. 
tbu«  exprofses  himtioif  in  regard  to  roasted  chicory  :  *  — 

'*  It  posscsites  in  no  degree  the  pleasant  aruina  which  recommends 
the  genuine  roasted  coffee. 

"  The  active  ingredients  in  roasted  chicory  are,  first,  the  empyrcu- 
matic  volatile  AW  :  thitf  is  pro<luced  during  the  roastinf? :  and  though 
not  to  frogranU  this  oil  probably  cxcreiiiea  upon  the  system  some  of 
tbe  gently  exciting,  nerve  soothing,  and  hunger  staying  inlluence  of 

•  Loe-dl^p.  Stft,  >16,andS17. 


138 


CHICORT,   AND   ITS   AD0LTERATIONS 


tbc  similar  injrredients  contained  in  tea  and  coffee;. and,  second,  the 
hitter  principle.  When  ttikcii  unmixed,  this  substinoe  is  lo  uian}', 
wbik'  ihey  are  unaccnstnnied  to  it,  nor  only  disajn'eeivWev  but  nawpeous 
in  a  high  deiircc.  It  may,  hoivifver,  like  many  other  hitter  principles, 
possesm.  as  1  have  saiil,  a  tonic  or  strengthening;  prnperty.  Taken  in 
niodernte  quantities  these  ingreilients  of"  cJncnry  Bre  pnibably  not  in- 
jnrinus  to  healthy  hut  by  prohmfred  and  frequent  use  they  produce 
lieaithurn,  rranip  in  the  stomach,  ]nF3  oC  appelite,  acidity  in  the 
moulh,  eonstlpsiticm  with  intemiittcnt  diarrbcea,  weakness  of  the 
limbs,  tremblings,  eleepleasness,  a  drunken  cloudiness  of  the  sense?, 
&c.  &c.  At  the  best,  therefore,  chicory  is  a  substitute  for  coflee 
to  which  only  those  to  whom  the  price  is  an  object  ought  to  have  re- 
course." 

Thi;*  opinion  of  Professor  Johnston  ngrees,  therefore,  nearly  with  that 
of  M*Culloch,  already  quoted,  to  the  effect  that  chicory  "has  nothing 
to  recommend  it  except  its  cheapness." 

For  ourselves,  we  would  remark  that  while  chicory  is  substituted  to 
an  cnormoufl'extent  for  coffee,  it  yel  possesses  none  of  the  characteristics 
of  a  true  substitute.  We  believe  that  the  nunntity  of  "empyreunmtic 
essential  nil "  present  is  inntutesimal,  and  tliat  tlie  *'  bitter  principle" 
consirits  chietly  of  burnt  sujiar. 

Although  we  are  nut  ilispotted  to  attach,  therefore,  much  weight  to 
t?iese  sO'calledactipt  in^r<fietih  in  roasted  chicory,  it  is  yet  certain  that 
it  does  contain  constituents  possessing!  active  and  mctlicinal  properties 
not  of  a  desirable  character  ni  an  article  of  fiKnl. 

Thus,  it  is  very  certain  that  the  infusion  of  roasted  chicory  is 
aperient. 

In  proof  of  this  we  will  cite  the  resulta  of  some  observations  of 
our  own. 

Three  persona  partook  of  chicory  at  breakfasts  The  infusion  was 
dark-coloured,  thick,  destitute  of  the  nprecable  and  refreshing  aronm 
so  characteristic  of  coffee,  and  wa.**  of  a  bitter  taste. 

Each  individual  experienced,  for  some  time  after  drinking  the  infu- 
sion, a  sensation  of  heaviness,  a  feeling  of  weight  at  the  stumach,  nnil 
frreat  indisposition  to  exertion  ;  in  two,  headache  set  in ;  und  in  tlie 
third,  the  bowels  were  rclnxcd. 

In  second  and  third  trials  of  the  chicory,  the  same  feelings,  weight  at 
the  stomach,  and  want  of  energy,  were  exjwrieneed,  but  no  headache 
or  diarrhoea. 

Several  other  trials  were  subsequently  made,  with  nearly  similar 
results. 

But  chicory,  it  will  be  said,  la  seldom  taken  alone  in  this  country, 
and  when  mixed  with  coflee  these  effects  are  not  proi.hiued. 

Two  persons  partook,  for  a  considerable  period,  twice  a  day,  of  an 
article  denominated  coffee,  costing  one  shilling  aiul  sixpence  a  pound, 
and  largely  adulterated  with  chicory  :  during  nearly  the  whole  of  this 
time  they  both  sufiered  more  or  less  from  diarrhcca. 


^ 


CHICORT,   AND   ITS  ADrLTER-XTIONR. 


139 


From  the  result  of  these  trials,  therefore,  we  are  warranted  m  con- 
cluding that  nt  least  some  doubt  is  attached  to  the  assertion  of  the 
**  whoicsnme"  properties  of  chicory  root  a*  an  artirlo  of  diet. 

So  well  are  niothem  in  France  and  fiermiiny  luqiiiuntod  with  the 
aperient  pro|)ertie«  of  chicory,  that  they  freijueiuly  give  iiifaTita  and 
young  children  n  strong  infunion  of  the  roAKted  root  as  an  aperient, 
preferring  it  to  ordinary  medicine  on  account  of  lU  less  disagreeable 
tlftvour. 

Again,  it  is  the  opinion  of  an  eminent  ociillfit  in  Vienna,  Professor 
Beer,  that,  the  onntinual  uNe  of  chicory  seriously  affects  the  nervous 
system,  and  gives  rise  to  blindnes**  from  amaurosis. 

The:*u  are  seriniis  effects  of  the  use  of  chicory,  and  should  make 
those  in  autliority  hesitate  before  they  foster  the  use  of  this  article 
by  pivin;;  to  ita  sale  an  undue  and  unfair  preference.  * 

The  greater  pHrt  of  the  chicory  used  is  grown  in  this  country,  and 
does  nut  pay  nny  duty  ;  and  vet  it  is  allowed  to  be  mixed  with  coffee 
to  *ny  extent,  an  article  bearing  a  very  hit:h  duty. 

Of  the  "nutritive"  propcriie.s  of  chicory,  of  which  Sir  Charles 
Wood  entertained  so  liijrii  mi  opiiiirtu,  we  need  say  but  little,  feeling 
Hamred  that  the  reader  will  scarcely  be  disposed  to  question  the  accu- 
racy of  the  assertion,  that  a  nioulliful  of  good  wheuten  bread  contains 
more  nourishment  than  u  oup  of  iniusion  of  chicory. 

Chicory  and  cofTee,  then,  mny  be  lliiis  contrttsled. 

They  diOer  from  ench  oilier  in  llieir  bnlanicnl  nature,  in  chemical 
Coinp«>sition,  ami  in  phy>iological  iictinn  ivnd  pru[Krrties. 

Cuffce  is  the  fruit  nr  seed  uf  a  treu,  while  chicory  is  the  succulent 
ro4tt  of  a  herbaceous  plant.  Now  it  is  a  well-tiscertained  fact,  that  of 
all  parts  of  vegetables,  tlie  fruit  imd  see^ls  usually  possess  the  nuist 
active  properties  :  this  is  no  doubt  due  to  the  circumstonce  of  their 
being  Ireely  exposed  to  the  induence  of  liiiht  and  air  — agencies 
which  promote  chemical  changes  in  tlie  plant,  and  so  cflVet  the 
elaboration  of  those  complex  organic  substances  on  which  the  activity 
of  vegetables  depends.  On  the  other  hand,  it  must  be  manifest,  that, 
as  the  roots  ore  removed  from  the  intluencc  of  these  powerful  agencies, 
they  CAonnt  be  so  richly  endowed  with  active  properties ;  ami,  mdeed, 
there  are  but  few  roots,  which  contain  either  alkaloids  or  vnlaiile  oils 
— tbe  two  classes  of  cAusiituenis  which  give  to  colFec  im  peculiar 
▼irtnes.  The  distinction,  therefore,  between  the  properties  of  tne  seeds 
and  niots  of  plants  is  very  important,  and  it  is  especially  so  in  the  case 
before  m». 

The  iiifiisiou  of  the  one  is  heavy,  mawkish,  and  nearly  destitute 
of  aroma;  that  of  the  other  is  light,  fragnuit,  and  refreshing. 

Coffee  contains  at  least  three  active  jirinciples,  or  constituents,  viz., 
t]ie  volatile  oil.  the  tannin,  and  the  alkaloid  caffeine ;  in  chicory  there 
arc  no  analognus  constituents. 

Coffee  exerts  nn  the  system  mnrkcil  and  hiahly  important  physio- 
logical eflccla,  of  u  beneficial  character.   There  is  no  proof  that  chicory 


140 


CHICORT,   AKD   ITS   ADCLTKRATIONS. 


exerU  any  one  of  these  effects,  while  it  is  very  questionable  whether 
the  properties  which  it  really  docs  possess  are  not  really  hurtful. 


Adulteka TICKS  OP  Cbicokt. 

What !  chicory  aduli^rateil  ?  A  substance  used  to  adulterate 
another  article,  itself  adulterated  ?  Imposi^hle!  Improbable  as  the 
thinf;  appears,  it  is  nevertheless  true. 

When  it  is  remembere*!  that  all  the  vegetable  substance*  employed 
in  the  adulteration  of  coffee  re^^uire  to  be  charred  or  roasted,  and 
that  to  effect  this  a  suitable  apparatus  U  require*!,  such  as  but  few 
retail  grocers  possess,  it  at  once  becomes  at  lea^t  {M*obable  that  these 
suhstances  are  prepared  for  them  by  other  parties. 

This  impression  acquires  increased  force  when  it  becomes  known 
that  the  majority  of  grocers  bay  their  chicory,  not  in  nibs,  but  in 
ptncder^  and  that  this  is  supplied  to  them  by  certain  wholesale 
ckieorr  houses  which  charge  for  it,  in  general,  a  less  price  than  for 
the  niba,  or  angrouiid  root  itself^  or  than  genuine  chicory  powder  can 
be  fairly  sold  at. 

'Vhe  subsUmces  which  are  either  subetitut^  for  chicory,  or  mixed 
with  it,  are  very  numerous ;  «everal  of  these  we  have  ourselves 
detected^  while  otben  have  lieen  discovered  from  time  to  time  by 
different  parties.  They  tnciutU  all  Most  employe<i  in  the  tuiulferation 
of  coffee;  indeetl  the  jjreator  number  of  substances  met  with  in 
aitulterated  coffee  are  introduced  into  it  through  the  chicory  with 
which  it  is  mixed. 

This  conclusion  is  deduced  not  only  from  the  examination  of  a  con- 
siderable numb^  of  sanplcs  of  powilered  chicory,  but  Irom  evidence 
derived  from  other  sources. 

Dr.  Pereink  in  184J,  published  in  the  **  Pharmaceutical  Journal** 
two  very  useful  articles  on  the  aiiultfration  of  coffee  and  chicory : 
from  the  first  of  these — that  oo  coffee — we  extract  the  following 
remarks:  — 

**But  while  tke  groocn^  on  the  one  hand.  eheM  their  coftomers 
bv  ailulteniting  tauflce  with  cbioorr,  the  ohicorr  dealer?  in  turn 
CMit  the  gn->cerv  }yr  adnlteratinp  chicory;**  aud  be  then  goes  on  to 
dMtribe  cvrtaiu  aduUeratiiuu  of  chMX>rv,  thoie  with  Btxmhrv  poM:der 

Another  circumslaMe  wludi  pfoves  not  only  tibat  chicory  is 
Adtthanbad,  hnx  ako  tkat  iha  leUctw  oi  ehleoty  puwtlet  arc  in  some 
OMM  partieB  to  the  aduUeratioiv  »  that  the  nowder  is  tooietames 
said  ttiuer  t^  market  tvrico  at  which  getiuicte  chicory  can  be  procured. 

The  MibstaiKV*  with  whtcfa  diioory  has  bean  mi,^ laiiH^l  to  be 
aduUermlcU,  are  all  thi«e  article*  which  har*  be««  •wnHvmled  under 
Co4ire;  nameiy,  dlfferrat  kinds  of  roasted  cora,  aa  wlnrt,  and  rye^ 
oeormtt  CBrroft,  mm^wU'tmntt^  Anf  rooi;  swrifcrf;  haktd  Uters, 


CHICOUr,   AND   ITS  ADULTEBATIONS. 


Ul 


hurnt  sugar   or   biack  J6ck^    Venetian   red^  atid  other   analogous  red 
earths. 

Wiih  regard  to  the  use  ofeanots  and  parsnips,  Mr.  Guy,  in  evidence 
before  the  Parlianieiitary  Coinniiltfe,  makes  the  fblltiwiiig  statement  :  — 

"  I  renjeinber,  one  year  when  ehitiory  was  worth  *il/.  per  ton,  manu- 
facturing 700  tons  of  carrots  into  chicory.  Tliey  were  grown  by  one 
gentleman  in  Surrey,  and  supplied  U>  the  house  where  X  was,  and  350 
ions  of  parsnips." 

Besides  the  above  named  articles,  *'  coffee  jUghU  **  and  "  Hambro* 
powtter"  hiive  been  used,  as  also,  it  has  been  alleged,  exhaiuted  tajt^ 
Icnown  as  crqoU,  and  oahhark  poinler. 

The  following  engraving:*  exhibit  the  microscopical  characters  of 
chicory  adulterated  with  wheat  Hour,  also  with  a  substance  resem- 
bling ground  acorn,  of  oak-bark  Ian  powder,  and  of  exhausted  ton  or 
croata, 

Ar.ao. 


leOTT. 

a  a  ar«  the  rfll*  ■ud  wimI*  of  fkintrf  root,  vhllp  ilxMf  mirkr^l  ^  U  art  lt>a 
nwvti  eorputclH  of  tuAttU.  No  bo<U«a  Us  IM  leul  tCMiobUosUictc  occu>  in 
gmulD*  clucary  powder. 

Acmrding  tn  Dr.  Pereira,  "Ifitmbro*  powder  consists  of  roasted  and 

ground  peas,  &c^  coloured  with  Venetian  red.  The  term  cnffrejiights 
IS  applied  tn  the  thin  membranous  ront  (endocarp)  which  separates 
from  the  coffee  seed  in  the  act  of  roasting. 


149 


CHICOKT,   AND   ITS   ADULTEKATIONS. 


Tn  Dr.  PereiruH  arlk'le  on  Chicory  wc  meet  with  ihc  following  re- 
miipka  in  reference  to  Venetian  red  :  — 

"In  a  previrus  number  we  explained  tbe  nature  of  Venetian  rt<l. 


n  a,  nib  of  cAtery;  6  ft.  fngmcnU  containing  ngmeronf  lUreh  (kv|iuw1m.  rc- 
tcmbllng  Ibowc  of  fKXim  ;  c  r,  wiMuatc  iikruli  itraouk*  :  (f  il.  |K>fti<L>ii«  i>r  »  brown 
tnrmbrwM,  irilbuut  Kmtunit  urgituiMlluu,  vvrjr  cumin liiiIj^  ubaemd,  uid  Jv 
rini,  frutn  the  lutaof  ue  teed. 


iron,   nbtaiueU   by   enlcininn 
Tlie  "iilTcrcnt   colours  oi'  the 


It  is  essentially  the  aevquioxide  of 
couunon  coppciaa  (nulpliale  ul'  irun). 
product  dupeiiil  on  tlic  tcmjfcralure  to  which  the  8*.'S(|uioxid.»  is  sub- 
jected. When  it  lias  l^een  exposed  tn  nn  intense  while  !ie*L,  its 
colour  deepens,  and  it  is  llioii  termed  tiurple-bruKti.  The  lighter  tint 
of  Veucliun  red  is  produced  by  auullerution.  Our  infornmnt  (a 
maiiulueturer)  \oU\  us  that  Vem.'tiaii  red  wan  *  adulleraled  to  suit  the 
various  priced  of  the  umrket.*  \Vc  did  not  think  it  vxpi'dient  to  prv 
into  the  iiaturu  of  the  adulleratin;;  injji-edient,  but  u  iViyiid  suggests 
that  it  is  reddle,  the  subatimce  used  for  nmikin};  sheep. 

*'  Vcnetiuii  red  h,  we  believe,  the  princi[ial  sutwUince  at  present  used 
for  colourinu'  rliifory :  (H.ciisionally  oiher  agcntiJ  have  been  employed. 
A  deolcr  tclU  us  tb:it  he  once  bought  a  quaiiiity  of  chicory  which  cou- 
tiiined^O  per  cent,  of  lo^wouti  and  mahogany  dust 


CHICOBT,   AND  ITS  ADULTERATIOKS. 


ua 


Rb»UI.T9   or  TUB   EXAMINATIOH  OF   SaUTLES. 


The  results  of  the  Microscopical  examination  of  T^iViV-ybitr  samples 
of  cUcorj  powder,  iiiadti  some  tiuie  back,  some  of  which  were  put- 


Fii.i». 


TtiMjtnwton  ixhlUU  t)M>  stnielnm 
liUdiuut-lcn. 


In  OAK-Bin  mwm,—ihM  raMntf 
M.    l>rkwii  wlUi  Um  CAiMn  I.ncida. 


cliaseil  of  diffcreot  grocers  and  others  obtained  fVom  manufacturers, 
were, — 

l»l.  That  Fourteen  sumpleti  were  adulterated. 

*2rid.  TImt  in  yiite  the  adulteration  consisted  of  roasted  Cora. 

3r<l.  That  »rorchc<t  Benns  were  present  in  Four  of  the  samples. 

4th.  That  in  One  case  ground  Acont  was  »letected. 

The  resulu  of  the  examination  of  Twenty-three  other  samples  made 
at  a  Bubeetjuent  pi'riud  were, — 

Ist.  "I'hnl.  Elecen  or  one-half  nf  the  samples  were  adulterated. 

•Jnd.  Thql  FotP"  of  the  chicory  potcderi  were  adulterated  with 
rxtasted  W'hetti- 

3rd.  Thiit^Tinuw/  Acorns  were  preMent  in  an  equal  mtmher  ofca$es. 

4ih.  Thst  Two  of  the  samples  contained  Sawdust^  and  one  Mahogany 
Saiifdnnt. 


U4  CHICORY,   AND  ITS   ADULTERATIONS. 

5th.  Tlml  Mangold- wurzel  waji  detected  in  One  of  the  chicories^ 
6tb.  That  i«  One  instance  roauted  Carrot  was  present. 


Thli  dmrloff  exliiblta  the  ■Iruelum  ■Irlovt'd  in  th*  Tak  known  1»  KorTolk  hjr  tht 
BOHM  of  "  Croat;"  uid  tueU  for  fuel,  fee 

Lastly,  the  results  nf  the  cxAmination  of  Thirty-eight  additional 
samples  of  chicory,  hntli  ns  pnrrhQ!«pfl  from  shops  nnd  as  pronirod  from 
inanufactiirprs,  nnd  whirh  cx;iniinntion  was  in^titutod  inninly  for  the 
purnoBo  of  (Iptcrniinin;!  whi-ther  Vonctmn  red  or  other  analogous  fer- 
rugmous  earth  wil-*  i'niplr»veil  to  colour  ehicory,  wlto, — 

1st.  That  out  of  the  t^i'^htnen  saiuples  of  chicory  procured  froia 
manufacturers,  Five  were  adnlttfrutfd  with  roasted  wheai  farina, 

2nd.  That  ffCP^n/Zof  the  samples  yiehled  a  coloured  ash, 

3rd.  That  out  of  the  Sixteen  samples  of  chicory  purchased  at  the 
establishmPTits  of  different  grocers  in  the  metropolis,  One  was  odul- 
temteil  yi\t\\  rtmxted  fari^ui. 

4th.  That  xhaaxhes  of  several  of  the  samples  were  highly  coinured, 
indicating  the  presence  of  some  rtd  ferruginotts  earthy  as  reddle  or 
Venetian  red.  In  two  samples  the  incorporation  was  so  imperfect 
that  we  were  enabled  to  separate  large  particles  of  the  Venetian  red 
from  the  chicory  powder. 


CHICORT,    AND   ITS   ADrLTERATIONS. 


145 


* 


We  have  now  shown, 

Tliat  L'hieory,  ftn  urucle  used  to  mlulterntc  another  article,  is  itself 
largely  adulterated. 

Ttiat  the  dcal*:rs  in  or  man u fact urera  of  chicory  ore  in  many  cases 
tbeparties  wbo  practiiie  this  adulteriition. 

We  are  sorry,  however,  to  declur*.%tliaL  in  those  instances  in  which  the 
retail  grocers  do  not  themselves  adulterate  the  chicory  they  vend,  we 
are  iinshle  in  AC(|uit  them  of  pnilty  knowledge  of  nnd  participation  in 
the  fraud  :  this  knowledpe  is  displayed  in  the  tact  that  the  fraudulent 
•rrocer  frequently  purchmacs  chicorv  in  powder,  at  a  price  at  which  it 
IS  not  possible  to  pro'iurc  genuine  chicory. 

The  prices  demiuidcd  for  tht;  several  sumplog  nnalysod  varied  from 
5d.  to  U,  per  lb. ;  the  ordinary  charjie  bein;;  8rf.  The  price  of  chicory 
in  powder  to  the  trade  ranges  in  general  from  20*.  to  32*.  per  cwt. ; 
thus  the  profit  of  the  retail  grocer  on  the  sale  of  chicory  powder  is 
fleldom  under  cent,  per  cent,  and  often  much  above  it. 

On  the  Detection  of  the  Adulterations  of  Chicory. 

The  Chancellor  of  rbe  Kxchequer,  in  May  (1850),  stated  to  the  House 
of  Comninns,  that  "  having  desired  tlie  iioanl  uf  Inland  Kevenue  to 
Btnte  wheiht-r  there  was  iiny  ready  and  avjtiliible  proof  of  the  mixture 
of  chicory  with  coffee,  he  had  received  a  reply  In  the  etfect,  that  four 
experienced  persons  having  been  employed  in  mnking  experiments,  the 
re!*ult  of  the  incjuiry  wns,  that  neilher  by  chpmical  tests,  nor  in  any 
other  way,  cnidd  they  aswrlain,  wiih  any  degree  of  certainly,  whether 
the  mixture  eontiiincd  chicory  or  not."  • 

Notwithstanding  thid  fornml  and  apparently  outhoritntivefitatomcnt^ 
the  fact  is  that  few  tilings  are  easier  uf  deteetiuii  than  the  presence 
of  chicory  in  coffee  bv  meiins  of  the  niiciroscope  :  the  detection  of 
the  adulterations  of  enicory  itself  are  for  the  most  ptu't  not  more 
difficult. 

The  identification  of  chieorr  with  certainty,  either  in  the  pure 
state,  or  when  mixed  with  other  articles,  by  other  means  than  the 
microsco|>e,  is  by  no  means  easy,  if  it  be  not  impossible,  in  the  present 
Btate  of  science. 

It  has  been  repeatedly  stated  thnt  coffee  and  chiiMiry  maybe  distin- 
guished  by  the  manner  in  which  they  comport  themselves  when 
placed  on  the  surface  of  water;  the  ciiicory  powdur,  it  is  said,  soon 
(finks,  while  coffee  floats.  In  the  case  of  the  majority  of  samples  of 
chicory  examined  this  test  completely  failed,  as  the  powder  did  not 

*  On  tMrinjt  rrnnindfrl  of  thU  Rf*pnr|  hy  Mr.  Srhnli-RpM.  Mr.  QcnrftP  PlillMpi  makMlhU 
(lAtablerciilir :  —  "  Yri.  that  !•  »  fnr  back  u  IHICi.  Tho  i^et  U,  ths  aubject  b«d  not  then 
been  atuiiira  lu  rrjpirrl*  ihf  uliilieriTlr^ii  orrnffr-*"  an'l  chrory  " 

Au  that  until  rpt'fotl*,  nn  thnwIinloUin  thii«  publirl)'  ji*nv'r<t  br  Ihf^  rlilef  ■rifntlflr  ant  ho* 
t\Xy  coon^rlvd  with  th»  kxtUp,  lh«  mKcr*.  f^t  noythliiit  Oh*  Kxriic rotild  do,  ml|tht  nilul* 
tttwtr  their  coffee  and  cblcorjr  a>  much  ki  Ihrj  ]ile«>rd  !  Prrlt/  prutcctlun  <ii  the  rrrmu* 
inilf  1 

L 


14« 


CHICORT,    AND   ITS   ADULTERATIONS. 


sink,  but  rested  on  the  surface  for  a  cnnsidcrable  time,  nnd  ronlinned 
perfectly  dry, —  a  result  po-sihly  attributuble  to  the  presence  of  the 
lard  iisL'd  in  tbe  roustinjj;  of  the  niba. 

Another  way  nrcommended  lo  detect  an  admixture  of  chicory 
with  cniTee,  is  to  add  t^nwe.  of  the  flusppclc-d  powder  to  cold  water. 
If  chicory  be  prefccnf,  the  writer  will  rjuickiy  become  coloured,  and 
by  the  depth  nt"  the  cohnir  the  proportion  of  chicory  may  be  f;ucA]icd 
nt.  This  melliod  is»  however,  utterly  fallncious  since  the  colour 
may  arise  from  the  presence  of  burnt  sufrnr,  so  commonly  used,  or  of 
roii8te<l  wheat,  wirrot*  and  olhcx-  siniiliir  subatunces. 

The  Hdultenitifin  with  chicory  has  been  attemfited  to  bo  established 
by  haviitin  re^jard  t*»  tbe  relative  specific  gravities  of  inl'usinn^  uiaile 
from  ei)iml  qunntilies  of  coffee  and  chicory.  It  hns  been  found  tbrtt 
the  infusion  of  coffee  is  of  much  lighter  spccifio  gravity  than  one 
of  chicory,  the  difference  in  fact  bcin{^  about  1  to  3  ;  but  ainte 
other  sweet  roots,  as  well  as  maizo,  rye,  &c.,  yield  infusions  equally 
heavy  with  that  of  chicory,  this  test  is  useless  as  a  means  of  de- 
termminfj  the  fact  of  I  he  adultcrnlinn  of  cnfi'ee  with  cliicory.  The 
colour  of  the  infuston  and  its  specific  gravity,  doubtless  ftff"»ird  rough 
and  general  indications  as  to  wliether  any  paiticular  samples  i>f  coflee 
are  genuine  or  not,  but  it  is  imposfiible  by  thesii  characters  to  pro- 
nounce an  opinion  ns  to  the  nature  of  the  afUiltcrntion  practised. 

Tijo  difficult  V  of  dettN*iiTi|^  chicory  by  cbcinicid  moans  arises  fi*om 
the  absence  of  any  peculiar  and  distinctive  principles  in  the  roasted 
root.  Various  attempts  have  been  made  witli  the  view  to  discover 
some  characteristic  reactions  and  peculiarities  of  composition  ;  Messrs. 
Graham,  SteTdiouse»  and  Campbell  especially  have  directed  their  at- 
tention to  this  subjurt. 

These  chemists  have,  amonpst  other  points,  endeavoured  lomake  use 
of  the  colour  and  specific  gravity  of  the  diflerent  infusIauK  U!'e<l  as  a 
means  of  detecting  the  adulicrations  of  coffee  with  chicory  and  other 
roots  ;  but  these  data  are  not  capable  of  affording  any  precise  or  re- 
liable conclusion. 

They  have  also  endeavoured  to  avail  themselves  of  the  presence  of 
glucose  or  grape  sitgttr  in  chicory  ns  a  means  of  di^criminaijun  ;  thus, 
while  the  siipar  in  roasted  citflee  rarely  exceeds  I  {wr  cent.,  and  is 
usually  only  half  this  quantity,  in  roiytcd  chici»ry  it  has  been  found 
to  range  from  \\'i)fi  lo  9H6  per  cent.;  but  Mince  other  sweet  roots, 
as  beet  root,  mangold-wurzel,  turnips,  dandelion,  carrots,  and  parsnips, 
coniain  on  the  avera*;c  as  much  sugar  as  chicory,  thi»  mean^ 
utterly  fails  as  a  test  for  chicory.  The  utmost  that  can  ju^^tly  be  in- 
ferred from  the  presence  of  a  considerable  nnioonl  of  suj^ar  in  (jround 
coffee  is,  that  it  is  adulterated,  and  prohiiUy  with  one  or  other  of  the 
roots  above-named.  Further,  the  prefcetjce  of  sujjrar  in  small  quantity 
affords  no  proof  of  the  genuineness  of  coifee,  since  some  of  tlie 
cereals  and  other  substances  employed  to  adidterutecoiree  are  equally 
deficienlwitb  it  in  saccharine  matter.    Lastly,  sugar  isoften  purposely 


CHICOBT,   AND   ITS  ADULTEBATIOJJ8. 


u: 


»dde(3  to  cofTee,  aomelimps  durinni  the  roafttlngf  and  subsc^^nentlj  In 
the  form  of  burnt  sufjar  or  black  jack. 

Again,  they  hnve  nvailcd  theiiiK'Ivcs  of  the  (iimntity  of  *i/»crt  present 
in  toe  aahcit  of  coflVc  and  other  TO<:ctnb!;e  udultiiruntu  as  another 
inemJtfl of  discrimination.  The  silica  ofroaslerl  coHue  averupes  Ufunllj 
about  n  quarter  and  rarely  Hppruuijhes  one  halt"  |>er  cent.;  while, 
as  hxs  been  already  »hown,  the  sand  and  silica,  iuMilublu  in  !U-ids»  of 
four  samples  of  rnA:«tcd  chicory  aninimted  to  as  much  as  I0'6H, 
IS'lUf  lU)  71,  and  35*85  |)er  cent,  of  the  ash  :  but  in  roasted  dandelion 
root  the  proportion  of  silica  is  as  great  as  in  chicory,  jri  eat  part  of  the 
i^ilicA  in  both  I'tiscs  being  derived  from  the  dirt  Kiill  adhering  to  the  im- 
j>erfectly  cleansed  nwts.  The  same  la  the  case  with  the  rooisoCcurrotd 
and  parsnips  pre]>ared  ill  tlie  same  rough  way  for  use  as  chicory  roof, 
The  presence,  iherelore,  of  a  larj;e  excoKs  of  ailica  does  not  prove  the 
fad  of  adulteratinn  with  chicory  ;  indeed,  it  can  scarcely  be  said  to  uf- 
fonl  decisive  proof  of  adidtcration  of  any  kind,  hince  any  excess  of  silJca 
mijcLt  be  due  simply  to  the  fact  of  a  little  snnti  becnmtng  Hccident^iUy 
mixed  up  with  the  cotfee.  In  the  cereals  a^tiin,  with  the  exception  of 
maize,  the  at-h  of  which  coniaiu*!  about  2  per  cent.,  the  silica  is  high, 
OS  >hown  by  the  researches  of  Messrs.  Opslon  nnil  Way.  wlio  stale  that 
Id  wheat  the  ?iliea  varies  from  20*5  to  5-4'6  per  cent. ;  in  barley  from 
23  6  to  70*77;  in  onis  from  3848  to  5003 ;  while  in  rye  it  is  about  922. 

Lastly,  Messrs.  Graham  and  Stcnhouse  have  examined  the  f/«A  uf 
cotTee  and  chicory,  and  certain  other  adulterants,  with  a  view  to  dis- 
cover distinctive  characters.  The  principal  dtlferences  inthecomposi* 
tion  of  the  ash  are  shown  by  the  figures  givrn  below  :  — 


Silica  and  sand    - 
Carbonic  acid 
Sc^uioxide  of  iron 
Chlorine 


In  Coffee  Ahh. 

0-44  to  0*98 
0  26  to  I'll 


In  ('hlcorj  Aih. 
\0i\9  to  35-85 
1-78  to  319 
3  13  to  5  32 
3-28  to    4  1*3 


Extending  tlie  comparison  further,  however,  we  find  in  a  variety 
of  other  vegetable  substances,  even  of  those  uned  in  the  adulteration 
of  chicory  and  coffee,  an  excess  over  the  rpmnlitics  usually  contained 
ID  cofice  of  nil  the  cons^tituents  referred  to  above.  Some  of  the  sub- 
stances in  which  excess  of  silica  occurs,  have  already  been  mentioned. 
Carbonic  acid  occurs  in  nearly  the  same  pro^jortion  m  acorns,  j>ar!inip, 
beet  root,  carrot,  and  turnip,  as  in  coflee  ;  the  quantity  of  ubioriue 
approximates  to  chicory  in  aconis,  ]>&r»nip,  carrot,  turnip,  ond  dan- 
delion roots;  lastly,  the  ir\tn  h  excessive  in  dundelitm  and  beet 
root,  and  would  be  so  no  doubt  in  carrot  and  parsnip  roots  impor- 
fe*:lly  rleansed  and  freed  from  dirt.  Bcaides,  all  c(mclu«ioiis  base<l  ujwn 
an  excess  of  iron,  except  tlie  general  one  that  adulteration  with  »uuie 
substance  containing  an  excepts  of  that  metal  ha.i  been  practised,  are 
precluded  by  tlie  fart  that  cliicory  and  other  roots  employed  to  tophif- 
ticate  coflVw  are  themselves  often   adulterated  with  red  ferruginous 

L  2 


u& 


CHICORY,   AND   ITS   ADULTKnATIONS, 


n 


eartlis,  as  Venelinn  reil  and  rwUlIe,  contafning,  frequentl/,  exoena  of 
carlmnio  aciil,  limi*.  iron,  ami  pilicn. 

The  ash  of  €f>frc'e  adultcrnteij  with  ony  of  the  cerenls,  and  also  lo  a 
leas  ex(cnt  wlih  lupins,  peas,  and  bean;",  is^  ot'courife,  distinguished  by 
the  Urge  amount  (»f  phosphnrir  noid  present.  In  coffee  the  phosphoric 
acid  may  be  set  dftwii  ut  about  10  percent.;  in  chicory  it  varies 
from  6"85  lo  11*27;  in  lupins  it  is  usually  about  25  per  cent^  uiid  in 
maize  44  per  rent. 

^^'^ith  regard  to  the  nttroj^en  of  roH'ee  and  chicory,  the  autfinrs  of 
the  lEeport  under  eim>ideration  remark  ; — "Tiie  pro|>ortion  of  nilro- 
cen  ill  oofTpp  i}«,  Ihurf  ftire,  greater  thiin  in  chicory  ;  but  the  difference 
is  not  BudiiiiDiitlv  murketl  to  distiiifruish  the  two  substances  rendily 
from  each  other.  The  conclusion  may,  however,  be  drawn  that  le,^s  than 
2  percent,  of  nitrotren  in  coffee  is  a  stronj;  presumption  of  adidlfratiun.'* 

It  is  obviously  best,  therefore,  not  to  waste  time  in  the  prosecution 
of  chemionl  ineihoHs  of  research  leading  to  no  certain  results  but  at 
once  to  have  recourse  to  the  microscopti ;  by  this  instrument  ali  the 
adulterations  of  coffee  and  chicory  with  vetrclable  substances  are  dis- 
coverable with  ease  and  certainty.  In  the  case  of  chicory,  it  is  only 
neceaiary  to  ascertain  by  it  whether  those  structures  characteristic  of 
its  root  (see  _figit.  3U»  34,  an<l  35.)  are  present  or  not,  to  observe  well 
the  site  n\'  the  cells,  whether  thev  contain  starch  or  nor,  the  size  and 
character  of  the  vessels,  und  espectaUy  whetlier  tJasa  iacticentia  are 
present 

For  this  purpose,  a  grain  or  so  of  the  powder  should  be  placed  on 
a  slip  of  plass,  a  drop  or  two  <if  water  ndded,  and  the  larger  par- 
ticlc«,  which  swifll  up  iiiid  become  more  visible  tfiiiii  when  in  the  dry 
ptnte,  torn  into  pieces  by  means  of  needles.  A  Utile  ol"  t!ie  powder 
should  then  be  plflceJ  on  a  clean  slide,  covert'd  with  a  piece  af  thin 
glass,  aud  subjected  to  examination  with  the  J-or  |-inch  object- 
glasses. 

The  adulterations  of  cliicory  beinij  for  the  most  part  the  Sflme  as 
those  of  cofiee,  similur  means  must-  be  !ij»1  rocuurse  to  for  their  detec- 
tion: when  these  consist  of  ve(;otable  Bub^^ances  of  any  kind*  the 
microscope  will  be  found  *o  supply  the  only  ready  and  certain  means 
of  detection  ;  wlieii  vf  chemical  substances,  as  burnt  su^ar  or  Vene- 
tian I'ed,  chemical  methods  of  research  must  be  resorted  to.  For  a 
detailed  descriplinn  of  the  characters  of  the  variuua  substan<'cs  used 
in  the  adulteration  of  coffee  and  chicory,  and  of  the  means  for  their 
discovery,  the  reader  is  referred  lo  the  jireccdin^  ariiirle  on  Coffee. 

The  act<?ctton  of  substances  containing  Rtarch  by  ehemicai  meana  is 
attended  with  even  jrreater  dilficultles  than  in  the  case  of  coffee,  the 
blue  colour  deveiuped  on  the  uililition  of  iodine  being  obscured  by  the 
deep  brown  colour  of  the  infusion  of  chicory. 

It  may  be  thus  effected,  however :  iodine  may  be  ftp[died  to  a 
small  (piantity  of  the  article  placed  under  the  microscope,  but  in 
order  to  determine  the  Quantity  present  we  must  proceed  as  follows: 
—  A  carefully  propareti  infusion  of  the  article  ie  lo  be  made  :  this  is 


I 


I 


I 


d 


CHICOUr,    AXD   ITS   ADULTERATIONS,  149 

to  be  divided  into  two  parU :  in  one  the  sugar  is  to  be  determined 
by  Fehliii^'s  sitlution,  or  by  converting  it  into  ulcuhol ;  ilie  ruber  is  to 
bu  boiled  with  tlilute  6ulpliuric  acid  until  nil  tlie  starcli  i^  elmn;;ed 
intu  gmjic  >ugar,  tVoni  llie  ninotiiil  vt'  which  prtisent  (ileduciLn^,  of 
course,  tlie  glucose  not  tU'rived  from  the  conversion  of  the  starch)  the 
»tAreh  itself  limy  Ito  ralcutat«d. 

The  evidence  of  Uie  use  of  Reddle  and  Venetian  red  is  principally 
derived  fntin  the  incineration  of  u  certain  ijuaiuity  of  tbe  suspected 
chicory  pnwder,  and  by  unulysis  of  the  ush.  All  vegetable  sub- 
pianccri,  wliether  coloured  or  not,  yield,  un  incineration,  a  greyish- 
white  ash.  'I'he  ash  of  coloured  earthy  substances,  on  the  contrary, 
after  being  burned  in  a  crucibh',  remains  mure  nr  less  coloured. 

As,  however,  chicory  >»  the  root  of  a  plant,  and  as  the  eai-ihy  matter 
is  but  tteldom  entirely  removed  from  it  by  wnshing,  the  ayh  of  even 
jrenuine  chicorv  noi  unfrequenlly  exhibit.^  on  this  account,  a  slight 
decree  of  colnuratiun,  being  occajtionaily  brownish,  or  of  light-fawn 
colour.  It  is  only,  therefore*  when  the  ash  is  decidedly  coloured^  and 
espeeiAlly  when  nf  a  red  or  rusty-red  colour,  ihat  the  presence  of 
Venetian  I'ed,  reddle,  or  suuie  other  analogous  substajice,  la  reuUered. 
certain. 

In  these  facts,  therefore,  we  have  a  retidy  nietins  of  determining 
whether  a  sample  of  chicory,  or  any  other  Vfgetable  powder,  contains 
an  vlwixture  of  any  mineral  colouring  matter  o<intaiiiing  iron,  a  con- 
clusion which  may  be  further  couBrmed  by  chemical  analysis. 

Oh  the  Quuntitaiive  Estimation  of  Setquitmde  of  Iron  in  Chicory. 

Aitiiough  the  presence  of  iron  is  sufficiently  indieatetl  bv  the  colour 
of  the  aali  of  chicory,  and  most  (»ther  vegetable  substances,  yet  iu  some 
caM**  it  bec*omes  necessary  to  deteriuiuc  its  amount. 

For  this  purpose,  the  ai>h  (say  of  .'300  grains  of  chicory)  should  be 
boiled  with  dilute  hydrochloric  acid  until  all  the  iron  has  become 
dissnlved,  the  acid  evaporated  nearly  to  dryness,  about  an  oum'c  of 
distilled  water  added,  the  Milulion  filtered,  nnd  the  iron  precipitated  as 
se8<{ui<ixide  by  meamiof  f»olntion  of  ommoniu,  the  precipitate  collected^ 
wa>hed  with  hot  water,  ignitcJ,  «nil  weighcil. 

Thin  proce.vt  is  npplicjible  otdy,  however,  in  the  absence  of  earthy 
phosphates  t>r  uluminu,  a»  these  are  atw  precipitated  by  aiumouia. 

The  alkaline  carth»  may  !«,•  diesolvcd  out  of  tiie  atumoiiia  precipi- 
tate by  means  of  an  exceedingly  dilute  solution  of  hyilrocldoric  acid. 
This  will  not  ufTect  luateriully  either  the  iron  or  the  alumina.  By  ft 
Bolution  of  nitric  acid,  I  part  to  30  or  40  of  water,  the  iron  aUo,  if  in 
small  ipiantity,  may  be  separated  from  the  alumina. 

Hy  the  fbllowiog  process  the  scsquioxidc  of  iron  may  be  separated 
from  the  alkaline  earths,  alumina,  lime,  and  magnesia  :  — 

The  ignited  and  weighed  residue  is  to  bo  diMoIvL'd  bv  digestion  with 
conuentrated  hydrochloric  acid,  or  by  fusion  with  bisulpbate  of  jKitassa. 

L  3 


CHICORT,    AND    ITS  ADULTERATIONS. 


ISO 


Boil  the  solution  first  with  «nme  sulpliatc  of  snda,  and  tlien  with  soKi- 
tii^iL  of  ttoilii.  witic'b  will  luko  up  the  iilumiiiii.  Wftsli  the  reMitluo 
thorough] V,  (1is<«ilve  it  in  hyilroithloric  aciil,  precipitate  tbesesquioxide 
of  iron,  obaerviiii;  the  iiefessnr^r  profJiutians,  with  sueciuate  of  am- 
ininiiii. 

Or  the  iron  may  be  prtcipiiated  by  sulphide  r>f  ammonium. 

Mix  with  the  ac"i  solution  ammonia,  until  a  precipitate  just  be^ns 
to  form,  ilien  with  siilpliide  of  anim<iaiiini  ;  si^[i.irate  the  precipitate 
which  rontains  iron»  also  iiiunf;anpse,  shoiilJ  that  nict;il  be  present,  by 
filtrntion  ;  dissolve  it  in  hyilrotrhloric  acid,  and  separate  the  iron  from 
the  manganese,  if  any*  by  siiciMnale  of  ammonia.  If  there  is  no  reaaim 
to  suspect  the  pro^t^nce  of  nminL'nneK*  the  precipitation  with  succinate 
of  ammonia  may  bi^  miiitled.  I'he  aluminu  Hiid  the  earthy  phosphates 
are  in  the  HItnite ;  hut  if  too  much  ammonia  is  added,  they  too  would 
in  part  he  thrown  dfiwn. 

The  succinate  of  ammonia  is  nscd  in  the  following  manner:  — A  very 
dilute  liolurion  of  anunortia  is  addi-tl  ilrop  by  dri>p  ti>  the  sohitiun  con- 
taining the  iron,  until  a  small  portion  of  the  mL^tal  precipitates  in  lh« 
furmof  hydnitedsesfjiiioxicle  :  a  jrentle  heat  istliennpniicd  to  aseertain 
whether  the  nrecipitiile  will  re<il?5iilve  or  nnt ;  if  it  u>ies  so,  nmream- 
nioiiiu  iH  added,  until  the  application  of  heat  fails  to  dissolve  the 
precipitule  farmed.  If,  on  the  cnrilrnry,  it  r«rouJns  undissolved,  and 
the  fluid  continu*'s  to  br  nf  a  brownish-red  colour,  all  the  conilitions 
requisite  are  Inllillyd.  Itut  shnuhl  the  fiuid  be  c^>I^lU^le^s,  tno  much 
amnnmia  Iuh  liecn  nddml,  tn  whteh  ease  a  small  qunntlrv  of  hydro- 
chloric  acid  must  be  adde-rl,  and  then,  a;^ain,  nioni  ainnionio,  until 
the  point  desired  is  obtained.  A  perfectly  neutral  rinUition  ofsuci-inate 
of  ammonia  is  now  to  bp  iiddc<l  so  Ion;;  as  any  preeipitate  falU  ;  a 
gentle  heat  is  then  applied,  the  fluid  Is  afterwanU  allowed  to  cool,  and 
when  rnld  it,  \n  filtered,  the  pi-eeipitute  washed  on  a  filter,  first  with 
cold  water,  aiit)  nt'i.^rwjirds  wiili  hot  solutiuu  of  aiuuuHiia;  it  Js  then 
dried  and  ignitvil  thoruu<;hly  until  it  is  all  converted  into  sesquioxlde. 

The  eases,  then,  nf  coflec  and  chicory  afford  striktn;;  illustrations  of 
what  can  be  ejected  in  the  discovery  of  adulteration  by  means  of  the 
micriiH'Ope. 

Tlie  article  nn  Chicory  may  be  concluded  by  a  review  of  reasons 
tirj^ed  both  for  and  a^;iinst  the  admixture  of  chicory  with  coflfee 
taken  from  the  author's  bi>ok  entitled  "Food  and  its  Adulterations." 
Some  of  the  remarks  contained  in  this  review,  requin*  to  be  moililioil 
to  eome  extent  in  eonsequence  of  the  alteration  wliit'h  has  taken  place 
in  the  law  since  the  review  was  drawn  up,  by  which  it  is  required 
that  chicory  should  not  be  sold  mixed  with  cofiw,  excei>t  the  fart  of 
such  mixture  is  specified  by  a  tube).  Thi»  law  in,  however,  con?tantly 
evaded:  the  mixture  is  sometimes  stild  without  the  label;  in  other 
cases  it  is  palmed  off  where  coffee  only  in  nsked  for  ;  aotl  lastiVf  in  aoiue 
icslances  the  so-called  mixture  consists  almost  entirely  of  chicory 


I 


d 


CHICORY,   AND   ITS  APULTEHATIONS. 


51 


Review  of  Jteasons  urged  both  For  and  Against  the  Admixture  of 
Chicory  with  Cofft^r. 

Various  reasons  have  been  urged  hoth  in  favour  of  and  a^inst  the 
"ndulteralion,"  nr,  as  the  Cbuncellor  more  gently  phraaea  it,  the 
"  mixing  "  of  chicory  with  coffee* :  these  we  will  next  proceed  to  con- 
sidtfr. 

Jfi  favour  of  the  adulteration  it  i»  a[lc;;pd, — 

First,  that  the  admixture  of  chicory  with  coffee  improves  coffee^  and 
thftt  such  addition  in  approved  by  the  public. 

In  order  to  nscertjiin  whether  ihe  mldition  of  chicorjr  to  coffee  be 
really  an  iinprovt'nicnt,  wc  prepared  three  infusions,  one  of  coffee, 
another  of  chicory,  and  rhc  third  of  botli  these  mixed  in  the  propor- 
tion of  three-fourths  coffee  and  nne-fcmrlh  chieory. 

The  infvsion  of  ciffee  wns  perfectly  trnnsparent,  and  of  a  dark  and 
rich  brown  colour;  it  emilted  an  od^mr  in  m  high  degree  penetrating 
and  refreshing,  \\iv\  to  the  ta«te  it  w:ia  agreeable,  and  rather  bitter. 

Having  been  taken  for  a  few  minuter,  it  produced  a  feeling  of  ge- 
neral wnriiuh,  and  a  state  of  bodily  and  mental  activity  and  invigora- 
tion. 

The  infusion  of  chicory  was  opaque,  staining  the  sides  of  the  vessel 
containing  it;  it  |KWse*tfed  a  nenvy,  thoutih  ncrhiips  some  persons 
might  be  of  opinion  not  a  disagreeable  smell,  wholly  unlike,  ho^vever, 
the  vohtllle  and  diffusive  odour  of  ci»ffee;  in  taste  it  was  more  bitter 
than  the  coQee  infusion,  wiih  a  certain  degree  of  sweetness. 

Having  been  swallowed  for  a  few  minuies,  it  occasioned  a  feeling  of 
weight  itt  the  »tomach,  and  a  general  heaviness  and  iudispositiou  to 
botlily  and  mental  exertion. 

The  combined  infusion  of  chicory  and  coffee  partook,  to  some  ex- 
tent, of  the  characters  f^^  the  infusion  of  genuine  coffee,  as  might  be 
snticipatfd  from  the  coffee  \i  cont&ined. 

Altogether,  we  were  unable  to  bring  ourselves  to  believe  that  the 
addition  of  chicory  to  cofffe  in  the  projwrtion  of  twenty. five  percent. 
of  the  lonner  was  any  improvement ;  on  the  contrary,  we  were  satistietl 
that  the  quality  of  the  brverage  was  greatly  imjiairt'd  by  the  addition. 

I'ersons  who  are  foolish  enoujih  to  regard  a  slight  sensation  of 
wei;;hl  and  fulness  in  tlio  region  of  the  stomach —symptoms  really  of 
incipient  indigestion  —  as  evidences  of  the  beverage  being  iMissessed  of 
incieAsed  "  strength"  and  "  b()dy,"  and  whose  nasul  organs  are  insen- 
sible to  the  delightful  aronia  of  coffee,  wight  |Kissibly  be  brought  to 
consider  the  atlditton  an  improvement. 

In  contrasting  the  pn»pertie«  of  chicory  and  coffee,  we  woubl 
once  more  observe  it  must  not  bo  forgotten  thut  the  former  article 
it*  wholly  destitute  of  that  i>eculiar  priticlpk'  '"  caffeine ^'' Xi\>ox\  which 
the  virtues  of  coffee  in  part  uepend.  and  that  iherelbre  for  every  ounce 

i.  4 


isa 


CHICORT,   AND   ITS   ADULTERATIONS, 


of  chicory  in  a  pound  of  coffee  there  is  so  niucb  ihc  less  of  thut  atima- 
tutin^  and  invigorating  iiitrogenised  product. 

AlLiiwing,  however,  fur  th«  sake  of  arij[UTnent,  that  the  admixture  of 
chicory  in  moderate  propoi-tions  is  in  the  ojjini^jji  of  poirit;  pergon!*  an 
improvementf  it  is  very  cortain  that  by  others  it  i^  n»t  coii*iciered  to 
be  sa;  ftiid  auch,  tliercfore,  ought  surely  to  be  nUintJrd  o  choice,  and 
not  be  compelled,  as  they  frequently  are,  to  drink  chicory  ftllhough 
they  dislike  it. 

But  the  udinixture  of  chicory  with  coift'c  in  the  proportion  of 
twenty-five  per  cent.,  tbu  ulrnnsft  that  cnn  be  uMowed  by  any  person 
to  eoiiiftitut^  an  improvLnueot,  doea  ni>t  in  general  tsatisfy  tlie  desire 
for  profit  on  ilie  ptuL  of  the  grocer ;  he  use?*,  in  most  cases,  a  very 
much  larger  pri>porti(in  of  chicory  thiin  thi.*,  and  the  shilling  coffee, 
**the  p*ior  mnn*s  beverage"  contains  onc-hulf  or  tliree-finirlh*  chicory, 
and  in  some  inatances  consi^tts  entirely  of  it.  Now  no  truthful  JM-Tson 
will  OBsert  thut  chicory  in  thc6e,  the  more  common  projiortions,  is  aa 
iniprovement  to  coffee. 

Second,  that  th^  »wtf  nf  chicory  increaxex  (he  consumption  of  coffee. 

This  stateinenL,  ultliou^h  recently  put  fortli  by  no  leas  an  authority 
than  A  late  ChflnL-ellor  of  the  Exrhe*iuer,  is  ju.*!  the  very  reverse  of  the 
truth*  which  is,  that  tlie  use  of  chiciry  diminishes  tiie  consumption  of 
coffee.  This  we  have  already  clearly  j)rnved,  and  it  is  not  necessary 
that  we  discuss  tliis  {xnnt  again.     It  \it  settled. 

Third,  that  the  poor  uian,  bif  the  empioj/ment  of  chicory,  hat  an  arHcle 
placed  within  his  reach  which  othtrrwue  he  could  not  obtain. 

This  argument,  although  f!f>eciDu«f  i.s  utterly  fallacious. 

Cienuine  coffee,  ground,  or  in  the  berry,  may  now  be  obtained  at 
numerous  reop'-uiableeAtablishmenis,  at  \s.  'Id,  and  I».  -ki.  per  [Mumd, 
this  article  costing  the  grucer  more  than  tUree-founhs  of  the  sum  he 
deinamli  for  it. 

The  mixture  of  chicory  is  never  sold  under  I*,  per  lb.,  and  the  cost 
of  chicory  lo  tlie  grocer  very  frequently  does  not  exceed  '<id.  a  pound, 

Which  of  these  two  articles,  therefore,  we  ask,  is  the  beiU  poor 
mans  bargain  f 

Shilling  coffee,  u  vended  at  the  present,  is  vile  and  often  deleterious 
rubbish,  and  we  recommend  the  poor  man  never  lo  purchase  it. 

W«  say,  therefore,  so  far  from  the  pnor  man  being  beneliteil  by 
the  use  of  chicory,  that  out  of  every  shilling  he  spends  in  what  is 
ral.«ely  denominated  coffee,  he  is  frequently  robbed  oI'Dr/. 

We  can  well  understand  how  the  [xtor  man  or  the  pnor  man's  wife, 
having,  on  a  Sftturrtay  night,  only  u  few  shillings  to  spend,  and 
desiring  to  make  thpse  go  a*  far  as  jKwsiMe,  is  judui-ed  to  purchase  ihe 
chea|)cst  articles  he  or  she  can  procure,  overlooking  the  fact,  that, 
uUhough  jjrofessedly  the  cheapest,  they  are  often  in  reality  the  dearest 
in  the  end. 

We  wish  the  poor  man,  therefore,  clearly  to  understand,  that 
chicory  is  not  to  be  compared  to  coffee  in  any  respect,  and  we  would 


\ 


\ 


CHICOKT,   AND   ITS  ADDLTERATIONS. 


153 


have  him  nvoid  t}ie  "r-lienp  and  rutting  shnpn/*  distinrruiithed  hy  large 
placards  and  huge  piles  or  damaged  goods,  nnd  buy  his  cntVee  at  some 
Louse  of  known  and  acknowledgt'd  reputation  and  recpectability. 

Apprehensive  tliiit  Gdvernmeiit  will  he  forced  to  take  notice  of  the 
BCandaloits  practiced  now  »o  rifu  in  ihe  article  coffee^  ibe  ailiilterating 
grofers  have  already  begun  to  raise  ihe  cry  of  "  dear  coffet?,"  and  they 
tell  u«,  that  if  the  admixture  of  chicory  with  cofice  be  piohibited,  the 
price  of  the  latter  article  will  be  2t.  the  pnumi. 

The  answer  to  this  statement  is,  that  exi-ellent  genuine  cnfffe  may 
now  be  obuiined,  at  ODtabli.Hbnients  which  do  not  tifie  chiL-ory  in  their 
business  at  all,  at  prices  varying  from  1/r.  'Id  to  Iji.  tif/.  per  pound. 

Fuurtli,  that  the  iaw  sanc^ionn  tftf  aiiuUcration  of  coffee  with  f/riVory, 
and  therefore  that  the  grocer,  in  mixing  these  articles,  is  guilty  of  no 
fraud. 

As  the  law  at  present  stands^  it  must  be  conceded,  we  are  sorry  to 
«y,  thiit  in  mixing  diicory  with  c<iflee  the  grocer  does  not  violate  the 
law,  but  only  does  that  which  the  executive  and  its  cinicers,  to  ihcir 
shame  be  it  ^aid,  not  nhme  i<nnction,  but  arltinlly  reL-ommeiid. 

We  hdld,  however,  that  in  vending  nn  article  as  cortc*^  which  is  not 
coffee,  the  grocer  is  guilty  of  a  moral  fraud,  and  tlmt  which  iH  morally 
wrong  no  act  of  parliament  aud  no  ministers  cnn  make  niornlly  right. 

Firlk,  and  tnstly,  it  is  alleged  that  i  here  is  no  necetisity  for  legishiiive 
ioterlereuce,  since,  bt/  buyiug  the  affee  berrie*  iu  the  whole  atatey  the 
pubUii  can  protect  Uxelf, 

Thofte  who  use  this  argument  cannot  but  be  aware  how  inefficient, 
prai'ticidly,  is  the  protection  here  referred  tit. 

The  poor  man  has  not  the  money  wherewith  to  purchase  a  mill; 
and  if  he  ha<I,  working  early  nnd  late,  riiting  at  six  In  the  morning,  and 
going  to  bed  late  at  uight,  what  time  ur  spirit  has  he  to  attend  to  such 
niatcerfl  ? 

Again  :  others  not  so  poor,  and  who  are  in  a  position  to  moke  the 
necessary  purchase,  arc  perhaps  equally  engagetl,  or  ignorant  of  the 
extent  to  which  they  are  cheated. 

Even  of  (hose  who  have  both  money  and  leisure  we  nffirm  that  not 
one  in  twenty  avaiU  himself  of  the  protection  whitli  the  purchiiseof 
the  whole  berry  uflurdit ;  nor,  since  he  pays  a  fair  price  for  an  article 
which  be  specifics,  ought  be  to  be  called  uprm  to  adopt  measures  of 
extraordinary  precaution  against  fraud. 

We  are  not  dis]>osed,  however,  to  underrate  the  value  of  this  means 
of  prolectiun,  and  we  have  pleasure  in  stating  tliat  elUcieut  coffee 
mills  muy  be  prucureil  at  a  trilling  cost. 

We  put  it  to  coffee  merchants  and  respectable  dealers  whether  it  be 
not  advisable  tliut  they  should  themselves  take  some  steps  to  supply 
the  public  with  cheap  and  effective  coffee  mills. 

Wc  have  now  to  consider  the  chief  arguments  wliich  have  becaor 
may  be  advanced  against  the  adulteruliou  uf  coffee  with  chicuiy. 


a 


154 


CHfCORT,   AND  ITS  ADULTERATIOX8. 


W 


As*iingt  this  pmetiee  we  allege, 

Firat :  thnt  surh  adulteration  nece»sitate»  the  commiimon  of  a  moral 
/rami,  anil  further,  that  it  is  irequentl^  made  the  cloak  for  pccaDiarj 
i'ratid  and  extoruon. 

WJit'ii  lipurcliaser  enters  a  shop,  asks  for  an  article,  pays  thepriee 
demanded  jor  it,  he  hiis  a  ri^ht  tu  expect,  tliab  he  Miall  ubtain  that  for 
■wlucli  lie  a^k*,  and  not  u  mixture  of  twu  (iifVeront  tliinjis,  one  of  which 
111*  probably  ptisittvcly  object-s  lo,  and  the  rclatire  proporfions  of 
which  iini  ri'ijidrtttd  bv  the  will  ami  conscience  of  l)ie  vendor.  The 
grocer  who,  undfr  such  i  irrtimjita.m'es,  plrtcci  in  the  liiinrln  of  rbe  pur- 
chaser an  adulrcratcd  conimodiiVi  commit£  a  moral,  and  freijucntly  a 
pecuniarv  frnud. 

We  will  suppose  the  fuUowinjr  onse  of  poisoning,  not  an  improbable  or 
unfretjucMit  onj  :  —  An  infunt  has  been  given  an  overdose  ol  Godfrey*! 
corilial ;  the  proj>er  reniefly  i.**  n  ^Iroiiff  infusion  of  cofiee  —  liie  cof" 
already  in  iLe  house,  inismucb  as  h  is  the  most  ipiii-kly  obtained,  is 
used;  it  confti-ta  prini'i[)(»llv  or  perhaps  entirety  of  chicory.  TTte 
chiid  dies.     Who  is  the  party  morally  responsible  in  this  cose  ? 

Second  :  that  it  is  unjust  to  the  grower  K\i  cc\?^iiit. 

The  jrrower  of  coffee  has  at  least  a  right  to  demand,  in  consideration 
of  llje  heavy  tax  which  he  pays  for  the  privilege  of  bein^  permitted  to 
iaiix>rt  his  eoflee  into  ETt^Uiiid  for  diHpuf^u],  that  the  sale  ot  the  article, 
and  its  estimation  with  the  jnddic^  be  not  injured  by  the  practice  of 
adulteration,  carried  on  midur  the  sanction,  and  with  the  connivance, 
of  the  legislature,  and  even  uoiler  the  very  name  of  coffee. 

The  payers  of  duty  on  other  excisable  articles  are  prtttected  against 
adtdteratioji  by  Inw^  and  the  coflee  ^^rowcr  has  a  full  right  to  demand, 
incotninon  honesty,  the  some  umotint  of  protection. 

Third  :  that  the  revenue  is  injured. 

Whatever  lesi^ens  ibe  consumption  of  on  excisable  orticle,  of  cnume 
iDJureti  the  revenue.  It  has  been  proved  that  the  uiixlnn;  of  chicory 
with  cotTee  lessens  the  consuin|itioii  of  coffee,  and  therefore,  by  so 
much  is  the  revenue  diminishetl  and  injured. 

If  the  Iffiw  in  revenue  were  so  much  gain  to  the  public,  there  would 
be  less  reason  to  complain,  but  this  is  not  the  case ;  the  advantage 
is  pocketed  by  unprincipled  pn)rers. 

Ffitirth  :  thai  the  public  is  defrauded. 

That  the  public,  and  especially  that  lar^  section  of  it,  the  poor,  U 
exteni»ively  defrauded  by  liie  atlulteration  of  coffee  with  chicory,  to 
»ay  nothin*;;  of  roasted  curn,  beans,  dog  biscuits,  &c.,  has  already  been 
cleorlv  proved.  Let  those  who  entertain  any  doubts  upon  the  subject 
con-tnit  the  Table  of  Analyses  which  we  gave  in  (>ur  Keport  i>n  CotTee. 

We  have  now  clearly  shown  thai  the  disa<lvttnlages  and  evils  re- 
sulting from  the  mixture  of  chicory  with  coifee,  in  the  manner  and  to 
the  extent  now  practised,  arc  preal  nnd  manifold,  and  ttat  Ihey  de- 
mand the  application  of  a  suitable  remedy. 

The  remedy  which  we  propose  is  simple}  moderate,  and  just :  it  isp 


COCOA,   AND  ITS  ADULTERATIONS,  155 

that  the  "Ti-ewury  minute,"  aiutlinrisiDr;  the  mixture  of  chicory  with 
coffee,  be  resciudyiJ.  The  effect  oi'  tlus  would  be,  to  place  colTee  upon 
the  same  fuotin*;  with  hU  other  excisuble  articles,  as  tea,  pepper,  &c., 
and  that  penulties  would  attach  to  its  adultenition. 

Chicory  would  of  ciHirse  still  be  snhJ ;  but  in  place  of  belnpr  so  olan- 
deatinelv.  It  would  be  vended  op<'nly,  and  under  ha  pnijKT  name,  and 
ai  its  fair  value. 

Public  morality,  the  interests  of  the  revenue,  of  the  grower,  the 
convuincr  of  cuOee,  and  of  the  honest  tradesman  alike  require  the 
adoptiun  of  the  remedy  here  puinteil  out. 

'ibe  law,  as  we  arc  all  awitre,  nanctiuna  the  adulteration  of  cnffce 
with  chicory,  to  the  injury  of  the  levenue,  and  the  loss  of  the 
public  in  health  and  pocket.  Thi^i  f,tkm*^.  Uw,  however,  does  not 
]M*nnit  the  adulteration  of  coffee  with  at^orchcd  wheat,  beans,  carrots, 
&c.,  but  subjects  parties  practising  these  deceptions  to  prosecution, 
And,  in  caae  of  convictiim,  heavy  penalties.  Sueli.  at  feast,  is  the 
law,  but  under  the  present  government  it  U  uselcsji  law,  itince, 
itutwitbHtanding  the  prevalence  of  these  adulterations,  it  is  rarely 
enforced. 

lint,  singular  to  say,  the  law,  while  it  provides  in  word  against 
certain  of  the  adulterations  to  wUicli  cuffee  is  liable,  is  silent  with 
respect  to  the  adulteration  of  cliicory ;  so  rliat  that  which  is  an 
offence  in  the  case  of  colfec,  is  not  illegal  in  that,  uf  chicurvt  with 
which  the  manufacturers  may  mix  corn,  beunt<,  carrocs,  mangold- 
wurzel,  moliogany  sawdust,  &c. :  tbis,  lo  say  the  least,  is  grossly  incou- 
listenL 

Raw  or  kiln-dried  chicory  it  free  of  duty.  Roasted  or  ground  Sd. 
per  pound  at  present,  but  from  5tli  April  18.57.  4f/.  per  pound. 

The  quantities  imported  can  only  be  learned  by  an  application  to 
the  Board  of  Trade. 


COCOA,  AND  ITS  ADULTERATIONS. 

Catoa  is  prepared  from  the  seeds  of  Theobrtnna  Cuceio,  so  named  by 
Linnieus  from  the  Greek  word  ^/di*,  God,  and  iiftutfiay  food,  signifying 
that  cocoa  was  a  food  fit  for  the  gods. 

It  ia  a  small  but  handsome  tree,  indigenous  to  the  West  Indies  and 
Central  America.  *' It  grows  spontaneously  in  Mexico  and  on  the 
coast  of  Ciiracois,  and  forms  whole  forests  in  Demarara.  It  is  culti- 
vated also  in  the  Mauritius  and  in  the  French  island  of  Boiu-bon." — 

The  seeds  or  beans  are  enclosed  in  a  pod  or  fruit  somewhat 
like  that  of  a  cucumber,  being  usually  about  five  inchea  longi  and 


COCOA,   AND   ITS  ADULTERATIONS. 

three  And  a  hull*  in  ilianieter.  Each  fruit  contains  in  penornl  from 
twenljf  to  tliii'ty  beans,  tUsposeJ  in  five  rows,  which  are  diviik'tl 
frotii  cneh  olhor  bv  partili'ins.  Occupying  ihe  ilivisiiiim  <tt*  ihe  Iruil 
um\  surroumliii;;  ihc  ^i^cdi  is  a  roitv-culoureil  spon^'y  substuiicv*  re- 
temhling  thiu  of  WHter-inulons. 

The  above  description  applies  to  fruits  of  nvenige  sizy :  snuietimea 
llie  fruits  are  so  Urge,  esput^iallj'  thost'  grown  in  Central  America, 
ih:tt  they  contain  us  many  as  from  forty  to  firtr  aeetln ;  while 
others,  an  those  urown  in  the  Wect  Indian  Island:*,  Berhiee,  and  De- 
merara,  are  mm-h  smaller,  ami  i-nclo^  only  from  »ix  to  fifteen  seeds. 

During  ninturafiou  ilie  fniiLs  chau;fe  from  <;reen  to  dark  yellow; 
they  are  then  phu-kcil,  u[>i':iied,  (lie  seeds  cleared  of  the  spuitgy 
eubstHuce,  and  spread  out  lu  dry  in  the  air. 

Ill  tlie  West  Indies,  imniedialely  that  they  tire  dried,  the  beans 
»*&  packed  uj»  and  arc  ready  f*»r  the  market;  but  in  the  Caraeeas 
they  ure  subjected  to  slight  fermentation  :  fur  this  ptirp»i»e  they 
ore  either  put  into  cheMs  nr  tub:!,  whieh  are  covered  over  with 
Iward^,  the  beamt  beinp;  turned  over  evt^ry  morning  to  C(]ua1isc  the 
fornientution,  ur  else  tiiey  are  put  into  pita  or  tienL-hcs  duj;  in  the 
earth.    Lajitly,  they  are  exported  to  the  sun  and  dried. 

Uurinji  the  pnn-CM  the  beans  emit  a  good  deal  of  lUoiaturCf  lose 
weight,  as  well  Hi  part  of  tlieir  bitterness  and  acrimony. 

The  seeds  whiih  hiive  ninlerjrone  the  process  of  fermentation  are 
considered  the  besti  they  are  larjrer,  of  u  darker  brown  coluur,  and 
after  roasting,  throw  olT  their  husksi  readily,  and  «plib  easily  into 
several  pieeeii  or  lobes.  They  have  an  agreeable  ntildiy  bitter  tast«, 
without  acrimony. 

The  beans  of  Guiana  iind  West  India  cocoa,  while  ihey  are 
smaller,  llatter,  smootlier,  And  of  a  lif^hter  colour,  are  also  more  ^harp 
and  bitter  to  the  (aste.  "  They  answer  best  for  the  extraction  of  the 
butter  of  cacao,  but  utfurd  a  lesa  aromatic  and  agreeable  chocolate.'* 
—  f/re. 

Johnston  slates  (hat  the  bitterness  and  acrimony  of  (Astc  **■  is  greater 
in  the  heum)  of  ilit.*  niHinUnd  than  in  thuAe  of  the  American  Islanfls. 
The  cocoa  of  Central  America  is  however  of  superior  tpiality,  or  at 
least  if*  more  generally  enteenied  in  the  Ktiropejui  markela  than  that 
which  is  grown  in  the  West  Indies.  It  still  reijuns  a  (;realer  dej»rce 
of  biiicrness,  and  this  may  be  one  reason  for  the  prel'erence  given 
to  il. 

" 'Tlie  cocoa  of  Trinidad  is  the  variety  chiefly  consumed  in  this 
country.  The  i|ualitv  of  the  mainland  cocoas  which  come  to  the 
Knglisii  market  trum  liahia  and  Guayaquil,  fur  example,  has  hitherto 
been  always  interior." 

The  reason  of  this  is,  that  until  recently  the  duly  on  foreign  cocoa 
was  greater  than  that  on  colonial  cocoa^  beinji^  in  the  one  case  2d. 
per  pound,  and  in  the  other  \iL  and  5  per  cent.  This  had  the  effect 
of  excluding   all  the  foreign   cucoas    of   better   quality  and   liigher 


i 


COCOA,  AND  ITS   ADULTERATIONS.  157 

Frice,  which  found  their  way  to  Morocco,  Francis  Spain,  and 
tnly.  Now  thnt  the  duty  is  equalised,  it  may  be  expccljed  that  the 
finer  kinds  of  foreign  cocoa  will  find  their  way  into  the  Knglish 
market. 

Previoiia  to  being  useil,  the  beans  nre  masted  in  an  apparatus 
similar  to  thnt  of  a  eoHce  roaster.  When  tlic  urnma  is  well  (iiJvelo|K'd 
the  roasting  is  known  to  be  finished.  The  heims  are  turned  uut, 
cuoled,  and  freed  by  faiininff  ami  siflint;  from  tlicir  liiisks. 

Ox-on  has  been  in  use  in  Mexico  from  time  imirifmorinl.  It  wjw 
introduced  into  Europe  by  the  Spaniards  in  lo'iO,  and  by  them  it  was 
long  kept  a  secret  from  Uie  re»t  uf  the  world. 

Composition  af  Coam. 

The  followinft  is  the  cmnpusition,  flcconling  tn  Lanipodin?,  of  iOO 
parts  of  the  seed.i  of  West  Indian  cocoa  deprived  of  husk  : — 

Fatty  mntter     -----    5310 
Albuminous  brown  matter,  containing  the  aroma 
of  I  lie  bean    .  -  -  -  - 

Starch  ..... 

Gum     -.-.-- 
Lignine  .  .  •  •  - 

Ited  pigment     -  .  .  -  - 

Water  ---.-- 
Loss     ..--.- 

100-00  parts. 

This  annlysis  entirely  nreilooks  some  of  the  more  important  con- 
Btituents  of'  cocoa,  as  the  volatile  aromatic  oiV,  tJte  theohromttw  nnalogous 
to  the  theine  of  tea,  and  the  hitter  aw!  astringent  principle.  The  pro- 
poriion  of  starch  appears  also  to  be  somewhat  unueTraied. 

Tlie  average  cumpibiLion  of  the  entire  buaii  when  deprived  of  its 
husk,  is,  according  to  Johnston,  nearly  as  follows  :  — 

Water           -  -  -  -  5 

Starcli,  gum,  &c.  •  -  -  22 

Gluten,  &c.  -  -  -  -  20 

Oil  (ci)coa  butler)  -  -  -  51 

'I*hcubromiue  -  -  -  2 

100* 

Cocoa,  then,  rontjilns  s  great  variety  of  important  nutritive  prin- 
ciples; OS,  in  addition  to  the  vohitile  oil,  the  iheobromiiie,  snu  the 
bitter  principle,  gum,  starch,  much  fut  and  gluten :  like  milk,  it  con- 

•  Otiirr  analjriM  of  cucoa  «re  (Iven  by  M.  VA)tn  In  till  iii>ik  entltl«d  "  Uei  SubMancM 
Allfiiirnlairei." 


tss 


COCOA,   AND   ITS   ADnLTERATIONS. 


tains  ever^  ingredient  necessary  to  tbe  growth  snd  sustenance  of  toe 
bodf. 

I'he  volatile  oil  is  developed  during  the  process  of  ronstmf;  t  it  is  to 
it  that  the  aroma  is  due,  and  whioli  is  so  powerful,  when  the  coc-oa  U 
first  ro.i'tteil.  Its  action  on  the  system  is  probably  simitar  lo  the  cor- 
respondio'T  otI^  of  tea  titid  crpffet',  uUUough  less  considerable,  since  the 
quantity  of  this  nil  in  eneoa  is  but  small. 

l^h^obromiite,  like  theineit  \s  a  while  crjstallisable  faibstancCf  but 
diil-.TS  from  it  in  ronlainin^  a  much  larpcr  proportion  of  nitro^ren. 
The  pro|inrtion  of  this  siihstnnce  is  usually  about  the  sjinic  n^  in  tea, 
nftnieiy  2  per  cent.  It  exists  also  In  smnller  quantity  in  th«  busk  of 
the  bean. 

The  hitter  aiul  astringent  priaciplex  are  probably  distinct :  the 
hitttTne>»  is  j^realer  than  that  of  coffee,  but  the  astrtngtincy  less  than 
in  f'ither  tea  or  coflee. 

The  concrete  fat  or  oil  is  the  predominant  in^erlient  in  cocoa, 
forminj;  over  one  half  the  weight.  In  its  presence  ooetm  differs  re- 
niurkidily  from  tea  jm«l  coffee, 

Tliis  fntty  oil,  H;rmetl  butter  of  cocoa,  ta  of  the  consi«t«nc«  of 
tftlluw,  molting  only  at  ]'i*2^  Fahr.  It  is  white,  of  a  mild  and  agreeable 
flflviiur,  anil  is  nnt  apt  to  turn  rancid.  It  is  soluble  in  boiling 
a1oolu>l,  from  which  it  is  nrecipilnted  as  the  spirit  bectmics  enlil.  To 
obtain  it  in  quantity,  the  beana,  ofter  havln*;  l>ccn  steamed  ami  sonkeil 
in  boilinjr  water  for  some  time,  ure  stibjected  lo  strong  pressure  in 
canras  bags.  The  proportion  of  butter  procured  by  this  method  is 
fVom  five  (o  hjx  ounces  to  a  pnund  nfeiH'oa,  some  of  the  oil  remain- 
ing bebitid  in  the  beans.  It  posse^He^i  u  re^hlisih  tinge  when  &r>t 
expresBC*!,  bul  it  bei.'omcd  while  by  b4itUngwiih  water. 

Ci>coa  likewi}(e  differ:*  remarknblv  frtirti  tea  and  cocoa  in  contaimns! 
a  considerable  amount  of  jr/»rcA,  an  im]>ortnnt  constitui-nt  in  nearly  alt 
the  more  vulunbli*  vegetable  articles  of  food. 

Ln-'tly,  it  cotitains  a  very  large  atimunt  of  gluten^  uBually  about  !20 
cent. 

The  ifheU4  or  AiuAjr,  which  form  about  12  per  cent,  of  the  weight  of 
le  seeds,  contain  a  little  theobromine,  a  very  small  quantity  of  fat, 
some  mucilage,  no  starch,  and  much  vegetable  tiitsue  or  lignine. 

Structure  of  the  Cocoa  Seed, 

It  is  of  very  great  im|>orlance  that  the  minute  structure  of  all  TCge* 
table  snbstAnces  em^iloyed  in  food  and  medicine  should  be  ihorougtily 
understood;  lor  without  such  knnwledgi'  it  is  quite  imimMible  to 
detect  the  adulterations  to  which  the  majority  of  them  are  liable. 

The  structure  of  the  seed,  or  bcnn.  o^t  it  U  someliniei*  called,  of  ibe 
cocoa,  is  very  chnracteristic,  although  son:ewhat  coniplic  :'cd :  in  it» 
as  in  other  seeds  two  parts  require  to  be  distinguished  the  shell  or 
husk,  and  the  seed  proper. 


COCOA,    AND    ITS   ADLLTLRATIONP. 

Th€  firtt  structure  mitiVH  on  the  surface  of  the  husk,  consists  of  a 
considerable  number  of  tubular  Jibres  uf  large  size,  and  containing  gra- 

Fig.  M. 


FhU  iWgWTlM  fVfmicaU  the  liAmlar  jttrva  tMuallj  oinprvcil  In  RTtKier  or  \tm 
•UHiktn  oa  UM  MrthM  of  lh«  Cooua  biiu.    Tho  flbrw  ut  miguifltcl  100  dl»< 


matter  nnd   minute  corpuscles  ;  tliey  are  more  ^bundtint  on 

•eeds  llian  others;   they  do  not  ap[M-ar   to   form  part  of   the 

bul  belong   ralber  to  the  8eed-veb«el,  and  they  are  probably 

ived  fWiro  the  spongy  substance  which  surrounds  the  Reeds  :  iJie 

for  the  mo«t  purt  run  parallel  to  each  other  in  the  courae  of  the 

lour  axUt  of  the  seed. 

Toe  kiuk  uiay  be  separated  Into  three  or  four  distinct  tunics  or 
iiHmbnacB. 

Thm  Jir$t  or  outer  membrane  connists  of  elongated  cells,  adapted  to 
«ac&  Wnsr,  Mxl  dispcised  in  a  single  layer,  with  their  long  diilnieters 
pUcMl  tnnaveraely  t4}  the  axit4  of  the  t-ued. 

The  Merond  tuiue  is  confititutcd  of  liu'ge  ongulnr  cclk,  suprrimposed 
ifl  •CTtnl  clbflely  connected  layers;  towwds  the  centre  ot  the  mem- 


<1M 


COCOA,  AND  ITS  ADULTERATIONS, 


brane   funned    by   them   the  coUs   increase  greatly   in    size,    their 
parietes  become  thin  auU  diuphunouB,  and  their  cavities  filled  with  a 


«ir.4U 


Thit  fnffnvinf  rrpfWWnU  lh«  nro  tmter  tmitacif  Hf  hitatmf  tka  aMtfq^OocoA, 
ftiiMrtir  iriit  At  mfcwonrf  oarf  mttc*laot-l>farin(i  cfttu.    a,  outer  iiittnkriM4  k, 
tBule  t  c  nncltic*  eelU-     Thu  flgun.  &•  wdl  u  Itic  tUm  following,  «n 


mucilaginous  substance,  which,  in  the  bean  soaked  in  water  for  some 
hours,  IS  seen  to  be  considerable  in  quantity. 

These  two  meinbriines,  together  with  the  enlarged  cells,  are  de- 
lineate«l  in  jSfi:.  41. 

As  the  cell*  forming  the  seoond  membrane  approach  the  surface 
of  the  seed,  they  lose  their  mucilaginous  chai'acter,  become  smaller, 
and  return  to  their  original  size. 

If  now  the  surface  of  an  entire  seed  enclosed  in  its  tuetubrone  be 


COCOA,   AND   ITS   ADULTERATION;*. 


Ull 


exnniine'l,  several  raised  lines  or  fibres  will  be  observed,  commencing 
Bt  th«  end  of  tbe  seed  attached  to  tbe  seed-vessel,  ppreading  them* 


rig.  <%. 


In  tfelj  Scnra  Uw  c*^,  wott^f^nt,  ^nd  vlrof  remttt,  u«  dcllnrtUd,  which  eoo 
•tlUita  tl*«  4(«|)  portion  at  tlw  mcwu)  mtrobrftue. 

k1  res  out  over  its  surfuce,  nnd  temiinatinw  at  the  distal  extreniTF^ 
of  tbe  seed:  these  fibres  ar«  coiiif)o«t»il  of  spiral  veswU,  which  lie 
imbeddod  in  fibres  of  woody  tissue  and  the  cells  above  de^^cptbud. 

The  Jiecond  membrane  forms  the  chief  substance  and  thickne.is  of 
the  husk. 

The  third  membrane,  thin  and  delicate,  consists  of  anpulnr  cells  of 
small  size,  the  cavities  of  which  contain  mitnito  plobuk's  of  fa! :  in 
removing  the  outer  tunics  this  membrane  somclinie*  comt»s  oway 
in  part  with  them,  but  in  penernl  the  greater  portion  adheres  to  the 
Burfjire  of  the  seed.  This  meml>rane  covers  not  only  the  outer 
gurfftee  of  the  lobes  of  the  seed,  but  also  dips  down  between  them, 
and  furnishes  each  of  the  opposite  sides  with  a  covenn;» ;  it  is  most 
evident,  however,  on  tbe  external  surfuce.  It  is  probable,  notwith- 
ttanding  it  may  be  exhibited  as  a  separate  tunic,  that  it  is,  strictly 


1 


168 


COCOA,    AND    ITS  ADULTERATIONS. 


Hpeaking,  not  ta  be  repardcd  as  a  distinct  structure,  but  timt  it  rcaWy 
belongs   to  the  seed,  since  on  removing  it  colls  belonging   to  the 


iRtlili  cnfnTbif  Ihe  icrfr*!  ilraetarH  kbore  DsUeM  an  delloMtcd.  9,tkir4 
t»m^ :  ti,  rvuntM  rrflx,  iletlveil  from  the  wcood  nwiribnine.  I«lii||  upon  Ui« 
frunh  metnbnini.  «tMl  dlnalcd  M  the  lUici  of  Junetlor  of  ihe  Iom  tr.  futrth  iw 
Jttrcitf  tmetnl/rrtrnt ;  tl  d,  tkmo'tttd  buditt  :  e  c,  nivndfd  ntawi-4  nf  rrv**aUiiil  fatly 
"•<»"<'' .'  //i  fTfitah  tjfvmryariw. 


substance  of  tbe  seed  frequently  come  away  with  it;  thp  colourless 
cells  constituting  it  being  evidently  praiJuully  trnnsformeil  into 
the  coloured  ones  of  the  aee<i  itself.  To  earh  HPcd-luUe,  tliepefore, 
according  t4i  tho  above  description,  ihere  is  a  dislitict  membrane. 

Situated  in  the  interspaces  of  the  lobes  is  a  fourth  structure,  at- 
taebed  externally  to  the  second  membrane,  the  t-ells  tbruiinf;  which 
pass  down  upnn  it  for  a  ^hort  dii^Unce;  ahhough  clear  ami  trans- 
parent,  it  f.^hibits  a  fibrous  tttruclurc,  and  on  its  surface  a  ctmsi- 
derable  number  of  jimall  cry&taU  are  always  to  be  seeji,  us  well  as 
many  elongated  bodies,  rounded  at   either   exti*cmtty,  and  divided 


d 


COCOA,   AMD  ITS   ADULTEHATIOXS. 


163 


into  several  compnrtincnts  or  cells,  and  which  <Io  not  appear  to  be 
atiaclied  to  the  luenibrane  on  which   the/  lie.     Frum  ibcir  curious 


TU«  flffUK  PCpreMnu  thtfvJU  which  fonn  the  kernel  nfiha  wed.    In  .1,  the  eelU 
KDil  cunUlurU  tUrvh  u>rputcli:i  an  itiK<ulSnl  12311  lUmnictcra  i  whI  in  /t,  SIJO  dlft- 

appearnncc,  and  the  abpencc  of  connexion  with  any  of  the  other 
atrucl tires  of  the  cocoa  seed,  the  nbeer^-er  is  led  to  jnwpect  that 
they  arc  extraneous  and  probably  fungoid  growths.  We  have  de- 
tected them  in  every  sample  of  cocoa  seed  aubmiltcd  to  exauuna- 
tion.     Sce^.  43. 

Wc  have  now  completed  the  description  of  the  several  structures 
which  enter  into  the  composition  of  the  husk  of  cocoa. 

The  Jtff«v/,  deprived  of  Its  hut^k^  is  seen  to  be  composed  of  several 
lobeSf  an»nilar  in  form,  nnd  irregular  in  size  and  shape ;  undci  prea- 
gune,  these  readily  separalc  troni  enoh  othur,  arul  the  seed  breaks  up 
into  pieces,  which  are  known  as  •*  nibs." 

The  lobes  are  constituted  of  innumerable  minute  cells,  of  a  rounded 
form,  the  cavities  of  which  are  filled  with  starch  corpuscles  and  fatty 
matter. 

On  the  Burfiice  of  the  seed  these  cells  are  rendered  anjcular  by  cuni- 
prcsision,  and  are  usually  of  a  deep-red  colour :  the  lint,  however, 
varies  greatly ;  they  are  frequently,  in  parts,  spotted  with  purple,  and 
even  deep  blue. 

u  2 


164 

Each 
rountled 
bilum. 


COCOA,  AND   ITS  ADULTERATIONS. 


cell   contains   man^  itarch  corpuscles,   biiiaII   in  size,  of  ft 
form,  and  which  olten  pre&ent  an  obacure,  rudJatc^  or  stelktc 

Fig.  M. 


RtpraMnta  the  atnicttim  met  with  fa)  •  PMnpIc  of  oRirrtini  TvnmiAD  Cocoa.  It 
vlU  bt  nollcC4l  thtt  lA^-  (a#iM-a  farmdmo  tic  Atuft  of  toeoa  art  tittmt,  wkI  th«t 
UiM^nf  Ihf  arvd  ll«rir*mnuvh  Ivokm  iqi,  nanj  or  tliscvlli  bclnf  ni|>lurr<I,  an 
M  hi  prrtnll  trif  VMAM  oflhr  fUrckMrfOHdllwllI  fkl,poliilJ  or  itntv^nari'^  ht 
th«  ni«nufinturf  of  choroUlr.  a  cfieDi  of  (be  kcrn«l  of  eon«  i  ft  f\,  menil-rmn* 
on  aurfK*  of  lohM  ;  r  c,  tiwuM  of  onbrjo  i  d  rf,  &«■  muMa  of  alanJi  [  c  r,  loowt 

Placed  at  one  OJitremity  of  the  ftced  Is  the  embryo  ;  this  consists  of 
cellular  tlMue,  the  cells  or  meshes  of  which  encluse  numerous  starch 
grsntiles  and  spheruleji  of  oil. 

Now,  in  the  more  carefully  prepared  chocolates,  the  whole  of  the 
structures  represented  in  Jign.  40,  41,  and  42.  are  absent,  and  those 
delineated  \nfig.  43.,  and  especially  Jig.  44.,  only  are  met  with  :  in 
some  cases  the  embryo  even  ia  removed  ;  but  this,  since  it  forms  so 
inconsiderable  a  part  of  the  entire  seed,  and  contains,  moreover, 
starch  and  f»t,  appears  to  be  almost  an  over-refinement. 

Oti  the  Prnperties  of  Cocoa. 
Cocoa  may  be  considered  under  two  beads ;  as  ref^ards  its  action 
on  the  nervous  and  vascidar  systems,  and  as  a  direct  nutritive. 


COCOA,   AND  ITS  ADULTERATIONS. 


165 


The  physiological  actions  of  the  aromatic  oil  of  cocoa  and  of  the 
ibwhrumine  urc  probably  similar  to  those  of  ibe  corresponding  con- 
BiiCuents  of  tea  and  coflee. 


Exhiblw  tlM  Wrtfm  piMMil  In  ■  Mmplerrf  hmx/m/'m-sIm/ Flakkd  Cocoa,  which 
aMullr  aniaiulDM«arfaadAiufc.  an.  lubalw  fllim  tm  mufmet  ■  b  &,  ttamd 
nMmbraiu  of  hoik  t  c  «*,  iptrftl  »i  iirit  <  J  it,  etUt  irf  krrn»)  i  t,  mrmbrftnc  cwst- 
hm  lob**  I  /.  llMiN  of  tmSrjro  i  f  a,  tret  mamet  uf  iUrch  gnoulet  t  i^  K  Iomc 
•tartli  oorpiuclcs. 

The  special  actions  of  the  Tolatilc  oila  of  tea  and  cocoa  have  not 
ret  been  scientiflcally  invesligntcd ;  those  only  of  the  oil  of  coffee  have 
hitherto  been  made  the  subject  of  experiment ;  but  from  anatofEj 
tiiere  l»  good  reason  for  supnoBin;;  that  all  these  oiU,  which  so  cloBely 
resemble  each  other  in  their  ptiy^ical  i)rop<?rties,  agree  also  in  all 
es»ential  particulars  in  their  physiological  actions. 

The  Tolatile  oil  of  coffee  taken  in  tiiodcrate  <iuflntitie8,  as  already 
stated,  produces  a  gentle  excitement  of  the  nervous  and  vascular 
system:^,  dispels  hunger,  retards  the  wa«ite  of  the  tissues  to  an  equal 
extent  with  caffeine,  and  hence  allays  hunger. 

The  caffeine  of  coffee  and  of  tea  retirds  greatly  the  wa.ste  of  the 
tissues,  and  hence  is  indirectly  nutritious.  This  Is  shown  by  the 
diminution  of  the  quantity  of  urea,  phosphoric  oeid,  and  salt  in  the 
urine. 

As  a  nutritive  cocoa  stands  very  much  higher  than  either  coffee  or 

M   3 


166 


COCOA,   AND   ITS  ADULTERATIONS. 


tea,  in  consequence  of  the  large  quantities  of  fat,  starch,  and  glut«n 
■  coiitainetl  in  it. 

it  is  true  that  tea  contains  a  lar^r  proportion  of  gluten  than 
cocoa,  viz.  35  per  cent.,  a«  Lonipared  wuh  20  per  cent.;  but  most 
of  this  <zluten,  owins  t»)  the  ni:inuer  in  wliiub  lh«  infusion  Is  prepared 
and  drnnkf  remains  in  the  leaves,  and  the  l>enclil  of  it  is  of  course  lost 
to  the  system.  Again,  tea  does  not  contain  butter  or  any  considerable 
amount  of  starch.  In  the  cose  of  cocoa,  an  emulition  of  the  seed  is 
made,  and  in  this  way  all  the  active  and  nutritious  constituents  of  the 
article  are  consumed.  Owing  to  the  large  quantity  of  fatty  matter 
present,  cocoa  is  apt  to  disagree  with  some  delicate  Etoraacha. 

On   THE    AdCLTEBATIOV  OF   CoCOA. 

The  roasted  beans  or  seeds  of  eocoo,  when  ground  and  reduced 
to  paste  constitute  ilnke  or  rock  cocoa,  which  consists,  when  it  is  ge- 
nuine^  of  tuHhiit^  hut  cocoa. 

Other  names  under  which  cocoa  is  sold  in  this  country  are  granu- 
lated, soluble,  dietetiu,  honiofopatbic  &c. 

Now  there  is  nothing  in  these  names  to  indicate  that  the  articles  in 
question  arc  anything  more  than  varieties  of  cwoa,  or  to  Rhow,  what 
18  too  frequently  the  cA.<ie,  that  they  are  compounds  of  sugar,  starch, 
cocoa,  and  oftentimes  other  substances. 

The  practice  of  calling  these  mixed  articles  cocoA  is  manifestly  as 
improjKir  and  deceptive  as  it  is  to  call  Me  cowpowtd  of  coffee  and 
chicory^  Patent  Compressed  Coffee,  Finest  OM  Turkey  Collee,  &,c. 

An  article  should  be  sold  for  what  it  really  is,  and  under  its  own 
name;  if  it  be  right  to  sell  these  mixtures  at  all  they  should  be  sold 
as  the  law  now  compeU  chicory  and  coiTee  t^)  be  sold,  and  should  be 
labelled  as  mixturps.  Further,  ihe  prtiportions  of  the  several  ingre- 
dients entering  into  the  composltiun  of  the  mixed  article  bhould  be 
staled  on  the  wrappers. 

The  French  and  other  continental  manufacturers  of  cocoa  adopt  a 
more  str:»ighlfonvitrd  and  proper  course  :  they  never  eiiil  their  com- 
pound and  manufactured  articles  roci)a,  but  ehoeolate  ;  tlius  they 
even  denominate  the  cakes  which  they  prepare,  and  which  contain 
nothing  but  cm-oa,  chocolate  —  "chneolnt  sjins  sucre/' allhnugh,  with 
strict  propriety,  they  might  in  tliis  case  have  used  the  word  cocoa. 

The  cocoa,  then,  of  the  English  makers  in  general  ia  not  cocoa  at 
all,  but  chocolate;  whenever,  therefore,  the  word  cocoa,  an  adjective 
of  indefinite  signification  being  pre6xed,  is  employed  to  designate  an 
article  which  is  not  pure  or  genuiue  cocoa,  Otat  articie  ottght  to  Ite  con- 
sidered us  adulterated. 

The  works  of  Aecum,  Brande,  Uyv.,  juid  Pereira  contain  but  little 
information  respecting  the  adulteration  of  cocoa;  the  only  English 
writers  who  have  treated  of  it  at  all  fully  being  Mitchell  and  Nor- 
mandy. 


^ 


I 


I 


t 


COCOA,  AKD   ITS   ADULTERATIONS. 


167 


w 


The  6rst  of  these  authors,  Mitchell,  bos  the  following  observations 
on  the  subiect :  — 

**  ChcMjolule  is  aduHeratod  with  flour,  potato  starch,  and  su^ar,  to- 
other with  uocoa-iiut  oil,  lanl,  or  even  tallow.  Even  the  su-cuUed 
finest  chocolate  i:?  made  up  with  cUiified  mutton  suet  and  common 
sup[ar,  to;;ether  with  ordinary  cocoa. 

"If  in  breaking  chocolate  it  is  gravelly,  —  if  it  melt  in  the  mouth 
wilhonl  leaving  a  cool,  refreshing  taste,  —  if  it,  on  ihe  U'Iditioii  of  hoi 
water,  becomes  thick  and  pusty,  —  and,  lasily,  if  it.  form  a  gelalinoui) 
maw  on  cooling,  it  is  aduileruted  with  siurcb  and  sueh-like  sub- 
stances. 

^^  Where  earthy  and  other  solid  substances  are  deposited  from 
chocolate  mixed  with  water,  cither  the  beans  have  not  been  well 
cleansed,  inferior  sugar  has  been  employed,  or  mineral  substances 
have  been  added  to  it^  either  for  the  purpose  of  colouring  or  of  in- 
creasing its  weight. 

"  Moreover,  when  chocolate  has  a  kind  of  cliet^y  tuste,  animal  fat 
has  been  added ;  and  when  very  raiwid,  either  vegetuhle  oil,  or  even 
the  seeds  themselves,  have  been  employed  in  the  sopliiaticalioii, 

"The  mineral  substances  euiployt'd  in  the  muking  u|i  of  chocolate 
KK  some  of  tliu  ochres,  both  red  and  yellow,  to^^etlier  with  minium 
(red  leoil),  vermilion,  sulpliaic  of  time,  chalk,  &e.  Chocolate  so  uiluU 
t«rali'd,  more  especially  with  the  preparations  of  leail,  are  highly  in- 
jurious; it  is,  however,  only  the  Ulterior  chocolates  that  ore  thus 
ndulterated." 

Knnn  the  work  of  N3rmandy  we  extract  the  following  remarks  :  — 

"Unllirlunulely,  however,  many  of  the  prepiimtions  of  the  cocoa-nut 
sold  under  the  names  of  chwolate,  of  cocou  flakes  ami  of  chocolate 
]Kiwder,  consist  of  a  most  rlisgusting  mixture  of  bud  or  musty  cocoa* 
nuts,  with  their  itliells,  coarse  itugarot'the  very  lowest  ipiality,  ground 
with  potato  fltarch,  old  t-ea-hiz^ciiits,  course  branny  llour,  animal  fat 
(gcncjaliy  tallow,  or  even  greaves).  I  have  known  cocoa  powder 
made  of  potato  starch,  moistened  with  a  deco<!tion  of  cot>oa-niit 
ifaells,  und  sweetened  with  treacle;  chocolate  made  of  the  same  ma- 
teiiak,  with  the  additions  of  tallow  and  of  ochre.  1  liave  aUo  met 
with  chocolate  in  whicb  brick-dust  or  red  ochre  had  been  introduced 
to  the  extent  of  twelve  per  cent.  ;  another  sample  contained  twenty- 
two  per  cent,  of  peroxide  of  inm,  tJie  rest  being  starch,  cocoa-nuts 
with  their  shells  and  Uillow.  Messrs.  Jules  Garnier  nTid  Uarel  assert 
ihat  einnahar  and  red  lead  have  bct-n  found  in  certain  !i;imples  of 
rhfK'olate,  and  that  serious  acciilents  had  been  caused  bv  that  dia)>o- 
lical  Oflullerarion.  Genuine  chocolate  is  of  a  dark  brown  colour; 
that  which  has  been  adulterated  is  generally  redder,  th')ugh  this 
brighter  hue  ii  sometimes  given  to  excellent  chocolate,  especially  in 
Spain,  by  means  of  a  little  annato.  This  aildition  is  unobjectionable, 
provided  the  annato  is  pure,  which,  however,  is  not  alwavs  the  case." 

In  defence  of  the  practice  of  selling  sugar,  flour,  and  cocoa  under 

U  4 


IM 


COCUAy  AND  ITS  ADULTERATI0K8. 


llie  name  of  cocon,  it  is  alleged  that  these  articles  are  more  atslnhU  and 
more  digettlilln  ibun  cocua  is  alone  lu  reference  to  these  stutemeuls 
tbefolluwing;  considerations  prust^nt  themselves. 

Whun  a  cup  of  cocoa  is  luaile  by  puurinif  hot  water  uprm  It,  the 
sugar  4>f  course  dissolves,  as  when  ^w^nr  is  added  to  tea  or  coffee  :  it 
certainly  has  no  etTect  whatever  in  makin;^  the  cocoa  raore  soluble  or 
more  digestible  ;  and  llie  consumer  at  all  cvtints  mi^ht  be  left  to  add 
lor  htni^lf  as  he  does  tn  his  (en  or  collce.  The  Htarch  or  farina  usu- 
ally added  to  cocoa,  wbcn  boiling  water  is  poured  upon  it,  forms  a 
paste  or  jelly,  mure  or  less  thick.  This  serves  lo  entangle  the  particles 
of  cocoa  oil,  and  to  prevent  part  of  the  oil  from  aijceiiding  tu  the 
surface,  and  collecting  there  in  droplets.  In  a  cup  of  cocoa,  therefore, 
for  an  etpial  quantity  of  coroji,  there  is  just  n«4  much  oil  ns  though  no 
starch  was  present,  nlthough^  it  is  true,  imrt  of  (he  oil  la  concealed  from 
view.  We  do  not,  therefon*,  perceive  hi  what  way  the  Ktarcb  renders 
cocoa  more  dieestible.  l!)f  coursi-  the  more  sugar  and  siarch  added 
to  the  cocoa,  tbe  less  cocoa  there  is  in  the  mixture  and  the  le:)s  nil ; 
but  nearly  the  saine  end  would  be  obtained  by  uslui;  less  of  genuine 
cocoa.  Moreover,  alarch  in  the  proportion  of  about  12  per  cent-  is 
one  of  the  natural  coustituents  of  the  uouoa  bean. 

But  it  may  be  {rriinteii,  men>ly  for  the  sake  of  argument,  that  the 
starch  (the  suj^ar  h  ultoL^ether  out  of  the  question)  is  really  an  im- 
provement :  it  ran  <iidy  be  so  in  certain  proportions ;  yet  when  we 
come  lo  analyse  diSurent  preparuiiona  of  cocoa,  we  find  that  the  pro- 
portions of  starch  vary  from  5  to  50  per  cent.,  with  the  sugar  from  80 
to  90  per  cent.  Of  course  such  Urge  atlditions  oa  tliesc  cannot  possibly 
constitute  iiiiprovenientM,  nor  do  they  ;  in  fact,  souieuf  thefte  mixtures 
Lave  scarcely  the  flavour  or  evet»  the  smell  of  eocoa. 

That  these  large  additions  of  starch  nnd  sugar  are  not  improvements, 
any  body  may  satisfy  himself  by  c<mlrasling  the  smell  and  taste  of  a 
cup  of  cucoa  made  from  genuine  tlake  or  rock  cocoOf  and  one  mode 
from  the  ordinary  mixed  article. 

Neverthilcss,  we  do  not  go  the  length  of  stating  (bat  such  mixtures 
ought  not  to  be  permitteil ;  but  we  ate  of  Dpinit>n  that  they  ought  to 
be  sold  OS  mixtures,  and  the  proportiuns  of  the  ingredients  stated  on 
the  wrapper. 

Nearly  every  kind  of  Bour  and  starch,  especially  such  as  ore  inex- 
pensive, is  added  to  cocoa.  In  the  cheaper  descriptions  of  cocoa 
whrut  floHTy  ftotaio  gUireh^  nnd  gago  meal  are  chiefly  used,  as  well  as 
mixtures  of  tiiem  in  different  proportions  ;  one  dealer  ;;ivii)g  the  pre- 
ference to  one  kind  of  starch  or  ini.\turc,  another  to  another  kind.  In 
some  of  the  more  expensive  eocoaa  Eatt  Indian  arrowroot  and  Toua  let 
Mois,  or  mixtures  of  these  with  the  chcn])er  aiarehes,  are  cmploved. 

The  quality  of  the  sugar  used  varies  from  white  lump  to  tlie  in- 
ferior descriptions  of  brown  and  Ireacly  sugnr. 

Now  the  excessive  reduction  of  cocoa  by  means  of  sugar  and  starch 
sometimes  reuders  the  employment  of  animal  fat  necessary  to  give  it 


I 


I 


COCOA,  AND   ITS  ADULTERATIONS.  169 

a  rusher  oJiarAxrter ;  verv  oommonly  thi.i  re^luctinn  also  fnrtber  ne- 
ceasitAteA  the  use  of  coloured  or  ferruginous  earths^  m  Venetian  red^ 
na^er,  and  boie  Armenian, 

Mr.  George  rhrllipf  io  evidence  before  the  Parliamentary  Com- 
mittet;  on  Adulttinitiou,  states:  **lu  one  case,  where  1  succeeded  in 
ycelting  the  proportions,  from  a  manufacturer,  of  wtiat  he  (.'nlleil  his 
beat  soluble  cocoa,  there  were,  in  bis  own  Eancuagc,  coioa  forty- 
two,  lump  forty-tw<j,  white  and  red  fifty-two,  TUc  cocoa  represents 
the  nut,  the  lump  the  su^inr,  and  the.  white  is  starch ;  the  red,  oxide 
of  iron  to  colour  it.  The  per-centnge  of  cocoa  in  that  sample  would 
be  30  per  cent.,  and  that  was  stated  by  the  manufacturer  to  be  bis 
bett  vMMblf  cocoa."  If  that  waa  bis  bt»t  cocoa,  what,  we  wonder,  was 
the  comftositiou  of  bis  worst  ? 

It  should  be  known  that  Venetian  red  and  other  lerru»inous  eartba 
are  sometimes  contaminated  with  anenic, 

liesuUn  of  the  Examintdion  of  Samplrg, 

We  will  now  state  the  retulfn  derived  from  the  examination^  chemical 
Oiui  microMCopicJily  of  a  large  number  of  sampler  of  cocoa  of  diflerent 
kinds  pur^ha^d  from  dealers  resident  in  the  metropolis. 

The  results  of  the  examination  of  fiiiy-four  samples  of  rarious  kinds 
were, — 

Uliat  eight  samples  were  genuine^  these  being  flake  and  rock  cocoas ; 
that  is,  they  contained  no  sugar  or  starch,  but  consisted  entirely  of 
cocoa. 

That  wgar  was  present  in  forty-three  samples,  the  amount  forming 
from  5  to  »s  much  as,  in  some  cases,  50  per  cent,  uf  the  article. 

That  atarch  was  detected  in  forty-six  of  the  so-cidled  uocoas,  the 
amount  likewise  varying  from  5  to  50  per  cent. 

To  such  an  extent  did  some  of  the  samples  consist  of  sugar  and 
■larch,  that  they  contained  only  sufficient  cocoa  to  impart  some  degree 
of  flavoui-  tu  tlie  articles. 

Lasitvt  that  out  uf  sixty*eight  samples  of  cocoa  and  chocolate,  the 
•ahe5  of  which  were  submitted  to  exauiinatiou,  thirty-nine  contained 
coloured  earthy  substances,  as  reddle^  Venetian  red,  itmher^  &c. 

When  it  is  remembered  that  the  relative  prices  of  wheat  flour, 
potato  starch,  and  sagfi  meal,  also  of  sugar,  esii^cially  brown  sugar, 
Dear  so  small  a  prnjMjrtiun  to  that  of  cocoa  itaelli  tt  will  be  reailily  un* 
derntood  how  greul  is  the  inducement  to  3ub.stitute  these  articles  ior 
cocoa ;  and  it  will,  we  are  sure,  be  apparent  that  it  is  not  out  uf  simple 
regard  to  our  digestive  organs  that  they  are  added  to  cocoa  iji  such 
IftTfie  (quantities. 

ilie  extent  to  which  the  adidleration  of  cocoa  is  carried  may  be  to 
lome  extent  judged  of  by  the  fact  that  the  price  at  which  ^onie  of  the 
inferior  cocoa  mixtures  are  sold  is  much  less  than  that  at  which 
genuine  cocoa  can  be  purchased. 


ktli^v.. 


...-»?    I  ■•    *:   — »; 


COCOA,  AND  ITS  ADULTERATIONS. 


CHOCOLATE,  AXD  ITS  ADULTERATIONS. 


i:i 


Unlike  cocoOf  chocolate  is,  as  is  well  known,  a  man u foot u ret)  article  ; 
the  French  particularly  excel  in  its  prr-jioralion,  imiJtLng  a  variety  of 
combinations  of  c/>coa  wilh  ullier  subsluiice.*!. 

The  more  commoD  additions  are,  liowcver,  sugar,  and  vnrioiiH  kin<ls 
and  mixtures  of  starch  ;  in  the  bolter  descriptions  of  cUucoIutc,  Ma- 
ranta  arrowroot  is  employed. 

For  imparting  flavuvir  and  scent,  vanilla  and  cinnamon  are  cUteAy 
used. 

Occasionnlly  a  medictnal  chocolate  »  prepared  with  salep,  a  fucuta 
obtained  from  the  bulliuus  root  of  an  orrlus.  In  some  cases,  also. 
chocolate  i:^  made  the  voliirle  for  the  administration  ni"  viirious  re- 
metlicft,  the  taste  of  which  is  to  a  great  extent  concealed  by  the  cho- 
colate. 

Of  twelve  samples  of  chocolate  examined, 

One  contained  13  parts  of  sugar  and  25  partes  of  starch  iv  Lhu  100 
parts;  the  starch  consisted  of  a  mixture  of  L:ipiu<;u  starch,  Muruiita 
arrriwroot,  Indian  corn  flour,  and  sago  uifal. 

The  Jtecmtd^  of  3^  partd  sugar  and  30  parts  wheat  Hour  to  the  100 
parts. 

The  third,  of  13  parts  sugar  and  10  portj  sago  to  the  100  portii. 

The  fourth  «<amplc,  being  obtained  Irom  the  same  maker,  had  the 
same  comiHuiitioii  as  the  first. 

'Fhejifih  containc'il  15  per  cent,  of  a  mixture  of  wheot  flotir  and 
potato  frtarch,  hut  no  i^ugar. 

The  sixth  contained  14  per  cent,  of  sugar  and  IG  itrpotiifn  Hour. 

Tlie  Jii*rtf«/A  consisted  of  14  per  cent,  of  sago  mcul,  with  a  lililc  sugar, 
the  remaimler  being  cocoa. 

The  ftghth  con!*isted  of  a  mixture  of  eocoa  and  Mugnr  made  into  a 
paste  with  water,  the  cocoa  forming  itbout  56  i>er  cent,  of  the  article, 
or  little  more  than  one  half 

The  composition  of  the  ninths  tenOi,  and  eleventh  samples  was  nearly 
the  same. 

The  twrlfth  sample  consisted  of  a  mixture  of  sugar,  potato  flour, 
aogo  meal,  water,  and  c<tc(»a.  The  sugar  and  water  formed  42  parts  of 
the  article,  the  flour  at  least  10  part.** ;  the  cocoa  thus  formed  less  than 
half  the  article. 

Besides  the  above  ingredicmtA,  several  of  the  chocolates  contained 
coloured  /err nginuiu  earths.  Generally  the  proportion  of  starch  was 
much  less  rhun  in  some  of  the  cocoas  examined. 

Chocolate  being  a  compound  article,  no  valid  objection  can  be 
urged  against  tlie  jircsence  of  su^ur  and  starch-  The  fwints  to  Imj 
cun^idered  arc,  the  price  of  the  article,  and  the  proporlious  and  quality 
of  the  ingreilients  of  which  it  is  composed  ^  the  addition  of  the  red 
earths  of  course  cannot  be  justiljcd. 


171 


COCOA,   AND   ITS  ADULTERATIONS 


On  the  Detection  of  the  AduUeratiom  of  Cocoa, 

The  articles  emploved  in  the  adulteration  oF  cocoa,  and  v»ith  the 
meund  for  the  detection  of  which  it  is  net-es'Hry  that  we  should  be 
acquainted,  are  ihe  following  :  — 8ugar^  various  ftifurt  and  xUvehes^  husk 
of  Cftcoa^  chicory  root^  fatty  jnaUer^  and  coloured  ferragiuous  fiorths. 

On  the  Detection  of  Sitgar.  —  The  prescuoe  of  sujrar  in  cocoa 
may  be  readily  detected  by  the  taste.  To  deiernuno  the  quantity, 
the  following  simple  but  efficient  proceeding  may  be  adopted:  — 
Dissolve  a  weighed  quantity  of  co<>oa  coDtaiiiin;;  sugar  in  cold  wat^n*, 
Blter^  dry  the  residue  lirat  with  blotting  paper  nnd  then  on  the  water- 
bath,  weigh  ;  the  loss  will  inJicKte  very  nearly  the  amount  of  sugar 
with  which  the  sample  of  cocoa  operati^d  upmn  wns  admixed. 

To  show  to  what  extent  this  melhoil  may  be  rt^lied  upon,  wc  may 
mention  that  we  dissolveil  one  ounce  of  a  mixture  in  equal  proportions 
of  cocoa  and  PUgar  in  cold  water,  and  afterwards  dried  the  residue ; 
the  weight  of  thiy  was  only  twenty-eight  grains  sliort  of  the  four 
drachms.  Or  the  aqueoua  solution  may  be  eva[K>ruted  and  the  residue 
dried. 

The  method  of  determining  the  sugar  by  conversion  into  aloohol 
or  carbonic  acid  la  not  well  applicable  to  tlte  cocoa  mixture,  because  of 
the  atarch  present.  The  sugar  is  cane  sugar,  and  it  i^  necesaary  that 
this  should  be  converted  into  grape  sugar  by  the  action  of  dilute 
sulphuric  ai:id  in  order  to  render  it  readily  fermentable;  but  thia 
acid  also  converts  the  starch  present  into  fin<|!nr. 

On  the  Detection  of  Starch.  —  In  most  cases  it  is  sufficient  to  de- 
termine the  kind  of  starch  employed,  and  to  lonii  uu  afiproxiinate 
opinion  aa  to  the  quantity  present :  the  only  certain  method  by  which 
a  knowledge  of  the  kind  of  starch  cmp1oyc<l  can  be  obtained  h  by  means 
of  the  microscope.  In  some  cases,  however,  it  may  be  necesr^ary  to 
ascertain  with  tolerable  accuracy  the  quantity  of  starch  present. 

The  starches  emplAvcd  in  the  adulteration  of  cocoa  are  the  follow- 
ing :  wheat  flour^  potato  flour,  Indian  corn,  SHgo  meal,  tapioca,  East 
India,  Maranta.  and  Tous  les  MoU  arrowroots.  Now  utl  ih.ti»e  starches 
possess  distinctive  characters  by  which  they  may  be  readily  distin- 
guished from  each  other  by  the  aid  of  the  microscope. 

Cocoa  itself  contains  about  11  per  cent,  of  starch  in  the  form  of 
minute  starch  granules,  entirely  dtuerent  in  size  and  shaj>e  from  those 
of  coL-oa:  besides,  these  granules  usually  are  not  free,  but  ure  for  ihe 
most  port  embedded  in  the  relli  of  the  cocoa  or  else  in  its  butter. 

Now  although  cocoa  contains  i>o  nmch  starch,  the  only  means 
recommended  fur  the  discovery  of  the  a^luUeration  of  cocoa  with 
starch,  was  by  iodine,  which  of  course  gives,  if  properly  employed, 
indications  of  the  presence  of  fecula  in  every  case  ;  and  not  a  word 
was  even  hinted  rcsjjecting  the  employment  of  the  only  means  by 
which  the  different  starches  used  could  be  identified, — namely,  the 
microscope. 


COCOA,   AND   ITS  ADULTERATIONS. 


173 


The  characters  of  wheat  flour  wlU  be  minulel/  deiicnbe*!  under  tbc 
bead  of  Flour ;  but  ihey  huve  aireadj  been  brieilj  nolicid  and  reprc- 


Ff$.  47. 


•nAJTB,  i)Ans.fc  Co'*  Pmuot  Soira^  C^dooa. 
fin  a,  fltorefa eorpDRlM, etUi,  udtplnlTtMtltof  oocm  i  Aftb,  franulMarpoHafe 

fiumr, 

aetited  when  describing  the  adulteration!)  of  chicory  and  coffee.  See 
fig.  30.  p.  I'i7. 

The  ehartu'ters  of  fH*tato  flrinr  will  be  described  under  ihe  bead  of 
Arrowrotit,  It  may  he  siated  now  that  they  are  of  larjje  size,  ovate 
form,  distinctly  ringed,  and  with  a  fiinall  but  very  disliiicl  hilum  at 
the  smaller  extremity  of  each  granule.  They  are  well  represented  in 
A- ■•7. 

The  charoctem  of  tago  meal  will  also  be  given  under  the  head  of 
Arrowroot.  ITie  pranulcf,  nlihouj;h  smallpr  than  those  of  potato,  ore  yet 
of  conirideruble  sire:  but  they  are  particularly  and  easily  drMin^ished 
by  being  truncate  at  one  extremity,  as  represented  in^j^.  48. 

In  Jig,  49.  tlie  starch  granules  of  both  potato  flour  and  aago  meal 
ore  figured :  it  will  be  seen  that  the  dinerencea  ore  very  consider- 
ible  and  obvious. 


174 


COCOA,  AND   ITS  ADULTEBATTONS. 


The  starch  {^nniilcs  of  Indian  com  nrc  of  about  the  size  of  those 
wheat  Hour ;  but  thti  greater  number  of  ihem  are  polygcuiul,  and  hence 
they  exhibit  a  more  or  less  angular  outline.     See  article  Flour. 


^^4^48. 


fV'HiTI'l  Pt-M   UONaorATMlC  COCOA. 

a  •  «f  lUieli  fraaulH,  oelk  uid  frkginvnu  of  eooM  t  b  b  ft,  gruttiM  of  moQ 


Thp  characters  of  the  starch  granules  of  Afnronta  or  West  Indian, 
Curcuma  or  Ka9t  Indian,  Tapioca  or  ManiboL  arnfwro(»t.  and  of  Tool 
lea  Muiis  will  likewise  be  found  fully  detailed  in  the  article  Arrowroot. 

The  |rranules  of  Kajtt  Itulian  arroirroot  are  very  Hut ;  the  Jlrw 
upon  ibem  describe  segments  ur  |>ortiuDS  of  rings  only  ;  aud  the  ecntral 
cavity  15  not  visible. 

The  starch  granules  of  Wfst  Ittdian  arrotcrooi  are  of  nearly  libe 
same  sixc  at*  those  of  sago  starch.  They  differ,  hnwever^  in  not  bein^ 
niuUer-^haped,  and  in  the  slit  hilum  which  runs  transversely  acruM 
the  granule. 

Those  of  Tapittca  arrowroot  are,  like  the  starch  granulci  of  ngOi 
m oiler-shaped,  but  they  are  several  times  smaller. 


COCOA,  AND   ITS  ADULTERATIONS. 

Lmtlj,  tlie  ftorcb  granules  of  Totu  U*  Mois  differ  from  iiU  tlji;  others 
lA  being  vcrjf  much  larger ;  iLev  arc  flut,  wiiii  strongly  marked  slriw, 


/l^.  4». 


Jrtcribe  segments  of  circles  only^  and  tbey  present  a  snuill  but 

l-niark«ni  central  hiluro. 

Ib  orUcr  to  determine  npprnxi mutely  tlic  tpiantity  of  starch  present 

in  any  oooon,  firobably  one  uf  the  ^^implest  methods  is  the  tnllowing: — 

sugar,  if  prrient,  having  been  removeil  by  means  of  cold  water, 

cocoa  ij  to  be  boiled  thoniughly,  the  'tiTOCtion  ^tniined  throu<:b 

mit«r>[i    niirl  tli.»  fat  remiived  when  cnld  :  ihc  n^sidui' whit'l)  sub- 

t;  I  liquid  cnnflist<i  chiefly  nf  .it^rrh^  the  aniniitit  of 

I,  iMcd  either  by  measurement  in  gradnaied  tubes, 

ii  moy  be  dried  and  weighed. 

tbc  latter  ease  it  is  noeessary  1o  ascertain  by  previous  experiment 

boiled  and  dried  starch  of  eaeh  dilferent  flour  or  arrowroot 

ida  to  certain  aumunts  uf  the  raw  flour  or  starcb. 

idM  of  the  ({uantity  of  starch  present  nmy  be  formed  from 

tht  COMbtCDcy  of  the  decocliuQ  when  cold.     If  the  amouut  of  starch 


176 


COCOA,   AND   ITS   ADULTEUATIONS. 


is  rery  considerable^ — 40  or 50  percent., — the  liquid  will  be  thick ftnd 
jelly-likti. 


■ 


T«ri.nt  BBirrHKRv'  HoitrsorATnio  CocOa. 

a  CI  a,  KTuiDla  ittd  cell*  of  ooeo*  i  ^A  ft,  gimnutei  of  Oanna  ttcrek or  Urat  lea  Mob; 
r  Ci  (tmnuk»  of  Impiutm  ManJL 

Tn  makin;;  observMions  on  the  comparfttive  density  of  cold  decoc- 
lions  of  c(»oo.i  oontninin^  «]ilTi.Tmt  [»t!r-rcntn^eH  of  stiircli,  we  noticed 
that  after  a  tim<*  the  stan-h  rensei]  tn  W  unifaniil?  diffufted  throughout 
the  flui(I»  nml  that  it,  tks  well  as  the  heavier  pnrticlGs  of  cocoa,  subsided, 
leaving  a  supernatant  ittrntum  of  dear  li<piid;  this  stratum  vnrying  in 
thicrknt'ss  acuordinfr  to  the  quantity  ff  »tan.'h  prv-sent,  and  being  most 
shallow  where  ihere  woa  uioat  feculu,  and  deepettt  where  this  was 
least 

It  then  occurred  to  us  that  in  the  fact  of  the  subsidence  of  the 
starch  we  haH  a  mean!*  of  d^^lennininj;  approximately  the  per-centage 
of  that  substance  present  in  any  sample  of  cocoa. 

We  aocorilingly  filled  five  tubular  glnflse*,  each  seven  inohc.^  and  A 
half  in  height,  tliree-fourlh«  of  an  inch  in  diameter,  and  holding 
twelve  drachmi;  of  water,  with  five  different  cold  decoctions  of  cocoa, 
containing,  renpectively.  JO,  40,  30,  20,  and  10  per  cent,  each  of 
ntarch  :  in  the  first,  the  thicknes*  of  the  clear  stratum  was  one  inch  ; 
in  the  second,  one  inch  and  a  half;  in  the  third,  two  inches;  in  the 


COCOA,  AXD   ITS   ADDLTERATIOyS.  17: 

iiburth«  two  incbes  and  a  half;  md  in  the  fiAb,  three  inches.     It  is  to 
be  understood,  howeTer*  that  these  measttrements  are  approzimately 


Ar-^L 


o 


^9q 


Dcm'i  Onrtui  riAiMTLTtunD  Cnocounu 
9  •  It,  itenk  pmuto  uxl  cell*  at  euen%  t  hh  i,  grwtalM  of  foii^wn 


JfonwiAa  armimwt,'  <f,  ImUnn  cm-k  nwHiI,-  «  r,  iivfAftt  tfordl 


ccr, 
//,   CVrcmiM 


correct  onlj,  and  that  to  obtain'porfectly  nccarato  results  it  is  nocessarv 
tbat  the  experiments  should  be  carefully  repented.  The  proportion  of 
the  ingredienta  forming  ench  decoction  was  220  grains  by  weight  of 
the  mixture  of  coeoa  and  |K>tato  11i>ur,  to  eiybt  ounces  of  water,  the 
boiling  being  continued  for  five  mitiutes  in  each  cose. 

Or  the  amount  of  starch  present  may  be  determined  chemically.  The 
sugar,  should  any  be  present,  having  been  removed,  and  also  the 
fat,  either  by  expression  or  by  the  action  of  ether,  the  cocoa  is  to 
be  dried  and  weighed,  then  treated— once  or  twice,  as  may  be  neces- 
sary— with  a  weak  solution  of  potash,  which  will  dissolve  out  the 
starch:  the  residue  consists  chieflv  of  w(K>dy  fibre  ond  cellular 
tissue ;  this  is  to  be  dried  and  weiglied,  and  the  difierence  between 
the  first  and  second  weights  represents  the  amount  of  starch  pre- 
sent. Another  way  is  to  boil  the  cocoa  niter  the  remorul  of  the 
sugar  and  fat,  and  to  precipitate  the  starch  from  the  decoction  by 


COCOA,  AND   ITS  AnULTERATIONS. 


nicuDs  of  iodide  nf  potiuisiutn ;  the  blue  iodide  of  stfirch  is  formed, 
from  wUicb  tbc  starch  mny  be  calculated.  According  to  Brande 
iodide  of  starch  has  no  certain  compoMtion  ;  but  by  ibe  analysis  of 
Lorsaipne  it  appears  that  Jt  contains  41*79  paris  of  iodine  and  58*21 
of  starch  ;  or,  according  to  Rerzeliua,  two  aturas  of  iodine  with  one  of 
Btarch. 

Graham  gives  the  following  process  for  obtaioing  iodide  of  startb 
in  a  state  of  purity  :  — 

"  A  firm  jelly  is  prepared  by  boiling  potato  starch  with  water,  and 
after  cooling,  a  ijuanllly  of  hydrochloric  iictil  is  added,  sufficient  lo 
occasion  th*;  solution  to  become  liquid,  when  assisted  by  a  sliffht 
elevation  of  temperature.  The  solution  is  then  fdtered,  and  a  solu- 
tion of  iodine  in  jilcohol  is  niixpd  with  it.  no  long  lu  the  Utter  pro- 
duces a  blue  precipitate  ;  care  hoinf^  laki-n  not  to  add  too  nitichof  tlie 
noluiuiti  of  iodine,  ns  tbc  alcohol  of  tbut  solution  will  then  precipitate 
uncombined  starch."  * 

But  the  most  accurate  method  is,  nfter  the  removal  of  the  sugar,  to 
convert  the  starch  into  grape  sugar,  aTxl  to  calculate  the  amount 
cither  by  Fehling'a  test  or  from  the  alcohol  or  carlxmic  acid  formed. 

Tidce  200  grains  of  the  cocoa  mixture  ;  boil  with  about  ten  time* 
the  quantity  of  water;  add  nithcr  more  lliari  two  dmchme  of  dilute 
sulphuric  acid  (1  to 5),  and  Jtpply  hcnt  nntil  tbc  lluid  Ix-comcs  thin:  boil 
the  fluid  for  6  or  10  hours  in  a  tlask  with  a  narrow  neck.  pUcetl  on  the 
sand-bath,  replacing  from  lime  to  time  the  evaporated  water;  or  beat 
the  fluid  fn>m  twenty-four  to  thirty-aix  hours  in  a  water-bath.  When 
the  conversion  is  com]ilett%  which  in  ordinary  cases  may  be  ascer- 
tained  by  litK-ture  at  iodine,  Uilute  the  fluid  with  water,  and  det«r> 
mine  the  quantity  of  sii<!ar  present  either  by  Fehling's  test  or,  what  is 
better,  by  converting  it  into  alcohol  and  carbonic  acid.  Calculate  the 
stignr  from  cither  of  these,  and  flic  srarch  again  from  this.  The  com- 
position and  method  of  using  Fchling's  test  Is  given  elsewhere;  100 
parts  of  graj*  sugar  correspond  to  90  parts  of  starch.  The  method 
of  converting  grape  etiizar  into  alcohol  is  described  under  the  artidt 
Coifec,  p.  123.,  and  the  fermentation  test  under  Tobacco. 

On  the  Dvtectum  uf  Foreign  Futttj  Mutter.  —  Animal  oils  and  faU,  U 
lard,  tallow,  and  suet,  on  expiosure  to  the  air  for  a  tiuie,  dtiteciflllv  ins 
warm  place,  liecome  rancid  and  disagreeable  to  the  taste,  while  the 
butter  of  cocoa  under  the  same  circumstances  remains  |>er(ciMly  >i*e«t 

For  the  detection  of  these  adulterations,  therefore,  the  cocoa  or  cb<>- 
rolate  should  be  scraped  line  and  spread  out  in  a  thin  layer  on  a  plate* 
so  that  the  air  may  have  free  access  to  it.  In  a  few  days  the  fonfiip 
fatty  matters  will  have  Irecoiuc  rancid,  when  they  may  bo  detected  by 
the  taste  and  smell,  esj>einally  when  warmed. 

Another  way  is  the  /bllowing,  given  bv  Dr.  Normandy:  — 
The  presence  oi  animal  fats^  or  of  oiU,  may  also  be  rcoogniMd  by 

•  Elcravnli  of  Chemistry.  p.74t 


COCOA,  AND   ITS  ADULTERATIONS. 


179 


lifyin?  m  portion  of  the  chocolat*  as  follows  :  —  Hasp  about  2000 
ift  of  tnc  cli«>colate  untlcr  oxaminatlnii,  and  boil  them  with  water 
vome  caustic  putiit<h.  When  tlie  fut  \n  sanoriilii^d,  dilute  \\ni  mass 
with  a  suflicienC  quantity  of  water,  ami  filter  ttiree  or  four  tiiurs.  The 
milky  IJItrate^  which  is^  io  fact,  a  solution  of  soQp,  should  now  be 
rapenaturaU>d  with  nitric  acid  ;  this  will  <teparate  thetht^  which  will 
imit  on  the  liquor  after  cooling.  It  may  then  he  collccled  on  a  fitter; 
and  on  rubhin^  a  small  portion  of  it  between  the  fingers  the  odour 
will  generally  indicate  its  origin  ;  but  more  cfl'et'tunlly  still  by  heating 
it  in  a  ftanW  capeule.  Pure  butter  of  coeoa  has  no  riduur.  Or  the 
chocolate  may  be  exhauEted  by  sulphuric  ether,  ami  by  evaporating 
^Hl^  tbe  fat  will  be  left  behind,  and  may  then  be  identified,  as  just 

^^F   The  pre^nce  of  foreign  fatty  matter  may  sometimes  be  determined 

^Bby  noticing  the  form,  Aize,  and  con-(i»teney  of  the  droplets  of  fut  or  oil 

^^wKich   collect  on  the  surface  of  a   decoction  of  cocoa  after  it   has 

heconecold.     If  the«e  droplob*  be  firm,  shot-like,  undglubular,  except 

I      on  the  upper  surface,  which  is  f>lightly  flattened,  and  very  siiufdl}  rarely 

J       OUetding  the  twelftii  of  an  inch  in  diameter,  (hen  (here  ia  no  doubt 

'       bot  tltat  the  globules  in  question  cun^ist  of  the  lat  or  butter  of  cocoa. 

If,  however,  on  tlic  other  hand,  the  globules  be  large,  flat,  or  disc- 

!n.i.   exceed  the  size  nameil  consideraldy,  attaining,  M>me  of  them,  lo 

oirth  of  an  inch,  and  even  more  in  diiuneter,  then  animnl  iat  nr  oil 

'  «bly  present,  a  conclusion  whtcli  may  be  still  further  confirmed 

•ing  tne  fat,  keeping  it  f'>r  a  time,  and  observing  whether  it  be- 

rincid  or  not     The  suspected  cocoa  should  t>e  cooled  in  an 

■  exposed  freely  to  the  air,  antl  not  in  a  covered  one,  for 

(  case  the  ilruplels  of  oil  of  even  pure  uocuawill  fjeq^uently 

(MHWfet*  ia  Urge  and  flattened  dies.* 


k 


Oh  the  Detection  uf  the  Afinerai  Suh*tttnces  uud. 


Of  the  tnineral  -lubstances  employed  in  the  adulteration  of  cocoa, 
•Dme  are  used  for  the  sake  of  their  weight ;  of  these  the  chief  arc 
■■lAinMifi  of  lime  or  chalk,  and  tuipkale  of  lime  or  piaster  of  Paria, 
MpteiaO/  the  former. 

Olber  Aibatances  nre  employed  for  the  colour  they  impart,  and 
t]M>e  are  fi^juently  had  recourse  to;  the  principal  are  red  iron 
wrtfaii  M  r«d  ochrr,  Vmrtian  red,  and  umber. 

Ftn  the  detection  of  these  mineral  substances  fiOO  grains  of  the 
eocoa  sbould  be  incinerated,  and  the  a.-«h  weighed  and  analysed. 

Soine  idea  of  the  nature  of  the  mineriil  substunces  mixed  with  the 
DOOM  Way  be  formed  by  dissolving  a  portion  of  it  in  boiling  water,  and 
ohwiiilig  closely  the  charnctcr  of  the  nrecinitnte.  In  this  way  the 
of  ferrugioous  earth  may  sometimes  be  readily  discovered. 


tnfoniMlloo  m*j  ofton  b«  obUliM^  by  urcrtatninf  the  tnrltinf  pnint.  whicti  ll 
i«CMMol  Ut*  Imtlar  of  cocoa,  an4  the  Uti  tnn|tlor«l  for  lu  «dutu<iiUluii. 
K  3 


uo 


COCOA,   AKD  1X8   ADULTEKATIONS 


For  the  detection  af  carbonate  of  limf  and  ndphaie  of  lime  we  miut 
proceed  oa  (lestTibed  under  the  houd  ofTt'Of  at  p.  101. 

The  uh  of  ^Tonuino  cocua  is  pule  erey  :  if  any  of  (be  red  iron  earths 
be  present  it  will  be  more  or  le?s  coloured  with  the  red  oxide  ^  iron  ; 
and  ID  order  to  determine  the  (|uiiiitiiy  of  this  oxide,  the  prtxress  de- 
scribed in  ibe  artielest  ou  Tea  and  Chicory,  at  pp.  103.  and  14^,  must  he 
followed. 

Rtd  Ochre  consists  of  oxide  of  iron  with  silica,  and  sometimes  alu- 
mino,  clay,  or  even  cliolk ;  whik*  y'en^tum  ml,  when  genuine,  consists 
nf  the  sesquioxide  of  iron,  and  is  obtained  by  calcining  coppers  or  sul- 
phate of  iron.    It  is,  however,  often  adulterated,  espt^ially  with  chalk. 

It  should  be  known  that  the  colour  of  the  ash  obtained  by  the  in- 
cineration of  (trepurations  of  cocoii,  adulturatcd  with  red  ochre,  is 
subject  to  ctmsiderable  vuriution,  dependent  on  the  manner  in  which 
the  incineration  has  been  cundiictrd,  nhelher  in  an  open  or  covere<l 
crucible,  and  according  to  the  degree  fo  wliich  theush  has  been  heated 
and  the  length  of  time  it  haa  been  •subjected  to  the  process.  Thu!>  the 
ash  of  cocoa  so  adulterated  may  be  umde  to  assume  dilfercnt  colours^ 
Tanrjng  from  dark  brown,  light  brown,  fawn,  yellow,  ferruginous 
yellow,  up  to  rust-red,  according  to  the  method  of  incineration. 

In  sonic  of  the  samples  in  which  clay  and  plaster  of  Parix  have  been 
ileteuted,  these  itub^itunces  were  not  u»ed  for  the  sake  of  adding  bulk 
or  weight  to  the  cocoa,  the  quantity  present  being  too  muhU  ;  but 
they  no  doubt  entered  into  the  composition  of  the  earthy  colouring 
matters  employed. 

Alumina,  if  (jresent,  may  be  estimated  from  the  soda  or  potash 
solution  used  to  separate  the  nluiiiiua  from  the  iron  in  the  manner 
directed  fur  the  determination  of  alum  in  bread. 

Duty  \d.  per  lb. 

Cocoa  and  chiK-olate  paste  Id,  j>er  lb. 

Husks  and  sV'lls  "Is-  per  cwt. 

Lb-. 

4,563,782. 

4.471,561 

2,336,625 


Home  consumption    1654 

„  1855 

l^iae  months  of         1856 


The  same  nine  months  of  1855 


-  A  great  diminutioo. 
3,482,370.  lbs. 


The  following  nuestion,  addressed  to  Mr.  George  Thillips,  with  the 
reply  thereto,  will  show  how  admirably  the  llevenne  is  protected  by 
the  Excise  agninst  loss  from  the  ailulleration  of  cocoa. 
Mr.  Kinunird.  "HftTu  ynu  examined  any  cocoas  f" 
Replt/.  "  Though  that  is  under  um,  wc  have  not  imich  to  do  with 
k  ;**  and  then  follows  a  statement  of  the  inahilily  of  the  Excise  to 
detect  Venetian  red,  or  any  other  feiTUiiinous  earth,  nJlhough  this  is 
one  of  the  comuioaest  uf  the  uduhcraUoiis  to  which  cocoa  is  liable. 


I 


'  ^w    «« 


5%. 


SUGARj   AND   1T8   ADULTERATIONS. 


181 


h 


SUGAR,  AND  ITS  ADULTERATIONS 

Two  kinds  ofgu^ar  have  been  purticularly  distinn'uishcd  by  chemists: 
naaieljf  cane,  and  grnpc  sugar  or  glucose.  1'he  fir»i  is  obtained  frum 
tlie  sugar  coiie,  the  beet  rout,  tlie  maple  tree,  and  M»ine  ctberpUats; 
while  toe  second  is  contained  in  greitter  or  less  q^uantities  in  most 
fruits,  and  parlicularly  in  grapes,  figs,  and  honey. 

The  chief  part  of  the  cane  sugar  of  co:innerc«  is  obtained  from  the 
sugar  cane,  SaeckarTim  offiviaanwL,  of  which  there  are  several  wcU 
marked  varieties. 

"  Thou*;h  almost  unknown  to  the  Greeks  and  Honmns,  and  now  cuN 
tivated  nio*t.  exten^ividv  in  America,  it  is  a  native  of  the  Old  World, 
It  was  faniili.ir  in  ihv  hast  in  must  remote  times,  and  apjiears  to  have 
been  cultivated  in  China  and  the  Suutb  Sen  IsUnds  long  before  the 
period  of  authentic  history.  Through  Sicily  and  Spain  it  reached 
the  Canary  It>lan4ls ;  thence  was  tranApbmtcd  to  St.  Dotniniro  by 
the  Spaniards  in  IJJO;  aitd  from  this  inland  it  has  gradually  spread 
civcr  tliL'  West  Indies,  and  the  tropical  regions  of  the  American  con- 
tioent." —  JohmtoH. 

The  sugar  cane  is  one  of  the  tribe  of  Grasses:  it  usually  reaches  a 
height  of  about  12  feet;  it  rarely  ripens  its  seeds,  and  is  tbercfure  pro- 
pagated from  slips,  which  are  planted  in  rows. 

In  bome  tropical  regions  the  sugnr  cane  (or  rather  its  juice)  forms 
an  important  and  nutritious  article  of  fond.  The  ripe  stalk  of  the 
plaitt  IS  chewed  and  suckcil,  after  being  made  so(\.  by  boring  it ;  and 
enormous  quantities  are  consumed  in  this  way.  '*  Large  eliiploads,** 
states  Johnston,  ^  of  raw  sugar  cane  arc  daily  brought  lu  the  markets  of 
Manilla  and  Uio  Janeiro ;  and  it  iii  plentiful  in  the  market  of  New 
Orle&ns.  In  the  Sandwich  and  many  other  islands  uf  the  Pacific  every 
child  luis  a  piece  of  sugar  cane  in  its  mouth  ;  while,  in  our  own  sugar 
colonies,  the  negroes  become  fat  in  crop  time  on  the  abundant  juice 
of  the  ripening  cane." 

The  nutritive  properties  of  the  raw  juice  of  the  sugar  cane  depend 
upon  the  circumstance  that  it  contains,  besides  sugnr,  a  considerable 
propwtion  of  gluten. 

The  following  is  the  process  followed  for  the  manufacture  of 
su^nr : — 

^he  canes  are  cut  down  by  means  nf  large  knives;  the  leaves  and 
tops  (u*u  choppe*!  olfaiid  left  in  the  field ;  tlie  caues  are  carried  to  the 
null,  where  tiiey  are  crushed  between  heavy  rollers  which  squeeze 
out  the  juice. 

The  juice  is  conveyed  into  large  coj>per  vessels,  and  is  clarified 
chiefly  t»y  the  addition  of  lime  :  the  lime  neutrali»*8  any  free  acids 
which  may  have  formed,  and  al^  carries  down  with  it  the  gluten.  The 
jtuoe  ia  next  boiled  down,  and  is  transferred  to  wooden  vessels  to 

M  3 


ru 


SUGAR,   AND   ITS   ADl'LTERATIONS. 


crvstalUso.    Finnlly,  it  is  put  info  casks  having  ceruin  perforationB. 
to  allow  of  the  escape  of  the  treacle  or  molassea- 

Composition  of  the  Sugar  Cant. 

The  following  are  »ome  of  tbe  chief  analyses  of  the  sugar  cano 
whioh  have  hitherto  been  made :  — 


Sufar        -       .       .       -       . 

Cehultwe 

Mudl-itcnou*.  rv'tlnoQi.  fAUy, } 
and  albumtiioiu  mulierK         J 

Wattr 

Frcib  lucar  ewe     -         -       - 

nif-j. 

r«nfM. 

Jk^*I.la. 

I7A 

n-4 

71-0 

731 

Tmhlit  Owe.          RiU-n  C«». 

14-uM)           ,ia-aE« 

8-867                    »-U71 
»-4I5                    (mj 

o^vi             o-aco 
76\«0              7C7a» 

iCtt-DOO               IQU-OOO 

IIN-U 

lOOV 

The  su^nr  cnne,  especially  the  violet  variety,   is  eoated  wilt  a 
peculiar  kind  of  wax,  tenncd  cerasine,  nr  su^ar  cane  wax. 

The  following  are  the  more  important  analyseit  of  cune  juice :  — 


Sagar 

Various  orfutc  mittere 

SalU    - 

Water  - 


1B-7S4 

0140 

aa-Mo 


)i»«oa 


Fallr*. 


SO  DO 

■on 

■017 
Tft^O 


100-OtiO 


Jf^vwt- 


2Mvm 

r8mall 
f  quant)  Ilf4. 

7B3S2& 


99-««4S 


HIS 
■CiU 


lOO-OOO 


It  appears,  therefore,  from  the  above  analyses,  that  cane  sugar  con- 
tains from  18  to  20  per  cent,  of  saccharine  luattcr;  yet,  owinp'  to 
various  eircunKHtunces,  not  more  than  6  per  cent.,  acconllng  to  John- 
ston, iff  usually  ^otit  to  market  in  the  .statu  of  crystiittised  sugar. 

The  quiiriLity  of  »ii>;iir  present  in  cuiie  juice  may  be  estimated  ap- 
proximately by  taking  the  spcHGc  gruvity  ofthe  juice.  Prreira  st.itcs 
that  it  rnnj;es  ironi  ICKJT  to  I'lOti,  ami  Mr.  Fownes  found  it  to  vary 
from  I  070  to  I'OOO. 

According  to  Fownes  the  juice  has  the  following  composition: — Caue 
Kugar,  u  nutttldti  amount  iA'  grnpe  sugar  w  ^lucose^  gwn  ur  tUxtritie, 
phospfutUs  nf  lime  mul  mttfruejuay  some  othfr  mil  of  the  Mime  ffoxet, 
ndphate»  ami  ehlurifhs^  potnxhiimX  sodtt ;  and  hinlly,  a  peculiar  azntised 
trujffw  forming  an  insoluble  compound  witli  lime,  not  cori^niluhle  by 
heat  or  at'i<U,  and  readily  putreBuble.  <  If  <Nnliiiary  rfgetahh  a//*w- 
men  there  iire  but  indiatiiiot  truces,  and  of  tii.TCiiw?  or  Irgumnif  none. 

The   brown  sti^ar  of  commerce    has   the   lollowing   composition 


I 


I 


SUQAB,   AND    ITS  ADULTERATIONS. 


163 


W 


Although  eonsisiin;;  chiefly  of  cane  or  crystnlltsable  sugar,  it  yet  con- 
tflina  A  good  deul  ol'  glucosf,  and  is  coniaTiiiniitetil  hy  various  organic 
and  mineral  subsunucji.  Acconling  to  Avciiuin  its  tninenil  oonstitU' 
eats  uxe  siticm  pliatpliatc  and  subpliusphatc  of  lime,  carbonate  of 
lime,  luIpUatc  of  putosh,  chloride  of  potasiiiuni,  and  the  acelntes  of 
potssli  and  lime. 

Owiiij^  to  tbe»e  impurities  it  reddens  litmus,  and  is  not  completelj 
dissolved  hy  alcohol;  its  solution  furniidkes  precipitates  with  diacetate 
of  lead,  acetic  acid,  and  rau.«ilic  nnuuDnia,  and  it  ia  frequently 
darkened  by  the  addition  uf  scsquicblnride  of  iron.  By  keepin<;  it  be- 
comes  weak,  that  is  less  sweet,  soft,  clammy,  and  gummy,  —  changes 
ascribed  to  the  action  of  the  lime. 

Ordinary  brown  sugar,  prepared  from  juiec  wliich  has  not  been 
subjected  to  filtration,  contmns  almo^tt  invariably  a  great  many 
fragments  of  the  tis&ue  uf  the  sugar  cane,  sporules  of  a  fungus,  and 
■niniiilcul»?  to  be  described  hereafter. 

From  white  or  refined  sugar  the  above  organic  impurities  ore 
absent. 

The  crystals  of  sugar  are  double  oblique  prisms.     Fig.  52.  p.  184. 

The  foUowinf;  are  the  pr»)pcrtie6  of  cane  siij:ar  ;  — 

It  ia  the  sweetest  of  all  thu  sugars;  when  pure  it  is  white  and 
odourless;  it  is  soluble  in  reclitied  spirit,  but  not  in  etber;  its  watery 
solution,  aided  by  heat,  decomposes  the  metallic  salts  of  copper,  mer- 
cury, gold,  anrl  silver  ;  its  wntcrv  solution  with  yeast  undergoes  the 
vinous  fermentation  ;  sugar  protnoles  the  s<ilubility  of  lime  in  water, 
and  it  f(»rnis  both  a  soluble  and  an  insoluble  compound  with  oxide  of 
lead.  Lump  or  relinetl  sugar  '\s  permanent  in  tliu  air,  and  phospho- 
rescent in  the  dark  and  when  struck  or  rubbed. 

In  the  preparation  of  barley  sugar,  aciduiated  drops,  &c.,  the  c<mfec- 
tioners  usually  add  a  small  (juuutity  of  ereiun  of  tartar  to  the  melted 
sugar,  in  order  to  deslrtiy  the  tendency  to  crystallisatiuu. 

Crystallised  ungiir  melts  at  35G'  P.,  and  at  a  higher  temmrature  it 
begins  to  give  off  water,  and  li>  suffer  decompoitition  ;  ami  if  the  heat 
is  still  more  increased  it  loses  its  swectoe^a  and  becomes  bitter,  when 
It  is  called  burnt  sugar  or  carameL 

Although  mola.sses  and  treacle  are  usually  described  as  the  same, 
it  yet  appears  that  they  are  realty  distinct,  if  nut  in  their  general 
composition,  at  ail  event*  in  origin.  They  both  consiift  of  glucose, 
cane  sugar,  gum,  glulei>,  extractive,  vjtrious  salt*,  and  water. 

MolttxAeit  (Xinnisrs  of  the  ilrainings  Irom  raw  or  Muscovado  sugar. 
West  India  molasses  is  sometinirs  imported  <br  refining,  it  furnishes 
brown  or  bastard  sugar  and  trc*acle. 

Treacle  is  the  syrup  which  drains  from  refined  sugar.  It  has  gene- 
rally a  sp.  gr.  ol  1*4.  Puyen  I'egai-ds  it  as  a  saturated  solution  of 
crystnllisable  xugar,  of  which  it  contains  from  40  to  50  per  cent. 

Cane  sugar  is  distinguished  from  grape  sugar  by  it£  crystaUisabiUty, 

5(   A 


184 


SUGAR,   AND   ITS  ADULTERATIONS. 


iu  greater  swetitness  nnd  sulubilily,  in  b«Ing  reduced  to  charcoal  by 
sulphuric  acid ;  but  beiug  uiicbangcd  when  treated  with  caustic  ptHusb, 


CiTitoli  vf  Cajib  SroAt-   100  dbunsten. 

and  by  the  greater  difficulty  with  which  it  reduces  the  blue  bydratod 
oxide  of  copper  to  the  dtate  of  the  orange  sulKtxide. 

iVnotber  character  by  which  a  solutiun  of  cane  »ugar  is  distinguished 
from  that  of  grape  siignr,  is  tlie  properly  which  it  possesses  of  right' 
handed  circular  polarisation.  / 

On  the  Structure  of  the  Sugar  Cane. 
On  the  Pretence  a/ Fragment*  of  Svgar  Cane  in  Sugar — The  juiw 


LANE  Uu»"mi.  ouuuu^^  ou.iuv 


;>1TY 


SUGAR,  AND  ITS  ADULTERATIONS. 


185 


of  the  cane  is  cxprosaed  by  mc^juis  of  powerful  machlnorjt  and  during 
i\w  operation  iununierabli!  fragment'*  of  the  cunc  itaclf,  uituiy  of  them 
of  extruinc  iixinuteiiess,  become;  dt.*tai;boil,  uiid  puns  ititu  the  juice.  Ai 
this  in  its  nianulaclure  Iiitu  sugar  does  nut  undergo  in  j^eneral  any 
process  of  filtration,  ftod  as  but  few  of  the  franruQcnts  drain  away  with 
the  treacle,  the  greater  part  of  them  are  retained  in  the  stigar,  in  all 
iinfiltered  .sampler  of  wliich  they  may  be  readily  detected  in  great 
ubundunce  by  means  of  the  microscofic. 

Fur  the  more  ready  and  certain  identification  of  these  frao;- 
ments,  it  !s  necessary  to  give  a  sburt  outline  of  the  structure  of  tLe 
sugar  cane  itself. 

The  su^ar  cune  belongs  to  the  class  of  Endogen>,  and  consists  of 
nearly  cybiidrical  rods  or  stems,  which  are  divided  into  joints  at  irre- 
gular distances  of  some  three  or  four  inches,  and  its  structure  is  mode 
up  of  cellular  tissue,  woody  fibre,  vessels,  and  epidermis. 

The  parenehymoy  or  ccUular  tissue^  lorms  lue  most  considerable 
portion  of  the  sujior  cane,  and  it  h  constituted  of  ai^grcgations  of 
infinite  numbers  of  utricles  or  cells,  in  the  cavities  of  which  the  Juice 
is  encb-sed. 

These  cells  ore  usually  rather  longer  than  broad,  and  in  the  central 
ports  of  the  baiuboD  they  are  several  times  larger  than  in  its  outer  and 
border  part;  the  membranes  of  which  the  walls  of  the  celts  are 
forme^l,  are  all  finely  dolled  or  punctated,  a  character  by  which  the 
cells  of  the  sugar  cane  may  be  clearly  distinguished  from  most  other 
vegetable  cells.     Fig.  53. 

The  vootiy  fhre  traverses  the  cane  in  a  longitudinal  direction  in 
distinct  bundles,  which  give  tu  transverse  sections  a  dotted  appear- 
ance. Each  buntlle  is  constituted  of  a  number  of  greatly  elongated 
cells,  and  sometimes  encloties  vessels  ;  these  are  altfo  usually  more  or 
lejM  dottOii,  like  the  ordinary  cells  of  the  p.'irenchymo,  of  which,  indeed, 
l\\ejf  are  merely  niwlificatioits.     F\g.  fi3. 

The  ttMtU  follow  the  same  disposition  as  the  woody  fibre,  in  tlie 
centre  of  each  bundle  of  which  one  or  more  is  generally  included. 
These  vends  arc  of  two  kinds  :  the  one  is  the  interrupted  spiral  or 
dotted  vessel,  and  the  other  the  simple  or  coiitinuoui*  spiral  vessel. 
The  dolled  vessels  ore  sometimes  cylindrical,  but  frequently  |}<>]ygoiial, 
from  tlie  oomprenion  exerted  upon  thera  by  the  woody  fibre,  by  which 
they  are  immediately  8urroun<led,  and  the  markings  of  the  cells  form- 
ing which  tliey  tre<juently  exhibit  on  their  surfaces  :  the  ^f>iral  vessels 
are  fiiund  chielly  in  the  outer  and  harder  part  of  the  stem ;  they 
ore  formed  of  a  single  thread,  remarkable  fur  its  thickness  and  strength. 

The  epidermu  nr  cuticlf  is  known  by  the  elongated,  crenate  colls,  of 
which  it  is  com]Hised,  and  the  presenc*e  of  stomala.  At  the  distal  ex- 
tremity of  each  internode  of  the  cane,  the  ordinary  epidermic  cells 
ore  replaced  or  overlaid  by  a  layer  of  cells,  having  totally  different 
characters;  they  ore  usually  little  longer  than  broadi  more  or  less 


18B 


SUGAR,    AND   ITS   ADULTERATIONS 


rounded  or  oval  iu  shape,  with  tl»eir  edjjes  markeil  with  short  iJTid  w*MI- 
d«fined  lines,  disposed  in  a  radiate  manner  :  these  cells  rei>eiuble  sotue- 

F/g.  M. 


A  fTHftaenlof  SiroAft  CA)rt,ukcii  fVom  neor  tlic  centrt  of  the  ■1cm,  ihowiiit  tht 
liwt  «nd  rhBTscirt  nf  Uip  relti  of  whlrli  lh«  tNmiich<rn>a  it  tunned,  w  tr«||  ■■,  on 
the  left,*  tiirtlle  of  voodjr  fibre.  Urmwti  with  IM  Camera  J.ucldk.  uid  mag- 
uUnl  ino  dlMUMten. 


what  the  celU  found  in  the  stones  nf  fruit,  and  tlicjr  form  hy  their 
union  a  zone  round  the  cane,  polished,  bard,  and  of  about  the  third  of 
an  inch  in  depth.     Ft^.  55, 

Fruginents  of  su^ar  cane  are  present  in  jrreat  (juautity  in  Musco- 
vado sugar,  in  the  sugars  of  the  slio])s  in  general,  and  in  **  bastards/* 
a  prdduct  of  the  manufacture  nf  hnif  sugar. 

They  are  not  coninined  in  lonfuupar,  crushed  lump,  supar  caudy, 
nor  in  ocrtuin  of  the  Knst  Indian  su^iara :  in  the  prup:iriUioii  of  nil 
these  augars  the  cane  jiiioe  underffopa  a  process  of  filtration  which 
effectually  removes  utl  solid  and  bulky  impurities. 

The  presence  of  these  fragments,  in  many  cases,  serves  todistin;piish 
satisfactorily  cane  sugar  frotn  cither  beet,  maple,  or  pmpG  i^ugar,  n 
discrimination  which  otherwise  it  would  be  extremely  difficult  to 
effect. 

By  the  same  meanis  ali»o,  cane  siitrar  may  be  detected  when  mixed 
with  beet,  a  practice  which,  we  believe,  i^i  not  uncotiimnn  in  France. 

The  saccharine  juice  of  the  beetroot  is  filtered,  and  therefore  frag- 


I 


SUGAR,   AND   ITS  ADULTERATIONS. 


187 


mentti  of  thnt  plsint  ore  not  present  in  tbe  sujrar  nuide  from  it,  cis  tbey 
would  doubtless  tw,  were  this  means  of  purilkution  tiuC  nduptcd. 


Fig.b*. 


FrumaiU  of  t1i«SroAH  Civr.  rxhlbtUns  theatnietura  of  lh«  tvokindaof  TtM«la 
•mchcnur  loU>  lu  ctin.(KHitlao,  u  well  u  the  eclU  of  vbleti  the  vootly  llbrt 
lloanvlltBtvd.  n,  /'■<'(»' i^Mrfrinlinldrdia  vnod/Qbrt);  &.  c«lli  of  winvV./'''*^'' 
e,  ^p^rof  rcMti.     D»«n  vlUi  Ute  LuMfK  Luct^«,aiul  mtgtuJUd  3Ui  illiuncun. 

The  presence  of  sugar  cane  in  sugar  increases  the  bulk  and  weight 
of  the  article,  Ie^sen9  its  sweetness,  tend  thus  deteriorates  both  its 
(j^ualitj  and  value. 


Physiological  Action  and  Prvp^rtiet  of  Cane  Sugar. 

Sugar  contributes  to  the  formation  of  fat  an<i  lactic  acid  ;  it  supplies 
material  for  tiie  niaiiitenimce  of  reispinttion  ;  and  by  its  oxidation  it 
furnishes  heat  to  the  syat^^m.  Sugar  and  especially  treacle  have  an 
operient  tentlency. 

In  lS-^3  the  home  consumption  of  raw  sugar  amounted  to  818  mil- 
lions of  lbs  Thiaiseijual  to '28  lbs.  of  sugar  Ibr  each  person  resident  in 
Great  Britain  ;  but  »iiice  the  avL^nt^e  consumption  of  Ireland  is  not 
more  tlian  one  third  llint  of  England,  the  consumption  per  head  iti  tbu 
latter  country  must  be  considerably  over  28  lbs. 


188 


SUGAR,    AXD   ITS  ADULTERATIONS. 


On  THB  Adclteratioms  or  Cake  Sogab. 

Various  adulterations  have  been  stated  to  he  pr&cUsed  on  sugar;  M 
with  potato  augar,  starchy  fptm  or  dextrine^  finely  powdered  marhUj 
chalk  or  whitings  sandy  hone-dust^  and  common  suU. 

Fig.  M. 


'"iS^         -'u   _ 


A  portion  of  the  EriDViuiib  or  ttw  Cxvm,  ahovlng  Ttii  nro  Ktfrm  or  osLLi  of 
which  ft  ■•  eumiHMed  —  vii,.  Iborc  of  which  lli«  (tvotrU  nirfUK  of  Ui«  euie  ii 
Ibrmvd.  «n<l  tJioM  of  which  tti*  |H>li>lml  «onc  drwiibril  (ii  Ilia  teat  i«  chiefly 
eoMtltutwl.    Drftwa  vlUi  Uic  Ca^ncr*  LudiU,  kuJ  m«<ol&etl  Sua  di*inct«n. 

Sugar  bein^  soluble  id  water,  it  is  obvious  that  were  it  to  be 
adulterated  with  any  insoluble  substances,  the  discovery  of  such 
adulterations  would  be  very  enfty  and  certain,  for  the  i>nly  thin^ 
necessary  would  be  to  dissolve  a  portion  of  the  sugar  aud  to  examine 
the  precipitates  which  Hubaidcd. 

We  have  examined  over  100  samples  <>f8ugur,  and  the  only  insoluble 
substance,  excluding  ucfidenlal  imnurities,  whiuh  we  have  met  with» 
has  been  starch,  which  wiis  present  m  smnii  (quantities  in  four  samples- 
There  is,  therefore,  but  little  ibundation  for  the  tales  we  hear  alwut 
the  presence  of  sand  in  sugar. 

Formerly,  however,  when  sugar  was  much  ilearer  than  nt  present, 
it  used  to  be  extensively  adulterated  with  an  inferior  dc^'riptian  uf 


SUGAR,   AND   1T8  AtiULTERATIOKS. 


109 


!tu^ar  made,  from  potato  stnrch  by  the  action  upon  it  of  dilute  buI- 
phuric  acid.     Uut  this  adulteration  ]ia.i,  wc  holieve,  ceased. 

**  A  few  years  ago,"  writes  Dr.  Peroira,  "  I  ins|>ectcd  on  extensive 
manufactory  of  sugar  from  potato  starch  at  Stratford,  in  Kssex  :  the 
sugar  obtainetl  waa  sold  for  the  adulteration  of  brown  euj^ar,  and  the 
mola-'ses  produced  was  consuuied  in  an  oxalic  acid  manufactory."  * 

There  isapractice,  termed  the  "Mixing"  or  **  liandling  "  of  sugar, 
which,  although  not  an  adulteration,  u\i\y  here  be  describetl.  It  consists 
in  mixing  tni^ether,  in  various  nroportions,  8ugar  of  different  qualities 
and  prices, — as  moist  sugars  with  dry  ones,  very  brown  sugars  with 
those  of  light  colour,— the  resulting  article  presenting  a  tolerable  ap- 
pearance to  the  eye,  but  being  rarely  what  it  professes  to  be —  real 
Jamaica  or  Demerara  su^ar. 

In  reference  to  this  subject  some  remarks  from  Ibe  work  of  Dr. 
ScolTem  on  the  manufacture  of  sugar  may  be  qui»te*I. 

•*  If  the  West  Indian  sugar-growers  were  to  be  furnished  at  onoe 
with  a  never  failing  means  of  producing  a  large-grained,  and  there- 
fore an  easily  cured,  sugar,  to  the  exclusion  of  all  uther  sort-t,  their 
produce  would  have  to  encounter  a  diflicuUy  which  the  consumer 
would  learecly  imagine.  Such  large-grained  sugars  ore  very  un- 
faToui*able  to  the  perpetration  of  certain  mysterious  o|)erutions  of 
legerdemainf,  which  gnK'ere  understanil  too  well.  They  will  not 
mix.  A  (imall- grained  sugar  may  readily  be  ineor^ioruted  with 
glucose,  with  pieces  or  bastards,  and  other  less  innocent  bwlies,  with- 
out such  incorporation  being  discoverable  to  the  eye.  A  large- 
grained  sugar,  on  the  other  hand,  is  a  most  refractory  material  for 
tbcfc  little  manipulations ;  its  crystals,  no  matter  how  mingled  with 
contaminating  agentjt,  never  ceaiiing  to  manifest  their  native  bril- 
liancy, luid  thus  proclaiming  the  trnud.  It  is  most  easy,  then,  to 
understand  why  the  grocer,  as  a  rule,  does  nut  encourage  these  large- 
grained  sugars.  He  cannot  '  hantUe  *  them,  and  therefore  brands  them 
witli  a  fault.  He  says  th^y  are  deficient  in  aaccharine  matter  —  that 
they  will  not  sweeten.  True  it  is,  that  comparatively  small  portions 
of  these  large-grained  sugars  ore  sold,  and  cold  at  high  prices, 
but  merely  as  fancy  articles,  on  the  proceeds  of  which  the  grocer  nets 
too  little  to  make  their  sale  an  object  of  primary  solicitude. 

**  Such  is  the  source  of  one  prejudice  again&t  dry  and  large-grained 
sugars  — a  prejudiue  originating  amongst  the  grocer:*.  There  is  also 
another,  which  originates  amongst  refiners,  who  are  adverse  to  the 
general  cousuntptton  of  the^e  beautiful  colonial  sugara,  for  the  very 
ubrioaa  reason  that  the  consumption  of  their  own  staple  is  thereby 
le»6Ded;* 


*  Ur.  SUtrmtm  Cnhilt.  **  t*  tlHrfl  murh  poUto  lusir  fnjule  ?  "— **  A  jrear  nr  two  Mffo,  wtim 
«rer»  illft-unl   poinlfw*,  titefe  nerc  toni   mwlc  in   k  wr**!!  al  vne  ciubliiliment  1 
The  dl»rii>i'  111  tho  pDCalooa  did  not  touch  Ihr  tXAnh. "—Lftkeby  m  F.Tldnicc 
Commlltrc  on  Atlulimiloa. 
f  T«nn«d  bf  grucer>,  "  himatfng." 


»0 


BUOAB,   AND   ITS   ADCLTEBATXONS. 


Now  nearly  all  the  brown  sugars  of  commerce,  altbougb  Tiot  often 
athdieratedy  arc  ^et  in  a  very  iinj^rc  sLate.  Thus  many  ot  them  con- 
tain a  good  deal  of  treacle  and  glucose  i  and  all,  Jragments  of  sugar 
cane^  spomles  of  ajMngwt,  and  aI«o  large  numbers  of  an  insect  termed 
an  acanix. 

The  presence  of  these  vftricus  and  damaging  impurities  is  thus 
explained. 

The  presence  of  the  frojrmenla.of  cane  is  accounted  for  by  the 
cane  juice  not  having  been  liltL'red,  of  tlm  fungus  and  of  the  inRei.'ts 
by  the  fermentation  of  ilie  sugur,  and  the  presence  of  nitrogenous 
matter.  In  sugars  which  have  been  filtered  none  of  these  impurities 
are  met  with. 

Tlie  Sugar  Mite.  —  The  sugar  mite  or  Acams  iacehari  is  in  size  so 
considerable,  that  it  h  plainly  visible  to  ihe  unniiled  sight.  When 
present  in  sugar,  it  may  always  be  detected  bv  the  following  pro- 
ceeding :  —  Two  or  three  drachms  or  teaapounfuls  of  yugar  should  be 
dissolved  in  a  large  wine-glas^  of  tepid  water,  and  the  solution  al- 
lowed to  remain  at  rest  for  an  hour  or  so ;  at  the  end  of  that  time  the 
animalcules  will  be  found,  somt^  on  the  surface  of  tliR  Liquid,  some 
adhering  to  thti  aides  of  the  gla*s,  and  others  at  the  bottom,  ruixed  up 
with  llie  copious  and  dark  sudirnpnt,  formed  of  fni^numLs  of  cane, 
woody  fibre,  grit,  dirt,  and  standi  granules,  wliii'h  UKually  subsides  on 
the  solution  of  even  a  small  quantity  of  sugar  in  water. 

We  will  now  proceed  to  give  a  de^c^ptiun  of  the  acarus  in  (question, 

Fig.bG. 


I 


0*«  •ni  TOnmi  of  Utt  Acampa  •AcxntAii.  or  ttigar  iwm-i.  I>nwti  vlUi  tbe  Oknwn 
LucMa.  uiil  BiftcnlBcd  SUA  dUtncun. 


and  observe,  in  the  first  place,  that  the  whole  of  its  development  may 
be  clearly  traced  out  in  almost  every  sample  of  brown  sugar. 


SUGAR,  AND  1T8  ADULTERATIONS. 


191 


The  Acarfu  sacchari  is  first  visible  as  q  rounded  bodv,  or  eprp; ;  this 
gruduidly  cnl&rgfs  and  becomes  elongated  iiud  c)Uudrica2  until  it  is 


A  9cojlr  Ijiyxrr  or  medium  ilw,  nprcMittJRf  tU  RtUtudt  uiil  «p|>tftranai  wb*» 
sltre,  and  M  ««n  cnwllnc  ita  a  frm;aic&l  of  CMne,  Vtmwa  with  the  Caiaef* 
L,sclda,  uid  mignifird  titti  dlun<rtVT«. 


about  twice  as  Inn;;  oa  broad;  af^er  u  tiinCi  from  i]\Q  nules,  and  one 
extremity  of  this  ovum,  tlic  legs  and  proboscis  begin  to  protrude. 
These  stages  of  the  development  of  the  ncarus  are  ejihibitcd  ia,fig.  50. 

The  oetrufl  thus  far  formed,  goes  on  inerensini;  in  size  until  it 
attains  lu  full  growth,  when  it  is  visible  to  the  naked  eye  as  a  mere 
speck. 

In  its  perfect  state,  its  structure  is  as  follows :  —  The  bo«ly  is  oral,  or 
rither  somewhat  ovule,  being  broader  behind  thun  before;  from  its  pos- 
terior part,  four  long  and  slIlV  bristles  proeee<l,  two  togutht-r  on  each 
side;  and  some  eight  or  ten  smaller  ones  are  arranged  nearly  at  e'|ual 
distances  around  the  circumference  of  the  iKxly  ;  from  tin  anterior 
part  a  proboscis  of  complex  organisation  proccedia,  and  from  itti 
inferior  suri'ace  eight  legs,  jointed  and  fumi-thed  with  spines  or  haira 


iOS 


SUGAR,   AND   ITfi  ADnLTERATIOKB. 


at  eaph  articulation;  the  spine  which  issues  from  the  lost  joint  but 
one  of  each  leg  is  very  long,  and  extends  much  beyond  the  termiiia- 

Ftg.  M. 


lopmcnt,  and  M  It  frtHjiunitj  kpiw^n  when    iU«d.     Ilrawti  wltli    itM  CsfoAim 
LodJft,  and  macniftrd  IP")  iliamtUrf. 

tion  of  the  leg  itself;  lastly,  each  leg  is  armed  at  ita  extremity  with  a 
formidable  hook. 

Manr  of  the  above  particulara  are  faithfully  exhibited  in  the 
eneTavingiL 

In  most  samples  of  sugar  the  iicari  may  be  seen  of  all  sizes,  that  is, 
in  all  the  stages  of  their  growth  and  in  every  condition  ;  some  alive, 
others  dead ;  some  enttrCf  and  others  broken  into  fragments  ;  bodies 
bere,  legs  there. 


SUGAR,    AN'D   ITS  ADt'LTlCRATIOKS. 


193 


^ 


We  hnve  said  that  the  sugar  mite  is  very  commonly  present  in  ibe 
less  imi'tt  su^um  —  wc  mijihi  have  asserted  that  ft  is  tUnioiit  eonsLaiitly 
»),  the  »(tateiiient  being  bn»ed  ujton  the  exauiiDHlion  of  nut  less  than 
one  hundred  diflc*rciit  samplt^s  of  sugar. 

A»  II  rule  the  number  ofacari  present  in  any  Fam])le  of  suprar  may 
be  taken  as  a  fair  indication  of  the  purity  of  that  sugar;  the  purer 
the  sugar,  the  freer  it  will  be  from  the  9u;j;ar  mit«. 

Grocer/  Itch.  —  It  is  well  known  thut  grocers  are  subject  to  an 
aAcctiun  of  tbe  skin,  denontinatcd  *' grocers'  itcV'  of  which  one  of 
the  sTmntonis  is  extreme  irritation  and  itchmg. 

To  this  disease  all  {:rnK:ers  are  not  equiilly  Uiible,  but  those  more 
particularly  who  are  en^^aged  in  the  **  handling  "  of  the  sugars,  as  the 
warehousemen. 

Now  the  Acarus  xacchori  actually  bt*lnnj»«  to  the  same  genus  as  the 
^rarw*  jrcr/AiVi,  or  itcli-insert^  tluin  whinb,  however,  it  is  larger,  and 
possessed  of  an  organisation  still  jnorc  formidable. 

It  thus  beeomes  extremely  probable  that  tbe  disease  in  (]uesti<m 
does  really  arise  from  tbe  sugar  acarus  —  a  point,  however,  which 
notbin<;  short  of  microscopic  observatiun  can  satisfactorily  determine. 

On  SporuleM  of  Futi^i  in  Sugar.  —  Innumerable  sporules  of  fungi 
are  very  generally  to  l>e  observed  in  the  less  pure  kinds  of  sugar; 
they  i>ct-ur,  indeed,  most  abundantly  in  those  sugars  which  favour  the 
development  of  the  Acari. 

Thev  are  best  seen  by  dissolving  a  small  quantity  of  any  brown 
sugar  ID  water,  and  looking  fur  tbem  in  tbe  sediment  which  «ub:tides, 
and  which,  to  a  greftC  extent,  is  constituted  of  the  sporutes  in  ques- 
tion. 

These  s[K>ruIes  are  exceedingly  minute  bodies;,  usually  of  an  oval 
form,  and  either  fluaiing  uinirly  in  the  sugar  solution,  or  else  adhering 
together,  and  thus  (brminj:  little  beaded  threads.  Under  favourable 
circumstances  the  s[M)ruies  become  developed  into  perfect  plants  or 
fungi. 

Another  impurity  very  frequently  met  with  in  lump  sugar,  consists 
nf  mittuie  amvdust-iike  fragutcntiy  nnl  only  of  deal,  but  also  of  other 
woods;  tbcy  ffflen  occur  in  great  abumUncu,  and  of  their  presence  it 
is  not  easy  to  give  a  satisfactory  expUnatinn.  Possibly  they  are 
ilerived  from  the  board  on  which  tlie  loaf  sugar  is  broken  into 
lumps. 

Out  of  M pent y 'two  sampIeM  oT  brown  ntgar^  as  procured  at  diflerent 
shopa,  subjected  toexamination,yr^m/?iii/«<»/'«Ufl'ar  C4iHe  were  present 
in  ail  but  one.  These  were  usually  so  arauU  that  they  were  visible 
only  by  the  aid  of  the  microscope. 

SponUet  and  JUamentt  of  fw*gug  were  present  in  nearly  all  the 
stigars. 

The  acari  were  present  in  sixty-nine  of  the  sample**,  an<!  in 
many  in  very  conniderable  quantities. 

Grape  SMgar  was  detected  in  all  the  sugars. 


fffiOARy   AND    ITS   ADULTEKATIOKS. 

turn-  pr  lliv  Mignrfl  roiitnined  proportions  of  darch  so  consit 
t4t  Iktnil  tti  ilit>  inftTencc  that  thejr  were  adulterated. 


s-.^^O 


v.-.^^VS 


■f  iht  Vbnoi'i  nmiiil  In  bmwn  Mnr.     I>raWTi  with 
ftwl  niviralflcd  w  dluncUn. 


Cunerm  LaddA, 


Klt'vcn  iilIiiT  «aiii})l('H  of  lirown  au^nr,  as  imported  from  tlie  East 
iitxl  \V»'"t  Inilii'ji,  fiir!il»ln*4i  neurly  simiUr  rcsuhs.  Two  only  could 
Itit  ii'ffiii'tliMl  iiK  piir(<  uiu)  (it  t'lir  liiiiunn  cnii-tumptionf — a  white,  large- 
^lftllM<ll  C'utruitu  ttii^iir,  n'Mt'tiihli.i<^'  cniNliL'^l  lump  ;  and  a  pale  slraw- 
I'liliHirtMl,  lar^o-^niliKMt,  hiijlilv  rrvKltillini'  8ii;;ttr  fruin  Cussipore. 
Itoth  llii<»o  vii^iira  hud  im  *}nuUi  hi<i-ii  iuaxIv  fruju  jtiicu  purified  hj  fil- 
tratlon. 

Tho  rosulla  of  Iho  examination  »i  Jiftetn  tampleg  of  lump  tvgar 
wi»r«»,  ■ — 

1'hit  in  none  of  the  Rugara  wcro  A*agmcrita  of  cane  present. 

'j'lut  It)  ihrvo  uf  Ui»  MugarR  only  were  tracca  of  gnpe  sugar  to  be 

That  in  no  east'  wcro  acart  observed. 

That  in  none  uf  th«  sugars  wvrv  Bporules  and  threads  of  Aingi 
vinible. 

It  hhji  nuw  Ih'cii  dliown  thiit  the  inajoiity  o{  brown  sugars,  al- 
though not  udultoiattnl,  are  yet,  as  imporiod  into  this  country  and  as 
vended  to  the  public,  in  an  exceedingly  impure  condition. 


SUGAR,   AKD   ITS  ADULTEKATIOKS.  195 

Those  impurities  prevail  to  such  on  extent,  and  are  of  such  a 
nature,  —  consisting  of  live  unimalculse  or  ocari,  sporules  of  fungus. 


I  vt  maady  flhn  of  tfae  Fia.  ahcnrinc  iU  itruelura.    Dmwn  with  Uif 
CuHcm  LndiU,  «ik1  mafalflra  9Xi  dluaelcnk 

(jrit,  woody  fibre,  &c.,  —  that  we  feel  compelled,  bowcver  rcluctantljr, 
to  come  to  the  conclusion,  that  the  bnywn  nugars  of  commerce  are^ 
in  fiertfrrat^  in  a  ttate  unJU/or  ftumatt  coimttttplion. 

We  stronglj  urge  the  sugar  refiner  to  prepire  cheap  fomu  of  puri- 
fied sugar,  in  powder,  analogous  to  crushed  lump;  such  sugars,  we  are 
informed,  sre  extensively  cmploye<l  in  Scotland,  and  we  doubt  not 
but  that  tbejr  would  meet  with  a  Urge  and  ready  sale  in  tbis  country. 


On  the  Detection  of  the  Adidterationa  of  Sugar, 


tTbe  adulteral  ions  which  either  are   or  have  been  practised  upon 
sugar  are  tbote  with  ttarcb  and  starch  sugar. 
Otber  articles  aIU*g\M)   to   have  been    used    for    its   adulteration 
o  a 


196 


SUGAR,   AND    ITS  ADCLTERATIOXS. 


lire  cjum  nr  rlextrinc,  chalk  or  wliiling,  pypsum,  sand,  bnne  dust, 
and  i-ommnn  sidt.  Tln*?e  siibstanccf,  e^tcept  ihe  piim  and  salt,  are  all 
iiiHoluble  in  water:  tur  lljL'tr  supanillDn  nm\  idenLifictition  nothing 
more  in  y**nera!  wuuld  bt?  necessary  than  to  dis!«(ilve  a  portioii  of  the 
sugar,  liy  allow  the  precipitate  to  subside,  and  to  examine  it  with  the 
eye,  and  occnsinnally  by  chftnical  reagents. 

If  the  precipitate  he  earthy,  and  h\  on  ndilinfza  little  nitrate  of  silver 
to  a  portion  of  it^  it  turns  yeltow^  it  eoninists  in  all  probability  of  hone 
dust  orphospliate  of  lime  :  if.  on  the  addition  of  «n  ai-id,  it  effervesce, 
iC  then  cimsists  of  curbonatc  of  lime,  or  chalk  :  should  cfirbonic  acid 
not  be  eToJlve<i,  we  mny  then  test  for  gypauni :  if  the  preci[iitAte  is 
coinpoM^l  nf  sanil,  it  may  at  nnre  be  idciititied  by  the  eye  alone. 

For  the  estimation  of  the  ahnve  siibstnni-e^  ipiantitativelv, — rarely 
required,  howrror, — awt-ighed  portion  of  the  juijrnr  shoultl  bi*  dissolved, 
ami  the  proeipiute,  after  being  dried»  shimld  it^jelf  be  weii:lu'd.  IJut 
as  in  a  solution  of  Augur  part  ufthe  Ituie  iii  held  di»Rolved,  in  this  casc 
it  is  better  to  estiuiate  the  iiuantity  of  ihiit  present  from  the  ash  ; 
thia  is  effeuted  by  the  proeeys  deseribt.'d  under  tlie  beat!  of  Tea. 

Stilt,  when  present,  which  it  rurely  is,  must  likewist.'  be  estimated 
from  the  a^h :  a  solution  of  tbix  in  distilled  wuter  diu:«L  be  made,  and 
the  chloride  of  silver — precipitated  by  solution  of  nitrate  of  silver  — 
formed  nnist  be  collected,  dried,  and  weiched,  and  the  chlorine  con- 
tained in  this  calculated;  thia  again  must  be  esiimated  for  cldoride  of 
sodium. 

If  the  EUgar  is  adulterated  y^Uh  gwn  we  must  proceed  as  follows: 
the  8ur;nrniu8t  be  dissolved  out  by  means  uf  reclined  spirit;  the  gum 
will  be  Ufl  behind. 

Farinaceoajt  mtbitancen  may  be  thus  detecte*! :  —  The  sugar  must  be 
dissolved,  the  precipitate  examined  with  the  microscnpe,  and  (he 
characters  of  theitnrrh  cnrfiuMrles  noticed.  I^oiled  starch  is  scarcely 
likely  to  be  em|iloyed;  but  if  so,  a  precipitate  wmilil  still  oi-pur  in  a 
solution  of  suj^ar:  in  this  the  remains  of  the  stnrch  coqmscles  would 
stilt  be  visible,  and  with  iodine  it  would  luni  blue.  For  the  <|uanli- 
tative  estimation  of  sLarefa  or  farinaceous  substunce^  the  precipitates 
must  be  dried  and  wei;.'hed. 

Dextrine,  a  subntance  internie<liatc  in  its  character  between  gum 
and  starch,  is  detected  by  t^'Sting  a  solution  of  the  su^'ar  when  cold 
with  iodine,  which  gives*  a  purplish  colour,  and  abo  by  the  characters  of 
the  remnants  of  starch  corpuscles  still  visible. 

Lastly,  we  have  to  consider  the  n)cans  by  which  the  adulteration 
of  cane  with  starch  sugar  may  be  discovered. 

Starch  sugar  is  one  fonu  of  grape  sugar;  and  since,  as  we  have 
shown,  grape  sugar  is  piesent  fiom  natural  causes,  in  greater  or  lees 
amount,  in  all  the  brown  !iu^ars  nf  enmmerce,  it  is  evident  the  analysis 
necessary  to  enable  the  chemist  to  state  whether  a  sugar  is  adullentted 
vtth  Btareh  sugar  or  not  must  be  a  quantitative  one,  and  that  he  is 
only  justified  in  concluding  that  a  sugar  is  adulterated  with  that  <<ub- 


I 


6UGAB,    ANP   ITS  AT>ULTEnAT10N8. 


197 


Btnnce  wlten  the  nro[>orlion  discovered  forms  a  considerable  per-centage 
of  the  whole  artK-]e, 

The  teaU  ortiinurily  employed  for  the  detection  of  grape  sugar  are 
Trummer'sorthe  copper  test,  anil  the  potash  orMoore's  test.  A  solution 
of  grape  sugar  to  which  a  solution  of  causiir  potash  has  been  added  in 
excess,  when  boiled  becomes  of  a  deep  rich  brown  colour. 

Troaimer*8  te^t  consists  of  sulphate  of  copi>er  and  liquor  pota^sv. 
When  ttiesti  are  added  in  certain  proportions  to  a  doluiion  <ii'  pmpe 
sugar,  and  hent  is  a[>plied,  the  red  suUixide  of  copper  is  thrown  down. 

Several  nibilificationB  of  thU  test  have  been  suggested  ;  the  most  im- 
portant of  thcrn  U  that  which  is  called  Febliug'a  te^t. 

There  are  two  method:*  by  which  the  quantily  of  grape  Bugur  is 
determined. 

By  one  method  the  quantity  is  eslimnted  from  the  nnmnnt  of  a  80- 
lutiuo  of  deliniie  strength  required  to  precipitate  all  the  sugar,  a 
certain  measure  of  the  solution  corrcspondiu;;  to  one  grain  of  su^^ar. 

By  the  other  metho<l,  the  sugar  i»  calculated  from  the  suboxide 
precipitated,  the  solution  being  added  in  excesa 

'Xlie  copper  test  is  usei)  qu»tit;itivcly  in  the  following  manner  : 
—  A  drop  or  twi>  of  a  soluliou  of  sulphuiL*  orcnp[M.'r  is  ad<led  to  the 
solution  of  sugar,  then  solution  uf  caustic  potash  in  excess,  and  the 
mixture  boiled,  heat  being  applied  to  Ihe  up[>er  part  of  the  mixture 
in  the  test  tube. 

Fehltng's  test  litmor  is  prepared  as  follows : — 

Dissolve  69  giams  of  pure  crystallised  sulphate  of  copper  in  27(» 
grains  of  distilled  water  ;  to  this  add '276  grains  of  a  saturated  solution 
ol"  tartrate  of  pcitAjih,  then  add  80  grains  of  hydrnte  of  soda,  previously 
dissolved  in  one  ounce  of  distilled  water ;  shake  all  well  together, 
■nd  iutnxluce  the  liquor  into  a  vessel  capable  uf  holding  2000  grains, 
graduated  into  1000  equal  parts,  and  nil  up  with  df.<4tilk'd  water. 
Kvery  200  grain.H,  or  100  parts,  of  ibis  lest  liquor  are  sulUcient  to 
decompo.4e  one  grain  of  glucwe.  It  is  best  to  add  excess  uf  the 
solution,  and  to  weigh  the  red  suboxide  thrown  down. 

in  this  cose,  the  solution  of  sugar  to  which  excess  of  the  test 
solution  has  been  added,  sliould  be  gently  heated  on  a  sand-bath,  till 
the  suboxide  has  subsided  ;  this  should  be  collected  by  decantation, 
washed  with  boiling  water,  dried  and  weighed,  and  the  sugar  deiluced 
from  it.  One  hundred  parts  of  anhydrous  grape  sugar  corresponds 
to  198*2,  or,  according  to  Neubauer,  *J01  62  of  suboxide  of  copper. 

In  employing  the  test  quanltLaltvel^,  the  sojkiion  muni  be  added 
tittle  by  little,  until  no  further  precipitute  of  sunq^^e  occurs. 

The  solution  should  be  kept  in  a  dark  place;  ami  if  it  has  been 
made  for  any  time  bufure  usin^  it,  it  should  be  boiled  with  water  in 
the  proportion  of  one  part  of  the  solution  to  four  of  water.  If  this 
operation  cau^iea  the  separation  of  even  the  snuillcst  quauUty  of  sub- 
oxide, the  solution  is  unGt  for  use. 

o  3 


198 


HONEY,   AND   ITS  ADULTERATIONS, 


The  sDgar  solution  should  be  ver^r  dilute,  and  not  couiain  more 
than  one  ptr  cent,  oi'siiifar. 

It  mu9t  be  rememb4>rcd  lliat  the  DeparatGd  suboxide  of  copper  will 
grudually  diMoIve  in  ibe  supernatant  liquor  as  soon  as  tbis  becomes 
cold,  as  oxide,  into  wliicb  it  Is  converted  by  the  oxypen  of  the  at- 
mosjihero,  ami  henoe  tlie  necessity  of  washing  the  preci|>itftte  by  de- 
cuntfttion  in  bujljug  water. 

In  this  nrtiele,  as  in  tea  and  coffee,  the  war  not  onlyarrcsted  the  fall 
of  the  duty,  but  occasioned  a  retrogressive  move.  The  scale  of  duly 
on  ail  sucRr  alike  is  now  :  — 


TflIMh«rAt>ril. 
lUT. 

TUI  5ili  uT  Aprfl. 

ThmiAn. 

Candjr,  Brown   or    Whit* 

£   1.  4. 

J.   d. 

X.   d. 

rcHaod,     or    uiy    «<iua1 

In  quality  ihcn-to  ■ 

I    0  y 

16  e 

13     4 

Whitr  cU>ed  at  muaI.  but 

nM  eq-il  rtrflned    - 
VpIIow  MtufOTadu    - 

17    6 

H    7 

11     M 

IS    0 

19    9 

10   s 

BrowQ           ,.            -        - 

13    'J 

11    B 

9  e 

M«1m*m   .... 

ft    A 

4    « 

3  d 

Connumption  ofaU  Sort*  in  18/S4, 
Unrefined     -  -  .  -     8,100,423  cwts. 

Refined  .  -  -  -        304,128     „ 

Molasses        -  -  -  .        929,811     „ 


In  1855. 


Unrefined 
Refined 

Mulas^ea 


7,306,029 
:288.751 
921.574 


Nine  ManUu  of  1«56. 

Unrefined      -  -  .             -    5.463,488     ,. 

Refined          -  -  -             -        215,918     „ 

Moliisses         -  -  .              -        684,638     „ 

Being  all  lower  than  the  same  months  of  1855,  owing  to  higher 
price  and  hf^ht^r  duty. 
A 


HONEY,  AND  ITS  ADULTERATIONS. 

lIoNET  consists  of  the  saccharine  exudation  from  the  nectaries 
flowers  collected  by  the  bees,  and  modified  and  elaborated  bv  them 


HONET,   AND   ITS  ADtLTERATIOXS. 


199 


in  the  crop  or  honey  bflc,  which  is  an  expansion  of  the  (ESOphaj»us, 
and  from  which  it  la  dist'tiargeii  on  their  return  to  the  hivc^  and  de- 
posited in  the  various  cells  of  the  comb. 

It  consists  oferape  sugar,  manna^  ^f**  mucilage^  extractive,  a  little 
wox,  pollen^  acid,  and  odariferoua  substances. 

lloucy  usually  consists  of  two  parts,  one  lluid,  the  other  solid  and 
crystalline.  By  pressure  in  a  linen  bag,  these  niny  be  sepnrated  from 
each  other,  a  clear  syrupy  substance  passing  through  the  linen,  and 
the  white  solid  su^ar  remainine  behind. 

"  Both  the  solid  and  liquid  sugars  hare  the  same  general  pro- 
perties. Tbey  are  hi)th  equally  sweet,  both  have  the  saun;  chemical 
composition,  and  both  begin  to  ferment  when  water  and  a  little  yeast 
are  added  to  Ihem,"  —  Johnston. 

In  old  honey  the  proportion  of  solid  sugar  is  the  greatest. 

"The  solid  su;jar  of  honey  is  probably  identical  witli  the  sugar  of 
the  grape;  the  liquid  sugar  differs  from  the  solid,  chiefly  in  refusing 
to  crystallise,  and  in  contuininnr  an  admixture  of  colouring  and  odori- 
ferous substances,  prtxluced  by  the  flowers  from  which  the  bee  has 
extracted  it." — Johnston. 

The  honey  which  flows  spontaneously  out  of  the  comb  on  the  ap- 
plication of  a  gentle  heat,  consists  entirely  of  the  fluid  portion,  and  ia 
called  virgin  honey,  while  ordinary  lioney  is  pri^u-ured  both  by  pres- 
sure and  beat.  The  first  honey  collected  by  bees  is  also  soiuetinies 
called  virgin  honey. 

To  the  various  fnreitiin  substances  containedin  it,  including  especially 
pollen,  the  different  colours,  flavours,  and  o4lours  possessed  by  the 
noney  of  different  countries  and  diairicts  are  owing,  and  the  possession 
uf  which,  in  some  euse$,  causes  it  to  bo  so  highly  prized.  *^  Hence  the 
eslimation  in  which  the  honey  of  Mount  i<lH,  in  Crete,  bos  been 
alwnys  held.  Hence  also  the  perfume  of  Narbonne  honey,  of  the 
honey  of  Chamouny,  and  of  our  own  high  moorland  honey,  when  the 
heather  is  in  the  bloom.  Sometimes  the.se  foreign  substance!*  possess 
narcotic  or  other  dangen>u.i  qualitieH,  as  tn  the  case  with  the  Trebizond 
honey,  which  causes  headache,  vomiting,  and  even  a  kind  of  intoxi- 
cation, in  those  who  eat  it.  Thid  quality  is  derived  from  the  flowers 
of  a  species  of  rbododentlron,  Azalea  poiuica^  from  winch  the  honey  is 
partly  extracted.  It  wa«  probably  thio  kind  of  honvy  wbiub  poisoned 
the  soldiers  of  Xenophon,  us  described  by  him  in  the  Retreat  of  the 
Ten  Thousand." — Johnston. 

The  solid  part  of  honey,  examined  under  the  microscope,  is  seen  to 
consist  of  myriails  uf  regularly  formed  crystals  ;  these  crystals  are  for 
the  most  part  exceedingly  thin  and  transparent,  very  brittle,  so  that 
many  of  them  are  broken  and  imperfect;  but  when  entire  they  con- 
sist of  Kix.-sided  prisms.  They  ap|>ear  to  be  identical  in  form  with 
those  of  cane  BU^'ar,_;%»'.  52.  p.  IH4. 

Intermingled  with  the  crystals,  may  also  be  seen  pollen  granules  of 
different  forms,  sizes,  and  -ftructure ;  these   are  in  such  perfect  con- 

O  A 


200 


HONEY,    AM)    ITS    ADULTERATIONS. 

dition,  that  in  miiny  cii5e9  xhey  mar  be  referred  to  the  plants  from 
which  the  honey  bus  been  procured.     This  'a  a  very  intcrc^iing  and 


i^fii. 


CrTftAUof  lIo](«r,  InlcnvlanlvithUit  pr\l\at  (naolwrnf  the  flower*  fti>ni«bl«li 
Itic  Hwurjr  wu  gftUwmL    MAgnlflsd  Xll  tUmmctcrv. 

kutiful  fftct  in  relation  to  honev  Tliebces,  in  coHccting  the  li»af^ 
from  the  flowers,  carry  away  with  them  also  some  of  the  {>oU>'ii  "> 
those  ilowers ;  now  this  pollen  consists  of  complex  utricles  oi  cvtt*- 
difieriug  in  Hize,  shape,  and  orgnnis:ttion  in  diOereiil  orders  of  plinis 
and  iu  different  plants,  so  tlint  the  ob»erver  aci^uuinled  %kitb  th': 
characters  of  the  pullon  of  flowering  planu,  will  be  enabled  in  m'Q.i 
C4ue9  to  determine  wbeth*  r  any  Dartiinlar  honey  subinitled  to  bn 
examination  wa«  collected  from  flowers  of  foreii:n  or  native  gnwlb. 
whether  from  those  of  the  field,  the  garden,  the  hcathi  or  the  luountais- 


HONKT,   AND   ITS   ADULTEUAT10X8. 


aoi 


It  has  occurred  lo  ilie  author,  to  ranke  nnoilier  highir  interonting 
observatiuii  in  connwtioii  witli,  honoy,  showiiiy,  iii  a  very  sirikinj; 


tthomjt  by  thipt*f«nMef  nqntnof 
inutnle*  of  the /mnt  mtui  of  AeuM  :  a,  M^pullcn  gnnultB  of  fern  t  K^, 
tw*lh  i  r.  e.  •lltw  of  hmuc  ctunyMlu  flowvr.   Th«  oUwr  gnnuki  prmtol 
W«  bftvi  DM  i(lt«Ua«d. 

manner,  tlie  amazing  industry  maniAistcd  by  beta  in  llie  collection  of 
honey.  In  examining  the  bloMonis  of  our  native  heaths,  some  two 
or  three  years  since,  wc  were  surprise*!  to  oboerve  that  there  was 
ftcarcely  one  thai  had  arrived  at  muturity  that  did  not  exhibit,  usu- 
ally on  the  upper  surface  of  the  coroUa,'  one  or  more  djirk  opots, 
occasioned  by  |>erf<)mlioiu.  The  conjecture  at  once  occurred  to  us, 
thftt  these  perforations  were  made  by  the  bees  in  their  seorcb  for 


HONEY,    AND   ITS  ADULTERATIONS, 

honey,  and  in  order  to  racilitace  its  abstraction  from  the  tubular- 
sha[M;<Ul(3wep8.  It  was  not  lung  bufnre  the  cnrrectneaa  of  lii is  con- 
jecture was  ast-ortaiued.  TIte  bees,  on  ali<;htiii;;  on  the  flowers, 
almost  constantly  inserted  their  prnboscea  either  through  one  of  the 
apertures  already  ninde^  or  tliey  jiieroed  a  fresh  one.  Now  of  the 
Lountless  myriads  of  blossoms  in  some  miles  of  hfttth,  there  waa 
scarcely  one  mature  one  observed  by  us,  which  bod  not  been  perfo- 
rated. 

A  very  good  way  ofobtnining  thu  pullc^n  of  honey  for  microscopical 
examination,  in  to  di^j&ulve  a  tenspounl'ul  or  t^o  of  the  honey  in  water 
contained  in  n  conical  glasjs  and  to  examine  u  little  of  the  sediment 
which  subsides  in  the  course  of  a  few  minutes,  and  which  in  some 
honeys  is  very  considfrable.  The  water  causes  the  forms  of  the  gra- 
nules to  change  in  some  cases,  and  hence  a  better  plan  is  to  view  the 
pollen  as  containeil  in  ihe  fluid  part  of  the  honey.    . 

Jn  thu  "'Annals  of  Natural  History  "  will  be  found  an  article  by  the 
author,  illustrated  by  a  large  numbiT  of  figures,  on  the  rtnictureof  the 
pollen  granule  ;  this  w-dl  bi;  fuun<l  of  some  assistance  to  thost.*  who  raaj 
desire  to  identify  the  jjoUcn  faund  in  honey.  Another  useful  plan 
of  proceeding  is  to  collect  and  exnmtiiie  the  huney  of  tho  (lowers  from 
which  the  bees  are  siipjiosed  lu  hHve  coUeoteil  tho  honey,  and  to 
search  in  this  for  the  corresj>onding  pollen  granuloa. 

Tbk  Adultkxatiox.*(  or  Honey. 

The  more  usual  adulterations  of  honey  are  wilh  various  forms  of 
starchy  as  those  of  the  patulo  and  wheaty  and  with  $inrch  and  cane 
ntigars. 

Other  adnlterations  mentioned  by  Mitchell  and  Normandy  are 
chalk,  plaster  of  Fans,  ami  pipe  clay. 

The  starch  is  not  only  added  for  the  sake  of  weight  and  bulk,  but 
to  improve  the  colour  of  very  dark  honey,  and  to  correct  a  sharp  and 
acidulous  taste  which  old  honey  is  apt  to  acquire. 

On  the  Detection  tifthe  Adtilieratioiu  of  Honey. 

Of  the  adulteratiotis  prnriised  upon  honey,  some  ore  very  easy  of 
detection,  and  others  ditlicult,  if  not  impossible. 

The  general  method  of  pnicei-'din;:  in  the  examination  of  honey, 
with  a  view  ^odie^^ovL'^  whether  it  is  a-iluUtTiited  or  not,  is  as  follows:  — 

A  little  of  the  honey  is  to  be  examined  under  the  microscope,  when, 
if  it  contain  unboiled  starch,  (he  gi-anules  will  be  visible,  and  may 
be  identified  by  the  characters  which  they  present.  If  none  are  to  be 
seen,  a  sumll  (juanlity  of  tincture  of  iodine  is  to  be  added,  which  will 
show  whether  starch  is  present  or  nnt  in  any  lorm. 

The  starch,  as  well  as  any  insoluble  and  inorganic  material  which 
may  be  present,  may  also  be  discovered  by  dissolving  a  portion  of  the 


HONEY,   AND   ITS  ADULTERATIONS. 

The  ailullerations  of  booey,  the  discovery  of  whicU  U  more  difficult, 
nre  tliciae  with  cuiie  and  ^n^pe  sugar. 

Cane  sugar  becomes  charred  on  the  addition  of  sulphuilc  acid,  and 
it  is  stutod  that  gmpe  suj^ar  does  not  ;  this  dititiiietion^  however, 
does  uot  apjdy  to  honey,  for  it  becomes  charred  equally  with  cane 
su^ar. 

There  are,  however,  three  ways  in  which  the  presence  of  omc  m^r 
in  hmioy  may  be  determined,  two  of  them  beiii^  supplied  by  the 
Diiorox'opt:.  The  first  ja  by  the  size  and  e-peciallv  by  the  thickness  of 
the  crystals  of  sugar ;  their  shajH;  is  essentially  the  same  as  those  of 
honey.  The  rrywtuls  of  cane  sugar,  as  fcmnd  in  honey,  ditFer  from  those 
of  that  substance  In  beinp  much  larj^er,  thicker,  and  in  their  less 
regular  shapes  ;  the  angles  being  acted  upoo  by  the  fluid  part  of  the 
honey,  and  in  part  melted  down. 

The  second  is,  Biipposiug  brown  sugar  to  have  been  used,  by  the 
presence  of  the  sugar  acari,  di^eeniible  either  on  the  surface  of  a 
solution  of  honey  in  water,  or  in  the  residue  deposited  from  it. 

The  third  method  is  chemical.  Grape  is  sepuraicd  from  tlic  cane 
sugar  by  means  of  Febling's  solution;  the  sngnr  which  remains  is  of 
course  cane  sugar:  it  may  l)e  procured  in  a  state  of  purirvj  hy  means 
of  alcohol,  from  the  residue  left  on  cvaiioration.  This  method  must 
be  resorted  to  in  those  cases  in  which  the  cane  su;i:ar  has  been  added 
in  the  state  of  syrup,  and  when  in  consequence  iUt  crystals  are  thus 
destroyed. 

There  are  some  other  methods  of  discrimination  :  one  of  these  la  by 
the  aid  of  the  optical  saccharnmeicr  of  A!.  Biot. 

Another  is  the  process  of  M.  Pcli^ot.  This  consists  in  a  saturation 
with  sulphuric  acid  after  the  combinalitm  of  sugar  in  the  cold  with 
lime,  and  which  is  repeated  after  the  boiling  of  another  portion  of  the 
same  liquid.  The  diOerence  between  the  quantities  of  acid  neitessary 
to  saturuiioii  before  and  after  boiling  indicates  the  prOfHirtions  of  glu- 
cose. 

A  very  simple  prncess  indicated  hy  M.  Paven  in  his  work  entitled 
"Des  Substances  Alimentaires.'^andemplnyed  in  most  sugar  refineries 
in  France,  "  consists  in  washing  the  rough  or  moist  sugar  with  alcohol 
at  85°,  lightly  aiidutateil  with  five  liundredths  of  acetic  acid,  and  sa- 
turated with  sugar-candy.  The  liquid  dissolves  the  sugar  of  starch 
and  the  unerystidiisable  sugar,  white  it  dues  not  attack  the  crystals  of 
cane  or  beet  sugar." 

The  adulteration  of  honey  which,  so  fpr  as  we  are  aware,  it  ia 
scarcely  possible  in  many  cases  to  detect,  is  that  by  aiarch  angar^  since 
this  possesses  the  same  chemical  properties  as  the  sugar  of  honey. 
Afl  glucose  is  usually  made  hy  biviling  with  sulphuric  acid,  and  as 
the  excess  of  this  is  soraeiimea  neutrnlirtfd  with  chalk,  the  presence 
of  considerable  quantities  of  sulphate  of  time  affords  strong  evidence 
of  adulteration  with  sugar  of  starch. 


MILK,   AND   ITS  ADULTKRATIONg. 


305 


^ 


milk;  and  its  adulterations. 

If  the  testimonj  of  ordinary  observers,  and  even  of  mnnj  scientific 
writers,  is  to  be  ureJited,  there  are  few  aitii-ltis  offooil  more  liable  to' 
atlullerfttion,  and  tliis  uf  the  grosysest  UesiL'riptimi,  ihuninilk;  but  before 
proceeding  to  refer  to  the  adulleratioos  of  milk,  it  nill  be  {«ro|>er  to 
tre.il  of  its  L*onipu*ition. 

From  Oie  fuct  tliai  persons  may  be  entirely  sustaJiieil  u|>on  a 
diet  of  milk  for  nn  intb'tinile  period,  it  may  be  noiiclijttetl  that  that 
fluid  mudt  rontaiti  all  llie  element:^  net'essary  for  the  grovvih  and  sus- 
tenance of  the  human  body,  a  view  the  correcluoss  of  u hioh  is  fully 
eitablisbcd  by  cheiuicul  reciearcli. 

Composition  of  Milk. 

Milk  consists  of  tcaUr  holding  in  solulion  caaein  or  cheese^  sugar  of 
milk,  various  salts^  iind  in  susneitsion,  /ut/y  matter^  in  I  be  form  of 
mvrinds  of  semi-opaque  globules,  to  whiih  tbo  colour  and  opacity  of 
milk  is  due. 

Skim-milk,  burter-railk,  cream,  butter,  cur*ls  and-whey,  croam- 
cbecsc.  and  ordinary  cheese,  are  more  modi(icatiiin;a  of  milk',  differing 
only  from  each  other  either  in  the  abstraction  of  one  or  more  of  its 
constituents  or  else  in  the  variation  <»f  their  proportions. 

Skim-milk. — The  first  of  tbeee  (skitu-milk)  diflenj  from  ordinary 
milk  in  containing  a  less  nuniUiTy  of  fatly  uiatter,  a  [>orlion  of  this 
having  been  removed  with  the  cream  ;  it  still,  however,  contains 
nearly  all  the  cheese,  the  su-jjiir  of  milk,  Sf>me  butter,  and  tlie  salts  of 
mitk  ;  it  is  therefore  scarcely  Icfs  nniniious  than  new  mJIk,  hut,  in 
consequence  of  the  diminished  umount  of  fatty  matter,  is  less  adapted 
tn  the  development  of  fat,  and  tn  the  maintenance  of  respiration  and 
tbe  temperature  of  the  bo'ly.  In  some  cnses  where  fatty  nmtter  is 
found  tu  disagree,  and  where,  in  conserjiR'ncc,  milk  in  its'  usiiul  state 
cannot  be  taken  without  iiicunvenicnce,  »kiiu-milk  m^y  be  substituted 
with  a'lvantarre. 

Butter' milk.  —  Bntter-milk  approaches  skim-milk  in  its  composition, 
but  contains  a  still  smaller  quiintity  of  fat;  as  an  article  of  diet  for 
poor  persons,  it  has  the  recommendation  uf  cheapness. 

Potatoefi  and  buitcr-milk,  as  is  well  known,  taken  together,  form  a 
TCry  eontiderable  portinn  of  the  diet  of  the  peasantry  of  Irebind  :  the 
butter-milk  constitute*  an  essential  part  of  such  a  diet,  it  s'lpplyinjr 
the  nitrogenised  matter  necessary  for  the  growth  of  t!ie  body,  and  of 
which  tbe  potatoes  themselves  are  comparatively  deficient. 

Cream.  —  In  contradistinction  to  these,  cream  consir*ls  almost  en- 
tirely of  the  fat,  with  a  ver^  small  quantity  of  the  8u<far,  casein,  and 
the  otlier  const  itucnts  of  milk. 


SD6 


MILE,  AND   ITS  ADULTERATIONS. 


^ 


Butter.  —  Butter  tiiflcrs  little  from  cream,  but  is  more  completely 
separated  frotri  ilie  cbecse,  sugar,  and  ssUla ;  and  tlic  inajorily  but 
not  all  the  fat  globutcs,  in  place  of  being  free  aud  distinct,  have  run 
together,  so  ns  to  form  a  aemi-soltd  substance. 

Curds-and-  Whfy.  —  Cunig-nnd-whey  are  made  up  of  all  the 
elements  of  milk,  but  the  form  in  which  they  exist  is  altered;  the 
cheese  is  thrown  down  by  rennet,  or  by  the  addition  of  an  acid,  da 
acetic  aciil,  and,  in  its  descent,  carries  with  it  the  rrreater  part  of  the 
butter,  the  two  together  forming  the  curd;  while  the  whey,  or  serum, 
consists  entirely  of  water,  the  sujjar,  and  the  salts. 

Cream-Cheese.  —  Cream-cheese  consists  of  the  moist  curd  (that  is, 
of  the  cheese  and  butter),  the  greater  part  of  the  serum  or  whey 
being  remov(?<l  by  slight  pre^ure. 

Ordinary  Cheese.  —  Ordinary  t-'bcesc  conlnins  little,  or  much  batter, 
according  as  it  is  made  from  sKim  or  from  whole  milk :  the  casein  is 
precipitated  by  rennet  in  the  usual  manner,  and  aubjccle!!  to  great 
]iressure  in  mould».  Annatttnii  frequently  Added  to  heighten  its  colour, 
and  the  cheese  is  kept  untd  it  becomes  more  or  Ies!»  ripe. 

The  relative  proportions  of  the  different  constituents  of  cow's  milk, 
especially  the  fatty  matter^  are  subject  to  very  great  variation  :  the 
age  of  the  cow,  tne  time  after  culving,  fomi,  temperature,  weather, 
and  the  time  and  frequency  of  milking,  ull  occasion  considerable 
differences. 

The  constituents  of  cow's  milk  in  the  normal  state,  according  to 
il\f.  O.  Ilonrie  and  Chevalier,  are  as  follows:  — 

Casein              ...  4*48 

Butter            -            -            •  313 

Sugar  of  milk              -             -  4*77 

Salts,  various             -           -  0^ 

Water            -            -            -  «7-02 


1 0000 

The  following  U  the  mean  of  ten  analyses  of  pure  milk  by  Professor 
Poggiale  •  ;  — 

Water            ...  862*8 

Butter            -            -            -  43-8 

Sugar  of  milk             -            -  62*7 

Casein             ...  38*0 

SalU-            ...  2*7 


10000 

Ihe  casein  of  milk  is  an  albuminous  sub^itancc,  distinguished  from 
ordinorv  albumen  by  not  coagulating  when  healed,  by  its  congulation 
by  acetic  acid,  and  aUo  by  the  products  of  its  spontaneous  decompo* 

•  Cbrmlcal  Gwttte 


MILK,  AND   ITS  ADULTEKATIONS. 


S07 


it!t!on.  The  tutuh 


form  wilh  itiDSolnblt 


ds,  as  do  ftlso 


k 


* 


conipoin 
various  luetullic  sails  as  ttulpbute  of  copper,  luxl  bichloride  of  mercury. 

The  butter  c.onf,Ut£  of  a.  solid  and  liquid  iats^  in  combination  with 
glycerine.     Theumportinnnf  thiiiconslitueiaorniilk  la  very  viirtable. 

Ungar  of  miik  IS  a  crystallisuble  sugar  ;  it  is  much  less  susceptible 
of  fermentation  than  prupe  or  cane  sugar  ;  it  is  very  slijjbtly  Bolubfe  in 
alcohol,  und  is  less  soluble  in  water  than  cane  sugar;  it  ja  also  les« 
aweet.  Like  grape  sugar,  it  throws  down  the  oxide  of  copper  when 
its  solution  in  botled  with  sulphate  of  copper  and  liquor  pntnssie. 
By  the  action  of  nitric  aeid,  it  yields,  1ik»>  pum^  saccholautic  or 
macic  acid,  so  thul  it  is  intermediate  in  its  properties  between  hugar 
and  guBi.  This  of  all  the  constituents  of  milk  is  the  least  Uuble  to 
vary  in  quantity. 

Lactic  aciil  is  probably  rather  a  product  of  the  decomposition,  than 
a  normal  cnmitituent  of  milk. 

Salt*. — Of  these  some  are  soluble  in  alcohol  us  the  lactates  of  pot- 
ash,—  the  principal  lactute,  —  of  »(Mia,  ammnnin,  lime,  and  ma^esia; 
oCbcn  are  soluble  in  water,  but  not  in  alcohol,  an  sulphate  ol  potaah, 
and  the  phosphates  of  i>otnsb  and  soda  ;  lastly,  ihe  phosphates  of  lime, 
iron,  ana  magnesia  are  iiuoluble  in  water. 

For  all  proeticul  purp<^es,  in  order  to  ascerCam  wltether  a  milk  is 
genuine*  and  ofgoml  cpmlity,  it  ia  sufficu-nt  to  take  the  specific  gravity 
of  the  milk  by  thti  hydrometer  or  galnctometer,  und  to  estimate  the 
quantity  of  cream  by  the  lactometer.  Should  we  desire  to  institute  a 
quantitative  analysis  of  its  chief  constilucuts  we  may  then  adupL  tlie 
procesa  described  by  Hutdlen.* 

The  Butter.  — 'Vila  wei«:hed  qaantity  of  milk  is  mixed  with  one- 
sixth  of  ita  weight  of  common  unburnt  gypsum,  previously  reduced  to 
»  very  fine  powder.  The  whole  is  then  evaporated  to  dryness,  with 
frequent  stirring,  at  the  heat  of  boiling  water;  n  brittle  ina&s  is  ob- 
tained, which  is  reduced  to  u  fine  powder.  By  digesting  ibis  powder 
in  ether,  the  whole  of  the  butter  ia  dissolved  out,  and,  alter  evapuration 
of  the  ether,  may  l)e  obtainetl  in  a  pure  state,  and  weighed ;  or  the 
powder  iLielf,  after  being  treated  with  ether,  may  be  dried  and 
weighed  ;  the  butter  in  then  e»tiniated  by  the  loss. 

The  Sttgar. —  Afierthe  removal  of  the  butter,  weak  alcoholis  poured 
upon  the  (towder,  and  digested  with  it.  This  takes  up  the  sugar  with 
a  little  saline  matter,  soluble  in  alcohol.  By  evajwruting  this  solution, 
and  weighing  the  dry  residue,  the  quantity  of  sugoris  dL-ttruiined ;  or, 
as  licfore,  the  powder  itself  may  be  dried  and  weighed,  and  (lie  ftugar 
estimated  by  tlie  loss.  If  we  wish  to  estimate  the  simiill  quantity  of 
inorganic  saline  matter  which  has  been  taken  up  along  with  the  sugar, 
it  may  be  done  by  burning  the  latter  in  the  air,  and  weighing  the  re- 
aid  uc.f 

*   Afm*icn  ilcr  CtiPinl«  uiid  I'harmarle.  p,  363.,  eopl«tl  lo  "  Mitchpll't  TrraUie,"  p.  7*- 
t  M    P*l"0  Mp^raiet  cane  frum  iDlIk  augar  iij  iHMni  of  ordliurir  bruuljr ;  tlie  itroc««l 
will  be  found  Tull;  docrtbed  at  p.  lOU.  o(  th«  woik  quoted  •!  p.  9M. 


308 


MILK,    AND   ITS  ADULTERATIONS. 


Saline  Mutter — A  scc^HifJ  weighed  portion  of  milk  i**  now  carefully 
evapnrAtC'l  to  dryness,  and  tipiiin  weighed.  The  loss  slutws  the  quiin- 
tity  of  walLT.  'i'lie  dried  milk  is  then  burneiliii  the  nir.  Tht»  weight 
of  the  iiioombuatible  &&\v  indicates  the  propnrtton  of  inorgnnic  fvaline 
inatler  contained  in  ihc  milk. 

The  Casein. — The  weight  of  the  butter,  supnr.  suline  matter,  and 
the  water,  Lteinn  tbui<  known,  and  added  togetlicr,  the  deficiency  shows 
the  weight  of  the  ca«ein. 

Other  iiiL'thorls  may  be  pursued. 

Thus  the  cflsein  and  bnlter  may  be  precipitated  by  aretic  acid, 
the  precipitate  colIecLeJ  and  dried,  the  water  l>einjr  got  rid  of  by  nieans 
of  bibuluus  paper  and  afterwards  hy  ovtt|K»ration  in  a  water-bath  ; 
it  19  then  weij;hed;  the  ftit  is  dissolved  out  by  ether;  the  etherial 
solution  is  next  evaporated  in  a  \vei^hed  cu{>sule  with  a  gentle  heat ;  the 
wei;:ht  nf  the  reHdual  fut  \*  then  determined  by  the  increased  weight 
of  lh«?  ciLpsule.  J'he  diflerence  between  the  weight  of  the  dried  curd 
and  thi.'  butter  ^ives  the  oiiionnt  of  casein. 

Th<*  qiiiintity  of  snfjiir  may  he  estimiited  from  the  whey  by  the 
followin:;  process  of  Professor  Po^rgiale  ;  — 

"  TIjc  test  li(/uor  isprcpflred  by  aildin^  to  a  solution  of  sulphate  of 
copper^  bilurtrate  of  poiash,  nnd  dissolving  ihc  precipitnte  which  is 
formed  in  caustic  p<)tash.  The  Plrettpih  of  the  alkaline  solutiim  i« 
then  determined  with  «rreatcare,  from  the  ([uantity  of  su;;ar  employeil 
to  decolourisf  a  known  volume  of  the  liquid.  It  is  inipnrlotil.  to 
observe  that  milk  sugar,  and  not  cane  sugur^  must  be  enipbtyed  in 
rhifi  operation.  I  mude  several  experiments,  in  order  to  avoid  the 
determination  of  the  strength  of  \\w  solution  of  hinoxide  of  copper, 
which  is  decidctlly  the  longest  nncl  nio^t  ilelicnte  experiment,  llie 
following  proportions  eoohUiiitly  furnished  a  liquid,  twenty  cubic 
ijetitimetres  of  which  correspuiid  to  0  20Q,  or  two  deci;;ramme8,  of 
whey :  — 

Gnmmr*. 

Crystalliecd  sulphate  of  copper  -  -  -         10 

Crystallined  biiartrate  of  potash        -  -  -         10  . 

Caustic  [K>tash  -----         30 

Distilled  wiiter  -  .  -  -  .  200 


I 
I 

I 


The  filtered  liquid  is  perfectly  clear,  and  of  an  intense  blue  colour, 
Prettaratum  of  the  Wftet/.  — •*To  determine  tfie  amount  ofsugar-of- 
milk.  It  is  indispensable  to  separate  the  fatty  matter  and  theciuein  by 
coagulation.  This  is  easily  effected  bv  pbicins  fifty  or  «ixl.y  grammes 
of  the  milk  in  a  small  flask,  adding  to  it  a  few  dro[bs  af  acetic  arid,  a»d 
then  raising  the  temperature  to  between  104^  and  12^*.  A  traos- 
pnrent  li(iuid  is  obtained  on  filtration.  According  to  my  experiments^ 
1000  gniMiines  of  milk  yield  023  grammes  of  whey,  which  gives  for 
1000  grammes  of  whey  about  fifty-seven  grammes  of  sugar. 

Examination  of  (he  Whetf.  —  "  Twenty  cubic  centimetres  of  the  test 


MILK,    AND   ITS    AntXTERATIONS. 


209 


liquor  are  introduced  bj  means  of  a  pipette  into  a  small  flask,  which 
should  be  preferred  to  a  porcelain  capsule,  as  it  allows  of  the  liquid 
being  seen  from  top  to  bottom,  and  of  observing  with  thi»  irreatest 
east!  the  moment  the  decolouri^ation  li  complete.  The  liquid  is  then 
boiled.  On  the  other  hand  a  burette,  each  divijiion  of  wlueli  ia  equal 
to  n  fifth  of  a  cubic  centimetre,  is  611ed  with  the  whey  and  poured 
drop  by  drop  into  the  liquid,  agitating  the  latter  contintjailr,  and 
heating  it  after  each  ufhlitiun  of  whey.  This  is  continued  until  the 
blue  tint  has  entirely  diftapiieareiK  At  first,  a  yellow  precipitate  of 
hydraleil  protoxide  of  copper  is  formed,  which,  however,  soon  turns 
red,  and  sinks  to  the  bottom  of  the  flask.  When  the  operation  is 
terminated,  the  quantity  of  whev  employed  is  read  off  the  burette,  and 
the  weight  of  sugar  eoutaiiied  in  1000  grammes  of  whey  determined 
by  the  rule  of  thrt-e." — Pvggiaie. 

•*Milk  sugar  reduces  a  niucU  simalter  proportion  of  oxide  of  copper 
than  grapo  sugar;  for  whilst  1  gramme*  of  the  latter  decomposes 
6*926  of  sulpbat«  of  copper.  1  part  of  milk  supor  reduces,  according 
to  Neubanerj  4*331,  according  to  Mathaim  4*168,  parts  of  oxide  of 
copper. "  —  FreimuuM. 

A  vcrr  close  approximation  to  the  quantity  of  sugar  present  in 
milk,  mar  be  obtamed  by  simply  evBoorating  the  whey  t(t  dryness, 
weighing;  tlie  residue,  and  deducting  toe  weight  of  the  ash  left  in  its 
inciueration. 

Specific  Gravity  of  Milk. 

As  (he  composition  of  milk  variea,  so  of  course  does  its  specific 
gravity. 

Genuine  cow's  milk  has  an  averaRC  s[>ecific  gravity  of  about  1030; 
it  seldom  exceeds  1031,  but  is  frequently  several  degrees  l"Wcr.  The 
great  variatirm  In  the  specific  pravily  of  milk  is  occa:*ione<l  by  corre- 
sponding vnrijtiions  in  the  quantity  of  butter  or  cream  prcnent ;  the 
butter  of  milk  being  so  much  lighter  than  water,  the  greater  the  pro- 
portion of  butter,  the  lighler  of  course  is  the  milk. 

That  this  is  really  so,  is  sliown  by  the  following  table. 

^_        Tam^a   hhowing   thb  Vauiatio?!    m   tub    SpFCiric    Geatitt  or 
^^fe  GaNriNR  Mit.K,  and  tub  Relation  of  this  to  the  Pbr-Cbkt- 

^^^^^   aoBS  or  Cbbam. 

^^^^H  MiltL 

^^^^^^^^  spec  <>rar. 

^^^H  4     -  1008     - 

^^^^m  6     -         -     1030    - 


'*  Pmcnlui  rMwmrrMixU  that  th^  wh^  h«  flMirMi  vlth  ■  llttk  wfalte  of  t*g|  aitil  Bllrrrd, 
ati4  tb«  lltnie  ilkluud  «Uh  atiie  titno  lU  toiuinc  of  w*ter. 


»!•«;.  GriT. 

Cream. 

— 

2° 

_„ 

2* 

10-27     - 

36 

1026     - 

80 

—       - 

3* 

MO 


MILK,  AND   ITS  ADULTERATIONS 


Milk. 

Skim. 

spec  Grav. 

Spec  Gr»*. 

Cr*un. 

10-27     - 

-     1030     - 

-      9 

1026    - 

-     1028     . 

-     13 

1029     . 

-     1030     . 

-       8 

1030     . 

-     1031     - 

-      7 

1024     - 

-     1028     . 

-     10 

1027     - 

-    loai    - 

-     10 

1023     - 

-     1030     - 

-     25 

1024     - 

-      1031     - 

•     32 

1023     - 

-     1029     - 

-     10 

The  above  table  includes  fmmplefi  of  both  euorning  and  afternoon 
millers  as  well  oa  some  of  ihc  tir;jt  and  liist  milk  obuined  at  the  same 
miUcing ;  the/  are  not,  therefore,  to  be  tukeo  as  average  tainplcs  of 
milk. 

From  an  examinatioD  of  the  table,  it  nppoars  that  a  milk  ma/  be  of 
high  specific  gravity^  aud  yet  yield  but  Hule  cream  (nee  I);  or  it 
may  be  of  low  specific  gravity,  and  yet  afford  a  very  larye  quantity 
of  cream  (see  4):  al^^s  that  the  removal  of  the  cn^am  increases  the 
density  of  the  milk  (sklm-miLk)  several  de^j^rccs.  It  will  he  observed 
that  not  one  of  the  samples  in  the  table  shows  a  low  spmfic  gravity 
with  deficiency  of  ercam.  We  have  never  met  with  a  naiuriu  milk 
of  thi.s  kind,  and  believe  it  to  be  of  very  rare  occurrence. 

The  specific  gravity  of  the  scntm  of  milk  is  due  mainly  to  the  iufpo" 
contained  in  it;  and  o^  this  coD!«tituent  is  the  least  variublct  so  is  its 
vpecific  gravity  the  least  subject  to  variation, —  a  circumstance  of  cod* 
aiderable  importance,  as  will  be  shown  presently. 

TaBUE   8UOWIMO   TDB   DENSfTT    OF   SeBI'M,   AND    ITS   ReLATIOR   TO 

TUB  Specific  Gravitt  of  Milk. 


Cowt. 

Milk. 

SlwUk  OmiltT- 

Cows. 

MWk. 
SpMMc  OnvUy* 

Bp«Sku?;«io. 

]rw9 

10» 

IS 

i«n 

losr 

lOM 

icna 

93 

ION 

1077 

loas) 

iim 

34 

mi 

wrm 

luai 

1077 

23 

losa 

ton 

laio 

1027 

M 

tosa 

tOSB 

J008 

lO-ift 

77 

toil 

losa 

101  !l 

10S7 

ts 

LOSS 

1017 

I(W6 

10^ 

K 

1078 

1017 

1030 

low 

no 

IflST 

lOTi 

10 

I«H 

I0» 

31 

low 

loir 

1027 

lO'JT 

3? 

1030 

lOM 

I0Y6 

1 077 

33 

L>^ 

lOM 

1(«7 

loas 

34 

inao 

1077 

in-^ 

IfiiT 

as 

1074 

I07S 

J  010 

low 

36 

low 

lOK 

1(KH> 

1077 

37 

Ifi76 

1071 

KlVI 

\0W 

38 

love 

1078 

itm 

low 

39 

10S« 

1077 

19 

]0» 

lt«7 

40 

IMC 

1076 

» 

irri4 

iwr 

41 

1030 

1076 

SI 

1034 

lOM 

41 

ion 

MM 

MILK,  AND   ITS  ADULTERATIOXS. 


SU 


The  above  table  includes  manj  samples  of  milk  of  an  exceptional 
charActer. 

It  will  be  observed,  that  white  the  speei6c  gravity  of  the  milk 
extends  over  a  wide  ran^ie,  vorvinf^  from  10()H  to  IU3I,  ibut  of  the 
serum,  on  the  contrary,  is  dubjeot  only  to  a  flight  variation,  the  limits 
being  front  102S  to  1025. 

AVe  huvo  here,  then,  a  fixed  datunit  from  vrhich  to  determine,  with 
precision,  the  adulteration  of  milk  with  water,  a  point  of  the  greatest 
UDportonce. 

The  specific  gravity  of  «A/m-mi7A,  althouf^h  not  so  6xedasthutof 
the  »erum,  i»  yet  much  more  so  than  that  ot  whole  milk  :  itD  average 
weight  U  estimated  by  Fereira  at  1034  8. 


Variations  in  Composition  of  Afilk. 

It  has  been  stared  that  the  compositinn  of  milk  is  subject  to  very 
great  vuriatiou  accurding  to  several  nioilifyinj;  cirrumsinnoes ;  the 
chief  of  (lie^e  are,  tbu  age  of  the  cutv,  its  condiliun,  the  time  and  fre- 
quency of  milking,  iht!  nature  of  the  fuod,  hnusin;;  of  tbu  cows,  and 
temperature. —  We  shall  bestow  a  few  remarks  on  each  of  tliMecmijes 
of  vHriatiun. 

Injiuenee  of  Age  on  Milk, — With  respect  to  ai^e,  a  younjr  cow  with 
her  first  calf  gives  less  milk  than  with  hur  second,  third,  or  Jburth  calf, 
she  being  eonsidereil  to  be  in  her  best  condition,  tn  most  coses,  when 
from  four  to  seven  years  old. 

The  period  during  which  cows  give  milk  affcr  cnlving  is  usually  five 
or  BIX  months,  but  very  frequently  the  time  i-*  much  prulongcil  beyond 
this  ;  we  have  been  intbnned  of  an  instaufi;  nf  a  cow  continuing  to 
give  milk  for  three  years  and  a  holf  alter  calvin". 

tnjiutnce  nf  Condition  im  Milk. —  The  first  milk  yielded  by  the  cow 
aflcr  calving  is  yellow,  thick,  und  stringy :  it  is  called  colofitrnm,  and 
by  milkmen  nnU  oibeni,  "  beostings/'  This  state  <>1'  the  milk  Usts 
from  abuut  three  weeks  to  a  month,  but  i»  very  bad  for  ilie  first  ten 
ilays,  during  whji'b  tuue  the  luilk  is  ni>t  fit  for  use.  From  the  end  uf 
the  first  to  the  tt^ruiiuiitiun  of  the  third  ur  fourth  munllt,  the  milk 
is  in  its  best  conditiun. 

The  cow  carries  her  cnlf  for  forty  weeks,  or  ten  lunar  months:  it 
is  the  common  practice  to  milk  the  cow  regularly  for  the  first  seven, 
eight,  or  nine  months  of  this  period,  a  practice  which,  at  first  sight, 
appears  to  be  highly  objection  able,  but  whicii  is  really  not  su  much 
so  as  might  be  supposed;  und  it  is  rendered  absolutely  necet>t«ary  by 
the  fact  that  cows  could  not  otherwise  be  profitably  kept;  ncver- 
theiesft,  it  is  very  important  that  the  milking  should  not  be  continued 
too  long,  for  tne  sake  of  the  cow,  the  calf,  and  the  milk  itself:  in 
general  it  should  cease  at  the  end  of  the  seventh  month  ;  niuny  cow- 
keepers,  however,  continue  to  milk  up  to  a  very  short  period  of 
calving. 


»l» 


MILK,   AND   ITS  ADULTERATIONS. 


Another  very  objectionable  pracllc*  is  to  permit  the  cow  ngtm  to 
becoiTii'  in  fiilC  within  two  or  three  months  after  hnvlnji  riilvt'H  ;  the 
object  Iff  ihiing  so  Is  lo  derive  aa  nmrh  profit  as  pracliciibh'  from  the 
aniinul,  without  rrgnrU  to  tlie  ulfeet  un  iLs  eon»tiriili<]n«  tht;  qufiUtv  of 
the  niilk,  or  the  growth  of  the  ciilf.  It  is  impHssibU  to  i-Kiioeive  that 
a  citw  enii  cujitiimd  to  vieM  lur^e  qiXEHitihufi  of  j^^hjiI  milk  dnilv*  anil 
Aflbril.  lit  the  «aine  tJino,  siilFicieiit  iiouri»huiuut  ibr  carrying  ou  eflcc- 
lively  the  prouess  of  pestulion. 

Jnjiui'iice  ft/ FiKi*/ on  Milk. —  The  naturjil  food  of  the  cow  is  evi- 
denllv  that  derived  from  piislurcs,  viz.  grass,  the  milk  oVjtained  from 
c<kW3  fed  upnii  thia  being  of  excellent  4iuiilily  and  sutticientlj  rich  fur 
all  pur[to:tL-}i. 

The  next  most  natural  food  is  dried  grass  or  hay,  which  is  given 
larjiely  to  cows  in  winter,  the  milk  being  nearly  the  Bume  in  qualit/ 
as  from  grass. 

Beet  root  and  carrntts,  being  very  nutritioui*,  are  also  usually  jjiven 
to  cowB  in  the  wint<-T  f  imc  with  advantage.  With  regard  to  the  eflVet 
of  beet  root  nixl  carrois  on  iiiilk,  we  obtain  the  fnll(iwin£r  informNlion 
by  MM.  O  Henrie  and  Chevalier,  as  repopiftl  in  Mr.  MitoheU's  trua- 
tisc  Oh  the  "  Falsification  of  Kootl,"  p.  74. 

The  constituents  of  cow*3  milk  in  tho  normaJ  state,  according  to 
MM.  O.  Uenrie  and  Chevalier,  are  as  follow  :  — 

Casein  (cheesy  matter)  -  -  - 

Butter  -  .  -  -  . 

Sufjar  of  milk    -  -  -  -  - 

Salt*,  various    -  -  -  -  - 

Waltr  -.---* 


When  the  cow»  arc  fed  on  beet: 
Casein  -  -  - 

Butter 

Sujjar  of  milk    - 

Salts     -  -  . 

Water  - 


I 


When  on  carrots :  — 

Cnsctn  • 
Butter  - 
Sugar  of  milk  - 
ShIis     - 
Water  - 


IIILK,   AND   ITS   ADULTERATIONS 


3  in 


'  It  will  be  observed  that,  nocording  to  the  ulMive  taUU'S.  the  efleot 
of  fuodlng  cowfl  on  farrote  is  to  occasion  a  oli^ht  iliininutinn  in  the 
aninuni  ol'ousciii  amd  butCor,  but  an  inereuBe  in  tlie  quiinttt^  of  8u<;ur, 
while  feeding  them  on  beet  root  reduces  stUI  more  the  quantity  of 
cogi-iii  and  buiter,  but  very  largely  increaBes  the  supar* — effects  which, 
troui  the  richness  of  carrot  and  bt;el  in  sugar,  might  have  been  antj- 
ciputed. 

As  is  well  known,  a  very  considerable  number  of  the  cows  which 
supply  Lotidoii  with  milk,  are  kept  in  variouit  conBned  and  unhealtliy 
places  in  the  nic  trnpolis  ;  sut'h  cows  nre  MihJoni  turned  out  to  {jrass ; 
the  system  of  feeding  ndmited  being  altogetliLT  aptificia!  and  unnatural, 
brewers' groins  arid  disliilers'  wash  foniiijig  tlic  cliii-f  part  of  their  f<>i>d  ; 
these  stiiKulate  the  aniumls  unnatundl)',  and  under  the  ^timldus  large 
<|uantitiuet  uf  ndlk  of  inferior  quality  are  accreted,  the  cow  quickly 
becoming  worn  uut  and  discused  rii  conse([ueuce. 

In  relereiiee  to  the  eiTects  of  grains  uu  cows,  Mr.  Ilartey  luake^  the 
following  remarks:  — 

"  Brewera  and  distillers*  grains,  and  disfilters'  wajth,  make  the 
cattle  grain-sick,  as  it  is  termed,  and  prove  injurious  to  the  Jtlomach 
of  the  animal.  It  has  been  a.tcciiained  that,  if  cows  arc  fed  upon 
these  grains,  Sic,  their  cunslitulions  hcL-ome  quickly  destroyed."* 

MM.  Bous!<ingauk  and  Lebcl,  from  ex^Hiriuients  made,  have  arrived 
at  the  ciiTicIusion  that  the  kind  id'  food  has  nut  a  great  inlluenee  cither 
u|)on  the  amount  i>r  composition  uf  mtik,  provided  tiumitities  con- 
taining equal  pru[>ortions  td'  nutritious  niatti-r  be  givCTi. 

htflnence  of  Ternperaiure  on  Milk.  —  In  hot  countries  and  dry 
seasons  the  quantity  of  milk  yieldeil  is  said  io  be  let«a,  but  the 
quality  is  richer;  it  is  also  jttated  tliat  eotd  favnurs  the  produc- 
tioN  of  sugar  and  cheese,  whiUt  hot  weather  augm«.'ntd  ihu  aii^outituf 
butter. 

It  would  be  extremely  desirable  to  a.«certAin  precisely  the  extent  to 
which  the  quality  of  milk  its  influenecil  by  weather. 

Influence  of  the  Time  aiui  Frequency  of  Milhiuf^.  —  Willi  re^iard  to 
the  quality  of  milk  as  affected  by  thi>  time  and  fi*equency  of  milking, 
morning  milk  is  said  to  be  better  than  that  obtained  in  The  afterniMm ; 
and  the  milk  of  cows  when  milked  but  once  a  day,  is  richer  than 
eiihtT.  It  is  the  common  belief  tliut  the  XaaI  portion  of  the  milk 
obtained  at  any  milking  is  richtT  thiui  the  fust;  we  have  titken  pains 
to  aM:ertain  wht.*ther  there  is  any  loundation  for  such  an  opinion,  and 
find  it  to  be  really  the  cvlah  to  a  remarkable  extent,  as  will  appear 
from  the  foUuwin^  table. 

•  HarlfUa  Dalrjr  Sjr(te?n,  pp,  73.  «tid  74. 


r  3 


MILK,    AND   ITS  ADULTEEATI0N8. 


Table  krowing  the   DiFrBEBncE  m  thr  Qdautt  of  thb  Fia&T 

AND  Last  >fiiK  obtainbd  at  eacu  Mujuxo.  [ 

\st  Milk. 
Afternoon. 

Milk .  Ca^m 

Spec.  Gnir.  '^'*"* 


Cowi» 

1 
2 

:t 

4 

s 

6 
7 
8 


1027 
1026 
1027 
1029 

loao 

1030 
1029 
1031 


2nd  Milk. 

1033  . 
1023 

1025  - 

1024  ■ 
1024 

1022  ■ 

1020  • 

1030  ■ 


6Ii 


Trom  nn  <?x«mmfttion  of  these  tables  it  Bppears 


that  the 


milks  are  nf  mueli  luwcr  specific  pravity  than  the  first ;  ami  hence,  h*d 
the  sptTilic-grftvity  ti'«t  alune  been  mie^l  un,  they  would  have  b<m 
pnjnoufK'etl  tn  be  iiiferiur  in  riuhneiis  to  the  first;  u  eoitctuuon  the 
reverse  of  thiit  ivhirh  is  correct.  'J'lius,  while  the  ereiiin  of  the  whole 
eight  samples  of  the  first  milks  nmounteil  to  61 1  jjer-eentaies^  that  of 
the  last  Kmniinted  to  1-^H  ;  thut  if,  they  eontaine*!  mnre  than  double 
the  qnantitjf  of  cream.     This  fart  is  imt  without  practical  ini|>nrtancc 

It  is  a  common  practice  for  invalids  and  others  to  prtK*ure  their 
glius  of  milk  ilireet  from  the  cow  ;  wc  thus  perceive  that  in  this  way 
they  seldom  obtain  tlie  proper  proportion  of  butter,  a  circumstance 
which  ntny  be  uf  advnntii^e  in  <!ome  canes,  and  of  divadvanto^  in 
others.  In  London  it  is  now  eoinmoit  fur  cows  to  be  driven  t1irou{|ii 
the  streeta,  and  to  be  milked  in  the  presence  of  the  purchnser*: 
although  in  this  way  the  buyer  succeeds  in  procuring  it  gentiinOi 
he  tWs  not  alwHvs  obtain  the  best  milk. 

The  great  ddTfrenee  in  the  amount  of  cream  contained  in  tlie  first 
and  last  milk  taken  from  the  cow  nt  one  niilkinfr,  ap|»ears  to  be  silii- 
faotorily  explained  un  the   supposition  tbac  the  fatty  matter  of  (te 


MILK,   AND   ITS  ADULTERATIONS. 


215 


nillc  obejs  the  same  laws  of  graTity  in  the  udd<er  of  the  cow  that  it 
docfl  when  Kt  aside  in  an  open  vessel. 

The  following  tables  ehow  the  varietiea  in  the  specific  Jfravity  of 
tndkf  and  the  per-centages  of  cream  in  uiQriiing  and  af\ernoon  milk. 

Table  suowtsig  Tns    Spbcific  Geivitt  or  Pcbe  Milk,  akd  the 
Pbb-Cbktagbs  op  Cbeam. 


.^ 

Momutg  Milk, 

B 

I 

Milk. 

Spec.  CifflT 

tr- 

Cream. 

Card. 

1 

- 

1030 

- 

■       6* 

63gr8 

S 

- 

1031 

• 

-      7 

69    „ 

s 

- 

1028 

- 

•     H 

66    „ 

4 

- 

1030 

. 

.       9 

80    „ 

S 

- 

1031 

. 

-     10 

78    „ 

8 

- 

1028 

- 

-    n 

75    „ 

7 

L 

10A0 

_ 

-     12 

_ 

_ 

as  „ 

8 

- 

1023 

- 

-       5 

- 

- 

81     „ 

9 

. 

1029 

- 

-       7 

- 

- 

61     „ 

10 

- 

1028 

- 

-       9 

- 

- 

63    „ 

Average  nearly  1029     Total   -     77| 
Average  about  7J. 


Total  -     693 


Afternoon 

Afiik 

SSu. 

Mtlk. 
SfMT.  Gra« 

tj 

Crum. 

1     • 

1028 

. 

. 

7} 

2       - 

1027 

- 

. 

10 

3       - 

1027 

. 

. 

6 

4 

1(»2H 

- 

- 

9 

5 

1028 

- 

- 

14 

6       - 

1027 

- 

- 

74 

LondoiL 

•7      . 

1028 

. 

* 

22 

•8       - 

102(j 

• 

- 

6 

•9      - 

102G 

. 

. 

6 

•10       - 

102G 

- 

• 

n 

Card. 


69 

prs. 

in 

11 

75 

n 

78 

t» 

87 

n 

63 

»i 

98 

»» 

74 

« 

69 

i» 

86 

t» 

Average  about  1027      Total   -    96^ 
Averof^e  more  than  %\. 


Total  -     810 


The  Richmond  cows  from  which  the  first  six  morning  and  afternoon 
milks  were  obtained,  were  ft'd  portly  on  grass  and  partly  on  graiOK 

r  4 


«I6 


MILK,   AKD   ITS   ADULTERATIONS. 


It  is  deftiruble  that  the  foUowiug  particulAra  relating  to  each 
should  be  made  knuwD  ;  — 


C»«i. 

A^ 

Muiibir«rc«l««. 

Dttm^lmtC»tr. 

Vi^*tmV*mn. 

Hywm 

AvmIu 

Uqium 

7  month* 

T      .. 

'               H 

ft        • 

10      .. 

«         n 

IS      *. 

3         „ 

1             H 

■      ^ 

W 

*        n 

19       M 

•7 

fi         t* 

to  week* 

10      .. 

•8 

s 

10      ^ 

■9 

3  meatlu 

w     » 

•W 

U  week* 

» 

The  flamplcA  were  taken  from  the  milk'piill  containing  the  whole  of 
the  milk  obtained  iWiiu  each  cow,  uml  whilst,  »tiU  wurm. 

From  the  jirocfdinjr  tiibles,  it  appears  — 

1st,  Thiit  tbe  apeeijic  gravity  of  penuiiio  milk,  in  its  ordinarjr  condi* 
tiort,  vurieB  between  1031  and  10:26;  ond  thni.  the  average  specific 
graviiy  id*  the  inominj!  milk  is  about  10*^9,  and  the  aftenioon  1027. 

2nd.  Tb&t  the  amount  of  cream  ranges  IVom  4^°  to  '12?^  the  average 
beintiUi^ 

3rd.  That  the  quantity  of  curd  varies  from  55  to  98,  the  average 
beinc  75.  { 

liic  above  are  the  results  in  the  case  of  sampler  of  mHk  of  ordinary 
quidity;  but  exceptional  cases  sometiuioa  occur,  in  whiih  tlit*  i!i)Ocific 
gravity  is  less,  a.^  also  the  quanlily  of  cream,  curd,  butter^  and  clieejiC. 

On  the  HoHsiug  of  Cows, —  In  a  very  useful  litlle  pamphlet*  pub- 
lished some  time  since  by  Mr.  H.  Ku;:^.  surgeon,  on  Londcm  Milk*, 
we  meet  with  many  particubirs  relating  to  the  iuipru[n?r  mmie  pursued 
in  feeding;  and  houain;;  cows  kept  in  viu-iousi  parts  of  the  [Metropolis. 

"Anyplace,  any  hovelt"  writes  Mr.  Rngg,  "cow-keepers  seem  tu 
coniftder,  will  do  for  a  ct>w,  —  narrow  bines,  confine<l  enrnors,  &c., — 
and  yet  tliev  wonder  how  it  is  that  they  Io?e  ?o  nmiiy  from  disease. 
Can  any  nne  with  a  prain  *>f  common  sense  at  all  wonder  that  cows 
should  i»c  uflilrted  with  di?eaae  when  tht.'y  ore  huddled  together  in  a 
space  that  doc^  nnt  allow  tliem  sufficiunt  bronlhin^'-room,  with  lUeir 
heads  placed  close  un  tu  the  wall,  and  without  a  tiuflteient  current  of 
air  or  ventilation  ?  The  carbonic  ucid  expired  fnini  their  lun^rs  jj^, 
before  it  can  rise,  the  greater  |>art  inhaleil  yj:aiii,  unmixed  with  a  suf- 
ficiency of  pure  nir^  so  necessary  for  the  oxidation  of  the  blood,  and 
Consequent  vitality  of  the  body. 

"  The  air  of  (be  cow-houfes  ia  not  alone  vitiated  by  the  exhalations 
from  the  lungs  of  the  cows,  but  from  the  iniproijer  drainage  of  their 
sheds,  and  from  the  collections  of  all  kinds  of  oSal  and  filth  and  vege- 
table substances  in  a  sute  of  decompoi^iuon,  together  with  pigs  run- 
ning about  the  place,  or  euclosed  in  one  corner  of  the  shed.** 

•    OtweTTiltooi  on  London  MUk,  wcoad  cdiUoa.    \$.    lUilej  And  Mooa,  RcfCJU  ScrMt. 


MILK,   AND  ITS   ADULTERATIONS. 


217 


Other  ob»ervalions  on  the  same  subject  will  be  found  reconioil  m 
the  Harleian  Dairy  STStem,  p.  14. ;  Aitou*8  Dairy  Husbandry,  ji.  70. , 


Fig.  St. 
QouD  Uijjc 


'^^^'/f 


8 


•^o^'qqo 


,o«o' 


9  o^^abJ*'  •°.^'^p  «*<^§^ 


Thto  kikd  lk«    fire  MUivIdc  flfUM*  v*  all  dr»wa  la  •  M«I«  of  ktwut  980  tlU* 

mtiVTv. 

•nd  in  a  Pamphlet  on  the  Sanitary  Conditiou  of  tlie  Pariah  of  St. 
James^a,  Westminster,  by  the  Hon.  F.  Hyng. 

The  necessity  fur  an  ubundanre  of  pure  air  is  shown  by  the  follow- 
ing calcuUtion  : — Dr.  Thomson*  stAtes  that  one  cow,  consumin(;6  Iba. 
of  carbon  in  its  daily  food,  for  respiratory  purposes,  would  re'juird 
9^6j  cubic  feet  of  atmospheric  air. 

On  the  Characteristics  of  Good  MiVL 

Good  milk  is  a  white  homo;;eneou<4  fluid,  of  sweet  and  bland  taste, 
not  bec'uninj^  viscid  on  the  addition  of  ammonia.  It  slioidd  have 
a  specific  f^avity  of  about  1030.  and  should  yield  about  9J  per- 
ceotAges,  by  the  lactometer,  of  cream. 

•  EtjMrlakntal  BOTMrcbflu  00  tlie  FooUor  Anlin4lsp.  lU. 


MILK,   AND   ITS   ADULTEUATION& 


H 

^m  The  specific  gravity  o(  genuine  whole  milk  is  liable  to  vary,  ordi- 

^H  norily,  however,    within  toe  Unuts  uf  1026  and    1031 ;  that  of  the 

^^^^^ta  .    Poor  Uiuc 


scrum  from  1025  to  1028 ;  the  cream  is  likewise  subject  to  verj  gresi 
Tariation. 

Examined  with  the  mL(*ro<(rope,  it  is  found  to  contain  niTriadf  of 
beautifully  formed  globules  of  faity  matter  of  various  size,  and  reflect- 
in"  the  hghr.  strongly,  und  whicb  glubulea  are  entirely  and  readily 
soluble  in  cuu:?uc  |H)Uuih ;  in  fact,  gi>od  milk  under  the  microtoopt 
presents  the  appearance  exhibited  in_y^.  64. 

If  the  milk  exhibit  any  want  of  complete  homogeneous ness  or  ■ 
of  imjKTfoL-t  liquidity  ;  if  It  be  viscid,  or  become  bo  on  the  additioa 
of  ammonia ;  if,  examine<l  willi  the  mirr<isco(>e,  blood,  or  pus,  nr  colo- 
strum cr^rpusi^lea  are  present^  the  inilk  h  not  healthy  milk  of  good 
f|uaUty  ;  la-<tly,  if  the  fat  globules  ore  comijarativcly  few,  and  of  saaB 
litze,  the  milk  is  pitor. 

Cream  con^i^its  almost  entirely  uf  these  fat  globules,  some  of  whidi 
are  ufieu  met  with  of  very  considerable  size. 

The  curd  of  milk,  ns  already  explained,  is  com|)09ed  of  both  de 
cheese  and  the  fat  globules.     Its  appearance  under  the  microscOfie  if 


MlljKf  AND   ITS  ADULTERATIONS. 


219 


reprcAentei)  in  ^.  67.;  the  cuein  or  cheeM  is  distinguishccl  by  iu 
granular  texture. 

F'g.eti. 


-rifcrc 


I 


The  first  milk  yielded  by  the  cow  after  calving^  called  colostrura,  U 
ctuiracte rifted,   aa  before  noticed,  by  the  presence  of  numerous  cor- 
puMles  of  large  size  and  {rranular  ap|>caranoc.     Cow's  milk 
vtftte  orcoIo«trum  is  represented  in^.  68. 


the 


On  the  Apparatus  employed  to  determine  the   Purity  and  Quality  of 

Milk. 

Independent  of  a  quanlitative  chemical  analvsISf  the  purity  nnd 
4)ualitv  of  milk  are  oflon  judircd  of  by  ita  specific  jfravity  aiid  the 
quantity  of  fjiuy  matter  or  ercam  whirli  [lie  milk  furnishes. 

The  itperijic  gravity  or  weipht  of  milk  may  be  determined  by  means 
of  the  ordinary  Fpeeific-gravity  bottle  ;  it  is  more  frequently  aseertnined 
by  meain  of  the  common  hydrometer,  or  by  the  galactometer,  of  which 
several  varieties  hare  been  devised. 

The  best  of  the  palartnmetcrs  is  the  instrument  invented  by  M. 
Dinocourt*,  named  the  Centenmtd  GalacUtmeter, 

*  Con»lrucc*tir  d'inttniiDentt  4c  pbjulque,  et  de  rhrmle  ea  r«fT0,9.  Qual  St  Mlcbel  fc 
Tu\t. 


•u 


MILK,    AND    ITS   ADULTEttATIoNS, 


**  The  centesimal  galactometer  is  represented  ^J^-  70. ;  it  U  cum< 
poded  — 

'*  1st.  Of  a  stem  A,  a,  enclosing  scales. 


Ftg.er. 

CcmD  or  Miui 


"2nd.  Of  n  cyliu'Ier  S,  servin}{  to  float  it. 

"  3r<l.  And  of  n  bulb  V,  i-barfjed  witli  t>hnt^  serving  as  a  ballast,  so 
that  the  inslrunient  flaals  upri;;ht  in  the  milk.  Of  these  ihrefl  parts, 
it  is  only  necessary  to  wfU  imdi-rftt-ind  ono,  tbnt  wbiih  i-nrlows  the 
scales  An;  ilie  scale  A^  in  prtrt  coiotired  t/etlatr,  servea  to  wt'iijh  the 
milk  with  its  tTeam  ;  Ihe  first  depree  on  the  ti^p  of  the  scale  10  marked 
50,  The  following  exicnd  from  50  to  100  and  over.*  Each  deprce 
starting  from  100  in  mounting  up  to  50  represents  11  hundredth 
of  pure  milk:  the  de;n"ee»  foruied  by  a  line  »re  eipial,  us  50,  52, 
54.  &o. ;  the  deyrrccs  formed  by  a  dnt  are  nnetpial  decrees,  as  81^  83, 
85,  &c.  To  coniprchciul  well  the  raluv  of  (he  tie^rofR  ol'  this  seale,  it 
is  sufficient  to  irive  art  example  :  —  Sup|in>.sin;r  tlien  that  the  galacto- 
met«r  is  sunk  to  the  85th  di^gree,  thai  will  indirnte  85-Iiundredlhs  of 
pure  milk,  nnd  eonscnpiently  that  I5-hundredths  of  water  hud  been 
added  to  this  milk ;  the  galaetomeier  is  stopped  at  60  degrees,  there 

*  11  will  be  tfOB  ihAt  llii*  iciile  hfik  tiren  cut  do«n  to  h«lf  Ui  griwlMfttton,  M\i  ItiM  it« 
0  cnrreiponda  to  dUillled  vater  ;  we  bA««  auprrMir^  IIk>  Brat  M)  degrpM,  which  wouid 
have  lengthened  the  itcro  of  (be  tnitrutncnt,  and  have  rendrred  it  more  fragile  without  aor 
uttlttT- 


I 


MILX,  AND  ITS   ADULTERATIONS. 


fi2X 


will  be  4<^hundredlb5  of  water,  or  four-tenths  of  water  addeil.     We 
•ee    firom    this   that  in  adtlin<r  tu  the  number  uf    hundredths    indi- 


cated by  the  inslrament  a  complement ary  number  to  form  one  hun- 
dred, this  complementary  number  will  give  in  liundreiUli;)  the  tjuan* 
tilt  of  water  added  tn  the  milk  under  trint.  If  wo  wiy.h  to  nvoid 
rn^knntng  by  hundreiltbs.  one  may  count  only  by  tenth!) ;  wc  have 
only  to  notire  thut  the  first  tenth  is  whit^',  ihnt  the  jiecoiid  \a 
rohturetl  yellow,  the  third  is  whib.',  the  fiturili  yellow,  nnd  that  the 
fifth  is  alsn  white.  Thia  alternatinn  of  white  and  yellow  pivea  a 
very  evident  deoiarcation  between  each  tcntli ;  towurds  thu  middle 
uf  each  tenth  we  have  placed  the  figures  1,  *^,  ^,  4,  5j  to  indicate  ibeir 
order. 

"  The  space  comprised  between  100  to  120  is  also  coloured  yellow ; 
this  cnmprehcnd-i  the  different  densities  of  pure  milk  —  that  is  t4i  say, 
without  the  extraction  of  cri.*ain,  as  well  as  without  the  addition  of 
water:  we  have  prolonged  the  ecole  from  120  tu  136,  so  that  it  may 
aerve  in  all  eases. 

^  The  scale  a,  in  part  coloured  blue,  is  tlestiiicd  to  weigh  iikini-milk ; 
it  ie>  like  the  firsts  divided  into  100  decrees  or  hundredths,  of  which  tbe 
firtt  50  have  been  cut  off  as  useless  ;  each  degree  commencing  from 


2S2 


MILK,    AND    ITS   ADULTEHATIONS. 


100  to  50,  and  mounting  upwards  represents  a  buodredth  of  pure 
etkiinnieil  milk  ;  con»(;r|uentlir'^  Oie  ninnuer  of  estimating  the  quantity 
of  wut<*r  a^liled  tx»  »kiiti-rinlk  ia  uh^otutL'l}' (be*  ^laine  an  for  pure  milk 
with  its  cream;  the  oxamjiles  ^ivcn  for  cstimatiiifr  the  value  of  pure 
milk  are  applicable  to  skiin-oiilk.  Wc  muy  e'[ually  con6ne  ourselves 
to  estiiuating  ibe  value  hy  tenths  ;  these  tenths,  tiltemutely  coloured 
blue  un(i  wliito,  are  suiHcictilly  distinct  not  (u  bu  cunfouinleil. 

"These  two  scales  give  toe  vflUie  of  milk  only  in  hundredths; 
nevertheless,  it  will  always  be  easy  to  compare  these  ilegrees  with  the 
(ienaity  or  sptcijic  gravUtf  o/ milk ;  we  imiltTj^land  hy  the  word  denxity 
the  sijecifii'  weight  of  any  llfiuid,  water  lieing  lakt-n  as  a  thousand,  a 
litre  of  diHtilk'tl  water  weighing  1000  grammes  or  one  kilogramme,  at 
the  temperature  of  4°  of  tlie  centigrade  therjnometer. 

"  If  now  we  wiish  to  know  the  density  t>f  the  milk  under  trial,  we 
call  to  mind  thut  50  degreew  of  the  scale  A  of  the  gidactometer  cor- 
re!4poiids  exactly  with  1014  degrees  of  the  densimeter  of  M.  CoUar- 
deau't  and  that  each  tenth  of  the  scale  of  the  giilartometer  is  equal 
to  three  degrees  of  the  densimeter;  oonsetjitenlly,  three-tenths  and  a 
tliinl  are  equal  to  a  degree  of  this  densimeter  :  thus,  1014  corres[>ODd 
to  50,  1017  eoiTcspond  to  60,  lOiO  correspond  to  70.  &c." 

It  will  be  perceived  that  this  inHtrument  t^  eneentially  a  densimeter 
or  measurer  of  specific  gravity ;  and  since  the  apecillc  gravity  of  milk 
\i  subject  to  great  variation  from  naturul  and  other  caut^es,  ihe  galuc- 
toineter  is  of  course,  to  a  great  extent,  liubk'  to  the  same  fallacies  as 
the  densimeter  or  hydrometer,  although  both  are  capable  of  oiTurdlDg 
useftil  indicalions. 

Pure  milk  not  deprived  of  its  cream  has  a  less  specific  density  than 
skim-milk  caiise<l  by  the  lightness  of  the  cream.  If  the  cream  he 
either  in  part  or  wholly  removed  tVom  milk,  the  rci^idual  milk  will 
weigh  heavier  than  that  which  icuntuins  iti^  nuinial  |)ropurtion  ot'cream. 
Skiui-U)ilk>  therefore-,  tried  by  the  guIactouR'ter  sciife,  for  pure  milk 
only,  would  give  a  hijiher  specific  gravity  than  ordinjirily  belongs  to 
pure  milk,  aud  hence  the  error  might  be  committed  of  yuppusing 
It  to  be  pure,  an  error  whicli  can  only  be  correcteil  by  means  of  the 
lactometer^  by  estimating  with  it  the  pi»r-centiige  of  creom;  should 
this  i>er-centage  fall  short  of  that  which  is  proper  to  jiure  milk,  the 
B&m[>le  of  milk  is  one  the  value  uf  which  should  he  determined  by  the 
scale  for  pure  skim-milk. 

Again,  if  to  such  skiin-niilk  we  add  a  certain  pcr-centage  of  water, 
we  restore  to  it  its  proper  speciHc  gravity,  and  therefore  this  milk 
would  show,  with  ihu  centesimal  galactometer,  the  density  proper  to 
pure  milk,  and  hence  ibis  fraud  would  ei<<;u]>e  detection.  In  order 
tomeetcasesof  tbt3  kind,  which  arc  of  frequent  occurrence  —  namely, 
the  complete  or  partial  removal  of  the  cream,  it  is  recommended,  and 
indeed  necessary,  to  employ  the  lactometer,  and  ascertain  by  it 
whether  the  sanqile  under  examination  contains  the  proper  propor- 

■  «  16  centif  nde. 


■ 


MII^K,  AUTD   ITS   ADULTERATIONS. 


21% 


crewn  or  not ;    indeed  it  is  scarcely  posiible  in  any  case 
(0  come  to  certain  or  safe  conclusions  without  cmplojing  the  lacto- 


Tut  CurruiMAL  Q»i.tvTouwna 
(0»  a  r^rfwfrf  trait. ) 


90 


r-  lOO-    :3 


*^Hliio  P 


J 


MILKj   AND    ITS   ADCLTKRATI058. 

Where  the  gperific  prflvily  of  a  milk  is  very  light,  wid  thin  not  prft- 
iluced  by  a  large  excess  of  crcain,  it  is  due  tn  the  ndmixtiire  of  water, 
the  qunntity  of  vrhioh  may  be  defermined  with  con*;ideriibIe  necuracy 
by  thw  cuiiminn  hydromemr,  but  still  more  uccurately  by  the  centesimal 
g>diictoiut;ter. 

The  rea»on  for  hnving  two  ticales,  one  for  pure  and  the  other  for 
«kim-niilk,  it  will  be  perceived,  is  on  account  of  the  very  different 
densifies  possessed  by  eiich. 

The  great  advantage  of  ihe  centenimal  galnctometer  consi9t.<i  in  its 
centesimal  graduation,  whereby  caleulation  is  so  mui-h  facilitntod,  and 
in  the  wide  range  of  degrees  which  itaflords;  thus  while  in  the  hydro- 
meter the  range  of  degrees  from  pure  milk  to  milk  adulterated  with 
fifiv  per  rent,  of  wat*?r  is  only  fnmi  lOlG""  to  1031^  that  in  the  oen- 
teaimul  golnotometvr  is  from  50°  to  100";  by  which  arrangement  far 
greater  accuracy  in  estimating  the  density  of  mtlk  is  obtained  ;  thus, 
three  degrees  and  one-third  nf  the  galncrometer,  aj  we  have  seen, 
Corres|wuid  with  one  d^jee  of  the  densimeter. 

It  is  proper,  in  using  ihp-  ordinary  hytlrnmeter,  where  the  extremes 
of  temperature  are  great,  as  in  wintuT  and  summer,  to  take  the  spe- 
cific gravity  of  milk,  and  to  nsnkf  alh^wnncc  for  ihe  difTcrcnce  which 
temperalure  occasions ;  this  prc*'aulwn  bein^'  necessary  with  the 
hydrometer,  it  is  very  much  more  »o  with  the  centesimal  galocto- 
meier,  in  which,  from  the  delicacy  of  the  grnduaticm,  n  conipiirutively 
slight  alteration  of  temperature  occasions  a  difference  of  several  de- 
grees. 

When  it  is  desired  to  make  use  of  the  scale  for  skim-milk,  one 
portion  of  the  skim-milk  is  tn  he  set  aside  for  from  twelve  to  twenty- 
lour  hours  in  a  laolomeicr;  another  in  a  pan  for  the  same  length  of 
time  :  the  pcr-rentage  of  cream  to  he  noted  in  the  lactometer,  and  the 
density  of  the  uiilk  in  the  pan,  after  being  skinmied,  tiiken  in  the 
ordinary  nmnner  with  the  centesimal  galactometer,  corrections  being 
made  lur  the  tt^mperature. 

The  pamphlet  of  M.  Dinocourt  is  accompanied  with  coloured 
tables  of  forrections,  in  which  idlowuoce  Is  made  for  temperature,  — 
that  IS,  the  apparent  degrees  are  reduced  to  real,  —  the  degrees 
of  the  hydromeUT  or  densimeter  corresponding  with  those  of  the  cen- 
lesimul  galuclonu'ter  are  shown  side  by  side. 

Considered  altogether,  the  ceniesimal  galactometerof  M.  Dinocourt 
U  capable  of  affording,  especially  when  used  in  connection  with 
the  lactometer,  very  useful  and  accurate  indications :  murh  more 
60  than  the  ordinarv  hydrometer,  the  use  of  which,  in  taking  the 
specific  gravity  o(  milk,  ought  entirely  to  jiupemede  it. 

Ila  construction  will  be  comprehended  from  Af.  70. 

Of  all  the  constituents  of  milk  the  sugar  is  the  leaat  subject  to 
variation,  and  as  the  <leiKsily  of  the  senim  of  milk  is  principally  due 
to  the  'rjeeific   gravity  of  course  is  aUo  but  little  liable  to 

alter  fttemeut  is  founded  u{>oo  the  results  of  numerous 


MILK,  AND  ITS  ADULTERATIONS. 


m 


observationn.  It  therefore  long;  since  occurretl  to  115,  tbat  the  utilitr 
of  the  galactometer  might  be  greatly  enh.inccMl  by  the  iKlditiim  of  a 
centeHimat  .scale  for  tlie  serum  of  milk.  The  mlvanta^o  of  ihU  Hcnle 
wnuld  Ik*  ibat — starting  from  a  fixe<!  iminr^  the  normal  specific  gravity 
of  the  serum  —  it  wouI»l  ehow,  with  very  great  nicety,  the  extent 
of  the  more  usual  adulteratiuu  uf  milk,  imiiielvf  that  with  water;  lor 
in  pn»portion  u»  water  is  added,  fto  does  the  weijrht  of  the  wrrum 
diminish,  and  this  in  such  a  marked  manner  that  thequantiiyuf  water 
added  may  readily  be  deteruiined  in  per-centayes.  NumerouK  ohser- 
vatktns  ore  first  required,  in  order  to  fix  accurately  the  normal 
fi[>ecifie  gravity  of  the  serum  of  the  milk  of  tl»e  cow. 

MfthiHl  of  (ktermuiing  the  Cream.  —  The  amount  ofcream  is  deter- 
mined by  means  of  an  instrument  invented  by  the  late  Sir  Joseph 
Banks,  termed  a  lactometer,  lliis  consists  of  a  tube,  u<«ually  eleven 
inches  long  and  half  an  inch  in  diameter;  ten  inches  of  this  arc  gra- 
duated in  tenths  of  an.inch  —  that  ia,  in  hundredtlis  of  the  wbole. 
The  tube  is  filleil  with  milk,  and  set  H.>»idc  for  twelve  hourn;  the  cream 
a.scends  to  the  surface,  and  \Xa  amount  is  determined  by  the  thickness 
of  the  Btrutum  formed,  and  tvhi<:h  it)  ascertained  by  noting  the  number 
of  dej^CA  or  tenths  through  which  it  extends. 

Some  lactometers  resemble  test  tubes  in  slmpe,  and,  like  them,  are 
supported  in  racks  ;  they  arc  usually  graduated  only  in  the  upper  two 
inches;  uthers  are  provided  with  fei't,  and  are  frraduated  throughout 
their  whole  lcn<itb.  As  the  quantity  uf  cream  not  unfrequently  exceeds 
twenty  and  has  even  been  known  to  reach  eighty  per  cent,,  the  tubes 
should  in  alt  cases  be  graduated  for  nearly  tbeir  whole  length. 

The  construction  of  the  laitoincter  19  shown  in  the  accompanying 
wolxiciit,  representing  a  rack,  hulding  four  of  these  instruments. 

Cream  forms  more  quii-kly  in  warm  than  cold  we.ithur;  and  in 
making  comparative  observations  on  a  number  of  samples,  it  is  prnpur 
that  each  should  be  set  aside  in  lactometers,  at  the  same  time  and  for 
the  some  period. 

The  thickness  of  the  stratum  of  cream  formed  on  genuine  milk  ift, 
like  the  specific  gmvily,  subject  to  considerable  variation  ;  in  two 
extreme  coses  we  nave  met  with,  one  of  the  samples  showed  but  two 
degrees  ofcream,  and  the  other  eif^hty.  According  to  Dr.  Norniaiidy, 
the  tiiickne«s  of  the  stratum  of  cream  on  pure  milk  is  generally  from 
8  to  8|  per-centages :  M.  Dinocourt  finds  the  por-centages  t^»  range 
between  9  and  14^  while,  according  to  our  observations,  the  average 
does  not  exceed  Q\. 

It  must  be  remembered  that  London  milk,  as  delivered  to  houses, 
consists  iu  general  of  tlie  milk  of  different  cows  mixed  together; 
and  therefore,  iu  order  to  determine  what  ouuht  to  be  the  depth  of 
cream  fonned  on  po  'd  milk,  we  should  take  the  average  amount  ob- 
tained from  such  ntixe<l  milks. 

We  have  said  that  the  quantity  of  cream  varies  much  in  different 
aamplea  of  genuine  milk  ;  and  not  only  is  this  the  case,  but  it  should 

Q 


320 


MILK,   AND   ITS  ADULTEBATION8. 


also  be  known  that  the  amonnt  of  cream  yielded  by  any  sanip!e  of 
mitk  is   no  certain  criterion   by  which  to  judge  of  its   quality,   as 


ng.  71. 

Lactoiutis  axd  Staxd. 
(On  a  Fvrfnmf  Male.) 


The  dolleil  tlur*  ln>1imt«  Ibc  p«f-«-nlRr>  • 


iplH  of  tnilk  tium 


Rome  niitlca  are  rich  in  cream  and  deficient  in  casein  and  sugar,  and 
vicf  vertn. 

It  in  Mated  that  the  addition  of  a  small  quantity  of  warm  water  to 
milk  increases  the  lunount  of  cream  ;  the  belief  in  the  afcurocy  of  this* 
fUUcmcnt  is  general,  and  it  U  commonly  acted  upon  by  milkmen  ; 
nevertheless,  the  assertion  is  entirely  erroneous  —  the  addition  of 
water  to  milk  il*)es  nut  increiLse  the  quantity  of  cream  ;  it  merely 
fneilitatea  and  haiilens,  in  u  nin^t  remarkable  manner,  ita  formation 
iind  lepiirution,  ait  i»  shown  by  what  follows :  — 


MILK,    AKU  ITS   ADUtTERATIONS. 


327 


Six  lactometers  were  6Ueil,  one  with  pure  milk,  the  reinAimler  with 
tlie  same  milk  ililuteii  reKpectivuly  witli  ten,  twviitVi  thirty^  furty,  and 
fitly  per-centa;;e9  o!' water. 

Twt'ntv  ininutca  after  the  additiun  of  the  water,  the  laetometer 
ahowc'lf  in  the  milk  rontnining  fifty  per  cent,  of  water,  six  degrfes  of 
crL'am ;  in  that  with  forty  jier  cent.,  five  dejrrees ;  with  thirty  per 
cent.,  four  degrees  ;  with  twenty  per  cent.,  three  degrees ;  with  ten 
per  cent.,  one  degree;  and  in  the  pure  milk,  lialf  a  ilegree  only. 

At  the  end  of  forty  ntinutvs,  the  cre:ua  stuud  thus*  six  and  a  half 
dejjreca  on  llie  milk  containing  fifty  [ler  L-ent.  of  water;  aix  Ou  that 
with  forty  per  cvnt. ;  ti*e  ami  a  half  on  that  with  thirty  per  (.'ciit. ; 
five  on  that  with  twenty  per  cent, ;  four  and  a  half  on  that  with  ten 
|>cr  cent.;  and  four  on  the  pure  milk. 

At  the  end  of  twelve  liour^s  the  milk  with  fifty  per  cent,  of  wal«r 
showed  five  degrees  of  cream  ;  that  with  forty  per  cent.,  five  dejrrces 
and  three  quarlert»;  that  with  thirty  percent.,  six  and  a  half  de- 
preea  ;  that  with  twenty  \^t  cent.,  seven  degrees  ami  a  ([uarter  ;  that 
with  ten  |}er  cent.,  eight  degrees ;  and  the  pure  milk,  nuie  dep;ree8 
of  cream. 

It  thus  appears,  that  the  addition  of  a  large  r|uimtity  of  water  to 
milk  occasions  an  almost  immmliate  lonnation  of  cream,  but  doeA  not 
augment  the  amount;  of  this  fact,  in  iK>mc  ca:M.%  it  would  lie  an  itd- 
vantrtge  to  dairymen  to  avail  themselves.  The  adilitton  of  water  tn 
milk  of  ronrsc  lesfiens  ila  epecific  gravity,  and  80  fneilitate«  the 
ascension  of  the  creaiu. 

Tite  Lm'totu'iijtc. — S«me  years  since  an  instrument  termed  a  hirto- 
scofie  wa>  invented  by  M.  iJunne,  of  I'aris,  for  determining^  the  rich- 
ne^5  of  milk,  by  estimating  lUe  quantity  ot  butter  contained  in  it. 

We  have  procured  one  of  these  instrumt;nt9,  aeeompnuied  with  a 
deseriptiun,  and  directions  for  its  application  ;  frum  these  we  extract 
the  rohowing  observations:  — 

"  Milk  owt's  its  white  dense  colour  to  the  gluhulcs  of  fatty  matter 
or  buucr  which  it  contnins;  the  moie  numerous  these  gtubulcd  the 
more  opa>|ue  is  the  milk,  and  the  more,  at  the  same  time,  is  it  rich 
in  the  fitiy  ])nit  or  in  cream,  the  mure  or  less  opacity  bein^'  in  re- 
lation with  iLh  princiiKd  ipjality  —  its  richness  in  cream;  the  measure 
of  this  opacity  is  capable  of  ^ivin^  then,  indirectly,  the  measure  of  the 
riclnie»<i  of  the  Huiil.  am)  ut  indicating  Its  value. 

"Hut  the  degree  of  opacity  nf  milk  eannot  be  appreciated  upon  a 
mosA  of  the  fiuid  ;  it  is  not  possible  to  mea.sure  it  but  in  very  thin 
lavLTS,  and  it  is  this  which  is  done  with  our  hietcHcope.  ThI*  instru- 
ment is  constrnetcd  in  such  a  way  that  the  milk  may  be  examined 
in  it  in  layers  of  every  thieknes-*,  t'nnn  the  thinnest,  through  which  all 
objects  may  be  disttngulsheil,  up  to  that  which  ulh>ws  of  nothing  to 
be  |K*reeived;  it  give:*  at  onre  tli**  riehnvsii  of  milk  in  indiculing  the 
degree  of  opacity  to  which  the  prupiirtion  of  cream  stands  in  relation. 

Q  2 


2S8 


MILK,  AKB  ITS  ADULTERATIONS. 


**  The  instrument  coosiats  of  a  kind  of  eTe-fdaas,  composed  of  two 
tubes  sliding  one  within  the  other,  furnished  with  two  parallel  glasses, 
which  approach  each  other  up  to  contact,  and  separate  more  or  leas 


Ftg.Ti. 
Turn  LACTOtcon. 


the  one  from  the  other  at  will  by  means  of  a  very  fine  screw  ;  a  little 
funnel  destined  to  receive  the  milk  is  placed  at  the  upper  part ;  on 


I 


MILK,   ASD   ITS  ADLLTEHATION8 


the  nppositc  ftide  i^i  fixe<)  a  )miuUc,  wbk-h  nerves  to  hnltl  the  inslru- 
ment.  i'he  tuht*  wbicU  screws  witliiii  the  oiher  forms  the  anteriur 
or  ocular  part,  tliat  to  whiuli  the  eye  la  applied;  it  h  murked  with 
divisions  to  the  number  oi'20,  and  figures  which  indioiile  the  richuess 
of  the  uiilk. 

**  A  few  drops  of  the  milk  to  be  examined  are  poured  Into  the 
fiinneL  It  is  nuces^ary  to  ttdie  the  sample  of  milk  fruu  the  mass  of 
the  milk,  and  not  the  suiface  of  the  lii|uid  only,  where  the  layer  of 
cream  eoUectji;  if  then  the  milk  has  been  at  redt  for  some  time,  it 
must  he  H^riLated  a  little  in  order  to  mix  all  the  parts. 

'*  The  lunnel  being  full,  the  mmlar  tube  U  turned  from  right  to  left 
until  the  liquid  has  peneirutcd  betwtfc-u  the  plates  of  glo^,  and  col- 
lected at  the  bottom;  the  OL'ular  lube  in  then  turned  in  the  contrary 
direction,  from  left  to  right,  and  one  lookii  thruugh  it  until  the  tlame 
of  a  taj>er  or  candle  can  be  distingui.'<hed.     At  this  point  stop  and  ira- 

f>ress  a  slight  rotatory  movement,  until,  by  a  lillli:  manipulation,  the 
ight  id  lost  to  view,  without  going  beyond  the  moment  when  it  is  ex- 
tinguished, so  to  speak,  and  ceases  to  be  perceived ;  that  is  the  jmint, 
dcanitely,  where  it  is  ncce.-'siiry  to  stop;  it  is  only  then  required  to 
read  the  figure  of  the  division  to  which  the  uitow  corresponds;  that 
vre  supfKisc  will  be  25.  The  annexed  table  i^howa  to  what  degree  of 
richness,  or  to  what  proportion  of  cream,  tlic  figure  corresponds. 

"The  li^ht  ought  to  be  placed  at  about  a  metre  (at  least  three  feet) 
from  the  observer;  a  greater  distance  will  not  impair  the  aeeurocy  of 
the  operation,  but  it  is  not  the  same  if  one  looks  from  too  near. 

"One  may  a-wure  himiielt  of  the  accuracy  of  the  instrument  by 
adding  a  very  sniidl  quimtity  of  water,  or  even  gruel,  to  the  milk. 
Twenty  (legrees  of  wnter  are  sufHeient  to  change  the  transparency  of 
the  litpiid;  thus  milk  marking  2a,  will  mark  28  or  30  on  mixing  with 
It  a  little  water. 

^At  tbc  moment  when  the  milk  b  introduced  between  the  two 
plates  of  glass,  it  commonly  h»ppeu6  that  bubbles  of  air  are  enclosed 
w  the  layer  of  litjuid  ;  it  is  necessary  to  drive  them  out,  ami  this  is 
easily  done  by  imprefxiiig  certain  muvenients  on  the  milk,  by  sepa- 
lating  more  or  less  the  eye-pitce  so  lu*  to  cause  the  twopluteu  of  glass 
to  withdraw  and  approach  eaih  other  alternately.  When  the  trial  is 
tenniniitod,  the  eye-piece  is  to  be  removed  so  as  to  clean  the  instru- 
ment perfectly,  and  t^t  wijw  the  glasses;  the  gUsfCS  ought  always  to 
be  very  briglii,  and  ime  otight  to  avoid,  during  the  observation,  to 
tarnish  with  the  breuth  the  glass  of  the  eye-piece." 

Table  indicating  the  Riehneat  of  different  Kindt  of  Milk  after 
the  Degree  whtch  they  ahow  on  the  Lactuscope. 

Milk  of  cow,  giving  about  5  per  cent,  of  cream,  shows  40  to  35  on  the 
JacCoscope. 

Q  3 


aso 


MILK,   AND  ITS  ADULT£BATION8. 


Ditto  ilitto,  onlinary,  ^ving  frnm  5  to  10  per  cent,  ditto,  shows  3<3  to 

no  on  iivi  lac'loscDpe. 
TJillo  (liito,  KiiiliL-ienil)'  rich,  giving  from  10  to  ]<5  jter  cent,  ditto,  shows 

*iO  to  25  on  the  lacloacope. 
Dit(n  (lino,  very  rich,  giving  from  15  to  20  per  cent.  dJtto,  shows  25 

to  20  on  the  lactoscoiH'. 
Ditto  ditto,  excessiveijf  rich  (lost  extraction),  shows  20  to  15  on  tbe 

lacluscope. 
Ditto  ditto,  very  weak  (first  extraction),  shows  150  to  S  on  the  Ucto- 

scope. 
Milk  of  the  common  nss,  of  good  quality,  shows  from  50  to  80  on  the 

lactosciipe. 
Ditto,  very  weak,  shows  from  150  to  20  or  4  on  the  lactoscope. 
Milk  of  goat,  rich,  shows  10  to  15  on  the  lactosonpe. . 
Milk  of  woman,  rich  and  suhAtantiid,  ^nhows  20  to  25  on  the  lacto- 
scope. 
Ditto,  medium,  »hnws  30  to  35  on  the  Inctosrope. 
Ditto,  weak,  i«hows  40  to  45  on  the  lactoscope. 

It  must  Im;  rcuienibcrcd  tliat  the  lactoscope  has  regard  only  to  one 
elemt^nt  of  mdk,  and  does  not  e^limutu  the  amount  of  sugar  or  chrese. 
M.  J^onne  entertains  the  greatest  cunhdcnce  in  the  indications  which 
it  affiintB. 

The  (.•on^friiction  of  the  instnmiont,  and  mode  of  empluyment,  will 
he  more  riearly  understood  fn^mi  an  exan^inutiou  ot"  the  woodcut  on 
the  preceding  page. 

Si>mc  pcrsnns  form  their  judgment  nf  the  qtiality  of  milk  simply  by 
its  density,  regarding  all  Homplcs  which  do  not  indicate  a  certain  spe- 
cific gravity  t>f  inferior  ({ualitv.  ^V'c  have  already  seen  that  this 
method  is  very  fallacious  and  tliat  by  it  some  milks,  rich  in  uream, 
wouhl  be  pronounced  of  inferii)r  iiuulky,  in  con&e<juence  of  tlieir  low 
density;  while  othi.'rs  defioent  in  that  cfnstitoeiit,  would  be  declared 
of  superior  quality,  on  accnunt  of  iht-ir  high  density. 

OtherB  rely  U[ion  the  indk'utions  afforded  by  the  Ificlomoter,  which 
also  hiift  its  fallacies,  hut  whicli  are  not  so  great  when  the  instrument  is 
used  with  the  necei^sary  precautions,  as  those  relating  lo  the  S|»ecific 
pravily  of  milk.  I^ike  the  lactoscope  of  M.  Donne,  the  lactometer 
una  regard  to  only  one  component  uf  milk  —  namely,  the  fatty 
matter. 

'JTie  following  facts  wdl  show  how  fallacious  is  the  lactometer  in  some 
cases.  We  have  met  with  several  dimples  of  genuine  milk,  which 
gave  only  three  or  four  per-cent.ige»n(  creiini,  but  which  yut  |K>Sjtesse<l 
a  specific  gravity  of  1H30;  judged  by  thf  lacfnnietcr  test  alone,  stich 
milks  would  Im*  pronounced  by  all  lo  be  vcrv  jMxir,  and  by  some  even  to 
be  adulterated.  \ow  ihis  conclusion  would  lie  to  a  very  great  extent 
erroneous;  for  such  milks,  although  certainly  deficicni  in  butter,  have 
the  full  proportii>n  of  the  remaining  constituents — namely,  the  che»'se, 
and  the   sugar.     Again,   we  constantly  meet   with   smnpluti  of  uitlk 


I 


MILK.  AND   ITS  ADULTEUATIONS, 


231 


l^viiBBHVi^  ^^  morR  pcr-C(^ntA^  ofcrcflin,  and  which  nftvcrthc*- 
Ims,  at  lAl^wn  by  the  spcrifio  gravity  of  the  Rcrum,  arc  unquefitionubly 
wlolteratetl  with  large  qiianliti(!i>  ot'wutcr. 

The  observer  who  relied  upon  the  indications  of  the  lactometer 
would  huve  ro'^urdeii  nucb  samples  as  uf  average  ((uality.  The 
ini|uirer,  therelbr*.*,  shixttd  not  rely  solely  upon  the  bpeeitie  gravity  or 
lactometer  te^ts,  but  in  all  cii.-«e9  employ  both,  the  one  acting  as  a  cor- 
rective of  the  fiilhicies  of  the  other. 

For  nil  practi<:iil  pur])ose<i,  the  above  methods  of  examination  are 
sulficienl.  Should  it  be  cli-mred  to  institute  a  very  careful  analysis,  we 
may  then  adopt  the  processes  deecribed  by  iiaidlen  already  given. 


On  the  ADULTEaATioNs  or  Milk. 

The  most  prevalent  and  important  adulteration  of  mllic  iis  that  with 
water:  now  some  few  persons  who  have  not  reflected  closely  upon  the 
matter,  may  be  di.<4pt»(CMl  to  make  li«;ht  of  the  adulteration  of  milk  with 
water,  and  to  speak  in  raiher  facptious  terms  of  the  cow  with  the  iron 
tail ;  but  it  ia  surely  no  light  matter  to  rob  an  im])ortant  article  of  daily 
consumptioni  like  milk,  of  a  large  portioo  of  its  nutritious  consti- 
tuents. 

Kut  the  adulteration  with  water  is  not  the  only  adulteration  to  which 
milk  is  liable ;  the  large  addition  of  water  frequently  made  to  it,  so 
altera  iU  appearance  as  to  cause  it  to  as.iumu  the  »ikv-blue  colour  so 
familiar  to  us  in  our  yehtHtlboy  days,  and  so  reduces  its  flavour,  that 
it  l>ecoines  neceiii«ary  to  liuve  re*'ourao  to  other  adult<>rating  ingre- 
dients, namely,  (renclfs  to  sweeten  it ;  luth^  to  brini;  out  tin*  flavour ; 
snd  anno/to,  about  which  wc  shall  have  much  to  say  hereafter,  to 
colour  it. 

Further,  t^e^e  is  no  question  but  that  chulh,  cerebral  nuitter,  and  /itarch 
have  been  and  are  ocoasionnlly,  thou;:h  rarely,  uuiployed  in  the  adul- 
teration of  milk,  althougli  it  has  not  happened  to  ourifelves  to  meet 
with  these  substances  in  milk. 

•Starch  and  cerebral  mattr-r  have  been  met  with  at  different  times  by 
more  than  one  observer.  I*rofesfM»r  Qin-'ck^tt  has  tn  his  possession 
some  drawin^rs  made  Irom  sampler  of  adulterated  milk,  showing  the 
prcftence  ol'  both  slarch  and  cerebral  matter. 

With  regard  to  the  use  of  chalk,  a  manufacturer  of  preserved  milk 
recently  informed  us  tliat  it  sometimes  happened  to  him  to  find  car* 
bonale  of  lime  or  chalk  at  the  bottom  of  the  eva[»<»ratin<j  didhes  or  pans 
on  the  evaporation  of  large  quanlilieif  of  London  milk. 

There  is  ul»o  good  reason  for  believing  that  tttrnwric  as  well  as 
annatto  arc  »imii*tiines  used  to  culour  milk  and  cream  ;  also  gum 
tragaetath  to  thicken  cream,  ami  aafla  to  prevent  its  becoming 
sour.* 


*  Mr.  Gsf  fttalM  th«l  niUk  U  aDniftliRPB  Ailullrratotl  wUlt  dcroctloD   of  builvil  vliile 
carrotk. 

Q  -4 


fidi 


MILK,   AKD  ITS  ADULTERATI0N8. 


Further,  it  has  beon  stateil  that  frunif  dextrine,  and  emulsion  of 
hemp  sved  have  hean  atiipUtyed  ;  the  u&e  vf  the  iiittcr  urtiule  is  but  little 
probable. 

A  practice  frequently  rt»sorted  to,  nlib<tu|;h  it  is  not  an  adulteration, 
fthould  here  l>e  inenttoneii ;  n  piirt  ctr  even  the  entire  nf  the  creiun  ia 
removed,  (tn<3  th(*  skimmod  milk,  mixed  with  Bome  fresh  milk,  subse- 
quently Bold  a^  whole  milk. 

An  inj;enioue  writer,  who-tc  name  wg  dn  not  at  the  present  ainment 
remember,  bos  cunsidere*!  the  ^ubjeet  <*t'  ihe  supply  of  London  with 
milk  stutisueully.  and  Ik-  Iiuk  arrivfd  at  the  euncdurtton  tbiit  the  number 
of  cows  8Up|ilyiny  Loiidnn  is  iH<t  more  than  Hulhcient  to  provide  euch 
person  with  about  a  luhlespoonfiil  ptir  day.  It'  this  !*tii1trnient  is  cor- 
rect, some  iilen  niiiy  be  formed  of  the  extent  to  which  wnter  is  made 
to  do  duty  for  mtlk. 

7*he  rcMidti  of  the  examination  of  Twcaty-atx  samples  of  Landrm  milk 
were,— 

Thnt  Txcelee  tcere  genuiMy  but  of  thcae  two  showed  a  deficiency  of 

cream. 

That  Fourteen  were  tuivUeraterl,  the  adnllemtion  cnnsistin;!  princi- 
pally in  the  addition  of  water,  the  per-centagea  of  which  ranged  from 
10  to  .'SO  per  cent,  or  one-half  water. 

The  specific  gravities  of  the  rnilh  varied  from  1030  to  lOlo,  of  the 
serum  frnm  lOiiS  to  lOlU^  the  cream  i'rom  29  to  2  per-centi^es,  the 
avernge  being  nearly  lo  jh-r-centages. 


On  the  Detection  of  ihe  Adtdteratiuna  of  Milk. 


The  articles  employed  in  the  oduhcrfltion  nf  milk,  the  metb 
for  the  discovery  of  which  wc  buve  now  to  describe,  are  water,  su^far 
including  treacle,  suit,  annatto,  turmeric,  gum  tra^acauth,  stavcht  oere* 
brul  matter,  and  chalk. 

Certain  :dle<;ed  adulieraijijnH  of  milk,  either  not  likely  to  be  praC' 
ti8e<l,  or  but  niruly  ri-sorted  lo,  it  is  not  necessary  to  notice. 

There  arc  two  geiienil  incthmis  by  which  the  fact  ot  the  adulteration 
of  milk  may  be  determined  ;  the  one  ludiret-t,  a^  by  aqnantitative  ana- 
lysis of  the  ndlk  for  its  more  inquirtant  oonstiliientfl,  ami  by  the  de- 
fieiency  of  one  or  more  of  which  the  cxistenee  of  adulteration  may  be 
inferred  ;  the  other  direct,  as  by  iletuctiim,  either  throu<!h  chemistry  or 
tlie  microecopc,  of  tlie  adulterating';  Niihstunce  ur  substances. 

In  some  cases  these  two  liiethmLt  may  be  combined. 

The  methods  by  which  the  norm^il  constituents  of  milk  may  be  de- 
termined quantitatively  have  idre-idy  bt'cn  described. 

On  the  Detection  of  IVater. —  Milk  bein;;  much  heavier  than  water, 
«rhen  that   liquid  is  added   to  it  the  sfKcific  gravity  of  the  mixed 


I 

I 

I 


I 


UlhK,  AND  1T8  ADULTEKATION8. 


9S8 


article  is  \e»i  tLnn  that,  of  f^ennine  milk,  ami  the  diminution,  within 
certain  limii.s  \a  proportioiiuic  lo  the  ({unniitv  of  water  adde^l.  In 
fh'*  knowlciipe  of  these  fnctH,  we  are  fu^ni^he<l  with  aniethrxl  whereby 
the  iKluUoration  of  luilk  with  water  tiioy  be  determined  fjuanli- 
Ulivt'Iy. 

This  may  he  done  by  tnkini;  the  specific  gravity  of  either  the  en- 
tire milk,  of  skimmed  milk,  or,  still  letter,  of  the  serum. 

Aeeordiu**  to  M.  Lasnuigne,  pure  milk  at  S0°  F.  — 


I  According?  to  our  own  experiments,  the  following  are  the  ordinary 

I  «peol6c    gravities    of  milk   adulterated    with    various   proportions  of 

I  water ;  — 


Has  a  specific  gravity  of     • 

Wirh  25  piirts  of  wuter 
Will)  33  pftrU  of  water 


Water  per  Cent. 

Water  uone 
Al>out  \5  parta  - 
About  20 
About  35 
About  45 


1021 
1020 


Sp.  Gr.  or  Milk. 
1030 
1026 
10-23 
1018 
1015 


But  since  the  spi?ci6c;  gravity  oi'  even  genuine  milk  is  subject  to 
wide  runjieti,  in  certain  exceptional  cases,  owing  to  the  variable  rpinn- 
tities  of  fatty  matter  present,  it  is  in  all  cases  better  to  take  the 
specific  gravity  of  either  skim-milk  or  the  serum. 

The  fpeclfic  gravity  <A' nktm-miik  with  various  proportions  of  water, 
as  deduced  from  the  centeaimal  galactometerf  u  as  followtc  — 


Wu*r. 

SUm.Ullk. 

8p. 

Gr. 

of  Sktm-MUk 

Nfme 

. 

100 

31 

10  paHs 

- 

l»0 

27 

20  - 

- 

80 

25 

30  - 

. 

70 

21 

40  - 

• 

60 

19 

50  - 

- 

60 

It) 

Results  still  more  accurate  may  be  obtaincfl  by  taking  the  q>ccific 
grnvily  of  the  serum  of  milk,  since  this  is  subject  to  much  less  voria- 
tion  than  either  the  whole  or  skini-uiilk.  The  casein  ami  butter  ure 
easily  rumowd  by  the  atlditiun  of  a  few  drops  of  acetic  acid,  a  tpiuntity 
indeed  so  ».ma]I  iis  m^rtrcely  lo  aflect  the  gravily  of  the  serum. 

The  following  table  exhibits  the  results  of  various  a<lUttions  of  water 
to  the  scrum:  — 


234 


MILK,    AND   ITS   ADULTERATIONS. 


Water. 

Pure 

10  parts 

20 

80 

40 

ffO 


5«rum. 
39 
S5 

22 
20 
17 

14 


^ 


In  taking  the  specific  gmvity  of  the  serunt,  niid  in  determining  h*oni 
lliis  wh^ftlier  watiT  hus  been  uddeil  or  not,  llie  only  fullacy  to  which 
the  observer  is*  sulyect  is  lliKl  by  tlie  atlilition  of  ^iccbarmt*  inntler, 
wliich  wnult]  cause  the  serum  to  weiyli  heavier. 

Jiiit  in  the  cose  of  whtile  milk  there  are  other  sourcca  of  falUcj  to 
whicti  reference  to  some  extent  has  already  been  made,  and  against 
which  it  is  neccssury  to  gimrd. 

Thus  u  milk  mny  possess  the  proper  spocific  gravity,  and  yet  be_ de- 
ficient of  erenm,  whieh  mny  have  hin-n  ubslnicted  ;  ajinin,  it  may  be 
several  de;*rces  lij;hler  than  orUiuury,  and  yet  may  be  perfectly 
genuine,  this  arising  from  tlie  presetice  uf  itn  unusual  quantity  of 
fatty  matter. 

In  order  to  guard  against  these  falbicies^  therefore,  it  is  always  ne- 
cessary not  only  to  tAKe  tlie  weight  of  the  milk,  but  also  to  measure 
the  r|uaiitity  of  cream,  wineli  should  not  be  lew  than  8  per-ecnlagos. 

The  instrumenlfl  by  which  tlui  weit;ht  of  uiilk  is  taken  and  the  cream 
measureil  have  alreftdv  been  described. 

One  method  by  whit  h  the  quantity  of  water  may  in  genorfll  be  in- 
directly estimated  is^  by  determining  quantitatively  the  amount  of 
flugiir  present. 

On  the  Detection  of  Stiffar.  —  The  sugar  Uf^ed  is  usually  brown  sugar 
or  treacle :  the  presence  of  these  mny  in  cenenil  be  determined  as 
follows :  —  The  casein  anfl  butter  are  to  be  precipitated  by  means 
of  acetic  acid,  and  the  sei*um  cvuj>oratcd,  a  very  getitle  heat  only 
being  useit,  and  the  colour  of  the  residue  particularly  noticed ;  if  it 
is  darker  than  ordlniiry,  the  presence  ttf  sugar  may  be  suspected.  The 
resi<lne  may  then  i>e  di.*solved  in  distilled  water,  :i  little  yeast  added, 
and  the  solution  exftosed  for  some  hours  at  a  temperature  of  between 
70°  and  SO'*  F.  If  fermentation  ensues  '*  it  is  a  sure  sign  of  the  presence 
of  sugar,  for  milk  sugar  cannot  fenncnt,  at  least  in  so  short  a  lime, 
and  the  fermentation  is  never  britk.  Hut  the  smallest  itmportion 
oC  su|!ar,  either  grape  or  cane  8u;;ar,  very  speedily  gives  ru'-e  to  a 
tumultuous  fermentation."  —  Nonmmhj.  The  carbonic  acid  nmy  be 
coneole<l,  and  the  sugar  calculated  either  from  it  or  from  the  alcohol 
formed. 

If  eanc  sugar,  or  decoction  of  carrots  which  contains  it,  hos  been 
added,  jyerhaps  the  best  method  of  proeoeding  is  the  following  :  remove 
the  supar  of  milk  by  means  ttfKehlings  solution,  and  nflerwardBdetcr- 
luine  whetlier  cane  sugar  is  present  by  the  fermentation  test. 


MILK,    AND   ITS   ABULTEBATIOXS. 


935 


On  thfi  Detection  of  Starch.  —  For  (he  clctection  of  stari:]i  in  milk 
and  creuiii>  the  microscope  furnishes  the  readiest  and  most  certain 
lueunii.  A  little  of  the  milk,  spread  out  in  a  very  thin  Blrutum,  should 
be  examined  under  the  micro5copet  the  exuuiinution  bein^  iiided 
by  the  use  of  tincture  of  iodine.  For  the  quuntitfttive  determination 
of  the  starch,  vhicb  will  not  often  be  rct|uirL'd,  we  uxixy  proceed  oa 
follows :  the  curd  is  to  lie  separated  by  nie»ii8  of  ftcettc  acid,  col- 
lected on  u  filter,  dried,  and  Ireutcd  with  ellier  ;  this  will  remove  the 
fftt,  and  the  starch  and  casein  only  will  reniuln.  Lastly,  tlie  casein 
may  be  removed  by  means  of  a  weak  solution  of  potash.  A  more 
accurate  plan  19  to  convert  the  starch  into  prii|>e  sugar,  and  to  uul- 
culate  its  amount  from  this.  l*be  sugar  of  milk  nnif«t  Brst  be  re- 
moved from  the  evaporated  milk  by  digestion  with  alcuho],  and  the 
processes  followed  for  the  conversion  of  starch  into  sugiu',  and  the 
dctcrininfilion  t.f  its  amount,  described  in  the  artiule  Sugar. 

On  the  Detection  nf  Gum  Antbic  and  <V«m  Trof^acanth.  —  Thegenjra 
of  milk  is  to  be  evaporated,  and  the  residue  boiled  and  digested  with 

cohol,  which  wdl  tiikc  up  ihc  su^ar  and  leave  the  gunu  Or 
slcohol  may  be  poure<I  into  the  whey,  the  pum  will  be  precipitated, 
and,  when  drie<i,  may  be  identified  by  its  appearance. 

ior  the  detection  of  gum  tra;j:acanth  we  are  recommended  Ut  boll 
the  milk,  and  leave  it  at  rest  for  some  hours,  when  n  }>elatinoustranslucid 
dt^poitit  will  be  formeil,  which,  being  wa»bcd  with  a  small  quantity 
of  water  and  tested  by  a  few  drops  of  solution  of  iodiui*.  proiluces  a 
blue  colour  because  gum  tnigacjinth  contains  starch.  The  starch  h 
plentiful  nnd  is  in  the  form  of  starch  cor{macles;  these  arc  rather 
timall.  but  vary  much  in  .size  ;  many  are  irregular,  some  arc  rounded, 
others  are  s<jniewhat  polygonal,  while  a  few  are  muller-sbaped  :  in  the 
more  perfei't  gniins  11  rounded  hilum  is  Uistinctly  visible. 

On  the  JJrteclion  of  Cerebral  Alaiter.  —  'I'he  jircsence  of  cerebral 
matter  in  milk  may  be  determined  with  certainly  by  means  of  the 
micn»s<*opc,  p<irtion9  of  the  nt-rvc  tubules  being  readily  discovered 
with  that  instrument.  jL«i  shown  in  the  engraving.  Pif^.  7ii. 

On  the  Detection  of  Chalk.  —  If  llie  milk  be  diluted  with  water  and 
set  asi<le  for  some  hours,  part  of  the  chalk,  if  present,  will  have  sub- 
aided  as  a  precipitate,  when  it  may  be  sufficiently  ideutifici  by  its 
rtppeurance  and  its  effervescence  with  aiids.  Or  a  imrtion  of  the  milk 
mav  be  evaporateil  to  dryness,  tlie  residue  incinerated,  and  (he  chalk 
esiimjtted  from  it  in  the  manner  pointed  out  in  the  article  on  Tea. 

On  the  Dftectian  of  Suit  —This  must  be  det6rmine<l  from  the  ash  by 
the  process  descrilied  under  Annatto.  The  saline  tnste  of  the  ash 
will  show  the  presence  of  salt  if  that  substance  bus  been  employed. 

On  the  Detection  of  Annatto.  —  The  presence  of  aunatto  is  rendered 
probable  when  the  milk  evjiporaiwi  di)wn  to  a  small  quantity  present* 
n  reddish  or  orange-rod  colour  ;  if  this  colour  is  materially  altered  on 
the  addition  of  an  acid  and  an  alkali  to  the  milk,  being  rendered  pur- 
plish by  the  one  and  of  a  brighter  red  by  the  other,  its  presence  is 


236 


MILK,    AND   ITS   ADULTEUATI0N8. 


certain.  Lastly^  by  means  of  slcohol,  the  colouring  matter  may  be 
dis;iolved  out  ol*  thu  Aoft  re^tiihiu  ofeYnpariiteil  milk,  and  the  effects  of 
tbe  reaj^enU  muntioued  tried  upon  the  ulcoholic  extract. 


rtg  73. 
Uiui  ADOLTS«Aisp.wmi  Sflnr'g  BRiiiti. 


'^o^^: 


^.'    oC?. 


*  • 


^oJ-O' 


;»^45^~^.8 


Oh  the  Detection  of  Tttrmeric.  —  If  turmeric  has  been  used  in  aulv 
stance  to  colour  milk,  it  would  be  possible  tu  dt:tect  in  some  cases  the 
tunneric  celU.  H(»wever,  it  is  best  in  nil  cnses  to  proceed  hy  the 
method  indirnled  for  the  discovery  of  anruiito.  The  chief  difTerenoc 
is  that  the  lunncrie  is  rendered  deep  brown  by  alkalies. 

li  is  of  eoiirsc  rorely,  if  ever,  necessary  to  examine  milk  for  more 
than  two  or  three  iif  the  articles  above  cimnienttcd.  In  general  it  if 
sufljcient  to  determine  whether  water,  the  ordinary  adulteraliun  uf 
milk,  has  been  added  or  not. 

The  fullowin;;  Atalistit-s  regardin;;  the  quantity  of  milk  consumed 
are  by  Mr.  Itraithwaite  Poole.  The  consiimpli(m  in  the  United 
Kingdom,  excluding  chee^',  butter,  &c.,  is  taken  at  almut  1 150  millioa 
quarts  annually. 

*^  Mr.  Poole  assumes  that  an  average  milk  cow  yields  7  quarts  of 
milk  as  a  daily  average^  and  that  the  retail  price  is  3</.  per  (juort ; 
and  from  these  data  a  result  is  arrived  ut,  that  the  whole  supply 


FLOUU   AND  BREAD,   WITH   THEIR   ADDLTERATIONS,    237 


re<|uirGff  4^0,000  m'llcb  c<iw!i,  and  l]iat  xhn  retuil  value  auiounti  to  the 
prtMligious  Slim  of  14,000,000/.  per  annum. 

"But  limitin^r  the  inquiry  to  London^  the  itainc  aiitlinrity  AftAumea 
thftt.the  rarefuUy  rearetl  c«w8  ihat  Turnidh  luiwt  of  ilie  miiiply  t*i>r  the 
metropT)]!!!  yield  9  (quarts  yter  daily  aver&j^e ;  thiit  the  riuinbfr  lima 
employed  is  24,000 ;  that  tbo  qunntitr  of  milk  consuuK'd  Id  about 
IHQ  iiiillioii  cjuurtH  annually,  and  that  the  conaumcra  puy  not  leas  than 
1,600,000/.  for  il." 

The  following  detnilK  rcspectinjr  the  cost  of  milk,  and  it*  conveyance 
tit  Lniidnn,  are  nlso  on  tht*  authority  of  Mr.  Poole. 

"  The  railway  conipanii'8  iisu»llv  charge  at  the  rale  of  three  farlhinga 
per  galloiK  for  carriage,  if  the  dii^tnnce  Iw  within  fttrty  rniles,  and  h/. 
if  for  u  lnnj;cr  distance;  relurniaif  the  empty  can3  free  of  charjte. 
Nowr  this  milk  is  suld  bv  the  farmers  to  lar;rc  dealefit  at  from  5fl, 
to  yd.  per  j;mIUhi  ;  the  dealers  sell  it  to  retailers  at  from  7ti.  to  9d, 
per  gallon;  wliiU-  the  retailers  sell  it  Uj  the  housekeepers  of  the 
metropolis  at  from  3d.  to  4i/.  per  quart.  Nor  is  this  all;  the  neat 
milk  at  say  Sd.  per  *«allon,  beeomes  too  often  milk  and  water  at  4d. 
per  quart.  Con^iderin^  that  crtam  commands  a  price  of  from  2*.  to 
3*.  jM-r  quart  in  London,  milk  certainly  cannot  brinj;  in  less  than  5rf. 
to  6f/.  |M>r  quart  to  the  relHiler.H.  U  is  estimated  that  in  \H5A  the 
quantity  of  milk  brought  by  railway  to  London  ronsiderubly  exceeded 
.3,tKH>,000  quarts,  of  which  by  for  the  largest  proportion  travelled  on 
the  Eastern  Counties  Kailway."— Z)c/d(r«  Food  of  London, 


FLOUR   AND   TIKEAD,    WITH    THEIR 
ADULTKBATIONS. 

Tna  word  Bread,  adopted  a.«  the  heading  of  this  article,  is  employed  in 
a  generic  sense,  and  is  intended  to  include  the  several  varieties  of 
brcod  prepare*!  from  the  flours  of  the  seeds  of  tlie  diiferent  grasses 
employetl  for  bread  making. 

As  bread  is  made  from  flour  of  various  kinds,  it  is  necessary  to 
take  into  consideration^  in  the  first  place,  some  particulars  in  relation 
to  the  several  kinds  of  llonr,  a.<4  their  chemicai  con)[>niiition,  mioro- 
scopical  structure,  and  their  properties  and  differences. 

White  there  are  important  dii^linctions  to  be  noticed  between  each 
of  (he  Hours  employed  in  the  manufacture  of  bre^d,  there  are  also 
certiiin  [Mtints  of  re^emVdance. 

Thus  every  flour  used  in  the  preparation  of  bread  consists  of  mVrv- 
^enised  and  hon-nitrogenUed  elements  or  constituents  :  the  former  are 
vegetable  ^"irfn,  aihumen,  cwufinc,  Ikc^  which  have  been  named  after 


338 


FLOUR   AND    BKEAD, 


^ 


Ih6  mrresponding  prot<?ino  compounds  extitting  in  animal  substances  : 
llie  liuier  are  aUtrchy  dexirine  (\t  gum,  und  siigar  —  proUuuU  more  par- 
liculiirly  of  the  vegetable  kingdom. 

The  chief  flours  ar<f  those  of  wheat,  barley,  rjre,  oat,  Indian  com, 
and  rice. 

>VuKAT  Floub. 

TlR»re  are  Beveral  distinct  species  of  wheat ;  that  which  is  chiefljr 
cultivated  in  this  country  is  the  Tritic.um  vnlgare ;  of  (his  there  are 
(wo  vurietiefl —  T.  trstivttm^  or  Riiinmcr  whent ;  nnii  2',  hyftennmi^  or 
winter  whe»t :  the  former  is  sown  in  the  spring,  and  the  latter  in  the 
nutumn.  Of  these  viirieliefi,  again,  there  are  several  miKliftcations, 
into  the  deseriptioii  of  which  it  in,  however,  not  necessary  to  enter  on 
ihe  present  oeeusion. 

\VheiLt  seedit  i»r  grains,  ns  brouglit  tn  the  market,  and  as  supplied 
to  tlie  miller,  are  deprived  of  their  /w/^ff,  or  huuks. 

The  ninnlwr  of  piut.i  into  which  ground  wheat  is  separated,  ;uid  the 
amount  of  each  vit;lded  by  piven  qnuntitiefl,  viii  y  according  to  the  cha- 
racters of  the  wlieiit,  uihI  the  prucesses  udupted  by  different  millers. 

In  wht-ats  whii-h  are  liunl,  (he  inti'guuient<i  se]mrate  with  difticulty, 
and  therefore  (he  llour  pnidmeii  from  these  usually  contttins  a 
greater  proportitm  of  udlnTcnt  hran  than  ih)  those  ttourn  procured 
from  wheats  which  are  soft,  and  whiuh  part  with  their  epidermic 
coverings  more  reinlily. 

According  to  Mr.  lUrd,  a  miller  of  Darlfurd^  in  KenU  the  follow- 
ing are  the  proiliicts,  wiili  the  ipiaiitities  ubiaincJ,  of  one  nuarter,  or 
eight  bushels  of  ground  wheal :  — 


/t^. 


"  Produce  of  One  Quarter  aj  irAcd/,  it^ighin. 

Flour  -  - 

Uisruit,  or  fine  middlings 

Tnfi|iings,  or  specks    -  -  .  -  - 

Ik>t  pollard,  Turkey  piiUurd,  or  Iwcnty-ijenny 
Fine  pulhird  -  -  -  -  . 

Bran  and  coarse  pollard         -  -  -  - 

Loss  sm>tu!tiL'd  by  evu|HiratJon,  and  waste  in  grinding, 
dressing,  &c.  -  -  •  -  ■ 


303  llu. 

10  „ 

8  » 

15  „ 

18  .. 
60 

11 


29^ 


504  lbs." 

Aa  it  is  frequently  a  matter  of  much  im|K>rfance  to  determine  the 

conipa"«ifi<m  nt    smnples  of  wheat  flour,  wc    will  now   describe   the 
various  steps  by  whirh  the  analysis  umy  be  clfi'i'ti'd. 

A  wei;'hed  f|uiiniity  of  flour  is  to  be  made  into  a  paste,  and  well 
knendetl,  either  on  a  Meve  or  in  a  piece  t>f  mut^lin,  water  beinf;  poured 
over  it  until  it  ceases  to  acquire  h  utrlky  colour ;  the  water  carries 
away  the  starch,  and  dissolves  nut  the  nlbuiueii,  sugar,  gum,  and 
suits,  while  the  mase  left  ou  the  filter  consists  of  *^  crude  gluten." 


WITH  THEIE  ADCLTEHATIONS. 


239 


This  crttde  gluten  is  iteelf,  however,  coniiMiunded  of  no  less  than 
four  (.lislinct  sub.tUinceit  —  via.,  gluten,  vcgetHble  fibrine,  a  very  small 
quantity  of  oiucine  or  cueitie,  aud  oil,  in  the  following  proportions : — 


Gluten 

Vcjfetable  Bbrino 
Mucine  (casvine  ?) 
Oil      - 
Starch  (accidental)     - 

Crude  gluten   - 


20 
72 

4 

37 
-    ft  small  quantity. 

997 


Gluten.  —  This  substance  is  obtaine<l  by  boilinf(  crude  ||;luten  in 
alcohol,  which  extracts  tht;  glutei),  ciiseine  or  mucine,  and  the  uil. 
The  casetne  is  deposited  on  cooling,  nwd,  after  separation,  the  resitlual 
liquid  is  evaporated  unlit  an  adhet^ive  mass  is  obtained,  from  which 
the  nil  is  extracted  by  ether,  and  gluten  atone  remains. 

Vegetable  Jubriue.  —  This  is  insoluble  in  alcohol,  and  forms  the 
chief  part  of  the  crude  gluten  ;  it  U  left  nearly  in  a  pure  slate  iifieT 
the  action  of  that  reagent.  It  (uuch  resembles  in  its  composition 
muscular  fibre. 

For  the  other  cone^tiluents  of  wheaten  0our  we  must  search  in  the 
water,  whtcti  has  jiossc'd  tlir(iu;:h  the  sieve. 

SUtrch. —  The  stureh,  after  remaining  suspended  for  a  time  in  the 
water,  sul>sid**«,  forming  a  precipitate;  this  may  ha  readily  obtained, 
and.  after  drving,  its  amount  determined  by  weighing. 

Vegetable  Albumen.  —  This  substance  is  procured  by  boiling  the 
water,  whereby  the  albumen  is  coagulated,  and  lorms  shreds  or 
Hakes,  which  ri»e  to  the  surface,  where  they  coltecl  ns  a  pellicle. 

CwKitie.  —  After  (he  separation  of  tlie  oibuinen,  a  little  ucetic  acid 
is  to  be  added,  which  throws  down  tiie  cnseine.  'i'he  mucine  (nr 
caseineV)  present  in  crude  gluten  is  soluble  in  alcohol,  from  which, 
on  cooling,  it  is  thrown  down  in  the  form  of  while  Hocculi. 

Oil.  —  The  gn»»ter  part  of  the  oil  in  present  in  the  tmter  part  of  the 
grain,  frfim  which  it  follows  that  the  hran  contains  a  larger  profHirlion 
of  oil  lliiin  the  central  part  of  the  gmin.  It  Is  best  obluined  by 
digesting  whole  nr  bruised  wheal  in  ciher.  AVhen  wheat  paste  is 
wtt&hed  in  water,  part  of  the  oi!  passes  away  with  it,  and  part  remains 
in  the  crude  gluten. 

SHt^ar, — The  sugar  present  in  wheaten  flour  is  of  the  kind  denomi- 
nated glvcone :  its  lunount  is  deterndned  by  evaporating  the  water  to 
dimness,  and  dissolving  the  sugar  out  of  the  residue  by  means  of 
alcohol,  which  being  in  its  turn  evaporateil,  the  sugar  is  deposited 
in  a  granuhir  or  semi-crystallised  atule,  and  may  be  collected  and 
weighed. 

Qvm.  —  The  remaining  pnrUof  the  residue  of  the  evaporated  water 
conststa  of  gum  <>r  dextrine,  iusuluble  in  olcuhol ;  this  also  &huuld  be 
dried  and  weij^hed. 


FLOUR   AND   BREAD, 


Wa/*r. — The  quantitj  nf  wat«r  present  in  wheat,  on  an  averafte, 

viiriea  from  fifteen  to  seventeen  per  cent.,  ami  is  j^retiler  in  new  than 
in  ulil  whcat^  nnd  it  is  this  circuuidtaiiue  which  luokcs  the  former  of 
lest  value  tlian  the  latter. 

Mineral  awl  Saline  Comtittienfg.  —  The  more  important  of  these  are 
silieute  of  puUish,  and  the  iilkaline  and  earthy  pli()8|ibati»,  which  are 
present  in  considerable  nmouiit  For  ordiiinrv  purposes  it  is  n<«t  ne- 
cessary to  niiike  90  precise  an  analysis  as  tliat  iiidicjated  «bove  ;  it  will 
be  sufficient  to  fliieertain  the  ainoiint  of  crude  gluten  present  in  a  given 
quantity  of  flour. 

To  determine  the  nufintity  of  this  gluten,  n  little  instrument  has 
been  invL-nled  by  Mr.  liuland,  termed  tin  *'  aUurometer** 

Of  tliitt  instrument  the  foUowitig  dewjripliun  is  given  by  Mr.  Mit- 
chell :  •— 

**  it  consists  nf  a  hollow  copper  cylinder,  about  aix  inches  long^,  and 
from  three-quarters  of  an  inch  to  an  incli  in  diameter.  It  han  two 
principal  piirta  ;  the  one,  abmit  two  inches  hut;;;,  \s  ch»5ed  at  one  end, 
ibrminji  a  kiml  of  cu[»  capable  of  containin;^  about  210  grains  of 
fresh  gluten;  it  screws  into  the  remainder  of  the  cylinder.  The 
cylinder  boing  charged  with  gluten,  is  heated  to  iibout  4'JO'^  in  an  oil- 
bath.  Thu  i^iuten  by  this  treatment  swulls,  and  accoriling  to  ita  rise 
in  the  tuLie  (which  may  be  measured  by  a  trr^i^lunted  slem)  si>  is  ltd 
quality.  Gtnid  fliMtrs  furni:$h  u  gluten  winch  augments  to  lour  or 
five  limes  its  uriginal  bulk  ;  but  bud  tl<>oi>  give  a  gluten  whioU 
does  not  swell,  becomes  vi<(cous  and  nearly  tliiid,  adhering  tu  the  siiles 
of  the  tube,  and  giving  off  occasionully  a  disagreeable  oilour,  whilst 
that  of  gnofl  llf>ur  merely  suggests  the  smell  of  hot  bread." 

The  procecdiii:;  ad'»pled  bv  the  corn-chandler  luid  the  baker  for 
the  dcteniiiniaion  of  the  quality  of  whealcn  llour  is  still  more  simple. 

A  small  quiintity  (a  few  grains  is  sulBcient)  is  nnide  into  a  paste 
with  water,  and  its  quality  Jmlged  of  by  the  tenacity  of  the  dough,  the 
length  to  which  it  may  be  drawn  into  a  thread,  or  the  extent  towhieh 
it  may  be  spread  out  into  a  thin  sheet. 

The  following  analyses  by  Dumas  show  the  composition  of  100  parts 
of  wheat  Hour:  — 


Wheat  Flour. 

Odcsna  Flour 

Odexid  FUtur 

(Kl 

inty). 

(Soft). 

Water    - 

-    10-00 

Wafer  - 

-    1-2-00 

Water   -        -    10-00 

Gluten  - 

-    1096 

Gluten 

-    I4  5j 

Gluten           -    12-00 

Starch   - 

-    71-49 

SUrvh  - 

.    5G-50 

Starch  -         -    6200 

Sugar    • 

-      4  72 

Sugar   - 

-      8-48 

Sugar    -         -      7*30 

Dextriue 

.      3^2 

Dextrine 

-      4-90 

Dextrine        -      5*8! 

Bran     - 

-      2  MO 

Bran     -        -      1-29 

100  49 


087a 


98*46 


*  TrMti«e  on  the  Faltlflcailon  of  Xood,  p.  4a 


WITH   THBIlt  ADULTEIIATIONR. 


S41 


Whear<*n  flour  conlaina  a  j^eat? r  nmnunt  of  prntoine  or  nitrnj*enise<] 
i'4impoun<Ifl  • — that  ia,  of  blmid  and  desh  making  principles  —  than  anj 
Other  description  of  furinjL 

Other  aiiolyecs  of  wheat  and  tbe  rest  of  the  cereal  grains  will  be 
found  at  p.  227. 

Structure  of  the  Grain  of  Wheat. 

ScTcral  structures  enter  into  thu  formation  of  tbe  seed  or  grain  of 
wheat,  as  well  as  that  of  tlic  oilier  cvreals. 

First,  the  seed  is  Murrounded  by  moiiibraoc:),  called  the  testa  ;  second, 
the  surface  of  the  set-d  nrojKr  is  formed  of  untiuhir  cells,  filled  with 
glutinous  and  oily  matter  in  a  jrrunular  state  ;  while  the  sut)stancc  of  the 
seed  is  made  up  of  cells  filled  with  starrh  corpuscles.  Now  each  of  the 
parts  enumerate*!  difler,  ff>r  the  most  pariT  in  the  different  cereal  grains. 

The  testa,  is  in  part  hut  not  entirely  removed  in  the' process  of 
grinding  and  dressing  the  flour,  and  the  same  is  the  case  with  the  cells 
forming  tbe  surface  of  the  grain. 

The  following  is  tbe  exact  structure  of  the  grain  of  wheat:  — 

The  testa,  covering  the  immediate  surface  of  the  H<*edf  consists  of 
three  layers  of  cells,  two  of  which  arc  disposed  longitudinally  to  the 
axis  of  the  seeds,  and,  other  transversely.  The  longitudinnl  cells  are 
large,  and  the  margins  distinctly  beiidcn),  especially  the  outer  layer ; 
tbe  transverse  cells  are  also  beaded,  but  to  a  leas  extent. 

The  cells  forming  the  surface  of  the  seeds  are  large  and  angular ; 
(hose  of  its  substance  are  still  larger,  and  each  encloses  a  cont^iderable 
number  of  starch  corpuscles,  which  are  smaller  near  the  outer  parts  of 
the  grain  than  towards  tbe  centre.  These  several  layers  of  cells 
mar  be  described  as  three  distinct  membranes. 

The  structure  of  the  testa  and  of  the  substance  of  the  seed  are 
exhibited  in  the  engravings.     Figs.  74.  and  7t>. 

Viewed  with  an  object-glass  magnifying  420  diameters  linear, 
wheat  starch  is  observed  to  consist  of  definite  srains  or  particles; 
many  of  tiicse  are  very  email,  others  ore  of  considerable  dimensions, 
while  there  are  but  few  of  intermediate  sizes  :  the  siiiall  grains  are 
chiefly  round,  rarely  oval,  or  muUur-Nb.iped,  and  for  the  most  port 
proviiied  with  a  central  spot  or  hilum :  the  larger  granules  form 
rounded  or  flattened  discs,  with  thin  edges.  Neither  btluni  nor  con- 
centric rings  are  in  general  perceptible  on  the  larger  discs,  although 
in  some  few  a  central  tubercle  may  be  seen  as  well  as  indistinct 
annuli.  Occasionally  some  of  the  larger  granules  are  more  or  less 
twisted  or  turned  up  at  tbe  edges,  and  when  seen  sideways,  present 
the  appearance  of  a  longitudinal  furrow,  which  has  been  erroneously 
describeil  as  a  bilum :  this  appearance  is,  however,  deceptive;  it  is 
really  occasioned  by  the  partial  folding  or  curling  of  the  groin  on 
itself,  whereby  a  central  depression  is  produc^'d,  the  corpuscle  at  tlie 
*urae  time  beinf;  viewed  obliquely.  We  have  fre<|uently  seen  grains 
whit'h  when  stationary  presented  a  round  and  disc-like  appearance, 
but  which,  in  rolling  over  and  presenting  the  edges  to  view,  eidbibited 


ut 


TVOVR  AND   BBEAD, 

Fie  T* 


TMtatDdfDlvUDWOrml  of  n'HKAT.  TVuMrrrar  and  Mflinif  NWOMtal 
oalw  ■MMbrtiN  1  (  4.  middle  i  r  r-,  lancr  ncmbruw  or  turftM  oC  Um  mi<  fnVV 
U«CBl6*dS00i 


WITH   THEIR  ADU1.TEEA.TIONS. 


MA 


lon^tuflinal  furrow  described,  an  obacrvation  which  clearly  proves 
Its  nature.      A  few  grannies  attain  a  very  considerable  size;  these 

Fig.  75, 


Thli  ncnvini  nprftmU  t}i«  Kruoture  kh<I  ftppe*r«nen  of  tte  aUreli  ffranolM  of 

rtUiUisCi 


Wok  \t  PloI'k.  k*  m\mt  lli*  cluvwMvra  of  Um  atUwUmr, 
LacitU,  ftDd  nupilfltd  430  dlaoHtsn. 


Ur>i 


are  less  regularly  circular,  and  being  much  flattened,  reflect  but  little 
shailow  :  nomt^times  their  edged  are  taintly  marked  with  rudiutin;; 
lines.  Examineil  with  the  ptilari?)cope  they  exhibit  a  wetl  uuirked 
cnws.  Many  of  the  above  describtnl  pflrtioulur*,  m  also  the  charuiitcrs 
of  the  cellulose,  are  well  exhibited  mjig.  75, 


Babi.et  Floub. 

There  are  several  distinct  species  of  barley ;  that,  however,  which  is 
conunonty  cultivated  in  this  country  is  the  Hf/rdetan  distichon,  or  two- 
eared  barley. 

As  n»et  with  in  commerce  the  seeds  or  grains  ore  usually  cni*lo5ed 
in  the  mxW  or  hii^ks ;  denuded  of  these  they  form  **  Scntch  or  pnt 
barley^  when  rounded  they  constitute  **  prarl  barley**  and  this  again 
raduced  to  powder  is  called  ^^ patent  barley." 

The  analyE<ts  of  barley  flour  mu:st  be  conducted  very  much  in  the 
mauDer  as  that  of  wheat  flour. 
u  2 


TLOCE  AND 

Chemical  Compontion* 

The  proporlian  of  nzotiscd  compounds  in  bnrlfv  is  loss  llinn  in 
wheat  flour;  it  is  defirient  pjirticulurty  in  trude  gluten,  so  that 
barlej  paste  maj  be  nearly  all  wiislied  uwuy  in  water. 


Tan*  »oil  ■QffkM  ot  •evd  of  Bahlit.    Mafnl(l«d  yxidlutit<«n. 

The  milky  fluid  obtained  by  waahtng  bfirley  paste,  flepnsit*,  as  well 
a«  ihe  stATcb,  a  proteine  matter  supposed  to  be  iiuoiuble  caserne  :  if  this 


WITH   THEIR  ADULTERATIONS. 


US 


be  (ligtisted  with  a  solution  of  ammonia  it  is  dissolvet],  but  is  Again 
thrown  down  on  the  addition  uf  acetic  avid ;  the  liquid  which  haa 


vine  mirweiiU  thv  Btrnetun  inil  ehBr««ft«ra  ot  DAat.rT  STAUcm.  to- 
Itli  t>i«  cfllfUmr.    Unwa  with  U»  I'uiMrv  I.*>ctila.  uid  tntgnUt^  IM 

lejvwTled  the  slareli  and  insoluble  oasuiiic  still  holds  in  solution  a 
small  ijuantitv  uruibuineii  and  some  soluble  caseine. 

Hurley  fltnir  i»  less  nutritive  than  wheal  flour  ;  it*  stoi'ch  corpuscles 
are  less  soluble,  and  iherefbre  resiitt  more  tlte  action  of  the  gastric 
juice ;  the  huak  "is  slightly  acrid,"  and  it  is  somewhat  laxative. 

Structure  of  the  Grain  of  Barley. 

The  testa  of  the  jrruin  of  barley  differs  considerably  from  that  of 
wheat.  It  consists  usually  of  four  layers  of  cells:  tb«,'y  are  smaller 
than  those  of  wheat;  the  lonn^itudinul  cells,  of  which  tnere  are  three 
layers,  are  not  beadei!,  but  Uiofte  forniini;  the  outer  layer  have  their 
margins  slightly  waved ;  those  of  the  inner  layers  and  of  the  trons- 
verfe  celln  not  Iw-'inj:  even  wave<l. 

The  cells  of  the  surface  of  the  jrrain  are  not  nearly  so  large  as  those 
of  wheat,  am)  they  form  tbree  hiyent.  In  place  of  one  »»  in  wheat. 
Those  of  ita  Hubstnnce  also  differ  from  the  c(irre«ponilin^  cells  of 
wheat,  being  more  dclicace,  and  presenting,  when  emptied  of  starch,  a 
fibrous  appearance. 


246 


FLOUR    AND    BREAD, 


The  9tarcL  grnnules  of  bnrley  resemble  verj  closely  in  form  and 
structure  those  of  wheat,  so  that  th**  description  ulrenriy  giv(;n  ftpplia 
to  some  extent  to  the  starch  of  harley. 

Barley  starch  consists  of  smiill  and  large  grains,  with  but  few  of 
intermcdifttc  size:  the  former,  It  w  to  bo  particularly  obserred^  are 
three  or  four  times  smaller  than  the  eorrespoiulinj;  grains  of  whrtt 
starch ;  and  of  the  larger  grains  many  are  distinctly  rineed,  while  « 
much  greater  proportion  of  tlieni  presents  the  Inngitudinal  furrow, 
the  nature  of  which  has  already  been  described.  Those  characters  are 
sufficieiiily  well  marked  to  allow  of  the  diacriuiination  by  the  micro* 
scnpist  of  wheat  and  barley  flour  or  starch.  Examined  with  ibe 
polariscope,  they  exhibit  a  cross  not  nearly  so  strongly  marked  ai  in 
rye. 

Considerable  difference  is  observed  between  wheat  and  barlet 
flour  in  the  net  ion  upon  them  of  boding  wat^^rand  some  other  reageol*; 
thuiv  after  prnlonge*J  boiling,  in  the  case  of  barley  flour,  a  substan« 
remains  unili^sirilvcil,  wliir/li  has  been  denominated  '* /wn/pmr,"  whcret* 
wheat  Hour  Ireated  in  the  same  manner  is  nearly  all  dissolved. 

Bv  the  above  characters,  particularly  by  the  minuteness  of  the 
smail  grains,  nnd  by  the  structure  of  the  testa,  barley  starch  or  neil 
may  be  readily  and  satisfactorily  discriminttCed  when  mixed  with  wbext 
flour. 

Rtk  Flour, 

The  grass  from  which  rye  is  obtained  is  the  Secale  eereaU, 

The  seeds  or  grains  rc^eniible  thu^'e  of  wheat,  but  are  smaller. 

The  analysis  of  rye  flour  must  be  conducted  much  in  the  sao* 
manner  as  that  of  wheat  and  barley  flimr. 

Rye  flour  is  rather  less  ri-5U  in  nitrogenised  products  than  wbes* 
flour,  but  it  contains  more  sugar  \  it-s  |>iLsle,  when  repeatedly  wasM 
in  water,  brenks  up,  and  becomes  di]fiise<l  thn>ughout  thu  liquid,  '^ 
bran  only  being  left  behind  ;  the  milky  liquid,  after  having  deposittfl 
the  starch,  and  after  the  separarimi  of  llie  albumen,  is  to  l»e  ev*pc^ 
rated,  when  the  rt«4iilue  will  consist  of  sugar,  oil,  nnd  the  so-calW 
**  soluble  gluleit,"  which  may  be  dissolved  out  by  means  of  alcohol 

live  flour  is  said  to  be  somewhat  laxative. 

The  roasted  grains  are  imt  unfrequently  employed  in  the  ailBl' 
tcration  of  coflee. 

Structure  of  the  Grain  of  Bye. 

The  testa  of  rye  approaches  somewhat  closely  in  structarc  to  ^ 
of  wheat,  as  is  evident  on  nn  examination  of  the  subjoined  cngravlaf. 
There  are,  however,  certain  diflcrences:  thus,  the  cells  of  the  6i* 
and  second  coiits  are  smaller  and  much  more  delicately  beaded;  those 
of  the  third  coat  are  also  smaller  and  of  a  somewhat  diflerent  funn. 


WITH    THEIR  ADULTERATIONS. 


The  starch  granules  of  rye  flour  bear  a  general  resemblance  in 
and  sixe  to  those  of  wheat :  there  arc  these  remarkable  and  satia- 


e47 


•ftMtoAfRn.  Vrrllcal  «nd  tr«n«nrw  ▼)««•  za  n.  onUn  Aft,  middle 
Mul  '  r.  Inoer  c<wti.    Mafolllcd  30O  dlAOicten. 

diflercnccs.  liowcYer — viz.,  that  the  leswr  p'ains  arc  decidedly 
■nailer  than  the  correspondlntr  grains  of  wheat,  and  that  many  of  the 
lar^r  pranule*  of  rye  stareh  are  furnished  with  a  throe  or  four-rayed 
bilum.  Kxniuiiie<l  with  the  poluriscope  they  exhibit  a  very  strongly 
Marked  croas.     Fig$.  78.  and  79. 

Oat  Flour. 

TTmm*  are  aereral  distinct  species  of  oats;  that,  however,  which  is 
cktpflv  ruliivated  in  this  country  in  Acena  aatica. 

Tbe  oat  frrmins  or  seeds  are  usually  enclosed  in  their  husks ;  when 
deprived  of  these  iher  f<*rni  what  are  known  as  **groaii"  and  these 
conaiitut«  **  £mbdeH  groats,'" 
M  4 


^ 


J 


lU 


FLOUR    AND   BRKAD, 


Oat  flour  or  mcil  does  not  form  a  dough  or  paste  like  wheat  flour ; 
notwithstundLng  which,  however,  it  contains  a  large  amount  of  niirv- 


Pig.  79. 


Tlili  tnmvlnc  mirHenb  the  ilnioture  Anil  cltnrM'len  of  th«  >Urch  ffruialw  of 
Rrc TlOVIu    Drawn  wilb  the  Cunera  Lucid*,  and  taacuified  490 1 


h  mill 
dUoMt 


genised  matter  ;  this  oxittts  principrtlly  in  the  fnmi  of  "arfwin,"  a  sub- 
stance annlo^^ous  to  soluble  Citseinc,  and  obtained  in  the  some  manner, 
by  the  ndditinn  of  acetic  acid. 

"  Outmeal,'*  PiTeirn  remarks,  "  is  an  impiirtsnt  and  valuable  article 
of  food.  With  tlie  exception  of  maize  or  Indian  corn  it  is  richer  in 
oily  or  fiitty  mutter  thiiii  any  other  of  tlie  t:ultivated  cereal  grains; 
and  it*  proportion  of  protein  conipniinds  exeeeJs  that  of  the  6nest 
English  wheatoii  flour;  so  tliat  biitli  with  respect  to  it«  hent  snd  fat 
making,  and  its  flesh  and  blood  making  principles,  it  holds  a  high  rank.** 

Structure  of  the  Grain  of  the  Oat. 

The  membranex  covering  the  grain  of  oat,  contrasted  with  those  of 
the  other  cereals,  present  several  peculiArities. 

The  loiiffiiudiMat  c&ih  fonning  the  outer  nuiid>ranc  are  disposed  in 
two  layers ;  they  are  large  and  well  defined,  the  walU  being  rather  thin 


WITH   THEIR   ADULTEnATfONS.  1« 

andftlightly  waved:  from  tlie  up}>€r  and  outer  wall  of  some  of  the  edit 
springs  u  tjinglu  long  and  pointed  huir,  the  points  being  turned  toward* 


r*«la  •rOit.    a  a.  outer  i  1>  1>,  miiUli  t  bdiI  e  c,  JniMr  lunla.  UMtitA«d  900  dlft- 
Btttcn. 

tbe  summit  of  the  grain  ;  these  hairs  arise  from  the  colls  over  the 
:irhole  surface  of  the  p'uin,  but  they  become  more  numerous  Inwards 
ib«  tpex,  where  they  furm  a  beard  or  tufr,  as  in  wheat. 

The  iranjteerae  cells,  which  may  be  described  as  forming  the  second 
iuveatin^  nienibnuie,  are  Uiapofied  in  a  sin-zle  layer  ;  their  walls  are  les8 
accurately  defmud,  and  they  are  not  very  much  longer  than  brood. 

The  celij  forming  the  burfuce  of  the  seed  itself,  and  which  may  be 
described  as  the  third  cnvering  of  the  grain,  also  cunsivt  of  a  single 
layer,  and  they  arc  smaller  than  the  corresponding  cells  nf  wheat. 

The  starch  granules  of  the  oat  present  well-marked  strurtural  cha- 
racteristics. They  are  smaller  iu  size  than  ibosc  of  wheat,  vnryiog 
liut  little  io  dimcusions,  arc  polygonal  in  6gure,  without  either  visible 


FLOUR  AND  BBEAD, 


concentric  rings  or  hili,  but  with  central  depressions  and  thickened 
edges.     The  great  peculiarity  of  oat  starch,  however,  is,  that  many  of 


Thl»  vntravtng  rrprHcnt*  the  rtnirtur*  and  charscten  nf  ih«  fUreti  gorpanlM  of 
Oat  I'uxTi.  mm  m\*u  or  the  rfilniloaf.  Drawn  with  tlu*  Cmm^rm  ImcH^  and  au^- 
nlflcd  VAt  dlunetcn. 

the  grains  cohere  together,  forming  bodies  of  a  rounded  or  ova!  fipire. 
and  presenting;  a  reticulated  surface,  indi{.'3tivc  of  their  compound 
structure.  These  bodies  escape  readily  from  the  cellnlose,  and,  when 
oat  flour  is  tliffiised  through  w:ilcr,  mnv  frequently  be  seen  floating 
about  freely  in  the  liquid.  A  second  peculiarity  is,  that  unlike  the  other 
cereal  starches,  the  grains  of  oat  starch,  when  viewed  with  polarised 
light,  do  not  oxhibit  the  usual  crojweji.  The  above  particiitarrt  are 
well  exhibited  in  the  accompanving  engraving.  The  walls  of  the  cells 
of  the  eedulosc  arc  very  delicate,  and  appear,  when  the  cells  ore 
emptied  of  the  starch,  like  threads,  as  represented  in  the  enjrrnving. 

A  figure  of  oat  starch  is  given  in  the  new  edition  of  Pereira*8 
**  M-iteria  Medicu."  In  thi:«  the  lar;rer  grains  are  made  fully  ei|nid  in 
size  to  those  of  wheat  starch  ;  whereas  they  are  rcfllly  several  limes 
smaller,  as  represented  in  our  engraving.     This  error  has  probably 


WITH   THEIR  ADULTERATIONS. 


251 


arisen  from  the  artist  having  mjstnken  the  cnrnpound  bodio9  in  ques- 
tion for  sinrric  granules.  The  same  error  pervades  some  of  the  mea- 
surementfi  given. 

Indians  Cobx  Fi^ui. 
Zea  Mat/x,  or  Indian  corn,  h  raet  with  in  the  state  of  flour,  in  the 
»hopfl,  unrfer  tlie  name  of  "  Polenta  ;  "  it  cutefs  into  the  dietAry  of 
manjr  of  our  public  institutions  and  charities. 

Pig.  at. 


^^m  The  nniount  nf  nzntised  cnnstituenta  ta  less  In  maize  than  wheat ;  it 
contftinft,  however,  a  larger  qusntitjr  of  oil,  which  accounts  for  its  fat- 
tening propertiefl. 

In  those  unuocufttotned  to  its  u^c,  maize  is  considered  to  excite  and 
to  keep  up  a  tendency  to  diarrhwa. 

Structure  of  the  Grain,  of  Indian  Com. 

The  testa  of  the  grain  of  Indian  corn  U  made  up  of  two  rocmbranes  ; 
the  outer  of  these  consists  of  some  seven  or  eight  layers  of  cells,  all 


HtlitDfraTint  KprMcnti  the  atnictnr*  uid  ch«rirt«Ti  nf  tb«  itirrl)  ifninnlvi  of 
IifipikjrrDRN  Flocr.  Incluillit^  the  <xlM<»*.    Dnvo  with  ihe  Cudub  Liuids, 


WITH   TEEIR  ADULTERATIONS. 


153 


Tlie  iittter  membrRne  forma   iHr  surface  nf  iho  «eed 


pro|>ci 


and 


ronstnts  of  a  single  Inycr  of  veWa  resembling  tliof^e  of  the  other 
cereals. 

The  eellt  of  the  cellulose  are  very  nn^lar  like  those  of  rice,  but 
they  difl^r  tn  beiiip  snUdividieil  hy  niimerous  septa  forming  a  cellii- 
liited  network  or  blusleinu,  ouch  !«i)at:e  iucltXHing  a  separule  jtiirt-U  cur- 
puttelc. 

The  starch  cnrpuftcles  of  Indian  corn  hear  oonBiderable  resemhlnnce 
to  thnae  of  the  nat ;  like  them,  they  are  somewhat  polyp:onnl  in  oulline, 
and  preaenT.  wfll-nmrked  centml  depresjiions^  as  well  us  ocoiisionally  a 
divided  and  radinte  hilum ;  they  <iiif«r,  however,  in  their  nnivh  Inrger 
Bize,  in  not  lorminp  comptiund  bodi<'s,  anrl  in  preseniiiij;  under  the 
pfiariseope  weJl-deiined  cniuses.  Tlie  eentnd  depression  appears  to 
be  a  character  in  common  between  nearly  all  tlit;  starcli  ;n"ttnules  of 
the  cereal  grasses.  This  depression,  combined  with  the  disc-like 
form  of  the  grains,  crivea  (hem  a  general  resemUhmce  to  tliu  blood 
discs  of  the  mummaliii.  In  tliose  Insuiiices  in  wliicb  the  grains,  as  in 
wheat  and  barley,  are  curved  upon  themselvea,  the  depresuon  exists 
of  course  only  on  one  aide  of  the  disc. 


Rice  Fi/xih. 


^^^  The  seetls  of  rice,  Oriza  iatipa^  contain  a  much  less  proportion  of 
^^vsiitro^enised  compounds  than  the  other  cereal  grains,  and  parricularly 
^^Pirheat  —  viz.,  about  7  per  cent. :  the  (|uantity  o(  fatty  matter  is  also 
'^         less. 

The  substance  obtaiued  from  rice,  termed  gluten,  is  prectpttable  by 
j  acetic  ucid,  and  "has  a  creamy  consistence,  an  agreeable  smell,  and  a 

I  bland  taate ." 

Much  difference  of  opinion  has  prevailed  in  reference  to  the  value 

of  rice  an  an  article  of  diet,  ^ome  persona  pladn^  it  very  high.     Anu- 

lysis,  however,  clearlv  proves  lliiit  it  is  the  least  nutritious  of  the 

(rereal  grasseiji:  it  usually  contains  7  or  8  per  cent,  of  gluten,  and  wheat 

l^^i  flour  rarely  less  than  I'i  per  cent. 

^^k  Tliis  difierence  of  opinion  liait  probably  arisen  from  iho  fact,  that 
^^K'tice  is  seldom  eaten  by  itself,  but  is  partaken  of  usually  with  milk, 
^^Bbutler,  or  sugar,  ttic  nutritiou!<  properties  of  which  substances  have 
^^T^een  attributed  to  the  rice  itself. 

Structure  of  the  Grain  of  Rice. 

The  stmcture  of  the  husk  of  rice  is  by  no  means  easy  to  determine  ; 
it  is  best  examined  aiVer  it  has  been  immersed  in  glycerine  for  some 
time. 

The  outer  surface  of  the  seeil  Is  thrown  up  into  ridges,  these  being 
arranged  both  trausversely  and  longitudinally,  and  describing  between 


M 


FLOUR    AKD    BREAD, 


concentric  rings  Bre  rendered  more  oonepicuous.    To  these  variations 
in  the  condition  of  the  granules  of  wheat  flour  a  fifth  might  bare  been 


F'K  ^ 


a.  «twh  granDln  of  mw  wheat  flnnr  ;  b.  ditto  nfihe  mir«  tialni,  wttli   tnnlriure 
M  In  biud  I  r,  d*T/  hJiHi ;  il,  OotltJ,  MM  In  ptiddlns.     M«^illlca  lOO  JUuctcrt. 

added  represeiitinR  the  characters  of  the  starch  in  PriiiKh  gum  or 
firxtritte:  in  this  the  praniiles  are  destroyed  to  a  great  extent,  but 
here  and  there  granules  and  portions  of  granules  may  be  discovered, 
often  exhibiting  the  concentric  rings  and  sufficient  to  serve  for  its 
identification,  and  to  determine  whether  the  gum  was  made  from  wheat 
or  potato  flour. 


WITH   TnGIR   ADULTERATIONS. 


157 


It  is  by  means  of  British  pim  that  the  liatts  of  postipe  labels  are 
r<^mlered  adhesive,  as  may  l)e  shown  readily  by  siibiniltinji  ai^uial]  por- 
tion scraped  from  the  Inbel  to  examination  with  the  microscnpc. 

Composition  of  the  chief  Cereal  Orainn. 

Tlie  followinii  table,  drawn  UJ^  by  M.  Payen*,  shows  the  proportions 
of  the  proximate  principles  contained  in  tlie  chief  cereal  grains :  — 


Silica.  FhM. 

IWI  Pattt. 

HUrck. 

Wutmm  aad 

ram 

CvHuUm. 

MtluM- 
Kainof 

PdtMbMMi 

■^ 

-JL 

«odB. 

WlM«t,  lurd,  or  VfitnneU 

M19 

WT4 

gw 

S-Al 

40 

sw 

•if  Arrtc* 

(HW 

IS-iM) 

7  00 

TM 

SM 

a'l 

nr  TuanrcMi 

dffni.hArtT,     of ) 

Brir.  Fmnct  j 

63  30 

SOW 

BD 

TV* 

S-60 

r«& 

6H&<) 

1 6  3ft 

7*0 

IW 

a-40 

s« 

WhtCetuieile 

75»> 

n-«i 

B-Oft 

I»7 

3-0 

J-I2 

Fy». 

W«S 

Ulft 

l*i 

J- 15 

4in 

•JM 

Barfer 

MU 

13-06 

l-a 

K7S 

<15 

Sin 

OiU           .         *         - 

WW 

nas 

El  1.1 

ft-ftn 

7'tJ$ 

ZK 

Mall* 

OTM 

I  a- VI 

40 

8->« 

{      A90 

I'JS 

RJc* 

M»-1B 

7(tt 

in 

OW 

1   '■» 

OM 

l^* 


The  following  analyses  are  by  Professor  Johnston  :  — 


Mnmtntmr. 

Bnii<#Ka||lUi 
Wh«i7 

8cvi«h  Ort«wl.            '"^jU^  *■ 

Wai»r 

F«    - 

Starch,  Ac  - 

1< 

10 

1 

7i 

u 

IS 
«3 

14 
18 
6 
61 

14 

11 

a 
06 

100 

100 

100 

100 

w 


Tt  has  be«n  recently  aseertained,  by  careful  and  repeated  analyses, 
that  the  bran  of  wheat,  as  well  as  of  most  of  the  other  cereals,  contains 
A  larger  proportion  of  gluten  than  the  rest  of  the  grain,  and  conse- 
fjiiently  is  more  nuuiiious.  It  Is  of  importance  that  this  fact  should  be 
^'eneraily  known,  as  the  knowledge  of  a  may  serve  in  some  degree  to 
correct  the  preference  given  to  very  white  bread,  and  the  notion  that 
whiteness  aud  quality  go  ttigether.  The  very  reverse  of  this  is  often 
the  case. 

Professor  Johnston  gives  the  following  as  the  reltitive  proportion* 
of  gluten  in  the  whole  grain,  bran,  and  flour  of  the  same  sample  of 
wheat :  — 


•  Pr£vU  de  Clieinl*  [ndiutrtcllc.  p.a&4-    Paris,  IStt. 

B 


S58 


FLOtTR   AND   BREAD, 


Per  Oat 
12 
14  to  18 
10 


Gluten  of  Wheat. 

Whole  grain     - 
Whole  bran 
Fine  flour 

By  sifting  nut  the  hnitu  therufure,  wt>  render  the  meal  much  less 
nutritLous;  this  will  be  mure  appareul  when  we  stale  that  the  bran 
rarely  lorms  less  than  one-fourta,  and  ia  often  conslderitblj-  more,  of 
the  wbolt;  weight  of  the  ^rain. 

The  following;  xa  a  more  detailed  analysis  of  the  composition  of 
wheat  bran  by  Miller  :  — 

Composition  of  JVheat  Bran. 

Starch         -  -  -  -  52-O 

Gluten         -  -  -  -  14-9 

Sugar          -  -  -  -  I'O 

Fat              -  -  -  -  3-(> 

Woody  fibre  -  -  -  97 

Salu             -  -  -  -  50 

Water          -  •  -  -  13  8 

mTo 

It  baa  beenreoently  slated  that  the  bran  of  wheat,  in  addition  to  the 
large  per-centage  of  gluten,  lilcewiae  contains  a  peeuliar  feruieut,  which 
possesses  the  propertpr  of  rendering  the  tlour  or  bread  with  which  it 
IS  mixed  more  digciitible. 

It  should  be  known  also  that  the  small  or  tail  corn  which  is  usually 
separated  from  the  other  corn,  and  u»ed  by  the  farmer  himself^  is 
richer  in  gluten  than  the  large-sized  grain. 

The  next  table  represents  the  mean  l;ompo^iti(>n  of  the  ash  of  the 
chief  cereal  grains.  It  ia  tslcen  from  Pereira's  "Materia  Aledica,**  and 
is  drawn  up  from  the  cuteutitted  means  contained  in  Johnston's  **  Lec- 
tures on  Agricultural  Chemistry  and  Geology,"  2nd  eil.  1847. 


Whm. 

«*ai:'* 

OaM. 

a>«. 

■csr 

lltea. 

Poiuh       ... 

Soda 

sars 

9-OS 

13  64* 
H  141 

«.,| 

II-fiTJ 

sria 

lio« 

LllM           ... 

SSI 

ret 

SW 

4M 

1-44 

l-B 

Mafne*Jft   ... 

la-a 

7« 

9^ 

I0-S9 

Ifisa 

n-m 

Oiidi!  of  Iron 

•«7 

l'4fl 

0-4Q 

1-36 

O-M 

0*45 

Pho«phonc  w^    . 

4B-SI 

S8-06 

4S-S4 

49*5 

44 -ST 

*>**( 

Sulphuric  AChl      . 

0^ 

0*10 

lft-4S 

o-ss 

2-77 

Chiortn*    ■ 

. 

<HK 

frW 

Did 

0-97 

Sillu 

117 

S7IQ 

S-fiT 

oa 

1  44 

i-K 

AlMBOna   - 
Pw-cenUge  of  uh 

" 

0>S1 

*^ 

— 

»tc 

9STJ 

98'7e 

ioi*ai 

99  70 
■boot  1-5 

9VM 

about  3-0 

SfW 

i-is 

S-42S 

1-00 

WITH   THEIR   ADtJLTEEATIONS. 


259 


Messrs.  Oj;^**^'!  *n<l  Way  give  the  following  as  the  pcr-ccntagea  of 
silicM  h\  the  ash  of  the  onlinary  cereal  grains :  '^"05  to  5*46  silioi  fur 
wheat ;  fruin  236  to  TO"??  lor  barley ;  from  3S'48  to  JOCKI  ibr  outs ; 
and  9*22  for  rye. 

As  w«  may  doractimes  require  to  determine  the  phosphoric  acid 
present  in  the  different  corns,  vrc  Bpi)end  certain  processes. 

Dissolve  the  ash  in  ns  small  a  quantity  of  nitric  acid  ns  possible;  add 
acetate  of  lead  in  slight  excess ;  wash  the  precipitate,  which  cnnsifets  of 
phoBphute  and  bu^ic  nitrate  of  lead  ;  dry^  >gi)>LCt  tun\  weigh  —  the 
residue  is  phosphate  of  leatl,  plus  oxide  of  le&d;  dissolve  with  heat 
in  moderately  dilute  nitric  acid,  determine  the  oxide  of  lead  as 
sulphate,  calculate  from  this  the  oxide  of  lead,  and  deduct  the 
result  from  the  weight  of  the  first  residue;  the  difference  gives  the 
quantity  of  phosphoric  acid. 

If  we  desire  to  ascertain  separately  the  amounts  of  alkaline  and 
earthy  phosphates,  we  proceed  us  follows  :  —  The  alkaline  phoi^phates 
are  dissolved  out  of  the  ash  with  water,  and  the  phosphoric  acid  then 
precipitated  by  acetate  of  lead.  The  insoluble  portion  of  the  ash  h 
treated  with  hydrochloric  acid,  and  the  analysis  proceeded  with  as 
before. 

Another  method ;  — 

Mix  the  acid  solution  containing  the  phosphoric  acid  witli  an  excess 
of  solution  of  sesquichloride  of  iron  of  known  strength  ;  atld,  if  neces- 
sary, sufficient  alkali  to  neutralise  the  greater  portion  of  the  free  acid  ; 
mix  with  acetate  of  soda  in  excess,  and  boil.  If  the  quantity  of  oolu* 
tion  nf  sesKjuichlorideofiron  adde<lwas  sutUcient,  the  precipitate  must 
be  brownish-red.  The  precipitate  couAists  of  basic  phos[diate  and 
basic  ocetAte  of  seequioxide  of  iron,  and  contains  the  whule  of  the 
phosphoric  aciil  and  of  the  scsquioxide  of  iron.  Filter  off  boiling, 
wash  with  boiling  water,  dry  carefully  and  ignite  in  a  plat>num  cru- 
cible with  access  of  air;  moisten  the  residue,  after  its  ignition,  with 
stron?  nitric  acid;  evaporate  this  at  a  gentle  beat,  and  ignite  a<!ain. 
Should  this  operation  have  increased  the  weight,  which  is  not  the  case 
usually.  It  must  be  repeated  until  the  weight  remains  cuust-ant. 
Deduct  from  the  weight  of  the  residue  that  of  the  sesquioxi'de  of  iron 
contained  in  the  solution  added;  the  difference  is  the  phosphoric  acid. 


ON  THE  DISEASES  OF  THE  CEKEAL  GRASSES. 

Il  not  unfrequently  happens  that  flour  is  greatly  deteriorated,  and 
in  some  instances  rendered  even  positively  in)uriou<i,  through  the 
attacks  of  various  vegetable  and  animal  productions.  As  flours  thus 
diseased  are  sometimes  referred  to  us  under  the  impression  that  they 

■  3 


FLOUR   AND  BREAD, 

nre  aUuIteraled,  it  becomes  necessary  tbat  we  should  be  possesseil  af 
some  informalion  re8)>ectin<;  the  diseaaea  of  the  (.ereal  priisses. 

Tbe  principal  dist.'a5es  arising  from  the  attacks  of  fungi  are  Ergot, 
Smut  or  Dust,  Brand,  Rust,  and  Mildew. 

Eboot. 

(  Oidium  arbortifaeieru.') 

Ergot  IS  particularly  prone  to  attack  rye ;  It  does  not  confine  its 
raTUiies  to  iDnt  one  grass,  but  has  been  observed  to  attack  a  variety 
of  species  ;  and  anionjrst  the  rest,  the  ears  of  wheat. 

The  cngraTing  on  the  next  page  represents  a  section  of  ergolisetJ 
rye. 

In  Jlour  contaminated  with  ergot  the  etruotured  above  delineateil 
occur  of  course  in  a  niucli  hrokeii  and  dJvideil  state. 

Numerous  and  well  utteslud  instanct-^s  are  on  reeord  of  danf^crous 
and  even  fatal  ell'ects  resulting  iroin  the  consumption  of  bread  con- 
tAiniog  ergot. 

On    BCNT,    SmI'T   BoLt^,   OR    PEPPSS   BbAND. 

{Uredo  Caries^  Dec. ;  Uredo  ftrtklut  Bauer.) 

This  fung:u9  has  httJierto  been  met  with  only  in  the  grains  of  wheat ; 
it  is  easily  recc^i»cd  by  its  dis^U3tin<!  ftmell.  The  sjKires  or  spnrongia, 
analogous  to  seed  vessels,  arc  large  and  reticulated,  as  represented  in 
the  figure.  Some  duubt  exists  whether  this  fungus  is  deleterious  or 
not ;  by  many  it  is  considered  to  be  so.  Flour  containing  it  ia  fre- 
quently used  for  gingerbread.     Fig,  88. 

On  SMt?Ti  OR  DCBT  Braki). 

(Uredo  Segehim.) 

This  fungus  is  corapdratively  rare  in  wheat,  but  very  common  in 
barley  and  oats ;  rye  uocs  not  appear  to  be  subject  to  it.  It  has  not 
the  disagreeable  smell  of  the  preceding  species,  and  the  spores  are 
wreral  times  smaller.     Fig.  89. 

On  Host,  RBn-RAG,  Rbd-robi^,  Hbd-gum. 
{Uredu  ruhigo  and  Uredo  linearis.) 

These  so-called  species  are  but  young  st-ates  of  Puccinia  Orttminir, 
They  form  yellow,  brown,  oval  sjwts  or  blotches  upon  the  stem,  leaf, 
and  cba6r;  the  sporules  of  which  tbe  blotihes  consist  are  intermediate 
in  size  between  those  of  Vrfdo  aineg  and  U.  Segetttm ;  they  are  at  first 
round,  afterwards  oval,  and  attached  by  a  pellucid,  short,  and  alcnder 


WITH  THEIR  ADULTERATIONS. 


£61 


Btalk  to  the  surface  on  which  they  are  developed,  but  after  a  time 

tbtijr  bucuiuti  free. 

Fig.n. 


TW«  »Mr»*1n«  rvptcicnU  •  trftn<vcrM  KClion  of  EiGOT  or  Rt».    a.    Termir»l 

eoloutvd  thrrvl*  which  ranitltuie  lUe  block  nr  purple  portton  uf  the  gnla.  c. 
Thcecllk.  vllh  ihs  canUin»d  •i>heroUM  orciil,  wMch  torm  the  txtilyor  colourlM* 
pAft  of  ihcfrBtn,  ■tutftilflail  iV*  <liun«tcf«.  tt,  f,  /.  rettrcntit  mlnuu  ponlon  of 
tht  wmt  •tfuetanw,  man  hisUjr  macnUkd— rii.,  «7U  dlusiUn. 

Tlie  enjrravin^  (^-  90.)  represents  some  wheat  fiour  lurgely 
infested  with  Puccinia  Granunis  in  the  state  foruierlv  calle<l  Urtda 
fiibigo.  The^sample,  which  WIS  offered  for  sale,  wo*  brought  to  Dr. 
Muspralt,  by  whom  it  waa  forwarded  to  the  author. 


On  Mildew. 

(Puccinia  Gramiuis.) 

The  ripe  sporei  of  this  fungus  are  dark-brown  club-shaped  bodies, 

a  3 


S62  FLOUR  AND  BREAD, 

havin*^  the  broader  end  divided  into  two  compartments  filled  with 
sporules.     "  I  have  observed  this  fungus  wiih  the  rust  luiigi  in  a  way 

F,g.  Ml. 


Ttiti  ai|[rtr!nf  rrpfcjcnla  the  Btiorea  of  t'liKlio  r**iKv.  msfnlfled  49n  dlwtnettTlL 
t^BViof  mul*  from  •  prcfxirklton  bcloDsfni  to  tb*  Ute  Dr.  Ttnin. 

that  strengthens    my  opinion  that  they  are   identical.**  — /Vf>/eMor 
Jienxlow- 

In  the  enfrravinu'  Jif^.  91.  this  fungus  is  represented  in  all  tlie  stages 
and  conditions  of  its  growth. 

Penicilium  glaucum^  Fermentiim  cirvisiit^  ^'C, 

When  broad  baa  been  kept  for  a  few  duyii.  and  has  become  stale, 
certain  specii^  of  fun»i  arc  apt  to  become  developed  ii^  it.  One  of 
these  is  the  well  known  Penicilium  glaucum  which  forms  the  green 
mould  of  cliecse  and  other  decaying  organic  substances  :  it  is  descril>eil 
and  6gured  in  a  memoir  by  the  author  contained  in  the  thirty-sixth 
volume  of  the  "  Medico-Cliirurgical  Tranpacliono." 

A  second  species  is  Ffrmenfum  cirvhia,  or  the  yeast  fungus,  alst* 
descnbed  and  figured  in  the  memoir  above  alluded  \o.  Its  develop- 
ment in  bread  goes  in  part  to  show  that  the  vitality  of  the  yeast  is  not 
altogether  destroyed  by  the  baking  of  the  bread. 


WITH   THEIR  ADULTERATIONS. 


263 


A  tliiril  fungus  found  in  stale  brea*l  Is  very  rUflVrent  from  either  of 
tbe  others  ;  it  is  represented  in  Uie  engraving  fig.  92.    It  is  of  a  bright 


/>f.». 


UiaviBg  iiiwlc  from  ■pttpMntiua  MoncUis  tvDr.  8vA)'oe. 


yellow  colour,  and  it  ofWn,  from  its  abundance,  causes  the  bread  to 
Msuffle  in  patches  tbe  same  colour. 

The  Bearded  or  PotAonmu  Darnel. 

Tbe  poisonous  grass,  Loiium  temuientum  or  darnel^  is  by  no  means 
of  uncommon  octTurrencc,  and  numerous  arcidentF  have  from  time  to 
time  occurred,  in  consequence  of  its  becoming  mixed  either  with  the 
flour  of  wheat,  or  snme  other  cereal  farina. 
The  cflcfls  of  darnel  on  m»n  are  thus  describetl  by  Pereira:  — 
"The  ill  effecta  of  the  seeds  of  bearded  darnel  on  mnn  were  known 
to  the  ancient  (Ireoks  and  Uoinans.  llie  symntonis  which  they  pro- 
duce are  twofold  :  those  indicating:  ffa-itro-intestinnl  irritation. — such  as 
vomitin;?  and  colic  ;  and  those  whi<^h  arise  from  disorder  of  the  cerebro- 
spinal system, — such  as  headache,  giddiness,  languor,  ringing  in  the 


fi64 


FT.OUB    AND    BREAD, 


ear*,  confuMon  of  atglit,  diluted  pupil,  delirium,  beftvincss,  somnolency, 
treuibling,  convulsion?,  and  paralysis.     The^e  seeds  lUcrefore  appear 


r^.sa 


WbuT  FloPR  loftttc4  Vtth  t*ttecimia  Orantink,  In  AH  Mrlj  •!«««  of  dtrtlopiDCliL 
4SI>  diametui. 

lo  be  acro-nftrcotic  poisons.  Accordinjj  to  Seeger,  one  of  the  inr>st 
certain  signs  of  poisoninnj  hy  ihcm  ia  trembling  of  the  whole  body. 
Both  Hur<;hartl  iinil  Srhnher  (qnnled  by  Wibiiier)  mention  death  a,s 
having  resulted  from  their  use.  In  Conlicr's  cases  their  ill  effects 
were  directly  ascl'^tttine^l  by  experiments  made  upon  himself;  but 
in  most  olher  cases  ihey  were  the  result  of  otx-idental  iwiwrniug.  In 
general  they  have  arisen  fn>in  the  iiitfrmixture  of  bearded  darnel 
secHs  with  nthi^r  cereal  grains.  lu  a  prison  at  Cologne,  sixty  persons 
siiflTered  from  the  use  of  a  bread  mesi,  containing  it  drachm  and  a  half 
of  lolium  temulentum  in  six  ounCL'4  of  meal." 

As  the  chemical  l«ls  for  dame]  when  mixed  with  flour  are  not 
very  satisfactory  or  decisive,  we  have  submitted  the  seeds  to  micros- 
copical examination,  and  find  them  to  be  so  dilfurcnt  from  those  of 
wheat  or  rye,  tlnit  when  iidmixed  with  the:»e  in  the  btate  of  flour 
they  may  be  readily  iletected. 

The  itarch  corpuscles  rcKmble  very  closely  thos«  of  rice  in  form, — 


WITH    THEIB   ADLLTEEATI0N8, 


366 


tbat  is,  thcT  arc  polygonal, — but  thoy  arc  much  smaller,  (ind,  like 
those  uf  the  oat,  they  are  Ireqiientlj  uuitetl  into  compound  graiiu 


Ffr.  "I 


<5:^ 


Ik  in 


Mvullfld  JOO  iliMnct«r».    From  ■pcettnini  kladljr  ftarnUbad  bjr  the 
n«r.  Prof.  Utulov. 


of  Ttriotis  sizes,  the  larger  grains  consisting  of  some  fiftjr  or  sixty  starch 
corpus  tes. 

The  fitructure  of  the  testa  is  very  different  from  th&t  of  either  rio«, 
the  oit,  or  indeed  any  of  the  other  rereul  p'oins  :  it  \6  formed  of  three 
ooati  or  mfmbranes;  the  cells  of  the  oitter  coat  form  but  a  single 
layer,  and,  contrary  to  the  arrangement  which  exists  in  the  out,  their 
long  axes  are  disposed  trannvervely,  in  which  rf9i>ect  they  resemble 
rice  :  the  fibres  of  the  huak  of  rice  and  the  cells  of  the  testn  of  loliuni 
ore,  however,  very  distinct  in  other  respects.  In  the  former  the  cells 
are  long  and  narrow,  forming  fllires,  while  in  the  latter  they  arc  but 
between  two  and  three  times  as  loni;  and  brood. 

The  cells  uf  the  second  coat,  which  are  ranged  in  two  layers,  (ullow 


366 


FLOUR  AND  BREAD, 


A  vertical  tSisposiuont — an  arrangement  which  w  contrary  to  Uiat  vbk'U 
obtains  in  ail  the  other  cereal  graius  with  tlte  exception  of  rice. 


FvmfftiB,  nounonlj  foond  In  «tab  Bi««4. 

Tbe  cells  of  the  third  coat  form  but  a  single  layer,  and  resemble 
those  of  the  other  grains  described. 

We  have  now  to  consider  the  dineasw  of  corn  produced  not  by  the 
invasion  of  parasitic  fungi,  but  animal  pruduetiuns. 

On  Ear  Cockle,  FuKrLKs,  ob  Peppebcobn. 

{Vibfw  Tritiei.) 

grains  afTi-cted  turn  preen  at  firsts  and  ultimately  black;  tliey 
le  roundeil,  re»cinb1ing  a  small  peppercnm ;  the  busks  are 
spread  out  and  the  awns  twisted,  l>y  which  means  the  infected  ears 
are  rea<lily  observablf  amim^st  the  standing  corn.  The  blighted 
grains  are  filled  wirh  a  moist  cotton-like  substance  and  contain  no 
flour.  This  suK^tanceis  compn^erl  of  myriads  of  eel-shaped  Qninmlcules, 
Tvbieb,  as  soon  as  moistened  with  water,  exhibit  the  most  active  move- 
ments. A  most  extraordinary  circumjitance  connected  with  these 
animalcules  is,  that  they  may  be  so  perfectly  ilried  that  on  the  slightest 
touch  they  breiik  up  into  po»fder,  and  yet,  wbtn  moistened,  they  will 
revive  and  become  as  active  as  at  first.    This  operation  may  even 


WITH  THEIR  ADULTERATIONS. 

repeated  several  timefl  boibre  the  vitality  of  the  animalcules  is  finally 
destrojed. 


"StriKturr  of  tittfralnor  L»i  ii'M  riMri.iicnm.ar  Ainw/.  Bhnwinc  trumrM  klid 
Tortir*)  •MlloM  of  IMU,  mifnlflcd  9uD  dlUDrten ;  kIk  ibe  cturftrten  of  U>e 
vtarch  «ir]naelai.  nufiiUcd  MO  dUmsten. 

On  the  Wheat  Mlixse. 

{Ctcidom^a  Tritici,} 

This  is  a  two*  wingvd  fly,  which  miiy  be  seen  in  myriads  in  (he  early 
(lart  of  June,  in  the  evenings  froiu  seven  t*»  nine  oVlfK'k,  llying  about 
the  wheat  for  the  purpose  of  depositing  its  e^gs  within  the  blossomf : 
the  egfrs  become  hatched  into  yellow  maggotJi  or  caterpillurs,  and  by 
these  the  miscliief  is  occasioned;  they  cause  the  non-devclnpment  of 
tfaeorarVi  bo  that  the  grain  never  advances  bevond  its  condition  al  the 
time  the  tlower  first  expands.     AU  the  grains  in  an  ear  are  not  usually 


IfiS 


FLOUR  AND   BREAD, 


affecTed,  but  only  grntn«  here  and  tliere.     A  6gure  of  the  flj  and  its  ca- 
terpillar will  be  found  in  the  "  Tranftaciiona  of  the  Linna*an  Society." 


Fig.  9*. 


Vtuatnm  ViamtniiKn  Tunrt,  aiAciillIctl   lOO  HIvnetvt*.    Drmvioc  BiAde  from 
prtpftrftUoo  btloogiDit  lo  the  lau  Dr.  fcreln- 

AcABus  Famitija 

This  mite  is  never  present  in  flour  unless  this  has  become  damaged. 
It  dilTere  considerably  in  Etructuri*  fn)m  the  sugar  mite.     Fig.  9^. 

Another  species  of  acarus^  met  with  oo  one  occasion  in  wheat  flour, 
is  exhibited  in  the  engraviDf;,yt^.  96. 


ON  THE   MANUFACTUHE  OF  BREAD. 

Two  kinds  of  bread  are  manufactured  —  the  one  is  made  with 
yeast,  ferment,  or  leaven,  and  i»  henee  called  leavened  ;  the  other  is 
prepared  without  leaven,  and  itt  deiiomlimted  unleavened  ;  the  0|>eni- 
tion  of  the  substances  used  in  the  niunufucture  of  this  description  of 
bread,  are,  to  a  certain  extent,  analoguus  to  that  of  yeast 


WITH  THEIR   ADtJLTEEATIONS. 


26? 


I 


Lbavehed  oh  Febuentbd  Bkkad. 
Leavened  bread  should  consist  only  of  flour,  jeast,  ftnd  water,  with 
Fig.  aa. 


Acuuun  TABtnMt  or  iwol  witt,  frotn  th«  onm  to  th«  mMnn  >l«t«,  from  vA^l^fhmr. 
a  a,  ova ;  kh,  ftmn(/ ;  e,  mmk  ,  d,  /rmaia.    MsguiScd  7i  lUunclrra. 

a  little  salt ;  suc|i  is  the  composition  of  genuine  home'tnade  bread,  the 
flavour  of  which  is  so  agreeable,  and  so  very  dillerent  from  that  of 
urdinary  bakers'  bread. 

Jn  the  preijaration  of  the  bread  of  the  shops,  6our  of  inferior 
quality  tft  frequently  ufled,  and  this  is  mixed  up  wtlh  large  quantities 
of  salt,  potatoes,  toinetifnes  rice,  and  other  flours,  and  atuin ;  these 
sabstaoces  impart  to  it  a  taste  very  distinct  from  thnt  of  home-iiiade 
bread,  and  occasion  much  of  the  diflerenoc  observed  between  that 
descriptioa  of  bread  and  ordinary  bakers*  bread. 

YeoMt,  m-  the  Yeatt  Plant, 

The  substance  knovn  as  yeast  is  in  reality  a  plant,  belonging  to  the 
tribe  of  Ftwfn  ;  it  con^ista  of  a  multitude  of  minute  oval  or  circular 
bodies  or  sporules,  endowed,  under  certain  favourable  circumstances, 
with  extraordinary  powers  of  jyrowth  and  muUiptieation. 

Three  kinds  of  yeast  are  employed  iu  the  raanulacture  of  bread  — 


S70  FLOUB  AXD   BBEAD, 

y'lz.^  brewers*  yeast,  German  yeast,  and  patent  reui.    Soaaeblklfi 
use  one,  and  some  another,  but  the  greater   number   make  ue  « 


AciMTB  ham  Vlenr.    Drtvn  vUh  thtCuncn  Luddm,  mad  mtmMtAfKlltr 


patent  yeasty  on  account  of  its  cheapness.  The  fungua  is  of  tbt  ^ 
species  in  each. 

lirtveri  Kea*/.  —  This,  as  is  well  known,  is  of  a  lijihl  bnnrfl  * 
fawn  colour,  and  of  a  frothy  consistence  ;  when  recent,  it  is  ia*** 
slant  movement,  and  bubbles  of  gas  escape  from  it. 

Examined  with  the  microscope,  it  is  seen  to  constst  of  innumen^ 
minute  bodies,  termed  sporules,  of  variable  siie,  some  circular.  »* 
others  oval,  and  all  intermingled  with  very  many  globules  of  ctf%0^ 
acid  gas.  These  sporules  multiply  rapidly  when  the  jen(  ii  lA  ** 
active  coiiditiun. 


pwiM  nvnwnu  *■  Tu  Yiakt  Ftni•lc^  "  In  the  Ant  itMt  «r  iti  develop* 
, ar  thftt  of  •mrulea.    Ai  icocrsllr  nwt  with,  and  u  utej  In liw  ferntcnlm- 


Ai  fcocrsll/  nwt  with,  and  u  u*ej: 
if  WMd,  yiMt  wMMliU  of  ui  linm#nMnuinbtrof  lumUit  ■porulMliiUrmLs**! 
" '    I  cf  c*rbanl«  acid.     Orkini  vith  tb«  Cunera  Lucid*,  and  mftfiillUd 


I  for  breml  making.     Porter  yeast  is  objected  to  by  bakers, 

in  distiUeriea.     Small  beer  yeast  is  said  to  be  weak,  but 

LB  efiects,  and  ia  sometimed  used  in  niokiog  rolk."  —  Pi' 

YtaM. — This,  wbich  is  sometimes  called  ^^ dried  yeast" 
•porulcs  onlj,  with  but  little  adliur(*nt  moisture,  and  no 
nu  a  pute-Uke  substanre,  and  iKobtaiiKMl  from  a  fermented 
Itratioii.  It  u  imported  into  thh  couiury  prtncip^dlj'  from 
\n  hempen  baga,  each  holding  half  &  buii(ln>dweiyhL.  When 
uka,  it  ifl  apt  to  burst  them,  in  conee^^uence  of  the  carbonic 
ime»  evolved. 

iere   that  this  yeast  is  perfectly  wholesome,  and  that  no 
exist*  for  the  reports,  recently  set  on  foot,  as  to  its  po<- 
irious  properties  or  qualities  ot  nny  kind. 
't€U<-  —  This  is  prepared  trom  an  Infusion  of  malt  and  bops. 


I 


S7J 


FLOUR  AND   BBEADj 


It  is  a  thin  watery  lii^uid,  containing  innumerable  sponiloa  of  the 
yeast  plant  in  auapension.  The  hops  are  added  to  prevent  the  liquid 
from  bectiiiiiii^  raplilly  sour. 

Tlii^  mt((le  uf  prupurEtion  uf  patt?iit  yeast  is  considerably  varied  by 
different  bnkers.  Many  add  a  portion  uf  brewers'  or  German  yeast  to 
an  infuiiion  contaiuiii^  either  flimr  or  mult,  with  potatoes.  These  sub- 
stances supply  the  food  or  nourishment  upon  which  the  yeast  cellu 
groWf  and  multiply  with  niiioh  rapidity,  as  well  as  the  material  for 
conversion  into  carbonic  a<:id.  Yeast  cells,  in  the  course  of  u  few 
days,  make  their  appearance  in  a  simple  intrusion  of  malt,  and  occa- 
sionally even  of  Hour. 

Patent  yeast,  befnre  being  mixed  wilh  the  flour,  ts  sometiuiea 
allowed  to  drain  through  a  copper  bii»in  or  sieve  perforated  with  nu- 
merous liolcfl  ;  by  this  means  the  chief  part  of  the  mnshed  potati» 
cuifrloyed  in  the  prenaration  of  the  yeast  is  separated. 

DiMcoeery  of  the  DepelopmerU  of  the  Yeast  PlaiU^—Tew  productions 
have  created  more  interest  or  excited  j^eater  discussion  than  yeast; 
its  nature  and  the  mode  of  its  operation  have  been  made  subjects  of 
keen  iiKjuirv  and  dispute. 

These  pomts  are  now,  however,  to  a  very  great  extent,  set  at  rest ; 
it«  fungoid  character  is  geniTulIy  admitted,  and  its  modna  operandi  m 
panitieation  ii^  well  underittood. 

In  one  particular,  howevert  th(»  history  nf  the  yea«t  plant  waa,  until 
very  recently,  iiicomidute  ;  this  related  lo  its  development. 

Slost  observcrB  admit  that  the  ycusl  fungus  os  met  with  in  the 
different  forms  of  yeiist  in  use,  is  in  an  imperfect  state  of  ilevelopnient, 
and  frequent  attempts — the  most  notable  being  those  ofTurpin — have 
been  made  to  discover  the  perfect  plant  or  fundus.  All  their  efforts, 
however,  up  to  a  recent  period,  faileil,  Afore  ibrtunate  than  our  pre- 
decessor*, we  have  succeeded  in  tracfn^i  the  yeast  plant  throu;[;h  nil 
the  stages  of  its  o^wth  to  its  perfect  state,  that  of  a  fun;;u8  with  dis- 
tinct aerial  fructirtcation.  For  a  full  account  of  the  development  and 
structure  of  the  yeast  fun^s,  the  reader  is  referred  to  "  F«>od  and  its 
Adulterations,"  p.  152. ;  and  to  a  jiaper  by  the  author,  in  the  thirty* 
sixth  volume  of  the  "  Medico-Chtrur^'ical  Transactions,"  p.  26. 

Modtu  Operandi  of  YeatL 

The  presence  of  veast  in  a  substance  containing  sugar  or  starch 
which  is  convertible  nito  sugar,  nnd  nitrogeniscd  matter,  induces  cer- 
tain chemical  changes,  comprehended  under  the  termvinouaor  alcoholic 
fermentation. 

These  channfes  in  the  makin;;  of  bread  consist  in  the  conversion 
of  the  sugar  of  the  flour  into  alcohol  and  carbonic  acid  ga.i ;  the  latter,  in 
its  efforts  to  escape  from  the  dtmsh  with  which  it  is  mixed,  distends  iti 
forming  vesicular  spaces  in  its  interior,  and  so  causing  it  to  become 
porous  and  light.     The  alcohol  entirely  escapes  from  the  loaf. 

A  minute  portion  of  the  rtarch  is  converted,  by  tlie  agency  of  the 


WITH    THEIR  ADULTERATIONS. 


2:3 


ve»st,  ift(o  SHf^ar,  which,  in  its  turn,  is  chnnged  into  alcohol  and  car- 
bonic acid.  \f  we  exiimine  attentively  with  the  microscope  tlie  starch 
corpuscles  rnnfnined  in  ferniciitc<l  and  bnked  breiul,  we  observe  that 
they  are  still  entire,  olthoujjh  iiitcred  wimcwhat  in  fi>rin.  • 

J)uring  the  bilking^  part  of  the  starch  is  undoubtedly  convcrtctl  into 
gnm. 

Soim»  physininns  are  of  opinion  that  the  presence  of  yefl*t  imparts 
iiijiiiiouif  prnpertict  to  leavened  brea<l.  This  jKHiit  is  one  of  gryat 
prncti(;al  importance  ;  but  bo  far  as  wv  are  awnre,  no  complete  or  con- 
clusive obs*.'rvationR  have  yel  bec'n  miide  on  the  subject. 

It  1ms  been  computed  thni.  the  annual  loss  of  alcohol  in  bread 
making  amounts  to  about  *100,(X>0  r^tilUm^,  which,  at  1 9jr.  i>er  galluOf 
would  amount  to  285,000/.  Tiie  etfori?  hirberto  maflein  large  bakeriea 
to  «ave  the  alcohol  hnve  failed  :  20,000^  were  spent  in  the  fruitleu 
endeavour  to  collect  and  condense  the  alcoliul  in  thu  militarj  bakery 
at  Chelsea. 


Unleavened  or  Ui^ermented  Bread. 

Tlierc  are  two  kinds  of  unfermontH  bread :  In  the  one,  substances 
are  used  in  imitation  of  yeasty  from  which  a  gas.  Always  the  carbonic, 
i»  disenjiajied,  distending  the  dough,  and  rendering  it  vesicular  and 
light ;  in  the  other,  flour,  water,  with  perhaps  the  addition  of  salt, 
only  are  employed. 

The  substances  used  in  the  preparation  of  the  first  description  of 
unfermcnted  brcnd  nre  sesquicarbonate  of  ammonia,  carbonntc  of 
soda  and  hydrochloric  acid,  or  carbonate  of  soda  and  taiiaric  acid. 

or  these,  by  far  the  be^t  is  carlK>nate  of  amuumia :  this  is  a 
volatile  salt,  and  ItA  great  advantnge  is,  thiit  it  is  entirely  or  ttlmost 
entirely  dissipated  by  tlie  heat  employed  in  the  preparation  of  the 
bread;  and  thud  the  necessary  eflcct  is  produced  without  much  possi- 
bility of  injurious  results  ensuing. 

In  the  employment  of  carbonate  of  soda  and  hydrochloric  or  mu- 
riuUc  acid,  the  case  is,  however,  different ;  here  we  have  the  formation 
of  chloride  of  sodium,  or  uomuhon  salt^  with  disengagement  of  carbonic 
acid. 

Tn  those  instances  where  a  mi.xturc  of  carbonate  of  soiln  and  tartaric 
acid  are  used,  a  tartrate  of  soda  is  formed,  also  with  liberation  of  car- 
bonic acid. 

The  preparations  known  as  Bakings  E(^g>  and  Cvstard  pfttrders  arc 
combinations  of  carbonate  of  soila  and  tartaric  acid,  mixed  with 
wheat  flour,  or  other  kinds  nf  starch,  and  the  egg  powders  are  often 
cffloured  with  either  turmeric  or  chruntaie  nf  lead. 

It  is  extremely  doubtful  how  far  these  prepuratlons  mar  be  used 
with  safety  to  the  public  health  ;  for  our  own  part^  we  see  much  le«8 
objection  to  the  employment^  in  the  generality  of  caitea,  of  a  substance 

T 


274 


TLOUR  AND   BREAt>, 


like  yeiistt  which  contniTis  trat  Utile  saline  matter,  and  the  vitiHiy  ol 
which  is  for  the  ino-^l  ]ttu'l  liestroyed  by  the  heat  of  the  oven,  ibwi  i» 
the  use  (if  acids  mid  nlkidles,  of  ligf;  and  baking  powdci-s. 

A  sample  of  "  Borwidc's  Baking  Powder  "  examined  bj  u»  wefeumi 
compose)  1  of  an  acid  nnd  an  alkali  —  tartaric  acid,  ftnd  either  car- 
bonate of  pritnsh  or  sixla,  together  with  ground  rice,  a  fltnall  quantity 
of  wbt*at  lloiir,  ami  perhaps  a  little  8u?ar.  According  to  a  plan 
coiiunonly  employed  fiome  time  »inee^  the  liberation  of  the  cai^ 
bonic  acid  garf  was  effected  by  mcan^  of  hydrochloric  acid  added  l*» 
the  dough  cOntaiiiiug  the  alkali :  in  this  esse  a  ctilon'de  of  fodium 
or  oominon  eali  was  formed  instead  of  tarlrmte  of  so<la  or  fnla^  a* 
in  the  present  iustaiice.  Now  it  should  be  remen»bered  that  b»- 
drocblorio  acid  is  frequently  contaminated  to  a  fierious  extent  with 
arxenic.  The  action  of  tliis  nnil  other  nnalogoxis  powders  in  lightening 
or  leavening  bread,  like  (hat  of  yeast,  is  dependent,  as  already  re- 
niarke^l,  upcm  the  slow  extrication  of  carbonic  nciJ  gas,  which,  becoming 
dttru5e<l  throughout  the  tlough»  forms  the  little  cavities  noticeable  in 
white  bread,  and  wfaiuh  render  it  porous  and  spongy.  In  the  ewe  of 
baking  jHuvder  contaiiiing  tartaric  aciil,  as  soon  as  the  flour  (hruuj|l>' 
out  M^hich  the  powder  bus  been  diffused  is  mnistenvil  with  wattr, 
the  tartaric  acid  unites  with  the  soda  or  pot^h.  forming  a  tmrtrtl^ 
vt'  one  or  other  of  those  ba#es,  either  of  which  salts  posseascs  diiiretif 
and  aperient  properties.  It  is  on  this  account  that  bread  made  wii 
these  powders,  while  it  may  prove  of  service  in  some  caaes  af  djspepik 
in  others  is  calculated  to  do  harm. 

The  water  we  drink  is  lurgely  impregnated  with  a  lioit  of  saline  i>- 
ftredient-s;  the  bread  we  eat  is  uiturated  with  alum  and  ^ stuff; "sdJ 
It  behoves  n»  to  be  careful  how  we  add  to  the  large  amount  of  laliar 
matter  daily  ingested. 

That  these  observations  are  not  misplaced  or  over-strained  ••" 
appear  from  the  following  publiBJied  receipt*  for  the  prcparatioa  ol 
iinfcrnientetl  bread  ;  — 


To  make  White  or  Flour  Bread. 


Klour  dressed  or  household 
Bicarbonate  of  soda,  iu  powder 

Hydrochloric  (muriatic)  acid    - 
Water  .        _        -         . 


3  lb.  avoirdupdiM- 

9  drachms.  Apothcc*r» 

weijiht. 
11 J  fluid  drachini. 
about  22  Ouid  ounces. 


Observe  the  larpe  quantity  of  soda  and  acid  rerom mended  to  • 
employed  in  the  manul'acture  of  a  3lb.  loaf;  and  remember  that  it  i> 
no  easy  matter  either  to  blend  etjually  the  ingredients,  or  exactly" 

add  thero  iii  neutralising  proportions. 


WITH    THEIR    ADULTERATIONS. 


275 


Pereira  pa\'c  the  f"»I'Iowinp-  receipt  for  the  manufucture  of 
unlcnueDted  bre^j ;  tlie  pro|Hirtion8  of  soda,  und  acid  in  this  urennich 
lesa: — 

Receipt  far  Vi\fcrmented  Bread. 

Flour         -  -  -  -     lib. 

Bauirbonnte  of  soda  -  -  40  griiins. 

\  u  i>iut. 


C'oM  watpr 
Muriutic  acid 


50  drojM. 


L  unl«] 

^K    lesa:- 

^^^^^^K  Beeeiptfor  an  Egg  or  Bahiug  Powder. 

^^^^^^              Carbonate  of  soda  -  -  56  lbs. 

\                                  Tartaric  acid          -  -  28  lbs. 

Potato  6our            -  -             -  1  cwt. 

Turmeric  powder  -  -            -  J  lb. 

It  will  be  observed  that  rht^  quantity  of  tartaric  acid  in  this  receipt 
is  much  too  small  to  neulralj>c  tlic  soda.  It  is  better  ndupted  for 
puddin»^  thtin  bread. 

The  siicoiid  description  of  un fermented  bread  is  heavy  and  compact, 
and  ift  met  with  chiefly  in  the  furm  of  biscuits. 


On  ths  Adultebations  or  Floitr  and  Bbf.ai>. 

AdulterutioH  of  Fljur. — Tbii  adulterations  practised  upon  bread,  are 
often  effected  through  the  mediuto  of  the  Fi  oca  iVom  which  it  is  made: 
it  will  therefore  be  proper,  before  prrneedin^  to  descrilw  the  atlultera- 
lions  of  bread,  to  notice  thnse  in  whiuh  flour  is  subjected. 

The  substuoces  employed  in  the  adulteration  of  fiouff  include  many 
of  those  which  have  been  met  with  in  bread  itself. 

One  adulteration  of  Hour  is  with  bean  meui.  It  is  a  common  practice 
for  milters  to  add  bcRU  mcul  to  flour ;  and  it  is  said  that  this  uddition 
is  not  made  so  much  for  the  sake  of  profit,  ns  to  render  certain  de- 
scriptions of  flour  more  tenacious  when  made  into  dough,  bean  meal 
efl'ecting  this  object,  in  consequence  of  the  large  quantity  of  nitrogenou« 
matter  which  it  contains.  In  the  case  of  genuine  wheat  flour  of  good 
quality,  no  such  addition  is  required ;  when  the  flour  is  damaged^  beans 
are  used  in  considerable  quantities. 

Another  addition  sometimes  made  is  rictJUfW.  Tlie  purpose  served 
by  the  addition  of  this  article,  unless  it  be  exclusively  fur  the  sake  of 
adulteration,  is  not  apparent,  since  it  does  not  cause  bread  to  bind 
better.  It  causes  it  incleed  to  hold  more  water,  and  possibly  has  some 
effect  in  whiteninir  it. 

Again,  in  some  cuses.  barley,  rye,  Indian  com^  and  potato  (lours  haye 
been  added  to  wheat  flour.  ' 

T  % 


rLOtJB    AND    BREADy 

tJrt  pridence  of  Mr.  Emersion,  the  roAna^TPr  of  "The 

«Wf  Mill"  *t  Lec<lsi,  5«  given  bffore  the  Purliamenunr 

f^  F"*'  ^^^j^^^jj^jj^  wheat  flour  is  l'iv(juently  adullerared  wilh 

Ifc  per  *^"''  ^^  Iffirtey  fivvr^  wbicli  is  not  much  more 


of  wheat  flour. 


■*L~"^^-erT  curious  evi'icnce,  in  regard  ici  ilie  inlulu-niliitn  of 

*'^*]I^  IpvVii  liefore  the  Committee  bv  Mr.  Putt"  Brown,  a 

',  .■)ir5'»tdiHli"2^T=»"''  whnso  husint-ss  lleschieflj  in  London. 

M\t^  with  wheat  in  some  districts  to  cheapen  the  price. 

..,  vlieat  is  mixed  witli  barley  to  improve  the  quality, 

j4  jfrtfthnrnptonshirtt.     The  [)nt)r  people  connider  bailey 

gdnn  tvheflt  flour.     I  do  not  know  tuut  that  is  the  case; 

of  the  pi»int,  but  it  is  the  uuiversaj  opinion  of  the  [loor 


wrr' 


•.f^  five  the  above  qualities  to  my  flour,  I  add  one  part 
^g^  lo  iixty  parlJ  o!"  wheat  meal ;  never  more  tlian  one  in 

improre  the  appcftrancc  of  flour,  but  not  the  quality, 
,.  ta  tv  clieapen  it." 
^^oUt   mayor  of  Cnrk,    furnished  ihe  Committee   wilh 

eridenrc  in  regard  tu  the  u^e  nf  Dari : — 

iTan  Egvpiian  grain  culled    Uari,    that  was  importftl  in 

quanl'l**-**  at  one  time  into  Cork ;  that  to  a  moral  eertinnty 

^  purpose  of  mixing  with  wheaten  Hour  :  they  were  able  to 

f)r  d  ft  t«n,  while  the  other  waa  bringing  nearly  three  limes 

Mnntities  of  damaged  wheat  flour  an>  nlfto  annually  sold : 

^^^lly  more  adulterated  than  any  other  flour»  in  a  variety 

-^  ^  render  it  saleable;  aa  by  admixture  with  other   flours, 

^  and  carbonate  of  soda.      The  object  of  the  admixtures 

and  aoda  is  to  lmr<len  the  parliully  de(om|>oi)ed  gluten,  and  to 
1^  acidity  refulting  from  ilecoMipf»niiinii. 

fub»tance  frequently  addeil  to  Hour,  is  alum.     This  is  done 

__   the  flc'ur,  find  to  cttu*e  the  bn-ad  made  from  it  to  appear 

This  addition,  like  the  nuyority  (tf  the  other  ailulterations  of 

is  practised  by    millers.     It  is  only  a  few  weeks  since,  that  a 

residing  at  Bronisgrove  whs  fined  lor  adulterating  his  flour  with 

this  iiiilltT  ha*i  no  less  than  600  lbs.  of  that  suuswmce  on  his 

at  the  lime  of  the  discover)-. 

J^  fulwlance  called  mtneral  white^  which  is  a  hydrated  sulphate  of 
^Hg^  H  occaaionally  added  to  flour.  Several  millers  have  within  Ihe 
^ittm  months  been  convicted  for  putting  this  subst^mce  into  flour. 
£^  of  these  cases  occurred  near  Heaton  Korris. 

0g0viction9  have  also  recently  taken  place  for  using  silicate  of 
^j^pMU,  otlier  names  for  which  are  China  chty  and  Cortttah  clay. 

X  variety  of  other  substances,  it  has  been  alleged,  have  been  and 
gg^  used  ior  the  adulteration  of  Hour ;  and  it  is  most  prubable  that 


I 


I 


WITH    TnF.IR  ADULTERATIONS. 


277 


the  mnjority  of  them  have  been  tha»  einplnyed,  although  we  are  not 
ourselves  acriuainted  with  any  recent  cuseH  of  iheir  detection  in 
tlour.  To  »oine  of  theae  Btibstances  we  shall  shortly  refer  when  no- 
ticin';  the  iirlulteratinns  of  bread. 


On  the  AdnUerations  of  Cones  Fhur. 

There  is  an  article  in  common  and  dfiity  use  by  bakers,  denomi- 
natcd  "  Cones*'  or  '*  Cones  Flow**  With  the  exi&tetice  of  this  ar- 
ticle until  rccenlly  we  were  unacquainted,  nor  is  reference  once  made 
to  it  by  any  of  the  many  witnesses —  millers,  bakers,  ficc. —  in  the  evi- 
dence given  before  the  Purliouientary  (Jommittee.  Our  auentiun 
becnme  directed  to  it  in  consequence  of  the  Jollowing  ciroumsrunce.  i 

Dr.  Piiley,  of  Peterborough,  brought  the  uuthur  u  sain[de  *j»f  Hour 
for  examination,  seized  on  suxpieion,  nnd  whJi'h  Jie  ntftled  ihe  baker 
cjlled  "Cone;*  Flntir."  On  .jjibjecling  this  to  m)cro»co|jii:ul  examination, 
it  was  found  timt  it  rnnsistod  entirely  of  rice  flour. 

Thiii  induced  him  to  make  furlher  inituirie:^ :  he  soon  learned  that 
genuine  Cont'S  flour  oonsisld  of  the  Hour  of  a  jiartiuular  apccies  uf 
wheat  called  Heret, 

Further,  thui  it  wva  employed  by  bakcrfi  to  dust  the  dough,  as  well  as 
the  boartlti  ujxm  which  thi»  w  made  uiLti  loaves,  the  object  nt'  its  use 
beinjr  to  prevent  the  dough  either  adhering  to  the  boards,  or  the  loaves 
to  earh  other,  in  tfic  course  ol  bakin;*;. 

Having  learned  thu:^  mucli,  the  author  procured  from  bokers  nume- 
rous samples  of  Cnne.^  uml  subjected  them  to  exuminutiun  ;  the  results 
arc  exhibited  in  the  onnexeil  list.  The  names  of  the  parlies  of 
whom  they  were  obtained  are  not  given,  becnuse  many  of  tliem  were 
pnH.-uretl  indirectly,  and  in  aouic  ca»ea  through  the  instrumentality  of 
frieuds  Cones  (lour  ljt.'iitg  an  article  which  cannot  be  purchased  by 
the  public  in  the  uidjnory  way. 

Rcsulu  of  the  Microscopical  E&funinatton  of  Twenty-two  samples  of 
Cones  flour,  procured  chlelly  in  the  meiropoti»  in  the   autumn   uf 

U/  SampU. 
AdullenUed,    Contains  I^ye  and  Hice  tlours. 

2ud  Sample. 

Not  Cones  Jlour  at  all.    Consists  entirely  of  Rice  flour. 

Srfi  Sam/tie, 
AduUerateH.     Contains  Rice  flour. 

4/A  Snmple. 
AihUteraUd,     Contains  Rice  tlour. 

T  a 


'97B 


fttfi  SampU. 
Atiulterated.     Consists  in  great  part  of  Rice  flour. 

6M  Sample. 
Genuine. 

7th  Santple. 
Adulterated,     Consists  almost  cntiroly  office  Qour. 

8/A  Sample, 
Adulterated,     Curnposed  alrnvsl  entirely  of  Rice  flour. 

9th  Sample. 
Adulterated.     Consisting  chiefly  of  Rice  and  Bean  nnnrs^ 

TO/A  Sample. 
Adulterated,     Conlaius  iimcb  Rice  6our.^ 

Wth  Sample. 
Not  Cones  at  all.     Consists  of  Rice^  Indian  Com^  and  Bean  flours. 

Wh  Sample. 
Adulienited.    Consists  in  ^eat  part  of  Bean  and  Rice  flours. 

13/A  Sample, 
Adulterated.     Contiuns  mucli  Rice  flour. 

\Atk  Sample. 
Adulterated.     Contains  Barley  flimr  iind  alum. 

\fith  Sample. 
Genuine. 

16M  Sample. 
Adulterated.     Admixed  witti  both  Barley  and  Riee  flours. 

17M  Sample. 
Adulterated.     Consisting  in  gi-eat  part  of  Rice  flour. 

\Sth  Sample. 
Genuine. 

Wth  Sample. 
Genuine, 

20th  Sample. 
Genuine. 

21  Mt  Sample. 

Not  Conea  at  all.     Consisting  entirely  of  Rice  and  Indian  Corn 
flours. 


WITH    THEIR   ADULTERATIONS, 


•^7!» 


'22nd  SttmpU. 

\duUerated.  Consisting  chieHjr  of  Riee^  with  some  Indian  Com  flour, 
and  much  Suit. 


i 


It  flppcATK,  therefore,  that  Conesfltmr  u  rartty  to  he  obtained  genuine^ 
•  htd  is  tuhject  to  an  enormous  attumnt  of  aduUeration,  this  usually 
consiittinff  in  the  adilition  of  very  lar^e  <|iiJii)tilit^s  of  riVe,  rye,  harley^ 
heajij  nnu  Tndmn  com  flours,  and  sometimes  of  sali  and  aittm.  Further, 
lltat  come  of  the  Mt[D|des  do  mtt  cotdain  a  particle  of  tcheat  Jfitur^  of 
which  nloitu  Lhev  nhouM  ootij^ist. 

The  olijeot  of  these  additions  is  obviously  to  cheapen  the  article; 
and  that  this  purpose  is  effected  sometimes  to  tlie  extent  of  nearly 
one  hiilf  might  be  readily  proTcd  by  (pioting  the  several  market 
prices  of  the  diflercnt  varieties  of  gram  ubove  referred  to. 

Thnt  this  is  really  so  may  be  shown  in  another  war  :  m-'vcrnl  quali- 
ties of  Cones  flour  are  sold,  the  beat  being  nearly  twice  the  price 
of  the  worst,  and  the  adultcmtion  being  usually  in  proportion  to  tfae 
price. 

Two  (]ucstions  now  present  themselves  for  consideration  in  connec- 
tion with  Conrs  flour  :  the  first  is,  whether  any  real  necessity  exists  for 
the  U!se  of  even  genuine,  much  less  Qdiilterntetl  Cones  flour  ;  and  the 
second  is,  whether  this  flour,  e^peciully  when  Ddutterated,  as  it  usually 
is,  is  ever  opplied  to  any  other  purpose  than  that  avowed. 

Tlie  first  question  is  almost  suflicicntiy  answered  by  the  fact 
that  some  do  not  use  Cones  flour  at  all,  and  yet  do  not  experience 
iiity  great  diflieulty  in  the  manutaeture  of  the  breud  ;  there  is  there- 
fore •iimmI  reiu^ou  for  believing  that  price  bn^*  very  miieh  to  do  with  the 
general  em|ih>yiuent  of  Cones  flour,  even  in  those  cases  in  which  it  is 
really  used  lo  prevent  the  adhesion  of  the  loaves. 

With  regard" to  the  setonH  rpiestion,  there  enn  be  no  doubt  but  that 
Cones  flour  is  frequently  employed  in  the  adulteration  of  bread  :  this 
is  shown  in  some  eases  by  ihe  character  of  certain  of  the  adulterations 
lo  which  it  is  subject,  n.itnely  those  by  admixture  with  beun  flour, 
alutn,  and  salt;  now  bean  flour  in  actually  of  a  more  glutinous  and 
adhering  nature  than  pure  wheat  flour  of  good  i|uiility  itself,  and 
therefore  its  pre*ence  tends  to  un6l  it  for  the  very  purpose  for 
which  it  is  alleged  that  it  is  designed. 

But  wiine  bjikera  have  even  acknowledged  to  the  employment  of 
Cones  fliiur  for  purpoae.t  of  adulteration,  for  which,  from  Us  composi- 
tion, especially  when  odultomtcd,  as  it  au  cuustantlj  is,  it  is  so  well 
suited. 

Suppoi^ing,  however,  the  Cones  flour  to  be  employed  for  dusting  the 
dou^h,  ami  that  this  is  a  legitimate  use,  still  thife  docs  not  justify  'tis 
adulteration. 

In  the  article  Cones  flour  prepared  by  miller^  bakem,  then,  ore 
furnished  with  a  material  avowedly  wheat  flour,  but  which,  consisting  of 

T  4 


FLOUK   AND    BREAD, 


mixtures  of  difiorent  and  cheaper  Atmrs,  is  in  every  wtky  nuilcd  fur 
tbe  adulteruiion  of  brend ;  und   that  it  is  cuteusively  used  for  thi» 


JtlmltrrQiM  Cosu  WutVBt  eniwIftiM  efa  mixtiff*  AT w*r«r,  rtoa,  aad  hian  tomn. 
Uh^&A  tU  dlMEMMn. 

purpose  cannot  be  douhteil.  Tbe  svBtcm  adopted  by  millers,  of 
supplying  under  the  name  of  Cones  tlourand  as  wheat  flour,  compounds 
adapted  for  iidulteration,  is  surely  very  cunnini:ly  (ievised.  'ITie 
public  know  iiothiii<;  of  thi^  article,  the  musler  bakers  themselves  are 
Ignorant  of  its  u.^uct  eouipuMtloii ;  while  the  journeyman,  in  most 
cases,  when  he  ndii«,  bv  bin  niask-r^s  directions,  a  bushel  nf  Cones  to  a 
sack  of  flour,  lut»  im  ideu  that  he  is  adidtenuing  the  bread. 

Tbe  cose  of  Cones  Hour  affurds  another  example  of  what  the  rni- 
croicope  is  capable  of  efTccting   in  connection  with  the  subject  of 


WITH  THEIR   ADULTERATIONS. 


SSI 


ftdutterjition.  Had  it  nut  been  for  that  instrument  it  would  have 
been  utteily  impu$siblc  to  have  ascertained  by  scientific  means  the 
comp)»itinn  of  the  het(>rof*cnuou!i  mixture  cdleil  Ciines  flour. 

Tlie  adniirabK>  engravinjf  yf^.  i»8.  exhibits  the  characlera  presented 
by  a  sample  of  so-caIle(l  Conn  tlour,  toniposi'd  of  wheat,  rice, 
aud  beui  flours.  U  is  difficult  to  deienniiic  which  i^  iho  most  ex- 
cellent, (he  drawing  of  Mr.  Tufien  Weet  or  the  engraving  of  Mr. 
Hart. 

On  the  Adulteraiiaus  of  Brtad. 

Well  then,  flour  containing  any  of  the  nrtiiles  already  menlioned, 
the Bksad  made  from  it  must  of  course  do  m  likcwit»e;  but  other  and 
further  adulterations  of  bre»)  nre  practiced  by  bakers. 

It  is  notorious  that  the  great  majority  n^  bukers  add  either  alum 
to  their  bread  or  a  mixture  of  alum  and  suit  known  in  the  trade  by 
the  terms  "hartlp"  and  *Stuff;"  and  thus  in  many  c;)8t'8  the  ilour  re- 
<*eiTeA  two  additions  of  alum,  the  hnker  being  often  unaware  that  he 
haft  been  already  antiripatcd  by  the  miller. 

It  is  also  notorious  that  hnfcers  frequently  add  a  proportion  of 
potat/M's  to  bread.  These,  when  masheil,  are  mixk*d  with  the  yeast, 
which  is  said  to  feed  upon  the  potatoes,  and  lor  which  purpose  only 
it  is  fllleped  the  potatoes  are  usetl,  and  not  for  aduliv-ralioii.  AA'hen 
the  quantity  of  [mfutoes  employed  is  but  small,  this  may  be  mi  ,*  but 
there  is  no  doubt  thul  poLatoest  are  sionetiuiei*  abided  in  considerable 
quantities  to  bread,  especially  when  they  nre  eheop. 

Tlic  injury  to  the  properties  of  the  bread  by  its  ndulterution  with 
the  Hours  and  vegetable  substanoes  rvferrei]  to,  especiully  rice  and  |>o< 
tatoes,  is  very  jrreut,  as  can  be  rea<iily  proveil. 

Wheaten  flour  owes  its  superiority  over  nearly  all  other  kinds  of 
flour  to  the  lar^fe  amount  of  gluten  which  it  eoniaing,  and  which  is  the 
constituent  that  gives  value  to  it  and  upon  which  its  nutritious  pro- 
perties depend :  this  amounts  in  unlinary  flour  to  not  leas  lltnn  I'i  per 
cent.  Now  rice  and  potHtt>e9,  Imth  so  rommnidy  added  to  bread, 
contain  not  more  than  7  per  cent,  of  that  ftubntance, — that  is,  thry  are 
but  little  more  than  half  ns  nutritious  as  jjoful  wheut  ilnur, — nnd  i*on- 
sequenlly  any  brcail  to  which  thtse  articles  are  added  is  robbed  of 
much  of  its  nnuri.shmenl. 

But  the  evil  doet^  not  end  here  ;  the  riee  and  some  other  substances 
swell  up,  and  absorb,  when  made  into  bread,  a  much  hirger  quantity 
of  water  than  wheat  flour,  and  thus  the  quality  of  the  bread  as  a  life- 
sustaining  food  is  still  further  reduced. 

The  use  of  nhm  in  bread — nnd  it  is  almost  always  used  by  bslcers 
— w  parlinttaritf  itijuru>MA.  It  is  true  it  causes  the  bread  to  be  whiter 
than  it  wouhl  be  oiherwI.«ic,  indeed  whiter  than  it  was  ever  intended 
to  be  by  Nature;  but  it  imparls  to  brt»ad  several  other  properties: 
thus  it  hardens  the  nutritious  constituent  of  the  bread,  the  gluten, 
and  90  (on   the  authority  of  that  great  chemist  Liebig)  renders  the 


ssa 


FLOUR   AND   BREAD, 


bread  more  indigestible;  it  enables  the  baker  to  adulterate  his  bread 
with  greater  quantities  of  rice  and  pntutnes  than  lie  coulil  otiierwitte 
emploj  ;  undf  lu^^tly.  by  the  use  of  aium  he  U  able  to  puss  ofTan  in- 
ferior, and  even  a  damitged  flour,  for  one  of  superior  quality-  Is  it 
then  worth  while,  or  nither  is  it  not  very  foolish,  thus  to  injure  the 
projjurties  nf  the  brend  by  using  til  urn  for  the  mere  Fake  of  obtaining 
an  iiiHJuturallr  white  loafV 

The  piiblit^  then,  in  judging  of  the  quality  of  bread  by  its  colour,' — 
by  its  whiteness, — uomniit^  a  rau*t  serious  mistake  :  there  la  little  or  no 
connection  between  colour  and  quality:  in  f:ict,  very  generally,  the 
whitest  breads  arc  the  most  adulterated.  The  public,  therefore!  should 
lose  no  lime  in  correcting  itt  judgment  on  thi^  (loint. 

Affftin,  the  mistaken  taste  of  the  public  lor  very  white  bread  — 
whiJli.  be  it  known,  cannot  be  obtained  even  from  the  finest  and  be&t 
flour  except  by  the  use  of  Atom  or  some  oUier  subat&nce  similar 
io  its  operation  —  tends  to  the  serious  injury  of  the  bread  in  another 
way. 

The  outer  part  of  the  grains  of  wheat  has  been  proved  by  analysis 
to  be  much  richer  in  nuurishing  principles,  in  gluten  and  tn  oily 
matter  ejijicciiilly,  than  ihe  central  and  im>re  flitury  pHrts  of  the  grain. 
Now,  in  prepanngj  the  finur  descriptions  of  flour,  the  utmost  painfl 
are  t^ken  lo  peparute  ihta  highly  nutritious  exterior  p<irtion , of  the 
grain,  and  thus,  although  the  flnur  so  obtnineil  is  very  fine  and  white, — 
very  suitable  for  mukln<;  a  white  luaf,  (hat  fallacirms  test  of  quality, — 
it  is  yet  not  nearly  ^o  nutrtiUms  as  whole  uieul  lluur,  or  mvvii  the  less 
finely  dressed  qualities  o\'  wheat  ftour.  The  cunsumer,  now  better 
instructed,  is  in  a  posilion  to  judjio  of  how  much  be  sacrifices  for  the 
mere  s«ke  of  mi  arbitrary  and  falluciifUit  stjui'ianl  tA'  quality,  namely 
whiteness.  The  dsfltrence  in  nounshiuf;  properties  between  whole 
meal  fU»ur  and  very  finely  dressed  fluur  amounts  iu  umny  cases  to  fuUj 
one  third. 

Further,  alum  is  very  apt  to  disorder  tike  stomach,  and  to  ocoHUon 
acidity  and  dyspepsia. 

The  manner  in  which  it  does  bo  has  not  been  clearly  ascertuned. 
The  p^iwerful  clfects  of  nUiui  iis  an  astrin<;ent,  when  administered  ai  &, 
medicine,  are  well  known;  but  it  is  considereil  by  Mr.  Lewis  Thompioa 
that,  when  added  to  Itnur  nr  brend,  it  btiomcfl  (leconqn^sed  by  the 
gluten,  a  bi.sniphate  of  potash  bein^  funned.  Whether  this  view  is  cor* 
rect  or  not^  is  queiilionable,  and  it  is  entirely  opposed  to  the  opioioui 
and  statements  of  Licbig. 

Mr.  Lewis,  in  his  evidence  before  the  Parliamentary  Committee, 
does  not  advance  a  single /^nfr}/"  in  support  uf  btM  viewH. 

Liebig  considers  that  part  of  the  beneficial  :iction  of  wheat  flour  on 
the  system  in  due  to  the  M>luble  plio.t^phates  which  it  contains  in  stieh 
larjre  quantities,  and  he  HtAlcti  thut  when  ulum  is  added  tn  bread  these 
are  dcconqiosed,  the  phuMphoric  oc.id  of  the  jihofphntes  uniting  with 
the  alumina  of  the  alum,  and  that  thus  an  insoluble  phosphate  of  al- 


WITH   TUEIR   ADULTEnATIONS. 


US 


iiminn  ifi  formed,  and  the  beneficial  action  of  the  phosphates  conse- 
quently h'Kt  to  the  system. 

So  siitisflod  is  Liebig  that  this  U  the  case,  that  for  some  vcaM  pa.Ht  he 
has  recommended  the  emph>ym(.'nt  of  Hmal)  qtiantitien  of  Iimo  water 
for  the  purpose  of  whitening  bread  made  frommitstv  or  daninged  flour; 
and  it  was  stuted  at  the  re<rent  mectlnff  of  the  Bntiitli  Assticiation  at 
Glasgow,  that  lime  water  is  now  used  by  manv  Scotch  bukers. 

The  followin<r  is  Liebi^j's  own  statement  of  htii  views:  — 

"Many  salts  render  the  gluten  again  insoluble,  apparently  by  form- 
ing with  it  A  chemical  combinution. 

"  The  bakers  of  Helpiiim  diwovered,  about  twenty  years  ago,  how  to 
bake  from  damaged  flour— by  adding  sulphate  of  copper  (a  poison)  to 
the  dough — a  bread  in  appearance  and  external  properiiis  as  fine  as 
from  the  be^t  wheat  flour.  This  mode  of  improving  its  physical  pro- 
perties of  course  deteriorates  its  chemical  [>ro|)ertic3.  Alum  has  the 
same  effect  as  sulphate  ofcopiwr:  when  added  to  the  dough  it  renders 
the  hrend  very  lijtht,  ela<ttic.  firm,  ami  dry  ;  and  the  London  bakers 
in  consequence  of  the  demand  fi>r  white  bread,  such  as  the  English 
and  Amcrirnn  flour,  usually  so  ;jnf>d.  yields,  appear  to  hnve  been  com- 
|>clted  lo  add  ainm  to  nil  flour  in  the  bnkin;;.  1  saw  in  an  alum 
manufactory  in  Scotland,  little  mounds  nf  finely  ground  alutn,  which 
was  destined  for  the  use  of  the  London  bnkcrs. 

"  Sinct*  phosphoric  acid  forms  with  nlumina  a  compound  hardly  de- 
composable by  alkalies  or  acids  this  may  perhaps  explain  the  indiges- 
tibility  of  the  London  bakers*  brea<),  which  strikes  all  foreiifners.  A. 
smidl  quantity  of  lime  water  added  to  the  musly  or  dnmA<;ed  llour,  has 
the  Hame  fffect  as  the  idum  or  sulphate  of  copper,  without  being  fol- 
lowed by  the  same  disadvantaire*.*  —  Lftten  on  Chemistry. 

SupfHrsin*;  (or  a  moment  Mr.  ThompM(»n's  views  1u  be  correct,  it  has 
still  to  b€  proved  iJiat  bisulphute  of  potash  consiitules  a  wholesome  in- 
gredient in  bread.  Mr.  Thompson  states  of  it  himself,  in  the  evidence 
referred  to,  that  "it  is  a  siniridurly  sour  thing ; "  if  so,  it  is  surely  the 
occasion  of  much  of  the  acidity  resulting  Irom  tlie  use  of  bread  to 
which  slum  liiis  l>een  added. 

Enouf^h  has  now  been  adduce*]  to  show  that,  whether  the  views 
allude<l  t^i  are  corrert  or  not.  it  is  n  very  dangerous  thing  to  tamper 
with  artirlns  of  daily  food  and  of  large  consumption,  like  flour  and 
breud,  by  tlic  addition  of  chemical  substances  of  anjr  kind. 

It  is  curious  to  notice  the  arguments  to  which  the  defenders  of 
adulteration  are  driven  in  order  to  finil  excuses  for  certain  practiues. 
We  were  recently  much  astonished  at  one  of  iheiic  arguments. 

A  learned  chemical  professor,  at  the  Ule  uie*-.ting  of  the  British 
AssfH-itiiion  in  (rlasfiow,  defended  the  use  of  alum  in  bread  on  (he 
following  ground :  — 

lie  fltiitcil  that  Thames  water  was  so  alkaline  it  turned  the  flomr 
yelltiWy  and  hence  the  use  of  an  acid  became  necessary. 

Ilorae-made  bread  is  certainly  not  so  white  oa  bakers'  bread,  the 


2S4 


FLOUU   AMD   BREAD, 


^ 


ilifFerence  being  explained  hv  the  absenne  uf  ibe  alum;  but  it  if  cer- 
tiiinlv  nut  the  uwsn  that  Thames  water  has  the  remarkable  eQ'ect  of 
turning  tbc  Hour  jellnw. 

Bdt  the  real  and  actual  facts,  aji  re<rards  Thames  water  and  Ht 
effet'te  on  the  colour  nf  the  bread,  are  these  :  — 

The  alkalinity  of  Thnroes  water  is  so  triHing  that  it  is  scarcely  per- 
ceptible in  liie  motiit  delicate  test  piiper  :  atrain,  during  the  fermeiitalinn 
nf  the  bread  a  large  quuntity  of  ncid  is  generated,  infinitely  more 
Ihan  would  be  sufficient  to  neutralise  the  alleged  alicalinity  of  i'hamea 
uattrr,  and  t<*  counteract  any  tendency  which  it  is  said  to  puuess  to 
turn  flour  yellow. 

Aguin,  contrast  the  professor's  argvmeni  with  the  practice  recom- 
mentlfd  by  Barun  Liebi*;.  The  one  says  Thames  water  is  90  alkaline 
it  (iirn*i  Hour  yellow,  and  the  other  advises  the  use  of  an  alkali  to 
whiten  it. 

But  wc  will  suppose  that  the  pn>fessor's  views  are  not  altogether 
destitute  of  fnandation,  yet  they  wouhl  constitute  but  a  jKwr  rewson 
for  the  emplnyment  nf  alum.  That  substance  is  used  in  bread-making 
nearly  all  over  ihe  United  Kinplom,  and  yet  the  nw  of  J'hume*  water 
is  confined  to  the  Mcimpolis  and  its  vicinity.  We  repent,  then,  it  is 
curious  to  notice  the  chunicler  of  the  arguments  which  sfmielinies 
even  scienlilic  men  will  condesceml  to  use  in  defence  of  adulteration. 
Another  argument  by  which  the  use  of  alum  !a  defended,  is  thai  the 
quantity  employcfl  is  but  small :  uiK>n  this  point  the  following  evidence 
xnav  be  adduced  :  —  1 

llie  author  of  the  celebrated  treatise  "  Death  in  the  Pot "  writos:— «' 
"The  smallest  quantity  of  alum  which  can  be  employed  with  efTecl  to 
produce  a  white,  light,  and  [Kmms  bread  fwm  an  inferior  kind  of  flour, 
1  have  my  own  baker'it  nuliinritv  to  stnte,  is  from  three  tu  four  ounces 
uf  alum  to  a  sack  of  flour  weigliing  240  lbs." 

Dr.  Markham  gives  H  ounces  of  alum  as  the  quantity  used  to  a  sack 
of  flour. 

From  inquiries  which  we  have  made  amongst  bakers,  we  find  that 
the  quantity  of  uluni  usutdly  cmployeil  U  half  a  [Kiuiid  10  the  sack  of 
Hour  weighing  240  Ibs^  ami  rhat  the  qunntity  used  varies  according  to 
the  age  and  <:iinditiaii  uf  tlie  flour  :  thus  new  tlour  requirfs  mufh  more 
alum  than  old;  indeed,  :t  white  bread  may  be  made  from  old  flour 
without  any  addition  of  ulmn,  while  as  much  as  three  qniirt^'rs  of 
a  pound  may  be  adilcd  to  the  naok  of  very  new  fl^mr.  New  flour  \a 
that  wbii:h  come!)  into  use  about  November  and  Dfri-mbor;  hence  the 
bread  made  in  these  months  usually  conuina  a  large  pntportion  of  alum. 
Old  flour  is  that  used  in  the  two  or  tlirec  summer  months  preceding 
the  hnrveflt. 

Four  ounces  gives  about  30  grains  of  alum  to  every  4  lbs.  nf  flour, 
eight  <mn-.-e8  GO  grains,  and  twelve  ounces  90  grains.  Mr.  Mitchell, 
the  author  of  a  treatise  on  the  "  Fulsificaiion  oi  FoimI,"  states,  that  he 
detected  in  ten  4  pouud  loaves  of  bread,  819.^  grains  of  alum. 


•WITH  THEIR   ADULTERATIONS. 


8SS 


Withr(?9pect  to  con<1ition,  a  flour  which  is  iron k — that  if,  wliichdoes 
nut  bind  rt'adily  in  fonsi-'«iuence  of  a  deficiency  itf  gluten — reijuires  a 
.vu-cb  larger  proporlion  ol'  uliini,  un<l  in  this  cuoe  from  thrvc- quarters  to 
■%  pouml  of  thut  halt  miiy  be  added. 

Suit  Uah  n)Uoh  t)ie  same  ellcct  as  nlum  ;  that  ia^  if  makes  the  bread 
wliite  and  6rin,  und  Ucnctf  it  issonii-tinies  ust^il  in  exreu,  to  suppK  the 
pluci\  to  sonic  extent,  of  nlum.  The  ftvcrngc  qmnlity  ut'sult  Htlded 
Lv  bilkers  tu  braid  whcrrin  alum  iit  used  is  not  about  hixty  oiincfs  to 
the  "240  lbs.;  but  the  iimoutit  vnries  with  the  iige  ol'the  Hour. 

The  use  of  hIuiii  in  bread  is  ]>robibited  by  luvr,  under  cortnin 
pecunijiry  pL-nidtie.*;  this  law  is,  however,  rarely  ent'nrued.  We  giilher, 
riowever,  troui  llie  existence  uf  Much  :l  law,  tliat  the  legitihilureconi«ideni 
the  U)ie  of  altiui  in  breud  to  he  objeetionable. 

The  use  of  another  mineral  aul>:ttance.  cnrbonnto  of  mapieslii,  bus 
even  been  spe<:ially  reciimmeiided  by  Mr.  C.  Davy,  on  the  ground 
thutitimpioves  the  cidour  of  new  and  interior  flour,  and  increases  the 
yield, — neither  of  whieh  result^  uofar  ati  the  public  is  eoncerned,  are 
in  the  leaat  de^iirablc.  The  increased  yield  dimply  8i>rnitiei)  m/^re  icater. 
The  ijuaniity  of  nu^neaiu  required  varies  fruni  20  to  40  grains  lu  a 
pound  of  flour. 

\\\i  have  already  referred,  to  some  extent,  to  the  advUertUioH  of 
breiui  u^ith  tvater.  Bread  naturally  contains  a  large  quantity  of  water, 
esttmnted  at  66  parts  in  every  160  of  bread —  16  of  these  only  being 
naturui  to  the  Ihiur,  but  it  is  frequently  made  Ut  contain  p'euter 
amounts:  one  principal  means  by  which  this  is  eflected,  is  by  the 
addition  of  rice  or  rice  tlour  to  bread  ;  this,  swelling  u|>,  absorbs 
much  more  water  than  wheat  Hour.  PutattH.'S  useil  in  any  quan- 
tity, probably  have,  to  some  extent,  the  same  efl'eet.  In  the  inlr<»- 
duelion  of  nee,  then,  into  bread,  there  is  a  double  evil:  first.,  n  sub- 
stance is  put  into  tlie  brt^ad,  which  does  not  f>ofl»eftS  nearly  so  niuch 
nourishntenL  us  wheat  Hour;  and  si'cond,  by  its  means  n  hir^erqtmntity 
of  another  substance  is  absorWd  by  llie  hread.  and  whii-li  really  baa 
no  nourishing  propt^rtics  wbalever.  While  wheat  llonr  seldom  con- 
tains less,  and  often  much  more,  Uian  13  per  cent,  ot  gluten,  rice  has 
only  about  7  per  cent,  of  that  nutritiaua  substance,  and  potalues  are 
equally  deficient  in  gluten. 

Another  way  to  increase  the  quantity  of  water  in  bread,  is,  af\er 
having  incorporateil  aa  much  water  in  the  douxh  as  possible,  ti»  put  it 
in  A  hot  oven  :  this  causes  the  crust  to  form  speeuily,  and  thua  the 
escape  of  the  water  is  prevented. 

Lastly,  the  same  object  ta  in  a  measure  attained  by  throwing  sacks 
over  the  loaves  when  removed  from  the  oven  :  this  prevent:^  the  dis- 
sipation of  some  of  the  water,  which  is  apt  to  pass  ufl*  6o  quickly  from 
tiie  bested  loaves. 

Several  other  articles,  in  addition  to  those  enumerated,  are  stated  to 
be  employed  in  the  adulteration  of  bread,  and  theie  is  no  doubt  but 
that  they  have  been  thus  employed,  such  as  bone  athes^  bone  duity  white 


S8a 


TLOUR   AND   BREAD, 


chtfy  the  carlmnates  n/  siida  and  magnesiny  chalk  or  earhonate  oflim^-,  and 
planter  t\f  Ptiria^  gypsiiin,  or  sulphate  of  lune, 

La:!^tl}-,  sulphate  of  cupper  has  b<i*>n  UReiJ»  |)riuei]iftlly  in  rielgiiimt  for 
the  same  purpu^tis  lu  alum,  viz.  to  whiten  Hour,  and  Lo  c:^u.<te  bread  to 
hold  more  water. 

The  retnltg  of  the  examination  of  numerout  samples  of  fiavr  and 
bread  for  alum,  tttny  wiv  be  stated. 

Oi'  twenty-eight  samples  of  bread  tested  for  alum,  that  substance 
was  i'ounrl  in  every  one  nfthe  samples. 

Some  time  subsequently,  a  second  series  of  samples  of  bread,  tweutv- 
five  in  nnnihrr,  were  nlso  tested  for  alum,  uiid  tlii.i  salt  was  found  in 
tlie  whole  of  the  samples. 

Three  of  ihe  bakers  whose  bread  wngexarauicd,  and  found  to  rontaiit 
alum,  declared  that  iliey  ditl  nut  uild  ihiiL  MibsluiR-e  ru  their  biead; 
and  they  plueed  in  our  handii  i-anipleii  urcbe*  llour  of  which  the  breads 
were  matie,  wlmn  the  alum  was  fouBd  in  the  fhnir^. 

From  this  it  may  be  inferred  that  tlie  alum  had  been  introduced  into 
the  flours  by  the  millers.  This  discovery  led  to  the  examination  of 
other  flours,  in  aevend  of  which  alum  was  ulso  derecUMl. 

In  the  course  of  our  inve^li;?ations  rGspectin;;  the  mhilteration  of 
bread,  we  did  not  fail  to  puy  some  attention  to  the  subject  of  wre/g-Ai,  a 
subject  second  in  iniporiunee  only  to  that  of  the  adulteration  of  bread. 
We  procured  a  number  of  luaves  of  bread  from  ilitferent  bakers,  ns 
delivered  to  houses,  und  weitched  them.  The  results  were,  that  tliirty- 
one  and  a  half  loaves,  obtained  from  thirteen  ditfereiit  bilkers,  were 
deficient  eighty-six  ounces.  Scarcely  a  single  loaf  reached  its  proper 
weight. 

In  onler  to  cheek  dishonesty  in  the  weij^lit  of  bread,  the  following 
simple  plan  is  in  operation  in  KdinbuTirb,  and  it  is  described  by  the 
gentlenuut  who  sug^resled  it  as  hitviii^  worked  exceedingly  well. 

It  is  made  imperative  on  the  bilker  to  st.imp  the  wi*i;;ht  upon  all  the 
loaves  he  ttells.  'i'lie  ])ruvision  to  this  efiect  is  contained  in  the  Foliee 
Act  of  Edinburgh. 

Some  idea  ot  the  extent  to  which  Hour  is  adulterated,  and  the 
feelintj  which  exists  in  the.  mind  of  the  people  in  rcganl  to  it,  may  ba 
gathered  from  the  fatit  ihut  extensive  IVoplu's  Kloiir  Mills,  sup- 
ported mainly  by  the  working  classes,  have  been  established  in  a  f^^ik^ 
nianv  of  our  lar^c  manufacturing  towns,  as,  amongst  others,  Leed4| 
Hull,  Harntiley,  Bradford,  Thirsk,  liristol,  Keighley,  Ualiikx,  Koch- 
dale,  &c. 


On  the  Detectiun  of  the  Adulterations  of  Flour  avd  Bread. 

The  various  substances  and  articles  era)>loyed  in  the  adulteration  of 
flour  and  bread,  may  be  classified  into  the  urf^auic  und  ivorgunic :  under 
the  6r»t  head  are  included  bean,  rice,  rye,  burley,  and  Indian  ccMm 
tlours,   potato  Hour,  and  potatoes;   under  the  second,  alum,  plaster 


WITH   THEIR   ADDLTEKATIONS, 


1«7 


I 

L 


of  Parid  or  sulphate  of  lime,  gypsum,  terra  alba  or  mineral  wliite, 
silicalti  of  Riiigiteftiu,  whttu  day,  carbmmtca  of  limCi  mognvsia,  and  •iuila, 
bone  ashea  or  phosphate  of  liine,  bune  (liut. 

On  the  lieiffliun  a/  the  Organic  Adtdierations  of  Flovr  and  Bread. 

The  only  meanii  by  which  the  adulterations  of  dour  nml  brt^ad  with 
the  different  kinds  ol'  6our  enumerated  can  be  discovered,  is  by  the  mi- 
croscope. 

The  discovery  is  very  nmcU  more  easily  eflectcd  in  tlour  than  in 
bread,  because  the  lieat  to  wLicb  breaii  in  subjecled  in  bakinj^  alters 
somewhut  tlie  orii>iuul  Ibrm  of  the  starch  granules,  and  so  renders 
their  ideniilicutioii  less  easy. 

The  chaructery  of  the  stai'chei  of  the  sovernl  flours  used  in  the  udut- 
teratiuD  of  flour  and  bread  have  already  been  described,  with  the  ex- 
ception of  potato  starch  und  bean  tiuur. 


Beat  Flocb.    Mas&IRcd  4W  dluncien- 


Jftfttr  and  starch  are  distinguished  from  the  other  flours  used 
atlalleratiim  of  wheat  flour  and  bread  by  the  oval  or  renil'orm 
of  the  fjrunules,  the  elongated  and  divided  chanicter  of  the 
^hitum.  and  the  thickness  of  the  walls  of  the  celU  enclosing  the  starch 
corpuscles.     Fig.  99. 


lape 


FLOUR   AND    BREAD, 

A  description  and  fi^re  representing  the  characters  of  poUlo  flour 
will  be  round  under  the  article  Arrowroot. 

Fig,  100. 


WilCAT  Fl^ra,  ftdtiltenMd  wtUi  Bean  Jltmr.   Mufnlflcd  (SO  dIUMten. 

The  tululterntion  of  wheat  flunr  with  barley  flour  is  one  by  no  means 
Wtty  of  diw-overy  wlien  we  cnnHiie  our  observaiions  entirely  to  the 
form  nf  the  rtlnrcli  corpuscles  of  the  two  kinds  of  grain,  the  difler- 
encfs  in  the  churnctera  of  the  starch  not  l>eing  very  consideruble.  The 
corpuscles  of  barley  .itarch  are  smaller  than  those  of  wheiiT,  ami  this 
is  nenrly  the  only  tangible  ditrerenee.  However,  the  di5crimtnation 
may  be  effected  in  a  very  satiafuclory  manner,  by  mcanii  of  tlie  por- 
tions of  husk  present  in  the  flour.  The  structural  peculiarities  of 
the  testa  and  ot  the  cells  forming  the  surface  of  the  <;rain  of  wheat  and 
barlev,  have  already  been  pointed  out,  and  to  the  description  of  these 
reference  may  now  be  made. 

In  the  exuminaiion  of  bread,  in  consequence  of  the  alteration  ex- 
perieiiccil  in  ihc  form  of  the  starch  cnrpiisclos  by  the  heut  of  the 
oven  in  baking,  it  is  in  some  cases  espcciaUy  necessary  to  loi»k  carefully 
to  the  structure  of  the  portions  of  husk  met  with,  and  of  which  6gWTS 
«nd  descriptions  have  already  been  given. 

Now.  although  nothing  is  more  common  than  the  use  of  mashed 
potatoes  in  bread,  yet,  so  far  at  our  experience  goes,  it  ia  by  uo  means 


4 


J 


WITH   THEIK   ADULTERATIONS. 


!69 


etsv  to  iletect  their  prejicn(*e  in  brend.     To  what  circumsUnces  this  is 
owing  wti  are  nut  quiie  sure :  the  lunsLed  pulatoes  are  not  nauoll/ 


1%.  101, 


added  direct  to  the  flnur,  but  thvy  itre  gencmlly  incorporated  witU 
the  yeuAt,  which  is  allowed  (n  remain  in  contact  with  tliem  few  some 
hours,  this  being  said  to  fetrd  an«l  grow  u\wn  the  potatoes.  It  is  po8- 
dible  that  in  thin  way  the  miijdriiy  of  the  cells  of  the  potato  lK.*coine 
broken  down  ami  no  longer  recognisable.  In  u  few  canes,  however,  we 
have  succeeded  in  detecting  jmtato  in  bread  by  means  of  the  luicro- 
ncope. 

The  HcluUerntioo  of  flour  with  Durra,  is  also  discoverable  by  zneaiiB 
of  the  microscope. 

On  tke  StntctHre  of  **  Durra,^  HoUum  Durra  saiipiu,  Forshiil ;  Sorghum 

pulgare. 

The  testa  of  the  grain  or  seed  may  be  described  as  consisting  of 
three  membranes. 

The  outer  is  composed  of  three  or  four  layers  of  thicJc-waHe<l  ccll», 
rather  small,  about  three  tin>cs  longer  than  broad,  and  having  the 
mtirgina  finely  beaded,  somewhat  as  in  capsicum. 

n 


tto 


Tk  midlife  cot  q 
Ml  filed  wxtk  hmU 


FUHTB   A3n>  BK£AI>, 
•f  WTcnl  bfcnof 


wuk  tkni  va^^ 


inuat  /iMr.  KlDltintcd  with  /mUiib  i>r»j«rM-.  UkpiUad  00  AaMcftf*. 

Th«  lAirr/  tmiic  resembles  thul  of  most  of  the  otiier  seeds  of  the 
j^amtnuin,  and  conviau  of  a  single  lajer  of  angular  gluten?  cells,  but 
which  are  unuBUulIy  Hmall. 

The  substance  of  the  »eed  resembles  rcry  closely  that  of  Indian 
com,  difleriug  chiutly  in  the  larger  size  and  greater  angularity  of  the 
fltan^  corjtiuwlea,  as  well  aa  the  stellate  clioracter  of  the  bilum.  See 
Jg.  104. 

The  last  or;ranic  adulteration,  the  method  for  the  discovery  of  which 
we  have  to  describe,  is  thai  with  hone  dujtt.  Bone  dust  coosista  nf 
the  dost  or  llour  of  bones ;  now  bunes  iio:»se«5  a  well-defined  structure 
wiiich  it*  Ui  some  extent  trnceuble  in  the  Hour:  again.  l)one  Hour 
cnnsitiis  in  Ittr^c  part  of  ptio^tpbate  of  lime  ;  thi^,  on  the  application 
of  nitrute  of  silver,  turns  yellow.  If,  then,  on  examining  any  sample 
of  flour  with  the  microscope,  we  discover  minute  bony  particles,  or 
if,  on  adding  a  i^mall  quantity  of  a  solution  of  nitrate  of  silver  to 
the  flour,  while  under  the  microscope,  particles  of  a  deep  and  rich 
(redden  yellow  appear,  it  is  certain  that  the  flour  is  aduliersted  with 
bone  dust.     The  <piantity  uf  bone  dust  used  must  be  colcalalcd  from 


WITH   THEJK   ADULTERATIONS. 


SOI 


the  qtuntity  of  pbospbnte  of  Um«  conUined  in  the  uh  of  n  given 
quintitv  of  the  flour. 

^.101. 


Pflkof  Brtml,  ultiltcntted  with  potirht.  MmgnltM  191  ill«meler« 

The  method  for  determining  the  presence  and  quantity  of  phosphate 
of  lime,  ifl  as  follows  *  — 

The  ash,  af[er  being  weighed,  is  to  be  treated  with  water:  this 
will  dis-solri'  uut  the  soluble  salts  :  next  with  hot  acetic  ucid  whicb  will 
take  up  thf  i>hoapbat«  of  lime.  The  phosphoric  acid  and  the  \im>i  are 
then  to  be  »eparutely  precipitated,  the  one  by  means  of  acetaie  of  lend, 
and  the  other  by  oxalate  of  ammonia;  the  precipitates  must  be  col- 
lected, weij»hed,  and  i-alcuUted  for  pltosphate  of  lime. 

In  most  cases  it  will  be  sufficient,  after  the  removal  of  the  soluble 
phosphiitvs  from  the  ash  by  means  of  water,  to  precipitate  the  phos- 
phoric ttL'iU  only,  and  to  calculate  this  for  phosphute  ol'  lime.  (See 
p.  25».) 

On  the  DetecHan  of  the  Inorganic  Atiuiterotiofii  of  Flour  and  Bread. 
On  the  Petection  of  Excess  of  Water  in   Bread.  —  There  are  two 
methods  by  which  the  presence  of  water  in  exce^s  may  be  determined, 

c  2 


FLOCR    AND    HREADy 

one  direct,  the  other  indirecl ;  thiis  if  we  discoTer  the  presence 
rice  ill  bread,  we  »*oortnin  indirectly  the  fact  of  the  existence  of  a 


Fig.  104. 


A.  loAtTCfw  arrtlnn  of  (eitm.  «5Wi.  o,  mitfr  i  t,  nik1dl«i  r.  Irncr  co«L  n.lfnifl- 
tadlnUaeeilun  of  t^u,  «3iN).  n,  oulettfr,  miailloj  r,  Inner  lunlc.  c.*liw,M«fr- 
ffhtnff  <if  Mtd,  thowlnK  >tt>c  larrc  kn^ular  c«lla  filled  with  rittrch,  of  wbl«h  It  !• 
onfiiiMNvl-  )■,  'SuVi,  ■'•rt*  »'  mr|r  c«IU,  thowlng  th«  pwudo-cvll  •tradun.  In 
wlileh  the  riuxh  cvtvuM-ic«  »rv  Ki>ui>l«lr  lodsetl.  x  i,  *Xii,  >tueti  l>om  tMl4 
Htd  ftom  tubatftocc  of  grain. 

surpliiF   of  wnt«r:  in  the  direct  metbod.  a  weighed    portico  of  ihe 
bread  is  evaporated  in  a  water-bnth,  until  it  ceases  to  lose  weight ; 


WITH   THEIR   ADULTERATIONS. 


2'J3 


the  lofls  gives  the  quantity  of  water,  wbieb,  in  ordinary  cases,  ftmounts 
to  66  piU'ts  in  -150  pnrts  of  lircad. 

The  procehscs  for  the  detection  of  ekalh  or  carboimte  of  iimr,  et/p- 
tuiti  or  sulphate  of  limf^  and  HiUmie  of  magnenut  or  siHiptUme^  Tiiivc 
filreaily  been  described  ;  that  for  the  Crst-naiiu'd  substance  wUl  be 
Jbuni]  ut  jiage  101.,  tUul  for  ilie  ^ecuhtl  tti  jiitge  90^  and  that  Tor  the 
third  ut  |>ai<Te  101. 

We  iiave  then  uitU  to  consider  the  iiiet1iud»  by  which  nilnerul  white, 
white  elny,  earburiiite  of  nm^iiesia,  caiboiiate  nt' !»odu,  alum  or  sulphHte 
of  potaith  and  aluniinu,  and  sulphate  of  copper,  may  be  detected  and 
edlimated. 

Oh  the  Dttci'tion  of  ^finerul  White  or  Terra  AUm^  &c.  —  Mineral 
while  is  a  hydrated  sulphate  nt'  lime  ;  the  process,  therefore,  for  its  de- 
tection is  the  same  as  for  sulphate  of  lime. 

On  the  Detection  of  China  or  Coruiih  Clay^ — The  procew)  for  the 
discrimination  of  theseearths,  the  composition  of  ^^hich  is  nearly  iden- 
tical, ami  whirh  consist  essentiHlly  nf  silicate  of  alumina,  resolvt^s  ilwlf 
into  an  anatyais  for  silica  iind  iduminn,  the  processes  fur  the  detection 
of  which  havL>  alremlv  been  dctaiU'd  ;  thnt  fur  alum  is  given  at  p.  *1'^A. 
As  the  tluur  in  which  it  oci'urn  may  contain  alum,  the  »u1phurio  acid 
must  be  ttetcrmined,  and  a  cnrrespondinif  amount  of  nlutnina  tlcductcd. 

Oh  the  Detectiaii  of  Carbonate  of  Magnetia,  —The  next  salt  em- 
ployed to  adulterate  Hour,  the  process  for  the  detection  of  which  hod 
to  be  de:«cribed,  is  carbonate  of  wiignesta.  For  the  discovery  of  iu 
presence,  we  may  proceed  as  folluws :  —  In  ord^r  l)i  ascertain  whether 
It  or  any  other  carbonate  is  present,  a  liitle  hydrochlorii:  acid  iihould 
be  atldod  to  a  small  ipiantity  of  tlie  Ijread  or  llour  spread  nut  on  a 
slip  of  j^lass,  and  while  it  is  under  observation  with  an  inch  object 
glus.  If  ever  so  alight  an  efTerve^.-ence  appears,  some  carbonate  is 
surely  present,  it  may  be  of  lime  or  ma};neAia.  The  processes  for  deter* 
mining  tlie  presence  of  lime,  and  estiiuittinz  its  amount,  have  ali'eady 
been  de»cribed  ;  that  for  ma^iieiiia  is  us  follows  :  — 

The  ash  is  to  be  treated  with  a  little  dilute  hydrochloric  acid,  water 
mlded,  and  the  solution  filtered.  Ammonia  und  oxalic  acid  or  oxaliite 
of  animnnia  are  now  added,  till  no  furlht^r  precipitate  takes  place  ; 
this  prccipitntcs  any  linio  which  may  be  presi-nl ;  the  Iif]uitl  is  again 
61lered  and  treated  with  chloride  of  ammonium,  and  ummonia  added 
in  plight  exc4.'R<s.  Should  a  precipitate  form  on  the  addition  of  ammonia, 
tnnre  chloride  of  ammonium  must  be  adiled,  until  the  precipitate  is 
redisstdved  ;  lastly,  phodphate  of  smla  in  excels  is  added,  tJie  mix- 
ture stirred  with  a  glass  rod,  and  allowed  to  stand  at  rest  for  some 
hours. 

The  maj,'nesia  is  precipitated  in  the  form  of  phosphate  of  magnesia, 
the  precipitate  is  collected  upon  a  filter;  when  lue  tluid  has  drained  o(T', 
it  ij)  to  be  treated  repeatedly  with  a  mixture  of  water  and  anmtonia, 
in  the  proportitm  of  four-fihhs  of  the  former  to  one  of  a  solution  of 
the  latter.     This  operatiuo  is  rejieated  until  the  lluid  passing  thru>jj];U 

c  3 


FLOTR   AND    BREAD —ADULTERATIONS. 


Ok*  4Nvr  vcmm  to  lenve  a  residue  when  evaporated  nn  i  platinum 

'So  prwipitattf  iv-  now  drie'l,  transferred  to  a  plalinum  cru- 

•■-  w  fxjwisyd  (or  some  lime  to  a  gentle  heat,  whicb  is  ofter- 

iA*A5vtl  to  intense  redness :  lastly,  the  prt'Cipittie  is  wei^lietj, 

!*to*!,  for  carbonate  of  ma^esin^  br  two  sum^.    Hy  llie  first 

'  I.     ^  I  ihiily  of  magnesia  in  the  pyrophosphate  is  asccrtiiinett,  and  by 

i      » I  •  ud  this  magnesia  is  converted  into  the  carbonate  of  that  base. 

I '  '      I  •>r»ui9,  an<l  bulky  character  of  the  ash  of  any  flour  con- 

teio  -lii,  \s  itself  sutficient  to  excite  suspicion  of  the  presence 

v/  l'i'«     •'•K.^iatK'i'. 

l^it<  u\'\t  5ttU  employed  in  the  adulteration  of  ilour  and  bread, 
ikv  |a\kHMd  tor  the  detection  of  whicb  it  is  necessary  to  describe,  ia 

Ot   M/-    Di^teetion  of  Alum. — This  salt  consists  of  a   sulphate  of 

itid  i>otn.sh.     In  general,  in  analysinM;  flnur  or  bread  for  this 

•  >',  i(  IS  not  necessiiry  to  do  more  than  estftimtc  qunnlitatively 

itiv  iilMMiiuH;  it  is  salL'^r,  however,  when  we  desire  to  exclude  every 

|*<«*Mihiliiv  of  a  ntistidce,  to  esiinmte  the  i^ulphuric  iit'i<l  as  wull. 

l1io  Ibllowing  is  one  uf  the  best  processes  which  can  Ije  adopted  ;  — 

tncinciatu  1000  ^rrg.  nf  the  Hour  or  bread;  boil  in  n  Husk  with 
i  drtichiiu  of  nitric  acid,  4  of  hydrochloric  ncid,  and  4  of  wnter  ;  eva- 
M>vate  l«>  drynes*.  When  cold  adtl  one  ounce  t»f  distilled  wat*T.  and 
U'tl  for  a  few  minutes;  while  boiling  dilute  with  one  ounce  lifj. 
(k'lAuiv.  nnd  bdil  again  for  it  few  ininuti'S  ;  then  litter,  nearly  neutralise 
wiih  hydi'iH'hloriu  acid,  and  jirt'cinilute  with  ammonia. 

The  itrccipilated  alumina  sliould  be  washed,  dried,  i^inled  in  a  pla- 
liuMiu  di»h,  weighed,  and  cnleulated  for  alum. 

Thy  purity  of  the  reiigeniM  employed  in  this  amdvsis  should  be  pre- 
%inu»lv  a«eertnined,es]iecially  that  ofthe  siilutitm  ol  ptitiish;  indeed,  it  is 
taf'e*t  to  prepare  these  oneself:  the  nitric  nnd  the  hydrochloric  otid  may 
bo  oblaiiicMl  pure  by  simple  diMtillntlnn  ;  and  pure  (totush,  from  whirb 
iht'  votulitm  can  afterwards  be  made,  may  be  procured  by  the  action 
ofNtcohol.  Mistakes  have  fretjuenily  occurred  in  consequence  ff  a 
nvgloct  of  these  precaution*!.  When  the  potiL^h  eonuiins  a  minute 
ipiantity  only  of  alumina,  this  may  be  deiiucted  from  the  general 
rvsult. 

It  iboidd  be  reinembere*!  that  salt  sometimes  oonUins  minute 
ipiatitiiies  of  alumiiui,  as  well  as,  it  is  alleged,  certain  descriptions  of 
wheat. 

The  quantities  of  alumina  in  two  saraplfs  of  salt  analysed,  amounted 
in  the  one  sample  to  005,  ami  in  the  other  to  0  06  per  cent.;  we  muft 
therefore  not  infer  the  presence  of  alum  in  bre;id,  when  ([uantiiies  of 
alumina  are  diwovered  as  stiiall  ns  iIiohc  just  referred  to. 

Some  rhemists  have  described  the  ruUuwinj;  method  for  the  detection 
of  alum  :  — 

Soak  the  flour  or  bread  in  water,  filter  the  solution  and  treat 
with    ■nimonia,    the  precipitate  which  ensues   is   desc.ribed  as   olu- 


BUTTER,    AND   ITS  ADULTERATIONS. 


29ri 


minn.  Thi^  proce^^s  is  utterlv  falladous,  as  n  precipitAte  alnii)'s 
occurfl  under  such  circumstances,  even  in  the  absence  ot*  alum,  the 
pret'ijMtnte  in  frcneral  conifittting  of  nitrogenous  matter  ami  vartby 
phosphates.     We  refer  (o  this  proi-esa  in  unler  thiit  it  may  be  avoidcJ. 

Oh  tht  Detection  of  Suiphatenf  Copper — For  the  iletecrinn  of  copper 
in  brcail,  the  processes  described  under  the  hwid  of  Picklea  may  be 
followed. 

Ferrooyanuret  of  potasi^ium  is  a  rcrv  delicate  test  for  copper  in 
bread  :  if  the  bread  be  moistened  with  a  solution  of  th&t  salt,  it  will 
assume  a  pink  tin;;e^  more  or  less  deep  accordiii;:  to  the  quantity 
present.  It  is  titated  that  the  preaeni.'c  ol  <me  part  of  cop[»er  in  9(>00 
of  breiu]  may  Iw  discovered  in  ihis  way.  Fur  the  discovery  of  copper 
in  the  ash,  3000  or  4000  grains  of  the  bread  should  be  incinerated. 

Duty  on  all  flour  and  meal  i^d.  per  owt. 


Entered  for  Home  CoHsvmptiott. 


IKM. 

ISW* 

Whmtf  m»l 

Barlrf  tnral  ..... 
Oatinnl       ..... 
tiff  inral       ..... 
Pe%  mrkt        -            -            .             .             . 
BCU  IBM!      ..... 

tndtui  corn  meal     -                      -          • 
Buck  whrat  meU     -           -           -           - 

ToUl  of  mr«l  - 

Grand  Total  of  Cum  and  Klour  In  lu  equU 
»«lm!  of  Grain     -           -           -           . 

7S 

5 

I 

Cwt». 

1, tin,  101 

Ml 

758 
9*7 

IfiS 
19.1M 
S,ft74 

3.r3i,7l7 
5;iil 

3.73!*.  107 

1,940,3  rg 

a.ttl.MMt 

7.*iMlblo 

D.lSlJU 

ti.Suin 

BUTTER,  AND  ITS  ADULTERATIONS. 

Fbom  Bread  we  pass  on  to. Butter  ond  its  .\dnlteralion». 

Am  the  method  nf  mnking  butter  may  not  be  known  to  many  of  the 
readers  of  this  report,  we  will  proceed,  before  entering  upon  the  con- 
sideration of  ita  adulterations,  ingiveavcry  brief  outline  of  the  manner 
in  which  butter  it;  usually  prepared. 

u  4 


S9« 


ttUTTER,    AND    ITS  ADULTERATIONS; 


Butter  is  made  for  the  most  part  froni  cream  ;  the  cream  iscollecteil 
from  time  to  time,  and  pluced  in  u  covered  jar,  until  suflicient  has  been 
obtained,  when,  having  become  sour  by  keeping,  it  is  submitted  to  ihe 
process  of  churning. 

Butter  is  aUn  prepared  in  f^mall  r^uantities  from  sweet  cream,  and 
this  kind  is  esteemed  a  frr^iit  delicncv.  Very  excellent  butter  ia  like- 
wise £iuiuotimo9  mnde  from  full  or  entire  nulk  ;  the  disadvanti^cs  of 
thia  method  ore,  the  large  quantity  (>f  fluid  to  be  acted  on  bjr  the 
i'hurn,  whitrh  remlers  it  neceesnrv  Llmt  steam  or  aonie  other  powerful 
meclianicul  means  should  be  bad  recourse  to,  and  the  length  of  time 
which  elapse*  btforc  the  butter  forms. 

As  soon  as  the  butter  has  formctl,  it  is  removed  from  the  churn,  and 
well  witched  in  water,  it  being  kneuded  nt  the  same  time  until  as  much 
a3pos:iihlfi  ol'  the  ndliereiit  and  incorporated  whey  is  removed;  this*  i:* 
known  by  the  water  ccasinf;  In  become  tiirbid  and  milky.  If  intended 
for  sfllt  butter,  the  salt  Bhouh)  be  adtled  as  soon  as  possible  after 
cburninj;  and  washing,  as,  lefi  for  any  len^rlh  oi  lime,  the  butter  is  apt 
Iff  btoouie  mm^id,  Ureal  attention  should  bti  piud  to  the  quality  <*t' 
the  salt  used  ;  ihe  best  descriptions  are  rock  salt,  and  that  prepared 
from  salt  springs.  Sea  salt,  generally,  '\*  not  so  piHitJ,  on  account  nf 
the  presence  orsulphaie  of  magne«<iiL,  width  renders  it  ."onn^whut  bitter, 
as  well  as  of  cidoride  of  calcium,  which  lias  a  strong  allinity  for  water, 
even  altrartlng  it  from  the'  atmosphere 

It  would  be  out  of  place  in  this  report  to  enter  into  the  practical 
minutiK  of  biittcr-muking,  such  as  the  ternpifriiture  at  whirh  the  cream 
or  milk  should  be  cliurned^  the  best  kiniK  of  churn,  the  methods  of 
churning,  &c.,  nil  points  of  the  greatest  importance. 

According  to  Chevreul  and  Messrs.  Bronu'Tsand  Heintz,  butter  con- 
tains margaric,  butymleic,  butyric,  cupronit.%  capryHc,  andcapric  acids, 
together  with  glycerine.  The  ntar;:arine  or  ui;irgurate  of  gtyoerine  of 
butter  U  ootid  tit  Common  temperatures  ;  but.  the  combinations  of  its 
other  fatty  acids  wiih  glyeerinc,  constituting  bulyroleiue,  butyrinc, 
capronine,  capryline,  and  caprinine,  are  tlitid. 

According  to  IJromeTs,  100  parts  of  butter  rontarn  about  08  purls 
of  murgariiie,  and  flO  of  butyroleirif  ;  the  remainder  consists  of  the 
glycerine  compounds  of  the  other  acids. 

The  oily  or  buttery  part  exists  in  milk  in  the  form  of  innumerable 
very  distinct  globules,  of  varlou*  Hizen.  The  efl'ect.  produced  by 
churning  is  lo  break  down  the  greater  nuud)er  of  these  globules,  which 
then  run  together,  and  thus  fonn  butter.  The  operation  of  ihe  churn 
'm  tlierefore  chiefly,  if  not  entirely,  mecfianical. 

Examined  with  the  micruvcope,  butler  is  Heen  to  contain  a  great 
number  uf  milk  globules,  but  liMle  altered  iu  ibrio  and  Hixe ;  unlike 
lurd,  no  crystals  of  stearinc  are  perceptible. 

Keferring  to  works  treating  on  Fnc^.l,  we  do  not  meet  with  any  facta 
relating  to  tbe  adulteration  of  butter. 


BllTTEn,    AND   ITS    ADLLTERATION8. 


S9: 


* 


I 


OV  THK    Al>UI'TBBAT10NS   OF   BuTTEB. 

One  of  the  most  frequent  practices  had  recoorsc  to  in  the  cnse  of 
butter,  is  to  ineorpoiaie  wilh  it  large  qutintitiea  of  irafcr;  ihe  incor- 
poration 19  effecle<l  in  the  fnllowing  loamier:  the  butter  is  brouglit  to 
the  melting'  point,  water  un^l  mU  lire  then  stirred  to  until  the  mixture 
becomes  eolti. 

In  reftfrence  t<t  the  adulteration  of  butt«r  with  water  and  salt,  Pro- 
feniior  Calvert,  in  his  evidence  before  the  Parliamentary  Comnurtee  on 
Adutieraiion,  maile  lliese  remarks: — **  The  quuntity  of  water  and  salt 
that  5>ucb  an  article  as  butter  ought  to  contain  is  '2\  per  cent,  of  salt, 
»mJ  10  per  cent,  of  water.  In  the  butter  supplied  to  these  unions  the 
quantity  of  salt  varied  from  2  uptu  14  jwr  cent.,  and  the  water  from 
10  Ut  15  per  cent." 

Another  adulteration  to  which  butter  is  occasionally  subject, 
especially  the  inferior  k-nd  known  as  Botih,  consists  in  the  ad«lition  of 
jfttrcA,  usujdly  pofuto  Ji<mr.  This  adulteration  is  practised  only  at 
particular  times,  ami  is  dependent  upon  the  wholesnU-  price  of  butter. 

Ai;ain,  butter  has  been  known  to  bo  aduUernti.Ml  sometimes  with 
curds.  This  adullenition  is  i)articularly  mentioned  by  Sir  John 
Gotnlon,  mayor  of  Cork,  in  his  evidence  before  the  Parliamentary 
Committee  above  referre^l  to. 

Lit&tlvt  animal /aOt  are  occasionally,  though  not  frequently  employed, 
U  the  fat  of  vettl^  and  iard;  these  adulterations,  again,  are  only  resorted 
to  when  butter  is  very  dear  and  lard  the  reverse. 

HenlU  of  the  Examination  of  SainpUa, 

The  examination  of  Forty-vight  difl'ercnt  samples  of  butter,  both 

salt  and  fresh,  furnished  the  lullowing  results:  — 

That  all  the  »qU  Imltert  examined  contained  variable  and  usually 
very  I«r};e  quanliiics  of  uxtter^  the  amount  ranging,  with  one  ex- 
ception, from  8'48  to  2kG0. 

That  the  /rtfjih  bxtUerx  likewise  rontatned  variable  uid  of\en  con- 
sid(M*able  quantities  of  uvj/^r,  but  in  mitst  cases  very  murb  less  than 
in  the  suit  butters,  the  quantiri^-s  rari^inj;  from  418  to  15'43. 

That  the  quantity  of  salt  contained  in  the  salt  imitern  varie«I  from 
1*53  to  8 '24,  shoffinj^  thai  no  fixed  rule  is  acted  upon  in  sailing 
butter. 

That  in  \S\e  fresh  buffers  the  salt  variefl  from  0-30  to  2*91. 

That  the  per*centages  of  niilter  contained  in  the  samples  ranged 
from  H772  to  9G'93  ;  that  is,  some  at  l\w  samphit  contained  20,  30, 
And  in  one  case  even  nearly  35  per  cent,  of  water  and  salt. 

Now  the  presence  of  water  in  butter,  in  excess  and  when  purposely 
introduce<l.  a-'«<«ure<lly  con^ttitutes  an  adullenition  as  much  as  does  the 
addition  of  starch  or  animal  fats. 

To  many  of  the  samples  of  salt  butter  examined,  a  quantity  of  salt 


9M 


BUTTER,  AND  ITS  ADULTERATIONS. 


civor  nnd  iibove  the  amount  necessary  to  insure  the  preservation  of  lie 
Imtti'i'  Imil  no  tluubt  beun  purposulv  added  to  increase  the  weight  and 
bulk;  in  tliol,  fur  llie  unki?  dI' udulUration. 

It  it  iMiually  t'eitiiiii  ilmt  mucb  of  the  water  met  with  in  many  of 
iKi'  KuiiipU'ii  hud  beon  added  for  the  same  purpose.  The  ijunntiiy  of 
witti'i-  [iri'nt'iit  in  dome*  inferior  dcwriptioiis  of  butter,  as  especially  Bosh 
iind  ilir  wi>r«t  kitidN  of"  Hiillmids/'  is  really  surprising,  amounting  in 
«(inii'  ciiMH  to  mnn.'  tliun  a  liiinl  of  ilie  article. 

Oil  tbi'  pulilit^utinn  of  our  UeiKirt  (^^ii  tliu  Adulteration  of  Htitter  in 
"Tlii«  l.iuii;t'l,"  Mr.  Ktibert  Miller,  a  butter  factor  of  Wellington 
ChaMibLTS,  London  Uridge,  wrote  to  that  journal  to  tbe  following 
efl'uct ;  — 

"  To  tht  Editor  o/Th«  Lamcbt. 

"  Sim. — H«*in^iiti  rooted  lothe  article  in  your  publication  of  June4ih 
on  thu  '  Ar)iiUi!rticinn  of  Butter,*  by  the  conspicuous  mention  of  my 
nunio,  I  tihko  the  liberty  of  Mtiitin};  that,  although  I  believe  in  the 
fidi'lity  of  your  uniily^tea^  there  are  two  things  you  are  wrong  in. 
Finr.  ibo  auionuL  of  aduliorution  in  the  worst  sample  is  staled  to  be 
twenty-nix  j»cr  cent,  i  Recount  for  this  thus:  The  adulterating 
proceNfl  in  (u  bring  lUe  butler  to  the  melting  point,  then  to  stir  it  in 
wntcr  und  null  until  t,iie  mixture  h  cold,  rjrty  per  cent,  of  water 
may  Im>  iiHorponited  with  butter  in  this  way;  but  when  you  make 
your  |imcbHse,  »ay  half  n  pounrl,  u  considcnible  pnrt  of  ihc  water  of 
BdullcriUinii  will  cf<caj>Ct  and  it  you  put  it  iti  paper  considerably  more 
will  be  toal.  'Hit*  next  wiiy  ynii  iiii^ht  be  deci-'ived  is,  if  you  ask  for 
KepufkH  (Irish)  ur  Ulack  Jat  ks,  or  liosb  (Holland),  the  shopkeeper 
may  nuupcrt  your  sdenlific  object,  an<l  give  you  better  butter  mstead  ; 
but  if  tlic  public  adopt  your  suggestion  of  meltiug  butter  in  a  eleiir 
brittle,  llii-y  will  prove  what  1  have  almve  said,  that  twenty-six  per 
cent  of  mbilleralion  in  thcMC  l>utters  is  understating  tbe  amount. 

"  In  llie  natiH'  nf  the  trmJe,  I  may  timnk  you  for  your  article  •,  becauite 
a  nLi;;liljnunng  shop  selling  *  cbeu|)  butter'  i-ompels  other  shops  to  do 
so  aUo ;  but  the  traile  arc  now  nwiire  of  tln^  inirpiitous  article,  and 
are  borrilied  by  being  thus  compel  lt>il  to  cheat  their  poor  cuatomers 
with  *  cheap  butter^  while  tbcy  are  also  porft'trtly  aware  of  the  great 
losa  of  weight  to  themselves  by  culling  up  ibis  watery  butter  in  small 
f|uanlitieii.  The  triidf  wnubl  all  be  ghid  to  gue  uj)  the  sale  of  adul- 
leratetl  butter  if  u  puWlc  movemuiu  were  made,  so  as  to  compel  all 
the  •ihopkeepcrs  to  do  so  ut  the  same  time. 

"  I  am,  Sir,  yours  trulv. 

"  Robt.  Miller, 
"  VrtlllnrtoD  ChatntHirt.  L«nclon  Brldce,  June.  ISU. 

"  N.B.— 40,000  to  50,000  casks  of  adultornted  butter  are  annually 
sold  in  London,  and  the  trjdc  knows  it  as  welt  as  they  know  a  bud 
shilling;* 


I 


BUTTER,    AND   ITS  ADDLTERATIOXS. 


S9» 


There  is  a  praolicc  ratlipr  extensively  adopted  of  making!  a  <a-called 
fre?b  tVoin  suit  butter;  altbuu;:b  this  is  not  un  iidullerutiun,  it  is  jet 
n  deee|>ii(ju,  nut]  as  tlie  process  by  wbieh  ihe  transCoruistion  la  eflected 
i.4  rather  ingenious  and  itomewbat  amusing,  the  reader  iimy  bti interested 
by  a  description  of  it. 

**Epping  Butter, 

»  To  the  Editor  o/Thb  Lahcbt. 

*'  SiH, — Having  taken  apnrtniCQt£  In  tbe  house  of  a  huttcrman,  I  was 
suddenly  awoke  at  three  o'clock  one  morning  with  a  noi^e  in  the  lower 
pnrt  of  the  house,  and  alarmt'd  on  perceiving  a  lif;ht  beluw  the  door  of 
my  liedruum  ;  conceiving  tbe  house  Ut  be  on  tire,  I  hurried  down  stairs. 
I  found  tbe  family  busily  occupied  ;  and  on  my  expressing  alarm  at 
the  house  beinff  on  fire,  they  jocosely  inruruied  me,  they  were  merely 
making  Eppi.>n  rvttrr  ! 

*'  They  unhesitatingly  informed  me  of  the  whole  process.  For  this 
parpose  ibeymade  usetrf  Irisli  s.tUcd  butter  of  ii  very  inferior  quality. 
XTiia  was  repeatedly  wa-hed  wiih  water,  in  order  to  free  rt  from  die 
»alt.  This  bein;j  aecoiuplihlKMl,  ibe  next  process  was  to  wjudi  it  fre- 
rjuenlly  with  milk,  and  iIk*  niunufdcturij  wiiseouipleted  by  1  lit.*  addition 
of  a  small  4uantity  uf  itugar. 

'*Tbe  auiBteurri  of  fresh  '  Kpping  butter*  were  supjplicd  wiih  tliis 
dainty,  which  yielded  my  ingenious  lnndlnrd  a  protit  at  least  one 
hundred  per  oent.,  besiiles  eBlablishiag  his  shop  as  being  supplied  with 
Kpping  butler  from  one  of  the  firat-ratc  dairies. 

**  I  am,  Sir,  your  obedient  servant, 

"AStvdait. 

**  York  Road,  tombelh,  Juoe.  I6A3." 

Perceiving,  then,  to  what  an  extent  Halt  butler  is  Jidulterated^  with 
both  water  and  excess  of  salt,  we  vury  mucb  ihmbt  whether  any 
saving  is  cfleclod  by  the  use  of  ibis  description  of  butter;  aiihough 
Dominally  cheaper,  it  '\a  questionable  whether  it  be  not  really  dearer 
in  tbe  end. 


Oh  the  Defection  of  the  Adulteratioiis  o/Btttter. 

The  chief  adulterations  of  butter  are  with  water,  starch,  excess  of 
ftalt,  and  animal  futs. 

On  the  Detection  of  Water. — After  being  churned,  butter  is  kneaded 
in  water  in  order  to  get  rid  of  the  whey  wtlh  which  it  is  incorponited  ; 
the  adoption  of  this  prwe^s  would  iicci>uut  fur  the  presence  ot 'j  small 
quantity  of  water  in  butter. 

There  are  two  methods  by  which  the  quantity  of  water  in  butter 
may  be  determined  ;  diiu  i>tmple  and  popular,  the  other  more  scientific 
and  exact. 

Fir^t  Method. — Tbe  butter  is  to  b«  melted,  and  a  bottle  filled  with 


aoo 


BUTTER,   AND   1T3   AI>LLTKBATIOK9 


it.  Tht«  is  to  be  placed,  for  half  an  hour  or  so,  near  the  fire ;  the  water 
and  »u)i  will  becunit*  tjeparated  IVoui  tbe  butter,  nrid  sink  un  account 
of  lluMr  j^reatcr  weight  or  speciBc  jjTuviLy.  Owiii;j  to  ilie  water  being 
mixml  with  A  little  whey,  it  usually  presents  a  while  and  uiilky  uppear- 
ance,  vi-ry  distinct  from  that  (if  the  Imrit^r  ilst'lf,  whicli  fludTs  upon  it, 
and  whit;h  is  more 'or  lesit  yclKiw  ;  the  quantity  itf  wutiT  i*i  tlioii 
roughly  estimated  hv  noticing'  the  hci);Ut  it  reaches  up  the  botile.  In 
many  eu^e^  it  will  \}i'  found  that  the  water  constitutea  a  fourth  and 
even  a  tliird  of  Che  artK-ie, 

Setond  MelljO'l. — One  hundred  gniins  of  the  butter,  which  must 
not  hiive  been  previously  fxposfd  to  ilie  air,  or  part  of  the  water  will 
already  have*  become  dissipated  and  lost^  niuatbe  evaporated  inaauiall 
glass  or  iKircelain  dish  or  capsule^  over  a  water-bath,  until  it  ceases 
to  lose  weifjlit;  the  butter  and  the  eapt^ulc  nmsr  then  be  weighed,  and 
the  wri}»IiL  of  the  capsule  deducted  ;  the  dclieiency  on  the  original  100 
{grains  represents  The  per-cent^ige  of  water  i.-uiitained  in  the  butter. 

It  is  possible^  that  in  some  cases  the  question  mij|;ht  arise,  as  to 
whelher  the  Huid  separated  im  nieltin*;  butter^  consisled  of  wnter  or 
whey,  or  of  both  mixed  ;  this  point  may  be  det<^rmined  by  estimating 
the  amount  of  rtuvand'milk  present  in  the  I'upiid,  This  is  effected  by 
the  procejts  described  in  the  article  Milk.  One  thousand  grains  of  whey 
usually  eonl;iin  about  sixty  grains  of  sugar  of  milk. 

On  the  Detertimi  of  Starch.  —  Slarrli  in  btitti>r  uiay  he  readily 
detected  and  its  iimount  estinmted.  For  its  detection,  nothing  more 
is  necessary  than  1o  exumine  u  minule  portion  of  the  buuer  6pread 
out  in  the  ihinnesl  |>o?Kible  layer,  and  covered  with  a  plate  of  thin 
chiss,  with  a  half  or  ipiarter-inch  ohjecC  filass,  tincture  of  iodine  being 
in  sntnii  ea-*e)t  emjiloyed  at  the  same  time.  Tlie  ^tnrch  will  be  recog- 
nised by  the  (unti  )tf  the  granules  and  the  action  of  iodine. 

To  estimate  ilj*  fjuantitv,  tho  folKiwing  proceeding  may  be  adopted: 
—  The  butter  may  be  melted,  when  the  >tnreh  will  separate  with  the 
water;  the  jirecipitate  may  be  collected  on  a  filter,  dried,  and  weigheil; 
or  the  fat  may  be  reinoveil  by  means  of  ether,  when  the  residue  will 
conxiiit  chieHy  of  the  sturch. 

On  the  Detection  of  Lard, — We  are  not  acquainted  with  any  very 
direct  method  by  which  the  preseni'e  of  1  -rd  in  butter  may  be  dis- 
covered. So  far  as  we  have  observed,  one  of  the  bewt  tests  is  furnished 
by  the  microscope:  lard  t-onsiabK,  in  the  solid  ntate,  in  great  part  of 
vryst^als  of  murgaric  and  stearic  acid?,  while  in  butter  no  such  Ibrnm- 
tions  are  met  wiih»  but  only  nuraerouf  milk  globules.  When,  there- 
fore, crystals  similar  to  those  represented  in^i^.  } 05.  occur,  there  is 
gooil  reason  to  Busjiect  the  admixture  of  lard. 

Agiiiii,  the  melting  (Kunts  of  lard  and  butter  somewhat  differ. 

Oh  the  Deteftion  of  Salt. — A  weigheil  portion  of  the  butter  must  be 
incinerated,  and  the  salt  determined  from  (be  a^h.  In  general  the 
whole  of  the  a»h  of  salt  butter  may  be  counted  as  salt. 

Duty,  5».  per  cwt. ;  *2s.  6//.  from  llritish  [wsscssiona. 


LARD,   AND    ITS  ADCLTERATIOX8. 


301 


Tmports  taken  for  home  consumption  :   185-4,  478,811  cwts. ;  1855, 
448|268  cwts. ;  nine  monlfas  uf  18.56.  363,877  cwts. 


LARD,  AND.  ITS  ADULTERATIONS. 

Lavo  is  the  oilv  portion  of  the  fat  of  die  pig.  Tbe  prucess  by  wliit  h 
ihin  is  Kpiirated  from  the  vesiciiliir,  fibroug.  and  vascular  tissut's  in 
which  it  is  eitht-r  enclosed,  or  by  which  it  ia  surroumied,  is  Icnuetl 
litrd  reudiTtg. 

The  piecx-s  of  fiit  to  be  convcrtcfl  into  lard  arc  ^onictiincs  saltcii  a 

litlle,  tbelH-'ltcr  to  ensure  thiir  prescrvniion,  and  are  stiiretl  in  barrel*. 

'Jlii!  fjt  wUiili  ienniediutcly  surrounds  tbe  kidneys  yields  the  be:(t  and 

purest  Iiinl ;  this  is  owing  to  its  being  In  a  freer  state,  that  \iy  it  is 

few  hiylily  organised.     The  procesM  is  ;i»  follows  ;  —  The  pieces  of  fat 

are  scored  or  sliced  into  leaser  portions  of  an  inch  or  so  in  di.imeter ; 

they  are  place<l,  either  with  or  without  the  addition  of  a  litile  water, 

in  cauMroHfi,  which  are  usually  of  iron.     The  mode  of  applying  heat 

M  rhe  tlure  varie?)  in  ditferent  ciise-i.     When  lord  is  made  on  a  small 

scale  the  flame  is  often  applied   dirtcdy  to  the  containing   vessel  ; 

sometimes  tlie  tlare  if*  meliod  in  u  wnier-batb,  but  ut^uully  the  hentin^ 

medium  is  steam,  which   is  contained   in  the  interval  between   the 

inner  and  outer  ve«»el  ()r  pan  ;  occasionally  a  jet  of  steam  is  thrown 

directly  uptm  the  Hare  contained  in  the  copper.     The  soluble  part  of 

the  tat  melis  out  and  floats  on  the  surface,  the  nniiiiiil  nuitter  and 

tiif-tue!)  each  forming'  a  s<-uui,  which  \»  skimmed  frotii  time  tu  time,  or 

finkin;;  us  a  deposit.     As  the  *iil  has  no  affinity  fnr  cither  water  or 

*alt,  it  docs  not  Like  up  any  of  the  water  which  may  be  present  with 

it  in  the  copptT,  whiU*  the  suit  used  lo  prcticrve  the  tat  ialls  as  a  se- 

tlimcnl.     The  oil   whilst  sllU  warm  and  llnid  is  turned  out  of  the 

copper  through  a  Ijp,  mul  is  rei'eive<l  eiihifr  into  bladders  or  c^isks 

t«;rmed  kegs,  and  benre  the  division  ot  lard  into  blatider  lard  mul  keg 

Inrti.     ll  i.s  u-Hually  the  best  description  of  liini  mily  which  i.i  siored 

in  bladders,  keg   lard   bcinp  lor  tbe   most  part  of  inferior  qiiulitv. 

Good  and  pure  lard  should  be  entirely  frt^e  from  either  taste  or  smell  ; 

it  ebould  be  firm  n[;d  wbile.  and  whtn  meltrd  be  Liliuo<<t  as  clear  and 

transparent  as  water;  ^ubjected  lo  a  Ccmperutuie  of  about  212°  Ffthr^ 

it   should   lic|uefv    without  ebuliiliou,  thus  e^howin^  the  absence  of 

water,  nml  should  not.  throw  down  a  jmrtick'  of  iK-posit.     Inferiiu*  or 

adnlterated  lanis  p<>»>e3s  characters  and  properiies  aliuotft  the  reverse 

of  these.     The  mfltin;;  |>oint  of  lard  varies  frnni  785°  to  87'^*''  Fuhr. 

According  to  Hraconntft  its  composition  is  as  follows ;  — 


aos 


LARD,    AND    ITS    ADLLTERATI0N8 


Proximate  Analysis  of  fresh  Lard. 
Steorine      1 

Margarine  j         '  "  ' 

Elaine        -  •  •  *        6*2 


Our  supplies  of  lard  arc  derived  prim'ip«lly  from  Ireland,  part  nUo 
couics  frnm  America  utkI  llambiir;<;l)f  wliile  Loiulon  and  our  cbief 
proTinctal  cities  posseus  lard  manufactories. 

The  ADULTERATTONa  or  Lard. 

We  liave  long  beerii  aware  that  lardL,  like  nearly  every  other  ortiile 
of  consumption,  is  linlile  to  adulteration;  indeed,  the  fact  tliut  it  w 
so  is  veijr  (ji^JiiTidly  known  to  dealers  as  aUo  the  nature  of  the  prin- 
cipal adullorulions  practised. 

The  chief  adulterations  of  lard  resemhle  those  of  butter,  and  ctm- 
sisit  in  tlie  mcorpi>r:ition  with  it  of  water  and  starch.  Sometimes 
the  ivaler  only  or  iho  starch  only  is  had  recourse  to;  in  others  buth 
these  adulterations  are  pnicti^ed  on  tUi.'  same  hird. 

We  have  ourselves  met  with  many  fanipUsof  lanl  adulterated  with 
potato  tlour;  but  one  of  the  earliest  to  draw  tilteTiti<iii  to  ihe  subject 
was  Mr.  George  Whipple  in  a  c»iiiinunicution  which  he  hroupht  before 
the  I'harrnsceutical  Society,  and  which  was  noticed  in  iu  Jciirnul  for 
January  I8d3;  in  this  he  t^tates  ibat  he  had  detected  large  q^uantities 
of  some  farinaceous  Ruhstance  in  hird. 

"This  adultertiLion,"  writes  Mr.  Whipple,  "  was  discovered  in  the 
ditTeront  varieties  of  lard — from  the  finest  blailder  to  the  common 
firkin  hird.  Tn  nn  examination  of  the  CTtntenta  of  two  firkins,  weighing 
105^  lbs.,  a  quantity  of  furinaeeouii  substance,  amountin*;  t!i  2'2|  Ibs^ 
WM  separated.  The  content*?  of  anoiher  firkin^  weighing  43J  Iha., 
yielde<i  12|  lbs.  of  n  similar  sulMtance." 

In  the  next  number  of  the  same  journal,  Mr.  Calvert,  of  Mnn- 
Chester,  publisht.'d  numc  further  observations  on  t)ie  adulteraiion  of 
"American  larii."  Ho  writes  —  "During  the  nnmernus  analyses  li 
inndc  some  three  years  since,  of  various  nrtieles  of  food  employed  in ' 
public  estflbtishments,  I  analysed  several  samples  of  American  lard, 
and  therefore  may  add  to  the  fact  already  mentioned  by  Mr.  Georcc 
Whipple  in  your  last  nundwr,  that  1  found  them  to  contain,  in  addi- 
tion to  starch,  from  ten  to  twelve  per  cent,  of  water,  and  from  two  to 
three  per  cent,  of  alum,  and  about  one  per  cent,  of  quicklime. 

"A  few  months  ago  I  was  able  to  asceriain  that  the  operation  is 
conducted  in  the  following  manner :  — 


LARD,   AKD   ITS  ADULTERATIONS. 


303 


**  The  futty  matters,  such  att  they  arrive  from  Amerifn,  are  m<?lte<l 
wilb  a  little  water  in  ra!se-l>*)ttoined  copper  pans,  llirnufjii  wluL-h  cir- 
culates H  current  of  ntffam.  The  <lirt  and  olber  heterogeneous  matters 
fall  to  the  bottum  of  the  pan?,  and  the  clear  grease  is  uliowed  to  run 
into  a  wooden  vessel,  when  it  is  stirred  in  cnnfaot  with  roM  water;  it 
19  then  put  under  revolving  wheels  with  a  thick  paste  made  of  jjotato 
starch,  mixed  with  a  little  jxitHsh  ftlum  and  iiuieklime,  which  appears 
to  farilitate  the  taking  up  of  the  water  and  starch  by  tli<^  fully  matter. 

*'The  cause  of  the  American  lurd  appearinjf  so  white  Ih,  no  dnubt, 
the  division  of  the  fatty  matttT  through  the  interpositiou  of  the  starrh, 
water,  ami  alumina. 

"  The  cpiantity  of  alum  should  he  such  that  a  small  excess  should 
remain  U>  prevent  the  starch  from  becoming  mildewed;  and  I  believe 
ihiit  the  nmnufiietnrer  al«o  add:*  it  for  tlie  purpose  of  cornumnicating 
to  the  liird  the  property  of  taciliuting  the  raising  and  increasing  the 
irhiteness  nf  the  confectioners'  pnstc,  in  whicli  it  is  largely  employed." 

It  should  be  understood,  thiit  Americnn  lard,  ns  brought  to  this 
country,  is  not  In  general  adulterated.  The  aduUeratiun  usually 
takes  place  subsequent  to  its  arrival,  and  is  the  wurk  of  some  of  our 
own  manufacturers.  The  rrason  "tvhy  Amerit^an  lard  is  so  frefjuently 
selected  for  adulteration  is,  (hat  it  is  of  inlurlor  <jtiidity  and  value* 
and  so  soft  as  to  he  almost  fluid,  pome  prouess  of  consolidation  being 
indispensable  before  it  can  be  em]>]oyed  as  lard. 

From  information  received  fnmi  a  respectable  lard  render,  it  ap- 
pears tiiat  the  addition  of  a  small  tjuantity  of  muttnn  xiut  to  lard  is 
very  common.  It  is  used  more  particularly  in  wtirm  weather,  and 
with  sort  lanlfl,  especially  American  lard,  which  diflers  from  ordinary 
lard,  in  that  it  consists  of  the  entire  fat  of  the  pig  melted  down,  and 
rot,  as  is  the  esse  with  the  best  English  lard,  o(  the  fat  only  which 
surroundi  the  kidneys.  Mutton  suet,  being  a  hard  and  firm  fat,  im- 
parts to  5ot\  lards,  even  when  added  in  very  small  quantities,  the 
connistence  and  solidity  requisite. 

It  appears,  therefore,  that  water,  starch,  glum,  and  caustic  lime 
hove  all  bii*n  asi.ertaim'd  Ui  be  empIoye<l  in  the  adulteration  of  lard. 
To  these  substances  we  may  add  the  folUtwing  :  —  rnrlH)nate  of  sotla, 
curbcmatc  of  potash,  and  salt  The  whole  of  the  alwve  adulterations 
may  be  readily  discovered. 

Possibly  in  acme  cues  other  atumal  fnts  are  used,  as  that  of  veal. 


JiemUs  of  the  Examination  of  Samples. 

The  re«iulls  of  the  examination  of  upwards  of  100  samples  of  lard 

were  as  follows :  — 

lAt.  That  lani  i«  not  unfrequently  ejtiiusiceh/  atliilt&rafffi^  the  ingre- 
dients employed  being  water  and  f}o(afo  flonr^  as  well  iis  certain 
saline  subBtances,  oa  fo^,  potash  alum,  carloHotet  i>/  potash  and  of 


IMKP,   AND    1T8   ADULTERATIONS, 


goda,  and  eatutic  iim^t  lbe««  botnf(  intended  either  to 

lurd  to  Imid  water,  or  to  improve  \u  eniiki»t«nre  uid  ooUwr. 
'2nd.  Tlmt  the  deftcription  of  fard  nioit  liubU'  to  lululteraiioo  a 

larfL  nnd  of  lhi«,  pttrticiUurly  tl\ut  which  w  inanuiMctured  hi  ~ 

Irifb  kuj^  lard  bviii^  but  rurely  n'liilli'rntnl. 
5rd.  'L'hnt  of  upwants  of  our  htimlrfti  smuplfH  of  Innl  »ui 

examination,  nnd  pmcurcMt  chirtly   tVom  reluil  dfulero, 

found  to  be  aduhfi-Hk'tl  wttli  pi>fato  starch, 

T\w  tuhtherAt'um  f\f\m'i\  [Mevails  ni)t  only  in  certain  localities  Iwt  al«o 
chieft/  nt  certain  timrs — that  »s  wlienevur  *  sufficient  suppW  of  inferior 
liirJ,  Auitahlf  for  mixin);^  can  hi*  prr>curc(] ;  for  it  ii  said  not  to  auvcr 
to  mlulterat'?  u  lard  nf  ^ootl  qiiidity.  which  commands  a  high  prioe^  and 
which  if  A|)oilod  hv  l>cin;r  tampered  with. 

It  will  be  rcadifv  itcrecived  thai  the  (|ualities  of  a  lard  tbas  aduUe- 
rated  nin»t  In*  dcriiiiixly  irnpjiirvd  f<ir  altnoH  every  purpose  for  which 
it  is  emphivcil :  thiw,  of  roiirf*c,  it  would  not  be  nearly  so  econnmical 
for  cuhnniy  purpows.  In  tiic  presence  of  large  (pinntititrs  of  jtutaXv 
tlour  the  co*»k  will  find  h  !»iim»'ient  explanation  of  the  extraordi- 
niiry  tenacity  with  which  fi^^h  Hometimtfi  adheres  to  the  frying  pan. 
yVgain,  the  use  of  Huch  IflriJ  in  machinery  mij^ht,  in  R«>mc  case*. 
produce  serious  eonsetpiencos  by  imiHHiinj;  its  action.  r..astly,  tli* 
Activity  of  aH  the  ointments  of  the  Pharmacoptcia,  mwle  with 
:juch  n  Inni,  would  be  much  injured,  especially  the  simple  ami  com- 
|H>nnil  iodine  ointments,  which,  if  starch  were  present,  would,  to  the 
a^tl•nif4hment  of  the  dispenser,  turn  blue,  or  almost  black,  in  tlie  art 
of  incorporation. 


On  the  Detection  of  the  AHuUeratiom  of  Lard. 

The  first  thing  to  be  done  in  order  to  ascertain  wUellier  a  lard  be 
ffenuine  or  adulterated,  is  Ui  nu-lt  it  at  about  a  tempentture  of  212** 
Fulir.  If  it  dissolve  without  ebullilioii  or  without  the  Occurrence  of 
M  dtfmsit,  wc  may  »afely  conclude  that  the  8am])le  is  genuine;  but  if 
ebuUitiun  take  place,  or  a  t^diment  is  thrown  down,  the  lard  is  un- 
questionably odulterdted. 

Detertion  of  Water,  — The  adulteration  with  water,  and  the  c^uantity 
present,  may  be  thus  determined  :  —  A  known  weight  of  lard  is  to  Ire 
exix>sed  to  heat  until  bubbles  of  vapour  cease  to  eicape;  the  loot 
indicates  the  per*ccnu*;e  of  water. 

Defection  of  Siarch.  —  The  presence  of  starch  may  be  discovered 
by  thoroughly  incorporating  a  solution  of  iodine  with  a  few  grains  of 
the  lard,  placed  upon  a  slip  of  glass;  the  laril  will  change  colour,  and 
become  deep  blue,  or  almost  black.  If  now  a  little  of  this  be  vieweil 
under  the  microscope,  the  starch  corpuscles  will  themselves  be  oeen 
coloured  by  the  iodme. 

To  determine  the  kind  of  starch  conlatneil  in  any  sample,  we  must 
use  the  microscope.     A  minute  piece  of  the  lard  should  be  placed  on 


LARD,   AND   ITS   ADULTERATIONS. 


805 


slide,  previuu»<1y  tlioroufihly  warmerl ;  the  moment  the  Unl  is 
Red  it  must  be  viewed  by  the  object  glass,  when  the  utarch  cor- 
puscles will  be  distinguished  standing  out  m  clearly  as  though  they 
were  in  water. 

Another  way  in  which  thp  Blarcb  corpuRcles  may  be  well  seen  by 
the  microscope,  is  to  spread  out  by  gentle  pressure,  between  two 
pieces  of  glass*  a  very  thin  stratum  of  the  lard. 


%Jf^^ 


Laid,  idultf ntcd  vilh  Pvtato  Hareh.    Ifsfnlfleil  M>  dUmcUn. 


Although  it  is  ea5y  enough  to  detect  starch  in  lard,  It  is  by  no 
meins  so  to  estimate  the  amouiit  present. 

Ether  does  not  readily  dissolve  lard,  particularly  in  cold  weather, 
so  that  by  this  reagent  it  is  very  dinicuU  lo  separate  uU  the  lard  from 
the  other  ingredients  with  which  it  may  be  admixed.  If,  however, 
ether  be  used  for  the  purpose,  the  lard  should  be  melted,  and,  while 
still  warm,  the  etber  should  be  ponred  upon  it ;  we  may  then 
kVeigb,  when  properly  drie^l,  eitht-r  tne  nil  ohrainod,  or  the  sediment 
;ft*  Still,  with  every  precaution,  this  method  of  sepnrnlion  is  very 
troublesome,  and  often  fails. 

Another  method  h  as  follows :  —  Put  one  hundred  grains  of  the 
.Ikrd  in  a  test  tube ;  apply  a  gentle  heat  until  all  escape  of  vapour 


306 


OATMEAL,    AND  ITS  ADULTERATIONS. 


ceases.  Fill  nearly  up  with  water ;  heat  as  before ;  allow  the  wlwkich 
has  rison  to  the  tsurfuee  (o  become  cold ;  collect ;  beat  ognin  witb  » 
little  more  water,  wlieii  a  second  portion  of  oil  will  be  ublained;  »M 
the  twfj  portions  together,  dry,  nnd  weigh. 

Although  this  method  is  simple,  it  is  very  troublesome,  »nd  giro 
only  approximate  results,  since  it  is  almost  impossible  to  sepunle  iB 
the  oil  by  heat  alone. 

The  separation  of  the  oil  is  said  lo  be  readily  elTected  by  meau  ^ 
essence  of  lurpentine.* 

DeUrmimition  of  Saline  Matters. —  For  the  determination  ofU* 
saline  uiatttird  present,  it  is  in  must  cases  sullicicnt  to  niuU  ibc  UnL 
collect  the  precipitates,  free  them  from  oil  with  ether,  weigh,  »*l 
aflerwards  taste  them.  Salt^alum,  and  lime  may  all  be  distiii;;ui^bc!<l. 
provided  Quantities  uf  lard  suOiciently  large  be  operated  u^ma,  \>) 
the  ta.ite  alone. 

The  processes  for  the  detection  and  estimation  of  alum  are  giTeii 
at  p.  294.,  of  salt  under  Annatto,  and  of  lime  at  p.  101. 

It  is  not  often  that  more  thun  one  or  two  of  these  salts  occur  txfgd^ 
in  the  t^ame  lard  :  supposing  them,  however,  to  do  so,  we  may  procenl 
rrenerally  as  follows:  —  Incinerate '2000  c^ns  of  the  lard,  diuolreott 
the  salt  with  distilled  water,  precipitate  the  chlorine  by  meant  of  niinU 
of  silver,  and  eatimftte  the  sotia  from  this;  boil  the  insoluble  portloorf 
the  ash  with  dilute  hydrochloric  acid,  divide  into  two  portions,  preci' 
pitate  the  Hme  from  the  one  by  means  of  oxalate  of  ammonia,  and  tK« 
alumina  from  the  other  with  strong  ammonia,  according  to  the  prooe* 
given  under  the  head  of  Hread. 

Lard  h  free  uf  duty  ;  consequently  we  can  give  no  account  of  qtuw- 
(itiea  taken  tor  home  consumption:  but  the  imports  were  iu  iWi 
274,^92  cwU.,  in  1855,  118,109  cwts.;  in  nine  months  of  l&5ti.  116.1^ 
cwts. 


OATMEAL.  AND  ITS  ADin.TERATIONS. 

Oatmeal,  aA  its  name  implies,  consista  of  the  furina  or  meal  nf  r^r*^* 
The  compoMtion,  slnicLure,  and  properties  of  tliia  lereal  - 

be  found  described  to  «ome  extent,  and  figured,  at  pp.  24;i.  i-v.  ^ 

which  the  reader  is  referred. 
Amongst  the  best  analyses  which  have  yet  been  made  of  the  <nl  tf* 

those  by  Messrs.  Norton  and  Fromberg. 


rifrn.  "  Dei  SuImUdcm  AIUn«nUlra."  p.  HA.     Troiiitoic  MlOW 


OATMEAL,   AND   ITS  ADULTERATIONS. 


307 


Sureh 

Gutt 
Oil    - 

Protaine  compound! :  — 
Avvnln      •           -           - 
Albiim^ti 

i;im«n     - 
RpldimoU 
Alkftlloe  ull*  ttud  iMfc 

Uii^mmtOma. 

PtoUMOktt. 

NifiUimiDtolHiA. 

Ajnl^tn. 

Ajnhitt. 

M«tfawn(mUq«. 

S&M 

«il 

1-tO 
ft- 14 

IVTfi 
0  16 
S-47 

ns 

-i-M 

64-M 
SM 

5  41 
6«JT 

ICM 
l.W 
1  4S 
S39 
l»4 

8479 

s-ii 

fr4l 

17  71 

1-76 

■  u-M 

7  38 

»17 
i  4A 
»•!» 
176 

100  00  N. 

ICOWF. 

100  t»F. 

lOODOV. 

The  compcMiticm  of  (he  husk  of  the  oat,  ai^iording  to  Professor 
Norton,  is  as  follows ;  — 


O.I        - 

Sng-r  wd  jum 

OiuUi)  atid  co««uUtcd  ftlbu-l 

OlhiloM 

)Udop  matter  uid  uh 

llmprtm. 

rtaUM  Oh. 

I'M) 
047 

I'M 
647 

07ft 

IM 

«4« 

6W 

IVO'OO 

IDOiW 

The  an:ilyfe!i  of  M.  Payen  will  be  found  at  p.  257. 

It  appears  from  these  analjses  that  oainicikl  itt  a  highlr  nutritive 
anic^lf  of  diet,  richer  than  even  wheat  flour  in  oily  and  nitrogenous 
matters. 

There  are  peveral  varieties  or  quuliiies  of  oatmeal  :  one  of  these  is 
Kubinson's  Patent  Groats  ;  this  coii«ii!is  uf  the  Biiest  parts  of  the  tloui' 
of  the  oat,  all  liuak  and  the  outer  and  harder  partii  of  the  grain  being 
removed:  another  variety  is  called  "round  oatmeal;"  it  consists  of 
the  oats  depriveil  of  husk  and  (ground  Inuj  a  very  coarse  powder. 
This  description  varies  a  {jood  deal,  the  outer  surface  of  the  oats  in- 
tended fur  the  better  sorts  being  rubbed  oS'  by  attrition  between 
aumes. 

In  the  preparation  of  fine  uatnieal  there  is  a  f!ood  deal  of  refuse 
matter,  auiounliu;^  generally  to  aUmt  one  fourth  or  fifth  of  the 
i'litire  bulk  of  the  oats:  this  is  unu]po^e'l  of  a  portion  of  hu«k,  which 
contains  much  silex,  and  the  outer  part  of  tht;  grain  conUiining  a 
little  starch  and  much  oil  and  nitrogenous  matter ;  this  is   usually 

X  2 


306 


OATMEAL,   AND   ITS  ADULTERATIONS. 


uiixed  up  with  the  commoner  descriptions  of  oatmeal^  especially  Ibat 
supplic'l  to  workhouses. 

Liisily,  ihe  (]ua!ity  of  oatmeal  depends  very  greatlj  upon  the  quality 
of  the  oal  from  which  the  meal  is  prepared. 


On  tbk  ADULTEXATione  or  Oatmeal. 

It  coald  hardly  be  supposed  that  sufGoient  inducement  exists  for 
the  eopliifiticntion  of  un  article  like  uatmeul ;  it  ni)pear8,  however,  that 
this  9uppf>!*ili(in  is  not  correct. 

Of  thirty  siamples  of  oatn)eal  submitted  to  examination,  sixteen^  or 
rather  more  ihun  one  hidf,  were  Ji/uutl  to  be  aduUeraied  with  large 
quantities  of  Ba&let  Meal.  But  oatmeal  frequently  sufTers  dofrri- 
orutiuu  in  other  ways  besides  by  admixture  with  barley  tluur.  One 
nf  these  couf^ist^  in  lidding  tu  it  the  investing  niembrniit's,  r^r /iiuA,  of 
the  oai^  harhy,  and  uheaty  technically  termed  "  rubble  "  and  *'  sharps," 
and  which  are  rejected  in  the  prepariUion  of  the  purer  sorts  of  oat- 
meal, jrrits  and  proats,  Scotch  ami  pi'arl  barley. 

On  referring  some  time  since  to  the  market  prices  of  oat  and  barley 
meals,  we  found  thtU  white  the  first  wa.<!  I6it.  per  cwt.,  the  latter  was 
only  8«.  per  cwt.,  that !»»  just  one  half.  We  thus  perceive  that  the 
indut;emcnt  to  adulterate  (»atmeal  is  very  great,— greater,  indeed,  it 
appcarfi^  than  many  cornchnnillerB  can  resist. 

The  lonowin>:  inforiuallon,  furnished  us  by  a  correspondent,  whose 
niune,  for  obvious  rca^ion^,  we  withhold,  shows  that  this  article  u  eub- 
ject  to  systematic  adultcraiion.      lie  writes  :  — 

"  Since  your  able  analyses  have  taken  pinre,  it  has  struc-jE  me  that 
I  may  be  able  to  give  you  a  little  informntion  as  to  an  artit-le  of  (otni 
which  is  adulterated  to  a  most  awful  extent, —  viz.  oatmeuL  \  will 
first  mention  oatmeal  as  sent  hUo  icorfthotuea^  pri,^ona^  and  charitable 
institutions^  which  are  generally  taken  at  contract  jirices.     I  enclose 

one  for  the  parish  of (or  1848,  where  I  find  the  oatmeal  wus taken 

at  14«.  i>er  cwt.  by ;  and  by  reftfreine  to  my  stock-book,  I  find 

the  market  price  was  17 s.  Gd.  per  cwt. ;  thus  the  oatmenl  was  reduced 
3<.  Gd.,  and  then  left  an  excellent  protlt.  Well,  ot  that  time  I  was 
trying  for  all  the  contract*  in  London,  and  could  not  succeed,  my 
price*  being  generally  about  4*.  dearer  thiin  any  onc*8  else  :  this  was 
a  mystery  to  me.  By  accident  I  found  out  oatmeal  was  adulterated 
with  barley  flour  which  is  bought  at  about  7s.  per  cwt. ;  this  being 
mixeil  with  tlie  oatmeal,  of  course  reduce<l  the  price.  I  then,  being 
us  wise  as  my  competitors,  tried,  and  have  served  the  above  work- 
house since. 

"  Now,  the  fault  lies  here.  If  the  workhouses  were  to  take  the 
contracts  at  a  per-centnge  on  market  value^  then  thev  would  get^i><W 
oatmeal ;  but  they  always  nd  down  the  price,  ami  thus  get  an  adulte- 
rated article. 

"You  will  Bee  the  prices  are  14*.,  15*.  6</.,  16*..  and  17*. ;  tlius  if  n 
man  wants  to  be  honest  with  them,  they  will  not  let  him.    1  have  again 


OATMEAL,   AND    ITS    ADULTERATIONS, 


309 


ami  a;;ain  wished  to  supply  nt  a  per-ceiu«j?e  on  market  value  ;  the 
answer  1  get  is,  '  WcU^  we  are  eery  weU  mtUjied^  ami  have  uo  com- 
piaints.^ " 

We  kuve  ourselves  been  at  some  painti  to  verify  the  stAtemenls 
iiUMle  above,  and  for  that  purpose  have  proeure«l  samples  of  oatmeiU 
ftfl  supplietl  lo  some  of  our  unions  and  cnaritable  institution!! ;  these, 
witlioul  excepiion,  we  have  found  on  examination  to  be  largely  adul- 
terated with  biirletf  vieui,  as  deiioribed. 

Other  adulterations  of  oatmeal  are»  according  lo  ProfcMor  Calveit, 
with  rice  nnd  maize,  Ue  states,  in  his  evidence,  already  referred  tu 
in  the  nrtirle  liutter  :  —  '*  I  have  fountl  uatmeuJ,  ceneruUy  speaking, 
in  fact  alwnys,  mixetl  witti  rice  nnd  maize.  The  effect  is  this,  it  makes 
less  porridjfe ;  in  other  wurds,  it  is  a  direct  Inw  lo  the  ratepayers,  be- 
cause the  cook  in  the  workhouM  mnai  uHe  a  larger  proportion  of  this 
adultorateil  onrmeal  to  make  a  certain  i^uantity  uf  porridge,  than  if  it  is 
pure  outmcal " 

Tlie  followine  evidence  was  furnished  to  the  Committee  on  Adulter- 
ation, by  Mr.  Mackenrie,  id"  Glaagow,  the  editor  of  '*  The  Reformer's 
Gazetto-,"  in  regard  to  the  adulteration  uf  oatmeal :  — 

"  S"me  few  years  a;ji),  when  great  destitution  prevoiltid  in  the  West 
of  Scotland,  espeeially  in  the  Higblamls,  a  large  »iira  of  money, 
ftmountinj{  lo  50,000/.  or  60.000/.,  w»s  devoted  to  furnishing  provisions, 
including  oatmeid,  to  the  Highlanders.  At  that  period  information 
was  given  nic  that  u  very  lar^e  ({uantity  of  that  oatmeul  was  adul- 
terated  in  the  grossest  manner  :  u  letter  w&$  :«ent  to  me^  which  I  thought 
it  niy  iluty  to  publish,  and  ibe  contractor  who  furnii^hed  the  meal  re- 
ferred to  in  tliut  letter,  thrcati'uetl  me  with  tin  action  of  damages. 
The  ciiju  was  tried,  and  the  nmtJ'actor  found  jjuilty,  and  adjudged  tu 
imprisonment  for  three  inonth;i,  and  to  pay  a  tine  of  300/.  The  oat- 
meal was  mixed  with  britn  iin\J  thirds,  the  common  lood  lor  horses;" 
tliirds  being  the  refuse  and  shell  (if  the  wheat. 

"To  my  amazement,"  eontinuc*  Mr.  Mackenzie,  "the  accused 
brought  forward  some  of  the  principal  millers  in  Glasgow,  to  swear 
that  it  was  quite  a  common  practice  in  the  trade ■" 

The  adulteration  of  oamieal  is  not  merely  ini|>ortant  in  a  pecuniary, 
but  is  of  some  conse<{uence  in  a  sanitary  ]>oint  of  view. 

The  properties  of  oatmeai  are  thus  described  in  Pereira's  "  Muteriii 
]V(eflica  :**  —  *'  Oatmeal  is  an  im|K)rtant  and  valuable  article  ol  food. 
With  the  exception  of  maixe  or  Indian  com,  it  is  richer  in  oily  ur  fatty 
matter  than  any  of  the  other  cultivated  cereal  grains,  and  its  propor- 
tion of  protein  compounds  exceeds  that  of  the  nnesc  English  wheAteii 
flour.  So  that  both  with  respect  to  its  heat  and  fat  making,  and  its 
Uesh  and  bl(K>d  making  principles,  it  holds  a  high  rank." 

In  the  same  work  we  meet  with  the  following  account  of  barley 
meitl  as  an  article  of  diet:  — "Barley  is  a  valuable  nutritive.  Con- 
sidered in  relation  to  wheat,  it  oAlts  several  pecuttaritic«i.  In  the  first 
place  it  contains  much  less  protein  matter:  in  other  words,  less  of  the 

X  3 


k. 


ASB  ITS  ADtTLTERATIONS. 


-ixvU 


principle;  though  Count  Rumford  conrfcUred 
tlrt«  or  four  times  as  nutritious  as  wbvat  flour. 

if  lilii  iffnrr n'sistanne  tn  ihc  action  of  the  gastric 

>{U4»op  of*  irs  more  difiicult  Bolubility  in  water.     Tbinlly, 

i,  and  therefore  this  should  be  remoyed  from 

:i<:al  purpoies,  as  in  Scotch  and  [warl  barley. 

><h  meal  ii  more  laxative*  than  wheat  meoL" 

iW  twts  It  appears  that  oatmeal  possesses  considerable 

'tjtifw  over  barlev  meal. 

i:t  ihf  recollection  of  some  of  our  readers^  that  at  (he 
,i   KAi  ity  Mr.  Wiiklcy  on  the  boilies  of  Home  of  the  poor  chil- 
^tw  Wl  viotims  in   the  pest-house   at  Tooling,  the  fact  trans* 
Um4  kib»  uatuieal  which  formed  tvn  considerable  a  part  of  their 
WM  MlftkaiTvl^r  adulterated  with  barley  meal. 


Om  Hf  DHedion  of  the  Aduiteraiimu  of  Oatmeal, 

ft  v'l  ':d    adulterations  of  oatmeal,   us  already  uoticed,    are 

i    f^i^  vvfune  matter  of  oats,  barley,  and  even  wheat,  termed 

**tut'We  '  and  "sharps,"  and  with  barley  meal:  these  adultemtions 

IMV  ^  detiH'lod  withimt,  in  most  eases,  anv  oonsideruble  difficulty. 

^1^^  lUtn'tum  of^*RubbU" — An  admixture  nf  Rubble  may  be 

impHHd  when  llie  sample  presents  a  branny  ap|>earancc  In  conse* 

«f  V^iKV  vf  the  presence  ot"  numeroiiri  pjirtietes  of  husk  or  bran,  as  well 

M  wJ  l^ii*  outer  yellow  portion  of  the  ]t;rain.     In  order,  however,  lo 

VMiurv  w^rtamty,  it  is  necessary  to  resort  to  ehemislry  and  the  micro- 

wvfHK     A  portion  of  the  article  may  be  analysed  quantitatively   for 

uiil:  the  ash  of  almut  500  grains  must  be  boiled  with  dilute 

I'lirarid;   this  will  dissolve  all  but  thesilica,  which  must  be 

«  oiuM.  Ignited,  and  weighed. 

Aivortliiig  to  Messrs.  Ogston  and  Way,  the  ash  of  oat  cnntains 
fKuii  »N  4H  to  50-03  per  cent,  of  silica,  barley  from  •23*1)  to  70'77,  rye 
aUnit  J»  'Ji,  and  wheal  'iO  5  to  54*6  per  cent. 

Vbii  uieth'id  of  procoedinjr  is  rather  adapted  for  the  detection  of 
iy«  and  wheat  rubble  than  that  of  barley.  Of  course  the  per-centage 
\tl  sdicn  in  rubble  is  very  much  bisher  than  it  is  for  thi?  whule  grain. 

In  thi>>e  eases  in  which  the  nibble  of  bttrley  meal  \isun  bt^eu  u^eil,  the 
■Urch  granules  of  that  cereal  may  be  readily  d»*lected  by  means  of  the 
iaicrosGofw*  as  also  portions  of  the  investing  membranes,  the  structures 
of  which,  #n  different  from  those  of  oat,  are  described  and  figured  at 
pp,  «4,  245. 

In  like  manner,  the  microscope  furniithes  the  means  of  discovering 
tbv  presence  of  whettt  rvhhle  or  »harp»  in  oatmeal.  The  starch  gra- 
uulet  of  wheat  and  barley  !io  nearly  resemble  each  other,  that  when 
mucd  togeiher,  it  is  not  easy  to  diatin::ut»h  the  one  from  the  other: 
the  investing  membranes  of  the  grain  of  wlient,  d(*scribed  and  figured 
Ml  pp.241 — 243.,  are,  however,  so  diiferent  from  thoiC  of  barley,  that 
ibcy  afford  a  certain  means  of  discrimination. 


I 

I 
I 


OATMEAL,   AND  ITS  ADDLTERAT10N9. 


»II 


On  the  Detection  of  Barley  Meal. — The  microscnpe  affords  the  onlr 
means  by  which  this  adulteration  can  be  discovered.     The   starcb 

Plig.106, 


OathraL  adalunlcd  with  horUif  < 


UAfsMM  ttSilUawten. 


granules  of  oat  and  barley  have  already  been  described  and  figures 
of  them  given  ;  the  differences  are  so  great,  that  a  momentary  ^nncc 
with  the  microscope  is  all  that  is  necessarv  to  enable  the  o!»s*;rver  to 
dUtinKuifh  genuine  oatmeal  from  that  adulterated  with  barley  meal. 
The  staroh  grranules  of  the  oat  are  small,  anpular,  and  frequently 
aj^gregateil  into  compound  bodies  nf  a  rounded  form,  while  ttiose  of 
barley  are  much  larger,  rounti,  and  flat. 

On  the  Detection  of  Hice  ami  Maize. — These  adullerations  may  be 
promptly  discovered  by  means  of  the  microscope,  See^j^.  83.  p.  233., 
and^.  82.  p.  231. 

It  is  very  possible^  however,  to  mistake  the  starch  granules  of 
wheat  for  thone  of  barley  ;  but  wheat  tlour  is  rarely  used  in  the  adul- 
teration of  oatmeal :  this  error  may  be  avoided  by  a  curelul  examina- 
tion of  the  portions  of  test*  met  with,  the  structure  of  which  in  wheat, 
barley  and  oat  is  so  very  different,  as  will  appear  from  nn  examination 
of  the  descriptions  and  figures  given  under  the  article  Bread. 

Customs  duty  on  importation,  4^r/  per  cwt.    The  quantities  imported 

\  4 


3tS 


ARKOWROOT,  AND  ITS  ADULTERATIONS, 


and  taken  for  home  consumption,  were  as  follow  : —  1654,  4^6  cwts. ; 
l%55j  752  cwu.  1  niue  mouluB  of  IdJQ,  5,321  cwtH. 


ARROWROOT,  AND  ITS  ADULTER ATIONa 

Thb  term  *'  arrowroot "  was  origiDally  ap[>lied  to  ihc  rhizome  or  root 
of  Maranta  arvndhiacea^  in  coivsi-qupnce  of  its  suppotied  efficacy  in 
counteracting  the  eiTects  of  wounds  inflicted  by  poisoned  urniws. 

Of  Ute  years,  the  signitication  of  the  term  has  been  much  extended, 
and  it  is  now  employed  tu  designate  olnu»»t  every  fcculu  which  bears 
any  resemblaitce  to  true  or  Marantu  arrowroot,  no  matter  bow  dis- 
similar the  plants  may  be  from  which  it  is  obtainefl. 

Attending  this  enlarged  use  of  the  w«»rd  arrowroot  are  certain  di*- 
adrfintagcs.  Many  persons  consider  ihut  all  arrowroots  constitute 
one  and  the  same  article,  varying  ottly  in  quality,  and  according  to 
the  place  from  which  they  ore  procured ;  while  but  few  persons  are 
aware  that  there  are  several  distinct  kinds  of  arrowi-oot,  the  produce 
of  distinct  plants,  great  uncertainty  and  confusion  being  thus  created. 

To  increase  this  confusion,  tlie  word  "genuine"  is  often  prefixed  to 
the  term  "  arrowroot,"  and  a^  there  are  several  kinds  of  arrowroot, 
must  there  be  several  genuine  arrowroots  :  these  vary  in  value  from  s 
few  pence  to  two  or  three  shillings  the  pound — from,  in  fact^  ilic 
value  of  genuine  Maranta  arrowroot  to  that  of  genuine  potato  arrow- 
root.   With  these  paruculars  the  puUic  at  large  is  but  ill  acquainted. 

The  difficulty  and  confui«ion  is  still  further  enhanced  by  applying 
to  the  arrowroot,  as  is  generally  done,  the  name  of  the  place  Irom 
which  it  is  obtained:  thus  we  have  genuine  West  Indian,  Jamaica, 
Deroerara,  Bermuda,  St.  Vincent,  East  Indian,  Brazilian,  African, 
Guinea.  Sierra  Leone,  Portland,  British,  and  a  variety  of  other 
arrowroots.  Some  pci-soni  suppose  that  each  of  these  names  repre- 
aents  a  dificrent  kind  of  arrowroot ;  others  imagine  that  they  all  in- 
dicate one  and  the  same  production ;  while  the  fact  is,  that  in  some 
cases,  as  in  that  of  East  India  ani>wroot,  one  name  mny  be  indiscri- 
minately applied  to  two  distinct  kinds  of  arrowroot,  and  in  others,  six 
or  ei^ht  names  all  signify  but  a  single  kind  or  species,  as  is  the  CI 
with  West  India  arrowroot.  This  great  variety  of  names  is  objection- 
able, not  merely  becauiW  it  temls  to  confuse  the  public,  bntl>ecause  it 
oflTers  to  the  fraudulent  great  facilities  for  adullorauon  and  imposition, 
of  which,  us  wc  shall  sec  hereafter,  they  have  not  failed  to  avail  them- 
velres. 

The  remedy  for  this  state  of  things  is  t»imple :  each  reHlly  distinct 
arrowroot,  that  is,  every  arrowroot  which  is  the  product  of  a  distinct 


r 


LANE  LIQPw;;";/.  ST/L;FOaD  LiiiVERSlTY 

ARROWROOT,   AND  ITS  ADULTERATIONS. 


313 


W 


plant,  sbould  be  designated  by  the  oaine  of  the  species  from  which  it 
IS  derived,  as  Maruitu,  Curcumii,  Tocca,  Muuibot,  Anim,  Potato 
Arrtiwrool,  &c. 

The  empLo.vni<?nt  of  these  terms  should  not  be  optional,  but  com* 
puUirry^  for  the  better  protection  of  the  public  pf^ninst  fraurl  in  this 
article  of  fcxxl.  The  propriety  of  tbia  suggestion  will  become  still 
more  evident  as  we  proceed. 

We  shall  now  describe  each  kind  of  arrowroot  separately,  observine 
of  them  all,  that  when  pure  they  are  non-nilrogenised  subttLances,  and 
therefore  adapted  to  the  forioation  of  the  fat  uf  the  body,  and  to  the 
maintenance  of  respiration  and  temperature. 

BIakanta  Abkowboot. 

Maranta  arrowroot  is  obtained  front  the  rhizomes  of  Maraida  arun- 
dinaeett,  one  of  the  family  of  the  Murantacea. 

A  rhizome  is  an  underground  jointed  alcm  placed  horizontally  in 
the  earth,  giving  otf  from  its  upper  surfacCf  branches,  and  from  the 
lower,  roots;  the  starch  or  fecula  is  contained  in  the  joints  of  the 
rhizome,  being  deposited  iu  innumerable  minute  cells. 

The  following  account  of  its  prenarntion  is  given  by  Dr.  Pereira  in 
the  new  and  greatly  improved  edition  ol'  his  "  Mnleria  Medica  :"  — 

**  The  starch,  or  fccula,  is  extratted  from  (he  rcnits  (t«l»ers),  whon 
these  arc  about  ten  or  twelve  months  old.  The  process  is  entirely  a 
mechanical  one,  and  is  performed  vither  by  hand  or  by  miichinc. 

"In  Jamaica  it  is  procured  as  follows; — The  tubers  are  dug  up, 
well  wa^Jied  in  water,  and  tlien  beaten  iu  large,  deep,  wooden  morturs 
to  A  pulp.  Tliis  is  thrown  into  a  Inrge  tub  of  clean  water.  The 
whole  is  then  well  stirred,  and  thu  librous  riart  wrung  out  by  the 
hands  and  thrown  away.  The  milky  liijuor  being  pa<ued  through  a 
hair  Bieve,  or  coarse  cloth,  is  suftered  to  settle,  and  the  clear  water  is 
drained  off.  At  the  bottom  of  the  vessel  is  a  white  mas>s  which  is 
again  mixed  with  clean  water,  and  drained ;  lastly,  the  mass  is  dried 
on  sheets  in  the  sun,  and  is  pure  »tarch. 

"  In  Itermuda,  the  roots  are  first  deprived  of  ibeir  paper-like  scale*, 
and  then  rusped  liy  a  kind  of  wheel  rusp,  and  the  fecula  well  washed 
through  sieves  nnd  carefully  dried. 

"Upon  the  Hopewell  estate  in  the  island  St.  Vincent,  the  CArefutly 
skinnetl  tubers  are  washed,  then  ground  in  a  mill,  and  the  jtulp 
washed  iu  tinned  copper  cylindricuf  washing  machines.  The  fecula 
is  Hubsetfuently  dried  m  drying  houses.  In  order  to  obtain  thu  feuuU 
free  from  impurity,  pure  water  must  be  use<l,  and  great  care  anil  at- 
tention paid  in  every  step  of  the  process.  The  skimming  or  peeling 
of  the  tubers  must  be  performed  with  great  nicety,  as  the  cuticle  coii- 
>  tains  a  resinous  matter,  which  impartscolourand  a  disagreeable  flavour 
to  the  starch.  German  silver  palettes  arc  used  fur  skimming  4he 
deposited  fecula,  and  shovels  of  the  Mme  metal  for  packing  the  dried 


3M 


ARROWROOT,  AND   ITS  ADCLTERATIOSS, 


fccuU.  The  drying ia  efTected  in  pans  corered  by  white  gauxe  U)  ex- 
clude du£t  und  insecUt.'* 

Pure  fttid  unadulterated  Maranta  arrowroot  should  be  of  a  dall  nA 
opati^ue  white  colour,  crepitating  or  crackling;  when  presaed  b«tw«ct 
the  hngcrs,  and  treated  with  about  twice  its  weight  of  conceatnttti 
hydroirhloric  ackl  it  should  yield  iin  opaqne  paste. 

The  above  characters  and  ft[ip*»Rran(vs  may  all,  however,  be  $mawA 
by  curtain  of  the  other  arniwroob* ;  the  mioroiitcope,  therefore,  afonii 
the  only  read^  and  certain  means  of  distinpuishin*!;  this  arrowroot  fron 
all  other  epecies,  and  these  again  from  each  other. 

Ki-auiined  with  thai  inslruuient  the  jirranules  or  paitidci  «f 
Maranta  arrowroot  are  found  tu  be  usually  inorv  or  less  oblong  and 

Fiit,  vat. 


aurch  tnuiDktaf  MaB4*ta  •frovnM>t.c«ll«4eofniDonlf  Wc«t  Indlk  tmwMl- 
Drawn  with  Lh«  Cuners  Luddft.  ttad  tiiaOlA*^  94U  Oittmcim. 

ovate,  but  aometimcs  they  are  mussel-shaped  or  even  almoM  W»* 
angular:  they  vary  considerably  in  sixc,  but  each  of  the  Ur^ 
granules  is  marked  by  a  number  of  delicate  concentric  lines;  si  »* 
broad  or  lai^e  extremity  of  each  a  distinct  sjwt  is  visible,  orJin«r*'T 
coiiaidered  to  be  a  cavity,  and  denominated  the  "  bilum ; "  tlii*  spot » 
someiimes  circular,  but  most  frequently  it  is  seen  M  s  ^ort,  ifasrT 


AHHOWROOT,   AND    ITS    ADULTERATIONS. 


315 


line,  running  transversely  across  the  granule ;  it  fumisheit  a  most  dis- 
tinctive ff-'aiure  by  which  Maranta  arrowroot  may  be  at  all  times  very 
readily  iiJeiitified. 

When  bojhng  water  is  added  to  Maranta  or  any  other  arrowroot^ 
irs  physical  condition  undergoes  a  great  and  surpri^inf;  alteration,  the 
nature  of  which  may  be  clearly  traced  by  means  of  the  niicru&uope.  A 
t4ible^iioonl'ul  of  arrowroot,  on  wliit-h  a  pint  of  boiling  water  is  poured, 
inmieuiately  lo^es  its  whiteness  and  opacity,  becomes  transparent,  and 
the  entire  of  the  water  is  as  it  were  converted  into  a  thick  and  jelly« 
like  substance.  If  a  little  of  this  be  diffused  through  cold  water,  and 
examined  with  the  microscope,  it  will  be  seen  that  tae  starch  granules 
are  altered  amozinjrly :  they  have  increased  to  twenty  or  thirty 
times  their  original  volume  ;  they  are  more  or  less  rounded  ;  the  con- 
centric lines  and  the  liJlum  are  obliterated;  the  membrane  of  each 
gnuiule  is  ruptured,  and  a  granular  matter  has  escaped  from  its 
interior. 

The  appellations  which  have  been  bestowed  upon  Maranta  arrow- 
root ore  very  numerous;  their  use  ought  t^)  be  wholly  discontinued, 
for  the  reasons  already  assigned  :  thus  it  is  sometimes  called  West 
India  arrowroot,  Janiaicn,  Demcrarn,  Bermudii,  Bcrbice,  St.  Vincent 
arrowroot,  &c.  1'he  impropriety  of  denominating  it  West  India 
arrfiwriKit  if  bhown  by  the  circumstance,  tliat  the  Maranta  plant  is  cul- 
tivated in  the  East  aa  well  as  in  the  West  Indies. 


Cavva,  or  Tous  1X8  Mois  Akboweout. 

Camia  «da/u,  the  plant  from  the  tubers  of  which  the  starch  known 
M  I'^tuUt  Mois  is  obtained,  belongs  to  the  natural  order  Murantacete^ 
which  includes  Morauta  arunditmcea^  or  West  India  airowroot. 

The  starch  is  obtained  much  in  the  same  manner  ns  that  of  the  other 
arrowroor^ ;  that  U,  the  tubers  are  msped,  and  the  fecula  separated 
from  the  pulp  by  washing,  straining,  decantation  of  the  supernatant 
li<luor,  and  desiccation  of  the  deposited  Btarch.  It  i.<i  imported  from 
St.  Kilts. 

The  jelly  yielded  by  it  is  said  to  be  more  tenacious,  but  leas  clear 
and  translucent,  than  that  of  otlier  arrowroots. 

Owing  to  their  large  ttize  the  stircb  granules  exhibi:  a  glistening  or 
satiny  appearance;  they  differ  from  other  dietetic  starches  not  only 
in  their  much  greater  dimensions,  but  in  certain  other  particulars. 

The  granules  or  corpuscles  are  nearly  all  very  large,  flat,  broad, 
but  ovate;  sometimes,  like  those  of  East  India  arrowroot,  pointed 
at  tbe  narrow  end.  The  hiium  is  situated  in  the  narrow  extremity  of 
the  granule,  and  the  rings  are  exceeilinj;ly  Cue,  regular,  and  crowded. 

The  only  starch  with  which  they  are  at  all  likely  to  be  c«infoundcd 
is  that  of  the  potato  ;  tbe  granules  are,  however,  larger,  of  a  different 
shape,  being  flat,  and  the  striv  are  much  more  regular  and  numerous. 


ADCXTEKATIOgm 


CvscuMA  Akiowboot- 

UTOwroot  U  obtained  frum  tie  tubers  of  Curatma 
MM  of  the  fumily  of  the  Zimgtberaceit. 

luojtf  "f  it«  preparation  does  not  differ  nmterially  from  tbat 
MfcritrJ  i"  nlitainin^  the  fecMila  from  the  tubers  of  JJaranta  antti- 

^m^*^  Kml  which  hits  nlrcaily  been  described. 

>•  '    iiualitie:)    of  Curcuma    urrowrtKit    are    imported    into    tbis 

^  irtmi  tlte  £asI  Indies,  principally  from  Calcutta,  a  white  and 

.11  vtiriely. 

tvhitti  19  the  best;  the  powder,  when  pressed  between  the 

i4^<.'i*,  feots  \v3s  tirm,  and  dcies  not  crepitate  to  the  same  extent 

M  Marnnta  arrowrottt ;  the  two  species  can,  hovrcver,  be  distinguished 

mom  ^-Hi'h  oihcr  only  with  ceriainty  by  means  of  the  microacope. 

K\.4ituiuil    with  that  instrument,   the  granules  appear  elongated, 

»..  1    .1.    iiiv|j:iilnrly  ovate;  being  tlat,  iboy  present  but  iittlt*  lateral 

;  the  linoH  which  mark  the  surface  are  tolerably  disiinet,  but 

^    i>.'»orib«  segmeutA  of  circles  ouly,  and  the  bilum,  which  10 


ARROWROOT,   AND   ITS   ADULTERATIONS. 


317 


nsuallv  very  indistinct   ami   sometimes   invisible,    is   placed   at    the 
nuTow  extreuiitj  of  uacb  granule.     In  size  the  panicles  var^  codb1« 


Fig.  K 


Crunu  UTOWTOOl.  eommonlj-  ilenomlnmtod  TmA  lodU  ArrovrooL     Dnvn  with 
the  CuticfK  Loddi^UMl  irufiiifi«tl  1'40  diunvUn. 


derably.  but  many  uf  tfaem  much  exceed  the  loj^est  cootained  in 
MftraiMa  arruwroot. 

Curcuma  arrowroot,  therefore,  is  distinguished  from  Maranta 
arrnwrooi  bv  the  Mze  and  form  of  the  granules,  the  position  of  the 
hrtum.  find  the  inromplete  ringfi  seen  nn  the  surfatvs  of  the  granules. 
Curcuma  arrowroot  is  cnmmnnlv  called  Knst  India  arrowroot,  the 
same  name  being  sometimes  aiiphed  to  Maranta  arrowroot  cultivated 
in  the  East,  and  sent  to  this  country;  we  have  thus  two  dininct 
species  of  arrowroot,  of  difierent  cjualilies  and  value,  confounded  to- 
gether under  one  name. 

Tacca  Arrowhoot. 

T&cca  nrrowrool  is  obtained  from  the  tubers  of  Tacca  oceanica^  a 
native  of  the  South  Sea  Islands,  afYer  the  chief  of  which,  Tahiti  or 
OtufaeitCf  it  is  usually  deugnatcd. 


518 


ARROWHOOT,   AXD   ITS  ADULTERATIONS, 


According  to  Ellis*,  it  grows  on  the  high  sftndjr  biuilu  near  the 
9e«.  or  on  ttie  sides  of  the  lower  mountains. 

In  Foreira'*  "  Elements  of  Materia  Medica"  the  followinif  account 
U  given  of  the  preparation  of  the  fecula  :  —  "At  Tahiti  tbw  la  pro- 
cure<l  hj  washing  the  tubers,  scrapin;;  off  their  outer  skin,  and  then 
rtnlueing  ifaem  to  a  pulp  by  friction  on  a  kind  uf  rasp,  uiikde  by 
windins  conrue  twine  (formed  of  the  eoec^a  nut  fibre)  regularly  round 
aboanl.f  The  pulp  \»  washed  with  sea  water  ibrongb  a  sieve,  made  of 
the  tibrous  web  which  protects  the  young  finndofthe  cocoa  nut  palm. 
T^e  ctrained  li<pior  is  reueiveil  in  a  woo<1en  trough,  in  which  the 
fvoUU  is  deposited;  and  the  supernatant  Itfjuor  being  pour»:d  off, 
Iho  «cilintent  is  formed  into  bulls,  which  are  dried  in  the  sun  fur 
Iwelve  or  twenty-four  hours,  then  broken  and  reduced  bo  powder, 
which  is  spread  out  In  the  sun  to  dry." 

Fig.  no 


TaCO*  ATTOVrDOl,  cftlM  ammlljr  TklilU  nr  ou).«lte  ttiruwrocA-    Drawn  with  Um 
CuncTft  Lui:idit,  bikI  tn«(nl£cU  '£lo  Uianivtcra. 

Tln^A  arrowroot  is  u  while,  stHrcU-Iiku  powder,  having  a  alijchtlr 
luUaiy  odour.     The  granules  resemble  souiewhat  those  of  sago  meal, 

•  'i  KMearchM. 

.    iiixt  Lilt!  tlud  of  the  raol  li  Kraped  o^T  by  «  cowry  tbell,  and  Ihe  root  tfara 
•  .  I.  i.r  of  coral. 


ARROWROOT,   AST)   JTS   ADULTERATIONS. 


319 


but  are  Tery  much  sinKlIer  ;  when  viewed  sideira^ii,  tlicy  are  muller- 
sh«p«il,  with  truncate  or  dihednil  baws,  and  when  seen  endways  ihey 
appear  circular,  and  occa.«>iijnaUy  angular  or  polyhedrnl.  The  rings 
are  fev  and  indistinct,  and  the  hilum  circular,  someliuicB  tiasured  m 
a  stellatt*  manner. 

TaccA  arrowroot  has  been  sold  in  London  for  some  years,  in  pack- 
ages, an  "arrowroot  prepared  by  the  native  converts  of  ihe  missionary 
etations  in  the  South  Sea  lafands. '  It  is  sometimes  spoken  of*  as 
"WiUiams's  arrowroot,"  after  the  rnissionarr  of  that  name. 

The  sliglitly  musty  odour  whtcli  it  usually  posseases  shows  that  it 
is  not  in  general  prepared  wirh  quite  the  same  amount  of  care  as 
is  bestowed  on  Maranta  arrowroot. 


* 


Mamihot  Abbowroot. 

The  flotir  or  farina  of  Manihot  tUiiiasima,  the  plant  which  yields 
'*  tapiocii,"  is  sometimes  imported  into  this  country,  under  the  name 
of  "Brazilian  arrowroot." 

To  the  application  of  the  word  arrowroot  to  the  fecuU  of  this  plant 
there  exists  no  objection,  since  it  resembles  closely  the  other  arrow 
roots  in  its  propertiea. 

The  description  of  Manihot  utilutnima^  the  Cassava  or  tapioca  pinnt, 
andof  the  manner  in  which  the  fecula  is  first  obtained,  and  subscquentHy 
converted  into  the  substance  called  tapioca,  we  shall  reserve  until 
we  come  to  treat,  in  a  distinct  report,  upon  "  Tapioca  and  xis  Adul- 
terations." 

Manihot  arrowroot,  like  the  other  kinds  already  described,  may  be 
distinguished  by  the  size,  fonn,  and  other  characters  of  its  constituent 
granules,  which  resemhle  somewhat  closely  those  of  Tncoa  arrowroot, 
Dut  are  considerably  smaller,  with  a  larger  proportion  of  granules, 
which  exhibit  a  circular  outline,  us  seen  in  the  field  of  the  microscope  : 
the  hilum  is  usually  fissured. 

The  price  of  tapioca  to  the  public  varies  from  6(/.  to  lOrf.  the 
pound ;  now,  as  greater  time  and  labour  are  expeudetl  iu  the  manu- 
facture of  this  substance  than  is  required  for  the  preparation  of  the 
arrowroot,  the  price  of  the  latter  ought  to  be  still  less  than  this. 


Potato  Asbowboot. 

PotAto  flour,  or  arrowroot,  soiuetimcs  called  Brititk  or  EngU»h 
arrowroot,  is  prepared  by  ra.Hping  and  grinding  the  well  deiinsed 
tubers  of  Solanum  titherovtun  into  a  pulp.  This  is  repeatedly  wahhed, 
and  the  water  strained  through  a  sieve,  which  contains  the  cellular 
tissue,  and  allows  the  starch  to  pass  through.  After  a  time  the  starch 
is  deposited  at  the  bottom  of  the  vessel,  is  again  well  washe<l.  and 
finally  dried. 

Potato  starch  forms  a  white  and  somewhot  gliateniiig   powder. 


»20 


ARROWROOT,  AND  JT8  ADULTERATIOK8. 


which  cncklefl  like  genuine  Maruita  BTrowroot  when  pressed  between 
the  fingers. 

The  gr&nulea  v&rj  greatly  in  size  and  ahape :  some  are  very  naall 
and  circular,  oihers  large*  ovate,  or  oyster  shaped.    The  larger  granules 


Fig.  Ill 


PoTAtv  SirewTOOt,  comisooly  ttUtd  Dritiih  urowrooL    I>rmwD  witb  Utt  I 

exhibit  numerous  very  distinct  concentric  rings,  and  the  hilum, 
whicb  is  small,  but  well  defined,  is  situaled  in  the  narrow  extremity 
(tf  Oiich  granule :  not  unfreouently  graniiles  may  be  observed  of  an 
oval  form,  divided  by  a  fine  line  into  two  portions  or  8cj>mentfi,  each 
nf  which  is  provided  with  a  hilum.  We  have  noticed  the  same  com- 
pound granule  in  some  of  the  other  arrowroots,  particularly  the  Tacca 
bpecies. 

The  granulw  of  potato  arrowroot  difler  from  tliose  of  the  previously 
described  starches,  in  their  larger  size,  in  iheir  form,  and  in  the 
number  and  distinctness  of  the  concentric  rings  which  each  granule 
presents  to  view. 

No  means  e:tist  by  which  potato  arrowroot  may  he  diaiingulshed 
so  satisfactorily  as  by  the  microscope  ;  yet  it  is  proper  to  state,  it  has 
been  observe*!  that  this  itubstance  is  acted  upon  by  certain  reagents 
in  a  manner  different  from  Marania  arrowroot :  Mixed  with  twice  its 


ARKOWBOOT,   AND  ITS   ADULTERATIONS. 


331 


Mght  of  concentrflted  hvdpochlarJc  aci(l»  Maruita  arrowroot  yields 
an  opaque  paste ;  whereas  that  formed  witb  yiotato  arrowroot  is  trana- 
parent  and  jelly-like.  When  boiled  v'nh  water  and  Bulphurie  acid 
the  Utter  evolves  a  peculiar  and  somewhat  disagreeable  odour,  which 
i«  ont  the  case  with  the  former,  when  treated  tn  the  «aine  manner. 
Tjostlvi  alcohol  extract±>  from  potato  flour  an  acrid  oil,  not  contained 
in  the  fecula  of  Maranta  plant. 

Potiiro  arrowroot  is  the  cheapest  of  all  the  ttarclies  regarded  aa 
arrowroots,  the  retail  priee  varying  fVom  4ti.  to  6d.  per  pound.  AI- 
fhough  a  cheap  and  useful  article  of  diet,  it  is  of  course  inferior  to 
Maranta  arrowroot. 

Akdm  AmmowRooT. 
Arum  arrowroot  u  procured  from  the  tubers  of  Antm  manil/jhtm^ 
the  common  "cuckoo  pint/'  "wake  robing*"  and  *Mords  and  ladies:" 


X 
^ 


\ 


0 


'■''  %#^^^^ 


O^o 


it  is  prepared  chiefly  in  Portland  island ;  hence  it  is  generally  called 
'*  Portland  arrowroot." 

The  mode  of  its  preparation  is  rerj  similar  to  that  adopted  with 

T 


3SS 


ARROWROOT,   AND    ITS    ADULTERATIONS 


the  other  arrowroots;  the  tubers  are  pounded  in  a  mortar,  the  pulp 
{»eflte«lly  washed,  and  the  water  snbsequenlJy  strained.     As  f  he  tubers 
are  very  aer'ul,  great  oare  w  required  in  the  wasliinw  and  straining  of 
this  arrowroDt,  so  that  the  acridilj  may  be  coniplelclj'  rt*niovcd. 

The  starch  granules  of  Arum  arrowrcwt  arc  very  small,  and,  except 
in  sire,  ihey resemble  very  closely  those  ot'Tacca  arrowroot;  but  this 
difference  is  sutlicieiilly  coti?t(ani  and  considerable  to  ensure  the  ready 
identiBcation  of  the  two  kiDd.^. 

Strictly  speaking,  the  word  arrowroot  may  be  applied  to  every 
pureslari'h,  that  is,  every  article  consifitin;;  onlynf  stan-h  the  proiluce 
of  one  plant.  Now  pure  starch  may  be  obtained  from  nejirly  any 
p^rain  or  plants  containing  starch  in  considerable  amount,  aa  from 
wheats  rye,  pwise^  rice^  &c.;  hence  we  may  have  arrowroot  procuretl 
from  each  of  the  grains  named  as  well  as  a  variety  of  others. 

A  very  excellent  arrowroot  has  recently  been  made  fnmi  Indian  corn^ 
and  ia  sold  under  the  name  of  *'■  Oswego  Prepared  Cam" 

On  the  AouLTBBATioiKS  or  Abeowroot, 
A3  arrowroot  is  used  in  making  pudding*t,  cakciv  8nc»  its  adulter- 
ations may  be  considered  with  those  of  other  articles  of  the  dinner 
table. 

The  adulterations  to  which  arrowrijot  is  subject  consist,  first,  in  the 
mixing  together  of  arrowroots  of  different  kinds  and  of  different 
commercial  value;  and,  second,  in  the  admixture  with  genuine  atrow- 
rool  of  other  starches  not  usually  recnjjnised  as  arrowroot,  and  of 
low  price :  occasionally  starches  not  arrowroots  are  substiiuied  lor 
arrowroot. 

The  adulterations  of  arro^vrnot  arc  usually  practised  at  home.  From 
evidence  kindly  furnished  inc  by  Mr.  Day,  of  Old  Cavendish  Street, 
it  appears,  however,  that  nut  unfrenuently  it  is  mixed  with  inferior 
starches,  as  those  of  potato  and  sago,  in  the  West  Indies. 

Results  of  the  Exawituttion  of  Samples. 

Of  Fifty  samples  of  arrowroot  subjected  to  microscopical  exami- 
nation, no  less  than  twenty-two  were  adulterated. 

In  suteen  samples  the  adulteration  ctmsisted  in  the  addition  of  a 
single  article,  wueh  cheaper  in  price,  and  very  inferinr  in  quality,  to 
genuine  nrrowroot,  this,  in  t^n  instances,  being  potato  Jtour;  in  five, 
sago  meal;  and  in  one  case  tapioca  starch. 

In  five  samples  it  consisted  in  the  employment  of  two  different 
articles,  potato  flour  and  sago  meat. 

In  two  instances  three  different  star<;he5  were  employed  in  the  adul- 
teration —  viz.,  itotato  fioar,  mco  meal^  and  t/ipioca  xtarch  or  fectda. 

Ten  of  the  arrowroota  contained  acarcelif  a  ftftrtitle  of  genuine  A/ii- 
ranta  or  West  [tulian  arrowroot^  for  which  lliey  were  sold.  Osecun- 
sisted  almost  entirely  of  stigo  meal;  two  of  potato  flow  und  sogo  metd; 


SAGO,  AND   ITS  ADULTERATIONS. 


323 


hto  of  jtotato  Jimtr^  wgo  meal^  anil  tapioca  ntarch  ;  one  of  tapioca  starch  ; 
Mttd /uMT  weru  cumpofteU  uniirely  of  potato  armwroot  or  starcb.  ^ 

On  the  Detection  of  the  Adulterations  of  Arrottroot. 

Tbe  luIulteracionB  practiced  u[H>n  arruwroot  are  all  of  tbcm  readilj 
discoverable  by  meanii  of  the  microscope. 

The  structure  and  characters  of  potato  starch  hare  already  been 
described  and  figured  at  p.  S'20. ;  those  of  sa^o  are  so  at  p,  325^ 
and  of  tapiocu  at  p.  320.  Tbe  grauules  of  sago  starch  are  of 
considerable  size,  either  ovate  or  more  usually  somewhat  inutler- 
fihupi'd,  rounded  at  one  oxtrLunity,  the  other  being  truncated  or  etse 
teruiiiiatiiiK  in  a  diheilrul  suiuuiit ;  the  hilum  is  placed  in  the  larger 
and  rounded  [lart  of  the  uraniile,  is  usually  surrounded  by  a  distinct 
rinji.  and  is  oirculiir^  cracking  freqiienlly  in  jl  radiate  niauner. 

The  strong  inditL-einent  which  exists  to  substitute  j>otatn  starch  and 
sago  meal  for  the  hi'tier  descriptions  of  arrowroot  -will  bii  evident 
when  it  is  known  that  these  starchi's  may  be  purchased  wholesale  at 
eoDiething  like  '2d.  per  lb.,  while  as  much  as  'is.  6</.  and  even  St.  6it, 
is  chiirged  fur  the  articles  so  often  falsely  denominated  West  India 
arrowroot. 

It  ihuH  appears  that,  In  ihe  useful  article  arrowroot,  the  public  is 
extensively  uefniudcd  of  its  mnney,  and  the  revenue  of  its  income. 

The  duty  on  arrowroot  has  been  recently  replaced  ;  it  is  now  only 
4hd.  per  cwt.,  whether  from  a  fori^iirn  or  British  fMssession,  being  the 
same  duty  its  is  paid  on  all  kinds  of  liour  and  meal. 

The  quantity  of  this  article  imported  was,  in  1854,  14,905  cwts.;  in 
1(^5,  12.442  cwts.  Uetaiued  for  home  consumption  in  1854,  16,334 
cwts.;  and  in  1855,  13,0B»  cwts. 


SAGO,  AND  ITS  ADULTERATIONS. 

The  farinaceous  substance  sago  is  obtnineil  from  the  sterna  of 
several  palms:  that  which  reaches  this  countrv  is  mostly  derirtsd 
from  species  belonging  to  the  genera  Sagus  and  Saf^verwt. 

Of  the  genus  Sagus  there  are  two  species,  S.  Itrvit  and  S.  pemina. 

Sago  Isvis  inhabits  tbe  islands  of  the  Indian  Arcliipel3;;o,  Sumatra, 
and  Uorneo,  growing  spontaneously  in  low,  swampy  lands. 

Udxbureh  ("Flora  indica'*)  stales  that  from  the  pith  of  this  tree 
•'the  granulated  sago  we  meet  with  in  Kurope  U  niede." 

**  A  large  quantity  of  granular  sago  is  proparcd  from  this  species, 
in  Sumatra  espceifllfy,  the  peninsula  of  MuJueca,  and  in  Horneo.  It 
is  chieJly  cxportc«l  to  Kurope,  Bengal,  and  China.  The  iarina  whieh 
is  brougDt  from  Link  on  the  norihern  coast  of  Sumafers,  although  in- 


^ 


T    2 


334 


SAGO,  AND  ITS  ADULTERATIUN9. 


ferior  in  whiteness  to  that  of  Borneo,  is  mucb  sought  af^er  on  bccovbI 
^of  its  bein*;  less  friable.  It  commonly  fetches  twice  the  price  of  tb< 
latter."— Perfrra. 

It  df>"*s  nnt  appear  from  Pcreira  whether  any  of  the  sago  obuined 
from  S.  gfmina  reaches  this  country.  "This,  the  Malar  sago  naliB> 
ifl  the  tree,  the  pitli  of  which  is  the  staff  of  life  to  the  iDbibituu 
of  the  Moluccas." — Roxburgh. 

Sago  of  pood  quality  is  also  obtained  from  Sagverus  stuchanftf. 
an  inhabitant  of  the  same  localities  as  the  uC her  palms  ^l(;nllOt)^l■ 
Whether  it  is  ever  imported  into  this  country  we  know  nut. 

The  sago  of  commerce  is  brought  to  England  from  Singapore  in 
bft^. 

It  exists  in  the  forms  of  raw  Mgo  meal,  sa^o  floor,  and  granuUleJ 

BSffO. 

Raw  Mogo  meal  is  procured  in  the  Moluccas  as  follows:— Wb« 
sufficiently  mature  the  tree  ia  cut  down  near  the  root,  divided  into 
pieces  six  or  seven  feet  long,  each  of  which  is  split  down  the  midiDe: 
tiie  pith  is  then  extracted,  and,  with  an  instrument  of  baml>oo  orhirf 
wood,  is  reduced  to  powder  like  sawdust;  it  is  mixed  with  water,  >m 
the  mixture  strained  throu;rh  a  sieve  which  retains  the  o-llaltf 
tissue  of  tlie  pith.  The  straini'd  liquor  contains  the  farinn,  whicb,  aft* 
beinff  deposited,  is  washed  tmue  or  twice,  and  is  then  fit  for  uw*. 

Ornnulated  nago  is  prepared  by  mixinj;  the  meal  with  water,  lad 
so  converting  It  into  a  paste,  which  is  then  granulated  unualli  ^ 
passins  it  through  a  sieve.  In  most  cases  the  granules  as  tbejrw 
from  Uie  sieve  are  received  into  a  shallow  heated  iron  Tesael,  sotbsi 
(bey  are  partially  baked. 

Soffo  Jitmr  is  prepared  from  sago  meal  by  repeated  siAing  lad 
washing  ;  it  is  also  usually  bleached  hy  means  bv  chloride  of  lime- 

The  farina  or  starch  ofsftflrn,  examined  with  iLe  micrttscnpe,  i»ie» 
to  consist  of  cranules  of  considerable  size  and  clongateil  form, ben; 
usually  rounderl  at  one  end  which  is  the  larger,  and,  owing  to  tk 
mutual  pressure  of  the  particles,  truncate  at  the  other  exireniij- 
Sometimes  the  fucette  is  single,  when  the  granules  are  niorcurlrW 
muUer-shaped  ;  in  others  there  is  double  fucette  :  the  hilum,  whenpflf" 
feet,  is  uin^ular;  but  it  is  often  cracked,  when  it  appears  ae  a  slit,  ftfl*. 
or  star.  Surroun<ling  the  bilum,  a  few  indistinct  rings  may  ofuttf 
be  perceived  in  some  nf  the  granules.  Examined  with  the  |wJtf^ 
•cope,  the  particles  usually  exhibit  a  black  cross,  tk«  hilnm  bcutf  tk 
centre. 

Granulated  sago  is  met  with  in  two  statea,  comiDon  or  hro9%.  •*' 
pearl;  and  nf  each  of  these  kinds  there  ore  several  kinds,  di{r*nngialk( 
size  and  colour  of  the  grains.  In  all,  the  starch  granule^  differ  mack 
from  those  of  raw  sago  ;  they  are  much  larger  and  lew  reffular,  rf^ 
due  to  the  heat  employed  in  the  preparation  of  granulat«cai^ 


8AOO»   AKD   ITS  ADULTERATIONS. 


k 


■■CdUM  SB  4lani«t«n. 

withpoTAto  Starch.  Uaaolly  a  factitious  sago  prepared  froin  potato  sUrcb 
Id  substituted  for  true  sa^a 

Pereira  boa  the  following  remarks  in  relation  to  factitious  sago  :  — 
"  This  is  prei»ared  in  both  Germany  and  in  France,  at  Gentilly 
near  Paris,  with  potato  starch.     It  occurs  both  white  and  colnured. 

"  I  have  two  kinds  of  white  factitious  s*^n,  one  small  jsrained,  the 
grainH  of  which  are  scarcely  so  larfee  as  white  mustard  scods;  the 
other  Iurf!o  f^rainod,  the  (STflina  of  which  arc  intcrniediarc  in  sisc  be- 
tween white  mustard  seeds  and  coriander  seeds.  The  first  I  met  with  in 
English  commerce;  fortbeotherl  am  indebted  to  Professor  Guibourt. 

"  1  have  aliin  two  kind}<  of  coloured  factitious  sa^o,  both  larye 
grained;  one  re<l  *«  *he  other  brownish  f,  and  sumewhat  resembling 
browniith  pearl  sago." 

Pereira  also  states  that  he  received  from  Prof.  Guibourt  sample** 

*  *'  TVila  I*  prrhapi  tbc  kind  mvfitiuonl  by  rUmliv,  aj  being  UlilAed  lagu  colourmi  with 
coehln'>al." 

t  "  lliU  li  pt^xpfl  ib«  brow*  •ort  of  Gorman  aAgo  ntwl«  from  potato  •urcll,  ind  Mid  br 
DIarlMcli  to  b*  colourail  «ljb  Uant  Hiiar." 

'-— —  T  3 


896 


SAOOj    AND   ITS  ADULTERATIOXS. 


of  "  Sagou  lies  Maldives  de  PUnche  donn*'  jinr  \n\"  and  "Sagou  de 
la  Nouvelle  Guinee  dtiime  par  lui,"  and  tbut  he  found  ihem  to  Iw 


Fif.  111. 


Jlon*  gmmuUM  of  Baoo,  tltcr*J  br  h«mt.  m  In  mtking  {miii«bir«cf  ngo.    Mt^niflcd 
:c2fl  diuneun. 


factitious  sagos  prepared  from  potato  starch.     The  prains  of  the  New 
Guinea  sago  were  bright  red  on  one  side  and  whitish  on  the  oihcr. 

Of  thirtt/  eaniplos  of  pranulaied  sago  giibmiitcd  to  examination^ 
five  were  found  to  he  factitioWt  and  to  consist  o^  potato  flour. 

Oh  the  Detection  of  the  Adtd/firationjt  of  Sago. 

The  microscope  cun  alonp  detect  the  adulrcratinns  of  sago  flour  and 
^anulatt'd  sajro,  and  especially  distinguish  factitious  from  genuine 
Mgo.  The  charucTcrs  of  siigo  starch  have  already  been  described  and 
figured,  as  also  have  ihose  of  potato  at  p.  320. ;  in  ^anidated 
sago,  whether  true  or  fiifse,  the  granules  are  of  course  much  altered; 
those  of  potato  are  (>woneii,  irregular  in  shape,  sometinies  ruptured, 
and  the  striae  effaced,  &c. 

Import  duty,  4^*/.  per  cwt.  Quantities  imported:  1854,  128,789 
rwts.';  1S55,  92,800  cwts.  Home  consumption  :  1854,  121,046  cwts.; 
18.'5rj.  108,499  cwts. 


m 


TAPIOCA,   AND   ITS  ADULTERATIONS. 


327 


#W*Mm0  «at*i  eonipB«tJ  of  ^tPlaf ojImt.    MagnMcd  2S5  dl«inttfr*> 


TAPIOCA,  AND  ITS  ADULTERATIONS. 

TuR  article!!  known  u  Ctiss&TA  meal  and  bread,  Caaaavft,  Tapioca  or 
BriLzilun  arrowroot  and  Tapiocn,  are  obtained  from  difTorcnt  species  of 
the  penui  Manihot^  one  of  tne  Euphorhiacca,  One  of  tbese  is  -V.  aft'- 
lisjtima^  the  bitter  Cassava,  a  nHtivc  of  the  Brazils,  where,  us  well  as  in 
other  ports  of  South  America,  it  U  cultivated. 

The  starch  is  associated  in  the  large  tuberous  root  with  a  poisonous 
milky  juice  containing:  hjdrocjanic  acid  and  a  bitter  acrid  principle. 

Another  species  is  Maniftnt  Aipi^  or  aweet  Cassava,  the  juice  of  the 
root  of  which  is  not  poisonous. 

A  third  species  is  M.  Janipka^  the  root  of  which  ti  also  devoid  of 
poisonous  properties. 

Cassava  meal  is  prepared  as  well  from  the  bitter  or  poisonous  species 
as  the  sweet  and  innocuous:  the  root  is  grated,  and  the  pulpy  mass  sub- 

T    4 


TAPIOCA,  AND   ITS  ADULTERATION 9. 

jected  to  pressure  to  get  rid  of  the  juice :  the  residue;  dried  and 
pounded,  constitutes  Casasva  meal,  and  of  ihis  the  bread  is  made. 

The  expressed  juice  dcpoeiis  after  a  time  the  farina  or  starch,  froa 
which  tapioca  is  prepared. 

This  furina,  washed  and  dried,  constitutes  ^lanihot  or  Brazilian 
arrowroot. 

Exsmiiied  under  the  microscope,  the  granules  are  seen  to  be  of 
small  size,  for  the  most  part  single,  but  sumetitnes  and  in  the  plant 
itself  alwiys  united  inio  compound  grains,  each  compotied  of  cw<^ 
three,  or  luur  granules.  Hence,  tike  tfaoiK*  of  sago,  tbej  are  usuallf 
muller-sUnpetl,  althuugh  when  seen  endways  the/ appear  circular  ;  the 
bilum  is  distinct.  No  differences  have  been  obsenrea  in  the  character^ 
ufthe  starch  of  bitter  and  sweet  Cassava. 

Fig.  I1& 


\ 
6 


6^  e^ 


/ 


SUKta  ffftitulM  of  MAfnuoT  DTtuiMMA,  Of  Tttpltca.    MicmlStS  ttl  dtuneUfm. 

Manihot  arrowroot  is  usually  importefl  into  ibis  country  from  Rio 
Janeiro. 

In  the  manufacture  of  tapioca,  the  meul  while  moist  is  heated,  and 
then  dried  on  hot  plates:  this  treatment  of  course  cauies  the  starcib 
granules  to  swoll,  and  many  of  them  (u  burst ;  they  at  the  same  time 
adhere  together  io  small  irrc";ular  masses. 


TAPIOCA    AXD    ITS    ADULTERATIONS. 


329 


Oir  THE   AoULTERATlOnS   OF  TaPIOCA. 

Manihot  arrowroot  or  starcb  is  occasionally  adulterated  by  admix- 
ture with  other  st&rcbes,  as  those  of  »ogo  aad  potato. 

Fig.  117. 


Stanh  itmBalw  of  T^pfacot  altcrvd  by  the  h»t  vmpliiyed  fn  lu prep«r«Uim.  ti%m' 
MllidXXS  OtuiHCen. 

Of  TtteniU'three  samples  of  tapioca  examined,  two  were  ascertained 
to  conat:!ft  oiAogo^  and  one  of  potato  starch, 

Manihnc  stiin-h  is  more  frequently  used  as  an  adulterant,  especially 
of  Marantu  urrowroot,  than  i»  ilaelf  adulLvrated. 

On  the  Detection  of  the  AduUeraiiom  of  Tapioca. 

The  only  means  of  detecting  the  adulterations  of  Manihot  arrow- 
moL,  and  of  tapioi'a,  is  furniBhed  by  the  microscope :  with  thnt  instru- 
ment their  detection  is  rendered  easy  and  certain.  The  characters  of 
»af;o  ntarch  are  described  and  figured  at  p.  325.,  and  those  of  potato 
Mtarch  at  p.  320. 

Import  duty,  sume  as  Su^o,  Arrowroot,  and  Flour,  i^d,  per  cwt. 

Quantities  imported;  IH54,  3,501  cwts. ;  1855,  4,473  cwu.  Home 
consumpliun:  1854,  4,444  cwts.;  1855,  4,305  cwta. 


330        PROPRIETARY   ALIMEN'TAUY    PREPARATIONS. 


PROPRIETARY  ALIMENTARY  PREPARATIONS. 

TiiK  ftrtjples  rofL-rred  to  under  the  above  head  being  proprietary, 
and  there:  being  no  recDjtfiiiseti  receipts  or  formularies  for  their  com- 
poaitiun,  they  *io  not  pr*jperly  ijouxe  under  the  be«l  of  nrticles  of 
cnnicuinpliuii  liable  to  adulteraMon.  Neverllielesa,  the  public  will  doubt- 
less be  glad  to  be  made  acquainted  with  the  composition  of  the  cbJef 
of  the^e  articles,  especially  tbose  which  are  described  as  being  possessed 
of  almost  miroculou!!  powers  of  curing  disease,  and  wbi<'h  are  sold 
under  certain  hi;!h  sounding  name<t,  und  at  exorbitant  prices.  I<nttl 
the  microscope  was  applied  by  ourselves  to  the  discrimination  of  dif- 
ferent vej:claljle  subst^uices,  it  wa«  not  possible  to  have  determined,  by 
any  known  nieuii8,  the  euuiposiuun  of  many  of  tbe  preparations  about 
to  b«  noticed. 

The  principal  of  these  preparations  are  the  following  :— 

Wharton  $  Ertalenta.    Sold  at  2*.  9d.  per  lb. 

A  anmple  of  this  article,  examined,  conHisted  of  a  mixture  of  Uie 
French  or  German  ieniilt  with  a  substance  resembling  nuzti«,  or  Imlian 
com  mfai. 

It  has  been  stated  thai  the  farina  of  a  grass  eal  led  "  T)ari,"  "  Durra,** 
&c,,  has  been  discovered  in  either  Enralenta  or  Kcvnlenta. 

We  have  succeeded  in  procuring  a  sample  of  this  article,  and  find 
it  to  resemble  very  closely  maize  in  struelure. 

"Oari"  is  occasionally  imported  into  \hh  country,  and  sold  at  about 
twenty-four  shillings  per  quarter,  that  is,  at  the  rate  of  rather  moi*e 
than  one  halfpenny  per  p<mnd. 

We  received  from  Ur.  Pereira  some  time  previous  to  his  deceftMi 
the  following  infurmation  respecting  **  Durra." 

**  i>ari,  1  suspect  means  Dnrra^  also  sjiell  Doura^  Dorn,  &c.  It  is 
a  corn  used  by  the  Arabs,  and  is  cultivated  in  the  south  of  Europe.  It 
is  the  llolcua  durra  xativtu  of  Forskiil,  the  Surghum  vulgare  of  some 
oilier  writers, 

**  Its  meal  is  said  to  resemble  that  of  Indian  corn.  Now  it  deserves 
notice,  that  a  German  microscopist  recently  stiite<i  that  he  found  the 
meal  of  Indian  coi-n  in  ervalmtOy  or  revaienta,  I  forget  which.  Did  be 
mistake  it  for  the  Sorghum  ? '" 

For  description  and  figure  of  Durra,  see  pp.  289 — 292. 

Du  Barry  M  RevaierUa.     Sold  at  the  same  rate  as  the  Ervalenta. 

Three  »uniples  of  this  article  were  examiiieil :  one  consisted  of  a  mix* 
ture  of  tbe  r^rf  or  Arabian  \enu\  ami  barley  Jiour ;  the  i^econd,  of  the 
same  ingredients  mixed  with  tvgnr;  and  tbe  third  sample  consiBt«d  of 
the  Arabian  Imtil  and  barley  flour,  with  the  addition  of  .saline  matter, 
chiefly  taii;  it  also  possessed  a  peculiar  taste,  as  though  flavoured  with 
ceUryteed, 


PROPKIETART   ALIMENTAEY    PREPARATIONS. 


.i:u 


Butler  8c  M'CuUoch't  Prtoared  Lentil  Powder^  \s.  Gd.  per  lb.,  was 
found  to  coiiBist  entirely  of  tn«  French  or  German  lentil. 

Edtcardg  lirothers  Arabian  Hepaienta,  In.  per  Ih.,  was  ascertained 
to  consist  of  lentil  fioicder,  probably  of  the  yellow  and  retl  lentil  mixed. 

NevUfti  Patent  Flour  of  LetUilti^  1*.  |H»r  lb. 

Two  samples  of  tliis  article  were  examined :  one  comtsted  of  the 
red  lentil  and  wheal  Jlour^  and  the  other  uf  tbe  same  species  of  lentil 
and  hurley  Jionr, 

Lentils  belong  to  the  natural  family  of  plants,  Leguminoxa^  which 
includes  the  several  kinds  of  beans  ami  peas  ;  they  resembU*,  to  a  very 
great  extent,  in  colour^  structure,  taste,  and  properties,  iho  coTnmon 
pea;  so  great,  indeed,  is  the  aiuiitarity  in  organisation,  that  it  is  diffi- 
cult to  discriminate  between  them,  even  by  the  aid  qf  the  niicri)5CO|)e. 

Lentils,  peas,  beans,  &c.t  oil  contain  a  considerable  umuuni  of  nitro- 
genised  matter,  iu  tbe  form  ^t  Legutnine ;  when  taken  as  an  article  of 
tiiet*  they  are  found  by  most  (o  be  sometvfaat  dilficult  of  digestion,  to 
occasion  distension  and  Batulency,  and  to  be  slightly  aperient.  These 
properties  and  effects  are  so  similar  in  the  ca.<<e  of  each,  tliat  it  is  almost 
impossible  to  draw  any  decided  line  of  demarcation  between  them. 

"  Purified  leniils  *'  are  prepared  under  a  patent,  by  Mr.  Nevill,  who 
formerly  supplied  Du  Barry  and  Co.  with  the  article,  at  10/.  per  ton  ; 
that  is,  Rt  about  one  penny  and  a  fraction  per  pound. 

Tbe  admixture  of  barley  and  other  iluurs  with  lentil  powder  is 
not  to  be  reganled  in  the  light  of  nn  adulteration,  since  the  cost  of 
barley  flour  exceeds  that  of  tbe  lentil,  being  about  13/.  per  ton. 

The  object  of  this  mixture  is  chiefly  to  diminish  the  strong  flavour 
of  the  lentils,  and  which  is  so  disagreeable  to  many.  Messrs.  Du 
Barry  and  Co.  still  more  ciTcctually  accomplished  this  object,  in  some 
cases,  by  the  addition  of  f^ugar. 

Kxtreines  meet :  lentils,  being  somewhat  cheaper  than  peas,  are 
supplied  to  many  of  our  workhouses,  to  be  used  in  the  preparation  of 
soup,  &c.  Thus  they  are  not  only  consumed  by  puupers,  but  by  the 
T\vh^  tiie  chief  difference  being,  that  the  latter  fretjuenlly  pay  'I*.  9c/. 
per  pound  for  them. 

As  the  cost  of  most  of  the  prepared  lentil  powders,  sold  as  Erva- 
lenta,  Revulenla,  &c. —  viz.,  2«.  9f/  per  pound  —  forms  a  very  serious 
ofast»cle  to  iheir  use,  suppotiing  that  in  any  renpcct  it  is  desirable  that 
they  should  be  more  generally  consumed,  we  have  framed  the  two  fol- 
lowing receipts,  whereby  a  considerable  saving  of  expense  ma/  be 
effected :  — 


\U  Receipt* 

Ked  or  Arabian  lentil  flour        -  -  -2  lbs. 

Barley  flour       -  •  -  -  -      I  lb. 

Salt       -  -  -  -  •  •     3  ox. 

Mix  Into  a  uniform  powder. 


PROPRIETARY  ALIMENTARY   PREPARATIONS. 

The  red  lentit  may  be  obtained  of  almost  every  corn  chandler,  at 
al)out  -UI.  per  quart  ;  the  cost  of  u  pound  of  our  Ervolenta  would  be 
about  *2d.  per  pound ;  and  it  is  perfectly  clear,  from  the  analyses 
which  we  have  given  above,  that  whatever  may  be  the  advantani 
posseaseil  by  the  rauch-vaunted  Ervalentaa,  Revalentas,  &c^  inat 
our  article  must  contain  them  all. 


Pea  flour 
Indian  com  flour 

Salt    - 


2nd  Receipt. 


Blix  u  before. 


Slbfl. 
lib. 

3  02. 


T*hc  characters  of  lentil  flour,  and  the  composition  of  Ervalenta, 
Kcralenta,  and  of  Lcatb's  Alitneutury  Farina  are  exhibited  in  tku 
following  cngravingfl. 

A!i.  Hi. 


ftamplt  Bf  WRAxrair'*  E>ru.Rjrr\.  u  It  •ppc«n  under  th«  mlcnwMpt. 
,  MBrch  corpUM-Iri   at  thf  Fhrhi  ii    l  Bntii.  :  /■  /i,   fntfrnK*'*   (*^  lt»t  'hnsk  i  r  r. 
MMcb  grutuJm  ftnil  mmmtt  of  tbt  cwImIuioc  nvembUnit  Inoiax  uuhji  asAL. 


PROPRIETARY  ALIMENTARY  PREPARATIONS. 


333 


Being  5atis6(;(l  that  lentils  and  |»oas  do  not  diSer  in  flieir  pro- 
perties to  any  great  extent,  we  hure  devised  the  ubove  receipt  to 

Pit.  119. 


Sample  of  Do  IUit7'*  Rvt(LI5T1  AaABicA. 

It  a.ftwdb  (rvnoW  flf  the  AxAAuy  i.C-<<Ttu  •omc  loow.  ottwn  lylnf  lothc  oelliaf 

tfi*  ctUulow  4  t  h  mtmnb  franaUt  of  BAIUJtT  rt-OOB. 

meet  those  coneii  in  which  any  difficulty  may  be  met  with  in  pro- 
curing the  red  lentil,  which  however  is  now  very  commonly  kept  by 
I'orn  cbandlera. 

From  the  several  preparations  of  lentil  flour  noticed,  we  will  pass 
tJ)  describe  certain  other 


Farinacboub  Foods. 

Gardiner  g  Alimentary  Preparation  consisted  of  Tery  finely  ground 
rice, 

LeaiKa  Alimetdary  Farinn,  or  Homceopalhie  Faririaceons  Foody  con- 
Histed  principally  of  \cheut  /four,  glip:htly  btdced.  sweetened  with 
^vgar^  together  with  potato  ntarcK  Indian  com  meal^  and  tnpiiKa. 

Semnliva  consists  in  some  cases  of  the  gluten  of  wheat  mixed  with 
a  proportion  of  wheat  flour;  in  others,  of  certain  descriptions  of 
wheat  flour  only,  rich  in  gluten. 


^ 


Fmd  ra 


CBtuvlj  of  hidttd 


Prmea  Arlkm^i  Pa 

The  Phmce  of  WUe^t  Food  was  cmin>o>cd  entirety  of  point<> 
Jfoatr. 

UnrtU  Porimtcetma  Flmr,  of  trMeatJIotter,  kmkid. 

Mn*timan$  \mtritiauM  Parma  oockftMed  entirelj  of  foialo  /low 
arti6ciallj  ooloored  of*  pink  or  rosj  tint,  the  colooriikg  matter  being 
pr«>T»»Wr  ro»e  puJL 

Bntm*t  Pftrinaeeoms  Pood  oaoaitHed  oC  vheat  JUmr,  baked^ 

Badert  Sttnjie  wi«  conposed  of   irAeo/  Jiuttr,    sweetened    witIi 

Hiut^»  f'itmpuHiuUd  Farina  poMCMed  a  timUar  composition, 
Jonfi%    PaU-rU  Flttur,  coniist«d  of  vheai  Jia^w^  tartaric  acid,  and 
carUnuite  of  toda. 


ANCHOVIES,   TIlEin   SUBSTITUTIONS,   ETC.  335 

Plumhe'4  Improved  Farinaceous  Food  wns  composed  of  tetitt  ctr  pett 
Jionr^  with  u  little  Tatxa  arrourroot^  some  potato  jUftfr^  and  a  very  Iilllo 
Maranta  arrowroot. 

Lastly,  Palmer's  X'itarobt)ra»t  cnnsistcd  of  a  mixture,  sweetened 
with  sugnr.  of  the  red  or  Arabian  Until  and  wheat  fiour. 

The  |>ubtic  is  now  in  a  position  to  jud^u  of  the  degree  of  relation 
whicli  exiiitA  between  tlie  hi^U-Koundin;;  titles  bestowed  on  many  of 
the  preparations  noticed  in  this  Report,  their  actual  conipositiun,  and 
the  properties,  so  loudly  vuuuted,  alleged  to  be  j»os*ess.e<l  bv  tliem  ; 
it  will  also  be  ablu  to  Ju<l^e  somewhat  of  the  extent  tu  which  tlie 
po(k^i  i>j  made  to  ftuffer  ihrou<rh  these  health  restoring,  life  pro; 
longing,  easily  digestible  arlidea  and  compounds. 

On  THE  Detection  or  the  CouposiTioif  of  Propbietart 

AUMKKTABT    PmKPARATIONB. 

In  the  majority  of  cajea  the  only  means  by  which  the  enrnposilirm 
of  these  articles  is  lo  be  determined  is  afforded  by  the  microscope. 
Br  tliis  instrument  the  starches  of  the  Aeveral  llourn  and  arrowroots 
of  which  they  are  i'()iii|>osed  can  all  be  idtMitificd.  The  characters  of 
nearly  all  these  have  already  been  described  and  figured. 


ANCHOVIES,  THEIR  SUBSTITUTIONS  AND 
ADULTKKATIONS. 

The  next  articles  of  the  Breakfast  Table  to  the  adulterations  of 
which  we  deaire  to  direct  attention  are  Anchovies,  and  Potted  Meats 
and  Fish. 

We  fin<l  but  little,  in  works  on  the  adulteration  of  food,  in  reference 
to  the  substitution  of  inferior  kinda  of  fish  for  this  much  esteemed 
variety  ;  although,  if  common  report  is  to  be  creditetl,  but  few  articles 
of  consumption  are  more  subject  to  substitution  and  adulteration  than 
the  anchovy,  whether  in  the  entire  state  or  in  the  forms  of  paate  and 
sauce. 

On  the  present  occasion  we  have  to  treat  of  the  entire  fish  only. 

Before  proceeding  to  give  the  re6ulu»  of  the  examination  and 
analyses  of  various  snniples  of  anchovies,  as  vended  in  the  melropolis, 
we  insert  an  original  6gure,  as  also  a  scieniido  description,  of  the  fish, 
taken  from  Tarrell's  excellent  work  on  the  British  Fitih^s, 

"  Generic  Characters^  — Distin^uiMhe^l  from  tlie  herring  in  havinir 
the    heud  pointed:  the  upper  juw   tlie  longest;   the    mouth    deeply 


divided  ;  tbc  opening 

ing  bAckwards  befaizul  the 
of  the  eyes;  the  gspe 
chial  ttpeituree    wm 
the  Tenrral    fine  in  ad 
of  the  line  of  the  con 
went  of  the  dor&&l ;  t_ 
smooth ;  branchiost^oiu 
twelve. 

"  I     have     follovvd   « 

Henung,  in  preserviocloty 

anchovy    the     old    uim  h 

which  It  waa  foriDeriT  katmi 

It    waq     cnlle.1    l^jfcoitamk 

^    from  the  fom»  of  tt^  Dyafts 

J    and    £nfrraulijt    mcmtialm 

I    pecAuse,  from    it.s  bittenta^ 

5    It  was  supposed   to  carrr  tt 

i  gall   in   irs    bead.     For'tU 

I    reaaoDf  the  bead,  aa  weO  tf 

{    ibe    entrnila,     are 

[  when  the  fish  is  pid 

■        "  Theiinchovy  is  a 

I  fish  in  the  MediterraneaB; 
,  from  Greece  to  Gibrahir, 
i  and  was  well  known  to  tk 
Orpfksfind  Komam,bYwfci« 
theli,,uor  prepared  fTom  il. 
called  ffarum,  was  in  gnA 
estimation.  Itseaetern  rmw* 
H  extended  into  the  BUek 
Sea, 

"The  fishing  fop  them  n 
carried  on  during  the  nigkl. 
and  lighta  are  iwed  wicii  tk 
neta. 

"  The  flnebovy  is  cotUBOl 
on  the  coasts  of  PortngJ. 
Spam,  and  France  ;  it  oixvn, 
I  have  no  doubt,  at  the  Ckn- 
nel  Islands,  ajid  h^  bed 
taken  on  the  Hampihire 
coas t,  and  in  theBrW 
^^^!!SF}  J.°  t^e  AppetMti 
to  Willuehby'8  wort,  it  a 
mentioned  as  havini;  b<«a 
taken  on  the  const.  ofM^alw; 
Pennant  obtained  it  nearbii 
own  residence,  at  DowniM 
in  Flintshire;  and  Mr.  Bidh 
eno  ha*  very  recenUy  obtaiocd 
several  on  the  coa,t  of  GU- 


ANCHOVIES,    AND   THEIR   ADULTERATIONS.  337 

morganshire.  It  is  8niJ  to  be  «oIil  fre<|iicntly  in  Liveri>o()l  market,  (ind 
is  reporti'il  lo  be  nt  this  iini«  nii  iiibiibitant  of  the  piece  of  water  below 
blacKWAll,  called  UngenhiLll  Reach. 

"  ll8  range  to  the  north  is  extenwye,  as  it  is  occasionally  taken  in 
the  Bultit^,  iind  on  the  coast  of  Norway;  but  ie  not  included  by 
Linnieus  in  his  Faums  Sutt^ica. 

"The  nnrhovy  appears  toattain  a  much  larger  size  than  has  usually 
been  nec-onleil  to  il :  fri)m  ftmr  to  five  inches  in  length  is  the  more  or- 
dinary size ;  but  Mr.  Couch  says,  *  1  hitvt;  seen  it  in  the  Oornifrh  seoa 
of  the  length  of  seven  incites  and  n  half;  and  I  have  met  with  speci- 
mens from  autumn,  through  tlie  winler,  to  the  middle  of  Maruh.  It 
is  therefore  probable  tl»at  a  fishery  nti^ht  be  established  with  good 
prospect  of  sucft'ss,  for  though  the  nets  cmployeil  fur  other  fish  can 
take  but  few  uf  them,  the  numbers  found  in  the  stomaclis  of  the 
whiting?,  and  other  ravenous  fisbcis  show  that  they  arc  iu  considerable 
abundance. 

"The  anchovy  is  immediately  reeogniscd  amnn^  the  species  of  the 
family  to  which  it  belongs  by  its  sh»rp*|iointed  hi-ad,  with  llie  upper 
jaw  coniiidLrably  the  lonsest.  The  length  of  the  head,  compared  with 
the  lenuih  of  the  body  alone,  is  as  one  to  three ;  the  depth  of  the  body 
but  two  thirds  of  the  length  of  the  head,  and  compared  lo  the  leh;:th 
of  the  whole  liiih,  is  as  one  to  seven ;  the  firstt  ray  of  the  dorsal  6n 
arises  half  way  between  the  poitilof  the  nose  and  the  end  of  the  tleshy 
portion  of  the  tail ;  the  third  ray  of  the  dorsal  fiu,  which  is  the  Ion<;est, 
IS  of  the  same  lenjith  as  the  ba^ne  of  the  fin  ;  the  [tectornl  fin  aniall ; 
the  ventral  fins  arise  in  a  vertical  line  in  advance  of  the  commencement 
of  the  dorsnl  fin,  which  is  over  the  space  between  the  veutrul  and 
anal  fins;  the  base  of  the  anal  fin  is  as  lonp^  as  the  distttnce  from  its 
commencement  to  the  origin  of  the  ventral  fins  ;  the  rays  short ;  the 
tail  deeply  forked.    The  fin  rays  in  number  are  — 

D,  14;  P,  13;  V,  7  ;  A,  18;  a  19. 

The  breadth  of  the  eye  is  one  fifth  of  the  length  of  the  whole  head; 
the  peculiLirity  In  the  comparative  length  of  the  jaws  hns  hecn  pre- 
viously noticed ;  the  pill  covers  are  elongated ;  the  scales  of  the  body 
lar^  and  deciduous ;  tbe  colrmr  of  the  top  of  the  hend  and  back  bluci 
wiui  a  tinge  of  green;  irides,  gill  covers,  sides,  ottd  belly,  sdvery 
white;  the  fins  delicate  in  structure,  nnd  greenish  white;  the  mem- 
branes connecting  the  rays  almost  transparent. 

**  In  a  wrieii  of  notes  on  the  occurrence  of  rare  fish  at  Yarmouth 
and  its  vicinity,  with  which  I  have  been  favoured  by  Dawson  Turner, 
Ewyy  there  is  mention  of  a  specimen  of  the  anchovy,  taken  on  the  beach, 
which  measured  six  inches  and  a  half  in  length ;  an  additional  proof 
of  the  large  size  acquired  by  this  fish  on  our  shores.'* 

To  the  above  we  would  add  a  description  of  the  condition  of  the 
true  anchovy  when  bottled. 

The  head  and  intestines  are  removed  ;  the  scales  and  fins,  with  the 

Z 


MS 


ANCHOVIES,   THEIR   SUBSTITUTIONS 


exception  of  iKo  peotornlfi,  am  flilowetl  to  remain  ;  the  fish  is  of  small 
■izt',  iilvvry,  ami  raihor  Ikt,  thii  line  t»f  the  back  slightly  cupveil,  and 
the  rtesh  is  usuiilly  of  a  pink  or  t^ahinin  colour,  the  depth  viirying  con- 
siderably in  (liflereiit  siitnples  auui^rJing  to  a;Te :  if  an  anchovy  be 
three  months  old,  it  will  be  pule  ;  if  »ix  months,  rather  pink;  and  if 
twelve  months,  a  beautiful  deep  piiik  colour. 

The  number  of  the  dn-rays,  whioh  may  be  eounted  in  the  fish  in  its 
preserved  state,  is  greater  than  thiit  ;.'iven  in  the  description  we  have 
quoted;  thus,  when  complete,  the  dorsal  fin  is  composed  i»f  sixteen 
rays,  the  anul  fin  of  nineieen,  and  the  cumki  of  twenty-six  rays. 

Anchovies  are  iraportcd  in  barrels,  and  are  preserved  in  brine  made 
with  rock  gait ;  the  buttling  \a  performed  in  this  country,  chiefly  by 
wholesale  pickle  and  Ii^th-suuce  makers. 


O5    TUB    AdUI-TEBATIONS    OF    AwCHOVlES. 

Several  kinds  of  fish  are  either  substituted  for,  or  mixed  with,  the 
genuine  Gorgona  anchovy. 

The  chief  of  these  are  T>utchy  French,  and  Sicilian  Fish,  and  occasi- 
onally S'srflinei  and  Spratii, 

In  niMition,  the  brine  in  which  the  first  arc  preserved  is  almost  in- 
variably hi;rhly  coloured  with  large  quantities  of  bole  Amtenian  and 
Feuetinn  red. 

Bole  Armenian  is  a  red  ferruginous  earth,  often  prepared  artificially 
bj  mixing  together  Veiieti:tn  red  and  chutk.  The  reason  of  its  being 
added  tci  nnuhovies,  it  is  allcgod,  la  to  improve  the  ajjpearanee  of  the 
fish  ;  but  the  real  reason  U  to  conceal  the  dirt  contained  in  the  brine 
whu-b  (luiTounda  the  fi.sh. 

In  entin^if  anchovies  some  persona  first  wash  the  fish,  bv  which 
means  they  no  doubt  get  rid  of  iiiiich  ctf  the  red  earth  and  dirt  j  but 
others  eat  the  fish  just  as  it  comes  uut  of  the  brine. 

From  an  examination  of  fwettt^'viffki  snuipWa  of  anchovies,  mostly 
in  bottles,  it  appears, 

That  seven  of  the  samples  consisted  entirely  of  Dutch  fish. 

Tlint  two  consisted  of  u  mixture  of  Dirrca  risn  and  Anchovies. 

That  the  brine  in  hvatiythre*"  of  the  samples  was  charped  with 
either  bole  Armenian  ot  Vtuvtian  retl^  the  <pmntity  vary  in;;  consider- 
ably in  amount;  but  in  most  c:isi*s  the  brine  was  saturnted  with 
these  eiirthy  p*>w«lers  to  such  an  extent  flnit  they  might  be  obtained 
and  collected  from  the  bottom  of  the  bottles  nlmost  by  teaspoonfuls. 

It  is  not  to  be  inferre<l  that  those  samples  iu  which  no  Dutch  fish 
were  detected,  consisted  of  the  true  anchovy,  since  we  hare  ascertained 
that  two  other  kinds  of  fisli  betides  the  Dulch  are  conimonlv  iin- 

-ted  and  sold  as  *'  true  anchovies,"  and  "  real  Gorgonas,"  —  namely, 
ch  and  Sicilian  fish. 


AND   ADULTERATIONS. 


339 


Now,  we  liave  no  iloaht  but  Umt  the  majority  of  the  aliovc  samples 
consisted  entirely  of  one  or  ollitT  of  these  fiali;  wehesitale,  however,  to 
pronounce  a  poaiiive  opinion  in  carh  case.  Although  it  is  not  dilli- 
ualt  to  distini^uish  Freneh  and  Sicilian  fish  from  the  Gor^ona  an- 
chovy, when  firHt  taken  froru  the  barrels  in  which  they  are  imported, 
yet  when  contained  in  bottles,  the  discrimination  is  often  a  matter  of 
considerable  dilGeulty^  and  in  many  cases  is  even  scarcely  possible. 
This  arises  from  the  siiueczing  and  mutilation  of  the  fish  in  (he  pro- 
cess of  boitlinpf.  aa  well  us  from  the  altered  appearance  due  to  the 
red  earthy  nuvtters  with  which  they  are  c<imraonly  corered.  AVhether 
chose  enga^C'l  in  the  trade  ore  acquainted  with  any  practical  charac- 
ters by  which  the  discrimination  of  the  fish,  even  wqcq  thus  altered, 
may  be  eflecled,  we  know  not. 

We  have»  however,  much  reason  to  think  that  Sicilian  and  French 
fish,  notwiLhalanding  their  resemblance  to  the  true  anchovy,  may  be 
distinguished,  by  experienced  peraons,  even  when  bottled.  Witli  a 
view  to  dett^rmine  this  point  we  forwarded  to  a  person  engaged  in  the 
anchovy  trade,  twelve  of  the  samples  referred  to,  each  being  labelled 
with  a  dialinct  number ;  the  following  U  bis  Keport :  — 


1.  Gorgona. 

2.  French  fish. 

3.  Ditto. 

4.  Gorgona,  not  fine. 

5.  Sicilian  Fish. 

6.  Gorgona. 


7.  Dutch,  inferior. 

8.  Sicilian,  good  quality. 

9.  Gorgona. 

10.  Dutch  Fish. 

11.  Sicilian. 

V2.  Sicilian,  beat  quality. 


k 


If  this  list  be  correct,  then  not  ohb  thibi>  or  thk  twkkty-jucut 

SAMPLES    KXAMINKD    CONSISTED    OP  GOBOONA    AnCHOVI£S. 

The  practice  of  imparting  an  unTiaturally  ret!  colour  to  the  fish  and 
brine,  by  means  of  Venetian  red  and  ImjIc  Armenian,  is  in  the  highest 
degree  reprehensible.  To  saturate  an  article  of  food  with  lor^^e  quan- 
tities of  earthy  colouring  matter,  is  objectionable  on  the  score  of 
cleanliness ;  it  is  equally  so  as  regards  health,  for  this  earth  contains 
a  large  quantity  of  iron,  ^ow,  this  medicine  la  not  suited  to  all  cases, 
and  it  may  even,  in  some  instances,  be  prwlueiive  of  mischief;  at  all 
events,  when  it  is  desirable  to  titke  iron,  we  should  prefer  that  it  be 
prescribed  under  the  advice  of  a  physician,  and  not  adiiuni-ftered  in 
an  article  of  food  by  our  grocer,  fishmonger,  or  Italian  warehouse- 
man. 

Again,  it  occasionally  happens  that  Venetian  red  contains  red  lead ; 
and  although,  in  the  analy^es  we  have  made,  we  are  happy  to  stato 
that  we  have  not  detected  that  j>oiiimioua  metallic  oxide  in  a  lingle 
tampUt  there  is  no  question  but  that  red  lead  is  occasionally  to  be 
found  in  bottled  anchovies. 

Anchovies,  even  when  thus  coarsely  reddened,  and  put  up  in  gloss 

X  2 


S40 


ANCHOVIES,    THEIR   SUBSTITUTIONS,   ETC. 


botlleflf  are  not  particularly  sightly  objecta.     Both  for  convenience 

and  appeariinee,  it  wouM  be  much  better  thai  they  nLouU  be  enclosed 
in  open-niouthetl  earthen  jars,  which  might  be  mft4le  of  different 
patterns,  and  tia  ornumcntal  oa  de:»ired;  bv  this  meADB  the  ne<:e«sii7 
for  colouring  would  be  done  away  with,  and  there  would  be  no  occa- 
sion to  use  wax  and  resin,  themselves  fre^piently  coloured  with  red 
lead,  to  coat  the  corks,  and  Rime  of  which  tiubstances,  on  the  bottle:} 
being  opened,  usually  And  their  way  into  the  contents.  Now  that  glass  19 
80  cheap,  if  bottles  continue  to  be  used,  they  should,  at  all  events,  be 
furnished  with  gloss  stoppers  in  place  of  corfca. 


On  thf  Dfiteetirm  of  the  Adulteratioks  0/  Awhomfs. 

The  DiUck  fish  may  be  distingiusbed  from  the  true  anehovy,  by 
its  being  invariably  aeprived  of  its  scales,  by  its  large  sixc,  while 
flesh,  general  coarseness  and  by  the  very  evident  scale-marks  which 
extend  over  the  whole  surface.  The  fins  have  the  same  dispositiun  as 
the  true  anchovy,  and  the  »amc  number  of  rays  ;  and  it  is  posjiible  that 
this  6sh  may  be  one  of  the  genus  Etigraulu^  of  which  there  ore  three 
or  even  more  species. 

The  French,  and  especially  the  Dutch,  fish  are  mt  only  of  much 
less  value,  but  also  greatly  inferior  as  articles  of  diet  t«»  the  true 
anchovy.  The  difference  in  iheir  c«st  may  be  e8timate<l  by  the  fact, 
that  dealers  find  it  worth  their  while  to  mix  them  in  dl^ercnt  pro- 
portions in  even  the  some  bottle.  There  i^  no  difficulty  in  distin- 
guishing the  Dutch  Ssh  by  the  characters  pointed  out  ubuve ;  but 
it  would  be  very  difficult  to  discriminate  butween  (he  linger  sum- 
pies  of  the  French  anchovies,  when  denuded  of  their  scales,  ond 
that  which  in  this  article  is  denominated  Dutch  Jixh^  and  hence  we 
infer  that  the  two  may  |H>ssibly  l>e  separate  states  and  conditions  of 
one  and  the  same  species. 

The  French  Fish  is  caught  off  the  coiuts  of  Nantz  and  Nice,  and  is 
imported  into  this  country  in  barrels  packed  in  brine  made  with  rock 

Mlt. 

It  closely  resembles  in  its  characters  the  true  anchovy,  and 
18  probably  of  the  same  genus.  Like  the  anchovy,  it  is  depnyed  of 
its  head  ond  intestines,  but  the  scales,  and  not  unfrequenlly  the 
brachijd  rays  and  pectoral  fins,  are  entire.  Moreover,  the  tilth  is  usu- 
ally somewhat  larger,  thicker  across  the  back,  tapers  more  towards  the 
tail,  and  the  flesh  is  much  whiter  than  the  Gorgona  anchovy.  These 
ditferences,  however,  are  not  sufficiently  marked  in  general,  to  allow 
of  this  tish.  when  bf^tled,  being  sutisfoctorilv  distinguished  from  the 
true  anchovy  by  an  ordinary  observer.  Its  commercial  value  is 
about  one  half  that  of  ilie  Gorgona  anchovy. 

The  tSieiliari  Fixh  resembles  the  Gorgona  anchovy  very  closely, 
rhich,  by  some,  it  is  considered  to  be  the  young,  it  being  smaller. 
*ier  it  be  a  state  of  that  species,  or  of  the  same  genus,  we  are 


I 


POTTED   MEATS  AND   FISH. 


341 


not  able  to  determine  with  certainty ;  its  value  i>  at  least  one  third 
less  than  ihul  of  the  Gorgona  anchory. 

In  none  of  the  samples  have  we  met  with  either  tpraU  or  tardinety 
althoui^h  there  is  nn  dimht  (hat  both  Oiese  6flh  have  been,  and  arc 
still  occaaioiiiilly.  sohl  a£  real  Gorgona  anchovies.  The  sprat  may  be 
readily  dislinguishefl  from  the  nnchovv.  by  the  dorsal  fin  which  con- 
sists of  seventeen  rays,  but  more  particularly  by  the  position  of  tJie 
ventral  fin,  which  is  placed  in  a  vertical  line  directly  under  the  first 
dorsal  iin-roy. 

The  vardine  is  a  short4>r  and  thicker  fish  than  the  anchovy ;  it  hu 
white  flesh,  and  the  relative  position  of  the  ventral  and  dorsal  fins  is 
different. 

On  the  Detection  of  Vetietinn  BctI  awl  little  A  rmenian.  — The  presence 
of  these  earths  is  sufficiently  indicated  by  the  red  colour  of  the  brine, 
and  by  the  colour  snd  earthy  character  of  ttte  precipitate.  In  order 
to  oblflin  ihem  in  a  separate  state,  the  fish  should  be  repeatedly 
washed,  the  washings  and  the  brine  evaporated,  tJie  residue  treated 
with  water  to  dissolve  out  the  salt,  and  then  incinerated  and  weighed  : 
finally  the  ash  must  be  tested  for  iron  and  chalk  according  to  the 
processes  already  given  ;  that  for  iron  at  p.  102.,  and  that  lor  chalk 
at  p.  101. 

Anchovies  and  all  fish  are  free  of  duty  on  importation,  and  no  re- 
turns are  taken. 


POTTED  MEATS  AND  FISH,  AND  THEIR 
ADULTERATIONS. 

PoTTBD  meats  and  fish  are  adulterated,  first,  by  admixture  with  sub- 
stances added  for  the  sake  of  bulk,  weight,  and  eheapncss;  and  second, 
with  others  designed  to  heighten  their  colour. 

Thus  they  arc  sometimes  adulterat4:d  with  large  quantities  of 
flour^  und  in  other  cases,  it  is  allied,  with  even  ckaik  and  placer  of 
Paris. 

Again,  gpmtM  and  other  cheap  fish  are  often  bruised  up,  and,  after 
being  sea.«iiDed,  are  sold  either  in  the  separate  or  mixed  state  fur  rcul 
Gorgona  paste. 

Lastly,  the  majority  of  these  pastes  are  very  commonly  coloured 
with  large  (juanlilies  of  Venettan  red  and  bole  ArmeuuiH, 


z  3 


84S 


POTTED  JfEATS  AND  FISH, 


BB8ui;r8  07  thk  £xAMTKATio:f  or  Samples. 

Twenty-eight  ftaoiplea  of  polled  meats  and  fish  were  examined,  and 
with  the  following  results  :  — 

Ut.  That  ihe  samples  of  Potted  Tongw  and  Ham  were  entirely  free 

from  aduUeralion. 
2nd.  Thai  four  out,  of  the  five  samples  of  Potted  Beef  were  artifidally 

coloured  by  menus  of  the  red  ejtrth>  hole  Armenian, 
3nl.  That  the  whole  of  the  samples  of  Potted  Bloaters  examined  were 

highly  L'oloureil  with  the  before-named  eariliy  substance. 
4tb,  That  one  nf  the  sonipLvs  of  Blnater  Paste  was  adulterated  in 

addition  with  a  large  proportion  of  starch  or  Jtour^  probably  wheat 

llotir  boiled. 
5th.  That  the  entire  of  the  samples  of  Anchontf  Paste  analysed  were 

still  more  highly,  and  even  \*ividly,  eoloured  with  very  lar^e  quan- 
tities of  bole  Armeman. 
6th.  That  two  uf  the  Anchovy  Pastes  were  In  addition  adulterated 

with /fowr;  one  with  a  lurL'e  per-cciitiige  of  wheat Jtoitr. 
7th.  That  of  the  twenty-eijiht  wintpK's  of  Potted   Meats  and   FUk 

subjected  to  analysis,  no  less  than  twenty-three  were  more  or  lesa 

impref^nated  with  the  red  earthy  material,  bole  Armenian. 

Tins  picture  of  the  ndnUeration  of  potted  meats  and  fish  is  surely 
bad  and  disgmceful  enough. 

The  difTerence  in  the  appearflnce  presented  by  the  uncoloured 
samples,  contrasted  with  those  in  which  the  bole  Armenian  had  been 
added,  wiia  most  striking,  and  usually  suflifient  to  enaM*.'  the  observer 
to  distinguish  by  the  eye  ulon^*  the  c«Hmples  to  whirh  this  scandalous 
addition  had  been  made.  While  iii  the  one  caf*e  the  paste  was  of  a 
pale  pink,  and  perfectly  natural  hue,  in  the  other  the  colour  was  such 
aa  the  flesh,  when  pnnnde^l,  of  no  fish  or  animnl  ever  presents,  it  being 
of  a  deep,  earthy,  and  brick  red. 

In  a  pr-evloui  Report  we  showed  th.it  one  of  the  principal  reasons 
why  artificial  eolourin"  matters  are  employed  in  the  ciise  of  Iwttlcd 
anchovies,  iii  to  conceal  the  dirt  contained  in  the  brtno  in  which  the 
fish  is  im[)orted.  In  the  present  instance  there  is  not  even  this  poor 
excuse;  the  only  purpose  f*erveil  by  the  emjjloyraent  of  the  bo!e  Ar- 
menian being  to  cause  the  potted  articles  to  present  n  striking  ap- 
pearance, but  one  whicl)  at  the  same  time  is,  in  our  opinion,  most  un* 
naturat,  and  but  liltte  inviting. 

In  ihQ  case  too  of  jtntted  meats  and  fish,  the  ordonring  injrredienls 
cannot,  as  in  anchovies,  in  a  measure  be  got  rid  of  by  washing;  for 
since  they  ore  incorjjorated  with  the  paste^  they  must  be  entirely 
consnini*d  with  the  meat  or  fish. 

'  practice  uf  adding  large  quantities  of  coloured  earthy  sub- 
licles  of  diet  is  dirty,  injurious  to  health,  and,  in  some^ 


AND   THEIR   ADULTERATIONS. 


34.1 


€Tcn  rlanprerous  to  life,  cannot  be  doubled.  The  cliief  medicinal 
{nfp*edfenL  in  bule  Armeninn  l»  oxide  of  iron  ;  this,  aIthou<rh  not  dan- 
f^erous.  might  in  some  Infiianet^s  be  prodiicllvc  of  prejudiciul  ed'ects; 
but  it  sotnetimea  happens  that  other  red  earth«i  arc  used,  nnd  these  as 
well  as  uiso  occasionally,  although  rarely,  bole  Armenian  ilself,  are 
contaminated  with  red  lead.  For  (hif  poijfonowt  ntbstance  each  of  the 
alfone  twenty'eight  samplea  hare  been  xfpiiratfly  aiuitlyseti^  withuut  how- 
ever^ we  are  happy  to  stcUe^  a  particle  of  it  being  ducovered  in  a  fingle 
inxtance. 

So  long,  then,  09  manufacturers  continue  to  mix  red  earths  with 
their  {M>ttcd  meats  and  fish, —  these  delicacies  of  the  table,  as  ihcy  arc 
commonly  considered,  f^o  often  had  recourse  to  by  the  gourmand  and 
the  invalid  to  rou.«e  a  flu^'gijig  appetite,  —  so  long  we  recommend  the 
public  to  refrain  from  purchasing  them. 

The  preparation  nf  potted  meats  and  fish  is  so  simple,  that  every 
housekevper  wav,  with  a  pestle  and  mortar  and  proper  seasoning, 
make  them  herself  without  ditHculty. 

Mr.  Kii^hardson,  officer  of  the  Local  Board  of  Health  of  Newton 
Heath,  near  Manchester,  gave  the  following*  evidence,  before  the 
Coniiuitlee  on  Aduhcraiion,  in  regard  to  the  addition  of  horseflesh  to 
potted  meata,  sausages,  &e. :  — 

"  We  have  in  Newton  five  knackers*  yards,  and  there  iti  otdy  one 
in  Manchester.  The  reason  ip,  that  they  have  so  mucb  toleration  in 
Newton;  and  it  has  been  a  source  of  great  profit  to  thorn,  because 
they  have  the  means  of  selling  the  best  portions  of  the  horseflesh  to 
mix  with  the  potted  meats. 

^'  I  can  say  for  a  fact^  that  the  tongues  of  horses  particularly,  and 
the  best  portions  such  as  the  hind  quarters,  of  horses,  are  generally 
sold  to  mix  with  collured  brawn,  or  pics'  heads  as  they  are  called 
with  us,  and  for  sausages  and  pohmiea.  I  understand,  aUo,  frum  those 
who  have  been  in  the  habit  of  niakio';  them,  tbut  hurRellesh  muterialljr 
assists  the  making  of  sausages;  it  is  a  hard  fibrme,  nnd  it  mixes 
better  and  keeps  thtm  hard,  and  they  last  linger  in  the  shop-window 
before  they  are  sold,  because?  cithtTwisj'  the  sausages  run  to  water  and 
become  sofl  and  pulpy.  1  believe  horstlifsh  oJao  materially  assists 
German  saussges  ;  it  keepH  them  bnrd." 

To  the  above  account  we  may  add  that  German  sausages  and  po- 
lonies are  very  generally  coloured  with  large  quantities  of  Veuetian 
red  or  reddle. 

Havinc:  now  gone  over  the  chief  articles  usetl  at  the  Breahfaut  Tahle, 
we  shall  m  the  next  place  proceed   tu  describe   the  adulterations  of 
I  those  coimumed  more  particularly,    tbough   uot  exclusively,  at  the 

I  Dinner  Table. 

^^-  Potted  and  all  otlier  meats  arc  free  of  duty. 


z  4 


UUSTARD,   AND  ITS   ADULTERATIONS. 


MUSTARD,  AND  ITS  ADULTERATIONS. 

The  plants  from  which  musfard  is  obtained  orCf  Sinitpis  nigrft,  or 
Mack,  and  Si/tapis  alba,  or  while  inu&t4ird  ;  xhej  belong  to  the  natural 
fuukily  Cruci/erie. 

The  black  mustard  plant  is  distinguished  by  its  seod  vessels,  which 
are  smoatli,  nnd  the  culour  of  the  seeds  tliemselves,  which  are  reddish, 
or  blackish  brown. 

In  tlie  white  nmstnrd  nfant  the  seed  Teasels  or  pods  are  clothed 
with  hiLirs,  which  render  tliciu  rough,  uiid  the  seeds  arc  yclluw. 

The  two  fpocies  of  musturd  ilitTer  in  properties  as  well  os  in 
botanical  characters. 

The  seeds  of  S.  nigra  are  more  pungent  than  those  of  S.  olba^  but 
there  are  other  differences. 

The  young  or  seed  leaves  of  white  niuiftard  are  usetl  for  salad. 

Both  speeies  are  indijjenouSf  and  may  roniinonly  be  seen  in  flower, 
in  the  month  of  «Iuiic,  in  wiiste  phire^  jind  fields.  In  the  brick  lields 
in  the  neiahbimrhoinl  of  Nottin"  Hill,  iliey  f;row  in  great  quantities. 

The  stibjoineil  particulars,  in  reference  to  the  nmnufucture  of 
mustard,  as  fumisbcd  by  a  iiianufuoturcr,  are  g^iven  by  Pereira  : — 

"  The  secila  of  both  bhick  ami  white  mustard  are  first  crushed 
between  rollers,  and  then  pounded  in  luorturs.  The  poundetl  seeds 
are  then  sifted.  The  residue  in  the  >ieve  is  culled  drexgingn^  or 
si/iittgs ;  whiit  passes  through  i.s  impure  Jiuur  of  nxustanl.  The  latter, 
by  a  second  .tilting,  yieUls  purejftmr  af  miubird,  and  a  second  quantity 
of  dresainjfs.  By  pressure  ilie  drL'{i<<in;zs  yield  a  fixed  oil,  w hick  la 
used  for  mixing  with  rape  and  other  oils." 

CompoiitioH  of  Mustard, 

Analysis  lias  detected  in  black  mmtard  seed  several  distinct  chemi- 
cal couipuimds  —  Myronic  acidy  M^rucyne^  a  volatile  oily  and  a  fixed 
oil  of  mnttard. 

Myronic  uctd  is  nn  inoiloru.i,  naii-viilatile,  bitter,  and  non-orystal- 
lisable  substance,  coiitiilnWig  nitro^uo  And  suljihur,  und  forminu;  tuOt« 
with  bases.  The  charm-teristic  prufierty  of  this  substance  is,  that  it 
yields,  with  myroi-yne,  the  volntile  nil  of  inustanl. 

Mi/rocytie^  the  emiUnin  of  black  niustnnlf  yields,  as  already  noticed, 
with  invronic  acid,  ihc  volatile  oil  of  mustard.  "  It  has  considenible 
resemblance  to  vegetable  albumen  and  viimbin,  but  a»  it  ciinnot  be 
replaced  by  either  of  these  substunccs  in  the  development  of  the  vola- 
tile oil,  it  uiu»t  be  rejjarded  as  a  substance  sm  generis.  It  is  soluble 
in  water ;  but  is  coagulated  by  heat,  alcohol,  and  acidc,  nnd  in  this 
state  it  IcMCs  the  power  of  acting  on  the  myronates,  and  of  yielding 
the  volatile  oil." — Pereira. 


MUSTARD,   AND  ITS  ADULTERATIONS, 


345 


Tbe  volatile  oil  of  mtutard  does  not  pre-exist  m  black  mustArd 
flee<U,  bul  is  foruicd,  us  alreaily  observed,  by  iha  mutual  action  of 
myronic  acid  and  rnyrouyne  in  uold  ur  warm  water;  it  is  this  oil  which 
gives  to  mustard  its  penctrnting  odour,  sharp  burning;  liistt*,  and  iis 
acrid,  rubefacient,  and  vuMicani  properties :  it  contains  nitrogtin  and 
sulphur  in  its  composition. 

The  above  detaiU  are  of  practical  interest  and  importance,  for 
since  heat  coa<;ulatcs  niyrocyne,  and  this  substance  is  necessary  to 
the  formation  of  the  vohitile  oil  upon  which  llie  greater  part  of  the 
active  properties  ofmustanii  depends,  it  is  clear  that  water  either  cold 
or  warm  only,  shntdd  be  employed  in  the  mixin;;  of  mustard. 

The  Jixed  oil  of  muxtrmt  is  usually  procured  from  tlie  siftings  or 
dressing  of  mustard,  which  consist  mainly  of  husk  :  it  is  stal^  to 
constitute  about  twenty-eight  per  cent,  of  ihc  seeds. 

Of  the  composition  nf  wfiitr  mustard  teed  wc  find  the  following  ac- 
count in  Pereira's  "Materia  Mcdica:"— 

*'  Kobiquet  and  Boiitmn  {Jonrn.  de  Pharm.^  xvii.  p.  279.)'  however, 
have  proved,  that  white  umsturd  cdiUains  neither  volatile  oil,  nor  any 
fluhfitunce  capable  td'  producing  it,  but  owes  its  activity  to  a  nott'Colatile 
acrid  gulf xtaHvi\  which  does  not  pre-exist  in  the  seeds,  but  is  readily 
Ibrmed  in  them  under  certain  conditions.  Another  chemical  peculi- 
arity of  white  mustard  is,  that  it  contains  sulpho-sinapisin.  (Henry 
and  Garrot,  ^(/UTH.  de  C'him.  J/w/.,  i.  441.)  Hence,  while  st'si|uichlo- 
ride  of  iron  strikes  a  deep  red  colour  in  an  infusion  of  white  mustard, 
it  merely  communicates  an  onuin^e  tint  to  the  infusion  of  black  mus- 
tard. Moreover,  the  thick  mucdaginous  liquor  obtained  by  digesting 
tbe  seeds  of  white  muista.rd  in  cold  water  is  peculiar  to  them.  (Cadet, 
Journ.  de  Phunn,y  xiii.  191.)  Simon  {Journ.  de  Pharm.^  xxv.  370.) 
baa  announced  the  existence  of  a  new  principle,  which  he  calls  entcin^' 


I 


Slntelure  of  Mustard  Seed, 

Kvcry  entire  seed  cousi.it8  of  two  parts,  the  husk  and  the  seed 
proper. 

The  husk  of  white  muttard»eed  is  constituted  of  three  distinct  mem- 
branes. 

The  outer  membrane  ia  transparent,  and  mucilagiooiui ;  it  coDsista 
of  a  layer  forme<l  apparently  of  two  difTercut  kinds  of  cells  of  large 
uxe  and  very  pet:uUar  structure;  those  of  the  first  kindareofanhexa- 

fonal  fij^ure,  and  united  by  their  edges  so  as  to  form  a  distinct  mem- 
rane,  tlie  (%n(re  of  each  cell  being  perforated;  tbe  ci^lls  of  the  secoud 
kind  occupy  the  apertures  whith  exist  in  tbe  previously  described 
cells,  and  they  are  themselves  traversed  by  a  somewhat  funnel-shaped 
tul>e,  which  appears  to  terminate  on  the  surface  of  the  seed:  immersed 
in  water,  these  cells  swell  up  to  several  limes  their  original  volume, 
occasion  the  rupture  of  the  hexagonal  cells,  and  become  themselves 


^ 


MS  1CU9TARD,   AXD   ITS  ADULTESATIOXS. 

modi  wrioUcd  or  eormgBted,   ihe  extremitj  of  tke  tabo  in  i 
CMCi  beizig  nca  protooitiiig  from  the  proxmute  tenaixuuoo  oC  tbs 


rrwmtDt  of  Um  ()«/«r  tnrmlifBM  irf  Hit  iMd  of  WWTB  Mcbtasd. 

Mkffnlfleil  i3u  dlunettn. 


celU.  It  is  pn»oibln,  however,  that  what  are  here  (U'<tcnbGi1  as  two 
different  kinds  of  cells  rt'iilly  furm  distinct  parte  of  the  same  <m.'1Is. 

It  hft-s  been  notieed  thjit  wiieii  white  mu&tnrd  seeds  are  digened  in 
water,  a  thiek  niucilagimms  lijjuid  is  obtained:  the  source  of  the  mu- 
cilage docn  not  appear  to  hnve  been  puinlL-d  out ;  it  is  certainly,  how- 
ever, derived  from  the  cells  forming  the  tissue  above  described. 

The  middle  tunic  consists  of  a  sinple  layer  of  very  minute  cells,  of 
an  ttnjrular  form;  it  is  in  the  cavities  of  these  that  the  chief  part  of  the 
colouring  matter  posaesfled  by  the  huak  is  seated. 

The  inner  memonuie  also  consista  of  a  single  layer  of  angular  cells, 


MUSTARD,  AND   ITS  ADDLTERATlONflL 


347 


which,  however,  are  several  time<i  lurgcr  than  thnse  constituting  the 
middle  tunic. 


Pig.  in. 


Fntfimnli  of  the  miABw  ud  mmtr  taola  of  loUto  oitMriArd  «cd,  the  forater  conHos 

■nil  lying  upon  a  part  (tf  llic  latter.     >l*f  nlSrd  W)  <l}Bin«lm. 
^ .  Parnon  trf  the  mvUlie  lnule.      if.  A  fnfnicDt  of  tb<  inmr  tutiic,  fli<nriti(  tbt 

■Irvedm  of  that  cwmbruie. 

The  «rtd  itself  is  of  a  bright  yellow  colour,  and  of  a  soft,  waxy  con- 
sistence, depending  upon  the  qiianlity  of  oil  it  contains;  it  consists 
of  innumerahle  very  minute  i-elis,  in  the  cavities  of  which  the  oil  and 
other  active  principles  arc  contained.     Fig.  124. 

Notvrithstnnding  the  terms  "  Hour**  and  "  farina  "  of  mustard  com- 
monly employed,  v\\>c  mustard  seed  does  not  contain  a  sinfflc  starCh 
granule,  as  may  be  ascertained  by  means  of  iodine  and  tne  micro- 
scope. 

In  black  mtistard^  the  outer  membrane  of  the  seed  consists  only  of 
the  larjfe  hexasonnl  transparent  cells  disposed  in  two  or  three  layers, 
and  not  perfnrateJ  in  the  centre  like  those  of  white  mustard;  tho 
other  structures  resemble  those  of  white  mustard.    Fig*  125. 


348 


MUSTARD,  AND   ITS  ADULTERATIONS. 


r 


On  the  Adclterations  of  Mustard. 

The  ordinary  aduUerntioiia  of  mustard   are  with  wheat  fliyur 
turmeric^  the  uMi|iIojiiieiii  uf  th«  fir.et  named  urtitie  neceasitating  the 

Fig.  tu. 


Buuri*  of  fvmJM  gnmiul  vktte  mumant.    Dnvn  with  tha  Cimtn  L«eldft,  mnA 
owcuUied  CM  (llunctair*. 

use  of  the  other  to  restore  or  bring  up  the  colour  to  the  original 
standard. 

Results  of  the  Examination  of  SampleM. 

No  !eS9  thnn  Forty-two  sampler  of  mustard  purchased  in  the  metro- 
polis were  subjected  to  examination :  the  whole  of  ilieiu  were  found  to 
consist  of  mixtures,  in  vuriuus  pruiHirtions,  of  wheat  flou-r^  turmeric^ 
and  mmtard. 

Other  adulterations  sometimes  practised  are  thos*i  with  Cajfenne 
pepper^  Sinupi*  AvensiM,  or  cHariork,  clay,  planter  of  Paris,  and  cAn*- 
mate  of  lead.  The  pepper  in  used  to  iniprtrt  piinpency  to  it  when  it 
has  been  otherwise  adulterated;  olay^  for  bulk  and  weijiht;  and  the 
cbromaCe  of  lead,  to  restore  the  colour  when  reduced  bj  other  adul- 
terations. 


MUSTARD,   AND   ITS  ADCLTERATrONS. 


349 


Mr.  Wnrington  states,  in  In>  evMeiice  before  the  Parliftmentarr 
CuuunitUe  on  Adulioration,  llmt  »otne  of  the  samples  of  mustard 

Fig.  185. 


[ 


nuit  or  Black  VvBtA%ttHr4.   WmgnlMianMuntttn, 

which  be  examined  containe<l  from  20  to  30  per  cent,  of  inorganic 
matter,  chiellv  sulphate  of  lime;  ihe  gemiini:  mustard  when  burned 
yielding  from  4^  to  6J  per  cent,  of  retiidue. 

Mr.  Gay,  tbrmorly  a  mustard  ornl  (;bicorj  manufacturer,  and  now 
Superintendent  of  the  Mustard  Depnrtmcnt  in  ht'r  Majesty's  Vic- 
tualling Yard  nt  Deplford,  furiiifbed  the  Couimitt«e  uiove  named 
with,  amongst  ntber  infurmation,  the  fullowing  respecting  the  udultern- 
tion  of  uiUKlurd.    He  state?, — 

"  I  Iwlievu  vcrv  f«w  scruple  tit  use  wheaten  llour,  turmeric,  and 
Cayenne  pepper.  The  adulterants  I  used  were  tlour,  turmeric,  Cayenne 
j^epper,  and  ginger. 

"  But  farina  is  also  used,  and  potato  starch  is  used  to  a  very  great 
extent ;  and  now,  I  am  oorry  to  say,  whut  ono  of  the  witnecws  called 


330 


MUSTARD,    AND    ITS    ADULTERATIONS. 


tern  «Iba,  or  plaster  of  Pari*.  I  hxvt  had  some  samples  in  my  office  in 
the  tnusUrU  Ueparimeat  since  I  bare  b«en  in  my  prL-sent  situation, 
from  which  I  bare  extracted  5  oumia  of  ^rpaum  in  the  pyuud  ;  from 


Mr.Ufi. 


Tkh  MifnvlBf  repKaenb  the  wtkJw  iklieHJ  bi  ft  Minpte  at  **  tkmUt  iMitrjfcii 
McRAKft,"  mariifd  wltk  lh*  nunci  of  Mimti.  i.  ft  J.  Co1i»«b  t  a  a,  ■nwMN 
Jhm-:  i h,  Btlli  at Ummane  lumJtr :  c.  pwrtlaa  of  Atn*  tJlhitA  wm>w7,-  < ■■lb 
of  ««ter  tBDlo  of  wAAe  wMttarvf  Marf;  «  c,  ftvfmuils  of  Ui«  mk/  lualf. 

another  stunptu  I  got  5  ounces  of  rice  and  wbeaten  Hour.  I  have  seen 
more  than  50  per  cent,  of  gypsum  in  mustard." 

With  re^fird  (o  the  adulteration  of  mustard  with  charlock,  Mr.  Gut 
remftrka,  "  When  raustanl  seed  is  worth  20a.  per  bushel,  and  charlock 
about  6i.  or  Sx.  a  bushel,  it  is  worth  buyini;.** 

It  is  also  alleged  thnt  pea  Jiour^  radish  and  rape  seed,  linseed  mcalj 
and  yellow  ochre  have  been  emplnyed  in  ibe  adulteration  of  mustard. 

No  less  than  four  diffiTent  nuulities  of  mustard  are  supplied  by  the 
mustard  manufacturer,  under  the  name  of  "Seconds,''  "Fine,"  "Super* 
fine/' and  "  Double  Superfine;"  the  chief  <lifference  between  these 
articles  i!^  that  the  lower  the  quality  tlic  larger  the  proportion  of  wheat 
Hour  and  tiirmoric  which  they  contain. 

These  sercral  mmlities  may  be  purchased  at  about  the  following 
rates:  seconds,  5a. ;  fine,  8c/. ;  superfine,  lit/.;  and  double  superfine, 
at  U.  ^d.  per  lb. 

The  practice  of  making  so  many  diQ*erent  qualities  of  mustard  Ja 


HU&TABD,  AKD  ITS  ADULTERATIOXS. 


351 


open  to  much  objection,  aince  tt  gives  the  wnacrupiiloua  donlcr  the 
greatest  scope  I'ur  impu-iitiun.  The  {loor  tuun  hnys  his  mustard  by  the 
ouncCf  and  lor  this  bv  usuully  piiys  it/.,  receiving  in  return  seconds, 
fine,  or  superfine  uiu^tunl,  according  tu  the  cutiscienee  of  the  vendor. 

it  L'un  now  \>Q  underi^tood  huw  it  bapjieiis  ihut  some  of  the  inixturea 
which  we  buy  for  inust;u'd  scarcely  pi>.ss>esa  the  Uavuur  of  that  article, 
and  how,  when  used  for  poukice^,  they  ])roduce  little  or  no  effect,  a 
matter  uttenlinit:!!  of  vitul  coniciiuenct:. 

Dtmbtiejiis  wc  !ibu.U  be  told  by  the  mustard  manufacturer,  that 
genuine  mustard  u  a  very  uopaI;itabIe  thing,  that  it  itt  bitter  to  the 


taste,  and  not  plcwant  to  lofjk  at;  bnt  the  answer  to  this  is,  that  the 
article  um.stard  is  not  ulwsys  mode  according  to  one  receipt,  and  that 
there  exiitt,  even  in  England,  u  few  manufacturers  who  make  and  sell 
only  genuine  mustard. 

Oh  the  Detectinii  nf  the  AdnJte  rations  of  Aftutard. 
The  deteclion  of  the  nrdinnry  ndultcralions  of  mustard  is  effected 
▼cry  readily  by  mean*  of  the  microscope.     The  chura^-tcra  of  wheat 
fiour  are  described  and  figured  at  p.  243.,  and  of  turmeric  under  the 
ncad  of  that  article. 


) 


ITmiAtda^la^  mad,. 


rapf  are  •ometimc*  cfflplored  in  the  adulterftiMti  d  mvtard, 
Mr  ftpjKiul  6|prei  aod  ducnpiioiu  uf  the  busks  of  tboM  acedii 


MUSTARD,  AND  ITS  ADULTEUATIONS. 


85) 


StntclHre  nf  Sirwpis  arpertsvt,  Qr  Charloch. — The  husk  of  thu  seed 
reseoiblefi,  in  colour,  very  firwely  bliwk  mustard,  from  which,  how- 
ever, on  11  careful  exnaiinatinn,  it  may  be  dwcriminated  by  meant 
itf  the  tniorcMCope,  notwithstanding  the  5(ateraent  of  Mr.  Gay,  mad« 
bcfon;  the  Parliamentary  Comnutiee,  **  that  no  annlytical  chemist 
could  detect  charlock  seed  mixed  with  muntard,  even  with  the  micro- 
acope." 

Fit-  l»- 


A\  hile  it  agrees  in  colour  with  the  husk  of  black  mustard,  it  ap- 
:bc8  ID  straeture  nearer  that  of  white  mustard,  from  which,  how- 


»»« 


MD6TA&i>,   A9D    ITS   ADULTERATIOXS. 


•vflTt  it  may  be  dbtuykbed  in  the 

ckief  difcvnee  m  ia  ne  cell*  of  tbc  oater  or 

■rcHaaBwidnoredriicate  than  tboMof  ibe  iMMkoTvyie 

tbej  are  perTurated  like  tbem,  bowever,  bat  in  addition  tber  cadi  teeB 
to  be  mikde  up  of  numerous  angular  verr  delicate  and  mtntUeceU*; 
tbcae  are  rexj  rfaaracteristii;  of  the  seeds  of  Oarlock.     Fi^.  128. 

tStntctare  of  Rape  SectL — The  membranes  forming  the  bask  of  rape 
«eed  are  m  distinct  that  no  dlffiouliy  need  be  eipeneneed  m  distio- 
guishing  thii  teed  froin  those  of  anjr  of  the  mustards.     It  is  f^mtpttamA 


M  Rut  iMltui  Hmc.  hat  vhkk 


tptOtt  Iff 


of  two  membranes,  tbc  outer  resembling  somewhat  the  second  mem- 
brane of  the  busk  of  the  mustards,  but  tbe  cells  ore  much  larger,  and 
in  consequimeu  their  cavities  du  nut  appear  black  in  p^rneral,  but  nior« 
or  lem  lisbt,  the  walls  of  tbe  cells  being  thick  and  well  defined  ;  near 
tbe  unibdicua  of  tbe  seed  the  cells  usually  are  disposed  in  a  linear 


MUSTAUD,    AND    ITS    ADULTERATIONS. 


355 


manner.     'I'he   innerraost  niembranc  does  not   prcacnl  any  peculi- 
arity. 

In  a  sample  of  rape  cake  forwarcied  to  us  for  examinatir.n,  and  sus- 
pected to  Ir*  ndulleriiteil  with  mustarU,  we  met  with  what  ap|)eared 
lo  be  the  husk  of  a  species  of  mustard.     It  U  represented  in^'.  131, 


Pit.  IXI . 


Trttttntr**  %aA  Vtrtimi  SerltoM*  nf  htitk  of  •  ipcrli*  nf  htr^TABD  8liii>  met  wllk 
In  ■  uMiiilc  xrKtalunLlMl  nrcftiMl  fiooitbi  coiwiuninlon  vf  «bich  loawaiitlt 
u%  niA  K>  twve  ilted.     SAi  diuDcler*. 

Jt  approaches  in  structure  mo9t  nearly  to  the  hn.sk  of  blark  mustard, 
hut  the  cells  of  the  first  coat  are  pcrforaled,  and  those  of  bnth  the 
6rst  and  scrnnd  coiit^  arc  oinch  1:ir<:cr  :  in  the  large  riizc  of  the  celts 
uf  the  second  coat  it  comes  sunienhut  near  to  tlic  liusk  of  rape  seed  : 
but  then  in  this  we  have  never  nut  with  any  outer  toat  of  large 
colourless  celK  llie  hu^k  in  question,  therefore,  belongs  most  pro- 
bably t<»8ome  foreign  }<pecies  of  uiu»lnrd 

Uadi>h  5C0<I,  on  account  of  its  price,  is  scnrcely  likely  to  be  employed 
in  the  uduHeralion  of  mustard  ;  it  is  not  necessary,  therefore,  to  give 
A  ilfsrrijilion  oi' its  flrm-ture. 

Fiir  the  ilijicovery  of  the  inorgmiic  aduiierationg  of  mufltard,  rei'ourse 
must  be  had  to  chemistry. 

The  proceM  for  the  detection  of  alumina  nr  clay  is  gi\  en  at  page  1 80., 
i/tgypiutn  ur  tulphair  vf  lime  at  p.  09.,  of  j/cHuw  ochre  in  the  article  od 

A  A   S 


85« 


PEPPEK,    AM)    ITS   ADL'LTERATIONS. 


Turmeric,  and  of  chrome  yellow  or  ehromate  of  lead  in  that  on  Coloured 

Sujiar  Coiififctionei  y. 

Mii.ourd  flour,  duty  Ijr.  Gd.  percwt.     Ditto,  mixed  or  maiiufscti 
(except  lloiir),  5*.  por  cwt. 

Imports  of  i]vur  in   1»54  Hml   1855.  3  and  2  cwls.  re^peotireh 
Mixed  ur  munui'uctureil,  niher  limit  ilour,  in  185-1,  97  cvrt<*..   and 
1855,  lOQ  cwts.     Kt'lained  for  home  coDSuutption,  95  and  78  cirti. 
each  of  tlie  years  specified. 


F 


PEPPER,  AND  ITS  ADULTERATIONS. 

The  nnliiral  fiimily  Pipfracea  im'UidL's  four  plonls  of  g^re^it  utility 
iiiunkiiid;  two  of  those,  Piper  ni^mm^  nr  bhick  pf[tper,  mid  Piper  Ioh- 
guMy  nwtre  n^cenlly  nnincd  Cfiacica  ftnxtiurghiiy  or  long  ]>»?pr>t'r,  nre'l 
rhielly  omployud  for  dioleiic  and  ruliimry  purposes;  whilst  the  nlhers, 
Piper  Cubehuy  nnw  Cubcbfi  o^civalix,  utui  Arifmthe  eloiigaUt^  or  the 
niatic'o  plant,  are  piiiK'ipidly  employed  in  tnedieine. 

The  plant  which  yields  Cayenne,  Capsicum  anunnm,  often  improperly 
termed  Cayetuie  pei>per.  dtn^s  nut  belong  to  the  family  of  Piperacete  at 
all,  but  to  that  ni'  Soitintfcete. 

The  pepper  of  cnninicrce  is  furnished  by  Piper  nigrum,  and  it  ii  to 
this  specie:*,  therefore,  that  on  the  present  occasion  we  shall  have  to 
direct  atlpntion. 

The  black  pepper  plant  tjrows  both  in  the  East  and  West  Indies,  in 
Sumatra^  JavEU  and  ntber  irUiiidB;  it  is  u  shrubby,  climbinj;  ptanKf^H 
which  attains  th*^'  hir-i^lil  uf  iVoui  uiphl  to  twelve  ftn:U    Tbe  burrie?,  or^| 
peppercorn*,  grow  on  ternnnuL  flinverstalks  or  iipadices :  tliuy  are  at  ^^ 
first  green,  but  i'hiin3:e  subsequently  to  red  unil  then  to  bliK-k.    When 
any  of  tbe  berries  on  a  spadix  have  begun  to  turn  red,  the  whole  are 

§atherc<l,  dried  in  tbe  sun,  and  the  utalks  separated  by  the  hand.  la 
ryinp,  ilie  succulent  part  of  cnL-h  berry  beenmcj*  contracted  nnd 
wrinkled,  forming;  a  hjir<U'ned  wrinkled  cortex ;  the  enrrugations  being 
niucli  raisied,  and  deseribiug  n  kind  ofelcvoted  network. 

The  follfHrinj*  more  tietniled  particulars  conoerninp  tbe  growth  of 
the  pepper  ptunt  and  tlif  j.^iitltering  of  the  berries  ure  extrauted  from 
M^CuHoeh's  *"■  Dictionary  of  Commerce"  ;  — 

"  It  climbs  to  the  height  of  twenty  feet,  but  is  said  to  bear  best 
when  restraineil  to  tbe  Tieirrht  of  twelve  feet.  It  begins  to  proiluce  at 
about  the  third  year,  and  in  in  perfection  at  tbe  seventh :  continues  in 
this  state  for  three  or  four  vears,  and  tleclines  for  about  as  manv  more, 
until  it  ceases  to  be  worth  keepint^.  The  fruit  grows  abundantly  from 
all  its  branches,  lu  long,  small  clusters  of  from  twenty  to  fifty  grains  j 
when  ripe  it  is  of  a  bright  red  colour.     After  being  gathereil,  it  is 


PEPPER,    AM)    ITS    ADILTKRATIONS.  357 

on  num.'*  in  llie  sun,  when  it  Io^o.h  its  red  cnlour,  find  becomes 
tJiil  (^lirivfllod  as  wo  »ov  it.  Tho  {;pain.^  nrc  fleimrateil  ("roni  the, 
Btulk?  by  lianri-rijl'bin;,'.  Thai  whicli  has  been  jriitheroil  ut  the  proper 
pi'pjod  pliiivela  the  leiwt;  but  if  plucki<!tl  inn  soon,  il  will  bc<:o]iic  broken 
iitu!  dusty  in  it^  removal  from  place  to  place.  The  vine  prutiuees 
two  erojHt  in  the  }ear,  but  ibe  seasons  are  subject  to  ^reut  irregu- 
lurittGii." 

Those  berricit  nre  the  beat  which  are  not  too  amoll  nor  too  much 
Ci'rrujjaleil;  which  are  heavy,  itnd  sink  remlUv  in  wnt*'r. 

The  two  varietie«  of  pej)pfr  known  as  "  blnik  '*  ami  '*  wlitte"  pepper 
Are  both  nbtuined  from  the  snine  jilnnl. :  bliick  ground  pe|.p|ier  is  the 
entire  berry  rL>duce<l  to  powder,  wliile  ibe  wfiite  eonsifits  oi'the  same 
berry  decorticated  or  deprivud  n!  its  (»uu*r  and  black  husk  or  covering. 

We  learn  fnun  Pereira  thut  throe  kinds  of  biack  pepper  are  distin- 
guished by  wholesale  dealers.     These  are  :  — 

''''  Mtihihnr  tiepper.  —  This  is  the  itiosl  viitiiuble;  il  is  hrotruUh'bhick^ 
free  from  sialks,  and  nearly  free  from  dust." 

^^Peitanfr  papptr.  —  This  is  broufniithhliek,  larpar,  smoother,  free 
from  stalks,  out  very  dusty.  It  is  sometimes  used  in  England  to  mS' 
nufactnre  white  pepi»er." 

"'■  Sumntra  pepper.  —  This  is  the  clieapeiit  iort;  It  is  black,  mixed 
with  slnlks^  and  contains  nuich  dust.  Unrler  the  name  uf  Sumatra 
pep|*r,  w»iin;  ilealerc  include  the  Peiiang  or  brownish-black  sort,  and 
tbp  black  Sumatra  sort." 

Three  kinds  or  varieties  of  Khiie  pejtptr  have  also  been  distin- 
guished. 

**  TeUtrherrp  pepftfr^  whi<:h  is  of  two  kinds  :  large  or  fineTellicherry 
pepper  is  lamer  and  whiter  than  any  other  descripticun  of  white 
pepper,  and  fetches  a  higher  price;  ninall  or  coriander-like  pejtjter  is 
shrivelled." 

"  C\immnn  white  pepper  comes  fnim  Penanj;  by  Slngjtpire ;  it  ia 
round,  and  not  shrivelled  ;  iL<(  vulue  depends  <in  its  size  uiul  whitL*ness." 

**  English  blrttrhfU,  or  white  pepper.  —  When  the  two  preceding 
sorts  are  scarce,  brnwii  iVMUinj;  pep|tep  is  bleuchi'd,  The  yellowest 
and  largest  grains  ure  t  tnriteo  lor  this  purpose,  for  neither  an  expen- 
sive nor  duiail  sort  would  pay.** 

On  the  Composition  of  Pepper, 

The  active  properties  of  pepper  dejwnd  upon  the  presence  nf  nn 
arrid  resiUy  a  volaHle  oil,  and  a  crystallisabte  substance  called  A- 
I       perine. 

The  follfjwin::  ia  the  romposition  at  hltxck'tkiiA  white  pepper,  accord- 
ing til  Pelletier  *  and  Lueii  t :  ~ 

I 

I  •  Auit.  de  Cttlio.  et  dt  Phyi.  xr.  941.  t   S:liw«rti«.  rhArm.  TabellA 

I  A  A     3 


S5d 


PEPPER,  AND  ITS  ADULTERATTOXS. 


BUck  I'epper 

[PcllcUvrX 

WliltePii>per(Luc&). 

Acrid  .«oft  resin. 

Acrid  re«in      -        -        - 

16-60 

Volatile  oil. 

Volatile  oil      - 

1-61 

PifiieriDe. 

Exiractive,  gum,  and  salts 

12-50 

Extractive. 

Starch             ... 

18-dO 

Guin. 

Albumen        -        .        - 

2-50 

Baaaorin. 

VVooily  fibre 

2900 

Starch. 

. 

Waler  and  loss 

19-29 

Malic  acid. 
Tartaric  acid. 

100  00 

Polasli,  calcareous, 

and  mairnesU. 

SnlU. 

WrM.dy  fibre. 

In  Lucii's  annl^'sis  the  pipt^riuc  is  pruTiably  Jucluded  in  the  resin. 

The  Tftin  in  very  acrid,  bolubk  ui  alc^'bol  and  etbt;r,  but  not  in 
Tolatilo  nib 

The  volatile  ail  has  the  odour  and  taste  of  pepper.  Its  specifio 
gravity  )5  0-9932. 

Piptrine  \^  a  crystallisable  substance ;  the  crystals  being  rhombic 
prisms  with  inoUnt^d  bnses:  it  fuses  at  212°  F.,  is  inst'lubtc  in  cold 
water,  and  only  slightly  so  in  bailing*  vrattir;  it  disitolvcs  in  ulcuhol. 
from  which  piperine  is  throtrn  down  wbon  water  it  abided  ;  vlber  and 
acetic  nrid  uUn  dl!*>olve  it,  but  llie  first  h  not  so  gooil  h  »i>lvont  as 
alcohol.  It  is  ta«<telc9S  and  inodiirous :  with  slrun<!  sulpliurle  acid  it 
forms  A  blixMl-rcd  li<piid ;  nitric  and  bydrnchloric  acids  turn  it  6rst 
greeni&h-yelbiw,  then  orange-,  and  jiftcrwards  rctl. 


Stritciure  of  Pfppcr. 

Structtirf  of  the  Berrij. — 'i'he  berry  of  the  black  jjcpper  plant  pos- 
sesses a  Rtrui'ture  of  oonsideraWe  cnmplieiiti»n,  and  of  much  intercut; 
and  sinec  wilhuut  an  accurate  knowledge  of  it^  minute  or^ranisalion 
we  cannot  hope  to  be  in  a  positicm  In  detect  the  numerous  adultera- 
tions to  which  tlii?  nrticle  is  subject,  it  becomes  necessary  to  de»cril>e 
somcwhiC  minutfly  tlic  tissues  which  enter  into  its  fiinnation. 

In  a  section  of  the  berry,  two  parts  arc  to  be  diailnpuishcfl  —  an 
outer  nud  an  inner:  the  f)r.«t  is  blac-lc,  or  reddiMh-bluck  ;  and  the 
second  more  or  less  white,  hard,  and  briiilcf  except  in  the  centre  of 
the  seed,  where  it  is  frequently  soft  and  pulverulent. 

AV'hen  a  thin  vertical  sectirm  of  tlie  outer  or  cortical  part  of  the 
berry  is  exauiiiied,  by  means  of  the  micn«C"pe,  it  is  seen  tn  be  com- 
posed of  sever.il  distinct  pnrts,  each  of  which  is  constituted  of  one  ur 
more  layers  of  cells.     Such  a  section  is  reprwenled  \\\Ji^.  132. 

TTio  external  part  n\'  the  berry,  marked  a  in  the  fiillowin<»  figure,  is 
constituted  of  cells  of  im  elonjjutcd  fonii,  yilaced  verli*-jilly.  These 
cells  are  provi<led  with  a  central  cavity  from  whirJi  lines,  probably 
minute  canals  or  channels,  radiate  tuwnrds  the  circumference ;  when 


PEPPER,  AND  ITS  ADULTERATIONS. 


359 


viewed  sideways,  tliey  opp«ar  rather  more  than  twice  u  long  lu  broad; 
and  when  seen  endwayf,  they  appear  luuslly  oval  in  sba[)ef  and  but 
litlle  iun;ier  than  hroutl.  Cells  of  a  somewhat  similar  character  are 
dcscril>cd  in  the  Rci>ori  on  Sugar,  us  entering  into  the  formation  of 
tlie  epidermis  of  the  sugar  cane. 


SmUoo  of  ft  PtrrcR  Bikiiv,  (hQwInn  tho  KWnil  l»jen  of  c«llt  of  wlikh  ih*  i-ohumI 
pnrt  u  ninalUutnl.  ■ml  tlic  juttctlon  of  ttiii  mt  /  «tth  thr  (Vnlrttl  iKittinn.  g. 
Orsvn  with  the  C«m«r«  LucMa,  ltd  nii(nl(l«<1  M>  dlameten- 


Thc  eells  next  in  order»  and  upon  which  the  previously  described 
cells  rcstf  are  small,  angular,  and  dark  coloure<l ;  tbey,  fts  well  as  the 
radiat<'  cells,  are  shown  h\^g.  133. 

The  smull  ancrulnr  cells,  just  noticed,  do  not  appear  t4i  separate 
readily  from  the  cells  whifh  occur  immediately  beneath  lliem,  and  of 
which  they  are  probably  mere  mollifications;  strictly  sjwaking,  there- 
fore, they  ou«;ht  to  be  considered  as  I'uraiing  part  of  the  layer  next  to 
be  described,  and  we  have  spoken  of  them  separately  only  for  con- 
Tenience  of  reference  and  description. 

A    A  4 


S60 


PEPPKU,   AND  ITS  ADULTliUAflOya. 


Tlie  cellfl  now  to  be  dcscnbed  aru  tvfo  or  three  timea  larger  than 
tiiQse  previously  noticed,  aud  verj  numerous,  lurming  about  half  lb» 


ntlM. 


.^^S^' 


A  portUm  of  tht  oerMx  of  the  Pirrnitt  Bkhbt.  vkwed  on  (h«  larfu*.  tKowiug  Ihf 
kIU  which  farm  tto  flnl  «ad  aeooail  lajcn.  DnvB  »iUl  Uu  Cmcrft  LocUk, 
•nd  mMpilflctt  ISudiametcm. 

thickness  of  the  cortex ;  they  are  all  more  or  less  ooloured,  and  the 
colour  deepens  aa  the  cells  ap]in>iioh  the  next  laver.  The  position  ot' 
this  second  layer  is  pointed  out  tit  h^Jlg.  132.  The  thirii  layer  is  very 
thin,  and  Is  coniijoscd  of  woody  fihre,  bundles  of  spiral  vwsseU  of  sniafl 
size,  and  formed  of  single  threads,  ;?^'.  132.  c. 

The  Junction  of  the  »ec<ind  with  the  third  luyer  la  pointed  out  by  a 
dark  line  ailufited  about  the  middle  of  tike  cortex  ;  see  Jig.  13*i.  c 

The  fourth  luyer  ta  composed  of  iniinerous  large  cells,  itnd  it  con* 
Btitutes  the  grenter  part  of  the  remaining  half  of  the  eorlex  {Jig.  \^%d). 
As  the  celU  approach  the  central  part  of  thp  berry,  they  bt'couie  much 
modified,  two  or  thrt^p  lim.'s  sniuller,  and  of  a  ileep  red  colour  (  Af- 
132.  e) ;  these  cells  might  be  deseribed  as  forming  a  fifth  and  distinct 
layer. 

The  numerous  cells  which  fttrm  the  fourth  layer  contain  a  very 
great  abundtinee  of  oil  ^lr>buk's,  and  it  is  in  it  that  the  Cd&ential  oil  of 
the  pepper  berry  is  chiefly  located. 

Tne  cells  which  form  the  fifth  and  la^t  tissue  which  enters  into  the 
composttion  of  the  cortex  of  the  pepper  berry  are  divisible  into  two 
or  three  layers,  the  outer  are  coloured,  and  the  inner  invariably 
colourless;  the  colourless  cells  present  a  reticulated  appearance,  form- 


PKrPER,  AND  ITS  AUCLTERATIOX?. 


361 


in;;  .1  triin5pArent  lamina  which  (retiuentW  si^parattfs,  as  a  distinct  tissue. 
h'ig,  132./ 

Fig-  IM. 


A  pvrtlon  oftht/oHrM  tnmina  of  tlie  cortrv  of  Piirnim  Himir.  •howin^  the  nil 
eoaUfiud  ia  UiieflaTiiln  uf  the  cclLf.  Ihairn  with  the  Cunc»  I.ucija,  uid 
tiMC«lS»d  Itm  di»in«Un. 

The  enUrnlpare  of  the  berry  or  ae«d  ia  constitutetl  nf  cells  of  large 
sixe  and  angiiliir  shape;  they  are  about  twice  as  lonu  aa  briiad«  and 
dispotwd  Id  a  radiate  manner;  in  the  outer  part  of  the  seed  tbey  nre 
■dlierent,  hnrd,  and  slonelike,  while  in  the  curitru  they  are  readily 
«epanil>]e,  and  often  (urm  a  powder  rt^senibling  tluur.  Fig.  132.  {.%  and 
Fig.  135. 

When  the  pepper  berry  is  macerated  in  viiter  for  some  hours,  th« 
oorticAl  part  apparently  separates  without  iliHicuItv  from  the  «?ed 
proper;  il',  however^  we  exiiniine  the  surface  nflliia  iTosely,  wcobwrve 
tbatitisofare<ldi:4h  colour,  and  it  becomes  evident  thai  a  portion  of  the 
cortex  18  still  adherent.  thi»  consisting  of  part  of  the  foiu*th  layer,  con* 
tainin^  much  uf  the  oil,  und  the  fifth  layur. 

It  now  becumes  tipimretit  that  the  terms  in  ooranion  use,  **  white 
pepper,"  und  '*decorlu*aled  popper,"  are  not  altogether  correct,  fur 
the  berry  i«  not  entirely  denuded  of  the  cortex,  nor  is  its  powder 
white,  for  if  a  little  of  it  b«  ditfused  through  water  on  a  slip  of  glas-V  red- 
dish particles  immediately  become  visible  :  these  are  fruj;ment<«  uf  that 
portion  of  the  cortex  which  remains  firmly  adherent  to  the  seed  itself. 

When  sections  of  the  inner  part  of  the  pepper  berry  are  immersed 


3«2 


PEPPER,  AND  ITS  ADULTERATIONS. 


in  water  for  a  short  time,  tlie^  assume  a  jrellowish  or  canary  tint,  and 
when  exaioined  with  the  microscope,  the  colour  is  seen  to  be  confined 


FOe  i». 


^r^^'tl 


I  mi 


'^  '*iT?l«^ 


ttttitmtit  the  cmfro/  forttomnl  Iht  Pkitrr  BnxT.  ihowlng  the  two  klmltof 
rrjlt  nf  wliteh  tt  I*  compcMcd,  th«  colourleM  And  ciolouml  cclU.  umI  «!•»  lu 
Jtinrtion  with  Ibo  cortex-  Dravn  w\th  the  t'Btncni  Luddft,  and  tnajpilScd  ISO 
(li«metcn- 

to  cerlnin  of  the  cL'Ua  only,  of  wliith  the  wcti'ms  arc  composed;  theae 
cells  are  rather  lurj;er  than  tlie  uniinary  ucIIb;  thej  «rv  place*!  at 
tolerably  regular  distancea  from  each  other,  and  thoy  refloat  a  deep 
yellow  colour.  In  recent  sections  which  have  not  be^^n  immersed  in 
water,  thf  celln,  which  afierwnnls  het^ome  yt-'ll'<w,  may  be  di^^iinguished 
by  a  darker  shadinv.  and  Rometiinea  bv  a  fnint  tint  of  rtdoiir.  The 
deepening  of  colour  is  dctcnnined  by  tiie  action  of  the  mUs  contained 
in  water  on  the  contents  of  these  colhs  which  differ  cheinically  from 
those  of  the  ordinary  cells. 

It  is  probfitly  in  these  coloured  cells  that  the  pipcrine  ia  located* 
Alcohnl  and  nitric  acid  deepen  the  tint  very  gretiily,  and  on  the  appli- 
cation of  concentrated  siilphurir  ncid  to  dry  scctidns  nf  tlie  pepper 
berry,  they  become  of  a  reildi^ih  hue,  (he  chanjjc  of  colour  boing 
limited,  in  the  first  instance,  to  the  i)cculinr  cells  in  question.  These 
results  of  the  use  of  9ul[ihunc  ncid  are  such  as  ensue  with  piperine 
iUclf. 


I 

4 


PEPPER,    AND    ITS  ADULTERATION'S. 


SfiS 


The  structure  nf  llie  centrnl  part  of  the  pepper  berrj,  antl  the  po- 
sition and  character  of  the  Cflnuret!  cells,  ari;  shown  mjig.  1.15. 

Now,  in  ^(lund  hluck  pepper,  all  the  stnielurcs  which  wo  huvc  de- 
scribcti  may  be  Lracecl  oui  in  a  broken  and  frugmentury  condition^ 
but  in  white  pepper  certain  of  these  tissuefl  only  exist — viz.,  a  part 
of  the  fourth  layer  of  cells,  which  eontuins  the  uil,  and  the  fifth  cellu- 
Ur  lamina. 

Before  the  observer  is  in  a  position  to  detect  the  adulterations  of 
pepper^  it  is  necessary  that  he  should  well  understand  the  appearances 
Rn<i  .-(tructure  of  j»roiunl  pepper,  l>uLh  bluck  nnd  white. 

When  black  pcp|>er  h  diffused  thrnu^li  wiiler,  little  pnrticles  of 
three  different  kinds,  intermixed  with  a  tine  powdery  substance,  are 
Tisible ;  i^oriie  of  these  nre  black,  others  reddish,  and  the  last  while; 
the  black  are  frag:inents  of  the  outer,  and  the  red  those  of  the  inner 
cortex,  while  the  white  are  the  pulverised  seed  itself.  The  white  pow- 
der i»  formed  of  (he  cells  of  the  seed,  some  united  in  two;*  and  threes, 
but  the  majority  either  sepHrated  and  entire,  or  broken  into  pieces; 


XSn   m  .iDCXXXftATlOAS. 


%km  tituy  iltoHiia  %«l  Em  hlMofad  wtdi 
«nii  fifaMi  «ataiBiBe«i  <riiii  thm 
nhiUf  p^>p«r  nu  block  tn^aoito  ought  feD  be 

praaai.  lUttftUv 
portof  tbe  berry. 
ftiMK  ndh  ocbsr,  wheiber  entiiv 

k»  ptftieks  flf  SM<  fcr  wticb 
by  penins  tfwf mted  with 

'QIW  <MMlM»  (»r  tb«w  4«llii  arw  tiUMi  vitb  •taneksnnolea  of  exccvd- 
1^  i^^iHami^  «Mi  w   ift  gruiuui  pupper,  but  of  the  oelU  are 

.liut  tNwv  ii^  2vtiiiriiit)r  a  m  Bttte  of  ■mfcciilar  moveaieiit, 
>t'  uil  nthar  this  starafc  leraaote*.  Ko 
-  H«*rrT  bveidn  dkow  j«C  deMribcd. 

•  b  outained  in  ibe  seed  or  central 

-11  tuuh;btr«)  widia  •olutioB  or  iodine 

(  cuila  Umi{{  tflected  in  tbe 


tbn^  vuttiU  bv  v<r,v  «(»«  to  bo  AM 
(bi»  tfctoi'MirKiiw  MmtfUiro  of  tbo 


U«t  HM  .VifuiiTUk&mHn  or  Pkptbi. 


Mftl^l  <-*>  ^Hir*  ff**^  ■A'^  tcoDdaliJUS  ailultenxion^  and 
I UU  uMM  ul'  ikil  tint  artioftw  pUcetl  uoder  tbe  superrisioa 


IfeMAb^ll* 


ff/Samftiea. 


Miny>^  uf  block  Mui  white  pepper  exunined  a 

UnMtd  mtal,  mmUard  husk,   wkt^ 

u»l  ^N/rpar^iu/.     To  this  list  niusi 

i.  nfvvwtlv  oitft  with  bjr  tbe  Excise  iu  Mtn|Jc9 

*  tritber  of  the  sweeping's  of 

Ic  u^i  in  imitation  of  ground 

■  ml ion  of  thut  article. 

\'<  the  following  evidence,  be- 

(4wiMUtWK  iM  .VauUviut.  iliig  ihe  odutteniiMi  of 

i   111  iit-xilv  twelve  j-etfswu  lll^ 
ultorttK-il.     "We  Mre  found  ricv. 


I 


PEPPER,   AXD    ITS   ADULTERATIONS. 


965 


I 


poUto  9tarph,  linseed  m«a1,  Chitia,  busks  of  rat^  ami  white 
roustarilt  Mfbeat,  brun  aiui  tlour,  and  jrround  pypjum  or  cry»tallijitfd 
sulphate  of  titiK'.  Tlio  stock  nmterinl  lor  ndiiherating  ncppi-r  i.i  tlie 
husks  of  ivd  aDil  white  inuatard  seeds  und  linaeei)  meat,  wuntied  up 
with  C\i\\h  '* 

Of  100  lbs.  of  an  article  seized  in  ISG'l  at  Clielmsford  as  pepper, 
2lb».  onljr  cimsinted  uf  pepper,  the  re»t  beiiijr  init^ks  of  nuiRltird, 
Cbitifl,  and  rice.  liape  ieednaM  also  been  found  in  pepper.  Mr.  (.inr, 
from  whose  evidence  we  have  before  rjuoted,  states  that  whiri;  pepper 
i^  sometime?  adulterated  with  boue  fbt»ty  commonly  cath'il  irory  dn*t. 
He  also  pave  the  foUowinjj  receipt  for  P.D :  — "  It  la  mnniifm-lured 
from  rape  or  linseed  cake,  niu^tanl  husks,  and  Cayenne  pepper." 

Some  years  since  it  was  not  uncommon  to  meet  witli  etrtijirioi pepfter- 
instnncett  of  their  oecurrence  are  tnentioiied  in  Tiionison's 
•*Annal*  of  Clientistr)","  and  also  by  Aeeuui,  in  the  seeund  edition  of 
his  celebrated  work  —  "  Death  in  the  Pot." 

Accnui  wrilcs:  "I  have  examinetl  Urge  packages  of  both  black 
and  white  pepper  by  order  of  the  Exeise,  and  have  foiimi  iheiii  to 
contain  about  l^  per  cent  of  this  artificial  compound.  Thi.H  .spurioua 
pepi»er  is  made  of  oil  eafce,  the  residue  of  ihe  linseed  fntui  wliieb  the 
oil  has  been  pressed,  common  clay,  and  a  ])oriion  uf  Cayenne  prpper, 
formetl  into  a  mass,  and  granulated  by  being  first  pressed  through  a 
sieve,  and  then  rolled  in  a  cu!<k." 

The  <"use  of  [K'pjier  affords  a  liimentable  instance  of  the  inelHciency 
of  the  Kxcii*e  in  checking  adulteration. 

On  the  Detection  of  the  Adulterations  of  Pepper, 

The  whole  of  the  adulterations  of  pepper  mentioned,  except  that 
with  the  husk  of  |>epp«rf  are  only  lobe  detected  in  a  certain  and  satis* 
faclnry  manner  by  means  of  the  microscope. 

The  characters  of  the  starch  granules  of  wheat,  rice,  and  potato, 
have  already  been  described  ;  tho-i?  of  wheat  at  p.  243.,  those  of  rice 
at  n.  !2.55.,  of  j>otalo  flour  at  p.  320.,  and  of  sapo  at  p.  325. 

The  structure  of  mvstord  and  rnpe  seed^  and  of  Cayenne^  will  be 
found  described  and  figured  under  the  heads  of  Mustard  and  Cayenne  ; 
the  meihod  of  delecting;  sulphate  of  Hme  is  given  at  p.  99. 

It  then  only  remnins  for  us  to  describe  the  structure  and  appear- 
ances ot  limeed  meal  and  o(  pea  Jlottr. 


^H  Structure  of  Linseed  Meal, 

Linseed  possesses  ii  very  lieautiful  structure;  four  coals  or  tunica 

I  enter  into  the  comiwsition  of  the  covering  of  the  »ee<l,  and  require 
description. 
'I  he  outer  coat  gives  the  polish  to  the  seed,  and  is  composed  of  a 


FEPFEB,   AND   ITS   ADL'LTEEATIONS. 

It  is  in  the  cells  which  rnrtn  litis  ttinic   thsl  tb«  macilt^  wbiclr 
linseed  yields  so  abandantlj,  on  infuiitm,  is  contAUied. 

Fig.  117. 


The  BCi'oiul  cO:tL  coiisists  of  u  siitf^le  layer  of  ec'll*>  enclosing  granular 
matt<^r ;  Iboy  atu  ot'a  rounded  loriii,  rjkI  h'.WK  tbick  wiUls. 
e  tktrtl 


Tlie 


mcmbroDe  is  composed  of  niirruw  elungatcMl  cells,  or 


PEPPER,   AND   ITS   ADULTERATIONS. 


367 


rftther  6bres,  some  hcin«  Inn^^itutlinal  arid  others  trnnsvcrse;  lliese 
give  it  a  KtriiUed  and  very  charncteriMic  appearance;  being  tirm  and 
htronji,  it  fonns  the  praiecling  tunic  of  the  seed. 

The  fourth  meinbninu  is  made  up  of  angular  cel]»»  many  of  which 
are  inure  or  less  tK^uure,  enc^lusii)"^  ma»se8  of  colouring;  mutter,  pro- 
bably of  u  rcsiniius  character,  and  which  readily  full  out  of  the  cell^,  an 
represented  in  the  fij;irrc. 

The  xubstiinctf  of  the  seed  coniiista  of  cells,  in  the  cavitfes  or  meshes 
formed  by  wlitch  the  oil  and  starch  ^runulen  iire  enclosed. 

The  oil  is  coniuinod  principally  in  ihe  outer  or  lanTC  superficiuf 
cells,  in  the  fonn  of  linlluint  and  peurl-like  irttnute  dri^pu  or  s^pliurulei*. 

Tlie  sUifch  granules  are  must  abundant  in  tiie  interior  of  the  ^rain; 
they  are  an<:ular,  mtuute,  and  two  ur  llirue  times  larger  than  ihoie  of 
the  |>epj)ereorn. 

The  whole  of  the  structures  above  described  may  be  snlisfuctorily 
"detected,  by  a  little  piitlent  investigalion,  in  the  linseed  redui-ed  to 
powder  or  nteal.  The  p^rls,  however,  most  frequently  and  clearlv 
ftcen,  are  iragmcnts  of  the  fibrous  ooat,  uihI  liltle  niujsses  of  the  seed, 
fVom  the  ed'xes  of  which,  portions  of  the  eeilulo^e  I'urmiug  the  trans- 
parent cells  project,  in  a  radiate  und  very  cliarncteristic  nmntier. 

Sf7vrtnre  of  Pea  Fluur. — I'ea  flour  resembles  very  clostly  bean  flour 
already  described  and  figured  under  the  article  Bread,  ihu  chief  diflfe- 
rence  consists  in  the  size  of  the  starch  corpuscles,  which  are  much 
smaller  in  pea  than  in  heiin  flour. 

On  the  Detection  nf  Pepjter  Huak*.  —  The  presence  of  an  undue 
quantity  of  pep|M>r  husk  in  black  pepper  may  be  ituspeeted  by  the 
■ppeiimnce  of  the  urtiele,  il^  dark  colour,  and  the  ijuunlity  of  husk 
visible  to  the  naked  eye  ;  the  only  way,  however,  in  which  this  admix- 
ture is  to  be  determined  with  certainty,  is  by  a  quuntilative  chemical 
analysis  of  ihc  «iiniple. 

It  is  not  ofinn  that  such  an  nnnlysis  ia  necessary. 

On  the  DrtectioH  if  Factitioni  Pepper  Berries. — The  suspected 
pepper  >houId  be  soaked  for  some  lime  in  water,  when,  should  it  con- 
tain artificial  peppercorns,  these  will  become  disinlo-gruled  and  fall  to 
pieces.  Their  conifK>sition  is  to  be  aacurlained  partly  by  chemical 
analysis  and  partly  by  mieroscopionl  examination. 

The  processes  for  the  detection  of  xulphate  of  iime  and  bone  f/iu/have 
already  been  described  elsewhere. 

Duty  on  pepper,  of  all  aurtJi.  is  6rf.  per  lb.,  and  5  per  cent,  thereon. 
There  were  entered  for  home  consunipiron  in  1854,  3,720,534  lbs.; 
lS6ii,  3.647,803  lbs.  ;  nine  months  of  iSfS,  2.G46,910  lbs.  It  is  evi- 
dent therefore  that  the  loss  to  the  revenue  arising  out  of  the  udultc- 
ration  of  this  single  article  moat  be  very  great. 


968  CAYENNE,   AND  ITS   ADCLTEEATIOKS. 


CAYENNE,  AND  ITS  ADULTERATIONS. 

Cayenne  Pepper  con5i?«ts  of  the  pofla  or  seed  TeneU,  ground  sol  rr- 
diiced  to  powder,  of  (lifll'r*.'nt  species  of  Cupsiatm^  but  p ri n cijw !I»  "* 
C  annuum^  and  C  frutettcens ;  the  Inlter  BjHTcip?,  heinsf  strtmfw  ifri 
better  flavaupcd,  yields  the  best  demrripiion  orC'iiyonne  pop^wr 

The  [lenus  cap$ieuni  hehinfrs  to  t)i«  SoUtnacta:  or  nightsha'Jf  fanU'r. 
which  nliHi  iiu-ludes  ihe  potato  phtnc. 

Capsicum  tinnNum  h  &  mittve  of  America,  but  is  cullivti«d  in  tk 
Wc9t  and  KttSt  Indies  And  to  Bomo  citent,  m  grucnhotues,  in  En;* 
land  and  other  Eiirop<'an  countries. 

It  18  nn  Qnniial.  herbaceous  plnnt,  Rud,  acoordinv  to  M 
**one  oi*  llie  hardiest  aiul  most  productive  pUnts  found  i  ■ 
climntes,  f^rowtng  luxiiriantlv  in  almost  nil  drr  tt^ils,  howevvr  imiifif 
rent.'*  In  this  country  it  Bowers  in  July,  and  ripens  it*  pr*^  in 
Oftdber ;  when  immature,  the  berries  are  preen,  and  only  ^(taallf 
beoome  re<l  as  thev  prow  ripe;  they  ore  used  Imrh  in  the  greirti  aaJ 
red  states,  and  in  the  undried  and  dried  conditions:  in  rbe  rmni 
state  they  are  emj)l()yed  for  pickling  :  when  dried  they  are  uw!  ta 
medicine  :  and,  reduced  to  ponder,  they  constitute  Car<niiie  pef^- 

The  dried  berries  ordinarily  sold  as  ckiUien  are  of  this  spfvia:  in 
this  condition  they  are  more  or  less  shrivelled,  oblon«,  broad  it  l^ 
di.-ttal  extremity,  the  calyx  and  stalk  bein|g[  usually  ndbertmt  tolk# 
broad  end.  They  vary  very  much  in  size  and  form  ;  the  larjrrtisn 
two  or  three  inches  long,  and  at  the  base  Are  An  im  h  or  more  widf; 
they  are  distinguifthcd,  according  to  their  siec  and  shape,  intoltff 
podded,  short-pmlded,  und  hcart'-ihapcd. 

Tlie  pods  of  this  capsicum  are  hot  and  pungvnt,  but  ikey  hartv 
aroma. 

The  pods  of  Capaicnm  fnitetcetu  constitute  what  is  known  atjf'— 
or  bird  pepprr,  and  when  proiind  they  furnish  the  best  descripu**' 
Cayenne  p*?pper.  They  are  small,  scarcely  an  inch  in  length,  sTm 
or  two  broad,  and  of  a  deep  oran^-red  colour.  Koch  bernr  saciVB 
usually  about  a  dozen  Battened,  rcniform  seeds. 

The  pfxU  are  hotter  and  more  fiery  than  tliose  of  C  anmmm;  Aff 
are  likewise  to  some  extent  aromatic. 

Two  other  species  of  Capsicum  have  been  deDominatod,  trcn  ^ 
form  of  the  fruit.  Cherry  chtUy  or  Chei^y  P^PP^ — Cap$iff%m  etM^ 
/ortne,  and  Sell  pepper  or  Captieum  grvswm* 

Composition  of  Cayenne. 

The  composition  of  capsicum  berries  is  shown  m  the  foUonlf 
analyses  made  in  the  years  1816  and  1817: — 


CAVENNE,  AND  ITS  ADULTERATIONS. 


:i69 


Bucholx'4 

Anal  tf  wis.* 

(18160 

Acrul  sofl  resin  (capsicin) 

. 

-       40 

Wax       .             - 

. 

-       7-6 

Bitter  aromatic  extractive 

. 

-        8-6 

Extraetite  with  some  gum 

. 

-     21-0 

Gum       -             -             - 

. 

-       9-2 

. 

-       3-2 

Woody  fibre       - 
Water    - 

- 

-  28-0 

-  120 

Loss 


6-4 


Fruit  of  Cajmcum  annuum,  witbout  seeds        -  1000 


BraeonmCs  Analym.^ 

(1817.) 

Acrjil  oil             -             -             -             - 

•       1-9 

Wax  with  red  colouring  matter 

-       0-9 

Brownish  starchy  matter 

-       90 

Peculiar  gura      -             -              -              - 

-      6-0 

Aiiimalised  matter           -              -             - 

-      50 

Wootly  fibre       ...             - 

.     67-8 

SalU:  citrate  of  potash  6*0 

Phosphat  c  of  potash,  and 

-       S-4 

Chloride  of  potassium      3-4 

Fruit  of  Capxicum  aiutniim 

-    1000 

Of  ft//i»iW«,  the  active  principle  of  Cayenne,  Pereira  gires  the 
following  account:  — 

"Obtained  by  digesting  the  alcoliolic  cxtrad  in  Pther,  and  evapo- 
rating the  ethereal  solution.  It  is  a  thick  liquid,  of  a  yeltnuri.4h-rcd 
or  reudiah-brown  colour,  which  becomes  very  lluid  when  hcatt-d,  and 
at  a  higher  temperQitirc  is  dissipated  in  fumes.  Half  a  grain  of  it 
volatilised  in  a  large  room  causes  all  who  inspire  the  air  of  the  room 
to  cough  and  snee/.e.  By  exposure  to  tiir  and  light  it  solidities  ;  it  is 
decolorised  by  chlorine ;  it  is  slightly  soluble  in  wnter  and  in  vinegar^ 
but  very  much  so  in  nlcohol,  ether,  oil  of  turpentine,  and  the  caustic 
alkalies;  with  baryta  it  forms  a  solid  acrid  combination." 

Structure  of  the  Capnicmn  Berry  or  Fruit. 
Each  capsicum  berry  is  made  up  of  three  parts — an  outer  skin  or 
epidermis,  parenchyma,  and  seeds. 


•GaellD,  HaDdb.d.Chnc.  U.  1310. 


t  Aqti.  de  Chlm.  Fhyi.  wU  in. 


S70 


CAYENNE,   AND   ITS  ADCLTE  BAT  IONS. 


The  epidermu  contirtM  of  flnttoncd  cells,  tortuoiu  and  Rncoltf 
in  form.  Viewed  on  the  outrr  or  upper  surface,  the  bonier?  m  ike 
cells  are  been  m  be  well  defined  ;  they  are  often  four-rided ;  lb*  »»fl» 
are  ikick,  beaded  here  oiid  tbere,  the  beading  of  one  cell  eorrr^p^^- 
ine  to  tbat  of  the  conli^funus  cells  ;  lastly,  the  lines  of  juucrkm  oltitt 
cells  are  sometimes  foiinlly  indicated. 

Vicwecl  on  the  inner  surface  the  cella  appear  less  aiijrutar,  but  m"* 
tortuous,  the  walls  broader,  and  much  more  beaded,     ^i^.  U8. 

When  frnffmcuts  of  tbc  epidermis  arc  seen  inimcr»od  in  »»l«. 
numerous  oilglaliides  of  a  det^p  and  beautiful  oninj'i.'-red  colour  ir» 
visible;  some  of  these  are  imbedded  in  the  cavities  of  thecclKt*' 
the  majority  doat  fieely  in  ibc  surrounding  wuter. 

These  scverid  Btructurul  particulars  are  well  sliown  in  the  follo*^ 
engraving. 

Fie.  ia«. 


UriDEUlM  af  CANimii,  DUlt-r  ■nit  Innrr  nirfhm.    Hafniawt 


In  the  ne.xt  two  figure.*  the  general  nppi'iirnnce  prcscn: 
epidermis  on  a  more  superficial  uxnmimaion  is  exhibttrd,  t 
details  being  oiuittod. 

The  /mrrtifAym«,  which  unites  the  80cd«  with  each  other,  i»4i^ 


whole  with  the  epidermis  and  peduneJe,  U  likewise  comfmaod  ofe^} 
ihe^  are  of  a  rounded  or  oval  form,  the  porietcs  arc  thin,  swl  l**J 
cavities  usually  contain  a  very  lar^^e  quantity  of  oil,  in  th»   ■ 


CAYENNE,  AND   IT9   ADULTERATIONS. 


371 


lonumcrable  droplets,  maiiT  of  uonsiderable  size,  and  which  impnrt  to 
this  objecr,  viewed  under  the.  mIcrt>scope,  a  rerv  beuutiful  nppeurunce. 
Fig.\4l. 


Ftg.  m. 


Aft«<n)mt«tf  Ui«  vMoKWof  UwcmpriBwm  bwry,  Tliwid  on  Hi  •otn  nxtkm. 


Fi^.  142.  represents  a  seelion  of  the  cortical  portion  of  the  poil. 

In  the  ieed^  two  parts  —  ih«  covering  of  the  seed  and  the  seed  itself 
—  require  to  be  dcscribciK 

Th«-*  coverinj?  of  the  *eod  possesses  a  very  peculiar  structure,  which 
it  is  difficult  fully  to  undcMtAiid.  and  th(.*reforc  not  ea-ty  to  dejirribc 
accurately.  It  is  of  a  bright-yellow  colour,  and  of  CI>n^ide^able  thick- 
new.  Viewed  under  the  mirrownpe,  its  outer  gurfuoc  presisnts  a  cel- 
lular texture,  the  marpins  of  whiit  appear  to  be  ihe  €!ell'i  bi'inj^  thick 
and  tortuouSf  and  the  cavities  dark  an<t  deiiressed,  as  though  tliey  were 
rather  apertures  than  the  hollow  interiors  nf  the  cells. 

Vertical  nectioni^  of  lhi«  covering  pn»sent  a  very  ninfridiir  appear- 
ance. In  this  view  it  appears  as  thoujfh  cumpoited  t>f  a  number  uf  tooth- 
like processes,  having  a  suraewhat  nirliute  di^ipOAiiion,  with  intervals 
between  each  prtx-e.^,  the  pointa  or  summits  of  the  teeth  ending  in 
very  minute  huok-Uke  hpines,  the  points  of  these  beinj;  lost  in 
a  inin  membrane  A^rming  the  external  covering  of  the  seed.  It 
ap[>ears  that  these  tuuth-likc  processes  really  cutuist  of  the  thiokeaed 

B  B  2 


873  CAYENNE,    AND   ITS  ADULTERATIONS. 

walls  of  contifruous  cells  (seej^.  143.);  that  fliis  is  reallyso  w 
from  an  examination  of  the  upper  of  the  two  sketches  on  tbc  Mini 
the  section  of  the  vccU  ;  thcjr  arc  best  developed  at  the  exlrcjuuy  cf 
the  seed. 

Fig.  140. 


The  seed  proper  conBiBts  of  minute  lingular  cells,  having  thidl'^ 
colourless  parieteii ;  their  cavities  arc  51  led  with  moleculei  and^ 
bules  of  oil  of  a  yellowisbor  reddisb-j^elluw  colour,  but  donotcM^ 
starch. 

On  tub  Adultekations  or  Caybnitk. 

Cayenne  is  subjected  to  ercn  mcyre  extensive  adalteratiMi  tM 
ordinary  pepper. 

Rendu  of  the  £jamination  of  SampUt. 

Of  Twenty-eight  Bamplea  of  Cayenne  submitted  to  mJuimyrf 
and  chemical  examination,  no  lesa  than  ticenty-four  were  ddbfiti^ 
And  Jour  only  were  genvine. 

2\if€7Uy-ttco  contained  mineral  colotring  matter$. 

In  thirtten  cases  this  con^i^red  of  r^  Uad^  whidi  waa  pnMitt 
tome  of  the  aauples  in  very  considerable  quantities,  whtl«  iatWi^ 


CAYEKKE,  AND  ITS  ADULTERATIONS. 


373 


maining  seven  samples  it  was  some  red  ferrugmouA  earth,  Venetian 
red  or  red  ochre, 

Vermilion^  or  stUphuret  of  mercury^   was    present  in  one  of  the 
Civennes. 

Six  of  the  Cavennes  consisted  of  a  mixture  ntf^ound  rice,  turmeriCy 
and  Cayenne^  coloured  with  either  red  leatl,  VeneUan  red^  or  ochre. 


ftc- 1«. 


i 


e'^ 


*.    I 


w 


(I.  nanwAirniQ  of  oiMleara  bnrj  dtuiteil  fmmedlktclr  b«fl»«th  the  cptdarmU  t 
IM  Mil*  [q  thi*  tttuatiim  m  of  «  nwrc  rouriOcd  form.  Mid  «r«  IrKtvrKd  by 
•pinl  twhU  Asd  vuodjr  flbn.    6,  the  faFcacAjnm  tnrruaadlug  tli«  wadft. 

A'ie  of  the  Cajcnnes  contained  larpc  quantities  of  talt^  sometimes 
alone,  but  mi>stljr  c<tmbinetl  with  rice  nnd  the  red  earth*  or  red  Uad. 

One  of  the  samph'fl  wa<i  adulterated  with  a  large  quantity  o(  the 
husk  of  white  muMttird  Meed. 

Lastly,  tivo  were  adulterated  with  Wee,  and  were  coloured  in  addi- 
tion, the  one  with  red  lead^  and  the  other  with  a  red  fermgiHOMs 
earth. 

The  object  of  the  use  of  reil  lead  and  other  red  culourini;  matters 
is  twofold ;    6r8l,  to  conceal  other  adulterations,  and,  second,  to  pre- 

B  b3 


374 


CAYKNNE,   AND  ITS   ADrLTERATIOX9. 


serve  the  colour  of  the  Cayenno,  as  when  exposed  to  the  light  (or  »ni 
time,  it  usually  loses  part  ol'  the  bright-r€<i  colour  which  it  «t  irf. 


Fig,  us. 


> 


> 


poneMW,  an<1  therefore  it  bec(<ni(*fl  <let«riorate«]  in  fhe  evo  *f  ^ 
purchaser.  The  red  lead,  &e.,  adiled  docs  not,  i^f  ctmtte^  pni^9 
the  colour  of  the  CaTfUiie,  but  simply  supplies  the  place  ofthAt  akii* 
it  loses  in  consequence  of  exposure. 

Salt  is  employed  fur  the  some  purpose.  This  substance  hi*  i  B^ 
markable  effect  in  brinninji:  out  the  colour  of  the  Cayeaar.  U  '^ 
howerer,  also  used  to  increase  its  wei'ihu 

The  adulteration  of  Ciiyeniiu  with  such  subslnncea  u  red  ladtfA 
mercury  U,  dDubtlps.s  highly  prejudicial  to  hcnlcb  :  it  bai  bttaMlii 
that  colic  and  parHlypis  have  bolh  been  produced  by  the  uae  of  Cif* 
enne  containinj^  red  lead. 

The  salt*  of  lead  and  mercury  are  character'sed  by  the  citfl** 
■tance  that  they  are  apt  to  accumulate  in  the  systi^m,  ami  finalrli 
produce  symptoms  of  a  very  serious  nature.     Thus,  no  matter  »•• 


CAYENNE,  AND  ITS  ADULTERATIONS. 


375 


amAll  the  imantity  of  mercury  or  lead  introduce*!  eocli  day,  the  system 
is  suro  in  tlie  end,  lilthougU  it  be  slowly  and  insidiouily,  lo  be  brought 


Fu.m. 


i 


* 


^■i^ 


rwMeal.<Mio»or(lu5MrforCArBtnrM.    Macnllvd  100  dlamclen. 

under  the  influence  of  these  poisons,  and  to  become  seriously  affected. 
The  quantity  of  red  lead  iiirroduced  into  the  system  in  adulterated 
Cayenne  is  however,  hy  no  mrutu  inconsidcrahie. 

A  case  uf  lead  poisontn<j  arising  from  the  consumption  of  Cayenne 
adulterated  with  red  lead  is  referred  to  in  the  evidence  of  Mr.  Post- 
gale  before  the  Parliamentary  Committee  on  Adulteration;  the  case 
WU8  received  into  tlniveraity  Ctillecc  Hospital.  The  man  was  in  the 
habit  of  consuming  large  ciuantities  of  Cayenne^  which,  un  being 
U»ted,  was  found  to  contain  lead. 

The  article  known  u£  soluble  Cayenne  was  stated  by  Mr.  Scanlan, 
before  the  Purlianientnry  Committee,  to  have  the  following  compo- 
sition : — '*It  contains  both  copper  and  vermilion  ;  the  copper  is  acci- 
dentally introduced  into  it  from  the  mo4le  of  prcpnmtion  —  it  h  token 
from  a  copper  still.  They  muke  u  sort  of  tincture  of  the  Cayenne 
pepper;  and  they  filter  and  pour  it  upon  a  quantity  of  salt  in  a  copper 

B  B  4 


c&TX7n»  jLBn>  m  ai>cxixratiox& 


^IW  .:i/&aA^ra«KNU  o^  Coffnme. 


by  ■>■■  if  tbe  nicraacope  :    the  strueture  of 
'•«■  ihw  I  iN  li  and  Ueir  microMopical 


f^.lM. 


<7^i^^ 


T-- 


1 


CAYENNE,   AND    ITS   ADLLTERATION8. 


377 


^ 


must  be  had  to  cheraistry.  TIic  fact  of  the  presence  of  red  earths 
may  indeed  be  aaccrlaincd  by  meuns  of  the  microscope,  by  viewing 
under  that  instrument  n  [>ortion  of  the  Cayenne:,  when  the  red  earthy 
purticlen  may  be  plainly  discerned.  To  determine  their  eumpuattlon, 
however,  chemistry  mu<4t  be  uppealeil  to. 

The  method  for  detecting  the  presence  of  red  earlbs,  and  for  their 
(lu^ntitative  delermination,  will  be  found  deembiHl  at  pp.  103.  and 
149.,  and  that  for  salt  under  tlie  head  of  annatto.  We  iiave,  then, 
now  to  dcecribc?  more  particularly  the  proceases  Co  be  followed  for  the 
detection  of  lead  and  mercury. 

On  the  Detection  of  I.,ead.  —  The  presence  of  lead  in  Cayenne  may 
bv  determined  by  simply  shaking  up  half  a  drachm  or  so  of  the  Cay- 
enne in  water,  and  adding  a  fewjdrops  of  hydrosulpburet  of  ammonium  ; 
if  lead  bf  prewnt  the  liquid  will  become  more  or  lew  dark  or  black, 
according  to  the  quuntltv  of  leud  present. 

But  it  .thonld  be  remembiired  that  irun  gives  a  g^reenish-black  pre- 
cipitate with  the  above-named  reagent;  and  therefore  it  is  not 
Quite  safe  to  trust  in  all  cusea  to  the  appearance  presented  un  the  ad- 
aition  of  solution  of  hydrosutphuret  of  auimouiuiu  U>  water  contain- 
ing Cayenne. 

It  is  be^tt^  therefore,  in  all  casea  to  proceed  as  follows  :  —  Incinerate 
loo  grains  «f  Cayenne  previously  dried  on  a  water  bath;  treat  the 
a^h  with  alMtut  half  a  drachm  of  stron;;  nitric  acid ;  heat  nearly  to  dry- 
ncMf  so  that  part  of  the  acid  may  become  di^aipaled  ;  dilute  with  din- 
tilled  water,  nltcT,  and  test  for  lead  cither  by  means  of  sulphuivtted 
hydrogen,  hydrosulphnret  of  ammonium,  or  cUe  iodide  of  potatitfium. 
When  the  quantity  of  lead  present  has  to  be  determined,  the«e  re- 
agents must  be  added  until  no  mure  precipitate  falU  down;  the  pre- 
cipitates must  be  collected,  dried,  weiglied,  and  the  red  lead  calcu- 
lated. 

On  the  Detection  of  Bixulpkuret  of  Mercury.  —  As  merenry  sublimes 
at  a  red  heat,  we  cannot  proceed  in  the  analysis  by  incineration ;  the 
solvent  must  be  added  to  the  Cayenne  direct;  and  this  advent  must 
consist  of  aqua  re^ia,  which  ia  a  mixture  of  niiric  and  hyilrociiloric 
acids,  in  the  proporlionti  of  one  part  of  the  former  to  two  of  the  latter 
acid. 

About  a  scruple  of  aqua  regia  should  be  udded  to  half  a  drachm  of 
Cayenne,  and  after  an  h(mr  or  two  a  small  quantity  of  distilled  water; 
the  mixture  must  next  be  filtered,  and  the  excess  of  acid  got  rid  of 
by  evaporation,  which  must  be  conducted  nearly,  but  not  quite,  to 
dryneas ;  a  little  water  must  then  again  bo  added,  and  the  aolution 
tested. 

The  t€«ts  employed  are  liquor  potae^tu  and  iodide  of  [mtus^ium. 
The  former  gives  a  yellow  precipitate,  and  the  latter  either  a  yellow 
or  more  commimly  a  beautiful  ncarlet-coloured  precipitate  of  biniodide 
of  mercury.  The  colour  produced  on  the  addition  of  iodide  of  potaa- 
sium  would  always  be  bright  scarlet,  were  it  not  tliat  the  presence  of 


378         CVRRY    POWDER,    AND    ITS    ADULTEUATIONS. 

orf^nic  mutter  Id  the  solution  modifies  the  ftction  of  the  test.  The 
sofutinn  of  todiile  of  potassium  should  be  adiled  in  very  minute  quan- 
tity, us  the  iodide  or  biniodide  is  readily  nnd  (dinost  instantly  dissolved 
in  an  cxceas  of,  this  rongeut;  and  it  should  be  knoivn  ihat  verr 
often,  when  the  cnlour  of  the  precipitate  is  rather  yellow  ilian  redf 
after  8t4uidin;jr  un  hour  or  two  it  will  frequently  change  to  the  cha- 
racteristic scarlet  hue. 

Cayenne  pepper,  grount!  Chili,  and  cftp)>i<:urn  pods,  are  charged 
alike  by  the  Custtuns  —  the  pepjMir  duty  of  6rf.  per  lb.  itnd  5  per  cent, 
thereon . 

We  have  not  been  able  to  procure  returns  of  the  quantities  im- 
ported. It  IS  evident  tliut  the  loss  to  the  revenue  in  the  adultera- 
tion of  this  nrtiete  must  be  very  preat.  We  have  never  heard  of  unj 
proceedings  instituted  by  thu  Excise  for  the  adulteration  of  Cayenne. 


CURRY  POWDER,  AND  ITS  ADUl.TERATIONS. 


Severai,  ingredients  enter  into  the  composition  of  curry  powder. 
The  Jirticles  of  which  genuine  i!urry  powder  of  oood  quidity  ordinarily^ 
cousidts  arc  turmeric,  black  pepper,  coriander  seeds,  Cayenne,  fenu- 
greek, earduinoniH,  cumin,  ning^r,  allspice,  and  cloves.  Of  these,  tur- 
meric forms  the  larj^est  proportion;  next  to  this  in  amount  are  co- 
riander seeds  mid  black  pi'pper  ;  Cayenne,  cardamoms,  cumin,  and 
fenugreek,  form  but  a  aiuali  portion  of  the  article;  whUe  the  ginger, 
clove«,  and  albpice  arc  in  many  cases  omitted. 

The  proiHTtics  nnd  slrueturc  of  several  of  the  above  in<n*e<lients 
have  been  already  fully  described  and  illlustruted  ;  as  turmeric,  black 
pepper,  Caycuiic,  giUf;er,  cluves,  and  allspice ;  it  thus  oidy  remains  to 
give  a  description  of  the  other  ingredients  which  enter  into  the  com- 
position of  curry -powder — namely,  coriander  seeds,  cardamoms,  fenu- 
greek, and  cumin  seeds. 

Coriander  Seeds. 

Coriander  {Coriandriau  soticurn)  belongs  to  the  natural  family  Um- 
belliferie ;  it  is  an  annual  plant  of  a  foot  or  a  f(H)t  nnd  a  hulf  in  height ; 
it  is  cultivate<l  in  Ksaes,  and,  although  nut  rcully  indigenous,  is  fre- 
quently met  with  growing  wild  jn  the  neighbourhood  of  Ipswich 
and  some  parts  of  Ls5ejc. 

Tlie  fruit  or  seed  vessels  are  globular,  about  twice  the  sixe  of  white 
mustard  seeds,  and  of  a  light-brown  colour.  Kuch  i'ruit  consistfl  of 
hemispherical  portions  termed  thericarps^  each  of  which  is  a  seed  ; 


CURRY    POWDER,  AND   ITS   ADULTERATIONS.       379 


each  mericarp  exhibits  un  Us  outer  surface  five  primary  ridges,  vrbich 
are  depresse*!  anil  wavy,  aini  four  secondary  ridgvs,  whirli  are  more 
prominent  and  straigbt.  Tbc  channels  are  without  receplflcie«  for  the 
essential  oil,  or,  as  they  are  Itfiliiii^^ally  termed,  vittee;  but  near  the 
commiMures  in  each  merii'nrp  then*  i:<  a  sinuU  vittii,  so  that  each  fruit 
18  providi'tl  with  four  of  these  receptacles. 

The  epldermia  or  husk  is  thick  and  brittle;  when  examined  with  the 
inicro:;C»pe^  it  is  observed  to  consist  of  narrow  fibres,  which  cross  each 
other,  and  »re  ditjpo^ed  in  a  waved  manner,  ll  is  united  to  the  seed 
by  tueiuis  of  luoite  cellular  (issue,  the  cavities  <}f  the  cells  l>eing  empty. 
Od  the  removal  of  the  husk,  these  cells  are  turn  thruugh,  ^OIlle  re- 
maining; attacheil  to  it,  and  the  rest  U)  the  surfncc  of  the  seed.  After 
the  scnaration  nf  the  hu^sk,  the  seed  is  still  of  a  brown  colour.  Beneath 
the  colts  above  described  succeeds  a  delicate  fibrous  membrane ;  and 


Fig.  M». 
Ta4SiTKiu>  flicnov  or  UKaiCAar  or  CokJAViuut. 


•  d,  flbres  fitrmbic  ttM  ttuak.    ft,  Um  Ioom  wlb  which  aoHa  the  bluk  to  (Im  Ncd. 
r,  lite  \*ytT  tif  (Iraplr-oolunrMl  mlU,  In  caatMit  with  the  wKtA.    •'  4  ctlU  com- 

next  to  this  is  a  Inyer  of  deeply -coloured  cells,  which  merpe  into  x\w 
cells  which  form  tlie  subatance  of  the  seed ;  these  are  anguhur,  with 


880         CUBUY    POWDER,    AND    ITS   ADULTERAT10K8. 


well-dtifinerl  puietes,  their  cftrities  enclosing  oil  in  a  molecular  con- 
ditinn.     TUe  inuture  «eed  does  not  contain  starch.     Fig.  14J. 

The  peculiar  structure  of  the  busk  of  coriander  seeds  afTordit  a 
means  by  wbicb  Iheir  presence  in  curry  powder  n)ay  be  readUy  de- 
termined. 

Cardamom  Seedg,  or  Orains  of  PaTodtM, 

The  seed  vessels  or  pods  of  cardamom  are  of  a  triangular  form, 
and  consiitt  of  three  valves,  tapering  at  either  extremity  to  a  blunt 
THiiiit  :  the  inenibrane  forming  them  is  thick,  tough,  and  fibrous,  and 
IS  made  m\\  ofcellular  li»uue  and  bundles  nf  woody  fibre,  whieh  spread 
out  from  ihc  tlowor-stHlk,  and  arc  viiiible  on  the  surface  lo  the  nakeil 
eye,  impnningthe  striated  appeai'ancc  characteristic  of  the  seed  vessel 
of  cardamom. 

From  its  interior,  the  seed  vessel  sends  oST  three  prolontrations  or 
septa,  which  divide  it  into  as  many  compartments;  each  of  these  con- 
tains several  hard  seeds  of  n  reddish  brown  colour  uud  exhibiting 
upon  the  surface  peculiar  markings.  The  seeds  ore  united  tojjether  by 
a  gelatjnous  parenchymatous  suhstimce,  which,  under  the  microscope, 
is  seen  to  consist  of  numerous  delicate  tubules,  tilled  with  granular 
and  oily  matter. 

The  covering  of  the  seed,  examined  with  the  microscope,  and 
viewed  on  itd  outer  surface,  is  observed  to  consist  of  a  single  layer  of 
coloured  cells-,  much  elongated,  nnd  of  uniform  diameter,  termiuating 
in  rounded  extremities,  the  cells  bi.Mng  accurately  adapted  to  each 
other.  BoTiealh  these  are  other  cells,  which  bear  a  general  resem- 
blance in  fi»rm  tu  those  previoualv  described,  but  differ  in  beinj;  more 
irregular,  much  more  delicate,  and  iu  the  ubsencc  of  colour:  tbcj  arc 
di!>po:>cd  in  an  opposite  direction  to  tfaoftc  of  the  outer  layer.    Fi^. 

Ill  transverse  sections,  the  elongated  coloureil  cells  appear  as  small 
canals,  of  a  rounded  form. 

Lying  beneath  the  coating,  and  forming  part  of  the  seed,  is  a  single 
row  of  hirge  cells,  resembling  receptacles.  Next  in  order  from  without 
inward.s  is  a  layer  of  small  cells,  deeply  colnured.  Next  to  these  suc- 
ceed the  cells  which  constitute  the  principal  part  of  the  seed:  these 
for  the  most  part  resemble  closely  the  cells  of  pepper,  being  very  an- 
gular, but  they  differ  tn  their  more  dtdicute  and  transparent  appear- 
ance, and  in  being  minutely  dotted.     Fig,  W^.B. 

Dr.  I'ereira,  in  his  ''  Mntena  Medica,"  ipiutes  the  statement  made 
bv  Schleiden,  that  he  has  discovered  in  the  colls  of  cardamom  "  amor- 
phous, paste-like  starch."  We  find  the  cells  to  be  completely  filled 
with  minute,  distinctly-formed  starch  granules,  resembling  closely  those 
of  rice.  Probably  the  Blatcment  of  M.  Schleiden  oroee  from  his 
having  employed  but  a  feeble  luagnifying  power  in  the  cximination  of 
the  seeds. 

The  presence  of  cardamom  seeda  tn  cuiTy  powder  is  most  readily 


OtmBT  POWDER,   AND   ITS   ADtJI.TEHATIONS.        381 


iletermincd  hj  means  of  tbe  dotted  and  Angular  cells  wbioh  fonn  the 
fiabstAncc  of  the  sceda. 

Cumin  Seeds, 

The  cumin  plant  {Cuminvm  Cyminvm)  belnnpR,  like  coriander,  to 
the  natural  ordur  Unibt'IIifene  ,  in  a  native  of  Upper  EgYpt»  but  is  c.\- 
tensivelj  cultivated  in  Sicily  and  Malta. 

Fig  un, 

Ocm  KsifBiun  Avx>  Tra.vsvsub  Siortov  or  a  CAKOiiiox  8brd. 
iNicnUM  no  AlaiMim.) 


^.PorUoBof  oMttlMnbKos,  fxhlblllnc  the  iloofated  erllforwhieli  U  !■< 

pCMcd.       B,     TnUWyWM    »tctiuli    ul  «nl.        mi,    p^'llm    furitlinf   ODtu    mtnlH 

h  h,  rverpUcle-Uli*  cvD*  f.  la^rr  Mf  r<jK>uii<l  c«lli.  litt,  tr«iup«rut  and 
■nlB'iUlyiluttvd  flilli.  or  vhkb  Uu:  autuluio]  ul  Uic  aetil  lUclf  1*  Riftilc  up,  and 
which  ftfc  &Um1  wlifa  gtveh  ouipuacU*. 

Cumin    seeds    resemble    somewhat  caraway  seeds,  but    they  are 


CURBT  POVDER,  JLKD   ITS  ja>CLTEKAT1<»& 


Urger^  ■Cnugfater,  mud  o£  a  Ugbler  ealov.     The  hwt  »  JwMe,  like 
that  oToonuider  aod  all  other  ombelliferam  plaaAi,  eaaMtimt  oTtwo 
each  mqicarp  hi  ftre  /ii— j  li^ii^whidi  are 


or  merwarps 
filifiira.  lad  fonrfwiJiry  ridga^  which  «« 
/iiiBJAul  wiih  Tcrr  foe  hnn  or  pricUea, 
ri4i[c  if  a  reeeptade  or  vitta. 
Tranamae  aw<ion>  of  a  cumin  seed  ezhihit 


b«t  hothare 

■eoondary 

the  faBmaiag  stmc- 


Tbe  hairt  or  prickle*  are  compoaed  of  ecik,  the  loMr  dtaaelers  of 
wiuch  are  arranged  in  the  long  axes  of  the  hain.  The  hs^  or  eorcr- 
ing  of  the  teed  ii  made  up  of  namcroiis  rounded  or  aapdar  cdU,  in 
the  audcC  of  which  the  lar^e  and  tnaimlar  iritt»  are  citsated ;  and 
between  the  htuk  and  seed  itaeli;  then  b  naaallj  a  small  spaee,  which 
is  formed  by  the  contraction  of  the  seed  after  it  hss  arrired  at  ma- 
lority.  The  surface  of  the  seed  n  of  a  pale-bnmn  cokmr,  and  its  in- 
terior whitish  and  transparent.  The  exterior  portion  of  the  seed  is 
ron»titiited  of  elongated  and  flattened  ceUsof  a  brownish  colnnr,  while 
the  interinr  and  chief  subetanoe  of  the  seed  itaelf  is  compoaed  of  nu- 
merous distinct  angular  cdh,  the  valU  of  whM^  are  thick  and  perfectly 
transparent;  their  oonienu  conii&t  priocipallj  of  oiL  The  seeds  dio 
not  contain  starch.    .F^.  147. 

Cumin  seeds  pomeas  a  rerr  peculiar,  medicinal  twte  and  amdl ; 
and  it  is  to  these  that  curry  powder  owei  the  greater  part  of  its  charac- 
teristic flavoar  and  odour. 


I 


fenugreek  Seedt, 

The  structure  of  Fenugreek  seeds  u  very  characteristic.  The  fau»k 
of  tlw  seed  connsts  of  three  membranes ;  the  outer  it  furrocd  of  a  single 
layer  of  cellft,  which  bearn  remarkalde  resemblance  in  ^lape  to  a  short- 
necked  bottle ;  the  lonj!  diameter  of  lbe»e  celU  is  ili^posetl  TonicAlly. 
the  narrow,  neck-like  part  being  most  external,  and  forming  the  other 
surface  *tf  tlie  membrane.  The  second  membrane  consists  of  a  single 
layer  of  cells,  two  or  three  tiroes  larger  than  the  former,  very  luuch 
flattened,  and  having  their  margin*  repilarly  and  beautifully  crenate. 
The  third  and  innermost  membrane  is  made  up  of  sereral  layers  of 
large  tramparent  cA\i  filled  with  mucilage;  these  cells  expand  greatly 
when  immersed  in  water.     Fi^.  148. 

The  »ee<)  itself  consi*ilfi  of  two  lobea,  which  are  made  tip  of  numerous 
minute  cellfl ;  tho9e  in  the  outer  part  of  each  lobe  are  nf  a  roundeil  or 
angular  form,  while  those  situated  near  the  innermost  part  become 
much  elongated,  the  long  axe*  of  ilie  coll*  being  placed  transverse!? 
in  each  lobe.  Tlie  entity  seed  u  covered  by  a  single  layer  of  siuoll 
angular  cells.     Fig.  149. 


384 


CU 


RRT   POTVDEB,   AXD  ITS   ADULTERATIOXS. 


ResuiU  of  the  Eiamination  of  Samples. 
Twenty/fix  samples  of  this  article  were  eubjecied  to  »o«l;m;  "^ 
tbesc  nearly  four-Jifths  tvet-e  adulterated. 


F$g.  148. 

OOTXB  COAT  0«  Tl«TA  or  *  r««coi 
(Mi«nifl«d  !Bl>  diAmetcrt.) 


J .  Partltm  of  th«  outer  «ivc1  te^cmd  nwmliraM  MrtpfWd  off  i  ■  ■.  I 

like  «1U  1  h  f>.  crruBlr.)   rrlU  >if  woofid  m*wib#«i»e.     B.  Tt»«»-  -  . 

oolMired  otllJ  mFninf  htia.//,  the  Iwft  olb  wbMl  ftna  Ik*  T 
bnuia,  tiled  with  muelace. 


CtmET   POWDER,  AKI>  ITS  AD ULTK RATIONS.         S86 

lit  appeared 

"lat  seven  only  verepmuine, 
TliBt  nineteen  were  aauUerated. 
I'lut  grtniwi  riccy  usually  iu  very    large  quantities,  was  preeeDt  in 

nme  sainples. 

Pig.  110. 

Tbavsvmu  Sicnoy  or  Lou  or  FurtiouuiK  Bass. 

(.llMnifiMl  £»  dlKinclwiL) 


in.  tivvrof  miKll  tnirulu-  evil*  on  the  nirfaef.  I.  ranotlcit  or  anfolar  ealla. 
r.  Tna  ••me  nllt  gntluallr  bKomlnc  more  «lotic*lrd  u  tbej  kpproarh  ttM 
(after  p&rt  of  lube    <!,  ilaglt  row  uf  celli  ft>rtnlng  Uw  laoennoat  nurgln  of  lobe 


ia(  jiottito  farina  wns  delecte'l  in  oae  sample. 
Tbat  ttalt  was  present  in  right  o\'  the  snnipli'S. 
That  llie  highly  poisonous  iiiotallic  oxide,  bbd  lbad,  was  detected  in 

no  1c99  tliun  eight  of  the  sample!). 
That  in  teven  of  the  samples,  ihendulteration  consisted  of  ground  rice 

only. 
I'liat  in  one  sample,  the  adulteration  eoiiaistcd  of  ground  rice  and  «o//. 
That  in  on£  !<aiiiple.  the  adulteration  consisted  o( ground  rice  and  kkd 

That  til  three  samples,  the  admixture  consisted  ofWf  only, 

c  c 


3:36 


CCKKT   POWDER,   AND    ITS   ATJULTERATIONP, 


Thnt  in  three  samples,  the  sdulteration  consisted  of  salt  and    bbd 

That  in  three  samples,  ttie  adulteration  consisted  of  red  leap  only. 
Thiit  in  a»e  suuifilo,  the  adulltiracions  con::'ijttid  of  bci>  lead,  potato 
fariuQ  and  salt. 

The  above  results  do  not  pve  the  whole  of  tbc  adulterations  to 
which  the  t^iiiiiples  uf  *.'urry  powiler  had  been  subjected,  since  tliey  do 
not  include  tiie  ferruginous  earths  ^nhich  were  shown,  in  our  article  on 
Cayenne,  to  be  so  frequently  employed  to  impart  colour  to  that  sul>- 
stanee. 

We  hflvfl  thus  shown  that  rnrry  powder  is  mlnlteratert  nearly  to 
the  same  cxleiil,  iind  with  ingrciliiihts  etjtially  p4'rnii,-ioua  as  C'nyenne, 
Since  the  quimiity  of  curry  powderenien  nt  ii  nieid  is  so  considerable, 
US  aduUeralion  with  red  lead  is  even  more  prejudiciul  and  dangerous 
thou  in  the  ca»e  of  Cayenne.  Not  lonj:  since  we  receiveil  a  jiarccl  of 
curry  powder  from  a  surj^eon,  iiceniii[uinteil  by  the  stHlement  that 
the  person  who  hflii  partaken  of  it  haiJ  been  made  very  ill  by  it.  We 
found  it,  on  analysis,  to  contain  a  larpe  quantity  of  lead. 

The  lead  in  curry  powder  hy  nn  ilimbt^  jtenemlly  introduced 
throuji;h  the  adulterated  Cayenne  eniplnvcd  in  lis  nuinul'uctnre.  It  19 
possible,  however,  that  chromate  of  lead  may  here,  as  in  some  oiher 
cases,  be  used  to  intensify  and  render  more  permanent  the  colour  of 
the  powder. 

The  whole  of  Ihe  injp*edients  re<juired  for  making;  curry  [towder 
may  be  obiauied  id'  most  seedsmen,  and  may  be  readily  prucure«l  of 
Mr.  13 u tier,  ofCovenl  Giirden  Market. 

With  tt  conimon  pestle  anfl  niorlar  the  feeds  may  be  reduced  to 
powder,  and  thus  thf  housekeeper  may  herself  prepare  jrenuitie  eurry 
powder,  of  the  best  rjuidity,  nt  a  L-nst  of  about  "id.  per  oumH!  Since 
currv  jiowder  is  retailed  at  (u/.,  8J.,  and  even  \n.  an  ounce,  it  evi- 
dently bears  an  enormous  proBt.  Whnt.  then,  muftt  be  tbc  ^ain  upon 
the  sale  of  un  article  which  r»  made  up  [irineipjdly  o(  turmeric  powder, 
salt,  ground  rice,  und  inferior  capsicmn  berries?  nml  of  such  a  mix- 
ture many  of  the  curry  powders  purchased  ul  the  shops  almost  cutirely 
consist. 

On  the  Detection  of  the  Ad\dterattoms  of  Curnj  Poicder. 

The  adulterations  of  curry  powder,  with  the  exception  of  potato 
farina  or  starch,  met  with  in  one  sample,  being  the  same  as  those  of 
Cayenne,  the  met  hmls  for  their  discovery  iire  idso  the  same;  the  reader 
is  therefore  referred  to  the  previous  ariirle  an  Cayenne. 

The  presence  of  |>otato  starch  is  detected  by  means  "f  the  micro- 
scope ;  the  characters  of  its  granulea  are  describes!  under  the  bead  of 
Arrowroot. 

Curry  powder  is  charged  by  the  Customs,  ns  a  manufactured  oi'ticle 
onenumerated,  at  10  per  cent,  ad  vaiorem, 


TDBMERICj  AND  ITS  ADCLT£RATIONS. 


387 


TURMERIC,  AND  ITS  ADUT.TERATIONS. 

TuHMGRic  powder  consists  of  the  ground  tubers  of  a  plant  bdanging 
to  tlie  same  genus  aa  ginger,  viz.,  Curcuma  longa,  and  which  Is  exten- 
sively cultivated  iu  India  aud  China. 

Composition  of  Turmeric. 
The  composition  of  turmeric  is  shown  in  the  following  analysis : — 


Johrt^ 

Analt/tis. 

Yellow  Tolatile  oil    - 

. 

1 

Ctfrcumin     - 

. 

-     10  to  11 

Yellow  extractive    - 

- 

-     11  to  12 

Gum 

- 

14 

M'oofly  fibre 

. 

57 

Water  and  loes 

- 

7  to  5 

100 


Vogel  and  Pelhtiert  AnalysiM, 


Acrid  volatile  oil. 

Curatmin. 

Brown  colouring  matter. 

Gum  (a  little). 


Starch. 
Woody  fibre. 
Cbluride  of  calcium. 
Turmeric. 


The  word  cvrcutnin  is  applied  to  the  resinous  colouring  matter  of 
turmeric,  which  is  soluble  only  in  ether. 


Stmcture  of  Turmeric, 

llie  structure  of  the  tuber  of  turmeric  is  well  exhibited  in  the  an- 
nexeil  fijiures. 

TuriiR'rie  powder  consists  of  largp  cells;  some  of  these  are  loosely 
imbedded  in  a  rclioular  ti.fsut%  but  othr-rft^  and  these  the  mnjnrity,  arc 
quite  fr^e;  ihcy  may  be  re<:ogni^c<l  with  fa<'ility,  under  the  micro- 
scope, by  their  size  and  bright  yellow  colour. 

when  crushed^  eatrh  cell  is  found  to  contain  colouring  matter,  as 
well  as  a  number  of  starch  grunulev,  resembling  ctovely  those  of  Cur* 
cuma  arruwnvot,  already  de^rit>e<l  and  figured. 

On  the  Hpplication  of  iodine  the  cells  become  of  A  deep  blue,  and 
with  potash,  of  a  reddish  colour. 

cc  2 


MS  TUBMERIC,   AND  ITS   ADULTEBATIOKS. 

Ok  the  Adulterations  or  Tdabuuc. 
or  Fourteen  san^plfs  of  turmeric  powder  subjected  to  Mtminatka, 
two  were  adulterutod  with  yellow  ochre,  to  the  ex  tec  I  of  neirljSO 

Fig.  160. 
BBonov  or  Tvub  or  TvnMMmc 


a  a,  Cpldmnli  i  ft  l>,  trknvpannt  f«1U  i  cr.  7«11ow  mnmn  t  Hd,  M  gJnhiUir  '- 
rt*lnoiu  muars  i  /,  dotltd  (tact  t  fi,  •lo«iftt*d  otlU  of  woody  flbi*.  IJtat  M  ^t 
■iilc  o(  the  duct. 

per  cent.,  while  nearly  nil  the  other  apeciracns  contAioed  conndinAB 
quantttiei)  of  alkali,  ciirbonate  of  soda  and  potash,  added  no  dulM' 
heighten  the  colour  of  the  powder. 

Inasmuch  as  turnierio  enters  so  Urgelj  into  the  cooipiisttioa  o/***? 
powder,  mustard,  ami  some  other  condimentd,  it  lH*cauie  u«ci^>? 
to  ascertain  whether  ii  was  liable  or  not  to  sophist) cation. 

On  the  Detection  of  the  AduUcration$  of  Turtnerie. 
Tdioio  ochre  con&ists  of  oxide  of  iron  ddutcd  wi  th  chalk ;  thf  n^  ^ 


TURMERIC,   AND  ITS   ADULTERATIONS. 


389 


turmeric  powder  roust  therefore   be  tested  in  tlic  manner  already 
directed  for  the  detectiun  of  those  two  subatancea.     The  presence  of 

Fig.  l»l. 


Till*  nifniTliis  KprMmU  the  aiipfaranee  aad  chuttclenof  awmHHt  grvimd 
TwuLMic   Dnvn  with  Uw  Cimcrm  LudiU,  ud  nu^lted  SSI>  iUunel«r». 


the  ochre  is  in  general  sufficiently  indicated  by  the  colour  and  weight 
of  the  a!«h. 

Should  the  tub,  SAT  of  100  ^ain«of  the  turmeric^  contain  alkali,  as 
carbonate  of  »oda  or  potash,  we  must  proceed  as  follows :  the  alkali 
mu9t  be  dissolved  out  uf  the  aab  by  means  of  distilled  water,  the 
solution  evaporated  down  to  a  small  bulk,  and  htMited  with  excess 
of  dilute  hydrochloric  acid;  the  solution  inu«^t  now  be  diluted,  and 
the  chlorine  precipitated  by  means  of  nitrate  of  silver  ;  the  precipitate 
colle«'ted,  dried,  weighod,  tbe  chlorine  estimated  and  culculatcd  into 
carbonic  acid,  and  this  again  Into  either  carbonate  of  soda  or  potash, 
according  lo  whichever  is  present,  and  which  may  be  ascertained  by 
means  of  the  blowpipe  ;  this  gives  with  soda  a  rich  yellow,  and  with 
potash  a  violet  Uanie. 

If  the  potash  be  mixed  with  even  one-twentieth  part  of  soda,  the 
flame  will  be  yellow  in  place  of  violet.  In  this  cose  it  will  be  neces- 
sary to  proceed  as  follows :  the  hydrochloric  acid  solution  is  to  be 

cc  5 


m  ISSCMmm;  Mi  m  ItSS, 


YINEGAB,  AM)  ITS  ADULTERATIOS& 

mad  m  tke  TobtBc  prhiciple,  to  the  |jn*tm<  of  vUdk  diluted 
wHli  rwiiMe  proportions  oC  vatrr,  Ttae^ar  ove»  iu  aroHA  Mid  pva- 

TUi  idd  csiila,  Kadr  fonned,  m  nouble  n—niij  in  certain  plaBl% 
m  Snmhmma  miger  or  Uaek  dder^  Pkmmis  tkwetjU/em  or  i>Mr  frw,  aitd 
XTAuj  UfphtroMM. 

It  Buij  be  readily  generated  by  the  f«niientatioB  of  TarMms  Teget** 
ble  and  aniuul  itiUtaoeca,  c^KciaUj  the  former. 

Fur  cfiiDm<m:i*l  purpnaes  it  it  nude  from  certain  vegetable  and 
«|Mnlaou»  iiif  itinnii,  a«  ihnae  of  the  grape,  malt,  and  the  sugar  eane  ; 
but  MS\y  ir<^euble  infu^on  capable  of  jieldina  alcohol  will  also,  when 
cxpoMd  10  the  neccMarj  condition^  fnmiflh  vin^ar.    In  most 


VIXEGAB,  AND  ITS  ADULTERATIONS. 


39 1 


ftad  bldead  whenever  vinegar  ia  roanufuctur&d  on  a  lnr<re  scale,  the 
vinoilt  or  ricoholit:  fermentation  precedes  the  uc*etoiw,  HDii  the  vinegar 
ie  forniert  entirely  m  the  e]t|)ense  of  the  ulcohol. 

Jim  tbt.-  euiLVersiuii  of  iilcohol  into  aeelio  aoiil,  it  is  saidf  ought  not 
to  be  re^iiriicil  us  essfiitiiil  lo  acetifieution,  since  »onie  vegetable  and 
aniitial  infusions  become  sour,  from  the  formation  of  acetic  ncid,  with- 
out any  previous  generation  of  Hlcc»hol. 

Acetic  aciil  may  be  formed  directly  from  the  vapour  of  crude 
alcohol  or  spirits  of  wine  in  comnmuhiculion  with  the  atmosphere, 
through  cither  an  ignited  pliuintun  wire,  or  h\  moans  of  the  black 
powder  obtained  by  bfHlin;r  prato-elkloride  of  platinum  and  potash 
with  alcoliol.  In  Gerujunv,  where  the  price  of  aleulxd  is  very  low, 
vinejjar  baa  been  manufacCured  on  a  larye  scale  ou  tbis  jirinciple. 
The  pri^>cess  will  be  found  de5cnb«d  at  page  3(i8.  of  **  Food  and  ita 
Adulterations." 

Certain  ronditinna  are  eitlier  es^entiid  to  acetifieation,  or  else  pro- 
mote preatly  the  rapiddy  of  the  process;  thus  the  presence  of  atmo- 
tpherie  air  or  ortfgen  li  one  of  the  conditions  indi^peie^able  to  tbe 
change,  the  rvaifou  of  wliich  is  made  apparent  by  thu  itubjmueU  for- 
mulie: — 

One  atom  of  alcohol  consists  of 

C,  H,0-fHO; 
One  atom  of  anhydrous  acetic  acid  of 
C,  H    O,. 
Now,  one  atom  of  alcohol  nWorbs   four  atoms  of  oxypen  from  the 
air,  to  form  one  atom   of  anlivdnnis  flccfic  acid,  and  three  atoms  of 
wat«r  —  a  chan;!e  which  is  thus  ex|ilHiiici]  bv  chcmicul  livndmls. 
C^  U,  O,  and  4  O  =  C^  U,  O',  and  3  II  O; 
or  C^  U,  O  +  ll  O  ami  4  0=  11  O,  C^  H^  O,  +  2  H  O. 

Thus,  wheu  alcohol  i»  converted  into  acetic  acid,  two  of  the  atoms  of 
the  oxygen  are  directly  absorbed  to  form  lite  acid,  and  the  remainin$( 
two  atoms  convert  two  atoms  of  the  bydropen  of  the  alcohol  into 
water  ;  the  at^im  of  water  of  the  alcohol  and  the  tw(»  fresh  atoms  of 
water  pro-luced  arc  nil  retained,  and  form  a  terbydrate  of  acetic  acid. 

Such  arc  ihe  chan<rest,  by  atom,  of  alcohol  into  aeelic  acid. 

It  is  therefore  evident  that  much  of  tbc  success  of  any  process 
adopt4Hl  for  thti  manufacture  of  vinegar  will  depend  upon  tbe  manner 
in  which  the  motber  liquor  is  exposed  to  the  atmosphere — that  is, 
U|>ou  the  constant  renewal  of  the  air,  and  the  extent  of  hurface  ex- 
posed to  its  action,  the  conversiim  of  alcohol  into  acetic  acid  takinf^ 
place  only  im  the  surfiure  of  thi;  liquid. 

The  kiiowledu;e  of  the  fact  that  atnioHpberic  air  wns  indi>t[tensable  to 
Rcetific'ati<mled  to  the  adoption  in  this  country  and  in  Germany  of  what 
has  been  termed  "Me  t^Hick  vinecnr  process"  by  wliicb  the  linnid  to 
be  cOUTerted  into  vinegar  ia  kept  vonstautly  ia  motion  in  a  uirided 

cc  4 


In  tke  ssBafiMtoTf  of  cW  firm  thmve  — impiI  tfe  prams  n 
4ael«d  m  bm  vbu,  CBpaUe  at  each  boidiiii;  Iron  CJOOO  to  |Q< 
faDoMaf  wm£:  cadi  rat  k  batflilM  vieh  the  UqatA  la  be  iiidifceJ, 
•Mi  the  npprr  half  whk  bondlet  of  bin  b,  sarh  as  are  in  ««iierml  ase 
frr  bffwiOM  or  beaooM.  Tbe  pacnp  in  the  centre  eteraies  tbe  iMfaor, 
tad.  Iff  If  M  otiu  rvttlive  motiim,  dbpersea  it  m  a  flhawcr  over  ibe 
auifate  of  tkm  hml  of  birth.  an<i  in  ileaoendin;;  throus^  the  same  it  is 
aket  by  a  ani«Il  A^^r-j^niiinsr  current  of  atmospheric  air.  which,  cttforn}; 
in  rontaet  with  tl»e  omltiplied  tiirface*  of  the  tiquor  tricklin;!  thmujih 
the  twi;rm,  ftpeeflilv  oriilifies  it ;  the  whole  hein^  kept  np  to  the  proper 
llMC  by  a  atc>ain  p«rir  of  pnre  iJn  pnasinz  through  the  Tat.  The  scidi- 
lleation  is  jpenemlfv  rtini|>I(?ro<l  in  twtrntT  Harft,  but  varies  in  inrfirae 
r4l»o  li)  the  fTprfHtftion  of  l)ireh  to  ib^  won  to  tie  »ci(lt6e<t ;  xih)  tbe 
whole  operarion,  intM!h«ii>'*iil  and  rhemical,  bein^  perfonniil  by  Memm, 
no  manMAl  lat>our  of  any  kiml  \n  p'^^uired,  Ktre  the  occa«i<mal  inspec- 
tion I'f  tiie  manager  to  ascertain  when  the  proceit  is  finished. 


TINEGAR,   AND  ITS   ADTTLTERATrONS. 


n93 


Tliis  apparatus  is  ortpalilo  nf  acriJifvin;;  any  fenwjiited  lirjunr  what- 
ever, ami  even  distilled  spirit,  wilU  a  cotuplu'tc  control  over  any 
waste. 

The  process  will  be  more  clearly  comprcliended  by  an  examination 
of  the  accompanying  enprravin;;,  which  was  iniidc  from  a  model  pre- 
pared by  Messrs.  IlUl,  Evans,  and  Co.,  and  shown  at  the  Great 
Exhibition. 

The  upper  circidar  opening  in  the  aide  of  the  vat  is  for  the  admis- 
«on  of  attnospheric  air,  the  lower  is  the  termination  of  the  steam  pipe. 
It  should  be  incntlnnetl  that  the  principle  of  the  process  was  dis- 
covered rpiite  iiulcjwndently,  and  about  the  same  time,  in  Germ:iny 
nnU  in  this  country. 

A  second  necessary  condition  is  the  presence  of  a  substance  capable 
of  excitinj,'  iVTineutation  —  that  i.s  a/erment. 

In  vegetable  infusioni,  as  tluwe  ol*  the  prune  and  malt,  the  nitro- 
penised  principles  onntaine<l  in  them,  ohielly  jiluten,  act  as  thefcriniMit. 
Viiit'jjar  itself,  vinegar  yeast,  lees,  beer  yeast,  leavened  breiid,  and 
many  other  similar  matters,  all  of  which  contain  pluten,  are  capable  of 
excitinp  fermentation,  and  so  promoting  the  generation  of  acetic  acid. 
KxpL'rience  has  shown  that  the  beat  fermfini  for  indm-injj  the  trans- 
formation of  aloohol  into  acetic  acid  is  a  portion  of  rendy*uiatle  vinegar 
itself. 

A  third  condition,  which,  tbnu^h  nnl^  like  the  former,  essential,  vet 
prcHtly  hastens  the  conversion,  is  an  increased  teniperature,  vnrvmp 
con^id'e^ably  in  ditTerent  cast's,  but  sometimes  reaching  as  high  as 
100°  Fahr.  ^  • 

When  any  spirituous  licjuor  is  exposed  under  the  conditions  re- 
qtiisite  for  acetification,  the  following  phenomena  are  observed  to  occur 
in  Piiccession. 

However  clear  the  liqaid  may  have  been  at  first,  it  anickly  becomes 
turbid,  currents  or  movements  are  soon  visible  in  it ;  it  is  said,  in 
common  language,  to  be  "on  the  work."  Slimy  partidea  collect  on 
tlie  surface^  gradually  forming  a  scum,  and  which,  aHcr  a  time,  falls 
as  a  seilinient  to  the  bottom.  The  Germans  call  this  scum  *^  vinfirar 
mother,"  since  it  is  capable  of  exciting  acetification  in  fre^h  portions 
cif  liquid.  During  the  process  the  temperature  of  the  licpihl  n-^es,  and 
the  peculiar  aroma  of  vinegar  Iteeome^  diffused  in  the  surnmnding 
air;  as  B4K>n  as  all  the  alcohol  has  beconte  converted  into  acetic 
acid,  the  temperature  falls  to  tliat  of  the  atmos])here:  the  motion 
cease*,  the  liquid  becomes  clear  and  bright,  and  its  cunveraiou  into 
vinegar  is  complete. 


Tnis  DirrBVETT  Kinds  op  Visbqas  ajid  their  MA^trrAcnmB. 

The  four  principal  kinds  of  vinegar  met  with  in  commerce  are  — 
wirui  eihtgiir^  nuiU  vinegar^  swgar  vinegar,  and  wood  vinegar,     Th« 


394  yiNEGARi   AND  IT8   ADULTERATIONS. 

first  three  of  these  depend  upon  fermentation,  and  result  from  tl* 
chnnjie  of  alcohol  into  aoetic  acid:  while  wood  vinc^r  Ja  oiiUiwJ 
witlumt  the  intervention  of  fornicntatiun,  by  the  destructive  dtfUlU* 
lion  of  w<hkI- 

Not  unfre<itiently  more  than  one  subatance  it  combined  in  iW 
manufucluri:  uf  vinegar;  thus,  ntixiures  of  nialt,  com,  and  f nnr  or 
treacle  are  ac«asion:ilIy  employed  ;  in  wliich  ease  the  resulting  tiDc^ 
\g  of  cour-^e  a  eombination  of  two  or  more  kinds  of  vinejrar. 

In  some  parts  of  Kofrland  vinejjjir  is  made  from  either  wAtdt 
perry;  these  kinds  are  dlstinjruisHed  by  the  prescnre  of  nialie  »4*itl 

DifttiUed  mnegar  may  be  obtained  by  the  distillation  of  iLn> 
\inegar  ;  what  i^  eominonly  sold  however  as  this,  is  generall  ■ 
more  than  diluted  acetic  acid,  and  in  tome  cases  even  pyroh^'    u< 
Kcid. 

Wine  Vinegar^  when  pxire  and  of  pond  ntialilTi  is  tbe  bwt  descn^ 
tion  of  vinegar;  it  is  liablevhowever,  tti  adultenttinn  with  pyrolig^wwl 
aciil.  It  is  sometimes  flavoured  by  the  addition  of  wine,  »nd  • 
di.'^tinijfuJslir'd  fnmi  all  uCher  vinegars  by  the  presence  of  hitartrafte^ 
pr>ta«b,  c.dlfd  usually  tartar  nr  wine-stone  The  prescutce  rf  iW 
uleohol  inereaues  its  aroma  and  punt*enoy. 

Owing  to  the  seareilr  iind  high  price  ofFreneh  wine  vincjTir.  it  W.ni 
three  times  as  dear  in  France  as  fnrroerly,  and  it«  cons- 
to  mlulteration,  Messrs.  W.  and  S.  Kent  and  Sons,  iriipitr' 
white  wine  vine^jar,  Imve  ln-eo  indufLni  to  prepare  a  vinegar 
as  nearly  as  pnssible  the  lluvuur  and  properties  ofFreneh  win> 
We  have  examincil  some  ^|ieoitiiens  of  thi^  article,  and  firi«i 
carefully  mnniiFuctured,  perfectly  genuine,  and  of  strength  qu.. 
to  that  of  wine  viiu-par. 

Mall  Vinff^nr. — 'Ihechief  part  of  the  vinegar  made  in  thiaoooBtiyii 
prepared  from  malt,  or  from  mall  and  com,  with  or  witltout  t\xpr. 

Sugar  Vinegar. — An  exeelleiil  vinejrnr  may  be  made  fr«m  »uj»af  ;ti« 
process  is  ilescribed  lU  page  371.  of  "Food  :tnd  its  Adultcmtions.* 

A  very  pure  antl  wbule^unc  vineyar  may  also  be  preporrd  Ir^l 
solution  ofsu^fur  or  treacle,  fermented  by  the  agency  of  a  fungal  tAvrf 
"  thf.  vinegar  plant."'' 

\Vc  were  favoured  some  time  bark  by  Rtr  Fletcher,  furjwa  « 
Bromsgrovc,  with  the  following  particulars  in  rcTureaee  to  the  tinejtf 
plant :  — 

"A  few  weeks  agn  1  had  a  young  vtnegHr  plant  •enl  m?,  wttiiti* 
following  direclions:  —  'Tut  the  phmt  in  an  earthen  jar,  addtoiJ 
half  a  |>ouiid  of  the  coni-sest  moist  sugar,  und  half  a  pound  of  tw^» 
with  five  pints  «>f  milk-wnrm  water  ;  cover  it  iighily  o%er,  •out* 
keep  out  the  diii*t,  but  not  the  air,  and  then  put  it  in  a  ntcMlerAf^r  «^ 
place  ;  there  let  it  remain  seven  weeks,  not  disturbing  it  more  Clua  »■• 
can  help.  Ai  I  lie  end  of  that  time  pnur  nlT  what  i^  now  tbe  on' 
vinegar,  and  keep  it  in  well-eorked  buttles  for  use.  Again  uMla^ 
plant  the  same  quonliiy  of  water,  sugar,  and  treacle,  u  before    ^ 


VINEGAR,    AND  1T8   ADULTERATIONS. 


395 


the  end  of  the  sroond  aovcn  wcckji,  me  plan 
two  thick  pancokes,  und  thcv  may  be  caaiiy  dividei],  care  being  uken 
ntit  tu  tear  (he  old  or  new  plant.  If  the  plant  U  ex|X)sed  1o  the  coM, 
or  kept  too  lon<^  out  of  the  lirjuid,  it  will  herume  bUtk  and  die.* 

"1  liurcwith  iiend  you/'  eontinues  Mr.  Fleleher,  "a  sample  of 
vine;iiir  thus  roanurautuved.  ShouUl  the  snnijile  be  worthy  of  your 
attention,  I  will  send  ytni  a  hirper  <_jiiAHiity  of  vinejj:iir,  a  young  plant, 
and  a  sample  of  pickle.s  nmde  with  tliin  kinil  of  vine;i:Ar." 

In  a  second  loiter,  Mr.  Kltiteher  writes  :  "Thi':  plant  I  have,  was 
given  me  early  in  the  wimtr,  and  it  n(H  only  has  suppliid  mo  with 
sereral  young  plunts  fur  friends,  but  vinegar  citougb  to  hut  me  for 
yearn." 

We  have  been  given  lo  understand  that  vinegar  plantu  are  sold  In 
large  numbers  by  the  chemists  in  Alnncltester  mid  the  sniTOunding 
towns,  and  that  vinegar  is  made  in  onnsideniMc  tpjantities  by  means  of 
thcM!  fungi.  We  also  know  that  sinee  the  publioiitiou  of  tiie  fact 
that  vinegar  may  be  thus  prepared,  many  persons  have  been  led 
to  try  it,  and  for  the  most  part  with  very  Katinfactory  resulta. 

Nearly  all  vinegar-makera  supply  at  least  four  different  strengths  or 
qualities  of  vinegar,  named  re!)|H'c(ively  Nos.  24,  22,  18,  and  16,  the 
brst  being  the  strongest*  and  llie  laat  the  weakest. 

Nil.  34,  or  Standard  vinegar,  as  it  was  called  at  the  time  when  the 
Excise  levied  a  duty  on  this  article,  is  now  seldom  made;  but  when 
a  very  strong  vinegar  is  required,  the  strength  of  the  ordinary  kind  is 
raisotl  by  the  direct  adilition  of  aeetie  or  even  pyroligneous  ncid. 

No.  22  is  in  most  cases  the  strongest  vinegar  really  manufactured  ; 
the  other  and  weaker  kinds  are  noU  however,  prepared  from  this  by 
the  addition  of  certain  quantities  of  water,  but  fnrtu  separate  wort^ 
as  it  would  not  pay  to  make  a  weak  vinegar  by  the  dilution  of  a  strong 
one. 

Further,  these  numbers  do  not  indicate  ahxolnte^  but  merely  reiativB 
strengtlis,  so  that  the  vinegars  ul'  diHerent  makers  having  the  »ame 
number  vary  considerably  in  the  amount  of  acetic  acid  contained  in 
them. 

It  is  thus  evident  that,  according  to  this  system,  much  inducement 
for  sophistication  on  the  part  of  retail  dealers  is  removed,  who,  if  tliejr 
wish  to  be  supulied  with  a  |»oor  und  cheap  vinegar,  have  only  to  order 
■  cmIc  of  the  Nos.  18  or  16  vinegars  of  any  of  the  makers. 

It  is  geiienUiy  slated  that  good  vinegars,  such  as  all  Nus.  24  ought 
to  he,  Bhuuld  contain  5  per  cent,  of  anhydrous  or  pure  acetic  acid. 

The  goodness  of  a  vinegar  is  indicated  lo  some  extent  by  its  sjK-cific 
gravitv.  No.  24  vinegar  ul  good  (lUiilily  tnhould  huvo  a  specific  gravity 
of  nol'less  than  1022.  No.  22  of  1020,  No.  20  of  lOiy,  No.  18of  1017, 
and  No.  16  of  101  J. 


▼mOAB,  AXD  ITS  ADCLTEEAT10X8. 


Osi   TOB   AsCLTYftATtlMn  Of  YtMWikM.. 


Tbe  ynaoftl  adakbeniiooa  of  rioe^ar  sre  wiUi  aoter,  nJphvric 
mdd  ■Dd  (vraf  Ji^por.  aad  khbcuiims  with  kcrid  iiiilwifiiiiiw,  as  chtlltes 
utdgraimg  vf  fvm£ae^  mad  •bo  witb  wii wi^gawwi  or  vetHe  adds. 

Tbe  water  m  added  to  increase  iu  mUc,  ealplittrk  acid  and  acrid 
vobaUDcct  to  make  it  p«uig«irt;  and  bomt  fi^ar  to  lestuic  the  colour 
leal  bj  dilution. 

Sone  of  the  Tinegan  9old  at  snail  hocksceiV  shop^  and  at  o^ter 
atalb,  coanat  of  litlle  eUe  than  diluted  <ul|ihuric  acid  and  water 
coloured  with  burnt  supu".  , 

Now,  tbe  law  allows  tbe  additioa  of  one  part  of  sulphuric  acid  to 
1000  of  Tuae^aTt  and  it  »  oolj  when  tbe  quantity  excee«L  that  amount 
that  it  can  be  conaidered  at  aa  ailulteratioa ;  and  tbia  it  verj  fre* 
quentl^  doe*. 

Tbe  uae  of  this  quantttr  of  sulphuric  acid  wat  permitted  on  Hit 
plea,  urged  hj  the  manafacturer,  that  it  was  necesjtary  in  order 
make  the  vinegar  keep.  That  it  is  not  requiaite  to  the  preservation 
of  well-made  rin^^r,  is  shown  hj  the  dreumstanee  that  several 
manufacturers,  especially  those  who  make  use  of  the  quick  vinegar 
prooesM,  do  not  tiaesul|4itirio  acid  at  all ;  and  yet  the  vinegar  made  by 
them  keeps  perfectly  well. 

Aa  baa  already  been  iioliced.  the  same  practice  prevails  in  tbe 
article  vinegar  as  in  mu«tard  ;  no  le»  than  four,  and  even  five  qaalitiea 
ftf  vine*rar  are  made,  differing  only  in  stren^h ;  the  consequence  of 
this  system  ia,  that  if  you  buy  vinegar  at  several  different  shops,  it 
will  be  found  that  some  of  tnc  vinejrars  will  contain  two  or  three 
taneB  less  acetic  acid,  tbe  aciive  Ingredient  of  the  vinegar,  than  others, 
•Uhoitgh  the  same  price  is  paid  for  them  all.  This  sysiem,  therefore, 
sffbrda  flfreat  boilities  for  irap»itiun. 

Other  adulterations  described  in  books,  tfae  msjority  nf  which 
are  probably  of  unfrequcnt  occurrence,  consist  in  the  addition  of 
nf/rir,  hydrochloric^  and  tartaric  acids^  ainm^  tail,  spurge  jiaXy  muHard^ 
petiitory,  and  inng  pepper. 

Vinegar  is  not  untreiiiiently  contaminated  with   arsenic,  this  beii 
introduced  through  the  Aulphunc  acid  iisctl  in  its  adulteration. 

**  Tou  get  ar«cnic,"  states  Mr.  Scanlan  in  his  evidence  before  the 
Parliamentary  Committee,  "in  oil  of  vitriol  to  a  sreat  extent.  This 
arises  from  the  omploynicnt  of  pyrites  instead  of  sulphur.  Oil  <:»f 
vitriol  is  made  in  large  ijuaniittes  by  alkali  makers,  and  when  the 
price  of  sulphur  is  high  they  use  pyrites  instead;  and  pyrites  almost 
invariably  contains  arsenic.  Irish  pyrites  contains  a  cood  deal ;  but 
I  have  under^ttiKxl  that  the  Cornish  pyrites  contains  still  more.  Some 
few  years  aco  I  found  an  enormous  quantity  of  siilpburic  acid  here  in 
London.  U  finds  its  way  into  muriatic  acid  utude  fi-om  that  sulphuric 
acid,  or  in  tfae  manufacture  of  which  that  sulphuric  acid  is  employed, 


VINEGAR,   AKD   ITS  ADULTERATIONS, 


397 


and  hence  it  mnj  be  rery  miachicToiu.  A  mixture  of  muriatic  acid 
anil  »mlu  hiu  been  used  in  hrend,  and  I  bavo  seen  muriatic  acid  eun- 
taining  a  very  fearful  quantity  of  arsenic." 

The  follonrm^  evidence  in  regard  to  (he  me  of  rtrrronire  sublimate 
was  given  by  Mr.  Gay,  before  the  Parliamentary  Committee :  — 

"Corrosive  sublimate  has  been  used  tor  years  and  years  in  some 
houses,  and  not  a  cask  bos  gtinc  out  without  a  certain  proportion  of 
corrosivL'  sublimate." 

Vhuirnum,  "  Do  yf»i  believe  that  corrosive  sublimate  was  mixed 
with  tlie  vinegar  in  injurious  proportions? 

"  I  du  ;  it  wus  done  to  f-ivc  strength  to  the  vinegar.  When  the  D. 
W.  and  O.  V.  liave  been  nseJ,  the  eorroslve  sublimate  is  put  in  to 
give  it  n  tartness  nguin  in  the  mouth." 

Chairman.  "Are  theae  technit-ul  expressions  in  the  trade — O.  V. 
for  nil  of  vitriol,  and  D.  \V.  for  distilled  water?  " 

"Just  80.     Corrosive  sublitmiLe  is  oalled  *  (he  Doctor.' " 

M'liitc  or  di^tiIled  vinegar,  as  it  is  called,  is  usually  marie  with 
water  and  acetic  acid,  what  is  sold  as  sueU  being  rarely  distilled  at  all. 


Resglts  or  AxAiTSBS  or  Samtlbs. 


The  chemical  annlysis  of  Thirft/'lfiree  sninples  of  vinegar  purehased 
of  various  tradesmen  resident  in  I^ondon,  furnished  the  following 
results:  — 

IsL  That  the  amount  of  acetic  acid,  the  most  imi>ortflnl  constituent 
of  vini'gar,  varies  ^p-eittly  in  tllRerent  samples,  the  highest  per- 
centage being  5'10,  and  the  lowest  2**29,  or  less  than  half  the  first 
amount. 

2nd.  Tbiit,  nncc  the  standard  No.  24  vinegars,  submitted  to  analysis, 
range  for  the  most  pari  eonsiderably  over  four  \*vt  cent.,  vinegar 
to  be  deemed  good  otigbl  to  contain  certainly  wt  teat  than  (uur 
per  Cfnt,  of  real  acid. 

3rd.  Judged  by  this  standard,  out  of  twenty-three  samples  of  vinegar 
purchased  of  dealers  in  I..imdon.  seven  reached  this  strength,  and 
contained  from  four  jwr  cent,  upwards  of  acetic  acid ;  the  per- 
centage of  seven  of  the  vinegars  ranged  between  three  and  lour 
while  in  the  remaining  nine  the  amount  of  acid  varied  from  two 
to  three  per  cent.,  it  t>einu  in  two  instances  —  9«mplea  17.  and  19., 
the  weakest  (A'  the  whole  —  as  li»w  as  'I'40  and  2*29. 

4th.  That  twelve  samples  out  of  the  thirty-three  analyfcd  con» 
tained  no  free  sulphuric  acid  —  a  fact  affording  convincing  proof 
that  the  use  of  this  aciil,  so  objectionable  in  many  re.<t|>ects,  is  not 
necewtry  for  the  preservation  of  well-made  vinegar. 

dth.  That  in  eight  sainples  the  quantity  of  sulphuric  acid  present 
did  not  exceed  the  amount  formerly  permitted  to  be  added. 


998  VIKEGAR,   AND  ITS   ADULTERATIONS. 

6th.  That  in  the  remaining;  caws  the  arooiint  exceiMied  thU,  and  in 
some  instances  wiis  three  or  four  times  a$  great. 

The  results  of  the  analyitis  of  a  sfcond  sfrieg  of  samples.  Twenty' 
eight  in  number,  of  the  vinegar  of  some  of  the  principal  vinegar  aianu- 
faccurers,  were  as  follows  :— 

lit.  That  seven  of  the  samples  were  entirely  &ee  from  sulphuric 
actiK  or  oil  of  vitriol. 

2nd.  That  eighteen  were  atTulteratcd  with  that  powerful  and  corro- 
sive minerul  arid,  the  amount  of  which  wafi  variable,  and  often 
Tcry  consldcrnble;  from  *6;J,  the  lowest.,  to  G'02,  the  highest  quan- 
tity in  1000  prains. 

3ril.  That  two  of  the  samples  contained  it  in  very  small  quantity  only. 

4lh.  Th:ii  in  three  samples  it  wa.«>  present  in  considerable  amount. 

flth.  Thiit  six  contained  it  in  very  considerable  amount. 

tiili.  That  in  seven  samples  it  was  present  in  immense  quantity. 

7th-  TiiJit  the  acetic  acid  alsu  varied  very  considerably  in  amount 
in  dillerent  samples,  the  highest  proportion  Winp,  in  1000  );raiita 
by  measure,  56  66  grains,  or  5*60  per  cent.,  and  the  lowest,  27'63, 
or  only  2  76  per  cent. 

8th.  Thnt  in  eight  sumjdes  the  acetic  acid  was  present  in  amoont 
over  fire  per  cent.,  which  h  above  the  standard  strength. 

9th.  That  in  tweha  saniplcii  the  (quantity  exceeded yi/ur  per  cent. 

10th.  That  in  setrn  it  wjis  over  thrre  per  cent. 

11  fh.  That  in  one  the  qumitity  nfatetic  acid  present  waa  so  exceed - 
ingly  sniid)  as  tn  he  tttffier  three  per  cent.,  —  that  is,  but  little 
more  than  half  (he  ppi»|»er  stren^^th. 

Tiie  sulphuric  arid  indicated  in  the  analvsps.  is  what  is  termed 
monobydrated  sulphuric  acid,  which  is  in  f;encral  very  much  stronger 
than  the  commercial  acid :  every  part  of  the  fonner,  therefore,  corre- 
sponds to  a  much  larper  quantity  of  the  latter. 

Again,  it  shnuhl  be  imrticuhirlv  reruembered  that  the  acidifying 
power  of  the  iiiiiieral  sul|ihurto  aiid  is  very  much  greater  than  that 
of  the  vegetable  acetic  acid  :  one  part  of  sulplturic  acid  acidifies  a 
much  Urgt^r  quantity  of  a  fluid  thnn  the  sanm  amount  of  acetic  acid, 
an  that  tiie  tiu'pliuric  acid  present  in  vinegar  does  not  simply  take  the 
place  of  a  similar  rpmntity  of  acetic  at'iil,  but  reprcsenia  several  times 
the  amount  of  that  acid. 

As  in  tlie  preparation  of  acetic  aciil,  and  distilled  vinegar,  copf»er 
■till:*,  leiul,  7.inc,  or  tin  pipes  arc  Homctinies,  thiujgh  by  no  meana 
conimfihty  used,  ^iiu'gar  is  occasionally  found  (o  be  contaminated  to  m 
dangerous  extent  with  those  metuls.  As  vinegar  is  capable  of  acltng 
Tcry  energetically,  in  the  course  of  a  few  minutes,  on  most  metals, 
their  nse  in  its  manufacture  ought  to  be  strictly  prohibited:  nmiT 
fatrd  accidents  have  resulted  iVom  the  impregnation  of  vinegar  with 
metallic  poisons.  The  metal  which  is,  however,  most  frequently  found 
m  vincsar  is  iron. 


VINEGAR,   AND   ITS  ADULTERATIONS. 


399 


u 


On  the  Detection,  of  the  Aiiuiteratioru  of  Viwgnr, 

The  rc««1ieat  means  wliieh  ran  be  adopted  orwcertaining  titc  qunlity 
of  a  vinejj.ir  is  by  d<'(*?rniininfr  its  specific  jjravitv;  this  may  )h*  dnne 
either  by  iiu'rini*  nf  ihc  (irdlnnry  hydrometer,  or  efse  by  an  instnimont 
constrm.'tod  on  ibe  same  principles  hs  the  irftlaetometer  of  M.  Dinocourt 
alreatlv  described.  The  oniinarv  gravities  of  vinewars  of  the  several 
qualities  are  suted  at  p.  395.  It  will  frequently  be  iViund  that  the 
vinegars  »»h\  at  the  shops  wuigh  several  dejirees  less  than  even  No.  16. 
vinegar,  which  is  the  p(M)rcst  made,  and  the  specific  gravity  of  which 
is  usually  1015.  When  the  gravity  is  below  tbis,  the  vinegar  ia  un- 
queyttfMiaUly  adulterated  with  water. 

On  the  Detenitinntion  of  the  Acetic  Acid  in  Vinegnr.  — The  fjuality  of 
a  vinegar,  and  whether  it  is  adulterated  or  not,  can  oAcn  be  ascertained 
by  determining  the  amount  of  acetic  acid  present  in  any  sample  ;  the 
determinaliun  is  ejected  by  saturaliim  with  knoM^n  tiunnLities  of  an 
alkali. 

The  acid  may  be  first  separated  from  the  other  constituent*,  im- 
purities, or  aduitcrution^  nf  the  vinegnr,  by  distillalion ;  bi'ing  volatile, 
It  passes  off  on  the  iip[iU<:atinn  of  heat,  anil  ir  thus  procured  iini  only 
sepamti^ly,  but  aUo  in  a  inure  Loncentrated  lorm.  Thi*  ijuantity 
of  vine;.'ar  tube  emph'vcd  is  10  fninccs,  which  should  be  distilled 
almost  to  dryness,  the  acid  tditaincd  being  then  neutralised  with  alkali, 
■ad  its  amount  thus  determined, 

The  process  of  distillation,  however,  is  tedious,  and  does  not  admit 
of  easv  application,  except  in  the  labirratnry  of  the  chemist.  The 
aome  end  cnn  be  attained  by  a  different  method  :  thus  the  alkali  may 
be  added  diretrtly  to  the  vinegar.  The  alkali  usually  employed  is 
mmIa;  it  may  be  used  either  in  the  form  of  the  pure  crr>tals  of  the 
carbonate,  the  recently  ignite<t  carbonate,  which  is  preferable,  or  a 
solution  of  caustic  9o<la.  The  drie<l  carlMtnate  is  prepared  by  igniting 
the  carbonate  in  a  crucible.  The  whole  *>f  the  water  of  crysialHsa- 
tion  should  be  driven  off,  and  the  white  powder  left  heated  to  redm^ss. 

Weighc<l  quantities  of  the  soda  ahouht  be  dtasolved  in  known  bulks 
of  distillcii  water.  In  this  way  the  re-ngcnt  may  be  applied  in  even 
decimal  portions  of  a  grain. 

Further,  it  is  not  only  necessary  to  prepare  such  a  dilution,  but 
also  to  have  the  means  nl  emptoyins;  it  in  definite  minute  ipjantities, 
— an  object  which  is  effected  by  an  instrument  tt-rmcd  an  alkalinieie-. 

An  alkaliineter  is  an  elongated  and  gniduuted  ]ilu»s  tube,  terminate 
ing  above  in  two  a|)ertures,  the  one  large,  by  which  the  instrument  ii 
repleniifhed,  and  the  other  small,  an*!  drawn  out  into  a  ]K>int  to  regu- 
late the  escape  of  the  fluid  in  drnpn.  The  instrument  which  we  em- 
ploy is  one  of  GrifBn's  septimul  allcalimeters  ;  the  scale  is  marked  into 
ten  principal  divisions,  wbicli  arc  again  subdivided  into  ten  les^^er  de- 
grees or  spaces,  each  uf  which  is  denominatcfl  a  '^septem,"  from  its 
being  made  to  coatiun  seven  grains  of  distilled  water.    The  entire 


m 


VINEGAR,  AJTO  ITS   ADULTEBATIONS. 


measure,  therefore,  h<ild9,  aa  will  be  perceived,  seven  hundred  grains 
of  ilisulled  water.  * 

Jn  many  dieinical  works  wc  are  ilirccted  to  mix  a  few  drops  of; 
•Irmi^  solution  of  liLttiu!)  with  (lie  vinei^iLrf  previous  to  ii»ii)g  the  soda 
BoiuLion,  and  tu  add  thin  until  the  oulour  of  the  rcldened  litmus  is 
restored.  These  ilircctioiis  are  erroneous,  and  lend  to  serious  miscal- 
culations; for  the  liimiis  does  not  agnin  becmne  blue  until  the  salumt- 
in£  point  has  been  Inng  paaseil,  and  the  li<{uid  hafy  Acquired  a  dccide<l 
alitnlinc  reaction ;  we  thertfore  recommend  the  a|>crutor  not  to  rely 
upon  the  indication:)  nfl'orded  by  solution  of  litmus. 

Again,  we  are  ttdd  to  continue  nddin;;  ihi^  »o*\-a  solution  until  th(» 
litmus  piiper  iiniueisecl  in  the  vinejjur  feusesi  to  turn  red.  Tliere  is 
here  a  source  id'frror  equally  ureat  as  in  the  former  ca^e;  for  the  lit- 
mun  j)ii|>LT  will  1m*  reddened  lim;;  after  the  acetic  acid  has  been  neutral- 
wed,  iliiiian.sin;;  frcim  the  discnfriiged  carbonic  ftcid  of  the  itoda,  ab- 
sorhed  and  retained  by  the  lluitl. 

Tliis  liilhicy  is  punrded  against  by  repeatedly  drying,  in  the  ccinrse 
of  the  prucesfi.  the  litmus  pjipcr  hefore  the  lire  or  the  fl.ime  of  a 
candle,  when,  if  ihe  redness  be  due  to  carbonic  acid,  it  will  vanish  on 
the  applicHUim  i>f  the  hunt;  but  if  to  acetic  acid,  it  will  be  jwr- 
umneiit.  Another  means  of  ;j;uarding  against  fallacy  nrising  out  of 
the  tiresencc  of  free  carbonic  aeiil  is  to  heat  the  vinegar,  and  so 
expel  the  acid,  or  to  set  it  aside  for  a  few  liours  and  tbu:(  aU(»w  of  its 
escape.  The  saturation  ts  coinplete,  when  the  Uimu.t  pajK'r  neither 
retains  the  xli^htext  »hude  of  re<lne»s,  nor  hiks  iis  hlue  tint  in  the 
Icoet  degree  heightened,  this  latter  indiralin;;,  of  eour»e,  alkalinity. 
By  the  use,  however,  of  the  solution  of  cau.stic  ftodo,  the  source  of 
fallacy  arising  out  of  the  disengagement  of  earbonie  aciil  is  avoided. 
The  (freat  objection  to  the  caustic  solution  is,  thai  it  very  quickly 
absorbs  carbonic  acid,  and  therefore  will  not  kee[>  for  any  length  of 
time. 

Mr.  Mitchell,  in  his  treatise  on  "The  Valsifitations  of  Food,"  Btat«s 
"that  if  B  drop  or  two  of  pure  vinegar  be  placed  ujwn  blue  btmua 
paper,  the  latter  will  be  reddened  ;  but  when  driwl  before  a  lire,  the 
red  colour  disappears,  and  the  original  blue  aijain  presents  itself." 

Althouph,  from  tlie  volatile  character  of  acetic  ncid,  it  might  be 
inferred  that  thia  statement  was  correct,  we  have  yet  found  that  the 
redtiesM  produced  by  this  acid  is  not  dissipated  by  the  <legree  of  heat 
which  is  employed  to  dry  the  litmus  paper,  but  on  the  contrary  r«* 
mains  fast. 

The  strength  of  the  solution  should  be  determined  by  atom :  one 
atom,  or  1*03  of  the  recent ly-ignitc<l  carbonate  of  Rodn  corresponds  to, 
and  will  saturate  one  atom  of,  aidiydrotis  acetic  acid. 

The  soda  should  be  added  to' the  water  in  tlie  proportion  of  six 

*  Ao  hD)irovcd  «)kall(niHi>f  or  Mnhr  li  now  madr  hr  Mr.  Rriinn,  by  atuitf  ofwhldi  Ml- 
dKb  fuuiuUM  of  tbt  Mlution  aiay  be  added  wlUi  trcster  accurscy. 


TINEOABy  AND   1TB  ADULTERATIONS. 


•iOI 


equiTolcnts  to  one  hundred  groina  of  diistUIet)  water.  If  a  pound  of 
tLe  solution  be  prepared,  the  siuiie  wei<:ht  of  water  should  be  poured 
into  ii  white  ijluss  bottlv,  the  lew]  of  the  li'juid  in  the  vessel  being 
exactly  ascertained  and  luarked  i  the  bottle  should  then  be  emptied, 
the  suda  disiiolved  in  a  portion  of  the  water,  end  returned  iiitn  the 
bottle,  the  remaining  wAter  being  added  up  to  the  mark  previuusly 
oiiule^  and  any  woler  tbul  may  be  over  being  rejected. 

An  ammonia  solution  is  free  from  theobjuetionB  attached  to  the  so- 
lution of  carbonate  of  soda,  when  the  precaution  pointed  out  with 
respect  to  ihe  use  of  the  liimus  paper  is  not  strictly  observed. 

It  is  extremely  dilHcult,  however,  to  obtain  a  definite  solution  of 
ammoniii.  and  when  procured,  to  maintain  it  of  unifurm  strength. 
Mr.  GriiHn,  of  Finsbury  Square,  |)erceiviug  the  advantages  of  the 
aramoniu  dolution,  proposes  to  prepiu*e  it  in  such  a  manner  as  entirely 
to  obviate  these  objections.  An  ingenious  plan  has  betn  devised  for 
noting  loss  of  scrcngili  in  a  solution  of  ammonia.  Two  nicely-balanced 
beads  are  immersed  in  it :  the  one.  so  long  os  the  solution  ia  of  the 

firoper  strength,  remains  nt  the  botlom,  but  griidually  ascends  as  the 
itjtiid  Ijccouies  heavier;  the  other  lies  just  uniler  the  surface  of  the 
lluid,  and  of  course  emerges  from  it,  and  makes  its  &{>pearance  above, 
under  the  ^ame  circumstAnces. 

Some  experimenters  determine  the  amount  of  acetic  ac3«l  by  weigh- 
ing the  quantity  of  carbonic  acid  evolved.  This  method  requires  a 
speeiul  apfjaratus ;  and  it  is  questionable  whether,  unless  ver^  care- 
fully employed,  it  gives  such  accurate  results  ns  the  soda  solution. 

A  note  must  of  course  be  kept  of  the  quantity  uf  soda  sulutJou  used 
to  neutralise  the  vinegar:  from  this  the  so<la  must  be  calculated,  and 
from  this  a^^ain  the  acetic  acid  estimated :  — 

On  the  DetemanaHon  of  Sulphuric  Acid  in  Vinegar.  —  Sulphuric 
acid,  as  we  have  said,  is  very  commi»nly  sdded  to  the  malt  and  other 
vinegars  made  in  this  country,  istensilily  for  the  purpose  of  making  it 
keep  better,  but  also  untpietitionably  to  augment  its  strength. 

We  have  already  expressed  doubts  us  to  whether  this  addition  is  at 
all  oeceftsary  to  well-manufactured  vinegar,  since  some  makers  dis- 
pense with  it  altogether;  as,  however,  the  law  has  allowed  of  the  addi- 
tion of  a  certain  amount  of  sulphuric  iind.  the  presence  of  this  can 
hardly  be  treated  as  an  adulteration,  although  sirirtly  it  really  is  bo. 
By  it  the  acidity  of  the  vinejjar  is  not  only  increased,  but  the  cost  of 
the  article  much  reduced,  and  in  place  of  a  volatile  and  arumatic  acid, 
such  ns  is  natural  Co  the  gastric  juice,  we  are  miide  tu  consume  a  hursh 
mineral  acid,  having  none  of  these  properties,  and  in  no  way  concerned 
in  digestion. 

Several  8lat«n>ents  are  pontaine<l  in  books  which  treat  of  adultera- 
tions, respecting  the  detection  of  sulphuric  acid  in  vinegar.  Thus,  it 
IS  said  :  — 

First.  If  a  pen  be  charged  with  vinegar  containing  sulphuric  nci<], 
■nd  words  wntten  with  it,  when  dried  before  the  tire,  they  turn  black. 


^ 


»   D 


Aa  At 

whaA  mjrwt,  ve  ifcfwadovs,  it  !iecma<a.  ■Binwir^  ta 
qomtit^  of  Hil^anc  acid  m  Uie  sUte  «f  coubtBfttio«  pmeat  m  g*- 
■oxae  viaefsr.  WHb  tku  view  ve  kftve  uttlvmd  JUfawit  nmple*,  of 
1000  eratBa  ead^  of  psre  vinegar,  and  obtained  the  feUovinc  — looate 
of  HUpfaate  of  Imtju  :  —  from  KeM*a  Bordean,  61  bon&edtka  of 
mfnin;  K«ia*fl  Ko.  17^  £7  huadiedtW;  aad  from  GHbert't  piirHMg 
■itgM,  46  hmKirvdUM ;  (be  first  eon«apoiidio|:  witli  25,  tbe  kcodS 
intb  34,  and  tlie  third  vrifa  19  faundrvtUbf  of  nilpbaric  acid.  In  all 
calcttUtiona,  tberefore,  tbe  arer^e  quantitT  of  combtoed  fttlpburic 
acid  tboold  be  dedneted  from  tbe  loul  amooDt  of  that  aeid 


VINEGAR,   AND  ITS  AI>CLTEBATI0N3. 


403 


In  Romc  inittanceii,  where  very  biird  well  watent  are  used  in  making  the 
vinegar,  it  will  be  necessary  to  t«si  separately  for  the  combined  and 
iree  sulphuric  add.  Indeed,  it  is  safest  to  do  this  whenever  rigid 
accuracy  is  required. 

The  combined  sulphates  present  in  vinegars  are  derived  partly  from 
the  grain  and  partly  from  the  water  enip!oye<l.  Whether  the  acid  be 
free  or  combined  may  he  ascertained  in  the  following  manner,  if  the 
liquid  remains  acid  after  the  removal  of  the  acetic  acid  by  distillation, 
the  acidity  is  most  probably  due  to  free  sulpliunc  acid,  the  amount  of 
which  must  be  ascertained  thus  :  — 

A  given  quantity  of  the  vincprar  is  first  precipitated  with  chloride 
of  barium,  in  order  to  ^et  the  total  quantity  of  sulphuric  acid  present. 

A  similar  quantity  is  evnnorated  to  drynefts,  Inrinenitcd,  and  the 
white  ish,  after  treatment  with  a  few  drops  of  nitric  acid,  tested  for 
sulphuric  ftcid.  If  the  acid  is  in  the  eninbiiicd  state,  there  will  be  no 
dilference  in  the  proportions  obtained  in  the  two  coses. 

Further,  the  (piJintity  of  acid  containeil  in  the  vinegar  before  ind 
after  distillation  may  be  determined ;  and  if  the  results  agree,  we  ob- 
tain additional  evidence  of  the  absence  of  free  sulnhuric  arid. 

Another  way  is  to  evaporate  the  vinegar  to  tue  consistence  of  a 
syrup,  and  to  separate  the  free  sulphuric  acid  by  means  of  alcoholi 
and  then  to  proceed  to  iletermine  its  amount  in  ihe  usuid  way. 

On  the  Detection  itfChiUiea  and  other  Acrid  Subxtancea  in  Viuegar. — 
The  ppesence  of  ucrid  substances  in  viiie|jiir  may  be  readily  detected. 
A  portion  of  the  viiie^iar  should  be  evaporated  nearly  to  dryness,  and 
the  extract  tasted,  when  the  presence  of  any  pungent  substance  will 
be  plainly  reveoletl  to  the  taste. 

Oh  the  Detection  of  Burnt  Sugar.  —  Two  or  three  hundred  grains 
of  the  vinegar  are  to  be  evaporated  on  a  water  bath  to  dryness,  the 
extract  boiled  with  alcohol,  the  alcoholic  solution  evaporated^  and  tlie 
residue  tasted;  if  it  be  of  a  very  dark  colour,  and  of  a  bitter  taste, 
burnt  sugar  is  no  doubt  present. 

On  ihe  Detection  of  Acetic  aud  Pyroligneo^u  Acidg.  — It  is  scarcely 
possible  to  detect  ihe  presence  of  ncelic  aciit,  since  this  acid  is  the 
chief  constituent  of  all  genuine  rinejrar  ;  but  nyroligneous  acid  may  be 
discovered.  PyroH^eous  aci<l,  as  its  name  implies,  is  formed  by  the 
destructive  distillation  of  w<hm1  ;  and  it  usually  ]>0!ises3e.t  a  smell  and 
taste  indicative  of  its  origin  and  dependent  upon  the  presence  of 
certain  tDipuritiea,  as  creoMte,  &c.  For  the  detection  of  this  acid, 
nothing  more  is  necessary  than  to  distil  tJie  acid  from  a  portion  of  the 
viiie;;ar,  to  concentrate  this  by  redistillation,  and  (iiially  to  judge  of 
It  by  the  taste  and  odour. 

Of  certain  alleged  adulterations  of  vinegar,  as  those  with  nitric, 
hydrochloric,  and  tarLiric  acids,  it  is  iinnecesoary  to  treol,  since  we  ore 
unacquainted  with  anv  instance  of  the  use  of  those  aeid.i  in  the  adul- 
teration of  vinegar,  although  it  is  quite  po^diblc  that  they  have  bceu 
and  may  still  be  used  in  rare  instances. 

D    D   3 


k. 


404 


TINEOAB,   AND    ITS  ADCLTERATIOX8. 


Ou  the  DtttcHon  o/Bitartrate  of  Potash  in  Vimogar, — Bitartrste  of 
potash  u  a  constituent  ot'  wine  vinegar,  and  u  we  are  often  called 
npon  to  vive  our  opinion  as  to  whether  certaio  Tinegars  are  wine  or 
malt  Tine^ar^,  it  a  acre  wary  that  we  Ahoitld  be  acquainted  with  the 
method  of  detectinff  that  salt.  For  instructions  the  reader  is  referred 
to  the  article  on  \Vtoe. 

It  should  be  known  that  the  presence  of  bitartrate  of  potash  in 
Tineffar  a0brds  no  certain  proof  of  its  being  genuine,  sinc«  this  salt 
iMLj  oe  purposely  oiMed.  In  this  case,  we  must  jud^  bj  the  specific 
gravity  and  the  anima  of  the  vine<;iLr,  especiallj  when  heated,  as  well 
aa  by  the  character  and  compnsiiion  of  the  extract. 

Oh  the  Dttectioii  of  Metaliie  ImpuhiieM  in  Vinegar. — Ten  ooncea 
of  vinefnu*  should  be  evaporated  to  dryness  in  a  porcelain  capsule,  and 
the  reftidue  re<iuced  to  a  white  ash  ;  if  the  asii  be  brown  or  nut- 
ooloured,  in  place  of  white,  it  contains  iron.  The  a&b  should  be 
treated  with  a  few  drops  of  pure  nitric  acid,  distilled  water  being 
added  af^er  the  lapse  of  a  few  hours;  the  solution  should  be  filtered, 
and  a  portion  of  it  te^tted  with  sulphuretted  hydrogen.  If  it  turn 
black,  the  vinegar  most  probably  is  contaminated  with  lead;  if  dark 
brown,  with  copper  ;  and  if  yellow,  with  tin.  If  there  be  no  change 
of  colour,  it  may  be  concluded  that  no  metallic  substance  is  present. 
It  is  proper,  however,  not  to  rely  for  the  determination  of  the  metal 
|Hvsent  upon  the  colour  of  the  liquid,  but  to  test  for  that,  the  pre- 
sence of  which  is  suspected,  by  the  ap(iropriate  reagents. 

The  foHowine  evidence  before  the  Committee  on  Adulteration  by 
Mr.  George  Phillips,  will  show  bow  the  Excise  protected  tlie  revenue 
from  loss  resulting  from  the  adultenlion  of  this  article  at  the  time  a 
duty  was  levied  upon  it : — 

Mr.  MoffaU.  *'  When  there  was  a  duty  on  vinegar,  was  it  mucb 
adulterated  ?  " — "  The  taw  allowed  a  small  per-centage  of  sulphuric 
acid.     I  am  not  aware  that  it  was  adulterated  beyond  tliat/* 

Again,  by  a  return  of  the  articles  examined  for  the  Inst  twelve 
yoirs,  it  appears  that  the  Excise,  with  its  70  chemists  and  4000  in- 
•|>ectors,  exaroined  only  one  sample  of  vin^ur  during  that  long 
period. 

Now  Tine^r,  again,  is  an  arlide  which  is  constantiv  aflulterated 
in  a  Taricty  of  ways.     So  much  for  the  ciBciency  of  the  kxcise. 

The  duty  on  foreign  vinegar,  which  waa  AktL  per  gallon  during  the 
war,  is  now  au:aiii,  by  the  Act  of  19  5c  20  Victoria,  cap.  75.,  5</.  per 
gallon  (-i9thJulv,  1856). 

Imports,  in  1854,  46,560  galls. ;  in  1855,  24,105  galls.  Home  con- 
fumptioD,  in  1854,  39,564  galls. ;  in  1855,  18,983  galli. 


40S 


PICKLES,  AND  TIIEIK  ADULTERATIONS, 

To  persons  unacquainted  with  the  subject^  the  title  of  tbi«  report 
^Pickles  and  their  Adnltorations,"  mar  appear  somewhat  tiingular; 
Btid  tbcy  may  be  disposed  to  aak  —  Are  not  the  ghirkins,  cflbb&^ea, 
beans,  &c.,  which  wc  sec  in  the  bottles,  what  they  appear  to  lie  ?  And 
are  other  ve^'t^tables  than  those  cotnuionly  known  to  us  mixed  with 
the  ordinary  kinds  ?  To  these  questions  we  thus  reply  :  —  "  Ghirkins," 
on  close  exaiuination,  olleu  turn  out  to  be  but  shrivelled  or  sliced 
cucumbers;  the  *' voung  tender  beans"  to  be  old  and  tough;  the 
"cauliflowers'*  to  Imve  run  to  »ec<l ;  and  the  **  rcil  caboage"  to  be 
nothing  more  than  white  cabbajre  turned  into  red  by  colouring  mat- 
ter, as  a  dyer  would  elmngc  the  colour  of  a  dress ;  further,  that 
amongst  the  vejietablcs  not  un frequently  employed  for  the  purijoete  of 
ptckie-raaking  are  some  whirh  do  not  enter  into  the  caluulaliun  of  the 
epicure*  u  vegetable  marrowr',  —  which,  when  cut  into  i)ieccts  form  a 
very  respectable  iniitution  uf  cucumbers,  —  and  sliced  turnips,  the 
identification  of  which  would  be  apt  to  puzzle  even  a  botanist  as  well 
as  certainly  all  those  who  are  uninitiated  in  the  secrets  of  a  pickle- 
manufactory. 

But  the  adulterations  to  which  we  more  cspeciallr  allude,  and  to 
the  consideration  of  which  our  attention  will  be  particularly  directed 
in  the  following  remarks,  are  those  which  refer  to  the  (juatity  and 
composition  of  the  vinegar  used  for  pickling,  as  well  as  to  the  means 
employed  for  preserving  and  heightening  the  colour  of  green  pickles. 

In  Accnni's  culebrateii  work,  "  Death  in  the  Pi)!,"  under  tnc  head 
PoisoMOtis  PiCKU'.A,  we  obtain  tlie  following  information  in  rela- 
tion to  the  "  greening  "  of  pitkles  :  — 

**  Vegetable  substances  preserved  in  the  state  called  pickles  by 
means  of  the  antiseptic  power  of  vinegar,  whose  sale  frequently  de- 
j>euds  greatly  u]Km  a  tine,  lively  green  colour,  and  the  consuuiptiou 
of  which,  by  seafariug  people  in  particular,  is  proiligious,  are  some- 
time.t  intentionally  coloured  by  means  of  copper.  Ghirkins,  French 
beans,  samphires,  the  green  potls  of  capsicum,  and  manv  other  pickled 
vegetable  substances,  oftcner  than  is  perhap:*  ex|>ccLed,  are  met  with 
impregnated  with  this  metal.  Numerous  futal  consequences  are 
known  to  have  ensued  from  ttic  use  of  these  stimulunis  to  the  palate, 
to  which  the  fresh  and  pleasing  hue  has  been  imparted  according  tu 
the  deatlly  formula  laid  down  in  some  modern  cookery  books;  such 
as  boiling  the  pickle  with  halfpence,  or  sull'eriug  them  to  stand  fur  a 
considerable  period  in  brazen  vessels.** 

Dr.  Percival  ("Metlical  Transactions,**  vol.  iv.  p.  80.)  has  given  an 
account  of  "  a  young  lady  who  amused  herself  while  her  hiur  wai 

0  p  3 


I  acuuuui 


PICKLES,  ASD  THEIft  ▲DCXTEXAnOSS. 


iaftw 


4V  COakCi^  MOkS  BSTC 

ifc  ■  «•  fa*  hoped  tfcM  tfacT  via 
flf  Ae  wfa  fr«ai  vlacfa  ihtj  arc  ex- 


ia  ft  bcO-oMtal  cr  vopptr 


'-T0  Pidie  Ghir^mB.—BoSL  tfae 
pflt  s  pew  li  nniBwg  hot  om  vcnv  csc 

~r<»  flMfe  grprftiiR— Tftfce  ft  %ift  of  vcrdwrv  ^e  b«nc«  oT 
iHMcl-nt.  fody  povOmd.  hftir  ft  piiit  of  dMM  raegv.  «d  ft  bit 
■kn  powder.  wi4  ft  Ettle  fao^  ndc  Pot  aB  a  a  bottle,  aboke  ii«  md 
lot  k  ftand  lin  ckar.  Fm  a  ■aaU  ii  ■■pfiniifal  iMo  niiBiBfeii,  or  wfaau 
efw  yo«  wiifa  to  greea.* 

lir.£.Ratfclddincu:  'Torendo-  piekla  gtaeoi.  bad  tkcm  vilb 
halfjpeace.  or  aUoo  tbea  to  stand  idr  twearffcar  boon  io  copper  or 


*Todetecctbepr«MBeeafeopper,it  ■  oa^ii umif  tomicctbc 

pieUca,  aad  to  pour  Bqaid  awamiw.  ifilated  viik  ao  equal  htJk  mt 
waiar,ovtrtbeA  IB  a  flopped  Tial:  if  tbe  pacUeioaBtaiatbeBiBaiaM 
i|Haari>^  of  copper,  tbe  aauMmia  aiawiiwii  a  blae  coloar.'* 

Tbe  aborc  renuHu  and  qaotalioaa  eoorcy  a  soaewbat  fearfal  pip- 
tore  c»r  tbe  coKjaring  of  picklea.     It  will  be  cmr  object  to 
bov  far  the  statexnenU  made  apply  to  tbeir  preaent  oooditMO. 


Renlts  of  Amalytct  of  Samplet. 

Twenty-Aree  samples  of  pickt«*  of  difiT^rent  dcacriptioai,  indui^ng 
mixed  pickles,  India  pickltrs  frbirkios,  beans,  Chilics,  &c^  were  sub- 
jected to  a  rigorous  cbemical  exammataooi  witb  the  foUowing  re- 
•olu:  — 

1st.  That  the  Tioegar  used  for  pic^in^  is  of  a  verjf  iceak  deseri^ 
etm,  the  per-oentage  of  acetic  acid  rmn^ng  between  )*48  and 
3'dl.  It  will  be  remembered,  that  in  our  I&?t  Ke(>ort  we  stated 
that  vinegar  of  good  qmdUjf  <Mgkt  to  contain  from  four  tofite  per 
etmt.  of  fmrc  acetic  acid. 
2nd.  That  nineteen  out  of  twentr  of  the  vinegart  submitted  to 
analraU,  poor  as  tbej  were,  yet  owed  a  portion  of  their  aeidi^  fl» 
nUphurie  acid,  tbe  amount  of  which  runed  in  tbe  diflcrenl  sam- 
ples from  *38  to  2'5'2  in  the  1000  grains ;  the  largett  ^uamtitg  tf 
Ihit  add  being  detected  in  the  vinegar*  in  trhich  the  red  euNkigm 
were  pickUtl, 
Srd.  That  in  the  whole  of  the  sixteen  different  pickle*  aaalj/Med  for 


I 


PICKLES,   AND   THEIR   ADULTERATIONS. 


407 


b 


copper^  THAT  rouoKous  mbtal  wqm  discovered  in  varioui  amoimtt : 
two  of  the  samples  contained  a  small  quantity  ;  eighty  rather  much; 
oney  a  conaiderahle  quiiiuitif ;  three,  a  very  coiuiderable  qwinttty ;  in 
one,  copper  was  jiresciU  i«  highly  deleterioxu  amowU ;  and  in  two^  in 
poisonous  nmoHfits. 
4tu.  Thut  the  pickles  which  contained  the  largest  guatUity  of  copper^ 
were  those  which  consisted  entirely  of  green  vegetableSf  as  ghtrkius 
and  beans. 

Nutwithjtanding  the  atatoments  ma(ie  id  books^  some  of  which  we 
have  noticeil  at  the  commencement  of  this  Itcpurt,  when  we  entered 
ujKjn  these  inquiries,  we  felt  convinced  thalso  poisonrmsM.  metal  as  cop* 
per  was  now  rarely,  if  ever,  employed  for  tht'  mere  purpose  of  lieii;hten- 
irig  and  nrescrving  the  colour  of  green  pickl&i;  we  are  therefore  both 
6ur]irisc<l  and  grieved  ai  ilie  really  fearl'ul  character  of  the  reaulcs  to 
which  Dur  invealigiitions  liave  conducied  us.  We  trust,  however^  now 
that  conclusive  evidence  of  this  tfcantlalous  practice  has  been  adduced, 
and  that  the  public  are  put  up  on  their  guard,  a  remedy  will  be  found 
for  thitt  great  evil. 

Pickles,  (loubtlcsa,  when  properly  preparc<l,  are  not  very  difrej^tible ; 
but  wc  now  sec  that  much  of  ihe  ill  L'tTcctd  so  generally  attributed  to 
their  use,  must  result  Irom  their  impregnation  with  so  potsonoua  a  con- 
tarainatiun  a;}  copper. 

In  siome  ca«es  the  copper^  usually  ihe  svfphale,  commonly  known  as 
blue  stone,  is  added  direct  to  the  vmegar  in  which  the  pickles  are  pre- 
served ;  more  frequently,  however,  no  direct  addition  of  copper  is 
made,  but  a  sutBcient  ijuantity  of  that  motui,  in  the  form  uf  an 
acetate,  is  obtained  by  the  repealled  boiling  of  the  viiie^'iu'  in  copper 
veuels,  but  since  vin<^^  is  so  commonly  uJultemied  with  sulphurio 
a<ud,  a  sulphate  of  copper  U  generally  formed  as  well.  Thu»  it  amounts 
to  precisely  the  same  thine;  whether  the  copper  ia  added  direct  to  the 
pickles,  or  whether  it  is  taLen  from  ofl'  the  copper  utemila  employed^ 
by  the  action  of  the  acids  of  the  vinegar. 

One  ot  the  worst  features  of  this  abominiible  practice  is,  that  the 
employment  of  copper  is  wholly  unnecessary,  aa  tlie  colour  of  green 
vegetables  may  be  very  well  preserved  by  other  means,  as  by  the  uBe 
of  pure  vinegar,  and  the  ud<ltti(m  of  a  jiroper  quantity  of  salt. 

Since  then,  oa  we  have  now  proveil,  pickles  are  so  constantly 
contaminated,  and  even  rendered  poisonous,  by  cupper,  the  only 
safety  for  the  public  is,  that  all  housekeepers  should  U\ke  the  mutter 
into  their  own  hands,  and  become  themselves  the  makers  of  their 
pickles. 

It  is  in  the  vtm-gar  employe^:!  for  picklc-m&kinc;  especially  that  we 
should  expect  to  find  acetic  and  pyroligncous  acids;  the  bitter  acid 
is  usually  detectable  by  the  slight  odour  of  creosote,  fn)m  which  it  it 
almost  impossible  to  free  it.  It  is  of  importance  that  the  efl'ect  of  the 
actiou  of  Uie  sulphuric  acid  contained  in  many  of  the  pickling  vinegars 

D  D  4 


'409  PICKLES,  AND   THEIR   ADULTERATIOXS. 

OD  the  colour  of  llie  pickles  sbould  be  determined.    Our  owa  ioipre»- 
•ion  is,  thnt  it  would  be  found  to  be  injurious. 

A  visit  to  a  Urge  pickle  wirehouse,  such  as  thnt  of  Mesan.  Oo»e 
and  Kluckwell,  duriof;  the  seosoo  of  pickle  and  preserve  making,  is 
not  without  interest.  The  vast  piles  of  vcsetabLes  and  fruit  readjr  to 
ba  iort«d,  cut,  boiled,  &c.,  is  really  astonianin^. 

U  B|ipeflr»f  hmrever,  that  pickle- making  u,  to  i  great  ezteitti 
independent  of  the  seasons,  and  (hat  most  of  the  different  kinds  oiT 
pickles  may  he  made  at  any  period  of  the  year.  This  the  makers  are 
Miabted  to  do  by  keeping  a  large  stock  of  the  various  sorts  of  vege- 
tablet  Immersed  in  orine  and  packed  in  barrels.  In  some  of  oar 
largett  cstahliahmonts  many  htindreil  harreU  thus  fiUe^l  may  be  seen. 
We  are  informed  that  the  "rcaicr  part  of  these  vegetables  come  firom 
abroad :  it  is  alli.'ged  tliat  thvy  are  kept  in  brine  for  the  sake  of  eco- 
nomy, and  that  they  would  keep  for  belter  in  vinegar. 


On  the  Detection  of  the  AdutteroHota  of  PichUt. 

Pit-kling  vinegar  is  of  course  liable  to  the  same  adulterations  u 
other  vinegar.  The  processes  emplnyed  for  the  detection  of  all  the 
more  usual  adullcraiions  of  vincgnr  have  alrea<ly  been  described,  and 
it  is  not  necessary  lo  repeat  thum  in  this  place ;  we  have  then  merely 
to  point  out  the  mt*thudti  by  which  the  presence  of  copper  in  pickles 
jg  to  be  determioed. 

The  presence  of  copper  in  pickles,  bottled  fruits  and  vegetable*, 
ud  preserve?,  is  nAen  unmistakably  indicated  by  their  cohmr. 

When  the  housekeeper  preserves  these  nrticlcs,  tlioy  arc  ufiually  of 
s  yellow  colour  rather  than  green,  hut  as  exhibiti'd  in  shop  windows, 
or  purchased  of  manufucturcrs  of  lhe«;  articles,  they  ordinarily 
present  a  vivid  blui^h-grcen  colour,  more  intense  than  that  of  the 
fresh  vegetables  or  fruit.  Whenever  these  articles  are  of  u  decided 
green,  tney  will  almost  always  be  found  to  cutitaiu  copj>er;  but  when 
they  arc  yellowish  <ir  brownish-green,  copper  is  never  present. 

The  copper  is  found  usunlly  both  in  the  pickles  and  in  the  vinegar; 
and  for  its  detection  the  following  proces-^cs  may  be  adopted : — 

For  its  detection  in  pickling  vmegar,  an  ounce  or  so  of  the  vinegar 
should  be  poured  into  a  teat  gliis^,  and  in  this  a  piece  of  thick  iron 
wire,  having  n  smooth  and  polishe<l  surface,  should  be  immersed  for  a 
few  hours.  If  copper  be  present  it  will  become  deposited  upon  the 
wire,  forming  a  coating  more  or  less  complete  and  thick,  according  lo 
the  quantity  of  copper  present- 
Thin  test  may  lie  so  readily  applied  that  we  recommend  the  public 
to  make  use  of  it,  and  so  ascertain  fijr  themselves  whether  the  pickles 
they  are  using  contain  the  poison  or  not  If  only  n  very  amidl  tpian- 
tity  of  copper  be  present  it  will  be  quickly  deposited  on  the  surface 
of  the  iron. 


POISONOD8   BOTTLED   FRUITS   AND   VEGETABLES.     400 

We  have  ourselves  tried  this  simple  proceeding,  first  wilh  bftlf  an 
ouucti  of  two  vinegars  in  which  the  pickles  were  eontaiiietJ,  in  which 
much  copper  was  present ;  in  each  ca^e,  afier  the  lupse  of  lliree  or 
four  hours,  a  welUiuarketl  coating  of  copper  h:ul  furineti  upiii  tbe  iron 
ro<i.  We  next  tried  it  with  two  vinegars  previously  asceiiained  to 
contain  the  sniallest  quantity  of  copper;  in  these  cases  also,  after 
the  hipse  of  a  few  hours,  an  incrustation  of  cojiper  was  formed. 

Another  very  simptc  and  eilicient  method  is  the  following  : — 

Put  three  or  four  drops  of  the  auspeiited  vinej,'rtr  on  the  blade  of  a 
knife;  add  one  drop  of  sulphuric  acid,  and  heat  the  under  surface  of 
the  knitie  over  (he  llame  of  a  candle  ;  the  vine;;ar,  in  evaporating,  will 
deiKisit  the  copper  upon  the  iron,  if  anv  be  present. 

r'or  the  detection  of  copper  in  the  pickles  themselves,  the  annexed 
process  may  be  adopted. 

About  1000 grs.  of  the  green  vegetables  of  each  of  the  pickles,  after 
having  been  sliced  wilh  a  ffluss  knife,  are  to  be  incinerate<l,  care  being 
taken  to  avoid  every  source  of  contamination  :  the  ash,  having  Ijeun 
pulverised,  is  to  be  treate*!  witli  t20  tlrops  of  pure  nitric  acid ;  I  02.  of 
distilled  water,  after  the  lapse  of  a  short  time,  udded,  the  solution 
filtered,  and  treated  with  excess  of  ammonia.  If  copper  is  present,  the 
solution  becomes  more  or  less  blue,  according  to  the  amount  of  the 
metal  present. 

For  the  qumdUative  esfimaiioH  qf  copper  in  pickles,  we  rauat  proceed 
as  follows  : — 

3000  or  4000  grs.  of  the  pickles,  inuluding  a  fair  proportion  of  the 
vinegar,  must  be  evaporated  tu  drym^H,  then  incinerated;  the  ash 
treated  with  about  two  drachms  of  nitric  acid    diluted  with  an  ecpial 

Quantity  of  water;  the  whole  boiled  (or  a  few  minutes,  evaporateti  to 
ryness,  the  residue  diluted  with  one  ounce  more  water,  boiled  ngitin 
for  a  time,  the  solution  filtered,  and  the  copper  precipitated  by 
means  of  sulphuret  of  ummunium ;  the  sij|[)hureL  of  copper  must  be 
collected,  dried,  wei^'hed,  and  the  co])per  determined. 

Imjiort  duty,  preserved  in  vinegar.  Id.  [wr  gidlon;  preserved  in 
salt,  irce. 

Imports,  preserved  in  vinegar,  in  I8.';4,  5328  galls.;  in  1855,  3998 
galls.     Home  consumption,  in  1854,  4904  galls  ;  in  18^5,  3278  galls. 


ON  POISONOUS  BOTTLED  FRUITS  AND 
VKGKTAliUiS. 

Am  attentive  examination,  wilh  the  eye  alone,  orvanons  samples  of 
bottled  Iruits  and  vegetables,  served  to  raise  suspicion,  and  to  produce 


410     POISONOUS  BOTTLKD   FRUITS  AND  VEGETABLES. 


the  impression  that  the  method  of  preservation  adopted  hy  modem 
prciiervcrft  of  these  ariiclea  wae  not  (juite  so  barmlcsa  as  that  unginallj 
proposed  by  Mr.  Saddiiigton.  We  lelt,  indet:d,  a  strong  conviction 
thut  t]ie  siiine  means  of*  coloration  waji  re»orte<l  to  in  the  case  of 
bottled  fruits  and  ve^eiubh'ji  as  ve  bad  already  ascertained  to  be 
employed  with  pickles.  In  order  to  determine  whether  this  convic- 
tion w:is  well  founded  or  not,  we  resolved  to  institute  a  scries  of 
rigornus  analyses,  the  results  of  which  we  arc  now  about  to  mike 
known. 

The  extraordinarjr  effect  of  copi>er,  in  heightening  and  rendering 
permanent  the  grevn  colour  of  fruits  and  vegetables,  has  already  been 
remarked  U{>on  in  the  reptfrt  iin  Pickles.  This  action  is  exerted 
upon  the  green  contents  of  the  cells,  the  chlorophylle,  and  hetiee  it  is 
the  coloured  portions  of  Tcgetahtcs  and  fniilSt  as  those  invested  by 
the  epidermis,  which  are  most  ufTcctcd  by  this  substance.  The  copper 
used  aocumulat^M  in  this  membrane  as  a  salt — as  an  acetate,  a  citrate, 
ur  a  nialate  uf  copper. 

The  presence  ot  copper^  however,  in  fruits  and  vegetables  is  not 
confined  to  the  coloured  portions;  it  penetrates  lhrout;h  the  whide 
lja.Hue;  and  a  considt^rable  part  of  the  metal  used  even  remains  diffused 
throughout  the  lluid  in  which  the  vegetable  substance  is  contained: 
hence  it  is  desirable  to  aniilyso  for  coitper  not  only  the  preserved 
article  itself,  but  also  the  tluid  in  which  it  is  immersed. 

Hendit  of  AnalyMts  of  SampUt, 

Thirty'four  samjilest  of  different  kinds  of  bottled  fruita  nnd  vegeta- 
bles were  therefore  subjected  to  chemical  analysis.  From  this  analysis 
the  following  eonclueiona  were  deduced  : — 

1st.  That  of  the  thirty-three  samples  of  preserved  fruits  and  vege- 
tables term  were  free  frum  curUamtnation  tcith  copper. 

2nd.  That  (weniyseven  samples  were  more  or  leu  impregnaied  with 
thai  metal. 

Slrd.  That  tracet  of  copper  were  discovered  in  three  of  the  samples. 

4th.  That  in  seven  of  the  samples  copper  uftu  present  in  small 
amount  otJy. 

5th.  Tliat  eight  samples  cx>ntained  it  in  coitsiderable  amount. 

6th.  That  in  six  samples  the  metal  was  present  in  very  cotisiderabUs 
armjiuiL 

7th.  That /bur  of  the  samples  contained  this  poisonous  impreguaUon 
in  very  large  qitautities. 

Hth.  That  the  snni[tles  of  limes  contained  copper^  the  one  in  smeU 
ainouni  only,  the  other  in  amount  more  considerable. 

i)ih.  'VUsX  gooseberries^  as  commonly  preserved,  contain  a  cotuider' 
able  amount  of  copper^  and  some  samples  even  a  very  large 
quantity. 

lOih.  That  rhubarb  usuaUj  contains  an  amount  of  cof^r  mort 


I 

I 
I 

1 


POISONOUS  BOTTLED  FRUITS   AND   VEGETABLES,     411 


cofiMiderabffft  same  sampieM  being  conhiminated  with  it  to  a  nery 
large  extent. 
Ilth.  That  greengages  in  g^nerHj  contain  a  sttlJ greater  rjumUity  of 
cupper,  the  metal  being  frequently  present  in  highly  dangerout 
amoimts, 
12th.  That   in  olives  this  poisonous  impregnation  is  in  the  largest 
amount^  although  its  clTucL  in  heightening  the  colour  of  the  fruit 
is  less  marked  than  in  the  other  coses. 
I3ih.  That  the  preserved   red  fruits,  tts  currants,  raspberries,  and 

cherries,  are  nut  tts  a  rule  conUtmmated  with  copper. 
The  absence  of  copper  in  n^l  fruits,  and  the  variation  of  the  quan- 
tity of  that  metttl  in  green  fruits  according  to  the  requirements  in 
each  cose,  afford  clear  evidence  that  this  dangerous  impregnation  iloes 
not  arise  from  the  mere  use  of  cnpperutensils,  but  thai  it  is  purposely 
introdiiCtid,  the  quantity  being  systeinutically  adjusted  in  dilterent 
proportion^  determined  by  the  kind  ol"  fruit  pi^eserved. 

That  this  conclusion  is  correct  is  cnnduiiively  shown  lu  another 
way.  According  to  the  method  of  preparatioti  ui^ually  pursued,  the 
fruit  or  vegetable  is  not  supposed  to  comu  in  contact  with  copper. 

The  fruit  or  vegetable  is  taken  dirL'ctly  from  the  baskets  or  sieves 
in  which  it  is  received  from  the  country,  and  carefully  packed  in 
bottles;  these  are  next  tilled  up  with  a  liquid,  consistmg  of  water 
holding  a  small  quantity  of  alum  in  solucion  ;  they  are  then  loosely 
corked,  an<l  submitted  for  a  certain  time  to  the  heat  of  a  watcr-bocb, 
so  08  to  ensure  the  coagulation  of  the  vegetable  albumen  ;  they  are 
afterwards  more  tightly  corked,  tied  over  with  string  or  wire,  and 
further  secured  with  resin  and  bladder,  or  with  a  metallic  capsule. 

The  presence  of  copper,  ihen,  in  bottled  fruits  and  vegetables  can 
only  be  explained  on  the  supposition  that  it  is  purposely  introduced; 
and  this  is  really  the  case. 

As  in  the  cuse  of  lK>ttled  fruits  and  vegetables  there  is  no  vinegar 
to  act  upon  the  copper  of  the  vessels,  the  copper,  usually  the  sulphate 
or  blue  t^tt/ne^  in  in  all  cases  added  direct  to  these  articles.  We  have 
the  authority  of  a  manufacturer  for  stating  that  the  quantity  of  this 
powerful  and  almost  poi»>nou!!'  substance  used  is  often  fully  as  much 
an  sixty  grains  to  one  gross  of  bottJeif  of  the  fruit ;  this  gives  not  far 
short  of  half  a  grain  per  bottle,  which  is  a  full  medicinal  dose. 

In  some  cases,  where  the  quantity  of  cupper  is  coDsiderable,  the 
metal  becomes  deposited  on  any  metallic  surface  it  may  happen  to 
come  in  contact  with,  in  the  course  of  a  few  minutes.  In  proof  of 
this  we  will  quute  a  pnrngraph  front  a  letter  written  by  Mr.  Bcrnuvs, 
a  chemist  resident  in  Derby,  addressed  to  the  ^  The  Lancet."  lie 
writes, — 

''  I  had  bought  a  bottle  of  preserved  gooseberries  from  one  of  the 
most  respectable  grocers  in  this  town,  and  had  had  its  contents  trans- 
ferred into  a  pie.  It  struck  uie  thm  the  gooseberries  looked  fearfully 
green  when  cooked ;  and  on  eating  one  with  a  steel  fork,  its  inteose 


^ 


41S     POrSONOUS   BOTTLED    FIiriTS  AXD  VEGETABLES. 

bittorncs89  sent  mc  in  search  of  the  sugar.  Afler  having  sweetened 
and  luiuhed  the  gooaeberrics  with  the  same  steel  fork,  I  was  about 
to  convey  some  to  my  mouthy  when  I  observe*!  the  prongs  to  be  com- 
pletely coiiteiJ  with  a  thiti  film  of  bright  metallic  copjier.  My  testi- 
mony can  be  borne  out  by  the  evidence  of  three  others,  two  of  whom 
dined  at  my  table." 

In  the  preservation  of  red  fruits,  no  copper  is  used ;  but  here,  again, 
we  are  inibrtneil,  thut  red  colouring  mutter,  as  decoction  of  loi^wood, 
or  iul'usioi)  of  beet  root,  is  not  uiifrequently  employed,  especially 
where  the  fruit  is  daranged  or  of  inferior  (juidity. 

The  coh>iir  of  green  fruits  and  veiretahlefl  w  sometimes  apparently 
heightened  by  a  stHiond  devlre  ;  the  bottles  in  which  they  are  enclosed 
are  made  of  a  highly  coloured  glass  ;  those  in  which  French  olivea  are 
preserved  ore  of  so  intense  a  green  as  to  impart  to  Che  fruit  as  seen 
through  the  bottles  a  deep-green  colour. 

As  a  rule,  the  uniount  of  copper  ordinarily  present  in  many  kinds 
of  bottled  fruits  and  vegeliibles  is  greater  lor  even  equal  quantities 
than  in  pickles,  which,  as  we  have  nhown,  aUo  frcjuently  contain 
that  metiil  in  tiirge  and  almost  pnismiou^  ipantity.  Add  to  this  the 
fact  that  while  pickles  are  used  in  ^inan  rjiijintily  only,  a  whole  bottle 
of  preserved  fntit  is  consumed  by  two  or  three  persons  at  one  time ; 
hence  we  perceive  how  much  more  dangerous  is  the  emplu/ment  of 
copper  in  the  cose  of  fruits  than  in  that  of  pickL>s. 

Ihc  present  adds  another  iiistaiiee  to  the  many  which  have  already 
been  adduced,  in  which  uianufucturers,  in  order  to  heighten  the 
colour  of  articles,  and  as  they  conceive,  often  very  erroneously,  (o 
improve  their  appearance,  have  sacrificed  their  flavour  and  quality, 
ami  have  rL^ked  health,  and  even  safety. 


On  the  Detection  of  the  Advlterationa  of  Bottled  Fruits  aitd  Vegetables, 

The  chief  adulterations  of  these  articles  arc  those  with  taltt  o/coppeff 
added  for  the  purpose  of  heightening  their  colour.  In  many  cases 
the  intense  green  or  bluish-grey  colour,  greatly  increased  when  the 
fruit  or  vegetable  U  cooked,  is  sutficieut  to  betray  the  preseuce  of 
copfwr,  e^iiwcially  to  an  accustomed  eye. 

For  the  detection  of  copper  by  chemical  means  we  must  have  re- 
course to  the  processes  des^-ribed  under  the  liead  of  Pickles. 

Tlie  copper  is  found,  as  in  the  case  of  picklod,  in  the  preserving 
fluid  ns  well  as  in  the  fruit  or  vegetable  itself. 

If  we  desire  to  test  the  liquid,  we  proceed  ns  follows  :  — 

About  threeounces  of  the  juice  or  fluid  in  which  the  fruit  orvi^etable 
is  preserved  are  to  be  measured  out,  uufl  placed  in  a  test  (ilass ;  the 
acidity  is  to  be  slightly  increased  by  the  uddition  of  alK>ut  three  drop« 
of  strong  nitric  acid,  and  a  polishetl  rod  of  iron  placed  in  the  fluid, 
and  allowed  to  remain  f(»r  al>out  Iwcnty-four  hours.  If  copper  ia 
preaent  in  considerable  amount,  the  surface  of  the  rod,  from  top  to 


POISONOtJS   BOTTLED   FEUITS  AND  VEGETABLES,      413 


bottom,  become*  covered  wilh  a  continuous  and  brifiht  coating  of  that 
niL'tal.  If  the  amount  of  copper  is  less  consi^lerablf,  the  upper  half 
or  «o  only  of  iho  roil  receives  the  coating.  If  the  quantity  is  very 
small  indeed,  no  perceptible  <Ieposit  of  copper  will  take  plncc. 

Hence  we  perceive  that  the  iron  rod  alTords  n  simple  nnil  most  con- 
clusive te-Jt  for  t:<)])|>er  in  I'ruita  and  regetables,  when  present  in 
anything  like  considerable  umuunt,  and  that  it  even  fierves  to  indicate, 
to  a  certain  extuat,  the  tjuuniity  uf  cupper  with  which  the  juice  of 
different  samples  is  impregnnled,  as  »hown  by  the  rapidity  with  which 
thed(.'poflit  occurs,  by  the  thickness  of  t)ie  coating,  and  by  the  extent 
of  surface  covered  by  it. 

If  we  desire  to  analyse  the  fruit  or  vegetable,  we  must  proceed  u 
follows ;  —  Three  ounces  of  each  of  the  fruits  and  vegetables  are  to 
be  weighed  out,  placed  in  crucibles,  and  incinerated  until  nearly  the 
w^hoie  uf  the  Cijrbon  is  dissipated,  the  colour  of  the  ash  being  care- 
fully nnted.  In  those  cases  in  whiih  the  fruit  or  vegetable  is  not  con- 
taminnteil  with  t-oppcr,  the  re-tidual  ash  is  observed  to  be  either 
white  or  greyish-white,  while  in  thitse  instances  in  which  copper  is 
present  it  U  conFiaiitly  of  a  pink  colour;  the  depth  varies  uniformly 
wilh  ihe  amount  of  eoppur  prest-nt. 

We  have  already  advened  to  the  pink  colour  of  the  ash  of  vegetable 
Bubatiuices  containing  copper,  as  affonling  nn  excellent  test  nf  the 
presence  of  tLat  nietii).  in  the  cose  of  bottled  l'ruit«  and  vegetables 
this  is  a  peculiarly  delicate  test. 

When  fruits  or  vegotubte  substances  are  carefully  incinerated  with- 
out being  in  ajiy  way  tlisturbed,  the  genernl  forin  of  the  fruit,  &c.,  is  in 
most  cases  tolerably  well  preserved  ;  and  it  is  then  itercLivetl  thai  the 
pink  colour  is  conlincd  principally  to  the  surikce  of  the  substance 
incinerated. 

In  those  cases  in  which  the  amount  of  copper  is  but  Tcry  Finf.IJ,  the 
pink  will  be  seen  on  the  Mirfnce,  only  here  and  there,  und  will  be  of  a 
pale  tint.  Where  the  quantity  is  lurger,  although  still  but  small,  the 
colour  will  be  more  genera!  nnd  more  decided.  Where  it  is  abundant, 
the  whole  surface  of  the  a.ih  will  be  of  a  brighr  and  beautiful  roay- 
pink  hue.  Lastly,  when  the  (juantity  of  cop[KT  present  is  very  con- 
fideruble,  the  residual  ai^h  will  be  of  a  deep  pink  colour. 

Olives,  when  incinerated,  do  not  leave  a  clean  white  ash,  so  that 
although  the  colour  way  be  very  well  detected  in  iheni,  it  is  not  of  so 
bright  a  pink  as  in  other  fruit ;  and  the  colour  is  not  confined,  as  in 
most  other  ca^s,  to  the  surface  of  the  fruit,  but  extends  through  its 
whole  Kub-'lance. 

When  a  portion  of  the  juice  is  incinerated  alon^  with  the  fruit,  u 
IS  usually  the  cose,  the  crucibles,  if  cnpf>er  is  nrcsenl,  become 
tinted  with  the  same  nisy-pink  colour  obser^-ed  on  tne  surface  of  the 
fruit  or  vegetable  incinerated.  In  some  cases  where  the  amount  of 
copper  is  considerable,  the  bottoms  of  the  crucible*  become  deeply 
and  beautifully  stained  of  a  bright  and  iridescent  pink. 


L^ 


ADITLTERATIONS   OF   PRESERVES  AND  JELLIES. 


TIiG  jilnk  colour  nf  the  ash  U  thus  explained.  In  the  course  of 
incinertitinn  the  acid  with  which  the  copper  was  combined  is  de- 
stroyed, the  bijzhly  characteristic  pink  oxide  alone  remaining  in  the 
fruit,  and  ita  presence  bcinp  revealed  by  its  peculiar  colour. 

We  have,  ihen,  in  ibc  colour  of  the  ash  a  certain  and  beautiful  lest 
of  the  presence  of  copper,  even  in  the  ninst  minule  quantitieR.  and 
likewise  for  the  determinalioTi  of  its  amount  to  ii  certain  extent,  not 
not  only  in  bottled  fruttit,  but  in  moat  vegetable  substances,  and  espe* 
citilly  in  pickles. 

The  tint  nf  the  aah  havin«  been  noted,  it  may  next  be  treated  in 
the  Kanie  manner  as  the  nsh  of  pickles. 

When  copper  is  present,  the  colour  of  the  acidulnted  solution  of  the 
ash,  when  anmmnia  is  added,  varies  preally,  from  a  ])ale  and  scarcely 
perceptible  bluish  liue  to  a  rich  and  deep  azure,  according  to  the 
quantity  of  the  metal  present. 

As  a  further  tost,  the  metal  may  be  separated  from  the  ammoniaral 
solution  in  the  follnwinf;  manner:  — 

Acidiilat^r  the  solution,  and  immerse  in  it  a  piece  of  polished  iron 
wire,  when  the  oojijwr  will  become  deposited  up<m  it.  A  coating  of 
copptT  may  often  be  obtained  from  the  acidulated  8o]uli<m  of  thti  ash 
in  cBffce  where  no  deposit  of  mt'tal  tukes  pliu-e  on  iumiersion  of  the 
iron  in  the  juice  in  which  the  fruit  ur  vegetable  was  preserved. 


ON  THE  CONTAMINATIONS  AND  ADULTERA- 
TIONS OF  PRESERVES  AND  JELLIES. 


i 


We  have  repeatedly  shown  that  the  adulterators  of  our  food  do  not 
Bcrujily  to  employ,  when  it  suits  iheir  purjHise,  the  most  deadly  sub- 
stances, undeterred  by  the  serious  eonsetjuences  whii-h  but  too  fre- 
quently result  from  their  use.  Thus,  it  has  been  shown  lliat  it  is  no 
uncommon  thinf;  fur  them  to  make  use  of  viirious  pn-paralions  of 
iron,  lead,  copper,  arsenic-,  mercury,  &c.  It  is  not  a  little  remarkable^ 
that  the  nmjority  of  the  substance^}  arc  had  recourse  to,  not  on  account 
of  bulk  nr  weight,  but  for  the  mere  sake  of  colours,  which,  thus  pro- 
cured, are  frequcully  in  &  high  dey^reu  ylarin^  and  unnatural,  these 
colours  being  obtained^  too,  at  the  expense  of  quality  and  flavour. 

Amonpst  the  artirtcs  which  have  already  been  treated  of,  and  in 
which  foreign  colouring  ingredients  have  been  detected,  are  tea, 
chicory,  cocoa,  Cayenne,  mustnril,  pickles,  bottled  fruits  and  vegetables, 
potted  meats  and  fish.  The  list  is,  however,  far  from  complete  aa  yet ; 
oud  on  the  present  occasion  we  have  to  add  to  it  other  arlicles. 


A1>C1.TERAT10>*S  OF   PRESERVES   AND  JELLIES.     415 

fed  jelliea  prepva)  in  copper  vessels  are  alvrn)'s  cnn- 
ft»  ft  greftler  or  leu  extent  witti  copper. 

Bat  imiWcweof  green  preserves,  as  in  those  of  picklo.s  bortlod 
irmtm  aad  v«sclafalei«  copper  is  tued  intvnliuually  fur  Lbc  iiuqntFtu  uf 
the  colour. 

la  tone  cases  the  preserves  and  jellies  are  actually  mluU 
Icralcd. 

Yc^etakle  jellies  consist  of  the  tliick  anri  transparent  part  of  ilie 
ftA  only,  tae  husks  and  seeds  hcinfr  removed.  Now,  these  really 
■  01  >y I  SI  portMUS  of  the  fruit  nre  rarely,  if  ever,  tlirown  awny  Hy  the 
^„Mm,w^tmmt»mmwm  of  pTeTerves  ;  but,  mixL'd  with  a  little  fretih  fruit,  tficy 
VCDMBed  offasgtxMl  jams.  IiiLliia  practice  huu!<ekeepersure  furnii>hed 
via  ft  fflroo^  reason  for  prepnring  their  own  presurvo.t,  iin<l  til.«ii  \\\i\\ 
■B  explaMUion  of  the  f^encral  ^lupt^riurity  of  Imhil*  nimk'  jtreserves. 

A  i^Hlar  use  is  said  to  bo  foinetlmeA  niiide  nf  the  refuse  partA  of 
frwtft  and  in  the  manufacture  of  hoine-inaile  wiiie^u 

OrvM  Marmalade^  which  when  genuine^  conisipts  only  of  the  bitter 
or  ServBe  orange,  is  frequently  Hdulterated  with  sweet  ornnpes,  with 
•pples  aad  turnips.  We  btivc  been  infornied  ihul  a  uiwcies  of  swede 
of  a  yetto«ir  colour  is  much  used  in  the  oflulteration  of  orange  amr- 
maJade. 

Lftstlj,  we  have  good  authority  for  staling  that  partly- decayed 
OTftDges,  and  even  suckcil  oranges,  are  used  in  the  ndultoratioii  of  this 
ftronrite  preserve;  these  statements  rest  upon  the  authority  of  an 
eye  witness. 

RtiMpbernf  jeUy  is  usually  nothing  more  than  currant  jelly,  to  which 
tlie  flavour  of  the  raspberry  \x\\a  beuu  cuuuuunicated  by  means  «t'i>rris 
root. 

The  ratpbeny  Jiaroun ft f^  for  sugar  confectionary  is  mode  entirely  of 
currant  jelly  and  orris  root. 

Lastly,  the  jellies  in  botilea  and  those  sold  by  confectioners,  as 
isinglass  and  calf's  foot  jelly,  consist  principally  o{ gelatine  variously 
coitmred. 

RetulU  of  Analyses  of  SampUs, 

Thirty-Jive  samples  of  preserves  and  jellies  of  various  kinds  were 
subjeeteil  to  microscopical  and  chemical  examination  and  with  the  ful- 
lowmg  results  :  — 

Isl.  That  the  A^JTj^erryyom  analysed  contained  a  very  considerable 
quantity  ot  copper. 

2n(l.  That  the  four  samples  of  Gootvberry  Jam  examined  alt  con- 
tained copper. 

3rd.  That  copper,  sometimes  in  large  amount,  was  detected  in 
twelve  of  the  fourteen  samples  of  Orange  Marmaiade  analysed. 

4th.  That  three  of  the  Marmalitdes  were  adulterated  with  large 
quantities  of  a  tegetahU  mhsiance^  most  probably  either  turnip  or 


k. 


41S  ADULTERATIONS   OF   PRESERVES   AND  JKLLIES. 


apple.  There  is  a  kirn!  of  t  urnip,  the  seeds  of  which  are  frequently 
atlvertiited  in  the  **  Ganlener's  Chronicle"  for  siiIp,  of  a  velloir 
cohfur.    und  wliit-h  i«»  callrtl  the  oninge  turnip.     We  kuu\r  not 
t(»  what  iiBc  tbii  can  be  put  unless  in  the  ndukcratiun  of  orange 
uiorinalade. 
5th.  That  the  nine  vamplei!  of  Greengage  Jam  were  all  inr)reor  1e59 
impregnated  with  capper^  It  being  present  lu  considerable  amount 
in  five  of  the  samples. 
6th.  Thtit  the  Gretngage*  contained  in   three   different  boxes  of 
Crystaiiued  Fruits  all  owed  their  deep-^een  colour  to  the  pre- 
tence uf  COppfT. 
7th.  That  the  Limes  and  Greengitgea  present  in  a  little  plass  jar  of 
iVuit  preserved  in  jelly  also  owed  their  brilliant  colour  to  a  salt 
of  ct}pper, 
8lh.  That  copper  was  present   in  the  three  samples  of  Candied 

Citnm  Peel  subjected  to  onalysis. 
9th.  That  capper  was  detected  in  no  leas  than  thirbfthree  of  the 
thiriy'Jice  samples  of  diffV-renl  preserves  analysed:    three  eon- 
tQine<i  traceti  only;   in  eleven  the  metal  waa   present  in  tniatl 
t/tuintitff :   and    in   nineteen  either  in  considerable  or  even  very 
large  anttmnt. 
Knowing  well  the  powerful  action  of  vegetable  juiees,  and  olso  of_ 
sunar^  U[tnn  copper,  we  have  l^r^^  entertained  the  bt^lief  that  thai' 
nietul  would  be  very   frequentlv  tletected,  on  analysis,  in  preserres,' 
janis^  and  jellies,  as  ordinarily  prepared:  we  must  acknowledge,  how- 
ever, that  (he  result  of  at'tuat  investigation  has  far  excelled  our, 
expectations,  since  it  h»sproveil  that  preserves  made  in  enpper  vessel 
not  only  almost  invartuhiy  contain  copper,  but  that  the  metal  isoftel 
present  in  very  consiilernble  quanlilies,  sufficient  to  tint  the  n»h  of  a1 
deep  pink,  and  to  cause  the  solution  of  the  a.*h   when  treated  with^ 
ammonia  to  become  of  a  decided  and  aomctiines  even  of  a  deep  blue 
colnur. 

But  the  still  larger  quantities  ^f  copper  detected  In  certain  of  the 
samples  of  ^reenpjiy;c  jam  seem  to  show  lliat,  as  waa  a8certaine<l  to  he 
the  case  with  bottled  fruits  aiul  vupetablfs,  some  greeninj;  salt  of 
copper,  the  sulphatt*  or  acetate,  is  really  iutentionally  introduced  for 
tlie  puriHwe  of  creating  an  artificial  viridity. 

It  will  be  perceived,  also,  that  three  of  the  aiunpli»9  of  orancc  mar- 
malade examintd  were  adulterated  with  largcfjuantiiie«  of  a  vegel«ble 
Bubstuncc.  resembling  in  it^  microscopic  slructure  either  himip  or 
apple.  These  ^amplc^  were  all  inirchased  in  the  beginning  of  Decem- 
ber. Many  other  samples  purcLiiiaed  in  the  fmnimer,  and  also  several 
procured  within  the  last  few  days,  were  all  entirely  free  from  any  such 
ad'uixture.  This  appears  to  prove  that  this  adulteration  is  practised 
chiefly  at  a  certain  period  of  the  year,  when  oranges  become  scarcei 
and  in  order  to  keep  up  the  stoik  of  marmalade,  so  called.  The  de- 
teotion  of  thli  adulteration  in  three  samples,  two  of  them  obtained  at 


ADULTERATIONS  OF  rUESERVES  AND  JELLIES.       417 


the  cstaMiabmenU  of  different  makers,  appears  also  to  sboir  that  the 
A<luIterfltioD  is  a  very  general  one. 

The  discIoittircA  now  mude  affird  contincinp  proof  how  fmproper 
and  even  dan^en)U8  it  is  to  moke  preserves,  as  is  rominonly  done  even 
by  onlinary  bousekeenors,  in  copper  saucepans.  The  vessiils  em]iloyed 
for  this  pnrpnt^e  should  consist  of  earthenware,  or,  if  metallic,  should 
be  lined  with  enamel. 


Although  we  may  fairly  expect  to  find  copper  in  any  preserved 
vegetable  substance  prepared  in  the  ordinary  manner,  yet  we  acarcelj 


4tS     ADULTERATIONS   OF   PBESER'V'ES   AND  JELLIES. 


expected  to  meet  with  that  poison  in  those  tAstcful  and  sparkling 
little  hnxes  of  bonbons  which  at  Christmas  time  are  sproail  out  in 
ahop  windows  so  attractivoly ;  noithor  did  wc  expei-t  to  fiiitl  it  mukiog 
its  way*  tliruugb  th«  citruu-pecl  used,  into  uur  very  Cbribtmas  pluia- 
pudding. 

FigiU. 


The  evils  and  dangers  arising  out  of  the  all-prevalent  and  very 
scandalous  ^»roctice  of  adulteration,  nothing  but  the  firong  arm  of  the 
law  can  snlliciently  check  ;  and  the  force  of  this,  ere  long-,  no  doubt, 
will  be  felt.     Kevorthclcss  we  are  happy  to  tind  that  great  and  im- 


SAUCES,   AXD  THEIR   ADULTERATIONS. 


419 


tiiedijite  jjootl  very  frequently  rpsiilu  from  the  exposures  wliieli  from 
time  to  time  we  are  c<)Tn{ieUe<l  to  make;  this  is  very  eviilent  in  the 
ease  oi'  pickles,  and  prejiervfU  tVuits  nml  ve(;otahI«-s.  AUIiou|:li  we 
still  see  in  shop  windows  liundreOft  of  Imttles  nf  these  urtioto'*  ex|K>9e<J, 
Itighly  rharpe'i  with  copper,  yet  it  must  V>e  allowed  that  a  very  in^^al 
impn»veincnt  has  ttiken  place  in  this  reflpect  since  the  period  of  our 
lipsr.  report  on  Pickles.  We  have  reasitn  to  believe  that  one  ven* 
lar;:c  mnnufacturing  Brm,  whieh  supplies  some  hundredii  of  retail 
estuUJphineutiS  both  in  town  and  cuuntry*  baa  to  a  very  great  extent, 
if  not  entirely,  ahtvndpned  the  u»e  of  eupper,  and  copper  utensils  in 
the  fircening  of  their  pickles  and  preserves.  Such  an  example  cannot 
but  have  an  excellent  effc'ct  on  other  manufacturers  and  prepurera  of 
similar  arlicles. 

On  the  Detection  of  the  AHuIteratimts  of  Preserves  and  Jellies. 

The  adulteration  of  one  kind  of  preserve  by  the  addition  of  nnoiher 
ebea|K'r  kind,  can  in  most  cases  be  discovered  by  means  of  the  inicn>- 
Bcope.  The  structure  of  the  strawberry,  raspberry,  and  currant, 
especially  of  their  !«eedft,  is  very  diflerent.  By  means  of  llie  same  in- 
striiuient,  vegetable  jellies  may  sometimes  be  distinfjuiithod  one  from 
the  otlter,  by  the  remains  of  the  dilTcrent  ti*suea  disroverable  in  them. 

The  adulleralitm  of  oranj;c  marmalude  with  apple  or  turnip  is  like- 
wise readily  discoverable  by  the  aid  of  the  microscope.    Fig.  153. 

Lastly,  the  presence  of  orris  root  in  any  jelly,  as  well  as  in  snutf. 
may  be  detected  by  the  same  means,  as  will  at  once  be  perceived  on 
an  examination  of  the  annexed  figure.   Pi^.  154. 

The  methods  employed  for  the  determination  of  the  presence  of 
copfjer  in  preserves  and  jellies  are  the  same  as  in  the  case  of  pickles 
sad  bottled  fruiU,  to  the  articlea  on  which  the  reader  is  referred. 


SAUCES.  AND  THEIR  ADULTERATIONS. 


A  oBBAT  variety  ofsub^tancas  chiefly  Te?oiabte,  enter  inio  the  mm- 
position  of  the  varioas  uuces  in  use.  The  following  Is  an  rnnmcra- 
tion  of  the  chief  of  these:  —  Tomato,  pnrlic,  fhallot,  sorrel,  nui'^hrooni 
and  walnut  catsup,  i^isina,  tamarinds,  the  secdf)  of  fenui*reek  and 
rumin,  fhc  leaves  of  a  Tariely  of  herlis,  as  laragon,  chervil,  mint, 
thyme,  marjoram,  Ac,  the  see<ls  of  an  Indian  plant  called  Dnhchoa 
titja  or  aoyri,  of  which  soy  is  made  ;  a  variety  of  spices  andcnitditiif^nts, 
oa  pepper,  Cayenne,  mustard,  mace,  cloves,  ginger,  and  nciirly  all  the 

e  E  2 


430  8AUCE9,   AND   THEIR   ADULTERATIONS. 

other  Bpioes;  salt,  treac-Ie^  and  burnt  sugar  u  colouring  agents,  nn< 
flour  as  a  lliickenin;;  ing^redient.  t)ut  oCtbeub'tve  articles,  Tariously 
combined,  and  in  ilitfereiit  propnrtioiis,  nearly  ull  tbe  sauces  m  use  are 
compounded.  Into  the  cuuipoHitinn  of  yome  few,  however,  aninitd 
jiubstjinces  enter,  as  tbe  utu»cultir  fibre  of  sbrimjw,  lobster,  and  an- 
chovy. 

The  following  are  the  chief  results  deducible  from  a  consideration 
of  the  analyses  of  Thirty-thrfc  s&inples  of  snuc-o  of  different  kind^:  — 

1st.  That  treacle  and  much  talt  formed  the  baaifi  of  the  five  samples 

of  InuiA  Sot  examined,  if  they  did  not  even  entirely  eonsists  of 

these  two  ingreclieut'i. 
2nd.  That  of  the  seven  sumples  of  Tomato  Sacck  aitalysed,  bix 

were  nrtlBtialty  coloured,  one  probably  with  c&cAiMro^  and    the 

rest  by  the  mJ-lition  of  considerable  quantities  of  the  ferruginous 

pigment  hnte  Amtfuian. 
Hrd.  That  the  saniplt*s  of  Kasenck  of  TjonsTRRs  examined  were 

almost  saturated  with  very  large  quantities  of  bole  Artneman. 
4th.  That  the  samples  of  Kssknck  or  Shsimpb  were  aatunued  to 

an  fqiiiil  extent  with  bole  Armenian. 
5th.  That   the  whole   of  the   pamplet*  of  Essence  or  AKCiioriRS 

analvK'd  were  adulteratetl  with  immense  quantities  uf  the  feiTu- 

ginouH  oxide  bole  Armenian. 
Ctb.  That  three  of  the  samples  of  £<feHcv  o/j4ricAory  contained  but 

a  ftmall  quantity  of  muscular ^bre, 
7th.  That  two  of  the  samples  contained  a  portion  ofyfow  — one 

being  a  sample  of  essence  of  shrimps,  and  the  other  of  essence  of 

lobster. 
8tb.  That  out  of  the  eighteen  red  sauces  submitted  to  examination, 

no  less  than  sixteen  ciuituined  hole  Armenian,  and  this  u^uuUy  in 

immense  quantities,  far  exceeding  whut  was  detected  in  any  of 

the  |K>itcd  meals  and  fish. 
9lb.  That  lead,  for  which  separate  anolysefl  were  made  in  each  case, 

was  not  detected  in  a  single  inxlancf. 
10th    That  tracet  only  o/covvt.vl  jcere  discovered  in  $ome  three  or 

four  sampler. 

The  above  results,  tlien,  regarded  as  a  whole,  although  bad  enough, 
are  yet  not  so  bad  or  serious  as  the  account  given  by  Accum  and  vnne 
other  writera,  of  the  adulteration  of  anchovy  paste,  &c  ,  would  leail  us 
to  infer,  since  lead  was  not  detected  in  a  single  instance.  There  is 
no  doubt,  however,  but  that  lead  does  soii^eiiuicA  occur.  Mitchell 
states,  "several  samples  which  we  have  examined  of  this  Bnh  sauce, 
*  [H>iso»ous  anchovy  sauce  *  have  been  found  contaminated  with  lead.** 

Further,  it  is  more  than  protiable  that  the  muscular  6bres  in 
several  nf  the  samples  of  anchovy,  lobster,  and  shrimp  sauces,  con- 
sisted either  entirely  or  in  port  of  the  fibres  of  other  inferior  and 
cheaper  fish. 


8ACCES»  AXD  TUEIB   ADULTERATI0K8.  421 

The  on]y  effeclual  rnmedv  against  ccrtun  of  tlie  adulternriona  of 
the  ^aucesi  especially  ibe  tie\x  sauces,  ix)iiflists  in  their  prepiirHtiun  at 
lioine.  Receipts  for  severtil  of  tlie  sauces  are  siren  at  page  51*2.  of 
the  utuhoKs  work,  "Food  anil  its  Adulterations." 

It  appears,  then,  that  the  reil  sauce!*,  as  those  of  shrimp,  hibsler, 
aiiehovYt  and  tomato,  are  almnAt  invuriatilj  hi>rhlv  otiUnin-d  with  hole 
Arnienmn.  TfaiB,  as  has  alroudy  been  pointed  out,  is  a  ntiturul  eurtU, 
containing  a  lurpe  ((uantitv  of  the  red  oxide  of  iron;  but  frequeTrlly 
an  article  is  made  in  imitation  uf  it,  enitm^linjr  of  a  ntixluie  lU*  Vt^- 
netian  red  and  elmlk.  Of  ihie  red  earth  or  dirt  us  much  um  from  ]0 
to  15  lbs.  are  added  to  100  ^alls.  of  aiichnry  sauce. 

Cooka  frequently  eolour  the  ^aucea  prepitred  by  them  for  the  table 
with  carmine;  this  when  •genuine,  i^  a  vegetable  colour,  but  it  is 
frequently  adulterated  with  vermilion. 

Perceiving  clearly  the  evils  connected  with  the  employment  of 
artiticial  colouring  matters,  jSIessrs.  Crosse  and  Blackwell  liuve,  to  a 
very  great  extent,  abandoned  their  use,  and  they  now  prepare  an- 
chovy sauce  free  from  colouriujj  matter.  The  difference  between 
the  ordinary  coloured  and  the  uncoloured  »aures  is  very  striking: 
the  tirst  is  usually  intensely  red  —  us  re<l,  in  fuct,  us  a  briekhut,  this 
redness  arisini;  entirely  frum  the  introduction  of  the  bole  Armenian, 
—  while  the  other  is  usually  of  a  pinki»h'fawn  colour. 

The  variouj*  colouring  matters  to  which  reference  hos  already  been 
H>  frequently  made,  are  used  not  merely  for  the  Huke  of  increaBiMg  the 
colour  of  articles,  and  thus,  as  it  is  very  often  erroneously  con.sidered, 
improving  their  appearance,  but  likewise  for  other  puriwses,  esjteci- 
ally  to  conceal  other  udulterftttons ;  thus  when  very  larjje  quantities 
of  wheat  Hour  are  added  to  mustard,  or  Hour  and  suj^ar  to  cocoa,  the 
natural  colour  of  those  articles  becomes  ^o  reduced  that  tlie  addition 
of  some  foreign  colcunng  matter  is  rendered  necessary. 

Not  unfretiuently  the  use  of  these  colouring  inaiters  tnvnlvca  con- 
sideritions  ot  cleanliness;  this  is  so  in  the  case  of  nnchory  sauce. 
The  quantity  of  refuse  matters  and  dirt  contained  in  the  fish  from 
whicli  this  is  prepared  is  often  very  trreut ;  and  it  is  tl»e  presence  of 
these  more  than  anything  else  which  cruises  the  sauce  to  present  a 
somewhat  unsifhily  ap|H*aTance  Iwforc  the  red  u:irth  is  adiled.  It  is 
this  eircumstande  which  has  chiefly  le*l  to  the  use  of  the  l>ole  Arme- 
nian ;  the  maker*,  in  place  of  carefully  reimiving  the  refuse  and  dirt, 
grinils  it  all  up  with  the  fish,  trusting  to  the  tiule  Armenian  tocunceul 
the  impurities,  tliereby  savin;;  hiniticlf  much  trouble  and  M>me 
UiSd.  \Ve  are  in^irnied  by  Messrs.  Criisi^ie  and  Hlnckwell,  thai  the  im- 
purities which  they  ore  obliged  to  remove  in  ilte  prejmratioii  of  the 
uncoloured  anchovy  sauce  arc  almost  incrvdible,  but  that  the  extra 
trouble  and  loss  are  fully  compensated  by  the  greatly  iuqiroved 
quality  and  tiavuur  of  the  article. 

Nutwitbstanding  this  improvement  tn  quality,  so  strong  do  Messrs. 

K  B  3 


in  SPICES,    AND   THEIB    ADULTERATIOXS. 

Crosse  and  BInokwell  find  (he  prejaiJice  in  fuvonr  of  tbe  red  sauce, 
thiir  many  purtiei)  absolulclv  refuse  to  take  the  tincoloured  sauoe  — 
preftrring  lUe  inllTior  article  simplj  bceausc  of  its  redness. 


SPICES,  AND  THEIR  ADULTERATIONS. 

W£  now  come  lo  tlic  consider atioa  of  ibe  important  subject  of  Spices 
und  their  AduJienitions. 

Tlie  spices,  ot"  the  adiilteration  of  whicli  we  are  about  to  treat,  are 
Ginger,  Cinnamon,  Cussia,  Nutmegs,  Alace,  Cloves,  Allspice  or 
Pimento. 

^Vbcn  it  18  remembered  tbitt  ranny  spices  are  sold  in  the  stale  of 
powder,  iind  mosl  ftf  (hi.'in  bt-ur  u  hijj:K  price*  and  that  they  are  nearly 
idl  sul'jecl  ru  a  duty,  wlilcb  iti  souiy  uascK  is  considerable,  it  might  be 
suppiaud  lliiit  they  would  be  peculiarly  subjecl  to  adultenitiun. 

rfotwitbsluuiliii;,'  tlieite  fUets  little  or  no  uttentinn  bus  hitbortubecn 
bestowed  ujwn  tliis  stubjeut  by  writers  on  the  ^ophittCicutiun  of  food, 
nr  even  by  the  Exci'o  uulhoritios,  whose  cluiy  ii  ^htmUl  l»e  lo  protect 
the  revenue  frimi  all  fraudii  rc-sulling  friMu  the  nduUeratlon  of  duly- 
{)aying  arlicles. 


GINGER.  AND  ITS  ADULTERATIONS. 

The  ginnjer  plant,  Zinziber  officinale,  belongs  to  the  \^ry  tiseAj. 
natural  order,  Zinzibfracea,  from  which  turmeric,  East  India  arrow- 
ru(Jt,  and  some  other  productions,  are  obmined. 

Ginger  grows  and  is  cultivnted  in  the  tropical  regions  of  A^ifl, 
America,  and  :^ierra  Lef>ne. 

The  stem  reucbeK  gener;dly  ibree  or  four  feet  in  height,  and  is  re- 
newed yearly  ;  while  the  root,  which  is  the  part  known  as  ginger, 
biilHnically  termed  a  rhizumrj  is  biennial. 

Tlie  HKits,  or  rhizonH'.s  are  dug  up  when  about  n  year  old  ;  in 
JnmaicA  this  occurs  in  Jnnunry  nr  February,  and  nftcr  the  stems  are 
withered.  They  are  well  wo.'thed,  freed  from  dirt,  and  in  some  eases, 
especially  with  the  bethr  kinds,  the  epldennis  or  outer  coat  i«  stripped 
otf;  and  hence  the  division  of  ginger  into  white  (serajied  or  uncoated), 
uiid  iul't  black  (unscraped  or  coaled). 

in  efrlinmtiiig  tbe  quality  of  ginger,  n  variety  of  particulars  have 
to  be  taken  into  conMderution  —  us  whether  the  rhizomes  are  coated 
or  uncoated,  their  form,  colour,  and  cuni^istence. 


SPICES,    AND   THEIK   ADrLTERATlONS. 


423 


The  rfaizomoa  of  ginger  ai good  quality  have  no  epidermis,  lire  plump, 
of  ft  whitish  or  taint  f^traw^culour.  soft  oud  mealy  in  texturi?,  with  a 
>hort  fracturef  exhibiting  n  reddish,  resinous  zone  round  the  circum* 
Terence  ;  the  tute  should  tie  hot,  biting,  but  aromatic. 

The  rhizomes  of  ginger  of  inferior  qnalHy  are  frequently  coated 
with  tIjL*  epidermis,  are  less  full  and  plump,  offeri  conlrarle*!  and 
shrivelle*!;  of  darker  colour^  beinp  of  a  hnmniah-yellow  ;  of  harder 
texture,  termed y7i>t/y ;  and  more  fibrous  ^  while  the  taste  is  inferior, 
and  less  aromatic. 

Composition  of  Ginger. 

Ginger  was  analysed  by  Bucholz*  in  1817,  and  by  Morinf  in 
1823. 


Blcuolz'b  AfiALVaii. 

Pale  yellow  volAtilc  oil     -        -  t  56 

Afomatic,  acritl,  soft  reiin          -  3'IjO 

Extrjirlivv  Aotubh'  In  alcohol  -  O'Cd 
Acidulous  and  acrid  extractive 

inAuluble  in  alruhul       •        •  10*50 

fium 12-05 

Starch,  analogous  to  bascorin  -  19*7$ 
Apotbeme,  extracted  by  potash 

(ulmin?)     ....  36-00 

Bassorin            ....  g-SO 

Woodv  ftbre    ....  8-00 

Wotcr             ....  11-90 


102-31 


MouM'a  AKJtLTsia. 

Tolltilc  oil. 

Acrid  doft  tfsin, 

Rcsiii  insoluble  in  ether  and  otL 

Gum. 

Starch. 

Woody  fibre. 

Vegeto-aniinal  matter. 

Osmaxoma. 

Acetic  acid,  acetate  of  potash,  sulphur. 

'J1ic  anbcs  contained  carbonate  and 
fiul|diat«  of  |>ota«h,  chloride  of  po- 
tastdtun,  pbo8[ibace  of  Hnie,  alumina, 
silver,  and  oxidea  of  iron  and  man- 
ganeae. 


The  volaHU  oil  is  pole  yellow,  very  fluid,  lighter  than  water  ; 
o<lour  resembling  that  of  gmgcr,  taste  at  first  mud,  afterwurda  hoc 
and  acrid. 

Soft  rexin,  obtained  by  digeitting  the  alcoholic  extract  of  ginger, 
first  in  water,  then  in  ether;  it  p(»ses3ud  un  aromatic  odour,  and  a 
burning  aromatic  taste.  It  is  readily  soluble  in  alcohol,  ether,  and 
turpentine. 


Structure  of  Ginger, 

Examined  with  the  microacope,  the  rhizome  of  ginger  is  found  to 
present  a  wtfll-markcd  and  ciiaracteristic  structure. 

llie  outer  coat  ur  epidermis  consists  of  several  layers  of  large, 
ai^ilar,  transparent  cells  of  a  brownish  colour,  adhering  firmly 
together,  forming  a  distinct  membrane,  and  when  macerated  in  water, 
becoming  !<oft  and  somewhat  gelatinous. 


•  Bnuidi'i  Diet.  ofMiCerU  Madlca. 


E  c  4 


t  Omvllu'a  lUudU  4.  Ctttn. 


4t4 


SPICES,   AND  THEIH   ADULTEKATION8. 


hying  upon  the  under  surface  of  this  nienibrane,  and  scAttered 
irrejiularly  over  it,  are  penorally  to  IwdL'tecied  oil  globules  of  various 
sizes,  and  of  a  dei'p  yellow  colour,  ha  well  as  a  few  cells,  identical  in 
Btructure  and  tint  with  those  of  tunnerle. 

In  the  substance  of  the  rhizome  itself  several  structures  have  to  be 
described. 

Fig.  155. 


A  portlan  aT  the  tpiilrrmit  of  th*  riUaomc  of  OlxoBK.  vhovlng  the  cbIU  of  whtrh  It 
U  compowd,  M  w«II  ■•  Uui  oil  glottale*. «  (t;  «1m>  tb«  lunnerio-llka  M)U,iA; 
■04  c  r,  crxftftlt  very  commoalj  uuUoeid  lo  gnat  uuinbcn  l>liig  bencKlh  tbt 
efidennb. 

It  consists  principally  nf  cells  bavin>;  delicate  transparent  walls 
minutely  punctated^  and  adhering  tojretber  so  ntf  to  fnnii  a  connected 
tissue.  Tliese  cell*  contain  in  llieir  cavities  starch  eorpuaclet,  which 
are  very  abundant,  and  tnan^  of  which,  as  the  cell  walls  are  easily 
broken,  are  seen  in  niopt  s<-H*lion8  to  have  become  effused. 

Lyinjr  here  ami  ihere  in  the  midst  of  the  ahovc-describe<i  cells  are 
other  colls  of  nearly  similar  bize  and  form,  but  of  a  bright  yellOw 
colour  ;  these  are  in  do  respect  distinguishable  from  the  coloured 
cells  of  lunneric. 

Itistotlie  presence  of  these  cells  that  ^-iiifier  owes  its  colour,  which 
varies  with  the  number  of  such  celU  contained  in  it. 


LftNE  UBRAivi.  ^^t^.uo 


uU  UNIVERSITY 


SPICES,  AND   THEIR   ADULT£.RATI0^8. 


425 


Traversing  the  rhizome  in  a  longiludinul  direction  nre  bundles  of 
wooiiy  fibre,  soinetinie!)  inclusing,  iwuuUjr  one,  but  ucvasiunolly  two  or 
even  more  dotted  ducts  or  vessels. 

The  starch  corpuscles  resemble  in  some  respects  thoae  of  East  India 
niTOwroot,  Curctana  angHMfifoiia^  but  are  yet  characterised  bj  several 
Uisiiuci  ruuturcfl. 


«f  llM  tOigrr  rMaoMt,  dtfMivvd  of  lt»  tpidermk  :  m  u,  cvlla  poaiftfulBs  Ibt  •Ufclt 
corpiM»M  -.  *  i.  ttMnit  pmuvlct  >  c  c,  tunB«rie-Uk«  c«lU  i  d  d.  voeoj  tbn  i  c. 


Although,  like  tooee  of  C.  angv»tifolia^  thej  are  u^untly  elongdtc<I 
and  tiuttened,  they  yet  differ  from  the  stiirch  granules  of  that  pUnt  in 
being  somewhat  smuller.  less  elongated,  and  in  the  greater  obacurity 
of  the  bilum  and  cuivcfl  lamella*. 

The  fltructurcfl  above  described  are  shown  in  the  preceding 
drawing. 

In  ground  ginger  the  above  structures  are  separated  from  their 


Gtmutmt  prcNmrf  t/uvfr  •'  fl  a.  oclli  which  eonUln  the  «l«reh  eaniuvlct  i  6  b,  looM 
•Ur\'h  (TRttulc*  I  r  r,  turnwrie-Uke  oelb  i  </  tJ,  wtKNly  Abr*. 

O.N    TUB    Ai>t;LTEBATI01fS   OF   GlKGBB. 

In  order  to  improve  the  colour  of  gincer,  and,  Hccordinj?  to  some,  to 
protect  it  from  the  attacks  of  ia:*ects,  it  is  i'renuenfly  rubbed  over  with 
lime  ;  in  other  ca.'ies  it  ia  washed  in  cbalk  and  waler,  when  it  is  caUe<l 
tthiie-wwihed  ginger;  lastly,  tbo  fiurftice  of  ginger  is  occasionally 
bleached  by  tneiuis  of  a  solution  of  chloride  of  bme,  and  soraetimea 
even  by  exposing  it  to  the  futoca  of  burning  sulphur,  nnd  is  thus  made 
ro  present  a  white  ami  floury  iippeaiatice.  iJyJtbese  procesaes  ■□ 
interior  einper  is  often  maile  ro  assume  the  AppeK-anee  of  the  better 
(lesoxtpuons. 

But  gin<,'er  is  fretiuenlly  HduUerated.  Out  of  Twefit^-one  samples  of 
i:inf;er  subnutied  to  e:£aniin»tioiu  no  less  than /?/][«/*,  being  more  than 
two  thirds  ol' tlie  wliole,  were  fuund  lo  be  uiluUeraied, 

The  substances  detected  were  various  in  character,  including  »agn 
tiuaiy  tapioca^  potato  flour ^  wheat  flour,  ground  ricefCat^cMne  pepper,  mwc 


SPICES,    AND   TH£1R  ADULTERATIONS. 


427 


f^  hiuks^  and  turmeric  poictier^  —  these  occuirinjf  in  various  quan- 
li*N  but  ID  lUe  inajurity  of  ciues  cunslituting  iliepnucipul  purtuflhe 
rtiele. 
The  Cayenne  pepper  and  mustard  hasks  are  no  doubt  added,  with 


Ffg.  I5S. 


Gtson  ■diilknited  with  taiy)  §>ou<tter. 


»  m,  cell*  of  (iuer  i  6  k,  ttMich  irsnulM  vT  Klnf  nr  i  r  <-,  Urao  jrtUov 
kBitofdiw  lA  UMMof  tsnsctk  ,  </  it,  (ra^ineiit  of  xmmIjt  obn  i  c  e,ilueh  oor* 


rlew  orconccaliiig  the  other  adulteratiuus,  and  of  giving  apparent 
igtil  to  the  giiigirr. 


Ccnj 

On  the  Detection  of  the  AtUUierutions  of  Ginger. 

iTbewboIc  of  the  substances  cmplnved  in  tlio  a'lultenitiQn  of  ginger 
ky  \k  dftccted  with  eu»e  and  ctTtamly  by  iiic'iiits  of  ihe  micruscope. 
hr  niicrtuM-upifal  cburacter^  of  inOHt  ul'the  uiticles  useil  liavc  already 
ten  desj'ribed  :  as  wheat  lluur,  at  p.  243. ;  ^mumi  rice,  at  p.  ^-Od. ; 
tyrnne,  at  p.  37B. ;  —  those  of  the  rL*iiiaining  articles,  sagn,  at  p.  326. ; 
MB  floor,   at  p.  :t*iO.  ;  turmeric,  at  p.  3H9. ;  and  mustard  husk,  at 

SSettructural  peculiarities  of  Cayenne  and  mustard  husk  are  so  well 
Irked,  that  no  dillii-ulty  whutevcr  is  experienced  in  ideniifying  them 
ken  once  seen  under  the  microscope;  but  ia  those  cases  iu  which 


J 


4S8 


SPICKS,   AND   THEIK   ADULTKRATIOXS. 


the  quaniilies  present  are  but  sni&ll  they  arc  apt  to  be  overlonk(*ti. 
It  i»  l)dvi^3lJte  tu  wash  away  i^ome  of  the  filareii  rrom  ttic  jturtion  of 
powder  about  ,to  be  placed  under  ihe  tuicroscuije ;  by  ibia  uieaus  tbe 
larger  [wirtidea  are  brought  more  clearly  into  view. 


fif.  iw. 


•  ■,  atttl  af  fln|R  I  b  A,  ffUrdi  frmnnlc*  of  vinfvr ;  r,  larfv  fcllov  ecll,  antJofOM 
ta  Ihtpc  »(  turtntrk  i  tt,  woodV  Rbra  i  e  c,  «Uroh  ftmuulM  «I  fvUiki:  //,  tUitk 
iMriMiai:ln  »f  »agu,  ftllciwl  bj  tttaX. 


The  ailulteratlon  with  wheat  flour  is  one  which  might  readily  escape 
detoctiiin.  The  observer  is  therefore  cau(iont->J  hufure  |irocecding  to 
the  exuinination  of  |)«wdered  j;inper  lo  compare  carefMily  the  struc- 
tural peculiarities  of  the  starch  granules  of  ginger  and  wheat  llour  : 
the  diflerences,  altliough  not  at  first  striking,  an;  reully  cnnsidurable. 

Since  ginger  contains  yellow  cells  very  closely  resembling  those  of 
turmeric,  wl>  can  only  cuncliide  that  turmeric  has  b^-en  added  when 
the  number  of  such  cells  is  much  greater  than  in  genuine  powdered 
ginger. 

The  adulterations  of  ginger  with  sago  and  potato  are  exhibited  in 
the  two  preceding  ongravings. 

The  following  engraving  represents  the  adulteration  of  powdered 
ginger  with  tnpioca  and  Cayenne. 


SPICES,   AND  THEIR   ADULTERATIONS. 


429 


Ftg.  loo. 


f 


Pemlcred  Onronido.'  •'tullereiMl  wlih  ' 

Hftffniflcd  y)o  dlameim. 

The  duty  was  5*.  per  cwt.  British,  an<l  10«.  foreij^n  po.^tcssinns ; 
it  is  now  5it.  of  whatever  orifiin.  Imports  in  185-1,  24»8o;J  cwt5. ;  in 
18^5,  16f503  cwts.  Hume  cunsuaiption  in  1854, 16,637  owts. ;  in  1855, 
21.413  cw(«. 

The  duty  in  1851  aroounte<l  to  7,362?.  0*.  9^/  It  Oierefiire  foIlowB 
that  on  this  small  article  the  revenue  sufTerii  n  loss  through  its  adul- 
teration of  some  thousands  of  pounds  yearly. 


CINNAMON,  AND  ITS  ADULTERATIONS. 

Cinnamon  is  the  bark  of  the  Ciannmomum  Zfylamcumy  one  of  tiie 
Lauracee,  or  Laurel  family,  to  which  als^»  l>elon<*  CiLs.iia  and  dmiphnr, 
an  well  as  some  other  plaut«  poasessiu*;  medicinal  properties,  especially 
Clove  bark. 

Cinnamon  is  cultivated  principally  in  Ceylon. 

"  The  cinnamon  bark  of  Ceylon  is  obtained  by  tlie  culfclvatioo  of  the 


SPICES,  A2ffD  THEIS  ADULTERATIONS. 

plant.  The  principal  cinnamon  garden*  lie  in  the  neighbourhood  of 
Culumho.  The  bark  peelers  or  choiiafis,  having  selected  a  tree  of  ihe 
best  quality.  li»p  ofi*  such  branches  as  are  three  rears  nM,  and  which 
Hpuear  pmuer  for  the  purpose.  Shoots  or  branches  inui'h  \t.'*»  than 
hair  an  iiieti,  or  inure  than  two  or  three  inches  iu  liiameler,  ure  not 
peeled.  The  peeling  is  effected  by  aiaking  two  nppusitefor,  when  the 
branch  is  thick>  three  or  four)  lonjzitudinal  incisions,  and  then  elevat- 
ing the  bark  by  introducing  the  neoling  knife  between  Jl.  When  the 
bark  adheres  firmly,  the  f^cporation  is  promoted  by  friction  with  the 
handle  of  the  knife.  In  twenty-four  hours  the  epidermis  and  greenish 
pulpy  mutter  (rete  muco.sum)  are  carefully  w?raped  oiT.  In  a  few 
hours  the  smaller  quiU»  are  introduced  into  the  lar;;er  ones;,  and  in 
this  way  a  congeries  of  quills  formed,  ollen  mea»uring  forty  inches 
long.  The  bark  is  then  (fried  in  the  sun,  and  afterwartls  made  into 
bundles  with  pieces  of  bamboo  twigs. 

•'Cinnamon  is  imported  in  bales,  boxes,  and  chesU,  principally  from 
Ceylon,  but  in  part  also  from  Madras,  TcUichen-y,  and  rarely  from 
Java  and  other  places. 

**  In  order  tn  preserve  and  improve  the  quality  of  the  bark,  black 
pepper  is  sprinkleil  amongst  the  bales  of  cinnatnoii  in  stowing  them  at 
Ceylon.  (Peicival.)  Mr.  Bennet  ^tate8  tliat  ships  are  snmeilmes  de- 
tained for  several  weeks,  through  tlie  want  of  pepper  to  fill  the  inter- 
stices between  the  bales  and  the  holds. 

"  When  cinnamon  arrives  in  London,  it  is  unpacked  and  examined  ; 
all  the  mouldy  and  broken  pieces  are  removed  from  it.  It  is  then  re- 
made into  bales.  These  arc  cylindrical,  three  feet  six  inches  long,  but 
of  variable  diameter,  perhaps  sixteen  inches  on  the  average.  These 
bales  arc  enveloped  by  a  coarse  cloth  called  frutiuy.  The  ciimawon  in 
boxes  and  chests  is  usually  the  small,  inferior,  atid  mouldy  pieces.** 

Composition  of  Cinnamon. 

The  constituents  of  ciimamon  are  volntih  oil-,  tannin^  mucilage, 
Coiouring  mattrr^  partly  soluble  in  water  and  alcohol,  but  not  in  eiheTf 
r^Jthi,  an  ariW,  gtarrh,  and  li^in, 

A  decoction  of  cinnamon  does  not  become  blue  on  the  addition 
of  iodine  ;  ihi.-*  is  portly  owing  to  the  small  quantity  of  starch  pre- 
sent, and  partly,  it  is  supposed,  to  the  presence  of  some  principle 
(tannic  acid?)  which  destroys  the  blue  colour  of  the  iodide  of 
starch. 

The  cinnamon  oil  of  commerce  consists  of  two  or  more  bodies.  By 
exposure  to  the  air,  the  oil  absorbs  oxjgen;  and  cynnamic  acid,  two 
resins,  and  water  arc  formed.  With  nitric  acid  it  forms  .i  white  crys- 
talline nitrate  and  a  red  oil,  and  with  ammonia  a  solid  crystallinu 
amide  is  formed. 


SPICES,   AND   THEIR   ADULTERATIONS. 


431 


Sirvciure  qf  Cinnamon, 
Cinnamon,  under  the  microscope,  presents  a  complicaled  and  very 

Fig.  I8i. 


LoBtfiludiiikl fMtlaa  of  Ci jrvAMo*  carried  LruMrWMljr  Uinmch  the  terk ,  R»c&Ub4 

14i>  diAmeltra. 
a  H.  •l«II»iD  r«ll>  :  h  h,  woody  ilbrv  :  «  r.  stkreh  c«lb  t  d  </,  ctarefa  gniinUi  i  «  c, 

(MU)il4r  cUiftuaoa-coloiucil  c«U«  M  bodla*. 

distinct  organisation,  which  is  bcJit  seen  in  longitudinal  sections,  car- 
ried through  the  thickness  of  the  bark. 

Ou  ihe  outer  or  external  eurfiice  of  the  section  are  observed  nu- 
merous stellate  cells,  separable  readily  from  each  other,  and  siniilar  to 
those  which  we  have  so  otten  bi;fore  described  as  occurring  in  other 
vegetablu  structures.  These  cells  lie  one  upon  the  other  in  several 
luvers,  and  form  a  considerable  part  of  the  thicknei^s  of  the  bark. 
They  arc  situated  in  the  intcTTals  between  the  woody  fibres  ;  tbey  are 


43t 


SPICES,  AND  THEIA   ADULTERATION'S. 


of  a  qundrnngnlnr  or  oval  form,  having  the  long  axes  placed  usually 
transversfly  to  the  baric,  iheir  breailtb  beinrg  preiittrr  tban  their  depUi. 
In  whatever  position  iliey  are  viewe^U  both  the  central  cavities  and 
the  rays  which  proccotl  from  them  are  visible.  Occasinnally,  though 
not  uBunlly,  a  few  stanh  granules  inay  be  seen  in  the  raivitics  of  these 
cells.  Proreediri^  from  without  inwards,  these  cells  are  succeeded  by 
others,  whieh  are  diatinjriiished  fmm  the  first  by  the  absence  of  raya, 
by  the  thinness  of  their  whIIh,  and  by  the  firmness  with  which  they 


fig-  1G& 


-Lc 


.*v1 


•:-«» 


^- 


Ommim  Cuutakov  pmnhr,  «nRfB)B*4  t9n  dtimctert.    o  a,  itolUle  eelli  t  ft  &i 
woody  tW«  1  e  t,  rtanta  gr*uul«i. 

adhere  to  each  other  ;  they  (renernlly  contain  a  few  jitarch  corpuscli 
These  cells,  which  form  several  series,  complete  the  thickness  of  tlie^ 
bark. 

Interspersed  between  both  the  first  and  second  kinds  of  cells  are 
numerous  woody  fibrep,  which  are  rather  short,  pointed  at  either  ex- 
tremity, and  fumi&hed  with  a  central  ennid.  It  U  these  which  impart 
the  fibrous  character  to  cinnamon,  particularly  obserTublc  in  fractures 
of  the  bark. 

The  »tarch  corpuscles  of  cinnamon  are  small,  more  or  less  globular* 
•mi  funiiflbed  with  a  very  distinct  hilum,  which  has  the  appearance  of 


8PIC£3»   AKD  THEIB  ADULTERATIONS.  433 

a  central  depression.  They  TuaaUy  occur  singly,  but  sometimes 
united  in  twos  or  fours. 

The  quantity  of  starch  in  cinnamon  is*o  small,  that  the  decoction 
of  the  bark  does  not  become  blue  on  the  addition  of  iodine. 

Lastly,  lying  in  the  cavities  of  the  most  external  of  the  second 
order  uf  colls,  are  frequently  to  be  observed  deep  cinnamon-coloured 
masses  of  granular  texture. 

The  above  structural  particulars  are  all  shown  in^.  161. 

In  ^ound  cinnamon  the  several  structTircs  are  disunited  and 
broken.  Tlie  stellate  cells  occur  stnglr,  or  in  grou|>s  of  two,  three,  or 
nion.';  the  wnody  fibre  is  disengaged,  and  is  scattered  fibaut,  resem- 
bling somewhat^  in  form  and  appearance,  the  hairs  wtucb  occur  on 
many  plants ;  the  starch  corpuscles  are  set  free  from  their  cells ;  and, 
lastly,  the  cinnamondlke  masses  maybe  seen  in  the  field  of  the  mtcro- 
Hcope,  dispersed  here  and  there.    Pig^.  162. 


COMPOSITION  AKD  structure  OF  CASSIA. 

Cnrnposilinn  of  Cassia. — Since  cassia  is  so  frequently  substituted 
for  oinnaiiiiM),  it  becomes  necessary  that  we  should  acquaint  ourselves 
with  its  composition  and  structure. 

If  tincture  af  iodine  is  added  to  a  decoction  of  cassia,  it  turns  blue, 
owing  tn  the  larger  proportion  i>f  filJirch  contained  in  it. 

Oil  of  cassia  y>o9SCHse3  nearly  the  same  properties  as  oil  of  cinnamon ; 
it  is  said  to  be  a  thicker  nnd  heavier  oil  than  that  of  cinnamon  ;  and 
its  oilour  and  flavour  are  inferior. 

StmctMre  of  Cwuia, — CasMa  —  Cinnamomum  Caiuia  —  belongs  to 
the  same  genus  of  pUnts  as  the  true  cinnamon,  it  is  therefore  not  sur- 
prising thiit  they  should  resemble  each  other  90  closely  as  they  do. 
Notwithstanding  their  striking  resemblances,  there  are  characters, 
however,  by  which  they  may  be  discriminated. 

The  bark  of  cinnamon  is  scarcely  thicker  than  drawing-paper,  and 
breaks  with  an  uneven  and  fibrous  margin;  while  each  slick  consists 
of  eighty  ten,  or  more  pieces  or  quUls  of  bark  inserted  one  within  the 
other. 

Cassia  bark  is  much  stouter,  being  oflen  as  thick  as  a  shilling :  it 
breaks  short,  and  without  splintering.  Ry  these  characters  alone  it 
is  easr  to  distinguish  cinnamon  from  ca<4sia  when  in  (he  whole  state, 
as  shown  by  the  accompanving  drawing. 

But  these  barks  differ  afso  in  colour  and  t.istc.  Cinnamon  is  paler 
and  browner  than  cassia,  which  is  usually  redder  and  brighter.  The 
taste  of  one  is  sweet,  mild,  nnd  aromatic,  leaving  no  unpleasant  im- 
pression on  Uie  t^mgne,  white  that  of  the  other  is  leas  sweet,  stronger, 
and  b  followed  by  a  bitterness. 

r  r 


4U 


These  characters,  however,  vary  In  different  samplea,  »o  that  it  is 
iinpossibte  by  these  meam  alone  to  distinguUh  cinnonion  from  cassia 


A,  Stick  orCivirAHOir  ortha  oitoml  •(«•  tad  sppearMiDe,  ibowtntf  th*  tblsnea 
at  tbc  iMrlt.  mnd  the  muincr  la  whkh  tbe  Uytn  art  cncloacxl  ine  wItliiQ  Um 
olhrr  I  (1.  rriM  »rrtiiin  iif  aamc,  eahilillliif  more  cucnplcUlj  the  number  of  Ih* 
Iktcn,  atiil  lltrir  dit[KMtUoii. 

S,  elk\.  uf  Camia  ftf  tlx  i)*tiir*]  >iu  uid  apprar»Dce.  •tiowliig  Um  thicknMi  uf 
thi  b&rk,  and  t)i«  ni«BU«r  in  aliicli  tli«  Ur«ra  an  vtK!l<H»<l  orlthlttauhoUur  | 
i,  eroM  McUon  of  Mitu,  cxhibltiag  tha  dUpoaltluu  of  llic  laTcr*. 

when  in  powder,  and  we  are  not  aware  thut  any  oertaiD  menns  have 
beca  pointed  out  ibr  cffecling  tbe  di!k.Tiiuiiiation,  especialijr  when  the 


SPICES,  AND  THEIR   ADULTEUATJ0N8. 


435 


tvro  are  mixed  in  dltTerent  proportions ;  but  here  again,  u  in  »o  many 
olher  cases,  the  microscope  ailbnis  us  tnvaluable  assiittaacc. 

Sections  of  caMia  bark,  viewed  under  the  luicroecope,  bear  a  close 
general  resemblance  to  thoae  of  cinnamoUf  but  dilTer  m  their  greater 


Loiiflltadliul  MettM  of  Casua,  evrtwl  tnnmrKir  through  tlui  berk,  mafnlffeil 

iwdiunelwn. 
o  a,  mIU  or«pld«rail>  t  b  *.  •telUlc  mH*  i  ti  d,  lUrch  mIIi  j  «  <,  flUntfa  gtannks  i 

f/,  frwittUr,  ctuuunoB-a»lwur«<l  mu>mt. 

width  and  the  relative  proportions  of  the  several  structures,  particu- 
larly in  the  Hize  and  iiumbcr  of  the  starch  (^Y>rpusrlcs. 

We  observe  on  the  outer  surface,  as  in  cinnamon,  the  peculiar 
stellate  cells,  the  cavities  of  which,  hnwcver,  much  more  commonly 
thun  those  of  ciuiiamon,  are  lUled  with  well-develo{)ed  etorch  cor- 
puscles. 

Lying  next  to  Uiese,  we  notice  what  may  he  termed  the  proper 
starch  cells,  usually  crammed  quite  full  of  starch  corpuscles,  which, 

r  r  3 


436 


SPICES,    AND   THEIK    ADULTERATIONS. 


while  tbey  have  tbe  same  general  form  as  those  of  cinnamon,  are  yet 
two  or  tliree  times  larger,  as  well  aa  many  limea  more  numerous. 

The  woudy  fibre  occurs,  &i  in  cinnamon,  inlersncrded  between  both 
descriptions  of  cells,  and  it  does  not  appear  to  ditter  appreciably  from 
that  of  clanamon. 


Fig.  IC& 


Oamti»t  CtiUTt  pDmln-,  rnKprrlftcd  790  dUrMten  i  n  «t. rtelUle  wDi :  AK.Tnedj' 
Sbrc  t  c  c,  aurch  celli  i  <i  <t,  rkicn  grtnulc*  ;  e  t,  gruialu  mmw. 


Of  the  entire  thickness  of  the  bark,  about  one-fourth  is  formed  by 
tbe  stellate  celts,  the  remaining  thrce*f'ourttiB  being  made  up  of  the 
Btnrch-bearinjj  evils. 

In  powdered  cassia,  therefore,  as  contrasted  with  powdered  cinns'- 
mon,  the  stellate  cells  and  wcvody  fibre  are  miiL-h  less  abundant,  while 
the  starch  granules  arc  at  the  same  time  much  larger,  and  tar  more 
numerous. 


SPICES,   AND  THEIR   ABULTERATIOKS.  437 


Oh  ms  Adulteeations  or  Civramov  ahd  Camxa. 

From  an  examination  of  tl»e  analyses  of  Thirty-lwo  samples  of 
cinnamon,  it  appeiired  that  of  the  twelve  whole  ciiiniunons,  jfMn 
were^pnuiw,  ami  \\\aX  five  consisteti  of  notliing  hut  cassia. 

That  the  essetdial  oil  \s  »ometin)C!<  abstruoled.  ami  the  bark,  after 
bcinf?  reduced,  soM  cither  whole  or  in  the  ground  suae. 

Tliut  of  the  nineieen  sampled  of  ^roumicinuamonf  three  consisted  en- 
tirely of  cauia. 

That  ten  of  the  samples^  or  more  than  one  half,  were  adulterated^ 
the  artiflex  most  frequently  employed  bein/;  cither  baked  wheat Jiour 
or  Ktgo  meal,  &epanitely  or  in  cnnthiiiatinn,  hut  Ktist  huita  arrowroot 
and  potato  Jiutir  were  likewise  dt*tecti*d  each  in  one  inetance. 

That  of  the  above  adulterated  sniiifites  three  Konaisied  of  cassia 
ailulteratedf  and  seven  o^  cinnamon  adulterated. 

That  six  only  of  the  nineteen  suiuplea  were  ^'tfBH/atf. 

In  the  prices  chiirged  for  the  sample9  of  einnainon  examined, 
whether  whole  or  in  powder,  ^'nuiiie  or  adulturated,  no  eon»tiint 
di0erence  waa  tu  be  observed,  and  cun»equently  the  public  AufTers 
great  loss  by  the  substitution  of  caisiii,  which  is  so  tiiueh  eheu[>er,  for 
einnamon,  and  a  still  jfretiter  loss  by  the  other  sophistications. 

The  wheat  flour  and  sa^o  detected  was  generally  baked,  to  make  it 
resemble  more  nearly  ground  cinoamun  or  cassia,  and  thus  the  better 
escape  detection. 

On  the  Detection  of  the  AduUereUions  of  Citauwum  and  Cassia. 

The  detection  of  the  various  adulterations  of  cinnamon  and  cassia 
is,  in  nearly  all  ciises,  easv  enough  by  means  of  the  uiieroscope  ;  a\\  that 
is  reqtiisite  is  tltat  tlie  ohserver  should  be  acquainted  with  the  struc- 
ture and  characters  of  genuine  caA.«ia  and  cinnamon,  as  well  as  of  the 
articles  em;:loyed  toadult(>rat4>  thcni. 

The  mixture  of  cassia  with  cinnamon  of  course  constitutes  an  adul- 
teration,but  very  frcouently  eaasiu  is  suhstiinted  for  cinnamon.  The 
mixture  and  substitution  arc  both  di»i.'Overable  with  the  microscope  by 
the  difference  in  the  size  of  the  starch  granules,  but  the  substitution 
may  be  detected  in  other  ways. 

Thus  when  slick  cassia  is  substituted  for  cinnamon,  the  substitution 
is  known  bv  the  areafer  thickness  of  cassia  bark. 

Again,  iLe  decoction  of  cassia  hark  turns  blue  on  the  addition  of 
iodine,  when  one  of  cinnamon  similarly  treated  does  not  become  blue. 

It  ia  stated  thut  the  oil  is  i^ometinics  removed  from  cinnamon  bark, 
this  being  subsequently  ground  to  powder  and  mixed  with  genuine 
ciimunion. 

This  fraud  may  be  discovered  in  two  ways  :  the  suspccletl  ciruiamon 
may  be  boile*!  in  distilled  water  for  a  time  and  the  oil  distilbnl  off;  the 
diatillate  mual   next  be  evapomted  to  get  rid  of  the  water  which 


488 


SPICES,  AND    IHEIB  ADULTERATIONS 


passfd  over  with  the  oil;  lastly,  the  oil  must  be  weighed,  and  the 
quantitj  oMalnt'tJ  compared  with  thnt  furnthhed  by  pcnuine  cinnamon. 

A  more  i'xpi-4itit>u5  process  is  to  examine  the  cinnftiiion  with  the 
microscope ;  if  thts  lias  been  acted  ujwm  by  U/ilinj;  water,  the  starch 
pranulcs  will  he  foun<l  to  have  lost  tlipir  projKT  fnrni,  to  have  become 
distort^-d  and  irregiilnr,  while  many  of  tliein  are  larger  than  natural. 
It*  the  einiianion  has  been  subjected  to  the  prohmged  action  of  the 
water,  the  granules  will  hare  become  so  broken  up  and  dissolved  that 
they  can  no  longer  be  detected. 

The  import  customs  duty  is,  on  cinnamon,  2d.  per  lb.  The  quan- 
tity entered  for  home  consumption  (which  forms  but  a  fraction,  about 
1-I3tb,  of  the  quantity  imported)  was  in  IHUli^  57,fi94  lbs.;  in  1854, 
54,056  lbs.;  in  1855,  42,943  lbs. ;  in  nine  months  of  1856,  22,771  lbs. 

On  cassia  (Itgnca  or  bark),  Id.  per  lb.;  cassia  buds  and  fistula,  frco. 
"Were  entered  fnr  home  coii!<uniption  (again  but  a  fraction,  about  l-6ih 
fo  l-7th,  ot'qunnlitv  impnrled)  in  185^  136,363  lbs.;  iu  1854,  124,303 
lbs. ;  in  1855,  110,219  Ihs.;  ia  nine  muntlis  of  185G,  90,197  Iba. 


NTTTMEGS,  AND  THKIU  ABULTEHATIONS- 

Tlierc  are  three  species  of  Alyrixtivu.,  whlt-h  furnish  nutmegs.  That 
which  yields  the  best  deacription,  Myristica  /rtifrran:!^  forms  a  tree 
from  twenty  to  twenty-6ve  feet  high,  somewhat  similar  in  appearance 
to  a  pear  tree. 

The  fniit  is  smooth  externally,  pear-shaped,  and  about  the  size  of 
an  ordinary  pcaoh.  It  consists,  firi^t.  of  au  outer  lleshy  covering, 
called  the  pericarps  which  when  uniture  separafes  into  nearly  enual 
longitudinal  parts,  or  valves  ;  secondly,  of  the  an/,  or  mace^  which, 
when  recent,  is  of  a  bright  scarlet  colour;  and  thirdly,  of  the  seed 
proper,  or  nutmeg.  This  is  enrlosed  in  u  sht-U,  which  is  made  up  of 
two  coats  ;  the  outer  is  hnrd  and  smooth  ;  the  inner,  thin,  closely 
invests  ihe  seed,  sending  off  prolongations,  which  enter  the  substiinee 
of  the  seed,  and  which,  being  cohinred,  impart  the  marbleil  or  mottled 
appearance  chupacU'ristic  ofnutmejj. 

There  are  two  krnd^  of  nutmegs  met  with  in  commerce.  The  first, 
calletl  the  trve^  rouiuU  rnltivated,  or  female  nutmeg,  is  the  product  of 
Jlfi/ristica  fragrtmti. 

The  seconii  kind  of  nutmeg  ia  called  i\iQ  false,  long,  wild^  or  vude 
nutmeg,  and  is  the  produce  chiefly  ot  Mgrintica  fatiiti ;  but  a  kind  of 
nutmeg  which  is  also  called  wild,  is  obtained  from  Myrittica  Mala- 
bariitt. 

In  the  Banda  Islands,  three  crops  or  harvests  of  nutmegs  are  ob* 
tained  in  the  year  ;  the  principal  gathering  h  in  July  or  August;  the 
secuiid  in  November ;  and  the  third  in  March  or  April. 


BPICES,   AKD   THEIR    ADULTERATIONS. 


4.19 


The  fruit  is  (fathered  by  means  of  a.  barb  iittachc<3  to  n  long  stick ; 
the  mace  ia  separntcfl  from  the  nut,  anfl  sepurnt*'!/  cured. 

On  aecouDt  of  their  liability  la  the  attacks  of  an  insect  known  as 
tbe  nutmeg  insecU  conHdcrftblecare  is  required  indryinir  them.  They 
shnuM  be  dried  in  their  shells*  as  ihey.ire  then  secure  frnm  the  insect. 
They  arc  ])laced  on  hurdles  and  sinoke-dried  over  a  slow  wood  fire 
for  about  two  months^  In  the  BMnda  Islands,  they  are  first  dried  in 
the  Bun  for  n  few  days.  When  the  ojwrotion  of  drying  i<  compIetQi 
the  nut-s  rattle  in  their  shells ;  these  are  cracked  with  mallets,  and  the 
dama;;ed,  shrirelled,  or  wnrni-caten  nuts  removed. 

"To  prevent  the  attjuka  of  the  insect,  the  nuts  arc  frequently 
limed.  For  the  English  market,  however,  the  brown  or  unlimed 
nutmeg  are  preferred.  The  Dukh  lime  them  by  dipping  them  into 
a  thick  mixture  of  lime  and  water ;  but  this  proeefla  is  considered  to 
injure  their  flavour.  Others  lime  (hem  by  rubbing  ihem  with 
recently*prepared,  well<sifted  lime.  This  process  is  soiuelimes  pmc- 
tiscd  in  London." 

Composition  of  Kutmegs, 

Nntmegs  contain  bnth  a  fixed  an<l  a  volatile  oil.  Th^  Jix&l  oil  is 
prepftred  by  beating  the  nutmegs  to  a  paste;  this  is  subjected,  en- 
closed in  a  boi;,  to  the  vapour  of  water,  iinil  llie  oil  afterwards  ex- 
f pressed  by  meaas  of  heated  pluteii.  It  is  Imported  in  cakes  whicb 
lave  somewhat  the  size  and  form  of  common  bricks,  and  are  covered 
with  leaves.  The  6xe<J  oil  procured  in  this  manner  contains  a  por- 
tion of  the  volatile  irilf  from  which  its  colour  and  fragrant  odour  are 
derived. 

The  volatile  oil,  on  the  presence  of  which  the  flavour  and  aroma  of 
nutmegs  principally  depend,  is  procured  bv  distillation  in  water ;  the 
produce  thus  obtained  at  Apothecnries*  IIhII.  London,  is  usually  4'5 
per  cent.  Now,  nutmess  are  frequently  deprive<l  of  a  portion  of  their 
essential  oil  by  distillation,  and  ai'ter  being  well  limed,  are  again  sent 
into  the  market  io  this  comparatively  valueless  state. 


Bonastre*s  AmtljfnM* 


Volatile  oil 
Liquid  fat 
Solid  fat     * 
Acid 
Starch 
Gum 

Ligneons  fibre 
Loss 


«0 
7-6 

24-0 
08 
24 
1-2 

540 
40 


10(K) 


•  JMira.de  Phmv.  IMS.  I.  ii.p. 
r  r  4 


sii. 


4«  anCBBf  ASP  THEIK  ADCLTKKA 


Ulfce»clk»  of  vatcr 
iW^VBMity  of  oil  ■■tilled 
«aRl^  01  the 


IMrh.MmBi^   Stt  MI7.     4E. 


Jt  of  m  rnunded  shape  ;  bot  occasion&Uj  k  few  of  ihc  granules 
itar;  »m]  all  have  wvll-marketl  central  depreanon*. 
«be  oelU  forming  the  coloured,  vein-like  portion  of  ib«  nut,  diL- 
from  ibe  other  cell))  in  colour  and  in  b*:*in^  des>tiltttc  of  Starch,  ctm< 
f  %;r>:n<r  ftpfiflrvutljr  onljr  a  Bmall  quaniilj  of  oil.  _ 


-c 


SPICES,   AND   THEIR   ADULTERATIONS. 


On   TUB  ADULTSaATIORS   or  NUTMBGI. 

Since  nulmega  tre  never  solil  in  the  powdered  state,  they  are  not 
lialilo  (u  itdulteration  hv  udmixtut-e  witb  foteijpi  in^L'diL*nUf  like 
SL'vorul  of  the  apices  wLicb  liiivti!  been  already  iiotim-d,  aa  ginger, 
ctnimitintu  and  vii»i*'m  ;  nevurtht.*less,  ihey  are  subjected  to  a  proi-'esa 
which  impuird  their  value  and  quuliiy  us  uiuch  as  thau^L  they  hod 
been  actually  odulterateii  in  ibe  same  niaiiner. 

The  wild  nutmeg  obtained  froni  the  Mijrutica  Maiahariea  has 
scarcely  any  flavour  or  odour,  and  nccortlinf]!  to  Kheede,  is  of  the  size 
and  H^ure  of  a  date.  "The  Turkish  and  Jewish  merchantV' writes 
Kheede,  "mix  these  nutmegs  with  the  true  long  ones,  and  the  mace 
with  good  mace,  selling  them  together.  They  also  extract  from  these 
inferior  articloa  an  oiX  with  which  they  adulterate  that  of  a  more 
genuine  (juality." 

The  w(irk  of  M.  Chevallier,  entitled  "  Dictionnaire  des  Alterations 
efc  Falsifications  des  Sub>l»nces  Alimentairc.%  MedicarnenteuKa,  et 
Commtfrcialea,"  in  treating  of  nutmegs,  cimtains  the  following  ubser* 
vations,  uuder  the  head  of**  Falsifications  :'* — 

"Nutmegs  are  sometimes  mixed  with  riddled  nuts,  eaten  by  insects, 
and  bccume  brittle;  the  small  upertures  are  then  closed  with  a  kind 
of  cement,  formed  of  flour,  nil,  and  the  powder  of  nutmegs.  This 
paste  bos  even  ser^-ed  to  fabricate  false  nutmegs,  inodorous  and  in- 
sipid. The  workmen  of  Mar^^eilles  have  even  made  thein  of  bran, 
cuiy,  ami  the  refuse  of  nutmegs:  these  nutmegs,  placed  in  contact 
with  water,  soften  down  in  that  liquid. 

'*  The  worm-eaten  nuts  are  et]ually  insipid,  and  almost  inodorous; 
sometintes  they  have  u  mouldy  odour.'* 

Eighteen  snmples  of  nutmegs  were  subjected  to  examination,  the 
result  being  thai  in  no  case  had  the  esstntial  oil  been  abitractrd. 

On  the  Detection  of  the  Adulteridiona  of  Nutmegs. 

The  only  adulteration,  excepting  that  by  admixture  with  wild  nut- 
megs, to  which  itappearij  that  nutmegs  arc  liable  —  and  this  d(.uht)ess 
is  of  rare  occurrence  — is  by  means  of  the  artificial  or  factitious  nul- 
megs  mentioned  by  M.  Chevallier. 

'i'l)et«  may  be  readily  discovered  by  soaking  them  in  water,  when,  of 
course,  tliey  would  reatlily  break  down. 

The  diflerenccs  between  the  cultivated  and  wild  nutmegs  have 
alrea<ly  been  describe*!. 

The  iiurmegs  from  which  the  oil  bns  been  abstracted  muy  Iw  re* 
cognised  by  the  presence  of  punctures  on  the  surface,  and  by  their 
much  greater  li;.'htness. 

It  is  singulai-  that  the  starch  granules  of  nutmeg  are  but  little 
aflected  by  boiling;  so  liiatthis  means  of  discrimination,  bO  satisfac- 


I 

i 


44S 


SPICES,   AND   THEIR   AP0LTEKATIOH8. 


torj  in  the  case  of  cinnamon,  rassta,  and  some  other  spices,  U  of  little 
or  no  valiiff  in  the  present  instance. 

Of  this  rcnmrkable  circumstance  it  is  not  easj  to  aSurd  aa«x[^ui*> 
tion;  it  probably  diipunds  U[>on  the  dilliculty  with  which  the  boi&if 
watur  muKOJ»  its  way  into  thti  substance  of  the  nut,  in  confet^ttCMem 
its  httrd  texture  unci  the  largo  ijuaiitity  o(  fixed  oil  contained  ia  iL 

The  iliOerentiul  duties  on  wilil  and  cultivate*!  nutmegs  oScT  I 
premium  for  the  substttutinn  of  the  inferior  for  the  Miperior  iitidt 

Import  duty  on  nutinogH^  Ix.  per  lb.;  wild,  so  called,  in  dwUla 
per  lb. ;  wild,  not  in  Rhell,  5iL  per  lb. 

Tnkon  for  home  con-iuinption  in  1854,  "206,049  lbs.;  la  )i^y 
i8£>,5l>6  lbs.;  in  nine  months  of  1866,  15-i,3ttO  lbs. 


r 


MACE,  AND  ITS  ADULTERATIONS. 

As  there  are  two  kinds  of  nutmeg,  so  are  there  two  kindi  ofmaA 
the  produce  of  the  same  plants;  thus,  there  is  true*  or  cultinErl 
mace,  and  fuUc,  or  wild  mace. 

Wild  or  false  mace  is  of  a  dark-red  colour,  aad  deficient  in  tfwt 
and  aroma. 

Compogiiwm, 

The  composition  of  mace  is  exhibited  in  tbo  following  antlnis  hf 
N.  E.  Henry  :— 
Volatile  oil. 

Red  fut  oil,  soluble  in  alcohol. 
Yellow  fat  oil,  in^'oluble  in  alcohol. 
Alcoholic  extractive. 
Amidtiu. 
Ligneous  tibre  with  lime. 

Structure  of  Maee, 

Viewed  under  the  microscope,  maco  presents  a  atructnre  Tef7  iof 
tinct  from  that  of  the  nuimeg  itnelf. 

Covering  the  surface  of  the  blades  is  a  delicate  membrane  eono^' 
ing  of  A  single  layer  nf  cells;  they  are  tubular,  mnch  elcm!*aied,  tspff 
at  either  end  to  a  point,  And  resemble  in  size  and  form,  altboo^  >* 
in  delii'acjr  of  texture,  ordinary  wooily  fibre.  The  long  diamclinfl' 
the  cells  arc  disposed  vertically  on  the  surface  of  the  inncc. 

But  the  chief  Hub«tance  is  made  up  of  other  cells  differing  ta  ■* 
and  form  from  those  already  noticed ;  these  contain  fixed  oil,  and  M^ 
starch. 

Imbedded  in  the  midst  of  these  cells  are  larger  eelU«  anuaa  cct* 


8fICE9,   AXD   THEIR  ADULTERATIONS, 


443 


ceptaclet^  which,  in  thin  sections,  whether  made  crosswise  or  length- 
wine,  Appear  as  apertun^s.     Tbcite  oontnin  the  essential  oil  of  mace. 

Scattorc'l  here  and  there  may  be  «ecn,  both  in  transverse  and  longi- 
tudinal Elections,  small  bundles  of  woody  fibre,  of  a  brownish  colour, 
enclosin;;  one  or  two  small  spiral  vessels.  In  transverse  sections,  the 
ordinary  starch  cells  arc  perceivecl  to  be  arranged  round  the  bundles 
hi  II  radiate  manner. 

The  Ftructure  of  mace  is  exhibited  in  the  annexed  wood-cut. 


TKAJrarciuK  Srcnojr  or  Macs. 


.  a,  rtccpUclu  tut  the  CMeolUI  oil  i   minj  at  then  anpemr    in  tlw  mrtlnn  u 


the  «MW«r«BO*  of  cloaMt  cctl*.  fn>m  the  drrumrtancc  of  their  not  being  cut  into 

til*  coumrififf  im"' 

Iwf*  ftlr-bUDNM  UMMlIf  ntMcmd    in    >Kti>tn«   immerfvd  tn  wkUr.     rf<l,  cclla 


nMllrri^mae*  !•  ItKatnl  citlpftr  in  thew  relU  or  renptaelM. 


flilM  with  flATch  curpUMie*.       r.    Ihc  itvch  cirpuarlea  Ioom.  mifnlflcd  430 
dluiwtcn.   /  tha  oeU*  fonalnf  tba  delletu  eoAt  or  eutkia  InvMlag  mftM. 


On  THB  Adultkbations  or  Macs. 

Like  the  nutmeg,  mace  may  be  deprived,  by  distiUation,  of  its 
esitenlial  oil. 

The  only  ailultcration  of  mace  known  to  be  practised  is  that  by 
admixture  with  wild  mace  ;  this  is  disiin^iished  by  its  dark-red 
colour  and  by  its  deficiency  in  flavour  and  artana. 


k 


444  8PICE8,   ANT)   THEIR  ADULTERATIONS, 

Of  Twelve  samples  of  mace  subjected  lo  examinatioa  the  whole  were 
genuine. 

Import  duty*  1^.  per  lb. 

UoiuG  consumption,  in  18^4,  2J5,584  Iba. ;  In  1855,  28,562  Iba.;  in 
nine  montliff  of  1856,  15,267  lbs. 


CLOVES.  AND  THEIR  ADULTERATIONS. 

Clovei  are  the  uncxpantled  flower-budu  of  Vuryophylltu  arotnaticutt 
a  tree  from  fifteen  to  tiiirty  feet  in  hei^jlit,  one  of  the  Myrtaoeto  or 
myrtle  tribe.  The  wonl  t-^i^re  \a  deriveil  from  chtt  —  Fri'nch  for  nail, 
from  a  faiicied  resemblance  to  a  nail  in  ihe  form  of  the  elore. 

The  flower-buds  are  arranjiLMl  on  termineLt  ib>wt'r-fttiiJk«  ;  they  aro 
either  ^'athere<l  by  hand  tir  obtained  by  beatinj^  with  bumlles  of  reeds, 
in  whJL-h  ctute  eioihti  are  itpread  Ueneuth  the  treea  tu  ealeh  ttit-m  ;  ibey 
are  afterwards  dried  either  by  the  fire,  or,  what  is  belter,  in  the  sun  ; 
they  are  imported  in  casks  or  bags. 

Composition  of  the  Clove. 

Cloves  contain,  according;  to  the  analysis  of  Trommsrlorf,  tolaiilf 
oil,  18;  altnoHt  ttmttrless  reMtiiy  G  \  tannin,  13;  diJicvUly-tolublf.  cTtraC' 
tive  icith  tutiian^  4  ;  gum,  13  ;  woody  fibre,  28 ;  and  water,  18. 

The  volatile  oil  is  obtained  from  cloves  by  rcfteated  diittillation. 
The  yield  on  an  average  is  said  lo  be  from  seventeen  to  twenty-two 
per  cent. 

It  has  been  aaicertainetl  that  the  oil  which  was  formerly  reyarde*! 
as  a  simple  oil,  is  reallv  c:i>!nj)ri4i,*i.l  of  two  vohitile  oili»,  possessiojj  dif- 
ferent i|ualitie9,  one  of  which  is  lighter,  and  the  other  heavier  than 
water. 

The  characters  and  composition  of  these  oils  are  thus  ^ven  in 
Pereira's  "Materia  Medicu.'*  ed.  1.  part  ti.  p.  1093. :  — 

•'a.  Light  Oil  of  Cloven  (Clftve-Ifytiro-Carbfm).—Co]o\ir\ess  sp.  gr. 
0'918.  incapable  of  cumbiuing  with  bae<eii,  but  absorbing  hydrochloric 
acid  ifas  without  yielding  a  crystalline  compound.  It  consists  of 
C,(,  n,  ;  hence  it  is  isomeric  with  uil  of  turpentine. 

**/3.  Hearry  Oil  of  Clocen  (Clove  Acid;  Engenic  Acid). — It  is 
colourless  when  receittly  prepari'd,  but  beccmen  coloureil  by  age.  Its 
specific  gravity,  according  lo  Bonastre,  is  107'^.  It  combines  with 
alkalies  lo  fonn  crystalline  salts  (alkaline  evgennte*^  clove-oil  alhalieg). 
If  a  »alt  of  iron  be  added  to  one  of  these,  it  yields  a  blue,  violet,  or 
reddiflh  compound  {a  f err uginottif  eugenate),  varying  somewhat  acconl- 
ing  to  the  nature  of  the  ferriiginou!>  salt  uined  ;  thutt  the  protusulphate 
uf  iron  yields  a  lilac,  the  persulphate  a  red,  which  becomes  vtotei  and 


SPICES,   AND   THEIR   ADULTERATIONS. 


445 


af\erwnnls  blue ;  while  Uie  sesquichloride  gires  a  vinous,  which  turns 
U)  red  (Ifcjnasire).     Nitric  acid  reddens  cldve  acid." 

The  iinex|)anded  flower-buds  are  not  the  only  parts  of  the  tree 
which  are  aromatic,  oa  the  (ootdtulks  and  fruit  or  seed  vestieU  are 
likewise  so  to  some  extent. 

The  peduncleR.  or /itotstalMs,  according  to  Guibourt,  are  aometimea 
substituted  for  cloves  by  distillers  of  the  oil. 

The  frulti  mother-^ves  oa  tliey  have  been  colled,  are  occasiouaUy 

Ftf.  16(4. 
PtTAL  or  OLDri'BCik 
(Uifnllkd  00  dlwBiton). 


A,  trkii««»nw  Motion  of  Ui« 
otptactca  In  vhirh  tlte  tmvn 
necjMarka  fur  Um  otl  In  ihU  vlrw  are  iiHltittnct. 


mUI  of  flnver-lnul  of  rinre.  •hovtnf  the  r^ 
Ikl   ull   \»  itinUlneU.      B,  tnrfKOt   of  pcUt  |  tb« 


met  with  in  commerce;    they  have  the  shape  of  the  olive,  but  arc 

CHuUer,  and  poasesa  the  odour  and  taste  of  the  clove  in  a  mild  degree. 
■  Strwcture  of  the  Chve. 

The  minute  alructure  of  cloves  i»  extremely  characteristic.     The 
rounded  head  or  Imd  cooauta  of  the  unexpanded  petals ;  if  a  transverae 


J 


8PICES,  AND  THEIB   ADULTEBATI0N8. 

section  of  one  of  these  be  made,  it  will  be  seen  to  be  composed  of 
cellular  tissue,  in  tbe  luitlst  of  whicb  are  muueruus  receptacles  for  the 
essential  oil  ^  tbese  extend  tbruugh  the  whole  thickness  of  the  leaf, 
being  Usually  three  or  four  deep. 

TMXMtnnt  8ccTio>  or  FLOiraB<iTA.LK  or  nu  Cum. 
i  U»r>fSed  M  dluneUn. ) 


A  rwtplMlw  lot  tho  CHRitial  oU  I  Ihe  PMtlon  belnf  i,  ihtn  one,  they  P««f"* 
tH«appcsrmnoeorft|irnum,lii  onufeqiiwio*  oftwhut  or*rwl  Into.  ^^  orlluiy 
tiM««  lummnillnK  llw  wiwjy  ftbee.  c  r,  h<in.)lr-  .if  w^tmIt  fibre-  »•  "» 
tuboIuilnwturtftndtnUTVlNUM.atf  which  trwlnicrTi»i  p.rtl»m  »ti\tt  •****}• 
fonaad.  r.  the  criilre  nfthe  aUlk  i  II  Mi|M!*n  d*rk  uuilu  U)«  mJcriMOOpo,  tb* 
MrvBtttR  b«to|  oUcuf*.   //,  dmplvU  of  oU. 

When  the  jwtal  Is  viewed  on  the  surface,  the  receptacles  are  aeea 


8FICB5,   AND  THEIR   ADULTEBATION'S. 


•147 


but  indistinctly,  being  otwcured  by  the  cellular  tiaauc  of  which  the 
surlace  of  the  petal  is  formed.     Fig.  170. 

Fig,  170. 

LosoaomaAi.  Iicnax  or  Flovib  Ralk  «r  TVK  Cum* 

{Hi«DlftMl  60  diwMWr*.) 


a  a,  itotptMlM  fbv  1h«  mhhUsI  oil.  ftrpnnng  u  apertam  from  b»Tlag  bMo 

out  Into  In  maklBf  Uw  Metlun.     ft.  crltulxr   ilt«ur.      r,  «i>od]r   fibre,      d,  Un 
tabalu  atniBtDr*  sAd  tstcnpteci  «litcb  forin  the  Ititeruftl  portioo  of  Uwi 
«,  Um  dark  ontnl  port  of  Um  flpwu*«ulk.    //,  d^ojiku  uf  till. 


In  a  trflDsirerse  teclioa  of  the  Jlower'utalk,  viewed  with  an  object- 
glius  of  one-inch  focuJ>  the   following   ajipearances  present   tb< 


lem- 


selvefl : — 

In  the  oerut  third  of  the  section*  numerous  large  holes  are  ob- 
served; these  arc  the  divided  rccepLocled ;  next  to  these,  passing 
inwirds,  are  bundles  of  woody  fibre,  forming  u  narrow  circle  in  die 


i^ 


SPICES,   AND   TaEIB  ADULTERATION'S. 


interior  or  the  stalk;  extending  from  these  to  near  the  centre  of  the 

Btalk  is  ft  tissue  formed  of  ntnnernus  tubular  cells,  with  Urge  fpnoes 
between  them.  The  recophioles,  as  well  as  the  tubuUr  cells  luid 
intppspaces,  cntuain  easi^nliiil  oil,  visible  in  sectionii  immersed  in  water, 
in  the  form  of  Innumerable  droplets.     Fig.  169. 

Longitudinnl  eeccions  exhibit  a  nearlj  similar  structural  smmge- 
ment.     Fig,  170, 

Cloves  contflin  scftrcely  any  starch. 

The  clove-stalks  present  a  structure  somewhat  similar  to  thnt  of 
cloves  tliemselvcs ;  that  is,  thev  consist  nf  cellular  tissue,  hollowed 
out  here  ami  there  into  receptncle«  for  ihti  ese'cntial  nil;  but,  in 
adilitinn,  the  dtnlks  are  provided  with  an  epiderinis,  or  coatinjr  nf  the 
stellate  cells,  which  areol'auch  freijuonl  ot!Currcnce  in  diflcreut  kinds 
of  bark. 


On  the  Adulter  at  io?fs  or  Ci^vbs. 

Cloves  ire  hut  seldom  sold  in  powder,  and  hence  the  liability  to 
nduheriitiori  is  f^reutljr  lessened  ;  ihejr  are,  however,  oceasionoll/  met 
with  ill  (hut  stale. 

Clove-stjilks,  ttUhough  very  inferior,  contain  some  of  the  active 
properliej*  inf  cloves^  and,  as  already  noticed,  are  occasionally  used  by 
dimllers  for  procuring  the  essential  oil  of  cloves.  We  have  reaAon 
to  helii-ve  rhai  in  some  rases  the  stalks  are  ground  np,  and  mixed 
with  thf  pnwder  of  genuine  cloves. 

The  (piidity  and  value  of  chivea  are  not  unfreijuentl^  impaired,  like 
Bome  other  «nicej!.  by  the  abstraction  of  the  essential  oil. 

This  frauu  used  to  be  exteustvidy  pnictiMeil  in  llalliind,  the  drawn 
cloves,  fur  more  effectual  uoriceulTuonl,  being  mixed  wilh  olheni  of 
good  rpi.ilily;  and  even,  in  snme  instnnres^  the  trouble  beint;  taken  to 
restore  as  nearly  an  possible  to  the  cximnsted  cloves  thtir  original 
appearHMce,  by  rubbing  thcrn  ovlt  with  aome  common  oil. 

Twenhj-Jlrc  samples  of  lIovcs,  wbnU'  and  in  powder,  were  snb- 
jcctcil  to  cxaminaliim,  the  results  were  tliut  one  imly  of  the  powdered 
cloves  contuinud  a  propniiitm  id*  ch)ve-stulks,  while  from  none  of  the 
whole  cUives  hud  the  esseolistl  oil  been  abstmelcd. 

Tbe  volatile  oil  itselli  as  imported  iiilu  this  country  from  India,  httS 
been  found  to  be  adulterated. 

Mr.  M'CulIoeh.  on  the  :iulhority  eif  MtlbuTn,  states  that  the  oil  im- 
ported from  India  contains  nearly  half  its  woiglit  of  an  insipid  ex- 
pressed oiK  which  is  dis^^overed  by  dropping  a  little  into  spirits  of 
wine,  and  on  shaking  it  the  genuine  oil  mixes  with  the  spirit,  and,  the 
insipid  separating,  the  fraud  is  detected. 

Cloves  readily  imbibe  moi!*ture,  whereby  their  weight  becomes 
greatly  increased,  a  fact  of  which  dishonest  dealers  have  not  failed  to 
HV»il  themselves. 


8PICES,   AST)  THEIR  ADULTERATIOKS. 


449 


On  the  Detection  of  the  AthdUratione  of  Cloves, 

The  adulteration  of  powdered  cloves  with  clove-sfalks  is  readily 
detecUMi  by  means  nf  llie  micruscope,  which  will  revcul  the  presence 
of  the  aiellattt  ccUa  nt'tlie  stalk.  If  the  essential  oil  bti»  W*en  removed, 
the  cluvca  will  be  dry  und  biltor,  no  ail  appearin^^  ou  the  surface  when 
the  cluves  are  pressed  with  llie  naiJ. 

The  quantity  nf  essential  oil  may  be  estimated  by  distillation; 
genuine  cloves  y\A\\  iVmn  17  to  22  per  cent,  ol'oil. 

Adulterations  with  foreign  rcgetuble  substaiicea  are  all  discoTered 
by  the  microscope. 

DuCVf  Id,  per  lb.  Home  confmmption  in  1854,  179,407  Iba. ;  in 
1823,  220,649  lbs. ;  in  nine  montba  of  1856,  151,254  Iba. 


PIMKNTO  OR  ALLSPICE,  AND  ITS  ADULTERATIONS. 

Pimento,  Jnuiatta  Pepper,  or  Allspice,  is  the  berry  or  fruit  of 
the  Eugenia  Pimento^  one  of  the  Myriucete.  It  |in>w»  in  tljo  Weflt 
Indies,  and  principally  in  Jamaica,  especiiilly  on  the  hills  on  tlie  north 
side  of  tiiat  island,  tt  forms  a  beautiful  tree,  which  attaiiui  some 
thirty  feet  in  height,  and  is  planted  in  regular  walks,  which  are  named 
Pimento  walks. 

The  fruit  is  gathered  after  it  bus  attained  its  full  size,  but  while 
still  green  ;  it  is  usually  sun-dried,  but  sometimes  kiln-drieil  on 
sheets  :  in  «lrying,  the  colour  of  the  fruits  i.'lmnge  from  greeu  to  reddish* 
brown ,  wben  ripe,  the  berry  becomes  black  or  dark -purple  in  colour, 
and  ifi  glutinous,  and  consequently  in  that  state  unfit  for  preserva- 
tion. 

Composition  o/AUspice, 

As  in  the  case  of  cloves,  the  essential  oil  of  pimento  is  a  mixture 
of  two  oils  —  a  light  and  a  heavy  oil.  The  pro)>erties  of  these  are 
thus  described  in  Pereirn's  "  I^fritorin  Medica  :*— 

**  By  diiitillntinn  with  water,  allspice,  like  cloves,  yiehls  two  volatile 
oils  —  the  one  lighter,  the  other  heavier  than  water.  The  oil  of 
pimento  of  the  shop«3  is  a  mixture  of  these ;  except  in  odour,  io  pro- 
perties are  almost  identical  with  those  of  oil  of  cloves.  By  distillation 
with  caustic  potash,  tlie  Hfiht  oU  x*  separated;  the  residue  mixed  with 
sulphuric  acid,  and  submitted  to  distillation,  gives  out  the  heavy  oil. 

"  a.  Light  Oil  of  Pimento  (Pimetilo-  fIt/firO'Carbon)  has  not,  to  my 
knowledge,  been  previously  examined.  '  Its  properties  appear  to  be 
similar  to  those  of  the  lir^ht  oil  <tf  (.loves.  It  floatt  on  water  and  on 
liquor  potasne,  and  is  slighty  reddened  by  nitric  acid.  Potassium  sinks 
in,  ftud  IB  icaroely,  ifst  allt  acted  on  by  it. 


^ 


o  a 


45(K 


SPICES,    ASD    TBEIR   ADULTERATIONS. 


•'i3.  Heavy  Oil  of  Pimento  {Pimentie  Acid). — Very  similar  to  dovc- 
ucid.  It  forms  with  the  alkalies  crrstiUIiiie  coinpoiiiids  {alkaline pimeu- 
tatea)^  which  bucoDio  blue  or  yrtuniiih  on  tlie  addition  of  the  tincture 
of  thii  chloride  of  iron  (owing  lo  the  formation  oV  a/errvgimnu  pimcn- 
tate).     Nitric  ucid  acta  violuuLly  on  and  reddens  iu' 

Boijostre*,  in  1825^  published  the  following  auulyais  of  the  composi- 
tion of  pimento  berries  :  — 


VoUtile  oU 

GrpRti  ciU    _  .  - 

SoUd  TmI  oil 

AMtritiKenc  (extract 

Gumin?  BMrirt     . 

(Tnlounng  matter  - 

Untnout  matter    - 

ITiirrytta^Uxiblp  iiigar 

Milirur  (lalltc  acid 

Lifn>^n        ... 

Saliiieatbei 

Water 

Lu«»  .  .  - 

KhI  mallrr  ln»oluble  lu  water 

PelllciiUr  ivktduc  • 

Drown  aoocuU 


I(h0 
f(-4 
0-9 

114 
3-0 
4*0 
I'S 
3-0 
06 

ftfrO 
S-B 
3!i 
I  C 


7-1 


fro 

1  G 

l-g 
30 

18 
98 
16*0 
31 


Toul 


1000 


lOO-O 


Coiuplicated  and  complete  as  the  above  analysis  would  unpenr  to 
be,  it  yet  does  not  embrace  the  etarch  whieh  is  contained  in  tlio  seeds 
in  larj^c  quantity.  Braconnel,  however,  detected  the  presence  of 
starch,  and  estimates  it  as  forniin*;  nine  per  cent,  of  tlie  seeds,  f 

Mr.  Whipple  estimates  the  yield  of  pimento  oil  to  be  about  4"37  per 
cent  of  the  weight  of  the  seed. 


Structure  o/Allspict. 

As  in  the  case  of  other  seeds,  the  pimento  berry  is  divisible  into 
husk  and  seed,  or  seeds  proper. 

The  busk  is  thick,  and,  when  dried,  aaft  and  brittle ;  it  sends  off* 
from  it!)  inner  surface  a  proton<^ation  which  forms  a  septum,  &nil 
divides  the  interior  into  two  parts  or  cells. 

Vertical  sections  of  the  AusA,  viewed  under  the  microscope,  present 
the  following  structures. 

On  the  outer  part  of  the  section  are  seen  several  large  cells  op  «- 
ceptaclet  for  the  essential  oil,  sometimes  two  or  three  deep;  more 
internally,  numerous  stellate  l:clls,  attached  to  and  imbedded  in  eel- 
lubir  tissue,  occur;  next  to  these  are  bundles  of  woody  fibre,  and 


•  Juurn.  dc  ChhD.  M^d.  L  1(0. 


t  Duncto,  Edlnb.  Diipou. 


SPICES,   AND  THEIB   ADULTERATIOKS. 


451 


delicate  spiral  vessels  ;  while  the  tieepeat  or  innermost  part  of  the 
section  cou^ijiti)  ufceltulur  Uiisue  oiilv. 


Fig.  ITI. 

VvrUoU  Bectlon  of  tluilc  of  FUntnlo  BtrTf. 

(MMnJfl«d  SSO  dJkiMten.) 

.  a 


I  or  iMiftHlii  ftr  I 

t.  OtUalw  MMa  lOnaiat  the  btacrmnt  i»wt  of  tbe  MCtiao 


Ml.    ft.  UMlUlc  Milt.    r.  Ctllnlu  tbmt 
d.  Btindle*  of  woody  flbn  uid  tplnl  na«J«> 


Occupying  each  of  the  celli  formed  by  the  husk,  is  a  small  tlattisb 
need  of  a  dark  brown  or  chocolate  colour.  After  ma<>eration,  two 
membranes  may  be  separated,  iillhou^fh  wiili  sonic  diniculiy,  from  the 
surfiice  of  the  seed.  The  most  cxlL'mal  of  these  is  tliin  and  delicate, 
and  consists  of  a  single  layer  of  elongated  and  an^lor  cells.  The 
intenial  tunic  is  composed  of  several  layers  of  laree  corrupted  and 
coloured  cells;  it  is  to  these  that  the  dark  colour  orUic  surlaoe  of  the 

0  0  2 


453 


BPICES,  AXD   THEIB  ADULTERATIONS. 


seed  is  dae ;  when  viewed  under  the  microscope,  they  exhibit  a  ch«- 
racteristic  port  wine  tint. 

F^.  ITt. 
rortloB  of  tiu  Ibinbrajm  on  Snrfhce  of  the  Soed  Proper. 
(Ufl<alflfd  3O0  diuMUn.) 


,T> 


a.  Ext«nul  mrmbruie.  eonfUtlng  ot  s  alngle  \*ytT  at  cloDgslMl  uaA  iBcaltr 
ocUi.  b.  lnUruAl  incmbnDt,  m«l«  up  Of  MVVf»l  Itjtn  of  lifgo  porl  wfmm 
ookiund  eell*. 

The  Structure  of  the  teed  proper,  qs  dlaplaycd  in  vertical  sections, 
is  aa  follows:  — 

Kuniiing  round  the  outer  part  of  the  section  is  a  single  layer  of  Urjje 
receptaclea,  the  rHUiuininj;  thifknesfl  being  nmtle  uu  of  angular  and 
trnnsparent  cellit,  tlie  cavities  of  which  ore  dlled  witn  numerous  well- 
defined  sUrch  praiiuli's. 

When  pimento  berrit-s  fire  reHuPod  to  powder,  the  whole  of  the 
foregoing  slmctupt's  become  disunited,  broken  up,  and  variously  in- 
termixea.  The  port  wine  coloiircd  cells  nre  particularly  conspicuous, 
and  aiTord  a  chnrBCtcr  by  which  the  nature  of  the  powder  may  be  at 
once  determined. 

l*he  several  structures  above  mentioned,  as  they  appear  in  genuine 


SPICES,   AND  THEIE   ADULTERATIONS. 


453 


ground  pimento  powder  or  allspice,  are  repreiented  in  Jig.  174.  on  the 
next  page. 

Fig-  173- 

▼flftfal  BaeUiM  of  Um  Read  Fropcr,  ofFlincstoBcrrr* 

(UvKlitdSMdlUHtan.)  . 


^^pQ&^ 


b  Um  «9pcr  put  sT  Iht  Mnti.  two  of  Ike  rvn-pfnrJa  for  ItM  oil  M  txhtlilted  i 
U)(l  In  ihc  luwsr  part,  a  a,  the  eclU  eualalnliitf  ihe  amMll  rouiulcd  tlarch  OM- 
pinclea  i  fr,  looM  •Urch  eorpiMck*.  mignillnl  W  diun«Un. 

Ov  THs  Adultebationb  or  Allspice. 

Of  Twenltf-ont  5arople9  of  ground  allspice  subjected  to  cxaminatton 
one  only  wus  adulterated  with  mnsUird  hwth^  a  reiiult  probably  mainly 
attributable  to  the  great  cbeapnesii  of  tbiu  spice. 

On  the  DfteetioH  of  the  AHuUeraHont  of  Allspice. 

The  adulteration  with  mustard  busk  is  one  which  is  very  readily 
discoverable  by  meant)  of  the  niicroscope,  the  structural  peculiarities 
of  which  will  be  I'uund  described  under  the  article  Mustard. 

G  o  3 


4M 


SPICES,   ATTD  THEIR  ADUT-TEHATIOXS- 


The  duty  on  pimenlo  ia  Sx.  per  cwt.  "Wholwale  price  about  6//. 
per  pouml.  Entered  for  home  coiuumptlon  in  1854,  3,632  cwts. ;  in 
1852,  3,535  cvts. ;  in  nine  months  of  1856,  2,781  cwts. 


Fit.  17*' 
QnovrD  PittBTfo,  OK  Aujcnc 

(MiCBlftwt  »>  dlAiMUn.) 

i 


n.  TnfmaatM  nThmlc.    h.  Stfllate  e«l1«.    r.  Exttrml  M«t  or  rMtntnne  of  and 
pfOMr.      d.  Port  wln»  roluurC'l  cwlU,  vMctt  foan  th«  mbmhI  membfVM  of 
■M.      «.    C«U<  of  ihf)  M««l.  which  ooDlftlD  tfaa  lUl^  (r«B«lM.    /. 
■Urdi  oorpiuelei. 


MIXED  SPICE.  AND  ITS  ADUT^TEnATIONS. 

Mixed  Spice,  as  the  name  implies,  \s  a  tnixture  in  difTerent  propor- 
tions of  ievernl  spices ;  those  of  which  it  is  usualtj  composed  are 
f^und  ginger,  pimento  or  alUpice,  with  cassia  or  cinnamon,  and 
sometimes  a  small  quantity  of  powdered  cloves.  Such  are  the  tisual 
in^^rcdienta  which  enter  into  its  composition.  In  some  rare  cnses^ 
however,  it  may  contain  other  spices,  as  niaco  or  nutmeg  ;  but  vhal- 
flver  the  constituents,  and  in  whatcTor  projxirtions  they  are  employed* 


SPICES,   AND  THEIR  ADCLTEnATlONS. 


455 


mixed  spice,  wh(!n  genuine,  ahniilil  confti.tt  entirely  of  a  combination 
of  apicca,  and  should  not  contain  a  particln  of  farinaceoua  matter  other 
than  that  proper  to  the  ariicles  composing  it.  Thus  it  should  never 
contain  wheat  Jftntr^  jwtato  furiwit  or  sago  meal^  and  whenever  any  of 
these  are  present,  the  article  is  to  be  conaittered  and  treated  as  adul- 
terated. 

Fig.  1-5. 
OixDiiTii  UiXKj>  iricm. 
OUffnlBvd  197  diwnelan.) 


a.  Wrtorly  llbr*  of  fflnj»r.  o*.  Crili  wT  w^f"  whlfli  conUIn  thf  Hirrh. 
ri*.  Sfarcti  (Tmnalri  ■>*  t}*fmw.  t.  OineT  lltKit  iif  plfiirnlo  nr  fclUpIr^.  V-  Su-l- 
UU  f*\\*  nf  ••me.  V.  Hutk  of  the  •rrd  ppiptr  nt  illllo.  ft"'.  Vorl  wIm  co- 
loured f*llt  of  lUlta.  ♦"■".  fitairh  r»\l»  \  and  f/**,  •Un>h  gnuiulM  of  Mne. 
e.  ttuvh  graniilc*  Kod  frafnMiiu  ofpowdcrtd  danimun. 

The    above    cnjrraving    repre«ent«   the    structure    of  the    several 
ingredients  of  which  genuine  mixeil  vptce  is  usually  formed. 

O  G  4 


4se 


ISIMGLA8S,  AKD   IT8  ADULT EBATIOXS. 


Os  THS  Az>ct.TiaATiosfl  or  Mixed  Sncs. 

Of  tbe  Twetttytix  samples  of  mixed  spke  subjectetl  to  microscopic 
exAtnination,  no  leas  than  t^jtetnj  or  coruiderablv  more  tb«n  one  hmli^ 
were  mdulterate^l;  anil  hence  it  is  seen  that,  of  all  the  spices,  mixed 
«pice  ifl  tbe  most  liable  to  adalteraiion. 

Tbe  substances  employed  were  wheat Jfovr  in  five  CMBes,  grottrnd  rice 
in  two,  »ago  in  four,  potato  fitmr  in  oue,  and  vegftabU  tuhtbMmces  tm- 
determinet]  in  tbrw  uftbe  samples. 

On  the  Detection  of  the  AduUeraiion*  of  Mixed  Spice. 

Tbe  whole  of  the  idulteratjons  of  mixed  spice  are  ilismverable  by 
means  of  ibe  microscope  :  the  charactcn  of  wheal  Hour  are  described 
and  Blared  at  p.  243.  ;  of  rice,  at  p.  265. ;  of  sago,  at  pp.  3:24 — 5. ; 
and  of  potato  tlourat  p.  320. 

Fullt^r  details  refpectiii*;  the  adullei^tion  of  bpiccs  will  be  ibund  in 
the  author's  work  entitled  "Fo-td  and  it«  Adulterations.'* 

The  prenent  alTords  an  additional  instuuce  of  what  we  have  so 
frequently  before  observed  —  nauiely,  ihat  the  higher  the  price  of  snj 
article,  the  more  it  heivnnes  subject  U>  adulteration. 

It  thus  again  appears  thni  tbe  public  und  rbc  revenue  are  exten- 
Bively  defrauded  torough  tbe  adulteration  of  the  majority  of  the  apices 
told. 

Duty  on  ground  spice  unenumerated,  U,  per  lb. 


ISINGLASS.  AND  ITS  ADULTERATIONS. 

IsiMGLAfts  is  the  air  bag,  or  swimming  bladder,  wimetimea  called  the 
sound,  of  various  tish,  chieHy  of  the  sturgeon  tribe,  and  belonging  to 
tbegeDas  Aeipenser, 

xVM  bag  is  a  membrane  filled  with  air,  situated  near  the  spine, 
above  the  centre  uf  gruvily.  In  most  tisb  it  coiiinmnicates  with  the 
{Esophagus,  or  sloniocb,  by  a  duct,  which  is  known  as  the  ductuM 
pneitmaiiau ;  in  others,  the  duct  is  impcrlorate ;  occasionally  there  are 
twoaaca,one  anterior  to  the  other,and  communicating  by  a  idiort  tube. 

Tbe  air  bag  is  made  up  of  an  external  or  peritoneal  covering :  a 
middle,  fibrous,  and  in  some  cases  muficulur  coat;  and  an  internal, 
highly  vascular  membrane. 

Tbe  following  are  the  principal  species  of  fish  from  which  Russian 
isinglass  is  derived  : — Aciptnaer  Uuto  or  tbe  Brlnt^a,  A.  Gouldetutadtii 
or  the  Oateter^A.  Ruthenus or  the  J^terlett  A.  SteliatiuoT  the  Sevrmga, 
Siluna  Giants,  and  Siprinus  Carpio. 


^ 


I8INGLA«S,  AND   IT8   ADULTERATIONS. 


457 


Tn  atlditioif  to  the  sbove,  isinglass  is  obtained  in  differpnt  parts  of 
the  woriti  iVom  seTural  other  kinds  of  fish.  In  Nt'W  York,  from  the 
Labnu  Squeteagtu^  of  Mitchell.  In  New  En^'land  it  U  procured  from 
the  intefitines  of  Morrkua  vulgaris^  or  the  common  cod,  this  limn 
being  denoininuted  ribbon  iinuglaAs.  In  the  BniziU,  it  is  nbt^iineil 
from  u  lar<;e  fisb,  probably  a  species  of  Hilumji;  urid  in  Iceland,  from 
the  Cod  and  Lot4i  Moloa  or  Littg. 

For  iin  fti'count  of  the  fisheries  and  the  mode  of  prepflralion  or 
drying  of  tlie  swimmin<r  blad<ler,  the  reader  in  referred  to  tlie  Author's 
work  •'  Food  and  its  Adulterutions." 

Tbti  principal  kind«  uf  iuinglass  arc  leaf,  short  stapl^^  long  staple^  and 
hook  itiinglatfd. 

S»tn(ivejr  ifhort  staple  and  book  isioglaMef  are  usuallj  of  inferior 
quality. 

162,000  lbs.  of  ifliDglaM  arc,  on  the  average^  shipped  every  season 
from  ]<u!=sia. 

In  urldition  to  the  tsin^Iasa  imported  from  Kussia,  a  vast  quantity 
is  muKiully  received  from  the  Brazils,  and  the  East  and  West  Indies. 
It  is  Imwever,  greatly  inferior  to  the  description!)  we  hare  noiice^l. 
Indeed,  Bniziiian  uinf;lius  is  oidy  fit  for  finin;;  purposes,  an<l  for  such 
it  is  tiljiiost  wholly  bou;»ht  up  by  tli«  pronrielors  of  large  brewing 
establishments,  who  couaume  ncaily  the  entire  (juaniity  im|>ortfid. 

Manufoi^tttre  of  Isingltua. 

On  the  arrival  of  the  isinglass  into  this  country,  the  best  kinds  are 
submitted  to  a  course  of  preparation  before  they  are  ready  for  con- 
flumptioo. 

The  Beluga  leaf  is  closely  examined,  and  all  discoloured  parts  cut 
away;  the  cuttings,  and  other  pieces  not  deemed  good  enough  for  tbe 
best^  ore  placwl  aside  as  aecondM  or  thinU,  Tbese.  in  some  ciues  are 
u»ed  for  fining  the  better  descripttoti  uf  ales,  but  more  generally  for 
winetf,  liqueurs,  &c.  It  is  also  rolled  and  cut  into  shreds  for  domestic 
purp<ises,  where  colour  is  not  an  immediate  object. 

Purse  isinglass  Is  mostly  sohl  to  the  brewers,  who  consume  a  rojit 
quantity  in  the  fining  of  their  .several  beveroj^es. 

Long  and  short  staple  isinglass  is  extensively  demanded  by  cider 
makers,  confectioners,  and  others,  to  wboui  it  i^  sold  in  tbe  same  state 
as  inijHtrted  into  thi*  country. 

Leaf  i»inglass  taken  Irom  the  Beluga,  after  having  been  picked 
from  idt  impure  or  discoloured  piecr-s,  constitutes  the  very  best  article, 
either  for  dieteticul  use,  or  for  the  hijrher  cliL-w  of  clarifying  purp(»8es. 
This  descripttiin  of  ipingiass  tins  to  undergo  a  process  of  mnnufuctiire 
before  it  is  ready  for  use.  What  are  (crtned  perfect  specimen  braves 
are  nearly  round,  llie  bladder  huvin;;  been  opened  lonj;itudinally, 
about  two  feet  in  (ureumference,  and  weijfh  froui  ei;;ht  tt>  sixteen 
ounces,  according  to  the  thickness  of  the  sound.     It  is  not  uncom- 


^ 


4fi6  ISINGLASS,   AND  ITS  ADULTERATIOX8. 

mon,  however,  to  meet  with  heavier  sAmplcn,  some  having  bo^n  Irnown 
lo  rencli  four  pnumls. 

A  Htuain  unginu  of  some  eight  or  ten  horse  power  is  ^nerftllj  used 
uniler  ihe  present  method  (pfjirepnrinii  iMitglass,  the  nrMunct  micJii- 
nery  consUtm};  of  a  series  v(  iKiwerfiil  roller*,  arrnngwl  in  pairs  in  % 
manner  resembling  I  hose  iisetl  for  expre8sin<j  the  juice  fnim  Uw 
sugar  cane.  The  rnller>)  when  in  motion  are  fed  with  leaf  isinghus  w 
fast  as  possible,  which,  in  pasfiin];  between  the  two  rollers,  bocoves 
amalpaiutited  and  spread  out,  and  a  expelled  fn)m  the  opposit«  side 
of  the  rollers  in  one  continuous  sheet.  The  iainglnss  thus  rolled  is 
called  *' ribbon,"  but  it  is  not  yet  ready  for  the  process  of  cnttins. 

The  sheet  or  "  ribbon"  rs  probably  ft  sixth,  eighth,  or  tenth  part  of 
an  inch  in  thickness,  and  as  it  is  necessary  to  reduce  it  until  it  is  as 
tliin  as  writinj;  nnper,  tt  is  passed  through  rollers  more  clcwelj  set, 
until,  iH  i)ie  ibiricnes.^  diminishes,  the  desired  result  is  obtained;  the 
width  of  the  "ribbnn,"  of  eourao,  increasing. 

It  is  Uf  be  reniArkeil,  that  in  rolling,  the  ribbon,  bein^  cnn6ned  to 
the  iivi<,llli  of  tlie  ryllwrs,  ^fenerully  nUiiut  two  feet,  increases  only 
lengthways,  andt  when  conipleled^  can  be  fulded  or  rolled  up  in  lh€ 
same  manner  ns  n  length  ol  cammon  Unen. 

Afier  a  brief  delay,  for  the  purpose  of  dryinjr.  the  next  and  la«t 
process  of  cutting  \a  efiecitiMi.  liy  the  introduction  of  mwJern  niachi- 
nery,  this  pnrt  nf  the  prcparntion  of  isinghiss  is  performed  with  wir- 
prising  celerity,  and  the  material  is  cut  into  very  fine  shre<ls. 

The  cutting  machine  is  a  cylinder  with  some  6ve  or  six  keen- 
edged  blfwles  fixed  in  a  tangential  direction  to  the  cylinder.  The 
same  engine  which  scrveHi  (o  r^U  out  the  isinglass,  as  already  described* 
sulHopS  to  turn  this  little  miicUine  at  the  rate  of  some  800  or  1000  re- 
volution* per  minute ;  tiikintj  a  low  estimate,  we  will  suppose  it  turns 
8tX^  tiniCFt.  On  I'xitniining  the  r\)indiT  we  find  five  or  six  blades  set 
in  it,  and  as  each  of  these  kniveti  severs  a  shred  from  the  width  of 
the  "ribbon/*  while  the  cutting  proccM  is  going  on,  it  follows  that 
four  or  five  ihousimd  shreds  are  t'lit  in  the  short  ^pace  of  one  Diinu 

Such  U  the  plain  and  simple  method  of  [ireparing  cut  isingl 

There  are,  however,  many  consumers  who  still  prefer  the  o 
fashioned  st^te  of  hand-cut  isingla^^.  In  thiii  cose,  the  thin  leaf 
pulled  to  pieces  with  the  fingers  or  divided  into  strips  with  Kissora, 
work  moatlv  j>crfonned  by  women. 

The  shreds  of  isinglasa  softened  in  cold  water  and  cxnmine<l  in  the 
microscope,  arc  seen  to  pos'was  a  fibrous  structure,  a  few  vessels,  gra- 
nular cells,  and  nuclei  being  scattered  here  and  there:  it  is,  in  fact 
an  organised  substance.     Fig.  176. 

0.1    TBB    AdCLTSBATIONB   Or   IstNGLABB. 

The  principal  adulteration  of  isinglass  is  with  gelatine,  an  url 
every  respect  much  ioferior  to  isinglass. 


OL 

tiat      , 

i 


I8TNOLA88,   AKD  ITS  ADTILTERATIONS. 


4&9 


Usually  shreds  of  gelatine  are  mi.xetl  with  those  of  tsinglasff.  Occa- 
sionally the  gelatine  is  incorporatetl  with  the  iftinglaiis  while  it  is  in 
sheets. 

Most  fre<|uently,  however,  gehtine  is  substituted  for  isinpliiss.  The 
best  isinglass,  of  course,  is  Russian;  this  is  often  ileteriorated  by  atl- 
mixture  with  a  very  inferior  article  termed  Brazilian  isingluMs;  in 
other  cases,  this  is  substituted  for  the  better  and  more  valuable 
description  of  isinglass. 

Resulta  of  the  Examination  of  Sample*. 

Of  Twenty'eight  isau\y\iis  of  isinglass  subjected  lo  examination,  ten, 
or  more  than  one  third,  of  tl>«  samples  consisted  entirely  of  oelatime. 

On  the  Detection  of  the  Adulterations  of  Isinglass. 

Between  isinglass  and  gelatine  several  welt  marked  distinctions 
exist;  some  of  iheso  are  sufficiently  simj>le  to  enable  the  ordinary  ob- 
server himself  to  distinguish  the  one  orticle  from  the  nlber- 

AU  (hut  is  necessary  to  effect  the  discrimination  i^  to  spread  a  few 
of  the  Btaments  out  on  a  slip  of  gloss,  to  moisten  them  with  water, 
and  after  the  lapse  of  a  few  minutes  to  note  well  the  apjiearances  pre- 
sentoil  by  them. 

Isinglass  and  gelatine  (lifTer,  especially  in  the  following  characters: — 

The  shreds  of  isinglass^  when  immersed  in  c«)ld  wateif  become  white, 
opaque,  soft,  and  swollen. 

The  swelling  is  equal  in  nil  directions,  so  that,  when  vieweil  with  n 
low  power  of  the  mieroscope,  the  shreds  appear  mure  or  le«5  quadran- 
gular. 

In  boiling  water,  they  dissolve  nearly  without  residue. 

The  smeU  of  the  dissolved  isinglass,  when  hot,  is  somewhat  fishy, 
but  not  unpleasant. 

The  moistened  .•hreds  or  the  solution,  exhilnt  to  test  paper  a  neutral, 
or  faintly  alkaline,  and  rarely  a  slightly  acid  reaction. 

Under  the  microscope,  the  tilamcnte  exhibit  a  well  marked  fibrous 
structure. 

In  acetic  aeid  they  swell  up,  and  become  soft  and  jelly-like,  the 
greater  part  of  the  structure  being  lost. 

Lastly,  "'ITie  ash  which  results  from  the  incineration  of  good 
Ruuian  i.singUss  is  of  a  deep  red  colour :  it  contains  but  a  small  por- 
tion of  carbonate  of  lime,  and  never  amounts  to  more  than  nine  per 
cent,  of  the  isinglass  used."  • 

The  Bhre<Is  of  gelatine,  on  the  contrary,  when  placed  in  coM  water, 
swell  up.  acquire  increased  transparency,  and  become  translucent  and 
glass-like. 


*  PbirmioQuiicftl  Jounul.  vet  x.  p.  Ifi. 


I  ef  riueda  of  Orlatiitb  ui4  1mwulj>«».    TTppar  Ann,  i 
tHm^on.    MagBUMTSdUBtMm. 

The  <lry  shrefison  the  uncut  surfaces  frequently 
shining  liutre,  not  unliku  thut  of  tinsel. 

In  boiling  water,  they  do  not  entirely  dissolve,  but 


Alt.    *..    .U.    L 


r  -mV  .     -I.. 


I8IN0I.A88,  AND   ITfl   ADULTERATIONS. 


461 


Lastly^  the  ash  is  difTorent  from  that  of  isinglass  in  nmount,  colour, 
and  composition.  "  100  jrruiriH  of  {joUtine  give  from  2*3  to  2'6  gmins 
of  oAu  vrhich  is  whit^y  contains  much  carbunute  of  UmOj  vr'ith  some 
chlori*ies  and  snlphntet"  —Letfiebv. 

It  is  thtTcfore  very  easy  to  distinguish  bptween  iBing^lnfts  and  gela- 
tine, even  when  the  ahredd  of  the  tvru  articles  are  mixed  together  in 
the  same  parwL 

The  discrimination  is,  however,  much  more  difficult  when  they  are 
both  incorporated  in  ihe  same  shreds  or  strips;  nevertheless,  by  means 
of  the  niicroaoope,  tliis  adulteration,  Brst  described  by  Mr.  Redwood, 
may  frequently  be  discoveretl. 

If,  on  examination  with  that  instrument,  the  shredit,  after  immersion 
in  cold  water  for  a  few  minutes,  exhibit  a  thick  U>rder  of  a  eleur  and 
structureleM  substance,  there  is  no  doubt  but  that  the  shreds  ore 
coated  with  gelatine- 
Some  of  the  better  kinds  of  Rmzilinn  isin^rloss  are  manufactured  in 
the  some  way  as  Russian,  and  sold  at  a  cbi^aper  rule.  No  doubt,  in 
some  instances,  this  is  mixed  with,  or  sold  as  the  bci^t,  and  it  hn^  been 
ascertained  that  acids  und  other  cheuiicuU  hare  been  ii>(L'd  to  improve 
its  colour;  but  the  test  of  gfKKl  isin-jlaas  is  in  the  jelly  iniide  thi'refrum. 
The  jelly  mode  from  Russian  isiiifilass  dissolves  rewiily,  furnishes 
scarcely  any  sedimeut,  and  ia  remarkably  firm,  pure,  and  translu- 
cent. 

On  the  other  hand,  Brazilian  islnjrlass  makes  a  far  inferior  jelly, 
with  these  renuirkable  dilTerences :  that  whihit  Kusainn  isinglass  is  firm, 
and  free  from  deposit,  Brazilian  isin<:lass  leaves  a  deposit  of  insoluble 
matter  amounting  to  twenty  or  thirty  per  cent.,  is  less  readily  dis- 
solved, und  the  jelly  is  opalescent,  and  milky. 

Oo  muktrig  hiaitc-matige  with  the  purest  Russian  isinglass,  milk  is 
needed  to  impart  the  snow-white  colour  of  that  jelly  ;  but  in  the  case 
of  Brazilian  isinglass,  hot  water  alone  will  render  it  nearly  of  that 
colour.  It  is  almost  needless  to  add  thai  the  blunC'timnge  is  nmnb  in- 
ferior in  quality,  und  the  large  percentage  of  insoluble  matter  renders 
the  jelly  proportionately  weak. 

The  quality  of  any  isinglosa  may  easily  be  tested  by  dissolving  a 
small  portion  in  a  glass  vessel,  with  about  a  tablespoonful  of  boiling 
water.  The  best  Russian  isinglass  will  instantly  dissolve,  and  scarcely 
a  particle  of  sediment  remain ;  the  soluble  matter  in  this  article 
being,  according  to  the  best  authorities,  ninety-eight  grains  in  every 
hundred. 

The  same  test  appbeil  to  Bnizilian  isinglass  will  extract  the  gelatine, 
but  the  shreds,  from  their  Bbrous  character,  do  not  entirely  dissolve  ; 
they  turn  white  and  retain  their  form,  unless  disturbe<t,  in  which  coaii 
they  break  up,  and  form  a  deposit  at  the  bottom  of  the  vessel. 

If  Russian  isinglass  be  adulterated  with  Brazilian,  the  admixture 
may  easily  be  detected  by  the  insoluble  shreds,  or  white  deposit,  which 
is  lore  to  Appetr  in  proportion  to  the  amount  of  Brasiiian  isioglasa 


k. 


462 


GELATINE,   AND   ITS   ADULTERATlONft. 


that  inaf  be  introduced.     Tbe  smell  of  the  Utter  iUo  it  iMi^iir 
from  pleasant,  »nd  forms  a  great  coDtrost  witb  tbe  faints  ioglMtt^ 
seuwced-likc  odour  of  Russian  isinglau. 
Dutj  frve.     Impurttttion  in  1854,  1,881  cwU.;  m  18^5,  l^cvti. 


GELATlNt;  AND  ITS  ADULTERATIONS. 

As  we  are  not  acquainted  with  any  trustworthy  or  practiAl 

of  the  method  of  preparini;  geluttne,  we  have  been  at  »ome  pais  to 

prucure  the  CoUowing  information  respecting  it£  manufacture. 

Ordinary  gelatines  ore  niiide  I'niin  tliose  pieces  of  skins  w\vA  ffi 
cut  off  by  the  tanner  ta  unlit  for  makin*;;  leather,  in  ouoKi^iicnoe  U 
thiekiicisa.  The  beet  description  is  ])repart:d  from  tbe  akin*  of  calva* 
bcadii ;  lliosv  arc  separated  fn>m  the  wbulu  t>kins  ftAer  they  km 
passed  tliiough  tbe  proccM  of  liming:;,  to  remove  the  bair  from  thtm~ 

The  skins  ure  next  well  w^hed,  to  get  rid  of  tbe  lime,  and  all  ifae 
piecc-i  of  flesh  itnd  fat  are  cnrefulty  cut  out;  some  manufacturniMik 
thcut  fur  a  short  time  in  a  dilute  solution  of  muriatic  aoidt  Ui  r^wn 
any  remaining  portion  uf  lime;  but  tbispmelice  is  both  injarkMsa^ 
unprofitable.  The  acid  furmj  with  the  lime  chloride  of  cstdm 
which,  if  it  is  nut  carefully  removed  by  washinj;,  ia  boiled  cpwhAAi 
akiiis,  and,  beinj;  boluhle,  remains  in  the  gelatine;  a  pirtionaflW 
hkins  is  aUo  dissolved  by  the  acid,  and  i»  thrown  nwsy  in  tlif  wsui 
employed  in  washing;  them,  which  thus  ocmsions  a  loaa  in  wcs^i. 

In  some  coses  the  skins  are  boiled  whole,  in  othera  they  are  tewihM 
small  piL'ce»^  or  even  reduced  to  a  pulp  by  a  machine  eapeciaDj  Mf 
Btructed  for  the  purjHise. 

If  the  skins  ure  cut  into  fine  nieces,  instead  of  b.ins  put  lotodH 
boiler  whtite,  the  t^elAiine  will  be  better ;  that  is,  it  will  he  of  a  lifkM 
uolour;  and  the  process  is  mure  economical,  as  one  bolf  tbe  timvsl 
be  saved  in  the  boillu^r,  and  much  less  heat  and  fuel  required.  A< 
the  j>elatine  is  darkened  by  ])rolouged  boiling,  the  nsductioo  *4  ii> 
skins  to  a  nulp  \s  a  point  of  very  fiKAi  importance  in  tb«  maaiftr 
lure  of  pclatine  —  ao  much  so,  thai  Mr.  Swinburne  baa  obtiMlt 
patent  for  this  method  of  prt^puration. 

The  skins  are  boiled  with  water,  in  the  proportion  of  aboit  •■ 
gallon  of  water  to  seven  ]>oundii  of  skin  ;  a  small  quantity  of  ooWS 
Bait  u  added  to  preserve  the  gelatine.  Alter  it  has  boiled  fur  abort 
twelve  hour:^  it  is  strained  and  cltirified  with  white  of  eggs,  aaJ  tti* 
run  upon  ghiss  plates ;  as  -oon  uh  it  is  solid,  it  is  mt  into  a5eci  tM 
laid  upon  nets  to  dry,  in  u  room  heated  to  a  temperature  of  about  1^- 
If  the  room  is  not  heated,  the  surface  of  tbe  gclatioe  becoma 


GELATINi:,    AND   ITS  ADULT EKATXOM.  4m 

with  iniall  air-bubbles ;  wbeo  the  gelsline  b  dry,  it  i»  cut  \ij  %  mm/' 
cbini:  111  the  same  manner  as  isinglass. 

The  size  of  tbe  filau  plutca  varies  ncrording  to  tb«  faocv  uf  Um 
manufacturer.  Tbe  urdiuary  size  is  6ft«en  br  eighteen  inckea ;  but  %u 
Bome  cases  thev  arc  three  feel  fujuare ;  tbe  plati»  or  filicei  uf  gelatuc 
are  f^nerally  aoout  fifteen  inches  ti>ii^  bv  tbree  wide. 

Thou;:h  tbe  skin  of  the  bead  uf  tbe  calf  only  is  lucd  for  making  jec^ 
latine,  the  whole  of  the  skins  l>oib  uf  the  calf  and  ox  are  perfut^y 
adapted  for  the  purpose,  but  ore  not  used,  as  tbejr  are  much  mare 
valuable  for  conversion  into  leather. 

In  snme  eotics,  cspeeiullr  in  warm  wenther,  the  skins  ustn]  are  some- 
what itecom|K>9ed,  but  this  is  not  ^enurallv  the  case.  This  eundition, 
although  reuioved  to  suuie  extent  by  repeated  washings,  cannot  be 
entirely  remedicil;  heiiee  gelatine  ntude  fnmi  such  damaged  skins  will 
always  retain  a  smell  and  taste  more  or  leiis  disatfreeuble. 

French  geluiine  is  usuully  much  whiter  thiiti  £ii;£lish ;  this  iii  owio^ 
principally  tu  the  calves  being  killed  in  Frunce  nuieh  yuungLM*  than  in 
lhi«  country. 

Gelatine  is  likewise  prepared  from  the  bones  of  the  ox  and  the 
sheep.  Ic  is  obtained  by  imilin^  bones  in  water  under  pcesiturv.  It 
]s  more  readily  procureil  by  employing  bones  which  have  Iweii  pre- 
vious] v  dig:estud  10  hydrochloric  acid  to  extract  th«  phoHphiUe  nCIiine. 
**ln  this  way  a  nutntious  soui»  is  prepared  in  P.ins  Cur  the  hoH[ilr.j|]« 
and  other  pauper  hatitalions.  Gelatine  has  been  extractt'ii  fr^Mii  ante- 
diluvian bontrs.  A  stmp  was  prepared  from  I'te  bones  of  the  jrivat 
luaslodon  by  a  prefet  oCone  of  the  depurtmenlr.  of  Fniiic-*." — Peretra. 

In  the  *'  London  Jnurmd  of  Arts  and  Seient^es,"  a  publit'utioii  which 
contains  the  specification  of  new  patenn.'d  iuvenliotips  wu  find  the 
fullowin;;  description  of  a  patent  granted  to  George  i'hilbrick  Swin- 
burne, of  I'itulico :  — 

*'Tbe  patentee  commences  his  speciOriition  bv  Ktiitinfj;  that  Iiereto- 
fore,  in  manufacturing  gelatine,  it  has  been  UHuat  (with  one  exception) 
to  act  on  large  pieiea  of  hides  or  skins,  anil  lo  emph>y  lu-ids  and 
alkalies,  together  with  mechanical  and  other  proL'esscii,  which  occupy 
considerabre  time,  and  are  likewise  costly ;  and  in  tlie  excepted  cose 
above  referred  to,  it  has  been  tbe  practice  to  reduce  the  pieces  of  hide 
iitto  the  state  of  pulp  in  a  pa[>er  machine,  and  theu  to  employ  blood  to 
purifv  the  product  obtained. 

*^  This  invention  consists  in  the  following  more  simple  mode  of  ma- 
nufacturing gelatine.  Tlie  patentee  takes  hides  or  skin^,  or  parts 
thereof,  as  fresh  and  sweet  as  possible,  find  free  from  hair,  and  he 
reduces  the  whole  into  shavings  ur  thin  slices  or  films,  by  any  suitable 
instrument  ;  he  soaks  the  shavings  or  films  i'or  about  five  or  six  hours 
incohl  water,  and  then  changes  the  same;  he  repeats  such  chanpng 
of  the  wiiter  two  or  three  times  each  day,  until  no  smell  or  tai^te  is  to 
be  detei:teil,  either  in  the  water  or  in  the  sliavingH,  and  then  he  remorea 
the  shavings  from  the  water.    If  this  product  ia  intended  Ibr  soup,  it 


464  GELATINE,  AND   ITS  ADDLT£RATIOy& 

\a  dried  on  nets,  and  is  then  rendjr  for  use.     If  geUtine  it  to  be 

tractedj  the  shaving*,  nfter  the  above  ftooking,  are  put  intoaavtiMe 
vessel,  witK  a  quantit}-  of  water,  suflicient  tn  cover  tbeni  whrn  )*i'<mi) 
down,  ami  they  are  subjected  to  a  heat  not  exceeciin^  >-■'"■ 
When  disMilvt'ti,  ihc  gelatine  is  to  be  strained  throujrh  l 
fabric,  subjected  to  slight  prewure  with  the  hands  or  oUterwi>i',  "t  ihc 
Buluiiun  may  be  [>ermiite(l  to  run  ull'  from  thf  vessel  without  «trvn- 
iiig,  hy  which  means  niiieh  of  the  •^elacine  will  bts  separattrd  from  tbt 
fibrou!i  matters.     The  prorluct  nf^clutine  thus  obtained  t»  run  in  tlun 
films  on  to  a  smooth  surface  of  slate,  or  other  suitable  materinl   '    •-• 
it  is  then  renioveil  on  to  net*  to  dry,  and  when  dry  it  is  cut 
an  Isin^Iaf^s  cutter  or  other  suitable  nppiiratua.     The  rcnidnr,    . 
not,  may  l)e  usei]  fiir  thickening  anup.  and  other  culinary  ;  iw  ,> 

"Another  tnanufacliire  of  geUiinoti9  substance*  b  priMtu  >:-\  Lt  •^^-' 
follnwing  prt>ces.s  frtim  cod  s^iundit,  or  other  liahy  matters  acpa^hk  d 
yielding  fXelatine  :  —  The^e  matters  nre  reduced  to  •havings  or  ttia 
films,  snaked  in  water,  nubjected  to  the  action  uf  heat^  and  the  jirrUiiae 
strained  or  run  off"  as  above  dcscribtnl.  The  patentee  nbtaini  a  fint, 
second,  and  third  pnHhtct  nf  nelatine,  which  he  fi>rni5  into  sheetv  ad 
when  ilry  vuts  U|t  the  same  with  an  isinylasa  culler.  This  maxmftt' 
ture  of  jk'elatme  will  be  found  highly  uaeful  ad  a  cheap  snbacitute  te 
isinglass  for  cfarifying  liquids." 

Itd'erior  j:ettitiite  is  u^e1l  in  lai^e  quantities  by  |inpcr  makers  ^tnv- 
hnt  and  tUk  niaimfaelurer!!  ;  but  these  parties  generally  putrljAae  U» 
skins,  and  prepare  the  gelatine  themselves. 

Unlike  i-iin;»lass,  the  shreds  of  gelatine,  aa  alreatiy  noticed,  eia* 
niiiu>d  with  the  nticroseope,  are  f>een  to  be  romposetl  of  a  tran^iaiMt 
and  j»crfectlv  bninojreikous  substance.     Scf*  Jig.  176. 

Glue  is  fiuire  a  dis^tinct  mantifacturc  from  gelatine,  and  is 
carried  uu  by  ibe  ^ame  |)tu*tie8.     It  is  made  from  boneiii 
of  skins,  and  hoot's. 


On  Tit£  Adultbbatiohs  or  GfiianiiE. 


J 


The  addition  of  a  small  nuantity  of  salt,  with  the  view  or., 
the  preservatiim  of  the  gelatine,  is,  of  course,  allowable ;  btti 
freiiuetitly  added   in  lar<!e  quantities:   it  then  causes  tht  fivUnv 
to  absorb  moisture  from  the  atmo^phe^c,  whereby  its  weight  it  m^ 
increitsed. 

In  some  cases,  gelatine  is  adulterated  with  nii^ar,  estber  Ifiwa 
or  white,  not  to  any  considerable  extent,  except  with  some  <*f  *^ 
inferior  qualities,  such  as  are  so  largely  used  by  the  xuanuiarturcn  ^ 
uuli^tor  Mieats. 

The  iellies  in  bottles,  and  those  sold  by  confectioners  aa  mnfim 
and  calves'  feet  jelly,  consist  principally  of  gelatine  variou^r  fc^ 
vourcd.  Jellies  made  from  calves'  feet  are  much  less  firm,  am  ir 
solve  quicker  than  those  auide  from  geUtine,  if  kept  in  a  wun  m* 


AXNATTO,  AND  ITS  ADULTERATIONS. 


465 


Oa  the  Detection  of  the  Adulterations  of  Gelatine. 

The  niJiiUcrarion  nf  frelaliiie  with  Bnlt  maybe  thus  detortp*]  :  —  200 
irraift*  »*"  the  polatine  mu«l  be  inoiiioruie'i  and  tlu»  nsh  ta-*!!-'!  for  salt  ; 
the  quantity  of  which  preseni  nmy  be  determined,  if  necessary,  by 
the  pn>cw8  given  under  Anna(U>. 

For  the  iiet**olion  of  the  sugar  the  following  prore«8  may  be  fol- 
Idwed  :  — Dissolve  the  f^elatine  in  water  ;  precipitate  with  tannic  acid  ; 
filter,  and  evaporate  the  sohuitm  to  <lryness,  when  the  sugar  will  be 
found  in  the  residue. 

A  better  method  is  the  followinp  :  —  Soften  the  gelatine  by  macera- 
tion in  a  little  water,  boil  in  alcohol;  this  will  take  up  the  sugar  and 
leave  the  gciatinc. 

GeUtinc  is  fre«  of  duty  on  importation,  and  is  largely  manufactured 
in  this  country. 


AXNATTO,  AND  ITS  ADULTERATIONS. 

TiiE  next  article  which  fall*  under  our  consideration  is  annatto ;  this, 
though  not  employed  as  fond,  is  yet  a<lded  to  several  articles  of  con- 
sumption, and  it  therefore  becomes  of  interest  to  ascertain  whether  it 
is  Hubject  lo  Adulteration  or  nut. 

Annatto  is  the  colouring  mutter  oUlnined  from  the  seeds  of  n  plunt 
named  Btxa  orelUma^  L.,  and  which  forms  the  lype  of  the  8imuI1  natu- 
ral or<ler  Bixinea.  It  is  a  native  of  South  America,  the  West  and 
East  Indies  ;  but  the  article  annatto  is  chictly  prepared  in  Druzil  and 
Cayenne. 

The  tree  is  an  evergreen,  and  the  aeeils  are  enclosed  in  poils,  the 
colouring  matter  being  sitntited  on  the  outside  of  the  seeds. 

It  appears  that  two  diflereiit  pr'»ce5ses  are  pursueil  in  order  to 
separate  the  colouring  matter.  According  to  the  ordinary  process 
the  seeds,  afler  being  reuioved  I'roni  the  poils,  are  brut«ed,  lran»ferre«l 
to  a  vat,  when  they  are  mixed  with  as  much  water  as  covers  tliem. 
Here  they  are  lelt  for  several  wpcks  or  months.  "The  substance 
thus  obtaine*!,*'  Dr.  Ure  states,  *  is  now  <uiueezed  through  sieves, 
placcii  above  the  stcef>er,  that  the  water  containing  the  colouring 
matter  in  suspension  may  return  into  the  vat. 

"  The  residuum  is  preserved  under  the  leaves  of  the  Annana  (pine- 
apple tree)  till  it  becomes  hot  by  fermentation,     ll  is  then  again  eub- 

B    H 


4«e  ANNATTO,   AND   ITS   ADULTERATIOKS, 

jecteU  to  the  satne  operation,  and  this  treatment  b  continued  lutui  co 
more  colour  remains. 

"  The  Hubstance  thus  extracted  U  passed  through  aieres,  in  oriler  Ui 
senarute  t)te  remainder  of  the  seeds;  and  the  colour  is  iillovt^  to 
auDside.  The  precipitate  i^  boiled  in  coppers  untd  it  is  rrttutviu 
a  consistent  piutc.  Ic  la  llicn  suHered  lo  cool,  and  is  dried  in  tbe 
ahiiflc." 

The  second  process  i:tthat  recommended  by  Leblond.  TleTinpnn 
simpl}^  to  waith  the  seeds  until  tliey  are  entirely  deprived  otcolov, 
to  precipitate  the  coluuring  matter  by  mean»  of  vinegar  »r  \aat* 
juice,  and  to  boil  it  up  in  the  ordinary  manner,  or  to  drain  it  in  hi^ 
as  is  practised  wiili  indi::o  The  annutto  prepared  in  this  war  0 
said  to  be  four  tiitned  as  valuable  as  that  made  according  10  tiic  fint- 
described  process. 

It  does  not  appear  from  either  of  these  descriptions  tltat  aarlbisf 
is  added  to  the  annutto  except  water.  Thia  is  important  with  relertaee 
to  its  adulteration. 

Before  proceeding  to  enter  upon  the  question  of  the  ailu'i 
any    article,  the  first  «tep  necessary  is  to  mnlce  onesell    : 
with  its  properties  and  (.hararteri^tics  ;  and  if  the  sub»taiiCL-  i-^  v.- 
tabte,  il  is  requisite  that  we  shoiilii  deternunif  its  structure  b*  m'-^w 
of  the  miiTOscope.     We  thus  obtain  certain  fixed  data  or  sitwU'^ 
of  comparison  from  which  lo  starL 

Structure  of  tfm  Stred  of  AMnaUo. 

SubjtH'lin;;  the  sced<4  of  annatto  to  examination  with  the  miuigiuy 
we  tind  that  their  outer  or  red  portion  does  not  exhibit  any  ver^ir 
finite  struciure.  that  the  surface  of  the  «eed  proper  tvinsisiAoTDtm^ 
or  elongated  cells  or  fibres,  vertically  disposed  ;  while  the  iniKr«iik 
pirlinn  cmsists  of  cells  filled  with  numerous  starch  conMudot*^ 
delini^d,  i.it'  medium  size,  and  resembling  in  form  and  m  tht  ^1^ 
gatc<l  and  stellate  hilum  the  starch  granules  of  the  pea  tad  bc»> 
Fife-  111- 

In  ^^^nwinr  mnnufuctured  annatto  but  little  structure  !»  m«iirit&> 
portions  of  the  outer  cells  are  however  seen,  as  well  a*,  in  tho«  ipa» 
mens  which  in  the  course  of  their  prejmnition  have  not  bcesia^ 
JGCted,  as  they  usually  are,  to  the  action  uf  boiling  water,  a  few  td  it 
starch  corpuscles. 

Annutto  is  used  by  dyers,  painters,  soap  makers,  and  to  coluut  wA 
butter,  and  cheese. 

By  dyers  and  soap  makers  it  is  frequently  pnrohasc«l  ftw  ta»  i* 
the  state  in  which  it  is  imported,  these  parties  adding  the  alkalis* 
solvent  a^  tbev  u^  11;  in  these  cases  it  docti  not  pass  throng  1^ 
hands  of  the  hn<;lish  so-eallctl  manufacturers  at  all.  In  olW  W 
the  manufacturers  re-prepure  it  in  the  several  forms  of  ruU,  e^ 
orange,  black,  and  lluid  annattoj. 


ANNATTO,   AND   ITS  ADULTERATIONS. 


467 


Compoiition  of  Annatto. 

The  pulp  surrounding  the  unfermented  fresh  seeds  was  found  by 
Dr.  John  to  consist  of  28  paru  of  colouring  rcMuous  mutter,  26  5  of 
vegetable  gluten,  20   of  ligneous  fibre,  20  uf  culuurJug,  ejttractive 

Fig.  in. 


W:  &'^  »  «  V  2> 


-^^■ 


nUi  tltnftlcd  bciw-M-n  iba  bMk  sad 


tf,  cell*  uf  MMi  proper  eoB" 


matter  4,  formed  of  matters  unnlnTous  to  rentable  gluten  and  ex- 
tractire,  and  a  trace  of  spicy  and  acid  maCten>. 
The  colouring  matter  is  soluble  in  water,  but  more  so  in  alcohol 
u  B  2 


4R8 


ANXATTO,    AND   ITS    ADILTERATIONS, 


and  alkalies.  The  latter  change  its  colour  somewhat  from  red  to 
uraiige.  When  annntto  is  use<l  ft5  a  dye,  it  i»  cut  in  pieces  and  boiled 
in  a  copfier  with  cruele  pearl  ashcfi. 

On  subjoftiiiff  the  soeelt^  nfannatto  to  examination,  we  obtained  an 
nsh  whiu'li  weighed  4'60  f^rains  per  f:ent..  and  which  was  nearly  whitr, 
with  here  and  there  >b  faint  tinge  indicatin;;  the  presence  of  a  iiit?re 
trace  of  iron :  it  yieMeil  *20  of  a  giain  per  cent,  of  aluniina,  tinged  onljr 
Tery  slightly  with  iron. 

The  red  or  outer  part  of  the  seeds  yielded  on  examination  nearly 
similar  restdt<4. 

These  riNulta  may,  therefore,  as  we  shall  see  more  fuUj  hereafter, 
be  tAken  as  representing  to  some  extent  the  proper  weight  of  the  ash 
of  genuine  annatto,  and  of  the  iron  and  alumina  which  it  usuallv 
contains. 


I 


On  the  Apultkbations  or  Amtatto. 

There  is  scarcely  an  article  witli  which  we  are  acquainted  sub* 
jeotfld  to  BO  large  an  aiuuunt  uf  adulteration,  and  this  ot'  the  grossest 
possible  description,  as  annatto. 

The  Niibstances  employed  are  various,  acme  of  them  boing  organic 
and  aihera  inorganic. 

The  itrpanic  adulterntions  which  we  ourselves  have  detected,  are 
tbo.«e  with  tnrmeriCy  rye,  harle^j^  anrl  wheat  llours. 

The  innrgame  mlulterations  observed  by  us  are  as  follow  ;  with 
tiulphitte  of  limc^  ctirhfmaie  of  lime  ^  sult^alkali^  an  oily  suhatance^  pro- 
bably soop,  r^*d  ferruginous  earths,  mostly  Vetutian  red,  red  Uad^ 
and  copper. 

The  employment  of  large  quantities  of  fluur  and  of  lime  so  reduces 
the  colour  of  the  annatto  that  it  becomes  necessary  to  have  recourse 
to  salt,  alkalies,  and  the  red  earths,  to  restore  it  to  something  ap- 
proaching its  natural  standard. 

The  efteut  ol'  salt  in  heightening  the  intensity  of  vcgetAble  reds  is 
well  known,  and  hence  its  use. 

The  lead  detected  WiLs  probably  introduced  into  the  annatto 
through  the  Wnetiiin  red  used. 

At  fii-st  we  were  disputed  to  regard  the  copper  in  annatto  as  an 
acciilentiil  impurity  :  there  is  good  reason  for  believing  that  it  is  pur- 
posely addc'l  to  prevent  the  annatto  from  l)ccomin!r  attacked  with 
fungi,  and  to  which  it  is  so  prone,  in  c»n5eijuence  csperially  nf  it* 
admixture  with  such  large  quantities  of  flour  and  salt.  The  saJt  by 
attracting  moisture,  hastens  tho  ilccom[:tositioa  of  the  flour. 

UeituUt  of  the  Examination  of  Samples. 

The  following  results  were  obtained  from  tlie  examination  of  Thirty' 
fnir  samples  of  annatto  of  all  kinds  fljr  imported^  as  obtained  from 
English  manufacturers^  an'l  as  purchased  from  dealers; — 


ANNATTO,   AND   ITS   ADULTEBATIONS. 


469 


1st,  That  of  the  thirty-four  aamples  of  annatto  of  all  kinds  ex- 
ftiiiined,  two  only  were  genuiue^  ftud  wero  entirely  free  from  adulteru- 
tion  ;  these  being  two  red  CAke  ammttos  a«  imf>orted. 

2iid,  Thai  the  whole  \ji  the  reiniininjj  Kauipleti  consisted  oi' mtxhtre$ 
i«  varitmx  propttrlums  of  one  or  more  substances^  these  amoniifiu};  in 
vtany  Cfites  to  one-'hal/y  and  in  some  ttutanet  to  even  two'thirds  of  the 
entire  specimens. 

3nl.  ThtLt  of  the  two  samples  of  Black  Annatto,  obtained  from 
manufaoturorSf  one  furnished  a  hij^lily  ferruginous  ash^  which  was 
very  alkalint.',  which  amounted  to  32'50  per  cent.,  and  which  con- 
siiited  of  un  alkali^  some  chalky  and  a  red  ferruginous  earth;  wliile  the 
second  yielded  un  ash  that  wei;:hed  35-'^6  (wr  cenL,  which  was  still 
more  ferr(if:inous,  and  which  consisted  ni  alkali  and  some  rtd  earth. 

4th.  That  of  tlic  four  samples  of  Orange  Cake  Annatto.  obtained 
from  manufai-tnrers.  one  ftimistieil  an  cuA  whioh  amounted  to  titf'OO 
per  cent.,  and  which  consisted  chii^ily  of  rhalk^  wlib  a  trace  of  lead: 
the  ash  of  the  t^oond  sample  weighed  o7'7*i  grains  per  cent.,  and  oUo 
consisted  principally  of  ehath ;  the  third  sample  contained  a  large 
quantity  of  turmeric  and  a  little  wheat  flour ;  the  ash  uuHjiiuled  to  •144 
per  cent.,  and  coitsisted  of  vhuth  and  bojne  red  earth,-  whilcr  the  u*/i  of 
the  fourth  sample  weighed  63*00  |jer  cent.,  and  was  composed  chieMy 
of  chalk, 

5ih.  That  of  the  two  samples  of  Red  Cake  Annatto,  procured  from 
niiutufacturers,  one  contained  a  very  lar^e  ouantity  u{  wheat  flour,  and 
yieUled  17'll2  per  cent,  of  ash^  which  consisteil  of  salt  an<i  liome  red 
earth ;  the  other  nUo  contained  a  very  large  quantity  of  wheat  /hur^ 
and  furnished  14  ;2()  percent,  of  ash,  consisting  chietly  of  salt  and  aome 
ferivginnxis  earthy  colanring  matter. 

tith.  Tliat  of  iht  five  sompleit  of  Orange  Cake  Aniuittos,  purchased  of 
different  retail  dealer*,  one  yielded  57"HO  per  cent.  lA'  u^A,  which  con- 
flisiL'd  principally  of  rAaU  ;  a  second  cnntauied  a  very  lur^je  quantity  of 
tunnertc^  and  gtive  an  luA  which  weighed  3f)'uf>  per  cent.,  and  which 
was  com}io«ed  of  ehaUl  and  a  red  ferruginous  earth  ;  the  third  contained 
the  starch  of  tago^  the  oeh  weighing  58*46  per  cent.,  which  was  coui- 
)KJsed  chiefly  of  chalk  ;  the  fourth  c<mtaineu  a  very  large  quantity  of 
turmericy  and  yielded  40*30  per  cent,  of  ojA,  cumposetl  of  chalk,  fervM- 
giaous  earth,  and  a  little  salt ;  while  the  ftllh  gave  0U't2  j»er  iieni.  of 
ash,  which  congiftted  principally  of  chalk  with  traces  of  lead. 

7th.  That  the  »anq>les  of  Hed  Roll  Aniuitio  nearly  all  containetl  large 
quantities  of  either  wheat,  bnrUy,  or  rye  Jioxir — u^^ually  the  latter,  to 
the  extent  of  30  and  even  over  40  per  cent. ;  much  saU  and  some  retl 
femtginouM  earth,  as  Venetian  red,  red  ochre,  or  reddle. 

lieviewing  then  the  results  of  the  miL'n)scopical  and  chemical  exami- 
nation of  the  thirty-four  samples  of  annatto,  it  apfwars  that  large 
quantities  of  turmeric  were  present  in  three  Siini])Ie^,  wheat  or  barley 
fiuur  in  fnur,  and  rye  fiitur  in  nine;  the  majority  ot  these  snuiplescun- 
taining  full  forty  per  cent,  of  Hour ;  that  chalk  was  present  in  a  great 

■  a  3 


470 


AJiJiATTO,  AND   ITS   ADULTEKATIOXS. 


nwoj  7Sie««  Ireqaentlj  to  the  extent  of  fiAy  and  ctcb  orer  sixty  per 

cent^  nipha/e  ofUmt  in  at  least  five  cases,  a  rrd  ferrvgimom*  earth  in 
a  great  manr,  s.n  alkali  in  iereral,  tali  in  manj,  Uad  in  fire  ca»e«,  and 
c^>pP^  in  &^  least  fuor  aamptes. 

The  iro*  and  alumina  amnanted  in  some  cases  to  near  tbree  and  eren 
over  fire  per  cent.  Had  all  the  samples  been  examined  qaalitaUvelj 
for  iron,  it  is  probable  that  stfll  larger  amoanss  wnuM  bave  been  met 
with,  as  the  wont  casei  were  not  specially  selected  fur  examination. 

\a  two  of  the  6vt!  fomples  in  wbich  Uad  was  det^^^d.  the  quiintity 
was  not  weighed^  and  19  described  as  /races  onlv,  while  in  tbe  utfaer 
three  ssmplen  rhe  nnantitiea  amounted  10*30,  '50,  and  to  1  "20  per  cent. 

M7  friend,  Mr.  Hogfr^the  sutborof  the  ^Treatise  on  the  Microscope," 
himself  procured  fome  samples  of  anoatl«\  and  found  them  to  be 
adulterated  with  rye  and  barleg  flours,  turmenc,  wJt,  red  mrik,  and 
carbonaU  of  lime. 

Lsstlr,  the  following  analyses  by  Dr.  Benwys  embody  the  results 
of  the  chemical  examination  of  the  ashes  of  bve  samples  of  annatto 
furnished  him  bj  the  author. 

No.  1 

Ash  of  100  grains,  wei»bed  62*40,  wbich  was  compofed  of  — 


Carbonate  of  lime 

-  37-88 

I 

Sulphate  of  lime 

-     »*82 

1 

Alkaline  sulphates 

-     4*34 

1 

Chloride  of  sodium 

.     6'42 

I 

Iron  and  alumina 

-     •214 

1 

Lead,  traces,  sand,  &c. 

.     2-80 

1 

62-40 

\ 

Xo.  2. 

No.  4. 

Ash  of  100  groins,  weighed 

Arth    of     100    grtins, 

weighed 

1970:  — 

13-&5:  — 

Chloride  nf  sodium     -  687 

Chloride  of  sodium 

-  431 

Sulphate  of  lime         -  412 

Sulphate  of  time 

-  5-92 

J  ron  and  alumina       -  1*40 

Iron  and  alumina 

-  1  32 

Sand,&c.      -            -  1-31 

Sand,  &c. 

.  2  40 

13-70 

No.  5. 

ISdS 

No.  3. 

Ash    of    100    grains, 

weighed 

Ash    of    100    crains,    weiirhed 

62  26  :  - 

17*20:- 

Carbonate  of  lime 

-  42  00 

Cbloride  of  »o<Hum     -  9*30 

Stilphnte  of  lime 

-     884 

Sulphate  «f  lime         -  4*00 

Chloride  of  sodium 

•     6  56 

Iron  and  alumina       -     *90 

Iron  and  alumina 

-     3*20 

Sand,  fiic,       -            -  300 

Sand,  &c.     . 

-     166 

17"20 


62'26 


AXNAXrO,    AND    ITS    ADULTERATIONS. 


471 


The  presence  of  Irar!  in  annatto  haa  lieen  detcctod,  not  only  by 
ourselves,  but  by  Accuin,  MitclK'lI,  Bernny.-*,  trnd  Noroiandy. 

Accum,  at  nape  270.  of  his  "Treatise,"  has  written  to  ibis  eflect : 
—  "Several  in»tanee«  have  come  under  my  knnwledjje  in  which 
Gloucester  cheeae  hiu  been  contaminated  with  red  lead,  ami  has  pro- 
duced serious  consetjiienccs  nn  beinf;  taken  into  the  stontnch.  In  one 
poisonous  finniple  which  it  foil  to  my  lot  to  examine,  the  evil  had 
Dcpn  caused  by  the  sophiitlicution  of  the  annatto  employed  for  colour- 
int;  chccfte.  This  substuncc  was  found  to  contain  a  portion  of  red 
lead."  Accum  then  Roes  on  to  nuote  the  particulars  of  a  case  re- 
conled  by  a  Mr.  Wrijrht,  of  Canibritijre :  —  A  gentleman,  after  par- 
taking of  some  tonated  cheepe  at  an  inn  t>n  two  difltrent  occasions, 
was  both  times  made  ill  by  ir.  The  matter  was  referreil  to  the 
manufacturer  of  the  cheese,  who,  on  inquiry,  ascertaiiii-d  rliat  the 
annatto  which  had  been  used  to  colour  (he  cheese  was  itself  coloured 
or  adulterated  with  Itoth  vcrniilinn  arxl  red  lotd. 

Mr. Mitchell,  in  his  "Treatise  on  the  Falsification  of  Foml,"  published 
of  1848»  states  paj?e  231: — "I  have  frcipicntly  examined  s|>ecimens 
in  annatto  which  hare  been  contuminatud  with  red  lead,  or  u  mixture 
of  red  lead  or  (K'hre.** 

Liistly,  Dr.  Normandy,  in  his  "Commercial  Handbook  of  Chemical 
Anftly.«i»,"  wriles,  "Untnrtumitely  as  it,  annatto,  is  very  ohen  atlul- 
terateil  with  red  Icail,  or  with  i>o|h  reil  ledtl  ami  rtchre,  the  u?e  of 
such  annatto  is  very  injurious,  and  serious  accidents  have  been  caused 
thereby." 

Two  of  the  autliors  quoted,  viz.,  Accum  and  Mitchell,  testify  i«i  the 
fact  of  the  presence  of  lead  in  annatto  and  cheese  of  their  (twn  know- 
ledge- It  is  not  oleiir  whether  Dr.  Normandy  dttea  go  or  not,  or 
whether  he  merely  re|>eats  ihe  statements  of  others  on  the  subject. 
Now  there  i;*  no  cvaditiir  the  evidence  of  the  first  two  witne?'5es. 

We  would  further  obfcrvi^,  tliat  in  some  of  the  samples  examined  the 
ingredients  were  so  badlv  mixed,  that  in  some  instances  we  picked  out 
specks  or  masses  of  the  substances  added,  us  of  the  different  kinds  of 
ilour  used,  turmeric,  chidk.  and  red  earth. 

Now  the  muntifai.'^lurers  of  unnutto  will  doiihtUiss  try  to  [H.'rsuo'ie 
us,  and  [wrhaps  others  who  are  not  manufacturers  will  do  so  us  well, 
that  some  of  the  substances  which  we  have  mentioned  are  introduced 
to  improve  the  article,  to  render  it  more  soluble,  and  to  make  it  keep 
iMUter.  We  are  ready  to  .admit  that  the  use  of  alkali  is  pertectly 
justifiable  to  render  it  more  soluble,  but  beycmd  this  we  do  not  ;!o; 
and  allowyy;  this  plea  of  improvement  to  have  all  the  wei^^ht  that  con 
possibly  belong  to  it,  enougn  will  still  remain  to  show  that  annatto  is 
subject  to  a  lur^e  amonntof  ailulterntion,  for  it  is  impossible  to  jut>tiiy 
the  use  of  turmeric,  of  Venetian  red,  or  reddle,  of  40  or  50  |t€r  cent. 
of  whvut,  birley,  or  rye  flour,  and  of  50  and  over  60  per  cent,  uf 
chalk  and  sulphate  of  lime. 

With  respect  to  the  plea,  which  may  possibly  be  nrged,  that  some 
II  II   4 


i 


4n 


AVSATiO^   jUTD   m  ADCI-TZAXTIOSS. 


wiD  kae*  ■gfecdty 
m4  iLtftfe  1 


t«Mi  tfci7  attnctad 

ncnM  IB  mIi  wtonb  wt^p^ta  13  per  eent^ 

irML     jUocWr  iiMili.  oM  of  tkn«  leac  by  Ur.  Bma, 

wkk  Mtiag  hf^g,  mJ  jtA  this  uwiImwiI  ■  bfee^HMAito^ 

fgJar,  ■■fffh,  aik,  aatf  s  ral  «aitli— ii«  •£  mmmmm^  im  S« 

ccM^  mmI  j^cUiag  170  per  ccM.  «r  fen  aad  tAmmt,  m  jtA  m 

8oae  of  tW  Maple*  exMuned  «d 
CM.  of  ttHMllox  aiirf  ocmU  it  he  thomn  tlwl  tke  re4actio«  Wi 
(O  1^  cnvnDCMM  cx(«at  warn  jtrifahir  —  vUdk  hovevcr,  it 
ic  wif — Ui«n  it  cannot  be  denied  it  i*  bigh  dme  tbat  tbe 
uiBftlio  ibAoU  be  abaBdoned,  and  tbat  sooe  Bnaeor 
•dopCed  vbicb  voohl  ezpreu  the  arcual  cnapoMciaa  of  ibe  i 

•erre  to  indicale  tbe  fact  that  tb«  article  tbai  redneed  

oni/.  flDd  Tfau  oAca  tbe  ■■■Hwf  pvt,  of  tbat  whicb  it  priiftir  ii  lo  be 
—  viz^  Sfinaito. 

Mr.  W)ikl«r,  wbo  gare  tome  bixhlr  intereBting  and  importaat  t»* 
formalirm.  in  rtruonl  (o  adulteration,  before  tbe  PaiiiaiiMntarT  Co«»- 
iui(ler,CJ>fiiiiiunk->ti:r<l  the  fullowin^ evidence  re^-recttnjr tbe annattoicnt 
i*ut  by  %  hiiu*K  to  whii-b  he  wa»  attaclie<l  in  earlr  life: — **  It  coorirted 
of  ffa^  anitatli)  half  a  pound,  powdereil  tiirnirric  thre«  oanoes,  pov* 
dercii  liiue  three  nunce«,  and  sol't  soap  ten  ounces.  But  freqaenlljr, 
when  there  wad  no  Ba;;  annatto  to  be  ho*!,  on  additional  (|tt&olitj  of 
turmeric  woa  put  in,  witli  some  re«]  colour  wbieh  I  do  not  now  recol- 
lect; but  often  it  wil<  wnt  out  without  a  |»artiele  of  unnatto.  Xbe 
powder  fur  inouldint;  the  annatto  coutifted  of  eight  ounces  of  wbuiaj^ 
and  two  iMine'.'s  of  Uutcb  pink." 

We  have  unir  ailvant*ed  enough  to  prore  that  annatto  ia  extenaivel/ 
and  icoridulouflly  adullerutetl. 

At  the  meeting  of  tbe  Plmrmieeutical  Society,  to  which  the  author's 
paper  on  the  adulteration  of  annatto  was  communicated,  ^Ir.  Tbeo- 
phdus  Ri'dwiHi'l,  whose  views  in  regard  tu  euiiventional  udu Iterations 
^C^  have  exeiteil  nn  much  iinrpni!»c,  uuilertiKik  the  Quixotic  task  of 
priivinir  thnt  the  varioti«  tubstaiices  fuund  in  ailullerated  unnatto  were 
ull  abided  V^  iniprnre  tiie  article,  Mr.  Retlwood  not  even  obje<:ting  to 
the  Bulphfite  nf  copper  found. 

Ainonpft  the  evidence  pven  before  the  Parliamentary  Committee 
in  defence   oi'  udulteriitiou^  excc|iting  only  that  of  I^Ir.  Kedwoud, 


ANNATTO,    AND   ITS  ADC'LTKUATIONS, 


4X3 


none  was  xnorc  remfirkable  for  extraordinary  aA^ortion  limn  thnt 
of  Mr.  Drew,  of  the  firm  of  Drew,  lleywanl.  iiiiil  Barron,  wbolcsule 
drii;;f;ists.  The  few  followirij^  particulars  will  serve  to  show  tlie  cbu- 
ruftur  of  Mr.  Drew's  evideriue  :  — 

llu  denied  that  anniitto  was  adulterated,  on  the  ^ound  thnt  it  was 
f>by!)icully  iii)(>oistble  to  uijx  tuniieric  with  aniutto,  the  fact  being 
thuE,  nothing  id  more  earty. 

In  nice  manner  he  denied  that  cinnninon  wo^  udultorated,  nnd  nllcged 
that  cossiu  was  as  dear  as  cinnamon  ;  also  that  arrowroot  was  m>t  adul- 
terated,  bidco  sti^  an<l  iK>taif)  powders  were  worth  as  mnrh ;  and 
Jnstlvt  he  llitlly  denied  that  nptces  were  adulteraicd  in  any  degree, 
these  asiiertions  being  iin<iupporttiU  by  a  particle  of  proof. 

We  now  come  to  uiuke  a  few  remurks  on  theeiuplnynient  of  annatto 
in  ilie  colouring  of  njiik,  butler,  but  prinripally  cheese.  We  would 
first  state  that  we  do  not  apprehend  thai  dmijter,  we  will  not  say  ever, 
is  olien  likely  to  I1^i^e  iVoiu  tlie  m:casionnt  presence  of  lead  in  an- 
nntto.  seeing  that  the  quantity  u>ed  to  colour  cheese  U  but  small. 

The  practice  of  colouring  cheese  with  annatto  entails,  however, 
*inie  cx[>ense  and  trouble,  while  it  serves  no  really  useful  purfMMe, 
and  nn  these  g^rounds  it  is  to  bt*  condemned  ;  but  on  this  point  we  will 
cite  the  opinions  of  two  well-known  autboriliea  on  diiiry  fanning;. 

In  ibe  ^'kural  Cyclopaedia,"  part  i.  p.  1*27.  we  find,  nmimgst  other 
renmrks  relating  to  annatto,  the  following:  —  "Another  variety  of 
annatto  iliat  is  commonly  employed  in  Knglish  dairies,  is  munufac- 
tui'L'd  in  Brazil  into  small  lolLs  t;aeU  tiro  or  three  ounces  in  weight, 
hart],  dry*  and  compact;  brownish  without,  and  red  within,  liul  its 
grand  interest  to  the  farmer  consists  in  its  very  extensive  use  as  a 
colouring  matter  for  butter,  and  especially  cheese.  The  clieese 
mukLTs  of  Gloucestershire  give  uno  ounce  of  unnulto  to  one  hundred- 
weight of  cheese,  and  tlKue  nf  Chesfhiro  eight  dwls.  to  sixty  pounds. 
But  as  thetw  nuanlities  are  far  too  small  to  medicate  the  checjc,  or 
even  to  oA'cct  its  Havour,  the  only  advantage  to  be  derived  from  the 
annatto  is  mere  colour,  and  surely  the  appearance  of  Stilton  or  Dunh>p 
chet'>e  uwm  the  table  is  to  the  full  uji  agreeable  lis  (hat  of  Gloucester* 
shire  or  Cheshire  cheese,  'llic  use  of  annatto,  therefore,  is  sheerly 
vrhimsical,  imposing  perfectly  U9elc3*s  trouble  on  the  manufacturer, 
and  some  small  ridiculous  expense  U|'>on  the  purchaser.  The  mo<le 
of  using  it  is  to  diasolve  it  in  the  hot  milk  immediately  before 
churning." 

Mr.  Stephens,  io  hi»  **Book  of  the  Farm,"  part  iii.  p.  288.,  makes 
some  observatiims  on  the  use  of  anaalto  to  colour  cheese,  nearly  lo 
the  same  cfTecl.  He  says  :  —  "I  have  not  recommended  the  use  of 
annotto,  or  arnotto,  for  dyeing  cheese,  because  I  think  by  it  the  chfe-ine 
fnrniers  imposo  u(w>n  thrniMflvcs  a  very  useless  iiiece  of  trnuble. 
All  the  quantity  enifiloyed  i;*  said  to  impart  nn  mn^uliur  flavour  to  the 
chi-ese  ;  which  being  ucknowledu'cd,  of  whiit  utility  is  it  ?  As  for  im- 
proving the  appearance  of  obeese,  I  suppose  it  will  uut  be  denied  that 


474 


ANNATTO,    AND    ITS    ADULTEItATIOSA. 


Stilton  ani)  Dunlop  cheese  look  as  well  upon  the  fable  u  Glouefftrr 
uud  Cheshire  cheese.** 


On  the  Detection  of  the  Atlvlterationit  of  AmidUo. 

Annntto  in  the  manufactured  stale  pre5enlinp  w  few  ervimK* 
of  structure,  it  is  a  very  easv  matter  indeed,  hj  means  nf  thf  ralm'- 
scope,  U)  (letet-tthe  prci<encein  it  of  most  foreign  vegelAble  sul»taBn^ 
n?  turmeric  potcder,  and  the  starch  of  wheats  rye,  hoHty^  ini  ff 
flowi. 

Tlie  tuniieric,  owiuu;  to  the  action  of  the  ?ult  and  alkali  u^ 
sent  witli  it  in  the  annatto,  is  generally  much  chanee'I  ;  ni 
colouring  mnttor  of  thf  >"ell:i)  is  discliargwi,  so  tbat~  i\\--  ■  in   'i 
pnscles  fonfaincii  williin  them  become  visible ;  loose  st^p  h  •. :  i    t 
turmeric  mav  also  he frpijuenlly  seen  presentinjr  their  usual  ii- a:!  ■ 
except  that  they  nre  much  increasea  in  size  in   eonscf^ucnt.. 
action  of  the  alkali  upon  tlieni.    Fig.  178. 

The  L*hiu*acters  of  turMitric  powder  will  be  found  Ue9onbe<i  »*  ^ 
387  ,  of  whciu  at  p.  243.,  of  rye  at  p.  240.,  of  liarley  si  |>,  2-W.  and  rf 
snjjn  star<-li  at  p.  1124. 

Tlic  presence  «>f  most  of  the  inorganic  adulterotioi^t  is  in  many  cwm 
sufficiently  manifest  by  the  appeiinnoe,  woijilit,  and  taste  of  tJM^idL 
Thu*i  the  weight  of  the  ash  pencrally  »*'rves  to  show  the  prv*?tn*«f 
sulphrite  find  cjirhoniite  of  lime;  the  colour,  the  pcesono**  <if thr  ii4 
earths ;  and  the  taste,  the  salt  and  alkali :  the  pro!>encv  of  salt  can  iodeol 
generally  be  ascertoinc'd  by  the  tafieof  thennnatto  luelf.  SountJMHb 
however,  a  cpiantitativc  cxtiniination  is  reiiuired. 

The  inorganic  substances  for  which  annatto  has  to  l>«  tested  dKB^ 
callv  are  sulphate  and  carbitnate  of  lime ^  carbonate  ofpobuA,  eUondf^ 
tttdium,  red  ferrugino^us  earths^  Uad^  and  copper. 

As  several  of  the^te  substances  sometimes  occur  in  the  aatoe  tailitafc 
we;Hh:ill  not  deju*ribe  the  prnce»ses  for  the  detection  of  eAcb  a^ 
substances  met  with  separately,  but  in  the  form  of  s  coralNrf 
analysis. 

Incinerate  100  grains  of  the  annatto.  \reighthcash,puIrerMr;lt«t 
with  about  half  an  ounce  of  distilled  water :  thi$  will  separattti* 
chloride  of  sodium  and  the  curbonnte  ofso^la  or  potash,  «}i>*ul<l  eiikf 
of  these  be  present;  and  the  quantities  of  which  maj  be  nlimaM  ^ 
follows : — 

Divide  the  solution  Into  two  parts  :  precipitate  from  rmclhetWaflM 
of  the  salt  by  means  nf  nitrate  of  silver^  and  calculate  tJie  eU«if^ 
of  silver  fortiiod  into  cltloride  of  sodium.  Evaporate  ilie  olbcrpori* 
of  the  solution  nearly  to  dryness,  treat  with  a  little  hydnocWonc  ari^ 
dilute  with  a  small  quantity  of  water,  and  proceed  in  the  wiiiiaM* 
nf  the  carbonate  of  soda  or  |)otaah  in  the  manner  indicated  in  tfe  ^^ 
cle  on  Turmeric, 

Boil  the  portion  of  the  ash  insoluble  in  water  in  a«  amaU  a  qatfi? 


AXXATTO,  AND  ITS  ADCLTEnATIONS. 


^7B 


na  possible  of  pure  but  dilute  nitro-hydrochloric  acul :  dilute  with 
wutor,  filter  ;  weigh  ihi;   resiilu),*   insoluble  in  the  ucid-i^  and  deduct  it 

r/g.  in. 


lift,  ■Ur«li  i)rkiitili-t  ;    c  r,  Mill  u(  ittmieHc  t  >i  i^  t***  lUticli  fruiolw  af 


from  the  gron  weight  of  the  uh  :  it  will  consist  of  silica,  sand,  and 
some  unburned  eurbon. 

Divide  the  solution  into  two  parts  from  one  ;  throw  down  the  sul- 
phuric icid,  if  present,  bv  meni^s  of  nitrate  of  bnryta  ;  collect,  wash, 
i^nitf,  und  weigh :  from  the  otiier  precipitnte  the  lime  with  oxalate 
of  ammonia:  culeulate  the  sulphurit*  ucid  into  sulphate  of  lime :  if 
there  in  any  exceu  of  lime,  ctdculale  it  into  carbonate  of  lime. 

We  have  now   only  to  estimHte  the   alumina  and  iron,  Uad^  and 

For  the  determination  of  these  it  U  he«t  to  oftcralc  upon  anothnr 
portion  of  ash  :  diMolve  with  heat  in  diitit&  nitric  acid,  evapornle  nearly 
to  drynew,  dilute  with  water,  and  divide  the  solution  into  two 
portions. 

Katiinate  the  iron  and  alumina  in  one  portion,  wparating  them  from 
the  phosphates  iu  the  manner  directed  under  the  article  Chicory  at 
p.  U9. 


476 


ANXATTO,   AKD   ITS  ADULTEUATIOXS. 


In  tlm  other,  estimate  the  copper  mnd  lead  qtuiiiiubnlj  m 
follows:  — 

Si:j>iir;iti.'  the  lead  from  the  copper  b)"  menus  of  pure  dilute  «u){iiartf 
anid,  adiii^d  in  tiliglit  excess  :  tlic  preei|Utnto  inu»t  be  washed  fint  tn^ 
water  acidulated  with  laulphuric  acid,  and  finnlly  with  spiritAorvtM; 
dr^',  ignite,  and  weigh. 


Akkatto  •duluntad  villi  rj/tJhiM:    H^nlftcd  as  dUmettn 


Precipitnte  the  copper  hy  means  of  xtilphurotted  hjdroj^ 
dry,  wer^^li.  and  calculate  into  the  sulphate. 

Or  t\w  following  process  may  bo  adopted  for  the  Bcparation  rf  tU 
lead: — Mix  the  concentrated  nitric  acid  solution  with  h\  '■ 
in  excem  ;  odd  u  larpe  quantity  of  absolute  alcohol   m 
ether  ;   let  the  precipitate  su)>eide,  lilter  the  fluid  otT^  w 
tate  with  alcohol  and  ether,  dry  it,  and  expose  it  to  a  - 


»j>- 


The  folli»winjE  process  for  detectinjr  and  e5timatin<:  tiUMUi^.- 
tities  of  oxide  nt'cojipiT,  in  hy  Mr.  Warinjxton  :  — 

*'Thi8  operation  depend:*  uiMin  the  solubility  of  the  fermcyiBiib  1^ 
copper  in  an  excess  of  a  solution  of  ammonia,  and  lu  deposiDM  «ilk 
its  well-marked  characteristic  appearances  as  the  amiaonia  cnfiirilv 


J 


CHEFSE,    AXD   ITS  ADULTERATIONS. 


477 


Thus,  siippoiiin^  n  frequently  occurring:  case,  where  the  oxiilc  nf 
coppLT*  in  vavy  small  fjuiinlity,  is  in  soliitinn  with  oxide  of  ircm,  nnd 
tlmt  tbi'sc  mijtali^  have  ^iwn  brought  to  thfir  hir«h^*8t  stiile  uf  uxidutioii ; 
ammoiii:i  is  next  ailJeil  in  excess,  and  then  a  (««  "Irnpt  nf  n  solution 
of  the  feiToeynnitle  of  potassium,  and  the  wliolt?  thrown  u|ion  a  filter. 
As  the  iimmoniii  escapes  from  the  filtrate  bv  standinir,  and  free  ex- 
posure to  the  air,  the  red  ferrocyanide  of  c<»ppor  will  he  deposited, 
and  if  the  oxperiraent  be  made  in  a  shallow  white  poroeliun  dish,  the 
result  will  be  very  dlstinet  and  characteristic,  and  on  earci'uHy  de- 
canting the  fluid,  will  be  fount!  on  th-jwhite  fiirface.  In  many  cases, 
the  process  of  filtration  may  be  dispensed  with  nltojjelher,  us  the  sus- 
pended peroxide  of  iron  dne«  not  in  the  lea.^t  intt?rfifre  wirh  the  de- 
pnsition  of  the  ferr'icvniiide  of  copper  from  the  solution.  I  have  found 
this  test  ^ire  «nerrin«(  iiidirations  incases  where  no  trare  of  blue 
colour  could  be  dwtin;zulsbed  in  the  amraoniacal  solution,  and  where 
no  precipitation  could  t>c  procured  by  hydrosulphurie  acid  gaa  or  the 
action  of  a  voltaic  circuit. 

"  When  organic  colouring  matter  is  present,  this  form  of  lest  is  also 
very  useful,  as  in  vinegars,  &c.*' 

Aunutto  iit  free  of  dutr  on  importation.  Quantities  imported  in 
1854,  4,371  cwts..  value  2\4\hL;  in  IH55,  '2.9CC  cwts.,  value  14,765/. 

Further  parliculurs  in  regard  to  (he  adulteration  of  unnHftowill  be 
found  in  the  author's  pAi>er  published  in  the  "PhnrnmccuticalJourDal  ** 
for  January,  185^. 


CHEESE,  AXD  ITS  ADULTERATIONS. 

CuBESH  consists  of  the  curd  of  milk,  freed  from  whey  to  a  certain 
extent,  and  ripened  by  keeping. 

The  curd  is  usually  precipitated  from  milk  by  means  of  a  srlution 
of  rennet,  which  in  prepared  from  the  dried  stomach  of  the  calf  and 
sometimes  the  pig. 

It  may  be  precipitated  by  means  of  acids,  but  tbeae  are  rarely  if 
ever  employed  in  this  country  in  the  mnking  of  cheese  ;  n!s*i  by 
several  other  substances,  as  pure  cunl,  old  chefse,  the  nutiiral  fluids  of 
tlie  stomach,  the  first  extract  of  malt  and  sour  leaven.  Professor  Jnhn- 
atun  particularly  recommends  trials  to  be  mnde  of  the  pure  prepared 
curd  :— •*  If,"  he  remarks,  "  we  are  able  to  rescue  the  umnutncture  of 
rennet  out  of  the  my«terio«s  nnd  empirical  handi^of  the  skilled  dniry- 
niiiid,  and  by  the  us«  of  a  simple,  abundant,  eonily  prepared,  and  pure 


479 


CHEESE,   AND  ITS  ADULTERATIONS. 


rennetf  can  command  at  once  a  ready  conflation  of  ih^  milk^  and  a 
curd  naturally  Bwcett  or  of  a  flavour  which  wo  had  foreseen  untl  com- 
mended, we  slioultl  have  made  a  considerable  step  towardii  the  pcr- 
fuftion  (»f  the  art  of  cheese  making.'** 

Curd  forreiiJiet  may  be  prepared  in  the  fuUowing  manner  : — "  Heat 
a  ijuanlity  of  milk  which  has  stood  for  five  or  six  hours,  let  it  coul« 
nnd  separate  the  cream  cuinpli^tely.  Add  now  to  the  milk  a  little 
vinegar,  and  heat  it  pentlv.  The  whole  will  coagulate,  and  the  curd 
will  separate.  Pour  off  tlie  whey,  and  wa^sh  the  curd  well  by  knead- 
ing it  with  repealed  portions  of  water.  When  pressed  and  dried, 
thitt  win  be  casoin  sufficiently  pure  for  ordinary  ptirposes.  It  may  be 
made  still  more  pure  by  dissolving  it  in  a  weak  solution  of  carbonate 
of  soda^  ullowinir  the  solution  to  stand  for  twelve  hours  in  a  shallow 
voself  fcparuting  any  cream  that  may  rise  to  the  mrfuce,  again 
throwing  down  the  nird  by  vinegar,  washing  it  frequently,  and  occa- 
sioniilly  boiling  It  with  pure  water.  By  repeating  the  process  three 
or  four  tiinL's  it  may  be  ubtuin^jd  almost  entirely  I'rec  from  the  fattv 
antl  salittc  tuatter?  of  the  milk."  f 

The  following  is  the  modus  ofwratidi  of  rennet  :  it  promotes  tbe 
convi>i*!>ion  of  the  sngnr  of  milk  iintn  luetic  acid,  which,  acting  Uke 
other  ucids,  occasions  the  precipitation  of  the  curd. 

It  has  been  objected  to  rennet  that  by  it  a  readily  fermentable 
and  decomposable  substance  i.s  introduced  into  the  cheese,  frequently 
causing  it  to  pa<i8  into  a  state  of  dccomtHisition. 

It  has  been  also  objected  to  rennet  that  tiic  stomachs  from  which  it 
U  prepared  arc  often  in  a  dirty  aud  more  or  less  decayed  condition, 
and  that  the  strength  of  the  rennet  made  is  very  uncertain. 

In  order  to  obviate  these  latter  ubjcctiotti^  the  preparation  of  a  solu- 
tion of  rennet,  of  btandard  and  ascertained  strength,  has  been  sug- 
gested; s-.ilt-,  saltpetre,  and  such  other  additions  being  made  to  it  as 
would  ensure  its  preservation.  Such  a  solution  would  appear  to  pos- 
sess several  advantages. 

The  profjoriions  of  caseinc  and  butter  tn  cheese  vary  with  the  kind 
of  milk  from  which  the  cheese  is  made ;  thus  »kim  milk  cheese  is  much 
poorer  in  butter  than  other  cheeses  made  from  vhole  milA. 

Cheshire  cheese  is  of  course  miide  from  whole  niilk  ;  Stilton  from 
cream  ;  while  cream  cheese  consists  of  the  fresh  cuni  uf  whole  milk. 

The  salting  of  cheese  may  be  effected  in  sevend  ways  ;  the  salt 
may  be  added  direct  to  the  fro.ih  curd,  and  this  is  the  metlioil  usually 
practised  in  Scotland  ;  or  the  newly  made  cheese  may  be  intmerse<l  in 
a  solution  of  brine;  or  the  surface  may  be  rubbed  with  dry  salt — 
theae  ntelhods  are  practised  in  Cheshire  ;  or,  lastly,  the  salt  may  l>e 
-Nlded  to  the  milk  previous  to  the  precipitation  of  the  curd.     Br  this 

ethod  the  curd  1:1  very  equally  salted,  but   the   quantity  of  salt 

*  jAhnitoii'i  LfCturn  mi  Airrleiilturil  Clirmiilry.  Xnd  edit.  p.  MV. 

t  Triuuictuiai  of  tbe  HighUDil  AsrictillufAl  Sucidjr.  Jiil|r,  IM7,  pi  SB, 


CHEESE,    AND   ITS   ADULTERATIONS. 

required  is  very  largCf  the  greater  part  of  it  being  retained  in  the 
whey. 

On    the    ADULTBRilTIOllS    OF    ClIEESB. 

We  referred  In  the  preceding  article  to  the  practice  of  colouring 
cheese  withiinmi//o, —  a  practice  which  we  have  shown  lo  be  useless,  to 
entail  seme  unnecessary  expense,  und,  in  consequence  of  tlic  a<iullera- 
tion  of  annatin  with  injurious  substances,  to  be  Httonded  in  some  cases 
with  rink  to  health. 

Oilier  colouring  matters  are,  however,  sometimes  employed  for  the 
same  purpose  as  annatto;  n^mvh%  maji^oiU  Jiitwers^  ifij/ry«,  and  the 
juice  of  red  tarroU ;  but  most  of  the  puler  coloured  and  all  the  high 
cotoured  chevses  derive  the  whole  of  tlieir  colour  from  anuatto.  Std- 
ton  and  Cheddar  cheest?  arc  never  coloured  in  any  way. 

It  may  l>e  objected  to  the  wlinle  of  theae  substances  that  their  em- 
plnyment  serves  no  useful  purpo.se. 

Various  articles  are  likewise  added  to  cheese  to  flavour  it,  and  to 
impitrt  u  preen  or  divemifie*!  coUnir, 

•*ln  some  dairie5,  the  leaves  of  sage,  parsley,  and  other  Iierbs,  are 
infutted  intn  eheesie  to  pive  it  a  green  colour.  In  other  datrie:*  part  of 
the  curd,  when  ready  lor  the  prei*8,  is  expfH'cd  in  a  sieve  to  the  air,  in 
onler  that  it  miiy  l>ecome  oxyjjenateil,  and  may  render  the  cheese, 
into  which  it  is  mixed  with  newly  preparefl  cunl,  of  a  diversiBed 
c«)lour,  ari<i  of  a  disposition  lo  run  speedily  into  putridity.  In  a  few 
dairie:i  rapid  putridity  is  induced  by  iin  intermixture  of  beaten  pota- 
toes. In  Koss-shire,  cheeses  are  for  teveral  days  buried  within  sea- 
mark, in  order  that  they  may  aoouire  a  blue  colour  and  a  peculiar 
itisie;  ttod  in  France,  a  considerauitt  quantity  of  cheese  receives  an 
olFensivc  smell,  resembling  that  of  a  pigatye,  from  the  intermixture 
of  fenugreek."* 

Cheese  ia  made  from  pntatoi^s  in  Thurin^ia  and  Saxony,  in  this 
manner: — "After  having  colletTted  a  quantity  of  potatne.H  of  good 
quality,  giving  ihc  preference  to  a  large  white  kind,  they  are  boiled  in 
a  cauldron,  and  after  becoming  cool,  tney  are  peeled  and  reduced  to 
a  pulp,  either  by  means  of  a  graler  or  mortar.  To  five  pounds  of  this 
pulp,  which  onght  to  be  as  cijual  as  pcisttible,  ia  adJed  one  [>ound  of  sour 
milk,  and  the  necessary  quantity  of  salt.  The  whole  m  kneaded 
together,  and  the  mixture  covered  up  and  allowed  to  lie  for  three  or 
four  days  according  to  the  season.  At  the  end  nf  this  tone  it  is 
kneaded  anew,  and  the  cheeses  are  plared  in  little  baskets,  when 
the  superfluous  moisture  escapes.  They  are  then  allowed  to 
dry  in  tlie  sbarle,  and  placed  in  layers  in  larpe  vessels,  where  they 
must  renniln  fur  fifteen  days.  The  oliier  these  cheeses  are,  the  more 
their  quality  improves.  Three  kinds  of  them  are  made.  The  first, 
which  is  the  most  commoni  is  made  according  to  the  proportions  just 

•  Rural  Cyelopadla,  pwt  tr.  p.  TTA.  art.  ChflcH. 


i 


«0  CHEESE,   AND   ITS   ADULTERATIOX6. 

•riven ;  the  second,  with  four  parts  of  potntocs  jui<l  iwo  pvU^T  ar-j 
dle<l  milk  ;  tlie  fKinl,  with  two  part*  or  potatoos  nml  four  pulitfi: 
or  ewe  milk.     Thesu  cheeses  hnve  this  a(lvanta<:e  nrrr  olber  Uaii^J 
that  they  do   not  engender  worms,  and  keep  fresh  for  a  nvoAtft 
years,  proviiled  ihey  are  placed  in  a  dry  situation  and  in 
vessels."  • 

Results  of  the  Examination  of  Samples, 

Tu-enhj  samplejt  of  cheese  were  subjcotod  to  analysts  with  ibe  W' 
lowin*:  n'sulls  ;  '— 

All  were  artiJicittVif  coloured^  in  most  coses  with  anwiUo. 

Ih  none  was  lead  present. 

Secernl  were  coloured,  on  the  outride  with  Veuetitut  rtd  oc  rtd£t 
pround  u])  into  a  paste  \r\t\i grease. 

In  none  of  the  clieeses  tras  any  guhsiauce^  either  organic  or  watfd 
prt'setit^  iidded  for  the  purpose  of  increasing  the  buuc  and  wei-bt  fl/ 
I  he  cheese. 

lliei'e  results  arc  so  far  satisfactory,  especially  as  respfKrU  lead. 

It  must  not  be  concluded,  hovrerer,  from  the  results  of  iheic  twetfv 
examinatiouN  that  lead  derived  from  the  adulterated  annaitornpbfM 
to  colour  the  chi>e£e  is  never  present  If  it  occur  only  in  one  hi^ 
out  of  u  hundred,  much  mischief  would  result  in  some  caaes. 

That  it  does  sometimes  occur  in  both  annatto  and  chcc9«  b  (rmvA 
by  the  evidence  of  Acrnm  and  Mitchell. 

Accum,  at  pa;r«  27fi^  of  hia  "  Treatise,"  afhrms  (hat  ieTioI  !»■ 
stances  had  come  under  Itis  knowlt^Ijie  in  which  dhHu-eJier  <i«a» 
had  been  contaminated  with  red  lead,  and  had  proiluced  M-riovx^^ 
sequences  on  being  taken  into  the  stonuich.  In  some  of  xhtxaa^ 
it  w.is  uscertained  tl^if  the  annatto  which  hiMl  been  u^ed  tu  <(3JMr 
the  cheese  was  il»etf  culoured  or  adulterated  with  both  Tcriai&oni*' 
red  lend.     See  p.  471. 

Mitchell  wriLeSf  "  I  have  only  met  with  cheese  that  contaJneJ 
on  one  occasion,  although  it  may  be  com|»arnlively  coninton." 

The  praciii'e  of  coating  cheese  with  Venetian  re>l  and  rwHIf  »• 
niore  objortionable  thitn  the  use  of  adulterated  unnattc^  sine 
this  contain  lead  in  any  cnsc,  and  fiince  some  |x;mons  arr  ibif 
enough  to  eat  the  rind,  the  t]uaulity  of  that  metal  comtuiaol  «puU' 
more  considerable. 

AIlluiu;rh  cheese  escapes  for  the  most  part  the  bands  of  ihr 
lenitor.  it  rlm's  n<>t   escape  the    attacks  of  fungi,  animilculrs 
inseotJi;  to  Uk-sc  it  is  particularly  prone,  id  consequenve  oTtti  lKni|< 
very  rich  in  nitrogen. 

Th"  prten  colour  of  mouldy  cheese  is  dnc  to  the  dcvclopmcBt  a < 
small  production  or  fuiigu;>,  the  common  Penicilium  gtantum* 

«  Quitrtrr^  Journal  of  Airlculiorr  toL  Ix.  p.  SIO.  i  Book  of  tbe  Fwa,  |art  &  f^ ' 


CHEESE,   AND   ITS  ADrLTERATIONS. 


4at 


motiMiness  may  be  produced  in  coraparutirely  nev  cheese  bjr 
(ion. 

is  sometimes  eflet^ted  by  inserting  inW  (be  new  cbei-se  rolls  of 
tlieese,  extracted  by  the  scm^p,  inlo  holes   jireviou>ly  made  by 
le  scniip. 

ituiil   that  liir*re   pin«  are  often  thruHt  into  checso.*,   and  al- 
to rt'inain  in  tiiem  for  u  comtidernble  lime  in  onler  to   pro- 
lie  miiuldinesis.     This  is  ii  verv  objeetionnble  proteedin^',  as  in 
the  colour  h  due  |»artlr  to  the  formation  of  a  9iilt  of  copper, 
'^nrtly  in  •umie  cases  lo   the  development  of  the  Ciin^ufj.  which 
place  in  consequence  of  llic  ndiniasiun  of  uir  into  the  interior  fif 
fie  eheesi". 

At  a  still  further  period  of  deeay  chrew  is  attacked  by  the  well 
Icnown  ch«'(»»e  mile  oracarufi,  Acarta  sin*  nf  Linnseu?,  iind  which  is  »o 
minll  ihnt  it  is  scarcely  perceptible  without  the  aid  (if  ihe  niicro^ope; 
thf  dry  tiuil  funetierj/  parts  of  cheege  ronsint  almont  entirply  of  ihexe 
ftcuri  and  their  oca  in  different  tttufjes  of  ^owth.    Fig.  1  ^0. 

'*  We  nftni  wonder  how  the  ehee»tt  uilte  \t  at  hand  to  attack  a 
ohee*e  wherever  depnsitetl ;  hut  «hen  we  Icarn  frnni  I,oc'wenhoe'c  that 
one  livotl  eleven  week?  giinuiifd  im  ils  biwk  lo  tin'  fmint  of  a  needle 
irithoui  fooil,  our  wondtT  i"  dlniini.«heil."  remark  Klil»y  :ind  Spence. 
Botli  tiiese  chi-ene  ni:i^<;nl!*  :ihd  miti'fl,  when  nimn-'roii«,  deslrnv  cheese 
rapidly,  by  crumbtini;  it  into  ftniult  pIcv'S  und  by  emitting  a  liquid 
suh.srunt-o.  which  cTiuses  the  decayed  parts  to  sprcu-i  speedily.  They 
may  ewily  be  killed,  however,  by  ex[K)-ure  to  dtroog  bent,  or  by 
plungin;;  the  cheese  in  'ouie  litpiiil,  huch  a*  whii'key,  cuprihle  of 
de^ftroving  the  hirrae  without  communicating  any  disagreeable  fla- 
vour.* 

He.iide3  the  casualties  from  fennentntinn,  chroe.  when  yet  qtiile 
fretih,  i»  Kubjevt  to  the  attack  of  the  chceseily  {Pwphila  coAri).  'Ilic 
fly  is  reailr  to  deposit  its  r^i'9  in  the  dt-epest  cr^ck  it  ctin  tiiid.  by 
ni<*ans  vt'  un  cxleiisile  ubdominal  tube.  The  f^pecilic  distinguishing 
chiirot-ters  of  this  insect,  as  dniwn  up  l>y  Mr.  Duncan,  are  a;!  fnlhiw  : 
—  "About  tw{»  lines  in  Icng^lh,  the  whole  body  nt'  a  "reenitih-blai'k 
cohiur,  smooth  and  fhininz;  front  itf  the  head  reddi.-«h<ycllow,  niiler 
yellow  on  the  untler  side.  Thij»lis  oihre-yeUow  at  the  base  and  n]*x  ; 
tibia  dei-p  ochre,  the  (irt^i  and  la.«t  pair  black  at  ihe  i)[>ex :  anterior 
tar!!t  bla'^k,  the  others  ocbrey.  with  the  two  Ia>it  joints  and  the  clawa 
black;  wings  clear  and  iri'lescent,  t^bghlly  tinged  with  rust  c<»lour  nl 
the  b:i5e,  halteres  (n'hrcy."t 

The  cheese  raacgots  produced  frnm  this  fly  ore  nt  larpe  as  the  flv, 
and  roihtuonly  railed  jiirw/vr*.  "When  this  mapaot  prcpures  to  Icaji, 
it  fir-'t  erects  itself  on  its  anus,  and  then  bemling  tt.'<t:lf  into  a  circle, 


•  Book  of  n»»  TmrTa,  pun  M.  p.  »« 

t  Klrb}  anit  fit«»f^**  lotroduct|<tt>  to  Bntomglufjr,  vot.  II.  p.  Hi, 
1    1 


4M 


CHEESE,   AND   ITS  ADULTERATIOXSU 


frivrn ;  the  rarond,  with  four  parts  of  potatoes  and  two  pmrU  af  «r- 
illwl  milk  :  the  tliinl,  with  two  pnrla  nrpoialoes  and  four  parts  of  cov 
or  I'wo  milk.     Thc!>o  clieeses  Imvo  thin  iidvmnta^e  over  ocker 
llmi  thi'v  iirt  mn  onj^umior  worms  nml  koep  frosh    for  a  m 
vctirs  pn>viilcd  thuv  are  placed  in  a  drj  situation  and  in  w< 


R^Mnlfi  of  the  Kxaminaiion  nf  Sampler* 

Tn-fnty  utrnplfn  of  cbeuse  were  subjtiottid  to  anaj^'sis  with  the 
Kmins  rt'Hiill* :  — 

AU  were  artificiaUy  calaunHi,  in  most  cases  with  annatio. 

/■  iHiii*  WM  i0tid  |»r«sent 

Sevtmt  tfVM  eiAmrtd^  on  the  outside  with  TViiWiau  red  or  rW^ 
Itrtuind  up  initt  a  |>ii«tc  with  greane. 

in  utme  ot  thr  rhcoHcs  ifviii  any  fmbKtanee^  either  orvanic  or  miW^. 
prttrnt,  iidiUnl  for  ibo  purpose  of  increasing  the  bulk  and  weight  oi 
(h*»  rht'o»o. 

'riK'Bi'  ti'sults  Bto  so  far  enlisfactonr,  especially  as  respects  leatt 

li  ntit^it  ititt  lio  cttnt-liidiM],  however,  from  the  results  of  these  lw?ntt 
i>xiuiMii»liitnA,  that  loud  derived  from  ihe  ndulteraletl  annacto  t^inplorril 
toooloiir  thn  rlnvsii  is  never  present.  If  it  occur  only  in  one  sample 
out  of  11  IninilriMl,  mueh  misfhief  would  rcpiilt  in  some  cases. 

Thnt  it  <lm»s  .<omi*timeK  occur  in  botli  nnnatto  and  checfie  is  prored 
by  lb>*  eviilcnei^  of  A<M-um  and  Mitt-liel]. 

At'i'um,  Ht  piij;u  27r>.  ("f  bis  "  Treatise/*  affirms  tliat  several  I'n- 
Klrtni'OH  bml  oomu  iiiuler  bis  know]L'i|>;e  in  which  Gloucester  cheo< 
buit  been  cuhliiminnlcil  witli  rcil  Icml,  ami  hail  pro»luce<l  sprious  coo- 
•ftpiohci'ii  im  Ik'IU^  l«kon  irili*  ibc  «ii»i[iiirb.  In  ^ume  of  iliesc  esse* 
It  wii!«  rt(»ccrt»incil  lli/ir  the  nnuiUto  ivliicb  luul  been  uned  u>  colour 
tlio  cbocni"  w»a  itsi'lf  coloured  or  uduUeruted  with  both  vcrmUwa  »"" 
I'ihI  liMtl.     Sec  p.  471.  .    I 

Mitchell  writeis  "  I  buve  only  met  with  cheese  that  contained  r«u 
on  one  otvimion,  itllbouffh  it  may  be  cmjiaratively  connnon-      _ 

Tb<!  pnu'ti.^o  of  coulinp  cbecse  with  Venetian  red  ond  rod<Ile  is  t  si^ 
uioiv  olyectioniiblc  tluui  the  use  of  adulterated  imntilln,  m 
thinonntain  lend  in  any  cft»e.  and  since  some  P*^''""*  ,*f^* , 
enouith  lo  oat  the  rind,  the  quantity  of  that  wet' 
U(oro  eoiiKitleralile. 

Althmiuli  cbccdf  escapes  for  the  most  part  uif- 
tiM'nlor.   il   'locii  nut   escape   llie    attacks  of 
ihSLHiti;  It*  these  it  is  puriioularly  prone,  in  oOl 
vorv  rich  in  nitrogen- 

'thi*  «i'»ou  eobmc  of  montdy  cheese  is  dij 
swrII  piodueiion  or  funpus,  the  common  P0^ 

•  (^ULrtsrli  JowrnsI  of  Afrlculmw.  toI.  ix.  p.  3io.  j 


414  COLOUBED   SL'GAR  CONFECTIONEBT. 

che«.*9e  is  coatetl  with  Yenctiim  red,  this  ahould  be  aeparulelj  examini 
tvr  Ictttl. 

The  general  method  of  prooec»din(i  ia  as  I'nllows: — About  500  grains 
nf  the  cheese  aboiiM  be  inrinoraleci,  and  the  uah  tested  for  lead  and 
iron  as  directed  under  the  head  of  Annatio,  &c. 

Iiiipuri  duty,  t2jf.  ad.  per  owl.  ^  fVoui  Briii&h  possessions*  It.  6</.  per 
cwt. 

[niporU  taken  fur  home  coiisiirniJtion  in  1«54,  390,220  cwl». ;  in 
\H55,  38t,'2tf>J  cwts. ;  in  nine  months  of  UoG,  275,014  cwt«. 


COLOURED  SUGAR  CONFECTIONERY. 

The  aJulteration  of  ai'ticlcB  of  sugar  eonfcetionery  is  a  Bubject  of  (he 
ver^  greiittist  importaneu  in  a  tiaiiitar^r  point  of  view :  that  it  must  be 
»o  IB  evident  when  we  i.'uii:iiJt;i'  the  potsoiiotis  cliaractvr  of  tuanr  of 
the  liubsianccs  used,  and  also  the  hir-^e  eousuiupCion  of  the»«  articles 
especially  by  cliildrcn  and  youn^  persons. 

That  thfsc  nrtioles  are  subject  to  vros.-t  ami  injurintis  ailidlorutioa 
haa  long  been  knonn,  and  tlie  siibjret  in  purtieulurly  referri'il  tii  even  by 
Aceum  and  other  early  writers  on  udultenitions.  Dr.  0'Shau<*:hno»sy, 
in  the  preface  to  n  pa(>er  on  cuhiured  sugar  confectionery,  published 
in  the  '•  Lancet/'  in  1»3.*),  mukea  tlie»e  remarks  :  — 

*'  In  tbe  lollowing  observuiions  it  is  my  principal  aim  to  lay  before 
the  public  and  the  medical  profession  a  culm,  d)t>pa5Monatc  statement 
of  the  existence  of  various  poisons  (ifatnboge,  lead,  copper,  niert-ury, 
and  chrouiuti'  of  leaii)  in  :*everal  articles  of  confectionery,  tbe  prepH* 
ration  of  which,  from  their  pf'culinr  attractions  to  the  younger 
branches  of  the  community,  has  grown  into  a  sepurate  and  niosi  ex- 
tensive branch  of  manufacture.  I  am  fully  aware  of  the  ha2urdous 
task  that  individual  undertakes  who  veutures  in  this  countiy  lo  sig- 
naliso  such  abuses." 


U»    TU£    Al>Ul.TEBAT10N6    OF    SuGAK    CoKFfiCTlOKKBT. 

Of  all  the  chief  varieties  of  articles  of  sugar  confectioner/,  wo 
subjected  no  less  than  101  samples  to  both  microscopical  and  chemical 
examination. 

From  an  examination  of  this  extensive  series  of  analyses  of  co- 
loured sugar  confectionery,  it  ap|>ears  — 


COLOURED   SUGAR   CONFECTIONERY.  465 

That  the  principftl  colours  employe*!  are  yellows,  reds,  including 
pink  and  scarlet,  browna,  purples,  blues,  and  grceiu. 

Of  ihe  yellows  — 
That  Seven  were  coloured  with  lemom  chrome,  or  the  pale  variety 

of  CHROMATE    OV    LEAD. 

Thrtl  I'^ire  wi-rc  enloupwl  with  oRAHGit  ciiROMR,  or  the  deep  variety 

of  CHROMATH   OF    LEAD. 

That  Forty-teven  were  coloured  with  the  bright  or  canary -coloured 
variety  of  chhomatr  or  lkad. 

Thil  Eleven  of  the  «:uiiple*(  were  t-olntimd  with  nAMnoOK. 

While  the  colour  of  the  tiiajority  of  the  above  samples  wus  confined 
to  the  surface,  in  many  eases  it  was  diffused  equally  throughout  the 
whole  maaa  of  the  sugar  used. 

Ofthereda— 

That  Sitty'one  were  coloured  with  organic  pink  colouring  matters, 

c(iusiittin>r  ill  most,  cuses  of  Coccus  C'ttcti,  or  cochineal. 
That  in  Ticelce  of  the  samples  thu  colouring  matter  was  red  lead, 

BED   OXWh   ur   LKAD,    Or   MIMUM. 

That  in  Six  cases  the  c(4ouring  ingredient  consisted  of  vermilion, 
cimharar  or  nisULPiiCRcr  or  mf.rcury. 

Of  the  browns  — 

Thfli  Eight  were  coloured  with  brown  fermginoxut  earths^  either 
Vandyke  brown^  Vmber^  or  Sienna. 

or  the  purples  — 

That  two  samples  were  coloured  with  a  mixture  of  Antwerp  bluet 
which  cnnsisis  principally  of  Prtissiaii  blue,  and  an  organic  red 
pigment,  most  probably  cochineal. 

Of  the  blues  — 

Thut  One  was  cf>Iouret|  with  indigo. 

That  Eteoen  were  coloured  with  PruMtian  hlue^  or  ferrocyaiude  of 

iron. 
That  Eterrn  were  coloured  with  Antwerp  blue,  which  is  a  modi6ca- 

tinn  of  Pnutsian  blue 
Thftt  in  Fifteen  ^uiiples  the  colouring  matter  consisted  of  Grrvan 

oa  ARTIFICIAL  ULTRAMARINE,  which  is  a  doublc  silicaie  of  alu- 
^  mina  uid  soda  with  aulphuret  of  sodium. 

r  of  the  gret^ns  — 

a  Thtit  Five  Mmpie4  were  coloure*!  with  the  pale  variety  of  Brdsis' 

^^L  WICK  ORaix. 

^^B  Thar  Four  were  cotoiire<l  with  middle  BacrnswicK  orrrh. 

^^B  That  One  was  coloured  with  the  deep  variety  of  Bruxswick  grebii. 

^^1  1  1 

■ : J 


48ft  COLOURED   SUGAR   CONFECTlONEBr. 

These  greens  consist  nf  a  n)ixturt\  in  diflferent  proportions,  of  the 
OUOMATSS  or  LEAD  and  Prmuan  hlue. 

That  one  sample  wu  coloured  with  vbrditrr  or  CjLBbohatb  or 

COPPKl. 

That  Nine  were  coloured  with  Schbelb's  gbebn,  bmbbald  gbbbk, 

or  ABSEMTE    OF    COri'KB. 

That  in  Fuur  of  the  samples,  the  oulourfl  used  were  painted  on  with 
MujTK  i^Ai>  or  cABBOMAT£  OP  LKAU.  Tliis  WAS  thc  CBse  In  all 
tlie  cake  oruaments. 

It  further  appears  from  the  above  analyiieb  — 

Tbat  Thirteen  nf  the  samples  were  ailulterated  with  hydrtUed  svl- 

phtite  of  timet  ^be  (piantity  varying  from  +"3  to  43  66  per  cont. 
That  TwetUtf-one  of  the  samples  weru  adulterated  with  did'erent 

kinds  of  Fimir^  in  quantities  varytnfr  from  I'G6  to2o^6  per  cent. 

In  .Seventeen  samples  the  farina  ronsisted  of  wheat  Jlour ;  in  Three, 

of  potato  Jhiur,  and  in  One,  of  Eajit  India  arrowroot. 

The  above  colours  were  variously  combined  in  liitlerenl  cases;  aa 
many  as  three,  four,  five,  six,  und  even  seven  eohmrs,  occurring  in  Uie 
Mme  parcel  of  confectionery,  including  three  and  even  four  poisons. 

The  following  specimens  are  of  this  kind  :  — 

SHgar  Seedg. 

The  colours  of  one  sample  of  sugar  seeds  were  crimson^  pitle  pinJt^ 
iif^ht  blue^  dull  greenish-blue^  ^g^tt  groM-preen,  orttnge-t/ellow^  and 
UmoH-yell*tw^  intermixed  with  while  globules.  The  colouring  ingre- 
dients employed  were  :  for  the  crimson  and  pink,  the  usual  fu)n-metaUic 
red :  for  the  blue,  Antwerp  blue ;  for  tlie  dull  ;;reeuish-bhie,  vRRuiTk-R, 
containing  lead;  for  the  grnss-grcen,  vw.v.  Hki'nswiok  ckkcx;  and 
for  the  orange  and  bright  yellows,  the  Dninge  and  yullow  curouatks 
OP  LRAD,  in  large  ijunniity.  A.th^  light  reddish-brown,  rO€  percent.; 
matter  insoluble  in  wnter,  chiefly  wheat Jiour^  9"00  per  wnt. 

Thus  no  le>s  than  three  active  poisons  conluining  leai>  and  coPFEft 
vere  presrut  in  this  r^ample  in  considerable  amount. 

T)og  ami  Hare. 

The  nr>!<e  and  ears  of  the  dog,  and  the  tongue  of  the  hnre,  are  co- 
loured bright  red  with  vkrmiuon.  The  body  of  the  dcg  is  spittted 
with  large  patches  of  gambook  and  burnt  nmber^  ns  also  was  the  figure 
of  the  hare  whifh  lay  at  its  feet;  while  the  green  pigmetU  on  the  base,  of 
which  there  wa*  a  very  large  f|uantlly.  contained  chbomatb  or  LBAO, 
and  consisted  of  the  pale  variety  of  Bbukswicr  OBBETf.  Aah^  dBrk 
reddish-brown,  2*0  per  cent. 


COLOLflED   SUGAR  CONFECTtONEBr. 


487 


P 


Mixed  Sugar  OmamenlM. 
The  confectionery  in  tliid  parcel  i«  made  up  ioto  a  variety  of  formr* 
and  devices  as  hatii,  ju;;fs  ba.-«kt'U,  and  dishes  of  fruit  and  vegetable:!. 
One  of  the  hat5  is  colourLMl  vellnw  vriih  chromatb  or  lead,  and  htut 
a  green  hatlmnd  around  it  coloured  with  arsbnite  or  copper;  a 
second  hiit  is  white,  with  a  blue  hathaml.  the  pigment  being  Prussian 
line.  The  baskets  are  colouri;d yellow  with  chromate  of  lead;  into 
the  colouring  oftiie  |iears  and  peaches  tlie  usual  mm-meiaUic  red  pig' 
ment,  chbomaxe  of  keao,  and  miiidlb  Hku.nswick.  grbe:*,  enter 
largely;  while  the  carrots  represented  in  a  iliah  are  coloured  through- 
out with  KEU  OXIDE  or  LBAD,  and  the  tops  with  the  same  green.  This 
ia  one  of  the  worst  of  all  the  samples  of  coloureii  8u;2ftr  ronfeotiom-ry 
:4ubiuitlcd  to  analysis,  as  it  contains  no  less  than  /tjur  tUadly  fMigoru. 

Twelfth  Cake  OmamenU. 

7^e  ornaments  in  this  parcel  consist  of  u  sliip  in  full  sail,  a  duck,  a 
fox,  and  a  bunch  of  flowers,  the  principal  colnurs  beiti^  green,  yellow, 
red.  and  brown  ;  the  chief  pigutents  employed  iirc  ciibomate  or  lead, 

RED  OXIDE  or  LEAD  Or  BED  LEAD,  VBBMILION,  ll>nru2,  Aud  ABSENITE  OP 

COPPER  :  these  being  present  in  poisonous  quantity. 

It  will  be  observed  that  the  list  of  colouring  matters  above  enume- 
rated includes  some  substances  of  an  injurioiLH  character,  and  many 
which  are  amongst  the  uitrnt  virulent  uud  deadly  of  the  uiineml  |>oi- 
sons.  Of  those  which  may  l>e  considered  w*  more  or  less  in  jurioui, 
are  Ftrrocyanide  of  iron  or  Prussian  blufy  Aidwerp  bltte^  QkHWiGK, 
and  Oermau  or  artijicial  ultramarine,  Araong»t  those  which  are 
deadly  and  poi:«onoufl,  are — the  thr^c  ciinoMB  teli^ws  or  ciiROMATfta 
or  lead;  bei>  lead  or  red  oxids  or  lead;  wuirs  lead  or  caB' 
BORATE  or  lead;  vebmiuoh  or  disdlphubet  or  mbbcdbt;  the 
three   Brunswick  gbkbks;    vebditeb  or  cardonate  or  loppke; 

and    EMERALD    GREKN,  ScIIKKLb's    UREE?(,    ur    ARSEMITE    OP    COPPER. 

Other  articles  whicb  have  l>een  stilted  to  l>e  ucM^l  in  the  colouring 
of  su;rar  confectionery,  and  most  of  which  we  have  ourselves  detected, 
are  ciai/y  rhdk^  Naples  ycUow  ftr  gulphuret  of  artewcuyH^  massicot  or 
oxide  of  Itatl^  aeetaie  and  oxichiarifle  of  copper. 

It  may  be  alleged  by  S4)me  that  these  siilmtances  are  employed  in 
quantities  ttio  inconsiderable  to  prove  injurious  ;  but  this  is  certainly 
not  so,  fur  the  quantity  u&ed,  as  is  uiiiply  iiidicuteil  in  many  easex  by 
the  eye  alone,  is  often  very  lurge,  and  aulficieiit,  un  is  proved  by  num- 
berless roeordei]  and  eontinuulty  occurring  instances,  to  ocL*a9iuu 
disi^aMe,  and  even  <leath.  It  should  be  remembered,  too,  th«t  th«  pre- 
parations of  lead,  nierciirv,  copf^H-r,  and  arsenic,  are  what  are  termed 
cumulative — that  is,  th*>y  are  liiible  to  accumulate  in  the  system  little 
by  little,  until  at  length  the  full  cHVcts  of  the  poisons  beoouie  inani* 

1 1  ■< 


«86 


COLOURED   SUCAR    CONFFXTIONKHT, 


f'ested.  Injurious  consequences  liave  been  known  to  result  fVora 
merely  rooisteniny;  wafers  with  the  toii'jue;  now  the  inprecJtent*  us^t] 
Ibrvfuouring  theao  include  rnnny  that  are  eniploved  in  sngiir  confec- 
tionery ;  hiiw  iiiurh  more  iiijiiriouB  then  must  the  eonsumption  of 
BUjrar  thus  paintnd  |»ro%-e,  wben  these  pigmeiita  are  actually  rcceirnl 
into  the  stomach! 

That  deadly  priiiiHtns,  like  tlte  above,  fiboiild  be  daily  u«c(]  for  the 
mere  sake  of  imparting  colour  (n  articles  of  such  ^nernl  cnn^uoiptimi 
as  ai^ar  conl'eftionery — articles  consumcil  chielly  by  chiMrrn,  whn 
from  their  delicnte  or'.Mnisntiori  are  much  more  5ascc]»riMe  than 
adults — is  l>«)th  surpnyin;;  and  lumentablti.  It  is  »ur|irUinj;,  on  the 
one  hand,  thiif  the  iiianufmtururs  of  thi'se  artick'S  shoiihl  be  so  reck- 
less as  to  ein[>loy  IIilmij  ;  and,  on  tlie  other,  that  tbe  uuthoritiea  sbould 
tolerate  their  u^e. 

Dr.  ThonisfMi  furnished  the  Pnrlianicntflrv  ComtnUlee  on  Adul- 
teration with  the  following  particulars  regarding;  the  udnlieratjou  of 
BU^'ar  confectinnery  with  (trrrn  allnt  L\r  sulphate  of  lime:  — 

**I  procure)]  Iromair^^ut  munuCactory  of  those  cuhstane^a  specimeiM 
at  'UffLTcut  prices.  There  were  ulxmt  Ion  different  huniple^.  uf  which 
I  litivt:  li)C  delailii  here;  I  wdl  Bri^t  speak  of  what  are  culled  niint^s  at 
Id.  a  p<niiid  ;  they  contained  3*0.'J  |K;r  cent,  of  a  Ruh»tanre  which  i« 
sold  under  the  name  of  terra  allin.  This  terra  allia  1  fnond  lo  be 
piaster  of  Paris.  The  ettM-nnd  sample,  nt  H45.  per  cwt.,  oonliiiucd  iO-M 
per  eenf.  of  terra  alba.  The  third  was  carroways,  at  .V/.  a  pf>iind,  imd 
contained  27*8"2  of  terra  alha.  The  fourth,  another  p[K»einien  of  car- 
roways,  at  ftrf.  a  pound,  containetl  19'2*2  per  cent,  of  terra  alba.  The 
dixth,  almonds  at  lOr/.  a  pound,  contained  "90  per  cent,  id'  tt-rrn  a.tba. 
The  seventh,  another  siimple,  :it  ftrf.  a  poutrd,  containetl  7"02  jier  rent, 
of  terra  alba.  The  eighth  sample,  at  Hd-,  coiitiiitifd  'i'2  76  of  terra 
allm.  U:i»pt»errieA,  at  \)d.  a  pound,  contuined  7'76  of  terra  alba.  Straw- 
berries, ai  \kl.  a  jKkund,  contained  8*:*8  per  cent,  of  lerru  alba. 

Mr.  Guy  states,  in  the  course  of  his  evidence  before  the  Committee 
on  Adulteration:  — 

"  I  believe  many  articles  of  confectionery  are  adulterated  ;  1  thmk 
carraway  comfits  are  very  extensively  aduiteratett,  and  aUo  many  nf 
the  peppt^rniint  lozengus.  I  believe  the  ha-iis  of  both  (hi'se  and  cori- 
ander and  almond  nnntits  are  flour  ;  after  the  seeils  are  put  into  the 
pan,  a  tittle  syrup  is  thrown  over  them,  ami  that  is  dusted  over  with 
eitlier  (lour  or  whiting,  or  plaster  of  Paris ;  a  pretty  stron«  coat  is  put 
.upon  them  in  this  way^  and  then  tliey  are  linished  with  a  stronger  and 
belter  syrup." 

White  lend  used  in  sugar  cake  ornaments  is  itself  often  estenstrely 
adidtcratcd  with  sulphate  of  barytes. 

Further,  immy  articles  of  suirnr  confectionery  are  flavoured  with 
•*  essences,"  which  are  often  of  iin  injurious  and  even  dangerous  cha- 
rauter^  souieof  theiu  containing  prussic  acid  and  fusil  oil. 


COLOUIIED   SUGAR  CONFECTIONERY, 


4S9 


In  reference  (o  the  use  of  these  csftenci*!*,  much  information  will  be 
fniind  in  the  evidence  given  before  ibc  Parliamentary  Cominiltee  on 
Ailulterution. 

Amongst  the  essences  ustKl  lo  flnvour  sweet  confectionery,  are  some 
prepi»rc»i  from  oil  of  grain  or  fusil  oil.  Pineapple  drupB  are  said  to 
otre  tbeir  llavuur  to  an  essence  prepared  front  that  deleterious 
substance. 

Other  cnrnpouniln  prepared  from  fusil  oil  are  made  to  iniitate  the 
flavour  of  Jiirgnnelle  pears  and  ribatone  pippins.  "  I  have  heard," 
states  Professor  Taylor,  "  that  some  oF  the  Jar^ionelle  pear  drops  and 
ibe  ribstonc  pippin  drops  have  produced  drowsiness  and  stupor  in 
ehddrQii.  It  is  iin  inipn->ition  on  the  public  to  sell  in  this  vray  a  ehe- 
luicutly  tlavourod  sub>tance  under  another  name." 

A  very  fragrant  fruity  espenee  may  be  proiUiced  from  rotten  cheese, 
by  treatment  with  ;>ulphuric  acid  and  bichromate  nf  potash. 

Another  essence  extensively  used  for  flavo;iring  sweetiiKMits  and 
confectionery  is  rntifia,  essential  oil  of  alinnndt<,  or  essence  of  pench 
kernels.  It  is  obtnined  by  distilHtig  bitter  almond  cuke  with  water, 
nud  it  contains  from  six  to  twelve  per  cent,  of  prussic  acid,  but  is 
most  variable  in  its  strength.  As  small  a  quantity  as  twenty  drops 
lias  l>een  known  to  oecHsicm  death. 

There  is  another  compound  of  prus^io  acid,  called  "  almond  llavour  :'' 
it  coDtJiins  about  one  drachm  of  the  essential  oil  lo  seven  drachm^  of 
apiril,  but  itd  strength  varies  very  much.  Many  fatal  vases  have  re- 
eulted  from  the  use  ot'  this  flavouring  suVjstance. 

The  prussic  acid  in  ihpjw  preparations  is  not  essential  to  their 
flavour,  iind  might  with  a  little  care  be  readily  separated,  zo  that,  as 
Pi'ofessor  Taylor  remarks  in  hts  evidence  before  the  Parliamentary 
Committee  on  Adulieriuion,  "there  is  no  excuse  for  selling  pruasic 
aciti  in  the*e  compounds  but  Uuincss  and  ignorance." 

Lastly,  the  paprrs  in  which  the  ornaments  are  wrapped  are  usually 
Colour(*il  with  vurioMx  [»iM!tonou9  pigmenti, — a  practice  which  ought  to 
be  fi>rbidden,  since  chlhlrcn  are  very  apt  to  put  these  papers  in  their 
m  jutlii  ^i\*\  .inck  them. 

In  some  other  eounirie?,  us  France,  Belgium,  and  Switzerland,  ma- 
nufacturers of  sugar  confectionery  have  hmg  l>cen  furhiildcn  to  use 
injurious  colouring  ingredients  under  severe  penalties.  Sellers  of  the^e 
articles  in  Paris  arc  also  obliged  to  put  their  nanie^  on  every  parcel  of 
confectionery  they  sidl;  they  are  held  responsible  for  all  aceiilents 
which  may  arise  tVom  their  consumption,  and  they  are  even  forbidden 
to  wrap  the  articles  in  coloured  paper:}. 

Following  the  example  of  the  Council  of  Health  of  Paris,  we  now 
furnish  two  lists,  one  of  colours  the  use  of  which  may  be  permitted, 
ami  the  other,  of  those  ctdours  the  employment  of  which  should  be 
strictly  pruhibitefl,  on  the  ground  that  they  are  all  more  or  les:f  dan- 
gerous to  the  public  health,  and  mo*tt  of  them  absolutely  poisonous :  — 


490 


COLOURED  SnOAB  OOMrEOTXOlTBAT. 


Lift  (/  CoU>ur$,  Ou  Use  o/wki^ 
mag  bepermitUd, 

Ybillows. 

HafTron. 

Turmoric. 

French  berries. 

Lake  of  ditto,  or  yellov  lake. 

Persian  berries. 

Lake  of  ditto. 

Quercitron  bark. 

Lake  of  ditto, 

Fiutic  wood. 

Lake  of  ditto. 


Rbds. 

Cochineal. 
Lakes  of  ditto, 
Carmine  and 
Brazil  wood. 
Lakes  of  ditto. 
Fink  madder  luke. 


Purples. 
Madder  purple. 
Logwood  and  indigo. 
An^  of  the  lakc^  with  indigo  or 
litmus. 


Txixovt. 
Gamboge. 
The   t£ree   dntme   ydUnrt,  or 

chzomatee  of  lead. 
Maaatoot,  or  protoxide  of  lend, 
Tellow  orfHmeat,  or  ■alplmret  of 

araenicum. 
King's  yellow,  or    avlpliiiret   of 

arsemoaoa,  with  lioM  ud  sol- 

phur. 
Iodide  of  lead. 
Sulphuret  of  aatimoKj,  or  Keptoa 

yellow. 
Yellow  ochre. 

Rbds. 

Red  lead,  minium,  or  red  oxide 
of  lead. 

Vermilion,  or  bisulphuret  of  mer- 
cury. 

Red  orpiment,  realgar,  or  biaol- 
phuret  of  arsenic. 

Iodide  of  mercury. 

Ked  ferruginous  earths,  as  Vene- 
tian red,  &c. 


Browhs. 


Vandyke  brown. 
Umber. 


All 


PUBPLBS. 

purples    resulting  from   the 


mi  X  ture  of  any  of  the  prohibited 
reds  or  blues. 

Blubs. 
Prussian  blue,  or  ferrocyanide  of 


iron. 


Iniligo. 

Antwerp  blue,  a 
Prussian  blue. 
Cobalt. 


preparation  of 


COLOURED  SUGAR  CONFECTIONERY. 


491 


tut  of  Coiimr»,  the  Uaf.  ofychick  '  LUt  of  OUmtrs,  the  Vie  ofwhtch 
may  bt  permitted.  thould  he  prohibited. 


bi.UK& 


Indigo. 
Litmus 


Gbksxs. 

Sip  green  (juice  of  Rhumnus  ca- 

tbnrticuft). 
Yellow  Iakt.%  or    French  berriea 

and  indigo. 
Any  of  the  vegetfthle  jellows,  or 

lakes,    with    indigo,    including 

Fenian  berries  and  indigo. 

Ob§.  —  Of  the  above  colours 
oaai  Map  ^tvcn,  i»  certAinly  Ijiibli: 
to  injurious  adultoratioo.  mid  it  iit 
•tated  tbut  Idmus  is  so  likewise. 


Blvcs  —  continued. 

Sinutt,  u  ^liuu  of  cobnit. 

Blue  verditer,  or  scMiuicarbonate 
of  copper. 

Uliraumrine,  o  double  silicate  of 
aiuminn  and  soda,  with  aulphu- 
|-«1  of  sodium. 

German  or  artificial  ultramarine, 
which  resembles  in  its  compo- 
sition natural  ultramarine- 

Gbeehs. 
The  three  false  Brunswick  greens, 

being    mixtures   of    the   chro- 

luatea  of  lead  and  indigo. 
Mineral  green,  gi-een  verditer,  or 

subcarbonatc  of  topper. 
Verdigris,  or  diftcclate  of  copper. 
Kmcrald    green,    or    arseuite    of 

copper. 
The  true  Brunswick  greens,  or 

oxychloitdtis  of  cornier. 
FaUe  ver'litcr,  or  subsulpliate  of 

copper  and  chalk. 

TuK  VARioos  Broncb  Fowdees. 

Gold,  silver,  and  cooper  bronzes ; 
these  consist  of  allovs,  in  differ- 
ent proportions,  of  cupfier  and 
sine. 

White  leadf  or  carbonate  of  lead. 

Bt  an  examinutitm  of  these  lists,  it  will  be  perceived  that  nearly 
all  the  substanre.i  now  L'lnploycd  by  rliu  manuftctnrers  of  coloured 
su^ar  ciinloctinnery  belong  to  the  second  or  prohibited  list.  Kvcn  the 
first  list  conLains  the  narn>M  of  two  or  three  colours,  the  use  of  which 
is  not  wh(»lly  free  fnjoi  objection,  —  av  indijjo,  liimus,  and  i^ap  green  ; 
the  two  hitter  in  ctMise^juence  *y^  their  Itubilily  to  adulteration. 
Genuine  litmus,  being  a  vegetable  ciduur,  is  of  uouise  harmless  ;  but 
ila  use  i<4  rendered  ubjcetioimbtu  from  its  being  frequently  adulter- 
ated, according  to  M.  Andral,  with  common  arsenic  and  peroxide  of 
mercury. 

From  ultranuirine,  in  contact  with  an  acid,  sulphuretted  hydrogea 


49S 


COLOURED   SUGAR   CONFECTIONERY. 


is  freely  liberntcd  ;  anrl  this  liberation  no  doubt  takes  pUre  r 

in  tlie  atoinach   wln-n  any  (.onfootionery  colouretl  hj  ihis   piguiciit  it 

partaken  ol";  lient:e  tin?  use  of  this  pigment  is  objectionable. 

For  oursL'ives,  we  alto;»etlier  objut-t  to  the  pi-actice  of  colourin; 
tu'ticles  of  consumption  of  all  kma»  and  descriptions:  while  it  uivrel 
fl^ratities  the  scn*e  of  sight,  it  serves  to  conceul  other  ailulrerations, 
anil  is  attended  in  a  variety  of  vriiya  with  the  gro»t«t  danger  t 
health.  The  danger  arises,  not  merely  from  the  wilful  eiupluymon 
of  subsUnceH  of  Known  hurtfulimss,  but  also  from  their  use  ihruu 
ignuriiiiee  uml  accident.  The  excuse  uf  ignuriinee  may  tell  suiu'^wha 
in  favour  of  ii)iiiiiiruciurfr.>t,  wliu  in  aome  caj>es  may  not  be  aware  u 
the  deadly  naltiru  of  the  arUclea  which  they  daily  use,  knowing  them 
only  by  their  eominon  or  popular  names. 

Serious  as  the  result*  recorded  in  these  analyses  really  are,  we  have 
reason  to  believe  timt,  wjme  years  since,  thin;;s  were  even  warse,  unci 
that  nothing  was  more  common  than  to  meet  with  articles  of  sugar 
confectionery  coloureit  with  verdigris  or  acetato  of  co[>per,  with  the 
venliters  or  eurbonute^  of  copper,  and  with  mineral  green  or  unenite 
of  copper,  all  of  which  :irc  virulent  poisons. 

A  few  of  the  cases  of  poisoning  resulting  from  the  use  nf  coloured 
sugar  confectionery,  will  be  found  recorded  in  ^^  Food  and  its  Adal 
terations." 


Ox  THR    DbTCCTION   OP    THE    Anri^TERATIONS  OP    SlTOAm 
CoxrKCTIOMEBT. 

We  will  now   proifeed  to  give  some  brief  directions,  which  may 
proi'e  of  assistance  to  others  who  may  desire  10  analyse  for  themselves 
•ny  suspected  samples  ol  coloured  ccmfectionery.     We  sliall,  however, 
confine  our  directions  chiefly  to  the  detection  of  those   substance* 
which  we  htive  ourselves  discovered  in  the  different  samples  subject 
to  exuniinatioii.     From  the  liirge  number  of  analyses  which  we  bar 
mwle,  and  the  results  of  which   we   have  already  niailc  known,  Ih 
pigments  detected  will  embrace  certainly  iill  the  most  important 
those  which  are  onllnarily  employed  in   tlio   cnlonriition  of  confec 
lion  cry. 

Of  the  colours  used,  some  arc  stdiible  in  water,  and  others  in- 
soluble ;  the  former  include  nearly  all  the  vegetable  colours,  and  t 
latter  most  of  the  mineral  colour;!.  In  this  piirticulur.  therefore,  the 
U  a  brond  distinction  l>etween  vegetable  and  mineral  colouring  m» 
ters,  which  wilt  be  found  very  useful  in  guiding  us  in  our  snbscque 
Operations. 

In  the  miijority  of  cases  there  is  but  one  eolonrin;/  mailer  preseni 
•nd  this  is  u.-^uitUy  confined  to  the  surface  of  tlie  various  articles  e 
confectionery,  while  in  other  cases  ditferent  colours  are  ustil  in  the 
same  article.    When  the  colour  is  confined  to  the  surface,  it  ifl  readilr 
remoi'ed  by  washing  in  distilled  water,  from  which,  if  mineral 
aoluble,  it  will  usually  be  precipitated  after  standing  for  some 


I 
I 


COLQURED  SUGAR  CONFECTIOXERY, 


405 


And  it  may  thenbcobtnincil  in  an  almost  unmrxed  stale,  and  weighed. 
When  liie  colour  is  Uiflusi'd  throughout  the  whole  nf  the  nrtiile,  tiie 
game  cud  can  be  accomplished  by  di»9olv)ug  it  in  water;  the  supur 
will  be  removed  br  the  water,  and  (he  eolouring  roatler  will  subside. 
But  should  the  articlR  contain  f^tarch,  or  any  other  insoluble  substance, 
il,  of  course,  goes  down  with  the  colouring  mutter.  When  diirerent 
colours  occur  in  the  same  article,  they  must  each  be  cut  out  wilh  u 
knife,  and  separately  washed  and  teste*!. 

In  many  cawa  a  shorter  method  of  proceedinj;  than  the  above  may 
be  adopted.  The  confectionery,  when  it  i»  supposed  to  be  coloured 
with  a  Bxed  metallic  »alt,  may  be  incinerated  in  a  capsule,  and  the  &a\i 
tested. 

Nearly  all  the  pijfments  used  may  be  referred  to  one  or  other  of 
the  Ibllowin;;  colours',  red,  yeUou\  hhte^  ^«««i  fcroim,  and  purple; 
other  tints  occur,  which  are  formed  by  various  combinaiioos  of  the 
primary  cotours. 


Vegetable  and  Animal  Redt. 

If  the  red  or  pink  colourinn;  matter  be  of  ii  vegftnhle  nature,  nr  in- 
deed if  it  consist  of  a  solution  of  Ooecuji  cacti  tir  corhiMfil,  this  may  be 
MCertained  by  simply  immer^in;*  Hmiill  portions  of  the  coloured  comfit 
or  lozcn^'C,  tbe  one  in  a  solution  of  cuui^tic  potash,  and  the  other  in 
acetic  acid  ;  if  it  be  a  ve;»ctable  colour,  or  the  nnimid  colouring  matter 
cochineal,  it  will  become  purijhsh  in  the  alkaline,  and  brilliant  red  in 
the  acid  solution.  Ifihe  coluur  be  not  thus  ntfected,  then  (here  is 
reamm  to  supp'vse  thai  it  is  a  mineral  colounnf^  matter,  mot^t  probably 
either  red  lead  or  vermilion.  Ina.tmuch  as  many  red  and  pink 
comtit-s  &C.,  are  coloured  with  non-metallic  colouring  matter,  it  is  as 
well  to  try  them  all  in  this  way  in  the  fir^st  inntancc,  and  so  save  our- 
selves the  trouble  of  analysint;  each  for  nieiallic  pigments. 

Mineral  Heds. — The  lead  ofthf  redaxide  may  be  obtained  either  by 
WAJihinrr  or  by  incinerating  the  cuuifiid. 

If  we  desire  simply  to  ascertain  whether  tbe  red  pigment  consist  of 
lead  or  not-,  we  have  only  to  treat  it  with  a  drop  or  no  of  nitric  acid, 
and  to  add  subsef]uently  a  little  dilution  of  ^ulphuret  of  ammonium  ; 
these  reugoiits  may  often  be  applied  to  tho  pi;^minL  upon  the  article 
of  su^ar  confccCionery,  bv  which  nioaii.'>  we  are  enabled  to  ascer- 
tain in  n  minute  or  so  wliethcr  the  colouring  matter  consist  of  or 
contain  lead  or  not.  We  nuiy  proceed  in  the  same  way  to  detect  the 
lead  in  umssicot,  in  the  chromat^'S  of  lend,  either  pure  or  when 
mixed  with  l*rus5ian  blue,- as  in  the  <)ilTerenl  BruntiwicK  greens,  only 
that  in  the  raw  of  the  ehromates  und  Bnmswick  greens  It  U  best  to 
use  hydrochloric  acid  as  a  solvent  for  the  lead. 

We  have  stated  that  most  of  the  mineral  pij^ments  may  be  procured 
in  a  separate  state  by  washing  out  the  sugar.  Having  in  this  cose,  bv 
a  preliminary  trial  aiicertained  that  the  pigment  we  have  to  deal 


COLOURED  SUGAR  CONFECTIOXERT. 

with  ronsuU  of  re<l  lead,  we  have  nolfaing  more  to  <lo  than  to  dry 
And  Wfigh  it  in  order  to  determine  tlie  qunntitj  present. 

But  in  some  cases,  owins  to  ibu  u«e  ot  sttirch,  chilk,  or  other  atlul- 
terntiiio;  ingredient,  it  will  not  be  poaalble  to  nhtnln  the  firep>raiiun 
of  lead  or  other  pigiiicitt  in  a  soparule  state.  We  inuiit  then  proeeetj 
as  rolh)ivs,  to  determine  the  amount  ol*  lead  present :  — 

The  levl  must  be  precipimted  from  the  solution  of  the  ash,  either 
Qs  a  sulphuret  or  an  ii>did'j  of  lead :  this  must  be  collected,  dried, 
weiched,  and  the  lend  calculated  from  it. 

There  is  one  source  of  fallacy  which  must  be  guarded  aj;ainsU 
If  the  9ti&ar  be  adulterated  with  sulphate  of  time,  tiie  lead  mar 
escape  deit^ction  proceedtn;;  in  tU'\s  manner,  in  caiise<pif  ni.*e  of  tta  beiog 
converted  into  a  sulpliulc,  In  this  e:i!te  the  soluble  {>i>rtion  of  the  u*n 
having  been  removed,  the  remainder  should  be  fused  with  a  mixture 
of  nitre  und  hisulphate  of  potat^h  ;  the  residue^  after  having  l>eeii  well 
washed  with  water,  i»  lo  be  treated  with  a  solution  of  ainmoniat^l  tar- 
trate ofammoniti,  by  whicli  meuits  the  Kulpbate  of  lead  i^  tuken  up, 
and  muv  be  precipitAtctl  by  means  of  sulphuretted  hydrogen. 

The  bisiilphuret  of  mrratry  or  fwrntiimn,  after  being  ob(ain<Nl  in  as 
pure  a  jitnte  art  poa.nible  by  wa.<thin^,  must  be  di.ssolvt^it  in  a4]ua  r«^ia, 
nitro-hydrocldoric  acid,  and  inuHt  Im*  tested  for  in  the  m.anner described 
at  p.  377.  It  h  no  unrommon  thing  to  meet  with,  in  the  SAnie  red 
pijl^cnt,  both  load  and  mercury,  vermilion  being  very  subject  to 
adulteration  with  red  lead. 

Detection  of  the  Yellow  Cohurn. 

The  yeUotcs^  like  the  reds,  may  be  either  ve^etahU  or  mineral;  but 
contrary  to  what  was  found  to  be  the  Cft><»e  with  the  rc<l8,  the  yellow 
cf>lourin;r  matters  employed  are  for  the  most  part  mineral,  consisting 
otUfRon  or  orange  chromes^  both  these  being  chromalen  o/ Uad,  mnd 
sometimes  of  either  Naples  yellow  or  masticot. 

Mineral  Yellows.  —  All  the  yellows  ^hould  therefore  bo  tested  for 
leui  in  the  fir?t  inaUince.  For  this  purpose  the  surface  of  the 
comfit  bhouM  be  tnuche<l  with  hydroobloric  acid,  which  u'iually  de- 
stroys the  colour  at  once  if  it  be  a  salt  of  lead,  especially  a  chromate; 
afterwai-dft  a  drop  of  a  solution  of  sulphuret  of  ammonium  should  he 
applied  to  the  same  9p>tt  as  the  acid,  when,  if  lend  tje  present,  it  will 
become  more  or  lc*s  black  Recording  to  the  quantity.  If  the  pigment 
contain  lend,  in  all  probability  it  is  one  of  ilie  chromntes,  and  if  not 
one  of  these,  wnnxicot,  which  consists  of  the  protoxide  of  lead.  The 
colour  of  Nu/tieM  uellow  is  altnoat  sufficient  to  distinguuh  it  from 
the  chrouiates  of  lead. 

The  chromic  acid  of  the  chromate  of  lead  is  to  be  delected  by  the 
process  given  in  the  orticle  on  Snuff.  The  chromates  of  lead  mar 
also  be  discriminated  from  massicot  in  must  cases  simply  by  their 
colour. 


COLOURED  SUGAR  CONFECTIDNERT. 


NnpU*  yeUow  or  sttlphuret  of  autimont/^  mar  be  tlins  iilenlified  :  — 
Di<t!iulve  tne  pi  riK^nt  in  hjtlroclilnric  luriti,  mlc)  t-Jirlnnc  nt-id  diluted 
with  wuter,  treat  with  sulphuretted  hv'lro^n,  when,  if  iintiiiiOTiv  i^  pre- 
ftont,  an  ornnpe-red  preeipilnte  will  suluide  verv  ditrercnt  frnrn  lliiit  of 
sulphurei  of  arsenic.  Anfithur  way  is  to  sublime  the  uncimony  in  a 
teer  tube,  and  to  exumiiie  (be  in(.-tuilic  crust  with  ihe  niicrof^cope. 

Vegetable  YeUowa.  —  Those  urticles  which  are  not  found  to  contain 
lead  (ihould  he  subseipientty  teflte<l  for  gamboge^  which  is  the  next 
pigment  most  commonly  employed;  and  if  it  do  not  prove  to  be  this, 
then  a  jKirtinn  of  ihe  conint  should  be  immersetl  in  a  Rolutjon  of 
caustic  fkoio-sh,  when,  if  it  become  deoiiledly  browncil,  the  C"I«iupinff 
matter  will  be  vegetable,  ami  moat  likely  turmeric^  mffron,  or  yeliine 
lake^  which  is  usually  formed  from  the  colouring  mutter  of  l-rcnch 
berries  thrown  down  by  uluniinu  or  lime,  but  it  niuy  be  made  from 
any  vegetable  yellow  ;  these  vegetable  yellows  are  not  \eTy  fretjuetitiy 
employed,  probably  on  account  of  their  liability  to  alter  and  fade  on 
exposure  to  the  atr  and  bght,  —  an  objection  which  also  ujtplieK, 
tlioui;h  in  a  less  degree,  to  pamhofre. 

If  the  pigment  hot  gamboge^  it  will  form,  with  distilled  water,  a  veU 
lowish  opaque  emulsion^  which  will  not  let  fall  any  dcpoiiit  This 
<*mulsion  should  be  evaporated  to  dryness,  and  alcohol  added  to  the 
residaum;  the  alcohol  will  take  up  the  gamboge,  and  when  water  is 
added  to  the  solution,  the  gambo;£e  will  be  precipitated.  If  to  the 
yellow  precipitate  a  drop  or  two  of  strong  ammonia  be  now  added,  it 
js  rediesolved,  producing  a  blooil-red  solution,  from  which  it  is  pre- 
cipitated pale  yellow  by  nitric  acid.  Turmeric  gives  nearly  the  same 
reactions,  anil  therefore  much  care  is  requisite  to  discriminate  between 
the  two.  Turmeric  docs  not  form  so  decided  on  emulsion  with  water 
as  gamboge. 

On  the  Detection  of  the  Blue  Colours, 

The  liluei  may  be  also  either  vegetable  or  mineral:  the  former 
include  litmM  and  indigo ;  and  the  laiter,  FniMsian  Mue,  Antwerp  blue^ 
the  two  rerrtiterM^  which  consist  of  carbonate  of  copper^  the  only 
dilVerence  between  them  being,  thai  the  paler  vcnliter  is  diluted  with 
lime;  aifmlt;  «mri/^wliich  is  o  bIoss  of  cobalt  [rowdered ;  antl  nrtijicial 
ultramnrtnCt  wliicti  is  made  in  imitutirm  of  true  ultramarine  nr  lazuliie. 

Vegetable  Bluet,  —  The  vegetable  blue,  litmus^  is  sufficiently  dis- 
tingui<*hed  by  it«  becoming  red  on  the  addition  of  weak  acid^.  This 
pigment  is  manufactured  from  several  species  of  a  lirhen  {Jittrrlln)^ 
und,  when  genuine,  ii  innocuous.  In  a  Kcport  of  M.  Andml,  ad- 
dressed some  years  since  Ui  the  Prefect  of  Police,  it  is  stateil  that  8ttme 
manufacturem  mix  common  arsenic  and  peroxide  of  mercuiy  with 
litmus,  and  M.  Andrul  therefore  considers  that  its  use  in  the  colouring 
of  sweet  confectionery  should  be  prohibileil. 

Indigo  is  sufficiently  distinguished  by  its  subliming  in  dense  violet 


4»6 


COLOURED  9UGAR  COXFECTIONEKV, 


vapours  when  heattfil,  by  forniin^  a  bliio  solntinn  with  concent 
sulphuric  ai-it),  ami  bv  ius  reiiminin;;  uiii-hiin^vil  In  alkalies. 

Mineral  Bines.  —  The  colour  nf  ffrnKymtide  of  irott^  or  Prustii 
blue,  is  immediately  (Ii!«cli!ir»ed  on  the  miililioii  nf  the  caustic  alkalii 
the  iron  being  throivn  (Kiwn  in  the  •'tato  ot'iit-roxiilo,  when,  if  ne<:eji*»i 
the  iron  may  he  collecteti  iin<i  weiahed  ;  the  ctdimr  is  also  destroyer 
by  iitcinerntion,  the  red  oxide  t>f  iron  (tnly  being  left,  which  i»«y 
weiybwd  nnd  calciiUtcd  into  Pru-isiun  blue. 

Auiwtrp  bltie  is  Pruasian  btuc,  I  he  enloiir  of  which  ie  rencloi 
liuhter  rimI  brighter  in  uDn-c.'fpienfe  nC  its  ditulittn  with  some  colour- 
less niiitenal,  uFinilly  ch:dk.  The  tests  for  Aiitwer|i  blue  are  there- 
fore the  same  iw  for  Pru9!*iaii  blue,  thtwe  forcarbnnnte  of/iW  t/r  trfutl 
being  Kuperadded.  Thir(  and  (he  preceding  prjfnient  is  in  penerl 
suRieiently  distinsui.'thed  by  adding  a  drop  nr  so  t>f  nolution  of  am* 
innnia  or  potash  direct  to  them  upon  tlic  t^ngar,  these  rengents  atom 
dorttroying  the  blue  colour. 

The  Veriiiterx  are  curlnmates  of  copper;  tlicy  lire  dislingtiiphed  froi 
otlier  BidU  of  copper  by  the  ewiupe  of  carlwnie  acid  on  the  adilitiao  nf 
any  mineral  acid:   when  lKnle<l  for  a  long  time,  or  heated  eiirefiiUv, 
the  carbonic  acid  escajie*.  und   the   pigment   becomes  brown.       J-httH 
re.its  for  copper,  find  the   niL>thod  by  which  ic  may  Ije  detenuine^H 
qtiantilatively,  will  be  found  described  under  the  head  of  Pickies  andt^ 
Pr*' serves. 

The  remaininjT  blue  pigments,  cohalt^  umiilt,  and  ultramnrine^  are^ 
distinguishe<l  by  1  heir  culitur  being  fixed  in  rlie  fire^  so  that  the  aii] 
of  sugar  articles  coloured  with  any  of  these  subptanoes  is  of  a  brigl 
blue,  the   tint  varying  accor<ling  to  thtf  blue  used,  as  well  as  aJso  il 
consequence  of  admi.\tuic  with  uncoloured  substances,  smrh  as  chsU 
hulplmte  of  lime,  or  pipe  clay.   These  colours  are  somewbot  expensivi 
especially  the  true  ultram»rin»\  b'lt  they  are  of  such  intensity  that 
little  goes  a  great  way  ;  there  is,  however,  a  cheap  kind  of  ultrama- 
rine, sold  in  the  shops  as  German  or   French  uUrnmariTtf^  the   pri< 
being  about  sixpence  per  ounce,  and  it  is  this  blue  pigment   whici 
is  chiefly  employed  in  the  colouring  of  su^ar  confectionery.     Il  con- 
sists of  a  double  silicate  of  alumina  and  soda  with  sulphurot  of  iwdiumi 
and  it  may  be  distingui-^heil,  when  free  fmui  admixture  with  other 
substances,  bv  adding;  to  it  a  little  hydrochloric  acid,  and  observing 
the  chIoup  of  sulphuretted  hydrogen  evolved.     This  mctluMl  of  di 
crimination  is,  in  thr  case  of  coloured  augur  confectionery,  for  the  ini 
part  inapplicaljle,  since  sulphuretted  hydn»jrcn  is  iklutost   invnriahlj 
thrown  off  whenever  hydrochloric  acid  is  added  f)  the  ash  left  on  ihi 
iitcineration   of  most  articles  of  sugar  confectionery.     The  pitrmonl 
ought  therefore  to  be  pro».-iired  in  a  separate  stale,  by  washing,  «n( 
the  acid  applietl  to  it  when  dry. 


COLOURED  SUGAR  OONFECTIONEKY. 


497 


On  the  Detection  of  the  Green  Colours. 

Vegetable  Greens. — Of  Uie  greetut^  there  is  but  one  vegetable  green 
used  —  nanicly,  jriJ/>  ^Tirrn.  Thi«  U  pre|»ai"ed  from  the  jj;reen  btirrk'a 
of  tbe  bufkfhoni,  iVutmnux  calharticus ;  but  its  use  is  to  be  objected 
to  on  accijuiit  of  its  frtHjuent  ii<luUcrntinn  with  greon  iiietaltio  pig- 
nicnl^  contnimn<^  either  copper  or  oTdCnic,  in  order  to  biM<;;hten  its 
colour  itnd  rentier  it  more  permanent.  It  is  bleached  by  chlorine  and 
acid  ft. 

Metallic  Greens.  —  Of  the  metnllie  (rrents,  eome  arc  simple  colours, 
while  (ithcrs  are  compt>5ed  of  a  blue  und  a  yellow  mixeil.  The  simple 
greenit  are  acetnta  of  copper  or  vertiigrig,  und  argettite  of  copper, 
etnerai/l  green  or  Scheele^g  green. 

Acetate  of  copper  is  dlstm^ished  from  other  jjreen  salts  of  copper 
by  the  action  of  sulphuric  acid  ;  the  acetic  acid  is  liberated,  and  may 
be  detected  bv  it3  wlour. 

Antenite  of  copper  is  best  recognised  by  means  of  the  arsenic,  of 
which  it  \a  in  part  composed  :  a  portion  of  the  colouring  matter  Hepa- 
rated  from  the  sugar  by  washing,  when  perfectly  dry  is  placed  in  a 
(est  tube  open  at  both  ends,  the  bent  of  a  spirit  lamp  being  applied 
outride  tht;  tul>e ;  tbts  will  cause  the  arsenic  to  sublime,  and.  condensing 
on  the  coid  $id«  of  the  tube,  it  tbmw  a  bright  meiallie  oru»t,  which, 
examined  with  a  Inw  power  of  the  microscope,  is  axccrtuined  In  consist 
of  minute  ociohednil  crysuls.     This  lejtt  i*  perfectly  conclusive. 

The  compound  greens  ordinarily  used  arc  those  eommoidy  sold  as 
Bnauwitk  greens;  ihey  are  the  colours  usually  employed  in  (uaking 
green  paint,  and  are  of  three  dltTcreut  tinta.  known  as  pale,  middle,  and 
deep  Hrunswick.  They  consitit  of  a  mixture,  in  various  prnporlions, 
of  usu:dlv  Antwerp  fc/uf,  but  sometimes  ultramarine^  und  chr ornate  of 
Iswi.  When  obtiiincd  in  any  nuunlity  iVom  the  confectionery,  and 
difiuseil  through  water  in  a  HJnitJuw-  di^h,  the  twit  colours  easily 
serrate,  iin<l  may  be  distinguished  by  the  eye  alone. 

They  may  usually  be  rccognitfcil  without  the  trouble  of  procuring 
them  in  a  separnte  state  by  washing,  by  adding  r^ageiite  direct  to  these 
pigments  as  they  cover  the  sugar  ornament.  If  ammonia  or  jtotash 
18  added,  the  green  colour  disappears,  and  is  replaced  by  h  yellow ; 
that  of  the  Prussian  blue  being  destroyed  by  the  alkali,  the  chromate  of 
lead  comes  into  view  again;  if  the  pigment  is  touched  with  hydro- 
chloric acid  it  bei'oraes  blue,  thiit  arising  fnim  the  solution  of  the 
chromate  of  lead  by  the  acid.  These  are  ready  and  very  HAtisfactory 
lestA.  Other  comftound  greens  are  occattiunally  made  by  mixing  a 
TcUuw  pigment,  usually  yw^  cArome,  with  one  or  other  of  the  verditcrs. 
Vhe  true  Brunttwick  greens  ore  oxichlorides  of  copper,  but  these, 
being  very  expensive,  are  seldom  employed. 

The  oxichJwides  of  copper  may  be  thus  distinguished  from  the  other 
green  salts  of  copper.   Dissolve  the  pigment  in  a  httie  pureaad  dilute 

K   K 


C0mL.B8A> 


wJ^mrri 


vUca  UKSWS    dovB 


Mspletcd  tbe  dcacnpoon  of  ihe  wetbods  hj  which  the 

pignesti  emplorcd  to  eolottr  sugar  coofectioaery  mar  b« 

il  MOV  reoMiat  oolj  to  indictte  tW  priw.*!*wj  b^  which'  the 

wtinfff^,  DOC  pigaMsli,  either  aaeertftined  to   be    used    hy 

or  othen  in  the  adaltermtioa  of  tugir  oootfectiooerr.  ouj  be 

TW  principal  of  these  rabetaaccs  are  Tanoot  kinds  of  <torc4,  rJkaO, 
Mai»  <;/'  '»>«.  kydratgd  tmlpkate  of  Hme,  aituter  of  Paris  or  gjptwm, 
i  wUr  potttr*  ejoy,  pi/w  oloy,  or  CoraitA  day. 

On  Mr  DtUtHom  of  Chalk,  PUuier  ofPorU^  and  Clay. 

Ordinary  planter  of  Paris^  aIthoa;:h  stated  to  be  emplojed  in  Uie 
^avttfiiK'ture  of  confectionorr  iniended  to  be  eaten^  can  M^rcelv  ever 
^sOkSim'e  when  this  is  rn'oistened  with  water  it  quicklr  become 
ajt*  —-•"■'"-•  •'-  wild  slate  after  incineration;  on  the  other  hand, 
hy^nle^l  sulphate  of  lime  does  not  remain  solid,  and  when  expi»ed 
toart^l  h^ai,  it  is  still  a  pow«ler.  The  process  for  the  qualitative 
1^  i^uantitAtive  delenninntinn  of  this  salt  is  described  at  p.  99. 

1*WM  i*  snfficientlv  identified  bv  its  appearance,  br  its  effer^esrin^ 
^  the  addition  of  an  acid,  and  hy  the  lime  which  l^  thrown  down  from 
j^folution  by  oxalate  ofomraonia.  See  p.  101.  Alumina  is  detected 
^  iht  process  indicated  at  p.  1 80. 


PORTEH,   AND   ITS  ADULTERATIONS. 


499 


On  the  Detection  of  the  Different  Kinds  of  Starch. 

Ttie  kind  of  starch  einplovf^d  a  detected  by  means  of  the  microscope 
A  minute  portion  of  the  sugar  should  be  plAceii  upim  a  slip  of  glass 
and  11  dntp  of  water  nddt'd,  if  the  sujiar  dis^ioWc  without  any  iippcar- 
nnce  ot  resiilup,  ibi.'  ><ululitui  beln^  ijuite  iransparciit,  (he  pinbulHltty 
i»  that  no  starfh  is  present,  but  if  there  be  any  residue,  this  nhould  be 
placed  under  the  mieroscojie,  when  ibi*  starch,  if  presi'nt.  will  usually 
DC  reco;2ni8ed  by  ihe  funu  of  the  i^runiileH,  but  abuuld  the  starch  be 
in  an  aiiuirphous  state  in  con8e(|uentie  of  ilif  having  been  boiliid,  then 
A  litlte  itMliiie  should  be  added  to  the  residue,  which  will  at  once 
reveal  its  presence.  The  quantity  ntay  be  estimated  in  either  of  tlie 
fullowiue  wnya  : — When  flturch  only  is  mixed  witli  the  sugar  the  latter 
mav  be  di&aolved  out,  and  the  precipitated  starefa  dried  and  weif^hed ; 
but  when  any  other  insoluble  substance  U  present  the  precipitate  left 
fitter  the  removal  of  the  sugar  mny  be  burned,  and  the  loi^s  of  weight 
will  pive  very  nearly  the  quantity  of  starch  ;  or  the  precipitate  may 
bt^  boiled  in  water;  the  st4irch  will  be  taken  up,  and  the  insoluble 
matter  will  subsiile  ;  the  supernatant  liquid  can  then  be  decanted  frum 
the  depo>iiL,  and  the  starch  ohtaincil  on  uvajwration  or  by  precipita- 
tion in  the  fonii  of  no  iodide,  by  iiieand  of  a  solution  of  iodide  of 
pttlnsiiium. 

Until  the  5th  of  April,  1857,  the  duty  on  sugar  confectionery  will 
be  2^^.  per  lb. ;  till  the  5th  of  April,  l'85»,  2d.  per  lb. ;  thenccafter, 
Urf.perlb. 

Suecadet  and  all  fruits  and  vegetables  preaerred  in  sugar  are 
charged  the  same  duty,  such  as  citron  peel,  &C. 

Gross  amount  of  duty  received  upon  Confectionery  in  the  year 
1854,535/.;  1K55,  45*29/. 

luiiKirts  in  1»54,  73,347  lbs.;  in  1855,  69,559  lbs.  Retained  for 
home  consumption  iu  the  first  year,  64.708  lbs. ;  in  the  second, 
62,368  lbs. 


PORTER,  AND  ITS  ADULTERATIONS. 

PoBTRR  and  stout  should  be  brewed  of  malt  and  hops  only,  tnd  the 
colour,  as  well  as  tlavour,  should  be  due  to  these  alone. 

The  colour  of  all  mnlt  litjuors  is  df  pendent  upon  the  degree  of  beat 
to  which  the  malt  has  been  sul^ected  in  the  kiln,  and  upon  the  amount 
of  ripeness  ihe  boos  have  attained  before  being  stripped  from  the 
poles.  Thus,  for  tne  pale  bitter  ales  Ihe  greatest  care  is  necessary  to 
jirevent  the  husk  of  the  malt  from  charring  in  the  least,  and  to  main- 
Inin  the  original  straw  colour  of  the  barley  ;  and  in  the  selection  of 
the  hops,  that  they  should  be  picked  as  soon  as  sufficiently  ripe  to 


500 


PORTER,   AND   ITS  ADULTERATI0X8. 


keep,  and  that  no  single  brown  or  withered  leaf  should  be  suffered  to 
remRin.  The  reverse  of  tilt  ihiit  is  the  ease  with  the  malt  and  bops 
required  for  porter.  The  malt  should  be  brijtklj  dried,  until  th« 
flower  of  the  ^Tuin  is  of  a  ligflit  brown  clour,  and  cnisbeswitb  a  crisp 
friability  hetwi;en  the  teeth;  the  hopjt^  aJuo,  shouhl  have  buns;  in  the 
autumn  ?un  till  they  have  attained  a  rich  ^Idea  hue,  and  the  seeds 
are  |terfcctly  <lcvelt>ped.  With  all  attention  to  these  refjutrementSi 
huwever,  the  beer  brewed  would  still  be  far  from  the  neeesaarjr  colour 
and  Havgur,  und  to  attain  these  the  maltster  U  compelled  to  prepare 
nmlt  in  a  peculiar  manner.  IL  must  be  remembered,  nevertheless, 
that  the  strcnffth  of  the  porter  is  due  almost  entirely  to  the  |>ale  malt, 
as  the  other  kinds  liave  their  Mccharine  properties  so  altered  by 
roasting  as  to  render  them  nearly  useless,  except  for  colotir  and 
flavour,  as  before  mentioned. 

In  addition  to  tho^e  distinctive  properties  of  porter  and  stout,  there 
is  one  ntlier  of  Mill  greater  importjtnee  —  the  peculiarity  of  the  fer- 
mentation. Up  to  the  couimenveraenl  of  this  Iu»t  sta|ce  of  the  process 
of  brewing,  the  manufacture  of  ]>ortcr  is  conducted  in  exactly  the 
mime  manner  as  tbat  of  ale,  wilb  tlie  addition  of  the  dilferent  flavouring 
malts  before  mentioned  ;  hut  during  the  fern^cntation  the  great  dif- 
ference is  effected,  as  nil  ihe  Bu^ar  is  converted  into  spirit,  excepting 
only  such  fKirtion  as  is  required  to  preserve  the  beer  from  the  acetous 
fiTiiieDtatlnn,  which  is  less  than  In  ale,  by  reaAon  of  the  larmier  amount 
of  hops  upwl  in  proportion  tn  the  strength  of  the  wort.  The  differ- 
ence will  be  best  appreciated  by  the  annexed  figures.  <ioi»d  porter 
should  weijih  about  twentv-two  jiounds  specific  gravity  »lH>ve  water 
p4T  barrel  of  thirty-six  {laltons  before  thif  fermentation,  and  t>in(;le  X 
ale  ulxnit  the  same;  but  after  femiiiiitfttion,  the  porter  will  be  found 
to  rctnin  only  fire  pounds  weijiht  j»er  han-el,  while  the  ale  has  seTen. 
Thus,  ordinary  ale  is  more  liablo  todfrantft*  the  sinmoch,  by  reason  of 
its  jtreater  swectnesit,  while  |X}rter  i6  more  beady  in  proportion  to  itd 
strength,  and  soporific  in  its  tendency,  from  the  strong  infusion  of 
boot  lo  its  composition. 

It  may  be  interesting  to  make  a  few  remarks,  succinct  as  possible, 
npon  the  prepiirntion  i>f  ninlt  and  hops  before  they  come  mlo  the 
brewers'  handii ;  and  upon  iainglusSj  the  only  substance  which  should 
be  used  for  tinini;  beer.  It  mny  be  well  to  observe,  before  doing  this, 
that  suffar  is  permitted  by  law  to  Jie  H«ed  for  brewing,  and  bus  been 
and  will  be  consumeil  extensively  whenever  malt  rises  to  a  siiflicienrl/ 
hi};h  price  to  render  it  profitable:  nevertheless,  it  is  advisedlr  the 
do<{nia  that  **  porter  and  stout  (and  indecil  all  malt  liquors)  should  be 
brewed  of  ntalt  and  hops  only,"  as  wn»enunciateil  in  the  cummence- 
vent  of  this  article ;  for  beer  brewed  from  sugar  has  greater  tendency 
so  tbe  acetous  fermentation  than  mnll  liquor,  so  that, setting  aside  the 
undoubted  superiority  of  flavour  in  the  latter,  tbe  risk,  buih  peenniary 
aviotherwiflCt  attending  the  use  of  sugar,  is  too  great  to  tempt  the 
yiAcnt  man  of  busioess. 


FORTBB,  AKD  ITS  ADULTERATIONS. 


501 


Jlfuft. 

Mftlt  u  barley  in  wliteh  germination  has  becu  carried  on  to  a  cert4iin 
extent,  and  then  suddenly  out  oH'  by  the  application  of  heat :  the 
process  is  conducted  as  follows:  —  M'lur  stoeninj^  the  barley  in  a 
cisteni  of  water  till  well  pwoIiIl'ii,  it  is  thrown  in  layurs  on  the  slate 
floors  of  the  lonj;  luiiU-lioufc,  buiUlinjfs  well  known;  it  then  ^'crmi- 
natea  nui<?kly;  it  Is  not,  huwcver,  allowed  tu  rest,  but  is  tunied  over 
rrom  time  to  time,  until  every  griiin  has  been  iiUke  ex[>o5eil  tu  the 
nir,  nml  to  such  light  ds  is  permitted  to  enleff  which  u  not  great,  oa 
the  growth  would  otberwise  be  Ibrced  too  speedily,  the  object  to  be 
attained  being  the  conversion  of  the  f^tnrch  into  sugar,  which  i^  known 
to  be  coukplete  when  what  is  called  llie  acruspire  has  reached  three 
iiarta  of  the  way  up  the  grain,  particularly  observable  by  a  thicken- 
ing in  the  back  of  the  *:ruinB  of  barley.  L)urin"r  litis  sta;;e  the  inidt 
emits  a  aniell  resembling  that  of  cucumber.  When  the  grain  has 
arrived  at  this  condition,  it  is  thrown  into  the  kiln  in  a  layer  of  from 


Barlrr. 


M«It. 


three  to  five  inches  in  thickness^  nccording  to  circumstances,  and 
while  there  it  is  turned  over  once  or  twice  in  about  twentr-fbur 
hours.  The  kiln  has  a  wire-gauze  bottom,  tbrou;:b  which  the  heated 
air  from  a  fiirnnee  of  Welsh  cnal  ascends.  The  briskness  of  the 
rire  and  the  time  of  drying  depend  u[>on  the  colour  require*!  in  the 
mall.  The  process  it*  then  complete,  with  the  exception  of  screening 
away  the  "  mult  dust,"— the  dried  roots  of  the  embryo  plant,  a  very 
nutritious  food  for  catile,  and  which  also  does  duty  sometimes  for 
ground  coffee,  Scotch  nnuff,  and  other  arlicles. 

In  the  choice  of  malt,  the  brewer  is  guided  by  the  growth  of  tlie 
acr(»spire,  as^  if  it  be  not  sulficiently  developoil,  there  is  less  saccha- 
rine matter  in  tiie  grain  than  is  requisite,  »nd  more  gluten  ;  and,  if 
overgrown,  the  saccharine  matter  is  absorbed  by  the  progress  of  the 
germination. 

Malt  contains,  besides  saccharine  mtttter,  a  substance  called  dynstase, 
which,  in  the  mash  tun,  by  the  action  of  hot  water,  and  agitation  by 
machinery,  converta  the  greater  |Hjrtion  of  the  starch  into  sugar. 

The  paie  malt  thus  manufictured  is  the  base  and  strength  of  alt 
malt  liquors.  It  now  remains  to  notice  the  other  malts  used  for  the 
[turpose  of  fliivouring  and  colouring  stout  and  porter. 

Amiter  tnaU^  used  in  the  proportion  to  pnie  malt  of  one  eighth  part, 
differs  merely  in  being  dried  at  la.'^t  faster  than  the  ordinary  kiml,  and 
by  a  hotter  fire.  The  delicacy  oi'  the  tlavour  of  stout  is  much  de- 
f>endent  upou  this  uuUt. 

K  a  3 


AOS 


PORTBB,   AND   ITS  ADCXTE RATIONS. 


SrowH  or  hloxen  malt  is  of  a  (larker  colour  extcmallj,  but  inlei^ 
nally  it  is  of  a  deep  brown  colour.  It  is  manufactured  by  b«?i  ^ 
placed  in  the  kiln  in  a  luyer  of  only  one  inch  in  thicknei^s,  and  nried  by 
a  fierce  fire  oi  wood  in  a  very  stiort  space  of  time.  Ttiis  inalt,  used 
in  the  proportion  of  one  lialf  of  the  pule  m:ilt,  ia  the  source  of  the  rich 
erapyreiimiiiie  flavour  of  siout  and  purter,  (imi  dues  much  towards  its 
colour  ;  but  this  is  finally  eficcted  by  what  is  culled  patent  mnlt^  which 
19  of  a  very  ilark  brown  colour.  This  innlt  is  pale  nmlt,  perfected  in 
the  kiln  in  tlie  orditmrv  way,  Hml  then  ri>us(ed  in  a  eiiniilar  manner  to 
collee,  utily  (tn  an  itittniti'ly  lar-jr-r  scale.  The  colour  of  porter,  as 
before  mentioned,  is  prinnjinlly  ilne  to  this  mall ;  but  it  is  so  power* 
iul  an  agent,  that  no  nridrc  th:m  one  liflicth  part  of  it  is  used  in  pro- 
portion to  the  other  mnlts. 

It  is  aluted  in  most  chemical  works  that  the  su;;ar  of  malt  it?  furmed 
at  the  expense  nf  the  starch.  If  this  were  so,  the  starch  corpusclea  of 
the  barU'y  nu^ht  to  exhibit,  when  examined  with  the  uucniscope, 
some  evidcnou  nf  this  convei-ston  in  an  alteratiun  of  form  or  substance. 
Under  the  highest  powers  of  thiit  instrument^  however,  no  diiferenc* 
in  form  or  oiuline  in  the  gninules  of  iinmalte<l  and  malted  barley  is 
perceptible,  llie  granules  i.f  mulr,  simply  showinj;  a  greater  t^-ndency 
to  cohere  in  niiisso^.  The  results  of  microscopical  ol)ser\ation  do  not 
appear,  limrefore,  tooonlirai  the  piatouicnt  tlnit  the  sugar  of  malt  is 
derived  from  the  starch,  but  they  point  to  another  constituent  of  the 
Eirain  of  barley  as  that  whicli  reiiUy  furnislie*  the  sugar,  namely  the 
cdiuloae.  This  in  uiaU  is  abnit-tt  entirely  destroyed.  Now  cellulose 
has  nearly  the  same  chemical  composition  as  starch,  and  its  transfor- 
malinn  ilnnblless  furnishes  much  of  the  f*ugar  of  nmlt.  The  presence 
of  the  celluhise  in  the  raw  (p^in,  lujd  its  abtence  in  malt,  may  be  readily 
shown  by  tearing;  into  pieces,  with  needles,  sections  of  the  ^ains  and 
washing  awuy  the  stiireh. 

The  fact  ut'  the  disapjwarance  of  the  cellub«e  is  not  only  interesting 
in  a  seieutilic  point  of  view,  but  is  uls(»  of  practical  iiupurtauce,  sinc*e 
it  supplies  a  rea<ly  means  by  whii-h  barley  may  be  distinguished  from 
malt,  even  when  the  two  are  n^ixed  together^  the  dJiscriaiination  for 
certain  Flxcise  purposes  Iveing  often  of  nun  li  consequence. 

The  above  oK-i^rvations  were  mudi'  jninclpaily  uiion  samples  of 
barley  un<l  malt  kindly  furui^hed  the  author  by  Mr.  Wren,  of  Hunt- 
ingford  ;  to  wbo^iL'  long  ex|K'rienee  in,  and  great  knowledge  of  ui&ltiug, 
he  is  indebted  for  many  practical  reiiiurkb  and  Bujjgcstiuns. 


I 


I 


Hops, 

Hops  will  next  demand  our  attention  ;  but  to  consider  the  kinds 
and  cultivation  of  these  fally  would  occupy  more  space  than  can  bfe 
aHTorded. 

Hops  are  a  very  delicate  and  precarious  crop,  alFceted  greatly  by 
the  weather,  and  ibey  aUo  full  a  prey  to  various  kinds  ut  blight,   of 


PORTEB,  AND  ITS  ADULTERATIONS. 


503 


which  the  most  dcTaittating  nre  the  y7y,  and  mould  or  rust.  The 
former  jh  the  well-known  green  insect  und  bluck  Hy,  tlint  attack  tb« 
rose  plnnt8 ;  ami  its  ravages  are  ho  j^reat,  tbut  three  i'cmrtbs  ul'  the 
years  crojM  ure  itometiijies  BacriBceri.  The  latter  is  a  fungus  which, 
attacks  the  hup  itselt",  and  not  only  prevents  its  proper  dL-Vflopment, 
and  thiiB  destroys  its  preservtitive  properties,  hut  also  coinmunieatea 
an  ijnpk'a?<ant  Huvour  to  the  beer. 

Like  the  vino,  the  hop  loves  tlie  sun,  and  can  scarcely  have  too 
muAx  oCit;  it  oUo  resembles  that  plant  in  the  soils  and  situations  it 
ujotjii  prefers — the  sunny  sides ut'&lnpin;^;  bills,  and  the  well-L'UJtivated 
suil  ^if  Kent,  resting  on  tlie  Kentish  ra;r  or  iroiisttioe.  The  uiOst 
choice  ho[fS  are  ^rown  in  East  Kent,  and  Che  next  in  esliinatioit,  in 
mid-Kent,  In  ordinary  seasons,  the  hups  grown  in  Kent  neurly 
suffice  for  all  the  nmlt  liquors  brewed  in  Kn";iriiul  \  but  in  seiLsuns  of 
scarcity  foreign  hops  are  nmcb  used,  liitlicnoi  the  bops  ^rown  in 
Belgium  have  been  considered  tlie  best,  and,  in  appeurance,  there  ia 
no  doubt  they  are  bO«  as  the  Be]<jian  growers  have  Uikt>n  great  pains 
to  imitate  our  mode  uf  prepanilion  and  packing;  but  the  huvarion 
hops  are  really  much  liner  in  f^uubty  and  llavoiu-,  and  the  aruma  is 
more  perfectly  preserved  by  their  method  of  preparatiooi  which  dill'ers 
from  ours. 

Some  few  hops  are  imporl«l  from  America,  but  thnurrh  very 
powerful,  they  are  so  nink  and  peeutiar  in  Havour,  thui,  without 
great  improvement  in  cultivation,  they  are  never  likel/  to  be  exten- 
sively adopted. 

The  preparation  of  hops  is  a  very  simple  process,  and  may  be 
related  in  but  few  words.  The  poles,  with  the  bop  plums  Hiill  litiiig* 
ing  on  them,  are  pulled  from  the  ground,  vrheii  tbe  bops  ure  picked, 
by  women  and  children  prmcipally,  to  a  great  number  of  whom  it 
atTords  a  tem)>orary  employment ;  they  are  then  dried  on  a  kiln,  some- 
what resembling  the  mall  Vdn,  but  the  heat  is  much  less«  and  tl^e  door 
of  the  kiln  is  made  of  liair  ototh.  A  small  portion  of  sulphur  is 
burned  on  the  kiln  tire,  for  the  purpose,  in  the  fir.-it  place,  of  preserv- 
ing the  hops  —  at  least  this  is  the  plea,  and  there  may  be  some  truth 
in  it,  as  the  sulphur  may  ilestroy  any  insect  or  fungus  remaining  iu 
the  hops,  but  the  grtrul  reason  tur  the  use  of  sulphur  ifi  its  bleu^liing 
property,  whiih  renders  Uie  hops  more  sightly  to  the  eye.  Alter  they 
have  been  thus  dried  and  bleac-hed  they  are  puckfMl,  by  presses, 
ti":htly  into  the  bags,  or  pockets  us  tbey  are  called,  to  excbuie  the  air. 
Tliey  are  packed  so  tightly  bv  the  hytlraulic  press  that  they  become 
lulTifieully  solid  to  be  cut  in  blocks  with  a  knife. 

All  Knglifth  hups  are  prepared  in  this  manner,  and  the  Belgians, 
finding  that  (he  ble:icliing  and  packing  have  a  great  elTuct  upon  the 
eyt%  have  followed  uur  example  ;  but  the  Biivoriun  growers  still 
adhere  to  the  custom  of  their  ance^itors,  and  it  is  to  be  hoped  they 
will  continue  to  do  so,  with  increased  attention  to  oultivutiua  and 

K  K  4 


B04 


rORTEB,  AND  ITS  ADULTERATIONS. 


packing,  which  will  render  their  hops  equal  to  the  best  English 

produce. 

The  mode  in  use  in  BaToria  is  as  follows  : — When  the  hops  are  rip© 
the  plant  \»  cut  ofT  vUtse  to  the  ground,  antl  the  hops  arc  left  on  the 
jKiles  to  dry  in  the  sun.  This  metho«i  preserves  the  aroma  entirely, 
und  all  the  ef^entiiil  nil  ;  the  connetjuence  is,  that  although  they 
ure  pnokeil  ](>o^(»ly  in  halt^s  and  look  like  withered  leavr-s,  they  have 
moro  strength  nml  flavour  in  proportion  t*)  their  qu&lity  thiin  Uie 
Englifih  hops.  It  is  somewhat  pru'inuture  Ut  spenk  of  this  methcMi  as 
reKBnls  the  preservation  of  the  hops  compared  with  that  followed  in 
Kn^ilaiidj  us  the  Biivariun  hups  nre  a  recent  importation ;  in  our 
variable  climate  the   process  by  which  they  are  dried  would  be  un- 

ftg.  MiL 


PORTEB,   AND  ITS  ADULTERATIONS. 


505 


brown  and  musty  by  keeping  :  in   such  a  condition  ih(.*y  are  whully 
unsaleable ;  but  ofUu  so  ^eut  is  the  dctuaiid  for  Imps  that  thu  must 


m.  lu. 


JbedottUtr,  A.  rufanf,  ihuwlnc  lh«  fflurm«taor«hleh  U  htevHl.dMiMOiid. 
markad  fr,  (King  Uie  in«M  ctuncterlalf.  R  I'^rtiail  ttOlim  nf  Mtd.»xhM^ 
Ibj  U>«  (Viw  >Maibcmaca,  uwl  Um  mUUa«»  of  Um  Mnl,  a.  llifW«i  Ml  <U»- 
mcterii. 

worthleas  description  of  foreign  hr>ps  are  purchawd,  and  subjected  to 
fumigation — by  which  means  th(>ir  colour  is  reaiorcd,  and  tlieir  pro- 
perty  of  checking  fermentarioi)  rcvive<i.  To  cffct't  this,  as  uiucli  a» 
10  Ib6.  of  sulphur  are  employcfl  in  some  eases  for  erery  hundred wui^liC 
ol'hops.  As  lurpe  a  quantity  as  10  per  cent,  of  free  nulphnric  acid 
b:i9  been  met  with  in  aauiples  of  blenched  hups;  lhi»  acid  is  formed 
by  the  oxidation  of  the  nutphuroua  auid  generated  durin;^  the  bleat^h- 
in«^  process. 

Having  touched,  though  imperfectly  and  cursorily,  upon  malt  and 


JKM 


PORTER,   AND  ITS  ADULTKRATIONS, 


hops,  a  few  words  upon  isinglass  will  complete  the  account  nf  the 
materials  used  in  tlie  brewing  of  porter.  For  many  of  tite  preceding 
details,  iii  rejiiird  lo  liops  cspocifllly,  we  are  indubteii  to  ^Ir.  Tbocnaf 
Druce,  of  the  IIiius  Town  Urewery,  CbeUea. 


Finings, 


The  best  isinglua  comes  from  Kuasia,  but  a  very  large  supply  from 
the  Unizils  ;  thai  used  by  hrewprs  is  the  carlilagi;  of  the  sturgeon  and 
other  fii^h.  Tbu  brewer  buys  it  as  iniporteil,  in  rough  piec^'A,  fts  al^i 
the  iirt'ssin^s  and  pickings  rejected  in  tiie  preparation  of  tlie  finer  oorta 
of  iainglusa  ibr  the  eonfectioner,  &«.  The  *' finings"  for  porter  are  thus 
prepared:  —  Tbt*  isinglass  is  put  into  t>ume  sour  beer  to  dts^nlve,  tech- 
nic-ully  to  cut,  which  takes  place  in  diHerent  limes,  accortiiug  to  the 
kind  of  iiiinglass  maiie  u^e  of. 


H 


On  TtiK  Adultrrationb  or  Fortes. 


™«^^ 


I 


^Xc  have  nnw  to  flesifribc  the  state  in  which  the  national   bevei 
nacRt  more  piirtirubirly  poritr  ami  *AtK/,  rciiches  the  oonHUUier.     Lik< 
the  other  urticles  which  have  engaged  our  attention,  it  is  of  course  ^_ 
adulterated.  ^M 

The  receipt  or  formula  accunlin^  to  wbieb  the  majority  of  articlev^l 
of  consumption  are  adluliteniteJ,  is  an  exceedingly  simple  one. 

First  there  is  sonielhiiiir  a<lded  to  augment  the  weiglit  and  bulk  of  the 
article;  Uieii  somethiiii^  tu  restore  the  j^fst  colour;  and  lastly,  Houietbing 
to  give  to  tbe  adullciruted  attd  weakened  couifMiund,  us  far  us  possihJe, 
the  taste  and  quulitie.*^  pij»sff«*ied  by  the  genuine  commodity. 

It  is  ai^eitrdiii;^  to  this  formula  ibat  porior  and  stout  arc  odultersted; 
first  water  h  added  to  increiise  the  bulk,  and  then  treacle^  ns^or,  uid 
*a//,  to  restore  the  colour  and  llavuur. 

The  ditutinn  of  the  beer  makes  it  less  intoxicating,  and  henc«  the 
occasionid  use  of  a  variety  of  the  other  articles  intended  to  impart  lo 
it  the  semblance  of  strength. 

JtexultM  of  the  Examinntion  of  SampUn, 

The  results  nf  the  chemical  examination  ol   Fifty^two  samples  of 
gtont  and  porter,  there  being  ihirty-iwo  of  the  former  and  twenty 
the  bitter,  proeoreil  both  fnmi  brewers  ami  publicans  were: — 

That  thesiiiiiiilesof  STOirr  either  ol>tained  from  aginL-t,  or  purchi 
at  the  taps  of  several  ni'  the   priiicipu]   Lnndnn  porter  brewers,  wi 
con^iderubly  stronger  than  those  prt>cured  frtun  publicans;  tbe  ulcoUc 
of  specific  gravity  'TOtJ,  temperature  60"^  Fahr,^  eontainol  in  the  former 
samples  ranged  from  7  12  per  cent,  the  highest,  to  4*6.0  the  luwesc 
whereas  that  ul'  tbe  stouts  procured  from   publicans  varied,  with 
exception,  from  4'87  per  cent,  to  3*25  per  cent.  _ 

That  the  same  diti'erence  of  strength  aUo  characterised  the  various 
bomplcs   of  i*oKT£B  procured  from  the  two  didercnt  sources ;   the 


of 
ty^ 

ohoI^H 
"uicr 

"^ 

mil*  1 


PORTER,   AND   ITS   ADULTERATIONS-  307 

amount  of  alcohul  in  the  porters  obtained  from  the  tfljw  varying;  from 
4  51  por  rent.  In  2*4*2  per  cent. ;  whereiis  thosti  purchased  of  publicans 
ran^rvd  from  3  ^7  per  cent,  to  ISl  per  cent. 

That  in  nearly  ull  the  stouta  and  purterii  tall  was  preaent,  often  in 
considerable  amount. 

That  in  some  of  the  saniplea  ctaie  sugar  and  treaeU  were  likewise  pre- 
sent. 

<irc&t  aa  was  the  variation  in  the  streni^th  of  the  different  samples, 
arising  mainly  from  diluflon  with  ivater^  there  m  no  doubt  but  that  if 
the  porter  and  stout  hail  been  procured  ilircct  Irnm  ihc  brewers,  in 
plucc  of  from  the  public  bouses  known  at>  brewers' tapfi,  the  di^erence 
would  have  been  Ibuiid  to  be  dill  (jroater. 

Such  is  the  simplest  tnrm  whirli  the  adulteration  of  these  heveragca 
UBUmes;  not  unfrcrpiontly  it  takes  a  more  complicated  and  serious 
form. 

In  some  cases  sulphate  of  iron  is  Ofldedt  especially  to  stout;  it  is  said 
to^ive  the  beer  a  head  :  it  of  c(mrse  nmkes  it  more  tonic  and  streugih- 
eoin^,  but  sulphate  of  iron  is  &  tonic  whiuli  di>e8  not  suit  all  persons; 
nnd  if  it  is  desirHble  that  we  should  tiike  it  at  hII,  since  it  U  a  medicine, 
it  is  mo-it  pro|ier  that  it  shook!  be  administered  in  suitable  cases  hy 
the  phy.-iician,  and  not  by  the  publican  or  brewer. 

Other  substances  sometimes  used  in  the  adulteration  of  beer  are 
bittern^  and  earmiuaticet  of  variouit  kinds,  as  geutian^  qnwiiia,  camomiU^ 
ginger^  coriander  and  caraway  seeds,  capsicum  and  grains  of  paradise, 
aa  well  as  liquorice^  alum^  and  suiphun'c  acid,  satis  of  tartar,  carbonate 
ofiofiii,  ctKCttiusiwiicits^tknti  tobacco;  it  is  even  alleged  tliut  optum  taid 
ttrvchhi/te  have  also  lieen  employed  fur  the  same  purpo^ie. 

Mr.  PliillipA  furnished  the  Committee  with  the  lullowing  informa- 
tion in  regard  to  the  adulteration  of  beer  :  — 

'*  It  is  chiefly  common  wdt  and  sulphate  of  Iron  that  are  used  for 
adulterating  beer,  and  alwi  quassia.** 

Mr.  KdwMi  \Vickham*8  cviilenoe  was  to  this  effect  :^ 

"From  niy  exjwrience  in  brewing  I  believe  that  ihejrreat  adulteni- 
liim  of  beer  takes  plai'e  in  the  cellars  of  the  |)ublicans  and  not  in  the 
breworie-,  ohhoui^b  I  know  it  is  done  by  some  brewers.** 

Mr.  Sehote^eL  "  Do  you  believe  that  The  a^lulteration  of  beer  is  a 
common  thin^?" — "Very  common,  so  much  so  that  the  exception  is 
nut  to  adulterate;  and  I  believe  th<>t«e  exceptions  are  very  few.'* 

Mr,  Mickham  gives  the  t^)l)nwin^  us  the  receipt  in  frequent  use 
anionifst  publicans  for  the  ailulicration  of  porter: — 

**  lo  one  barrel  of  porter  eij/hti^Qlluns  ot  water,  six  pounds  of  sujrnr, 
one  pound  of  gelatine  (nr  patent  size  will  do),  a  handful  of  cutumun 
salt,  extract  of  gentian  or  quassia  to  restore  to  it  the  original  bitter 
flavour,  sulphate  of  ommonia  to  brin(£  it  back  to  ils  colour,  liulf  an 
ounce  of  sulphate  of  iruni  and  if  require*]  to  taste  uldiftlv  an  ounce  of 
roche  ulum.** 

Again  .Mr.  Wtokham  slates,  "  I  have  known  single  instances  of 
tobacco  being  used  in  b^r.'* 


[  tobacc 


506  PORTER,  AND   ITS  ADULTERATIONS. 

Mr.  P.  L.  Simmonds,  in  evidence  before  the  Parliamentary  Coi 

niittee.fttfttcfi,  lliut  **  at  least  250  tons  of  eoccvlut  indicHS  are  annually 
iiiiported,  chiefly,  I  ^UJl^K>8t?,  for  th«?  use  of  bruwers." 

He  further  states^  "  that  frfim  200  to  300  tons  o!  tlie  hot  acrid  seeda  of 
cardunioms,  or  graiiHof  paradise, are  nUonniuifilly  imported,  and  chietly 
used  to  give  an  artiHuitil  strength  to  bot-T  and  spirit*."  Also  that 
"ccvcculiiH  iiidianti  ts  couimoidv  inlrodMrud  into  beer  for  the  purpOM 
of  giving  n  false  strength  to  it.  In  one  case  which  came  under  mj 
knowlt'dgc  the  piiblicun  wii:^  found,  using  it  fur  the  purpose  of  adulte- 
rating liia  beur  to  be  sold  the  nest  day.'* 

Mr.  Gay,  in  ihe  evidence  before  (pioted  from  more  than  once,  gave 
the  following  infurmution  in  regard  to  c(»C(:ulus  iudicus:  — 

Ue  states,  "I  have  ground  many  owts.  of  coeculus  indieus." 

Mr.  Miiffatt.  "What  is  it  used  for?"— "I  suspect  logo  into  the 
poor  man's  drink." 

"For  whom  did  you  grind  cocculus  indieus?** — **For  wholesale 
druggist*." 

]Slr.  tiodgers  alleges  in  bis  evidence  that  "  cocculus  indious  can  be 
obtained  from  the  hrewers*  druggists  under  the  name  ofiiiuZ/um.** 

Mr.  Simmunds  also  makes  this   tuniark  in   his  evidence,   **  In  l 
suburbs  of  I^undoii,  I  may  mcntinn  that  it  \%  a  common  practice  with 
llie  puhliaui.'i  to  adttltenue  beer  on  Saturday  nights  much  more  than 
on  othop  ni^hlit." 

He  likewise  deduces  the  inference  that  beer  is  extensively  adulte- 
rated, from  ihe  following  siatislicaJ  particulars:  — 

**  There  is  dtie  matter.'  he  observes,  "which  (»ccurs  to  me  as  being  ex- 
ceedingly singular,  which  i^,  that  the  cimHumptinn  of  mult  and  hops  con- 
tinues) stfitiuuury,  though  the  cun^umplinti  of  beer,  wilh  the  iiicreastog 
{Kipulntion,  must  havu  incrua*eil  very  largely.  In  the  last  fifteen 
years  there  has  been  scarcely  any  varia.ti*m  in  tlie  amount  of  ho|)s  con- 
sumed, and  M>me  substances  inu)*t  therefore  bo  used  very  extensively 
to  miiku  up  the  diflerence.  The  extent  of  land  under  eultivntinn  for 
hops  ill  the  last  three  years  has  averaged  50,000  at^res,  Iwing  only 
7,000  acres  beyond  the  culture  of  30  years  ago.  The  h'^me  produc- 
tion tn  the  lust  10  years  had  scarcely  increased  at  uU,  and  yet  the 
shipments  of  beer  and  ale  have  mure  than  trebled  in  value,  and  tbv 
home  consumption  must  neeessarily  have  increased  also." 

Another  fact,  proving  the  extensive  practice  of  adulteration  in  beer, 
is  related  by  Mr.  Wickham,  in  reply  to  a  (jue>*tioii  by  Mr.  Swift: — 

"  Is  it  not  customary  for  publicans  to  sell  the  beer  at  the  price 
which  they  pay  to  the  brewei-s,  so  that  this  adulteration  forms  their 
actual  profit?" — "Yes,  many  publicans  do  so." 

It  appears,  from  the  analyses,  that  salt  is  almost  constantly  prcsen 
in  porter.     This  a<Mittim  we  know  is  unide  in  the  first  instance  by  the 
brewers  themselves  ;  but  theie  is  also  no  doubt  that  a  furlher  qunniiiy 
of  it  is  fre«{uentlv  u»ed  by  the  publican  to  iisslst  in  bringing  up  the  davuur 
of  beer  which  has  been  rciluocd  in  strength  by  the  addition  of  water. 


ith  ^^ 


^   PORTER,  AND  ITS  ADULTERATIONS. 


509 


The  quantity  of  salt  cantiiiii^il  in  porter  is  often  sufficiently  larjjc  to 
commuiiiuite  n  perceptiblv  sulirie  mate  t<>  the  mouth.  The  suit  is  used 
by  the  brewers  in  the  fulhjwhij:  manner:  —  It  is  first  mixed  up  in  a 
tub  with  some  kind  «i'  flour  —  usually  wheut  tiuur  —  antl  the  uiijituro 
i»  cnst  hy  h.indfiilsover  ihe  surface  of  the  wort  in  the  cooling  vat.  U 
IS  «aid  to  assist  in  the  preserviiikm  nnd  finin;j  of  the  wort,  and  it  it 
ollef^Hl  thitt  these  are  toe  only  purixwes  for  which  it  in  employed  by 
the  brewer. 

>rr.  Morris,  who  wrote  u  book  entitled '*  Brewing  Malt  Liquors" 
some  years  since,  describes  and  reciMiimends  a  variety  uf  articles  to  be 
employed  in  the  brewing  of  beer  and  porter,  as  colouring,  coceuliis 
indirus,  swi^>t  Hag  hk)!,  qims^ia,  coriander  seeils,  cnpsiruni,  earuway 
seeds,  grains  of  paradise,  ginger,  beans,  oyster  shells,  and  alum.  "The 
colouring,"  Mr.  Morris  reuiark«,  "giv&s  a  gooil  face  to  the  beer,  an*l 
enables  you  to  gratify  the  sight  of  vour  diflferent  customers."  And 
again,  "  Beans  tend  to  mellow  malt  liquor,  and  from  their  properties 
add  much  to  its  inebriating  qualities  ;  but  they  must  not  oe  used  in 
too  large  a  quantity.  Oyster  shells  are  very  good  to  recover  sour 
beer." 

"  Alum  is  geuerally  put  into  the  vat,  as  it  givea  the  beer  t  smack  of 
«ge.'* 

"Cocculus  indicus  is  uf>e<1  as  a  substitute  for  malt  and  hops,  and  is 
a  grcfit  prescr^'alive  of  mnit  liijimr.  It  prevcnis  second  iVrmentation 
in  bottled  t}eer,  and  consequeiitlT  ilie  bursting  of  the  bottles  in  warm 
climates.     Its  effects  are  of  tin  iuebriiiting  nature.'^ 

Another  writer,  Mr.  Child  *,  aUo  the  author  of  a  work  on  brewing 
porter  which  went  Lbruugh  eleven  editiom^  gives  the  Ibllowing  receipt 
for  porter :  — 

1  quarter  of  malt. 

8  lbs.  of  hups. 

9  lbs.  of  treacle. 

8  lbs.  of  liquorice  rooL 

8  lbs  of  essentia  bina. 

B  lbs.  of  colour. 

Capsicum,  half  an  ounce. 

Spanish  liquorice,  two  ounces. 

Cocculus  indicns,  n  quarter  of  an  ounce. 

Salt  of  tartar,  two  drachma. 

Heading. 

Ginger,  three  ounces. 

Lime,  four  ounces. 

Linseed,  one  ounce. 

Cinnamon,  two  drachms. 


Th« 


MMDtia  bina,  be  itatet,  **  is  compounded  of  8  lbs,  of  moist 


*  ChUilon  Brawlni  Porter. 


ftU» 


PORTER,  AND  ITB  ADULTERATIONS. 


nrC 

qr*. 

Ibft. 

1 

2 

0 

0 

0 

6 

0 

0 

30 

CWl. 

qrt. 

nw. 

2 

0 

0 

0 

0 

4 

0 

0 

28 

0 

0 

6 

FUpar,  bniled  in  an  iron  vMsel,  for  no  copper  one  could  withstand  the 
hcul  sufBcieutly,  till  it  c^imejt  to  a  tbick,  syrupjr  consistence,  perfectl/ 
black  and  extremely  bitter." 

Colour  *^  is  composed  of  8  lbs.  of  moist  sa^r,  boiled  until  tt  obtains 
a  middle  state  between  bitter  and  sweet,  niid  which  gives  to  porter 
that  mild,  mellow  colour  usually  sn  much  admired." 

The  beadint!  "is  a  mixture  ofhiilf  alum  nnd  half  citppenu,  jrround 
to  a  fine  powder ;  and  is  so  called  from  ;;iviii;;  to  |»orler  the  beautiful 
head  of  frolh,  whicli  constitutes  one  of  its  peculiar  properties,  and 
wliich  landlords  are  so  anxious  to  raise  to  gralify  their  customers." 

Other  receipts  by  Mr.  Morris  arc  as  follow  :  — 

Mall,  25  quartert. 

Hops      -  -  -  . 

Cocciilua  indicus  berry 
Lejiliorn  juice 
Porter  extract 

MaU^  20  quarters. 

Hops      -  -  -  - 

Cocculus  indlcus  berry 
Sujsnr  -  -  - 

Pabia  amara  (nux  vomica) 
And  also  the  following  directions  :  — 

T^i  make  up  a  Vat  of  IfiO  Barrels. 

"  Use  half  a  barrel  of  colnuring,  a  qunrtcr  of  a  hundredweight  of 
cream  n^  lartiir,  a  quarter  (»f  a  liunrlreilwei^bt  of  ground  alum,  one 
pound  of  sail  of  steel,  and  two  barrclfi  of  strong  finin;j;s.  Mix  these 
well  lo}!Ctlier,  nud  put  them  in  a  vat,  rousin;;  it  thorouphly  at  ibe 
same  time.  Lut  the  vat  rumuin  open  three  days,  then  close  it  and 
sand  it  over. 

"  It)  u  fortnight  it  will  be  fit  for  use  — your  own  good  len&e  will  in- 
form you  bow  to  employ  it  to  advanlnRe/* 

The  extensive  employment  of  viirinus  driips  for  porter  brewing  led 
to  the  esubliflhmfnt,  ut  almut  the  fieriod  of  the  late  French  war,  of  a 
class  of  men  Icrined  "brewers' dru^jjists."  These  persons  issued  rejru- 
liir  price  currenis.  and  they  made  it  their  business  to  send  travellers 
all  over  the  country  with  limits  and  samples  exhibiting  the  price  and 
fjuidity  of  the  articles  manufiK-lured  by  tlicm. 

Mr.  At'cum  •  states  that  ''their  trndc  spread  fjtr  and  wide,  but  it  was 
amoiig*it  the  country  brewers  cUii'tly  that  ihey  found  the  most  custo- 
mers, and  it  is  amongst  them,  up  to  the  prcfient  day,  as  I  am  assured 
by  some  of  tliese  operators,  on  whose  veracity  I  can  rely,  that  the 
greatest  quintitica  of  unlawful  ingredients  are  soIiL" 


•  A  TnmtlH  on  the  Adulieritlon  orFood,  p.  \H 


PORTER,  AND  ITS  ADULTERATIONS. 


;u 


**  It  was  at  the  same  time,  also,"  writes  Accum,  **  tliat  a  Sir. 
Jai-kson,  of  notj^rious  memory,  fell  upon  the  idea  of  brewing  beer 
from  various  drug*  without  any  malt  nml  hops.  This  chemist  lYul 
not  turn  brewer  liimself,  hut  he  utruck  out  the  more  profitable  trade 
of  tcachitii;  hia  mystery  to  the  brewers  for  a  hnndsomc  fee.  From 
that  lime  forwards,  written  directions  and  receij)t-books  for  using  the 
cbemicid  prepnrati^ina  to  be  subalituled  inr  malt  mid  hops  were 
re-«]K'i:tiveIy  s'obi  ■  and  many  adepts  soon  afterwurds  afipeared  every- 
where III  iiistruet  breweni  In  the  nefarioujt  practice  first  pointed  uuC 
by  Mr.  Jm^kson.'* 

The  folhjwiiii:  remark,  contained  in  Dr.  Normandy's  work,  entitled 
*' Coranierciul  JIandbook  of  Cheniieal  Anidyais,"  would  lead  us  to 
infer  that  the  fraternity  of  brewers*  druggists  is  not  even  yet  ex- 
tinct i — 

*'  It  is  &  publit^ly  known  fact,  that  carts  may  be  Bcen  bearing  the 

inscription,  in  staring  paint,  of  'C ,  brewers'  drugpist.'     Sueh  a 

cart  I  have  myself  seen  a  few  days  ago  standinjr,  in  the  broad  light  of 
midday,  before  a  publican's  shop  nr  ^in  palace." 

Some  idea  of  the  extent  to  whieh  porter  is  adulterated  may  also  be 
formed  from  the  two  following  cfreumstiinees  :  — 

Thus  it  has  been  fhown  before  the  Parliamcntarv  Committee 
on  Public  Houses,  on  the  clearest  evideuee,  that  it  is  quite  impossible 
fur  a  publican  to  realise  any  profit  by  the  sale  of  beer  without  having 
rt'course  1o  adulteration. 

Again.  Mr.  M'C'uIloch,  a  witness  before  the  same  Committee,  not 
only  deposed  to  the  fact  of  tiie  extensive  adulteration  of  beer  by 
puliliciins,  but  he  alno  cjttiniafed  the  loss  to  the  Atate  ari^in^  out  of 
that  adulteration  at  100,000/.,  in  consequence  of  the  diminished  con- 
Bumptiun  of  malt. 

Not  only  is  beer  itaclf  adulterated,  but  frequently  the  very  mate- 
rials, out  of  which  it  i»  niade,  are  also  adulterated,  as  tbe  hops  and 
malt. 

On  the  AtbtlteratioH  of  Hops. 

Tn  regard  to  the  adulteration  of  hops,  Rfr.  Geortre  Phillipn  gave 
the  following  information  before  the  Conimtltee  on  Adulti>ration  :  — 
"  Mr>8l  of  the  40  samples  of  bops  I  liave  spoken  of  contained  prnins  of 
paradise ;  lu  oue  instance  we  had  c<mjl'uIus  indicua,  but  only  in  one 
instJince.** 

These  40  samples  of  hops  were  examined  by  the  Exci^  in  twelve 
years,  und  out  of  them  35  were  found  to  be  adulterated,  the  substances 
met  with  being  cooeulus  indicus,  gruin^  of  paradise,  quassia,  chiretta, 
gentian,  camomile  llowera,  coriander  seed:),  and,  in  one  instance,  ex* 
bausicd  tobacco. 

On  the  Adulteration  of  Mali. 
Barley  is  sometimes  substituted,  to  the  great  loM  of  rerenue,  for 


512  PORTER,   AND  ITS  ADXTLTERATIONS. 

malt.      For  further  information  in  regard  to  this  flubstitidiii  At 

rtiadcr  is  referred  to  pp.  50*2.  and  5\4, 

The  rcmetiy  by  which  the  adulteration  of  malt  liqaors  maf  bctafl 
apptiarH  to  us  to  1>^  hl-Iviu-  und  simple,  and  it  is  one  to  vhicn  «r  r?- 
cc'iilly  Ljid  the  i  ])portii(iity  of  directintr  the  attention  of  tb?  l^*** 
niittee  of  the  Ilnuae  uf  Cnnimons  on  Public  Houses;  it  ia,  fio'  m 
wait  iif/uors  should  he  pf^rinitteii  to  be  sold  by  iiny  pHltUcan  madtr  etr' 
tfiin  Jiitd  or  standard  ntreiigths,  the  t«Mj)  of  strcnj^  beifi^  wt  tW 
itpccilic  ifrnvH^  of  the  beers,  hut  principatlj  the  amount  nr  perceaL 
ago  of  alcohol  eontainod  in  them. 

Such  a  regiilalMm,  hropL-rly  enforced,  would  ofTectuallY  p«t  %\ 
to  the  ailuhcrutiint  til  ninlt  li<[u<irs  by  the  nd«li(ion  of  waur* 
salt,  and  most   of  the  other  oubittances  mentioned    in  tJti« 
report ;  imd  it  need  not  in  nny  way  interfere  with  the  differeitfl 
cognised  strcn<;ths  and  qualities  tif  mall  liquors  now  in  ujc,  at  tffit 
and  double  stouts,  ales,  and  porters. 

On  the  Detectiom  of  the  Adulteralioju  of  Pcrier  ohI  ^mL 

The  specijic gravity  nf  the  beer  phould  be  ascertained^  and  then  itMP* 
/i(7^,by  means  of  a  solution  of  ttni-d  carbonate  of  soda  of  known  itna^ 
The  porter  should  next  1>c  ftiihmilio-d  to  diKtiltation,  ustni^  abmrt^lMV 
grains.  It  is  necessary  that  the  ticetic  acid  of  tiie  porter  abii^  ht 
neutinlincd  previous  to  distillation,  otherwise  it  will  pman  owr  «fA 
tb(j  alcohol^  and  so  affect  the  quantity  and  speciSe  gravity  of  ik&r* 
tilled  liquid.  It  is  also  advisable  that  fully  two  thirds  of  tin  I«7v4 
be  distilled  uff,  otherwise  some  of  the  spirit  will  remain  behind.  11  (* 
easy  to  convince  oneself  that  this  is  really  the  eain;,  eiiUer  by  ilislflSaf 
three  separate  pints  of  the  sume  porter,  taking  off  different  qaaalilai^ 
or  by  removin<rthe  product  of  thi*  distilhition  of  tbe  siune  mmfk  tt 
three  ditTeriMit  periods,  when  spirit  will,  in  most  rosea,  be  fmuuBW 
present  in  the  lost  us  well  aa  in  tbe  first  portion  of  liquid  which  eamm 
over,  although  of  course  in  greatly  diminbhed  amount. 

Another  meuiiuriMl  portion  of  the  porter,  say  3^00  p^ni.  fthoaU 
next  l>e  tiiken,  and  the  gam  and  sugar  in  this  determined  in  iWfi^ 
lowing  manner  :  — 

The  gurn^  together  with  other  matter,  «hou1d  b<!  fn-ecipitatrd  fcf 
aubacetate  of  lead  ;  the  migar  reinainii  in  solution.  The  fluid  ptfS 
is  to  be  separated  from  the  solid:  this  is  best  etTected  by  decaaiibift 
and  the  addition  to  the  prccipitst**  of  small  quantttiM  of  dadU 
water.  Af\er  separation,  the  lead  in  each  is  to  be  g^t  rid  of  by  oflMi 
of  sulphuretted  liydn>};en,  care  being  taken  to  use  a  water  laCtl^ 
or  some  of  the  iron  of  the  sulphate  of  iron  uaed  for  obtAJnia(  A^ 
sas  will  pass  into  the  solution.  We  have  now  obtained  two  tit0 
liquids,  the  one  holding  chiefly  gum  in  solution,  and  the  (HbcruflK. 

Tliese  are  next  carefully  evaporateil  —  the  sugar  over  a  water  Wik 
until  it  ceases  to  lose  weight — the  gum  until  it  becomes  oenrly  tJUk 


PORTER,   AKV   ITS   ADULTERATIONS. 


513 


when  it  should  be  treated  with  a  liltt«  alcohol,  dried  and  wcijrhcd. 
Ftnailj,  both  the  sugar  and  the  gum  should  be  incinerated,  aud  the 
ash  deducted. 

Another  portion  of  the  porter,  equal  to  the  above,  should  be  eva- 
porated to  drrncflB,  and  the  weight  of  the  extract  detennined;  thiH 
should  BfYcrwards  be  burnt,  the  a:»h  weighed,  and,  ifneccssarr,  tested 
ibr  Bait  and  iron. 

The  several  resuUs  thus  obtjttned  are  all  lobe  calculated  to  the 
imperial  gallon  of  70,000  ^ruins. 

The  taste  of  the  ush  ia  usually  sufBeicnt  to  betray  the  presence 
of  50//,  and  *itii  colour  that  of  iron.  From  experiments  made,  we 
have  a.scerlained  that  when  suljtliate  of  iron  U  present  in  porter,  in 
as  small  n  iptantity  aa  two  grains  to  tho  nine  gallons,  the  well  burned 
ash  of  the  extract  will  be  found  to  be  more  or  less  coloured  with 
the  red  oxide  of  iron.  This  i»  n  very  delicnte  means  of  derei mining 
the  presence  of  iron  in  piirter;  and  if  iron  in  the  above  small  cjuan- 
tity  be  found  in  it,  tliere  will  he  every  reason  for  susfiecling  that 
sulphate  of  iron  has  been  itdded  to  the  beer;  for  the  ash  of  jienuine 
pnrter  extract  is  never  in  the  8li;ihte8t  degree  cnluured,  but  is  alwaySi 
when  well  freed  from  carbonaceous  matter,  either  white  or  greytsh 
white. 


On  the  Deiectiam  of  Bitiers,  Carminatit>e$^  S^c^ 
The  detection  of  many  organic  substances  sometimes  employed  in  the 
adulteriuion  of  porter  and  beer  is,  in  most  caaes,  a  matter  of  extreme 
dilficuUy,  and  in  others  it  is  altogether  im[>ossibIe  in  the  present  Btat« 
of  Rcience. 

The  following  is  the  general  methoil  of  proceeding  for  the  dipcovery 
of  the  hittern^  carmiuaiivtM^  and  acrid  suhHtaueei  employed  :  — 

The  extract  of  about  3000  gmina  of  the  porter  or  beer  ia  to  be 
treatc<l  with  boiling  alcohol,  the  alcoholic  decoctitm  is  tu  l>e  evapo- 
rated, and  the  extract  tnsted ;  the  presence  of  many  of  the  articles 
used  will  be  sufficiently  apparent  by  the  tnste.  This  is  especially  the 
case  with  the  hot,  pungent,  and  acrid  substances  used,  as  well  as  most 
of  the  bitters. 

On  the  Dittction  of  Cocctilus  Indttu*. 

One  of  the  mn^t  injurious  of  the  sab»tance9  ndded  to  beer  is  the 
extract  prepared  from  the  seeds  or  berries  of  coccuIh.%  ituiinu.  Its 
detection  in  beer,  and  especially  in  [>orter,  is  all  ended  with  very  great 
difCcuUv ;  imd  in  inuny  caseft,  when  employed  in  small  quantities,  it 
cannot  be  discovered  by  any  known  means.  Dr.  llcrapath  has  re- 
cently published  the  results  uf  some  experiments,  instituted  with  the 
view  of  detcrmiiving  the  presence  in  beer  of  picrotoxiity  the  active  and 
poisonous  principle  of  cocculus  indicus.  lie  directs  that  the  beer 
or  porter  should  be  first  treated  with  excess  of  acetate  of  lead,  so 


5U 


PORTER,   AND   ITS  ADULTERATIONS. 


fts  to  throw  down  all  gum  und  colouring;  matter.    The  dear  liq- 

u  then  to  be  Beparato<l  by  filtratiun,  and  the  excess  of  laad  prosipi* 
tated  by  sulpburetlt^d  li^drn^'t;!!.  AfUT  standing  Tor  sonic  time,  or 
boiling  90  aM  to  get  rid  nt'  uncuoibined  sulphuretted  brdrtigcn,  it  it  ti* 
be  liltenid  again.  Tho  Hqutir,  thus  obtained,  is  to  W  te^^ionttd 
at  a  mo<leratc  temperature  until  it  becomes  rulher  thirk,  aad  iWn 
trente<l  with  a  little  pure  animal  charL*oat.  After  sUinding  for  me 
time,  thn  charcoal  is  oollectci  on  a  filter^  waahed  with  Tcry  link 
water,  and  dilL-^d  at  a  steam  beat.  The  charcoal  contains  the  pier^ 
toxin,  which  may  be  separated  by  boiIin;cr  with  a  litlle  purt  tJicobd, 
filteriu};,  und  evaporating  to  dryness  on  slips  of  ;;ld»^.  It 
niaed  by  its  forming  plumose  tutU  of  acioular  crystala,  or  ebt 
shaped  forms. 

M.  Laaaaignc  has  statcl  that  picric  add  is  sometimes  aacd  to  i 
a  bitter  taste  to  bc^r  and  porter,  and  that  it  may  be  thus 
He  finds  that  this  aubsltuice  is  not  precipitated  by  siibacetate  of  In^ 
whicti  throws  down  most  of  the  other  colouring  maiters  of  beer,  tt 
welt  as  the  bitter  principle  of  liops  and  also  thnt  it  19  not  absorMlf 
common  bone  cliareoal  thoroughly  puri5ed  by  uciJs.  By  uilimm  Of 
one  or  other  nf  thcM  substances,  he  succeeds  in  obtaining;  a  lAltfiUr 
pure  snluLion  of  picric  acid.  M.  Lassaigne  states  that  while  purvbicr 
IS  alinoHt  entirely  decolourised  by  either  subocetate  of  lewd  or  piin6e4 
bone  chnronnl,  beer  adalternted  with  the  one  twclve-tbousjindtiicr  rrfl 
tho  one  eighteen -thou.'*anikh  purt  of  picric  acid,  remains  of  a  ydls* 
citron  colour.  Supposing  the  beer  to  contain  a  still  more  maatK 
quiintity  of  picric  iicid,  it  must,  subsequent  to  the  use  uf  imeor 
of  the  above  substances,  bo  evaporated  until  the  yeUow  citron 
is  produced.  It  is  possible  that  by  the  above  method  picrw  wi 
might  be  detected  in  poor  &nd  prtle  beers,  but  we  very  much  AaH 
whether  it  would  be  successful  in  the  case  of  London  stout  and  porter, 
ivhieh  lire  not  entirely  decolourised  by  cither  subacetate  of  leadsrf*" 
rifipd  charcoal. 

The  presence  of  cocculus  indicus  may  sometimea  be  d«t«rafa«lfcr 
the  cfTecta,  produced  upon  animals,  binis,  and  fishes,  of  tbe  afcohav 
extract  of  toe  beer  containing  thai  narcotic. 

The  process  for  the  detection  of  itrychuine  in  beer  will  be  htA 
describe<l  under  the  head  of  Ale,  and  that  fur  opiufn  in  oivaiitc  Btf- 
turea  under  that  of  Cijzars. 

On  the  Detection  of  the  Adutieration*  of  Hop*.  —  The  ttreral  tit. 
stances  elsewhere  enumerated  as  having  been  discnrerecl  in  hopa,| 
all  he  resdily  discerned  frequently  by  the  eye  alone,  and  in» 
by  the  microscope.     The  structure  of  Nirdamom  snd^  or  grwitt 
paradise,  which  is  the  article  most  frequonlly  employed,  will  oc  Al 
described  and  figured  under  the  head  of  Curry  Vowder. 

On  the  Drtecttnn  of  the  Adidierationt  of  Matt.  —  'JTie  admatazf  ^ 
unnialted  with  malted  barley  may  be  discovered  on  a  can*ful  pmssL 
n«  well  OS  microscopical,  examination  of  the  grains}  thcgruniofask 


rORTEH,  AND  ITS  ADrLTEKATIONS. 


M3 


arc  white,  more  friable,  and  sweeter  than  those  of  raw  barley,  and  the 
celtulose  is  Ascertained  hy  means  of  the  mtoroseo^ic  to  have  beeomc 
desitroyed.     See  p.  30i. 

It  huTtng  b(*en  proved  thnt  beer  is  enormously  aduUernted,  let  us 
now  intjuiru  how  far  the  £xcise  protects  the  revenue  in  the  cuAe  of 
this  articU'. 

As  btu  been  shown,  malt  and  Aon«,  the  ingredients  used  m  brewing 
bepr»  are  both  adulterated,  as  is  oh-o  the  beer  itself. 

It  appears  from  the  evidence  of  Mr.  PliitlipH,  already  quoted,  that 
the  Excise,  with  its  70  chemists  au<l  -1000  inspectors,  in  the  course  of 
twelve  years,  have  exAmiDed  only  40  samples  of  Ao/v,  of  which  35 
were  adulterated. 

With  regard  to  wia//,  the  Excise  is  in  a  state  of  happy  ignorance,  as 
Bpp*j?ars  from  tlio  followin"  remiirks  of  Mr.  Fbillips  :  — 

Mr.Villwrs.  "  What  information  can  you  (live  us  respecting  maUP** 
— "The  fact  is,  we  have  been  in  5<mie  tlifficulty  about  that,  and  I  be- 
lieve we  have  arrived  at  a  mcuna  hy  whieti  we  ciin  detect  any  mtxiure. 
It  is  po:iaible  wc  may  have  been  defmuilcd  nf  malt  duty  by  the  mix- 
ture of  grain;  some  traders  assert  we  have  largely,  but  I  rannoi  say 
of  my  own  knowledge." 

"What  would  be  the  nature  of  the  mixture  ?*' — "  Chiefly  barley,  I 
suppose." 

The  Excise  is  but  little  better  informed  respecting  beer.  Of  1 139 
samples  examined  by  the  Kxcise  iu  twelve  years,  taken,  when  about 
Ui  be  ex]M>rtcd,  from  vessels  for  the  purpose  of  ascertaining  their 
prnvity  so  that  the  drawback  might  be  allowed,  that  scientific  body 
succeeded  in  discovering  adultcrution  in  only  twelve  tiamples. 

Such  is  a  summary  of  all  that  tbc.soienlific  department  of  the 
Excise  has  been  able  to  effect  in  discovering  adulterations  in  bops, 
malt,  and  beer. 

The  Excise  duty  on  malt  since  tbe  5th  of  July,  18^16,  is  3«.  8</^  and 
6  per  cenU  thereon  per  bushel.  During  the  war,  from  May,  1954,  to 
6u\  July,  18vi6,  it  was  4*.  per  busheh 

Since  tlie  l4llx  of  August,  1855,  malt  made  under  certain  regula- 
tion boa  been  free  of  duty  for  distillation*  which  will  account  for  the 
falling  off  in  quantity  in  Scotland  and  Ireland  particularly. 

The  quantities  of  nuM  retained  for  home  consumpUon  were,  in — 


Itu. 

iw. 

ItfiA. 

Nlam  ManilK  ^ 
1«M. 

SocitUnil    ... 
Ircltnd        .            -            - 

Uolted  KtD|dom  . 

4,ica,wi 

l,6W,fJ76 

Bmbtb. 

>,4ll,!i|| 
l,SS7.«77 

BiuImU. 

BiHlMta. 

ai.oi*.a!» 

B61.IB3 

4i,in,m 

l«,8ll,TI7 

»,«7»Jil 

njMjaii 

L   L  3 


516 


ALE,   AND    ITS   ADULTEUATIONS. 


The  Excise  duty  on  home  groitm  hops^  imposed  at  different ^ 

and  levied  an  the  old  and  new  duty,  is  toj^ether  2if.  per  lb.,  and  6  per' 
cent,  iliereon. 

Fnreis^  hops  pay  a  Customa'  tluly  of  45*.  per  cwt. 

Foreign  hops  imported   in    1«54,  119,040  cwts. ;    in    1855,  24,662 
cwts.    LntBred  for  liumt;  consjuniptioii  in  16^4,  102,100  cwts.;    18« 
30,020  cwta. 

The  (|uiintiiies  of  home  grown  hops  that  pnid  Excise  duty,  am 
were  retained  for  linmi*  coiisiiinplinn,  were  (vtTy  varying  acconlin* 
to  the  orupii) :  —  Kn^rUnd.  in  1  So.S.  aO,954,.'j'02  lb«. ;  in  1  aS-^ 
9.293,992  Iks, ;  in  1855,  82,368,30*>  lbs.;  in  9  numtlis  of  1856.  not 
known,  the  duty  bcin^'  nil  charged  in  the  lost  3  months  of  the  year. 
Seotland  and  Irt^lund,  none. 

Duty  nti  awcubts  imlicH^,  5$.  per  cwt. ;  extract  of  ditto,  20  per  cent. 
advuhrem.  Importedin  1854, 1,309  cwts. ;  in  I855,430i:wU.  Ketaiaed 
fur  home  consuinptinn  in  the  Brst  of  these  years,  161  cwts. ;  and  in  the 
iteeond,  44  cwts. 

Duty  on  grtiiKx  ofparadue^  ISa.  per  cwt. ;  extract  of  ditto,  20  per 
cent,  ad  valorem.  Imports  in  1654,  249  cwt9. ;  in  1855,299  cwts. 
Home  consumption  in  the  corresponding  years,  300  cwts.  and  245  uwts. 

Duty  on  mu  vomica^  *2s.  per  cwt. ;  extract  of  ditto,  20  per  cent  ad 
valorem.  Imports  in  1854,  370  cwts. ;  in  18d6,2l8J  cwts.  Honoe  con- 
sumption, GO  and  31  cwLs.  Kxlract  of  nitx  vomica  imported  and  re- 
tutned  for  consumption  in  18'?4,  4  cwts.;   and  in  1855,  5  cwts. 

Botfr  and  ale  of  all  sortsi,  mum,  spruce,  pay  duty  on  importation  of 
I/,  per  barrel. 


1 

I 


ALE.  AND  ITS  ADULTERATIONS. 


>n  oi    ■ 


Thb  adulterations  of  ale  are  for  tlie  most  part  the  same  as  those  of 
porter  audbet-r;  that  is,  their  strengih  a  often  roduce<l  by  water f 
and  the  majnrity  of  substances  enumerated  under  the  head  of  porter, 
aa  bitters^  carminatwes,  sulphate  of  iron,  &c„  are  used  to  rectorc  u^ 
parenlly  the  redxiced  strenwih  aii<l  ilavour  of  the  ale. 

The  alleged  adulteration  of  ale  with  which  rtur  attention  has  been 
more  jiarticulnrly  oocupk'd,  is  that  by  nirychnine.  The  following  arc 
the  circumstunces  which  indnccil  the  Ekiiior  of  "The  Lancet,  Mr. 
Wakleyt  to  undertakes  through  the  author,  a  very  extensive  and  ri- 
goroui*  inquiry  into  the  subject. 

In  the  year' 1850.  a  lieport  cume  before  the  public,  in  which  it  was 
asserted  that  the  deailly  poison,  stryihiiine,  is  comoionly  employed  by 
brifwers  in  the  manufacture  of"  bitter  beer"  or  "pale  ale.** 

The  following  was  the  origin  and  foundation  of  this  Iteport  i 

In  the  course  of  a  leclure  delivered  at  the  "  Conaervatou^  des  Arte 


ALE»   AKD  1T3  ABLXTS RATIONS. 


«ir 


et  llotiers,"  AI.  Pu>'cn  is  assorted  to  Iiuve  stat«;d  that  strychnine  was 
prepared  in  liLrf*e  qu.inlities  iti  Fari«,  uml  tbut  the  French  nudiorilit^ 
hud  asccrtiiined  that  it  was  destined  for  Knj^Iand,  it  bein;»  cMtpff^cd 
in  tbc  manufACturc  of  the  ciflcbraled  bitter  beer  uf  that  country. 

This  stAti-ment,  after  havin;,*  appeaivd  in  tiome  of  iho  French  papers, 
and  iimoiin:«t  others  in  tlie  "  ConMitutionnel,"  flitractcd  iheiittention  of 
Bunie  Kngtish  juurnnli.^t^,  who  c(rninicnted  at  >>ome  lengtli  tiputi  it,  in* 
cauti»U9ly  treating  the  atssertiun  an  thuugh  its  truth  had  been  fully 
lucertained.  At  length  the  injuiiouB  Btutementniade  its  way  into  tite 
columns  of  **  The  Times  "  newspaper,  and  thus  became  universally  dJa* 
seminated. 

It  was  impoasihlc  for  the  brewers  of  bitter  beer,  the  prcparntion  of 
whicli  is  confined  to  a  small  number  of  jtersnna,  to  pass  by  withuut 
notice  so  grave  a  charge,  and  one  so  immediately  affecting  their 
interests.  Accordin;rly  the  two  cbief  llrnis,  those  of  Messrs.  AlUopp 
and  Sons,  and  Messrs.  Bass  and  C«.,  U>st  no  time  in  publicly  tlenying, 
in  tlie  most  unef[uiTocal  terms,  tliRt  strychnine,  or  airy  other  dele- 
terious aubstonce,  was  ever  employed  by  Cbeia  in  the  manufacture  of 
their  beer. 

These  celebrated  brewers  suggested  that  their  bitter  beer  should  be 
subjected  to  a  searching  cheniind  and  niieroscopicul  examinulion,  and 
expressed  their  winin;£ness  lo  place  the  inquiry  in  the  hands  of  "  Tha 
Anidyiical  tiuniiary  Committsion."  They  olFerud  to  throw  o|»eii 
their  breweries,  stores,  &c.,  in  llie  must  eoioplete  and  unreserved 
ninnner,  and  afford  every  facility  fur  the  lulletiit  investigation. 

Feeling  that  the  subject  was  one  of  great  importance  ;  that  it  in- 
volved the  public  health  to  a  great  <Jogrce,  ami  also  llie  pecuniary 
interests  of  a  trade,  which,  from  it^  magnltmle,  had  almost  assumed  a 
national  cbarat-ter  ;  that  it  also  affected  the  judgment  of  the  medical 
profession  by  whom  the  bitter  beers  had  been  so  strongly  recom- 
mended—  Mr.  Wrtkley  ultimately  agreed  to  undertake  the  inquiiy 
ujMiii  the  distinctly-declared  condition  lliat  the  results  of  the  inves- 
tij^atioii  and  analyses,  whether  favoumble  or  un!avour;ib!e  to  the  t^- 
putiition  and  t|uulily  uf  the  beer,  should  hv  unreservedly  and  faith- 
fully communicated  to  the  public. 

The  importance  uf  the  subject  will  be  duly  appreciated  when  it  is 
recollected  that  strychnia  is  the  active  principle  of  mac  vcmicUt  that 
it  is  remarkable  for  its  intense  bitterucss  and  highly  poisonous  nature; 
one  sixth  of  a  grain  having  been  known  to  prove  fatal. 

In  order  to  put  the  statement  to  the  test,  40  samples  of  bitter  beer 
Were  subjected  to  analysis ,  twenty  of  the  ale  of  Mengrt.  Jiaaif  and  Co-, 
and  the  like  number  of  samples  of  the  ale  uf  Men»r».  AlUopp  and  Sons. 

They  were  all  found  to  consist  of  the  products  of  malt  und  hoju,  and 
the  constituents  of /jurff  s;p-i]i^  UKi/er;  no  other  ingredient  of  any  kind 
being  discovered,  cither  organic  or  inorganic. 

These  sampb-s  were  procured  under  circumstances  which  preclude 
(he  poasibUily  of  error,  lalkcyt  or  of  preparation  for  the  selection. 

L  L  3 


SIS 


ALE,  AND   ITS  ADULTERATIONS. 


I 


IVTuny  of  the  samples  were  tiikcn  from  tlic  stores  of  Messn.  AUvf^ 
ami  ^ons,  and  of  Messrs.  Bass  and  Co.,  at  Blacltwall  and  tntb«aff, 
whilti  otliera  were  procured  from  the  principtil  ngerits  and  KHiIertin 
the  iiietro|>olis.  In  all  cases,  the  utmost  fuoilitj  fur  inT»tig«liixi*> 
aflorded. 

Some  of  the  ales  were  destined  for  exportation,  otiiera  for  ll»e  io«« 
trade;  whilst  the  dates  at  which  they  were  brewed  ext«ndMi  ant  i 
period  of  ni>arlr  two  yaxTA.  Not  nny  sample  of  beer  analvicd  m 
brewed  after  the  promulgation  of  the  itatemeot  concenung  IheMi* 
ployment  of  strychnia. 

Tlie  stores  ut  BliiokwiiU  belonjrinj;  to  Messrs.  Bass  nnd  Gou  ««l 
Messrs.  Allsiipji  and  Sont*.  each  comprise  inaitj  tbouaand  butta,  boft- 
heiidtt,  and  barrels  of  bilter  Ijecr,  wliich,  arranged  in  lierp.  -■      ;  '  ' 
one  above  the  other,  extend  over  a  upace  of  several  acres,     i 
of  these  stores  were  thrown  open  to  us,  and  liberty  given  to  t 
ever  cask  we  lUose  to  select      In  the  case  nf  the  agerits  :ii 
the  same  liberty  of  choice  was  pennttted,  and  in  this  manner  lu..  -■•• 
butt  was  opt-ncd  and  snmpleii  taken. 

It  i^hould  be  observed  that  the  rodks  are  all  brandeil  with  iheasott 
of  the  brewers,  and  that  in  miKit  discs  a  re<;i!iter  is  kept,  nntoalj  u 
the  breweries  and  stores,  but  also  at  the  agents'  and  l>otllr?»*.  of  tU 
diites  u,t  which  the  (illT<jrent  h>t.H  were  brewed,  all  di&nce  of  raislakra 
the  select ioo  of  the  samples  being  thus  obviated  bj  relereoorlo  (he 
marks  and  rejiistries. 

Under  the  above  circurostnnces,  and  after  the  most  scrutiniflaf  *>' 
aminalion,  mlcnxwopical,  chemical,  and  physiido^ical,  we  bavf  uiU 
to  detect  llie  smallest  atum  of  strychnia,  or,  indeeil,  <if  any  nthfr  t&ipr* 
ditiits  than  the  products  uf  molt  aud  hops,  and  ibc  ouuatiianBt' 
pure  sprin;;  water. 

Unknown  to,  and  wholly  independent  of  ounelvea.  Mettn,  Gnki* 
and  llunimin,  at  the  retpii-'St  of  Messrs.  Allsopp  and  Sons,  aotjiHftJ 
several  samples  of  their  bitter  beer  to  nnalytiis.  In  their  poMiM 
report,  it  is  stated  that  they  failed  to  discover  tlio  tligblMl  lna<I 
strvchniu. 

Those  pentleinf-n  likewise  plact^d  tliom^elve*  in  cnmmuuicatifla  *itt 
AI.  Tayen,  with  whom  the  report  was  stated  to  have  origiuialB 
order  to  a.tcertain  from  himself  the  exact  nature  of  the  aMtealit 
advanced  by  him. 

It  appears  that  the  charge  made  by  M.  Payen  waa  foainlcd oa •* 
fonuulion  uhtuined  by  M.  Ftdletier,  the  celebrated  fireparer  of  i|Va* 
ami  other  alkaloids,  in  France,  who  at  one  time  receivett  ao  ttnirrfif 
a  lar|;c  tpiantity  of  strychnia,  the  destination  of  which  wa«  at  6rst  ■*■ 
known  to  him,  but  whicii  he  afterwards  found  waa  ex|M>rlod  to  Titf* 
land,  and  used,  so  he  informed  M.  Paycu,  to  eonplete  the  biuffav* 
of  certain  kinds  of  beer. 

^'  We  have  reason  to  know,"  write  Meanv.  Grakam  and  UftfioA 
^  although  it  ia  not  stated  by  M.  Fayea,  that  theae  remarks  of  ^ 


ALE.  AND  ITS   ADULT  EB  ATI  ON  8» 


519 


leh'er  refer  to  a  periofl  of  ten  or  Iwelve  years  past ;  and  farther, 
althimrrh  not  informed  of  the  amcHint  of  the  order,  we  have  goo<i  au- 
thority trt  state  that  fifty  or  a  Kuntlrcd  ounces  would  have  been  consi- 
dered a  lai  jre  order  for  fltrychnU  at  tlmt  time.  The  ealculation  already 
eivert  shows  how  utterly  insipnificant  such  a  supply  of  stryebnia  would 
be  for  its  inmgined  application  in  the  pale  ulu  breweries.  It  is  like* 
wise  known  that  the  nianufucture  uf  atrychnia  baa  not  been  on  Uia 
inoreaw'  In  France  of  late  years." 

Kinally,  M.  Payen  exprejiseil  his  regret  that,  he  had  ever  said  the 
fraud  appeared  tit  have  beim  practised;  althf)iij*li,  at  llie  time,  he  ac- 
companied this  obserraliifn  with  the  further  remark  tliat  Ike  falsijica' 
tion  had  no  doubt  ceased. 

M.  Payen  excused  the  statement  made  by  him,  on  thv  (ground  thai 
be  did  not  orif^inate  it,  and  that  the  ehur;;e  had  been  made  public  in 
til e  year  18jO,  in  a  French  work  treating  of  tlie  Adulterations  and 
FalKifiuations  of  Food.  We  have  procured  the  publication  in  ques- 
tion, and  find  that  it  refers  to  the  matter  rather  as  a  va^rue  and  un- 
certain report,  than  as  a  <ii^iiiict  alle^tion  of  the  use  of  strychnia  by 
Kn^liyh  brcwera;  the  author  tioneltiding  hia  remarks  on  tlie  subject 
in  the  following;  words  :  —  "  AVe  hasten  to  say  that  this  sophistication, 
liko  the  preceding,   i.^  far  from  being  ba5e<l  upon  ascertained  facts."  • 

Tlie  fftllowing  iire  the  condudin;;  paragraphs  of  the  Kejxjrt  of  the 
Analvticjtl  Siinitiiry  Cnminission  of**  The  I-ancet"  on  tJie  subject :  — 

"From  the  pure  and  wholesome  nature  of  the  ingredients  employed, 
the  modvmte  proportion  of  alcohol  present,  and  the  very  consid (Table 
quantity  of  aromatic  anodyne  bitter,  denved  from  hops,  cnnluliied  in 
tliese  beers,  they  tend  to  preserve  the  tone  and  vigour  of  the  stomach, 
and  conduce  to  the  re^loratioti  of  the  health  of  that  organ  when  in  a 
llate  of  weakness  or  debility. 

"  These  bitter  beers  differ  from  alt  other  preparations  of  malt  in 
contaiiiinff  a  smaller  amount  of  extractive  matter,  thus  being  less 
viscid  and  saccharine,  and  Gon»c(]ucntly  more  easy  of  direction  :  they 
resemble,  indeed,  from  their  lightness,  a  wine  of  imiU  rather  than  an 
ordinary  fermentctl  infuMion;  and  it  is  very  satij*f«ctc»ry  to  find  tliat 
ft  l>cverage  of  such  general  consumption  is  entirely  free  from  every 
kind  nf  impurity. 

"The  admirer?',  tliercfore,  of  the  bitter  beer,  manufactured  by  the 
celebrateil  brewers  wc  have  meniioniMl,  may  enjoy  with  advantage 
this,  their  favourite  beverage.  TLe  report  so  commonly  circulated, 
that  it  conlaiiieil  a  deadly  {H>i>on,  wns  u  severe  reHeetion  oti  the  saga- 
city and  judgment  of  (he  members  of  the  me<iical  pn>fe»si<'n,  becausP 
it  is  perfectly  well  known  that  *bitter  beer  or  pale  ale*  first  acquired 
and  afterwards  maintainetl  its  general  celebrity  in  consequence  of  the 
universal  recommendation  of  our  proCesi^iim  —  a  recommendation 
which  is  now  found  to  have  had  the  best  possible  foundation.** 


«  DicUonMlrc  An  AltfrAlioDi  cA  FsblficaUoai  del  Subttucca  AJImeotiilrei.  *c..  p- 1  !•• 
h  V  4 


«20 


ALE,    AND    ITS  ADULTERATIONS. 


It  may  be  well,  before  proceeding:  to  deacribe  the  ti-stji,  lo  «in- 
sider  how  far  the  stnteuient  made,  that  strychuia  is  eniploTcd  in  the 
preparation  of  bitter  bf-er,  is  consistent  with  probability.  In  onlCT 
in  form  an  opinion  on  ihls  point,  it  is  necessary  to  nbtain  dear  idee* 
of  the  qtmniity  of  this  sulistance  necessary  to  impart  bift4*rne«f  to  a 
given  bulk  nt'  fluid,  to  detorniiiie  the  eheniic&l  condition  in  which  it 
exists  in  beer,  and  to  asccrtnin  the  amount  of  strychnin  which  may  b* 
introduced  into  the  syst^^m,  witli  safety  to  health  and  liie.  With  re- 
spect to  its  bitterness,  we  find  that  one  grain  only  of  strjchnia  imparta 
a  d*!i*ided  and  |<ersislent  biLitTiiess  to  ut  least  40,000  gruins  of  water, 
or  upwurds  of  liulf  u  Ki^llon ;  but  the  taste  of  the  »nmii  t|UHnlity  uf. 
strychnia  is  perceptible  when  diluted  with  420,000  gnuiis,  or  wn 
gallons  of  water. 

Hut  it  must  be  rcnienibercd  that  most  beers  contain  frei;  acetic  aci^ 
in  variable  nnioiint,  and  thnt,  therefore,  strychnin  added  to  be«r 
usmally  becomes  converted  into  acetate  of  strychnia.  Now  this  sail, 
Hltbou<!h  very  bitter,  is  les^  90  than  i>trychiiia  itself;  con»etjuonLly,  a 
larmier  amount  of  tUtf  combined  ulkahiid  i^  neccitsary  toiui|>urt  thesaxne 
de;r'ee  of  bitterness. 

We  have  ascertained  that  not  less  than  three  jfrains  of  ncc'Uite  of 
strvchnfii  ure  needed  to  give  a  persistent  and  suitable  bitterness  to 
half  a  ;;iitlan  nf  walfr;  it  is  therefore  evident  that  not  less  than  one 
^ain  and  a  h»l^{>^^t^v(dlnia  in  combination  with  acetic  acid  would  b« 
required  to  impart  siieh  a  dtyree  of  bitterness  to  the  same  quantity  of 
beer  as  10  render  lis  use  in  the  preparation  of  bittiT  beer  a  matt^^r  of 
any  muinenl.  Now  a  r^uaotity  of  strychnia  so  considerable  aa  thiii 
couid  not  be  taken  in  beer  consis^ii'iitly  with  safety,  or  even  without 
danger  to  lif*;.  Were  the  quantity  present  in  beer  much  below  this, 
its  use  woidd  still  be  iittenduil  with  the  greatest  danger,  since  tlicre  is 
much  reiison  to  believe  that  this  poison,  like  digit-tdis,  colehicuni,  and 
certain  otln-r  active  vegetable  prtKhKits,  is  liable  to  be  retaineil  in  tha 
aystein^  nnd  let  accumulate  in  it  to  such  an  extent,  as  at  leng^th  to  give 
i*ise  U)  the  tetanic  spasms  oud  other  Consequences  symptomatic  of 
poisonin;r  by  strychnia. 

From  all  these  considerations,  tlierefore,  we  conclude  that  the  state- 
ment made  concerning  llieuse  of  strychnia  in  bter,  under  any  circum- 
stances, is  {scarcely  consistent  with  probability. 


1 


On  the  Detection  of  Strychniiu.  ' 

We  now  come  to  treat  of  the  means  by  which  the  presence  of 
strycltniu  in  beer  may  be  determined. 

Wlitle  chemical  science,  in  its  present  condition,  fails  to  detect 
many  comp4>unds  derived  from  the  organic  kingdom^  it  is  fortunate 
that  this  is  iifit  the  ca!»e  with  the  majority  of  the  more  deadly  vege- 
table substances,  as  pruseic  acid,  morphia,  nicotino,  brucia,  aod  also 
strychnia. 


ALE,    AND   ITS   ADULTERATIOXS, 


S2I 


Tests  for  Strychnine.  —  Strjchnitiff,  or  strjcbnifl,  is  met  with  in  two 
sliites  —  the  oni;  iiiipurCt  the  otlier  pure. 

In  ils  impure  condition,  it  is  in  *:oiubi nation  with  ontilher  vepetahle 
principle,  tt'rnied  brticia,  an  J  for  which  thore  exisla  a  wry  characterislic 
chemicii)  test. 

Citmmercial  ittrychnia  is  verj  commonljr  impure,  being  admixed 
with  a  g^reater  or  less  amount  of  brucin ;  min'h,  however,  ot"  the 
Btrycbnia  nfianufDctured  contains  very  little  of  this  principle,  ond  is 
even  frequently  entirely  destitute  of  it,  »i»lhat  no  relinnre,  for  the 
detection  of  strycliiua,  can  lie  placed  ujwjii  (his  conianiinaliuiii,  since 
it  J8  not  constant.  The  principal  lest  for  brucia,  and  indirectly  for 
strychnia,  when  the  two  occur  logctherj  is  nitric  acid,  with  which  re- 
agent a  blonil-reij  cohmr  is  developed. 

Tor  ih<*  alkaloid  in  it.-^  pure  stale  there  arc  likewise  appropriate  and 
most  salisfaetory  tests. 

The  first,  antl  chief  uf  these  woa  proposed  in  1843  by  JIarchand*, 
wIk)  showed  that  if  a  fimall  quantity  <il  strychnia  berubl»ed  with  a  few 
drops  of  concentrated  ^idphurie  acid,  or  oil  of  vitriol,  c<'n!ainin;j  a 
Teryintnute  proportion  of  nitric  autd,  no  ehon^jeof  cnlour  would  ensue  ; 
but  that  rm  ihe  addition  of  a  small  cjiiantity  of  the  puce-coloured 
oxide  of  lead,  or  even  of  litharge,  a  beautiful  viuk-t  colour  is  iwime- 
diutoly  developed,  which  quickly  changes,  first  to  a  red,  and  then  loan 
oran;;e  tint, 

A  modification  of  this  te*«t  was  Bub9e(]uently  proposed  by  Mackfi 
who  suggested  the  substitution  of  peroxide  of  mangnnese  for  the  oxide 
of  lead.  In  this  case  precisely  ihe  same  chanj^es  take  place,  and  the 
Slime  development  and  play  of  colours  i^  prurluced. 

Again,  Ottot  has  suggested  a  further  modification  and  improvement 
of  the  test  by  the  employ  ment  of  chromnle  of  [H>ta5h. 

Lastly,  Mr.  Thomp!<on  recommended,  in  1 849,  the  use  of  bichromate 
of  potash  § 

One  or  two  drops  of  stronjr  sulphuric  acid  arc  to  be  allowed  to  fall 
on  a  minute  quantity  of  strychnia,  and  in  thl^  a  small  frag^uient  of 
bichromate  of  puto&h  should  be  pluccd>  around  which  a  beautiful 
violet  colour  will  be  rapidly  and  continuoui-ly  formed,  so  long  as  any 
of  the  strychnia  or  bichromate  of  (Hit as li  rcuiaiiis  undissolved  and  un- 
acted upon. 

The  whole  of  these  tests  are  exceedingly  delicate  and  satisfactory  — 
the  last  one  particularly  so;  and  by  it  so  minute  a  quantity  as  (he  one 
thousandth  of  a  grain  of  pure  strychnia  mav  be  detctrted.  Tlie  cohturs 
developed  are  the  same  whichever  reagent  bo  employed,  but  the  linta 
are  sccd  to  the  ffreaiest  advantage  wbeu  the  chmniate  or  bichromat« 
of  potash  is  used,  oo  account  of  the  solubility  of  these  saltfl. 


•  Jnurnftl  ir  Ptmrtnarlo  et  do  Chlrolr,  Senc  Striri.  torn.  If.  p.  300.,  18*3. 
t  Rucliitrr'a  Itcivitortuui.  Mcond  Mrl#t.  «oL  xlllL 
t  PhKrtDiuptiiUrl)P«  C*fntr«l-BUtt,  !>«:.  30.  IS46. 
\  Phanascrultr^  Jotirtia),  %*A  Is.  p.  31. 


rf^MJ  I       II.  rf< 
dc  fd^l^vic  acid  ■  rafsivd  ■  flvivtofctrid 

IW 

dfcg:  A»waate«ytheiiiiifcBM  i^hci^Egfcttr 
iW  etkotttl  Bolatiaa  it  to  be  i  iiyMMiJ,  mA  tW 

tliiifi  •fctinwit,  m  well  kwwa ;  and  of  tUs  propcft;  ■■<■— li^t  amv 
ke  tikcn  in  tke  ptCMSt  iMtaMe. 
Froa  two  lo  tiiree  ovmoa  mf  maamtl  ^araoal  are  to  be 
tknm^  half  a  ^loo  of  beer, 
■^lattMi  fnMn  ci^ttotwtivekMiriL  He  bMT  ■  to  b*  fibcred,  vWb 
it  win  be  obwrred  that  h  baa  leal  Hacb  of  iti  colaHr  md  a  pvtaott  af 
tti  brt«crnc» :  tbe  cbarono],  tbe  wboleof  wbieb  ikoold  be  ooBrcted  oa 
tbc  fitter,  u  tben  to  be  btiiled  with  tcaouneeiaf  spirH  of  vine;  tad 
c«tb«r  of  tbe  pUiM  denribed  mbore  maj  be  adopted  for  obtunni^  tbe 
strychnia  in  a  flate  of  purity. 
A*  tbe  proRCM  of  erapnratinn  U  one  of  c<msiderable  time  and  troable, 
anc 
I 


and  as  it  i«  difficalt  lo  obtain  &  perfectly  colourless  rcstdoe  in  tbtswaj, 
tbe  last  methotl  proposed  for  isolating  tbe  strvriinia  will  be  fiauad  tbe 
~^i«(  convmietit,  ai  well  m  expetliMona. 


ALE,   AND   ITS   ADULTERATIOX8. 


£33 


The  two  methods  of  purification  may  even  be  coniUncil,  anil  tlic 
piitash  and  ether  may  be  added  to  the  iii]uenus  residue  after  the  eui- 
|tluynieiit  of  the  sulutiun  of  lead  and  sulphuric  acid,  and  in  this  way 
a  very  pure  elhereal  solution  may  be  obtained.  l)f  tbetwo  ])lan!it  the 
nccesoary  precautions  bein»  observed,  the  (iv*t  is  perhaps*  the  best. 

AMiichever  proceeding  for  the  extraction  and  jiurification  of  the 
strychnia  be  followed,  several  precaiitiiin.4  are  retiuired. 

if  charcoal  be  employed  for  the  extraction  of  the  strychnia.  It  la  not 
simply  sutticient  to  add  the  charcoal  to  ihe  beer,  but  both  before  and 
during  filtration  the  beer  must  bo  well  shuken  yeveral  liines. 

Jf  (he  metlifMi  of  puriHcation  by  means  uf  ether  and  [>ota«h  be 
adopted,  the  spirit  of  ihe  spirits  of  wine  u.«ed  to  cep;imte  the  strychnia 
from  ibtf  charcoal  should  be  entirely  distilled  or  eraporateil  off,  which 
may  be  known  to  be  the  case  when  the  va[K>iir  evolved  ceai^s  ti» 
smell  spirituous,  and  to  be  pungent.  If  this  precautiun  be  not  ob- 
served, the  ether,  in  place  of  floating,  will  combme  wiih  the  water  and 
spirit. 

The  erher  employed  should  Ih?  stronj*  sulphuric  ether,  nnil  itahuuld 
not  only  be  well  shaken,  with  the  oi|ueous  residue,  more  than  once, 
but  should  be  allowed  to  remain  in  contact  with  it  fur  about  ludf  an 
hour,  no  that  it  may  have  time  to  di&tolve  out  the  strvctiuia. 

In  uddiii<;  the  potash  cure  must  be  token  lest  too  little  or  too  much 
be  employed  ;  if  too  little  be  used,  some  of  the  organic  matter  will 
remain  in  suspension  i  and  if  too  much  the  aqueous  solution  will 
1>eciinie  darkened. 

If  the  plan  of  purification  with  acetate  of  lead  and  sulphuric  acid 
be  practised,  the  h-ad  must  bo  added  until  it  fjct-asions  no  furihir  pre- 
cipitate, and  (he  sulphuric  acid  also,  until  the  intioluble  sulphate  uf 
lead  ceases  to  fall. 

When  it  is  remembered  that  concentrated  sulfihuric  acid  darkena, 
and  even  chars  nr;ranic  substances  of  all  kimli^,  the  necessity  for  a 
Complete  separation  fif  the  organic  impurities  will  bci.'oine  apparent. 

A  (rreen  colour  in  the  course  of  a  minute  or  twn  :dnu>st  constantly 
forma  around  tlie  Iragments  of  bichromat*:  of  p4ita.ih,  even  when 
strychnia  is  not  present,  and  this  takes  place  very  quickly  indeed  if 
any  ether,  sugar,  or  or^jnnic  matter  remains  on  the  elasa.  It  is  pos- 
sible that  this  colour,  formed  by  the  ;;reen  oxide  of  chromium  which 
becomes  liberated,  mi«;ht  be  erroneously  regarded  as  mu  evidence  of 
the  presence  of  strychnia. 

We  refer  to  all  these  particulars  because  unless  pointed  out  ihey 
arc  calculated  to  leail,us  thev  have  more  than  once  done  withoui**elve4, 
to  enibarraasment  and  disappointment. 

Before  procecilinif  to  analyj*e  the  samples,  preliminary  experimcnta 
may  be  made  with  beer  to  whicli  has  been  purposely  uddc<l  from  half 
a  ^ain  to  n  fn^in  of  strychnia  to  a  ^nllon  of  beer;  we  found  that 
we  could  invariably  succeed  in  detecting,  by  the  methods  indicaied, 
ibe  preseooe  of  the  poison  id  these  minute  quantities. 


524  GIN,   AXD  ITS   ABDLTERATIOX8. 

We  Ihuii  perceive  how  conclusive  are  the  tests  employed  fcr  t\t 

detection  nf  strychnia. 

The  following  process  hy  Mr.  Rotlgers  for  the  detection ol  ftrrtiwi 
in  the  iuiiiiidl  iis«u(?s  was  ptiblinhod  somi!  months  bnck  in  'T^ffniaa.* 
It  is  equally  applk-oible  for  ihe  discovery  of  that  alkaloid  in  beer:— 

"  Tbt»  tissues  of  the  IxKly  arc  riibbi-d  witli  distilled  water  id  ■  DKHir 
to  a  pulp,  and  then  (iigcst*Ml  aiYcr  the  addilirin  of  a  little  hydrocU'iric 
acid  in  an  evaporating  basin,  then  strainefl  and  evapur..*  !  •  '  't-"» 
over  a  water  bath  ;  digest  the  resiilue  in  spirit,  tilt»5r.  j'  lw 

rate  to  dryness ;  treat  with  distilled  water  acidulated  v>ui,  -  i<^-  -jojji 
of  hydrocliloric  acid,  and  fdter  ;  udd  excess  of  ninmcots,  anilipisif 
over  a  tube  with  chbvrciiforin  :  the  strychnine  in  nn  impure  coeditioBii 
enrirely  sonarntiMl  ^i-ith  the  ehlorofomi.  ThiJi  chlornfonn  aolfltkiil  ■ 
to  be  carefuHy  sepamtcd  by  a  pipette,  and  poured  into  n  gnall  <ttL 
and  wiped  to  dryness;  the  residue  is  moistened  withconc«iiiral«d  mj- 
jihurie  nciil,  and  heated  over  a  water  bnth  fur  half  an  hour;  vitT  » 
thL*n  added  and  excess  of  ammonia,  again  agitated  with  i*hlonii««, 
mid  the  strychnine  will  he  a^ain  sepHrated  by  the  rhlorof«m  ww 
in  a  state  of  sutBrieiit  purity  fur  testing,  which  chu  be  do«e  ito 
cvaporulin;;  a  few  drop*  on  a  piece  of  white  porcelain." 

Hut  wc  need  not  confine  ourselves  to  chemistry  in  onler  to  ohw 
evidence  ot  the  presence  of  strychnia  in  organic  HuifU,  a*  l^ywIV 
will  disclose  the  fjict  almost  equally  well. 

One  gallon  of  beer,  to  whiirh  a  gruin  of  strychnia  hail  hirca  puh 
]fusiily  added,  was  evaporated  to  an  extract ;  this  wa*  boiled  hrteK^J 
an  hour  in  a  mixture  of  ether  and  alcohol;  the  solution,  aAcrfiltn|i*t 
was  uvaporated,  and  the  residue,  of  a  H>ft  consislenc**,  was  SftatM* 
terod  as  a  pill  to  a  small  rabbit.  In  tht  counie  of  two  minulM  ^ 
nninial  iK'CJune  aflvoted  with  convuUive  twitching*;  the»c  weresli"*^ 
immediately  «uccee<led  by  a  paroxysm  of  convuUiwis  in  wlue^  ' 
Animal  threw  hinmelf  on  his  side,  the  head  and  neek  Winf  tkn'* 
back,  the  hind  and  fore  legs  extended  and  drawn  luurkwank  TW 
first  panixysm  was  rapidly  followed  by  others  and  in  leas  diss  ^ 
minules  after  the  administration  of  the  pill  the  rabbit  was  il««iil 
having  exhibited  the  peculiar  symptomn  which  characterise  pov««<M 
by  strychnia. 


GIN,  AND  ITS  ADULTERATIONS. 

GiM  w:'.g  made  orijrinally  in  Holland,  in  the  distilleries  of  SchW"- 
and  hence  that  which  is  brought  to  this  country  U  tenncd  Helu' 
Gin.     At  one  lime,  when  the  dutj  wa«  low,  it  used  to  be  Urgt^J  '^ 
ported,  but  owing  to  the  high  rate  of  duty  levied  upcm  it  fir  i*" 


GIN,  AND   1T8   ADULTEKAT10N8.  AM 

past,  which  was,  until  I846»  U.  Is.  lOr/.  per  imperial  jrollnn,  and 
that  period  lias  remained  at  15#., — but  little  now  roacht's  this 
mntry. 

In  Hollnnd  it  is  made  solely  from  unmalted  rjG  and  hurley  malt, 
rcnifiLMl  with  juiimcr  bcrrio.-*.  In  Britnin.  ^\n  is  ibr  tlie  must  part 
ulitaitii;d  fruin  ii  tiiixiure  of  nmit  mid  barlev,  molasses  3n<l  I'orn  Iwing 
somctitnes  employed,  particularly  when  there  is  a  ncan-ity  »t'  griim, 
and  it  is  usually  flavoured  not  only  with  junii*or  ln-rrie*,  hut  with 
certain  other  substance?!,  oiost  of  which  are  urouiattcs,  untl  stnonfrst 
which  are  the  following  :  cnriundfr,  cnrdainom,  nnd  carawnT  9€e*ls, 
STiiins  of  paradisCf  antrelica  root,  cahimua  root,  eru.-'bed  alninnd  cake, 
Uquiiricc  powder,  and  orange  peol.  These  ingredients,  viiriounly  com- 
bini'd.  Conn  what  rire  known  in  the  trade  as  "(»in-flavoLirin;i." 

Pure  ;iin  should  <-un6i3t,  us  iloes  liulhiuds,  soluty  uf  rectiSed  com 
spirit  iliivuured  with  junijwr  berries. 

0«    THE    AsCLTEBATIonS  OF  GlW. 

Gin  is  commonly  diluted  or  adulterated  with  large  quantities  of 
water. 

But  since  the  addition  of  water  to  ^in  renders  the  mixture  whitish 
and  turbid,  by  uecasionin^  the  preciprtutiun  of  tlie  oily  nnd  resinous 
matteni  of  the  juniper  ami  other  i^ubslances  caniloyed  to  Huvour  iho 
gin  previously  held  in  snlntinn  by  the  spirit,  it  becomes  necessiuy  to 
have  recourse  lo  certain  suhjitancea  tit  **  fine**  the  pn,  aa  it  is  tenned, 
that  is,  to  restore  the  transparency  of  (be  spirituous  mixture. 

The  i^ubstances  more  cotnmoiily  emploved  fur  this  purpose  are 
alum^  mltcarbonaie  of  potash^  and  oeeasionatly  acetate  of  lead.  Alum 
dissolved  in  water  is  first  added  tu  the  weakened  spirit,  and  then 
%  solution  of  subcarbonste  of  {tota^h.  The  whole  is  stirretl  tui*elher, 
and  left  st  rest  for  twenty-four  hours.  The  alumina  of  (be  alum, 
precipifoted  by  the  subinrboimle  of  ])otaj^b,  acts  "as  :»  strainer  upon 
the  milky  liquor,  and  rnrriefl  down  with  it  the  finely  divided  oily 
mailer,  which  produces  the  blue  eohnir  of  the  diliiteil  litjtmr." — - 
Accutn, 

Roche  alum  is  tfoinelimcs  used  fur  clarifying  spirituous  liquors 
without  any  other  addition. 

"Another  metlnMJ  eorisists  in  adding;  firHt  a  solution  of  siibaceUte 
of  lead,  and  then  a  solulion  of  alum.  This  practice  is  biifhly  dujigerous 
beenuse  part  of  the  sulphate  of  lead  produced  remains  disMilved  in 
the  tinuor,  which  it  thus  renders  pui.foniiu5.  L<nforlumi(eiy  this 
method  of  clarifying  spirituous  liquor:^,  I  have  good  reason  lu  believe, 
is  more  frequently  practised  than  the  preceding  method,  because  its 
action  is  more  rapid,  and  it  imparts  to  the  liquor  a  fine  cotnnit^xion^  or 
great  refractive  i>ower;  hence  some  vestiges  of  lead  may  often  be  de- 
tected in  mall  spirit." — ^cci*m. 

Another  substance  added  to  gin  is  stUpharic  acid,     Mr.  Mitdiell 


gtatci!  llinl  n  mixture  compnficd  of  olnm,  oarbonnte  of  polash, 
oil,  sutplmric  ncid,  and  9])irii:>  of  iv'ine,  is  frenuently  Added  to  ^o. 
**This<.'oin|»oiin(l/'  he  remurks,  "nnt  only  fines  ilie  gin,  but  cnmrauni- 
c&testo  it  tlie  property  of  *beading,'  or  lianginjr  in  pearly  drops  or  head< 
on  the  sidca  ul'  the  glasn  cunlaiiiing  it.  When  gin  does  thi!^  ii  u 
pt?nerally  supposed  to  be  atronp  in  proportion  a&  it  bends,  and  the 
iibove  mixttjre  communicates  to  weiik  gin  that  properly,  eo  that  it 
will  be  evident  gin  con  be  considerably  dilittcfl  with  warer,  and  yet, 
hy  ihe  addition  of  the  above,  appear  of  it8  proper  stren^tb." 

But  npnciiy  is  not  the  only  evil  produced  by  the  addition  of  water 
lo  gin ;  the  strength  and  flavour  of  the  ^in  are  so  reduced  that  it  be- 
i-oiiiea  necessary  lo  add  other  substances  lo  restore  the  qualitira  lust 
by  dilution :  these  being  su^ar  to  sweeten  it,  and  cayenne^  in  the  form 
oi'  tinrture  of  vopticunL,  or  grains  of  paradite^  to  give  it  pungency  and 
a|>|>arent  slrungth. 

The  flavour  ntid  properiies  of  gin  are  further  modiGed  by  the  uae 
of  compminds  known  &n  ** gtn /la Pourings .*' 

'i'her^e  fire  L-oniposcd  of  various  cordial  and  amroatic  aubstant 
each  difitilk'f  usually  giving  the  preference  to  a  formula  of  liia  own. 

In  Dr.  MuHpratt's  '*  Chemistry"*  will  be  found  several  receipts  1 
gin  flavourings,  copie<l  from  the  note  book  ot  on  extensive  spi 
rectitier.     Two  of  tliese  are  as  follows  :  — 

Plain  or  London  Gin  is  mode  as  follows:  — 

700  cations  of  the  second  rectification. 
70  lbs.  German  juniper  berries. 
70  lbs.  coriander  seeds. 

34  Iha.  almond  cuke. 

](  lbs.  angelica  root. 

6  ll>s.  liquorice  powder. 

For  the  munufnclure  of  Wesi  Country  Gin,  known  also  as  Plymontl 
gin,  the  Annexed  is  the  process  given  in  Dr.  Musprait's  work  : — In- 
troduce into  the  still  700  gallons  of  the  secona  rectification,  and^ 
flavour  with  — 

14  lbs,  German  juniper  berries. 
1^  lbs.  catfinius  root,  cut ;  and 
8  Ihs.  sulphuric  ncid. 

This  gin  is  much  used  in  Ccmiwal!,  and  pnrticulnrly  in  the  western 
counties  of  Englnnd  ;  it  in  al^o  u^cd  in  nmkitig  liriti^n  Hollands,  and 
in  that  case  is  mixed  with  about  five  percent,  of  fine  gin,  reduced 
to  twenty-two  nndcr-proof  with  liquor. 

Amtmpst  the  ingredients  enumerated  in  the  other  receiptee  and  not 
contained  in  those  above  given,  are  orange  peel*  calamus  rootf  caaata 
buds,  orris  root^  cardamoms,  and  grains  of  paradise. 

In  Shannon's  work,  '*  Ou  Brewing  ana  Distilling,"  we  meet  with 


Chraibirr,  Tliaorftlcal.  Practical,  and  Atul7tlcal. 


GIN,   AND   ITS  AULXTKBATIO^CS. 


537 


tbe  (uUowing  instructions  for  reducing  unswcotcncd  gin,  and  for  prfr- 
p:inng  luid  sweetening  Uriluh  gin  :  — 


"  To  Beducc  Unsweetened  Oin, 


**  A  tun  of  fine  gin 
Water 


252  gallons. 
36      „ 


Which,  added  together,  make      -        -    288 
The   Doctor   u  now  put  on,  and  it  is 

further  reduced  with  wiUer      -         -       19 


Which  gives 


307  guUona  of  gin.* 


**  This  done,  let  one  pound  of  ulum  be  just  covered  with  wnter,  and 
dissolved  by  bfiiiing  ;  rummage  the  whole  well  together,  and  pour  in 
the  alum,  and  the  whole  will  be  fine  in  a  few  hours. 


"  To  Prepare  and  Siveeten  Britith  Gin, 

"  Get  from  your  distiller  an  empty  puncheon  or  cask,  which  will  con- 
tain about  133  gitllotis.  Then  tjilce  a  cask  of  clear  rwtified  spirits  — 
r20git]luns  —  ol  the  usual  strength  at  which  rectifiers  seLt  (hcirgoo<ls; 
put  the  I'iO  gallons  of  spirits  into  jour  empty  cask. 

"Then  take  a  quarter  of  an  ounce  of  oil  of  vitriol,  half  an  ounce  of 
oil  of  almonds,  a  quarter  of  an  ounce  of  oil  of  turpentine,  one  ounce 
of  oil  of  juui[)er  berries,  half  a  pint  of  spirit  of  wine,  and  half  a  pound 
of  lump  sugar.  Ueal  or  rub  tfie  above  in  a  mortar.  When  well 
rubbed  together,  have  ready  prepared  half  a  gallon  of  lime  water,  one 
gallon  of  rose  water:  mix  the  whole  in  either  a  pail  ur  cask,  with  a 
slick,  till  every  particle  shall  be  diwtolved;  then  add  tn  the  foregoing 
twenty-6vc  pounds  of  sugar  di«>olved  in  about  nine  gallons  of  ruin  or 
Thames  water,  or  water  that  has  been  boiled:  mix  the  whole  well 
together,  and  stir  them  carefully  with  a  stick  in  the  i:)3  gallon  cask. 

**  To  force  down  the  same,  lake  and  boil  eight  ounces  of  alum  in 
three  quarts  of  water  for  three  quarters  of  an  hour;  take  it  from  the 
fire,  and  dissolve  by  degrees  six  or  seven  ounces  of  salt  of  tartar. 
When  the  same  is  milk  warm,  pour  it  into  your  gin,  and  stir  it  well 
together  as  before,  fur  five  minutes,  the  same  ns  you  would  a  butt  of 
beer  newly  6ned.  Let  your  cask  stand  as  you  mean  to  draw  it.  At 
every  time  yuu  propose  to  sweeten  again,  that  cask  must  he  well 
washed  out,  and  take  great  care  never  to  shake  your  cai^k  while  it  is 
drawing," 

But  it  appears  there  are  other  little  practices,  bcitides  those  con- 
nected with  adulteration,  which  itre  sometimes  had  recour-^j  to  by 
retailers  of  spirits.  Mr.  Shannon,  from  whose  work  *' On  Brewing 
and  Distilling"  we  have  just  quoted,  gives  the  following  advice  and 


528  GIN,   AND    ITS   ADULTEEATIOSS. 

recnmrncixlcitions  o.^  to  ocrr&in  mnnipulatinns  and  parliculm  vfcicii 
i>houlil  be  observed  in  retfiilinjr  !*pinU  oyer  the  counter. 

'*  When  jou  arc  to  draw  a  sample  of  goods  to  «>bow  a  penoa  tW 
hnR  judgment  in  the  proof,  do  not  draw  jour  goods  into  aphiilubt 
Ta^ti'd,  or  ir  uke  experiment  of  the  strenjzth  thereof  that  waj,  hcniiai 
the  prfHtf  will  not  hold  except  (be  pooth  be  exceetJincljf  fOtm^:  tan 
draw  the  pattern  nf  gootls  either  into  the  glus  fmm  Oie  cock,  to  nn 
very  9Ui;di,  or  rather  draw  off  a  soitdl  qu&ntilj  into  a  ViVdt  |«v1er 
pot,  and  pour  it  intn  your  ^lass^extendinjf  tour  ptti  ss  higtitbo*cd( 
<;Iits9  as  you  can  without  wa^tinf;  it,  which  midces  the  ^xAicUTjk 
l)ctter  head  abundantly,  than  if  the  same  goods  were  lo  be  pgi  ai 
tried  in  a  phial. 

'^  You  must  be  sn  prudent  as  lo  make  a  distinction  of  the  pflvai 
you  have  In  ileal  with  ;  what  goods  you  sell  to  gentlemen  for  tkcxr 
iiwn  use  who  require  a  great  deal  of  attendance,  and  us  much  farUM 
uf  payment,  you  must  take  a  considerably  greater  prioetban  of  odvn; 
whut  go(Mlfl  you  Bcil  to  perAonn  where  you  believe  there  is  a  n^'^tfK 
or  lit  lea.^t  «ime,  hazard  of  your  money,  you  may  safely  adl  tar  mm 
than  common  profit  ;  what  goods  vou  sell  to  the  poor,  efpedaDf 
medicinally,  0^  many  of  your  goods  are  sanative.)  be  ai 
flionate  as  the  casea  require.** 

HesuUs  of  the  Awdt/na  of  SampUa, 

The  following  are  the  results  of  the  analysis  of  Thirty'eigkt  tmfta 
of  gin:  — 

That  the  strength  of  the  various  samples  ranged  from  \Sfi4SglL 
to  34,160  grs.  per  imperial  gallon  ;  the  |)er-centagi*9  ranging  £■ 
2*2  35  to  48-80  per  cent. 

It  thus  appears,  that  some  of  the  spirits  contained  only  half  if  waA 
iilfohol  as  wad  present  in  sv>me  of  the  other  samples,  and  tbfrdbn 
that  their  ccnnmercial  value  was  redut^  to  the  enormous  cxteai  "f 
more  than  one  half;  thus,  supposing  sample  2.  to  be  worth  IfeMt 
gallon,  sample  3.5.  would  be  worth  less  than  6s.  per  galloa.  lai 
variation  in  the  strength  of  the  spirits  is  doubtless  princapttlly  attnba- 
table  to  dilution  with  water. 

That  the  quantity  <jf  su^'or  ranged  from  3  oz.  4  dr.  33  gr.  to  18  oil 
4  dr.  13  gr.  per  gallon. 

TliAi  two  of  the  samples  contained  oi7  ofeinnamoH,  or  mare  prob^ 
of  ctuxin. 

That  Jir^t^m  of  the  samples  contained  Catehiib  pxrrsi,  mmmo/iIm 
in  very  large  (tuantily,  so  that  the  syrupy  extract  Xeit  on  etapowtfaa 
possessed  a  burning  and  fiery  taste. 

That  in  no  cai^e  vratfree  wtUphuric  acid  detected:  it«  abMnotbikl 
sutliciently  shown,  by  alt  the  samples  bein;;  neutral  to  tett  (MLper. 

That  mott  of  the  samples  containe<l  combined  sulpbatea,  cfaidlvdi^ 
rived  from  the  water  and  alum  used  in  the  adultemtioa  aod  danAfl^ 
tion  of  the  gins. 


GIN,   AND   ITS  ADULTERATIONS. 


539 


In  aiMition  to  the  abore  adulterntionft,  we  have  the  authority  of  a 
[in  (liAtilltrr  fur  slutiiii;  tliat  the  practice  of  adUiiif^  Eulphate  <■■/  zinc^ 
as  it  is  conimouly  called,  tchtte  tUHol  or  white  copperun^  to  gin 
very  commnn.     Uero  nguin^  then,  we  have  obtained  evidence  of 
■•the  adulteration  of  gin  in  a  manner  calculated  to  prove  ii^jurious 
lito  health. 

It  15  impossible  to  conceive  of  more  Kandalous  adulterations  of 
gin  or  other  spirits  than  thnse  by  Cayenne  pepper  or  grainx  of  para- 
dixe^  I'nr  ihej  are  almost  equally  hut  and  puiij;;ent.  The  introduction 
i]ili>  the  iiloriiach  of  raw  spirits  is  sutficienlly  destructive  to  health  of 
itsflf,  but  the  uditition  of  such  powerful  and  acrid  substances  as 
Ciivcnne  ^nd  j^rnins  of  paradise  to  spirit,  forms  a  conipound  which  no 
human  5(omuch  or  nystoiiif  however  «tron;;,  can  long  wiihstnnd, 

Allliou^ih  sulphuric  acid  was  not  present  in  any  of  the  s:imple8  of 
Lomlon  ^in  which  we  examined,  it  is  yet,  no  doubts  sometimes  cm* 
ployed,  and  this  in  lur^e  quantity.  Dr.  Muspratt  statt^  that  it  is  so  in 
AVest  Couutry  gin.  if  any  sample  of  gin  exhibit  an  acid  reaction, 
the  presence  of  sulphuric  acid  may  be  suspected,  and  it  may  be  dis- 
covered limply  by  the  evaporation  at  a  gentle  heat  of  a  little  of  the 
gin,  placed  on  the  hob  of  a  fireplace.  As  soon  as  all  the  spirit  and 
water  have  been  driven  off,  tlio  sulphuric  acid  will  act  on  the  sugar, 
and  quickly  reduce  it  to  n  black  carbonaceous  mass. 

llie  adulteration  of  gin  with  Cayenne  pepper  is  mostly  effected  by 
means  of  tincture  of  capsicum,  and  it  is  practised  in  the  majority  of 
cases  by  the  publicans  tberoselves.  We  are  acquainted  at  the  pre- 
sent time  with  the  name  of  a  publican  whom  we  have  ascertained  to 
muke  periodical  purchases  of  tincture  of  capsicum.  We  know  the 
cht'uiist  of  whom  he  purchases  it,  and  we  have  detected  it  in  more 
than  one  sample  of  tht.*  ^in  sold  by  him  to  his  customers  at  the  bar. 

We  have  often  in  the  course  of  this  work  commented  on  what  we 
conceived  to  be  the  remissness  of  the  Excise  autboriiies.  Here  is  a 
gro«>9  adulteration  of  gin,  commonly  practised,  and  detectable  in  a 
ready  and  simple  munner,  by  which  the  revenue  is  defrauded,  and 
which  is  seriously  detrimental  to  health  ;  and  yet  we  do  not  remember 
to  have  ever  heard  that  the  Excise  ha<I  noticed  it  in  any  way,  or 
taken  any  Bte]>s  to  put  a  stop  to  so  iniquitous  an  adullerotion. 

The  differful  kinds  of  spirit*  are  obtained  in  a  comparatively  crude 
stale  from  the  grain  by  the  distiller.  Thi'y  are  afterward;*  submitted 
to  ptirification  by  the  rectifier,  as  well  as  procured  of  a  higher  strength. 
The  impurity  of  raw  spirits  arises  priucipdly  Ifom  the  presence  of  a 
peculiar  volatile  oil,  termed  /mil  oil^  and  possessing  very  deleterious 
properties.  Of  this  oil,  and  of  the  method  uf  freeing  spirits  from  it, 
we  meet  with  the  folhtwing  account  in  Vre's  Dictionary*  :  —  "Some- 
times, after  moist  autumns,  when  damaged  grain  abounds,  the  alcoltol 
distilled  froiu  it^  fermented  wash  containa  a  peculiar  volatile  body« 

•  4ihR41llon.  rot  l.p  M 
M   H 


CIS,  A3n»   IT»   ADCXT£K.%r[0>a. 


ri 


fat 

Ml 


If  ■»!>»■■  J  frcasj.     It  » 
tai  rhtmtm-iH  bf  JbdC  »  I 
of  tke  gi««l 

At  tlw  end  cCa  feir  Mom^  it 
ia  Ae  ifiititi,  and  Icsna  tfceaa  is  a  tern 
)e.    B7  Iwgdy  diliitiiig  tka  ifitsitt  wiili  wai<rr,  3 
at  a  ■uJeratc  l<i|mi|an,  Ike  ^nasv  put  oT  tku  oil 
Put  of  h  eone*  vw^  «lib  tke 
with  tbe  latter  nwain^  whkfc  are  caOed  hf  tW  datiDen 
^and  weak  fisiiiti.   Hie  iaSenalediBte  portioa  m  porer  cptrit.    ICIk 

ahrajt  laore  or  Icm  opaleaecat;  or  becoie  90  on  dilution  «tt 
-vatcr,  and  then  tlvow  ap  an  6Ay  pellicle  anen  ibetr  mrfikce.  TW 
;aliareoab  of  ligtit  wood,  woA  as  pme  or  wAlow,  well  calcixied,  tad 
in  MiAeieat  quancitjr  whk  tlia  apirila  prior  to  rectificatioB,  wfll 
re  then  of  the  gieatcr  part  of  ilait  oQ/  eootaaniBaltoa.  Anuml 
lal,  well  calcined,  has  at^o  been  found  nselttl ;  but  it  most  be 
ited  fur  Sfjme  time  with  ibe  enipTreamatic  spiritabefire 
Another  znetbod  of  feeparating  that  ofiensrre  oil  ia  to 
Aa  iBpwe  flpirits  with  a  qmuniitj  of  £at  oil.  rach  as  olire  oO,  or  o3 
of  alaKtods,  to  decant  off  the  o3,  and  re-distil  the  ^irits  with  « littk 
wat^T. 

"Diorcrtion  «nd  agitation  with  calcined  magnesia  for  annc  taam 
fnllowfHl  hj  filtration  and  distillation,  are  sliogooil  mcuis  ftir  im|wx>T* 
ing  the  flarour  of  alcohol.  The  taste  nf  the  oil  of  grains  is  best 
irco<wniaed  by  agitation  with  water,  whercbr,  on  standing,  the  Ha^ff>ti 
-fpint  throws  up  a  film  of  oil  visible  br  redacted  light.  If  the  spirit 
he  mixci  with  a  few  drops  of  nitnitc  of  silver,  and  exposed  for 
time  to  sunshine,  the  oil  will  react  upon  the  oxide  of  silver,  and 
a  brown  tinj^e  ;  but  if  there  be  no  oil  present,  the  spirits  will  rei 
limpid.  If  one  part  of  hyrlrate  of  potash,  dissolved  in  a  littJc  w 
hi*  uiixcd  with  150  parts  of  spirits,  and  if  the  mixture  be  well  sbuki 
tlien  slowly  evaporated  down  to  16  parts,  and  mixed  with  15  ports 
dilute  sulphuric  acid  in  a  phial,  to  be  then  corktHl,  there  will 
exhale  from  the  mixture  a  peculiar  offensive  odour  charBctoriacie  of 
the  quulity  and  origin  of  the  impure  spirit,  whether  obUiine<l  from  rai 
grain,  from  mull,  from  polntot:^  ryp,  arntck,  rum,  brindy,  &c.  Tl; 
ex(!cIlout  proresi*  niav  oc  uwid  hJao  for  te^iinjf  «rine«-  Lime 
nllcdlifl  alway*  injure  the  flavour  ofurtlent  npirrts  of  all  kinds." 

Dr.  Taylor  remarks  of  fusil  oil,  "thul.  in  small  uuanlitiejt  it  produ 
in  toxica  l.i(m.     I  have  ex[>erient:ed  the  effects  of  the  vapour,  and 
lliem  to  be  giddiness,  accompanied  with  a  feeling  of  suffocation  and 
•cn«c  of  foiling.     Headache  followed  which  last^  for  half  an  hour.** 


cause  I 
nnaif^H 

rat«^H 
ak(^H 
ru  <^H 


GIN,  AND   ITS  ADULTERATIONS. 


531 


1 

P 


"  Two  (Iranhms  of  the  oil  kUIecl  n  rabbit  in  two  hours,  three  drachms 
Id  an  tiouff  half  an  ounce  iu  n  ijunrter  of  an  hour,  and  onu  ounce 
in  four  minutca." 

Much  of  the  unwholcsomcncsa  of  spirit  ixDperfectl>  rectified  otlms 
i^om  its  contamination  with  fusil  oil 

Ou  the  Detection  of  the  Adulteraiitnu  of  Gin. 

Adulteration  with  Water. — The  adulteration  of  gin  with  water  may 
b«  determined  in  two  wuya,  the  one  indirt^ct  and  the  other  ilirert- 

The  indirect  method  is  by  estimating  the  quantity  of  alcuhul  con- 
tained in  it.    This  is  dTected  by  the  processes  deauribed  below. 

Method  of  Ettimatitig  the  Qtimitity  of  Alcohoi  present  in  any 

Spirituous  Lifjuid. 

Saecharometers^  SfC.  —  There  are  several  methods  by  which  tlie 
amount  of  alcohol  cuutained  in  any  spirituous  liquid  may  be  deter- 
mined with  greater  or  less  accuracy.  One  of  the  readiest  of  these 
meatu  is  to  ascertain  the  specific  gravity  of  the  spirit  by  a  specific 
frravity  instrument  for  liquids.  Of  these  instruments,  muiiy  diflereut 
kinds  have  been  invented,  witJi  scales  adapted  to  the  range  of  the 
liquids  for  the  deteimtnatiim  vf  the  deo^ity  of  which  they  huve  been 
coristructed  :  thus  wo  have  saccharometerg^  hydrometers^  aUoholometerSt 
specific  gravity  UottleSy  &c. ;  but  the  principle  on  which  these  instru- 
mental are  constructed  is  alike  in  all  cases.  By  the  saecharomrter  the 
amount  of  extractive  matter  in  beer  or  other  alcoholic  liquid  is  ascer- 
tained. 

St/kca*  Hydrometer, — The  instrument  in  general  use  for  determining 
Ihespecificgravily  of  spirituous  liauidsin  thin  country  is  what  is  known 
as  Hykes'  Hydrometer.  It  diifcnj,  towever,  from  the  ordinary  hydro- 
meter in  ilie  division  of  its  scale,  and  also  in  the  use  of  weights.  The 
hydnmiett^r  i.n-jilculated  to  show  the  strength  in  spirit  either  above  or 
below  a  certain  fixed  standard,  denominated  *^ proof ."**  The  stem  of 
the  instrument  is  graduated  and  subdivided,  so  as  to  meet  tlie  ex- 
trcines  of  variation  in  the  strtiigth  of  the  liquors  examined  by  it. 

Sykes'  hydrometer  is  the  inBtrument  mostly  used  by  the  Kxcise,  by 
brewers,  distillers,  and  pubbcaiis. 

Since  the  siHJcific  gravity  of  a  spirituous  liquid  is  subject  to  great 
variations  ul  differenl  temperatures  it  is  necessary  that  the  tem{>«ra- 
ture  uf  the  spirit  jit  the  time  of  taking  Un  weight  should  be  noted,  and 
corrections  made  !or  this  by  means  ol  certain  tables  which  have  been 
constructed  for  the  purpose.  The  standard  temperature  at  which  the 
ttpccific  gravity  of  the  spirit  is  usually  token  is  60°  Fahrenheit. 

*  "  Thli  liquor  po(  beltif  atttril  •wrmconl,  nr  bif  log  any  IngrMlnnt  dliinlTiKl  tn  It  to 
dirfml  lh»-  iirirngth  thrrntf.  of  ttiv  lamp,  of  &l^  Ffthr,.  «(>1gb*  cxartlf  f J  f>«rtj  o(  an  equal 
tiMHUurv  urdlttUled  waur." 

M    M    3 


S5% 


OIN,    AND  ITS   ADULTERATIONS, 


The  specific  gravity  test  for  detcrmiuiog  the  amo<int  of  aIcaM 
present  in  liquids  is  applicable  only  wheti  tbey  ore  Iree  rrvm  aziT  5oIid 
sub.stancc,  ns  cxlrnctive,  sugar,  &c  ,  the  presence  of  which,  by  aifectinf 
tlie  weight,  of  course  influences  the  s|vecific  gravity.  When,  thmt- 
fore,  any  liquid  contains  faccharino  or  other  solid  matter,  it  « 
requipilc  that  the  spirit  tihouM  he  sepanited  by  ili^tillution,  and  iitaS 
the  Ppecifie  gravity  of  the  alcolKil  thus  obtained  should  be  take** 
AVhere  strict  accuracy  is  require*!,  it  will  be  ucceewurv  to  have  ir- 
cnurse  to  di^itilliition  in  almost  all  cases,  since  there  are  hut  few  nurils 
which  do  not  contain  more  or  less  solid  matter. 

Centesimal  Alcoholometer. — A  considerable  improremerit  on  Svkfs* 
hydrometer  is  the  instrument,  invented  by  M.  iiny  Lus»ac  luanv  years 
since,  colled  the  centenunal  alcoholometer.  This  instrument,  wtieciii 
mersed  in  any  spirituous  liq^uid  at  the  temperiiture  of  15*  centii 
equal  to  £9°  Vahr.,  at  unce  mdicules  the  qunntity  of  alcohol 
sure  present.     As  its  name  intplies,  the  stem  is  divided  into  a 

Earts  or  'h'grees,  and  i»  so  contrived  (hat  each  degree  rcpredi 
uudiedlh  part  of  anhydrcius  or  pure  alcohol ;  thus  the  [x^nt  at 

it  floats,  when  immersed  in  any  spirit  at  a  certain  lenijieruture,  n  

cates  exaclty  the  per-centagc  of  absolute  alcohol  contained  in  that 
spirit.     The  great  Yutue  of  this  instrument  is,  that  it  jihowa  at  onct 
the  per-('enUi;:e   of  alcohol,    all   subsequent  calculations,   with 
loss  of  time  involved,  utid  the  possibility  of  inaccuracies,  being  th< 
avoided. 

Ebullioscope. — Another  instrument,  constructed  on  a  totally  dil 
ent  principle  to  the  ordinary  densimeters,  is  the  ehuHxoscope  or  eh 
tion  nkohalnmcfer.  This  instrument  is  based  upon  tJie  tncl  that 
boilio^r  puint  of  spirituous  liquids  varies  accordntg  to  the  amounCI 
alcohol  foiK.iined  in  them  (a  discovery  made  by  the  Ablto  Bn 
Vida.1,  of  Toulon),  without  its  bein^  essentially  modified,  like 
other  instruments,  b^-  the  presence  and  nature  of  any  solid  ingredit 
which  may  be  contamcd  in  them. 

There  are  several  forms  of  this  instrument;    there  is  the  ori^i 
one  of  M.  Brossard-Vidal,  and  ihc  Diodilicutions  by  M.  Conaty^ 
MM.  Lerebnurs  and  Secretan,  and  by  Dr.  Ure. 

The  nieniiriid  thermometer  used  in  the  modification  of  the  instru- 
ment by  MM.  Lercbours  and  Secretan  is  graduated  centesimaljy 
degrees,  which  correspond  to  those  of  the  centesimal  alcoholuuieter 
M.  Gay  Lussac,  and  its  bulb  is  plunged  in  the  liquid  to  be  provi 
The  liquid  is  carefully  heated  by  means  of  a  spirit  lamp,  the  flni 
of  which  should  not  be  strong,  lest  it  occasion  the  too  rapiil  ebulliti 
of  the  spirit.  Before  using  the  instrument,  it  is  nceessury  to  dcU 
mine  the  boiling  point  of  pure  water,  and  the  barometrical  pressi 
of  the  atmospht-re  on  the  day  on  which  the  experiments  .ire  made. 

In  Dr.  Ure's  modification  of  the  instrument,  the  scale  is  adapted 
that  of  Sykea'  hydrometer. 

Jt  would  be  of  the  greatest  possible  advantage  —  would  save  ii 


GIN,   AKD   ITS   ADULTERATIONS. 


533 


mense  time  aad  trouble  —  if  densimeters  of  nil  kind.-*  were  reviscdf 
and  were  reduced  to  une  uniform  centesimal  sculCf  aa  is  done,  iu  fact^ 
in  m&ny  of  the  inslruoieiits  in  use  on  the  ConUueiit. 

TUe  ebulliuscope  is  probably  sufficieiiUy  accurate  in  tlie  results 
-which  it  furuubcs  to  atifurd  consideruble  service  lo  the  disliUcr,  the 
rectifior,  the  wine  maker,  and  the  brewer;  but  is  certainly  not  so 
where  strict  analyiti:*  is  required. 

Dr.  Ure's  nio-iiticution  ot  the  ebullioscopo,  together  with  a  full 
descTiptinn  of  ittt  priiiciples  und  application,  may  be  obtained  of  Air. 
Joseph  Yourg,  Litile  Tower  Street. 

Aicithtfiometric  DUntometer.  —  Another  instrument  which  has  beon 
invented  fwr  the  determination  of  the  proportion  of  alcohol  in  tpiritu- 
oiiH  lii|uids  is  the  alcokulomctrtc  dilatumeter  of  M.  Silbermnnn.  By 
\\i\s  instrument,  the  antoiiitt  of  spirit  is  determined  by  the  uilistion  of 
the  spiritunuB  liquid  at  various  lenupcratures. 

Siteci/ic  Gravity  Botltc. — A  8till  more  accurate  method  of  deter- 
mining (he  quantity  of  alcohol  contained  in  spirituous  li<mids  from 
their  specific  gravity,  is  by  meuiis  of  the  nveajic  gravity  hottlt.  In 
using  this,  the  sumc  precautions  with  reganf  to  temperature  und  the 
presence  of  any  solid  substance  in  tlie  spirit  must  be  ob>erved. 

For  (»rdiimry  pur|K»<es,  in  the  hands  (.»f  niunufaclurcrs  and  dealers^ 
of  all  the  initttunients  for  determining;  the  strength  of  spirituous 
li<[uoi-s.  the  centesimal  aleuholorncter  nf  INI.  Gay  LuAtac  is  the  sufcst 
and  best,  nnd,  next  to  that,  Syktes*  hydrometer.  But  the  chemist, 
when  any  solid  matter  is  contained  in  the  liquid  to  be  examined, 
should,  in  all  east^.i,  separate  the  alcohol  by  distillation,  and  determine 
its  amount  from  the  diaiJllcd  liquid,  and  this  is  the  method  by  which 
we  have  proceeded  in  the  deterniinution  of  the  alcohol  contained  in 
the  samples  of  gin  tlie  results  of  the  analyses  of  which  we  have  made 
known.     The  exact  steps  to  be  adopted  are  aa  follows  :  — 

The  temperature  of  the  several  spirits  is  to  be  reduced  in  all  caaes, 
by  meana  of  u  solution  of  ice  and  salt,  to  one  uniform  degree  —  viz,, 
(jO*'  Fahr.,  and  ita  snecifn;  p-avity  at  that  temperature  determined  by 
means  of  the  specific  gravity  bottle;  1500  grains  by  measure  are 
next  distilled,  and  the  distillation  carried  nearly  to  dryness ;  the  di:!- 
lillcd  lir|uor  \i  brougfit  to  G0°  Falir,,  weighed,  and  it^  specific 
giavity  ugaiu  taken.  These  particulars  being  determined,  the  i>er- 
ci'ntnge  of  ulcoliol  is  ascertained  by  the  ilcobolo metrical  table  of 
Tndles.    (Se«j  p.  536.) 

The  third  coliiinn  of  this  table  exhibits  the  difTerencea  of  the 
'  specific  gravities  which  give  ihfi  denominator  of  the  fractiun  for  such 
d<*nsitics  as  are  not  found  sutRcicutly  near  in  the  table,  and  the  dif- 
fcHMice  of  their  numerators  is  the  next  greatest  in  the  density  found 
in  the  table;  for  example,  if  the  specific  gravity  of  the  li(]uor  found 
for  «0**  Fahr.  =  y  605  (the  per-cenloge  will  he  between  :W  and  34), 
the  difference  from  9609  (which  is  the  next  great'.'st  number  in  the 
table)  =  4,  and  the  fraction  is  i*i,  theretbre  the  true  per-ceutage  is 

11   )i    3 


w~ 

Q 

■ 

^H             S34                      GIN%   AND   ITS   ADULTE  RAT  IONS.                        ^^V 

^^B             33-i*s,  or,  (Iccimttlly,  thus,  33'31.     In  order  to  ascertain  the  amount,     H 

^^H             hy  volume,  of  alcohol  in  tlie  gin  or  other  Hpirit  iiiulcr  examination,      B 

ALCOHOLOMETRrCAL  TABLE  OF  TRALLES. 

1 

|OOM*«Mtm 

W  Fkhr- 

OUItevMvar 

AlMholln 
lOOMMXim 

00°  f  «br. 

PlffMMMor 

t^Hfint, 

Qi-*H3. 

•r»ririi. 

Undo- 

0 

&MI 

SI 

9-S16 

so 

I 

y-'j76 

J  A 

ftl 

9195 

30 

•i 

i»^>;i 

l.> 

M 

9^5 

ao 

3 

y-ii47 

11 

A4 

9*1M 

SI 

4 

9-933 

14 

U 

9-S14 

30 

5 

y-?i9 

14 

^6 

9*218 

31 

6 

QI'OB 

13 

w 

9  19'i 

31 

7 

3«*3 

13 

A8 

9  170 

» 

n 

M-BSI 

la 

W 

9148 

33 

9 

Q-DCV 

u 

00 

9116 

n 

lU 

9W7 

IJ 

01 

9-lM 

as 

II 

y-Ms 

1^ 

01 

VMS 

11 

12 

9-&H 

[l 

oa 

9000 

13 

13 

9S'i3 

\t 

til 

9*0U 

23 

14 

y  Nil 

II 

Its 

9-OIS 

13 

IS 

9-802 

10 

M 

8D8g 

.34 

14 

9rA 

1) 

«7 

SMI 

34 

17 

97HI 

10 

06 

8-04 1 

14 

^^^B 

18 

9*771 

}0 

OS 

8-017 

91 

^^^H 

19 

9-761 

10 

70 

Sttn 

7S 

» 

9-7(il 

10 

71 

8-M7 

15 

SI 

9J<I 

10 

71 

8-A41 

35 

91 

9-711 

U) 

73 

a-siT 

33 

U 

y7w 

II 

74 

8-7VI 

M 

U 

y7io 

in 

7» 

S-TfiS 

S« 

a 

y-iifl 

10 

TO 

8738 

16 

M 

O-fixy 

II 

77 

8-711 

V 

17 

9fu9 

Ul 

78 

S'flSS 

37 

IS 

yf-;8 

tl 

T9 

8-SU 

37 

w 

9ft57 

n 

SO 

»*a3i 

T7 

80 

9C4r. 

n 

SI 

8-601 

98 

SI 

9f^l 

I'i 

81 

8'fi7ft 

38 

SI 

Q-firi 

ii 

tl3 

S'S47 

38 

la 

9ft>9 

f3 

H4 

S-ftIS 

3A 

u 

y-.-M 

13 

S3 

8-4*S 

ao 

SB 

9-aH;i 

13 

80 

84S4 

30 

so 

9-57n 

13 

87 

8-488 

SO 

it 

9-SiS 

11 

SS 

8-8W 

31 

SB 

9-jni: 

13 

»9 

s-aos 

31 

39 

!*-52ti 

13 

«Q 

S'SSl 

3S 

40 

9-510 

16 

91 

8-»» 

U 

41 

9-491 

16 

91 

B-MS 

31 

4t 

UiPi 

It 

9S 

S-SM 

» 

43 

9-«I 

17 

M 

8-194 

M 

44 

9-4't4 

17 

96 

arm 

37 

45 

9-4,.'r 

(7 

M 

8-iia 

39 

4G 

9-4'« 

18 

97 

8-077 

41 

47 

9'30l 

IS 

99 

8-U34 

43 

411 

9  37  J 

18 

99 

7-9M 

46 

49 

9  3M 

19 

100 

7-939 

49 

AO 

9as5 

19 

^^H 

t  is  necessary  to  proceed  as  follows  :  —  In  order  to  find  the  ner-ccnt- 

^^P            age  of  absolute  alcohol  of  7*939  specific  gravity  in  a  sample  of  apirit,     H 

^^^■^^                                           *  AnhyOroui  Alcohol  of  ipccl6c  ffravUr  7'9t&.                                               ^M 

GIN,  AND   ITS   ADULTERATIOSS. 


i.15 


divide  the  number  of  grains  ilistilled  over  by  tlie  specific  gravily  of 
ihe  di»liUet1  spirit.  Multiply  this  quotient  by  the  per-centa;;e  ac- 
cording to  TruUcSf  and  divide  this  sura  by  the  bulk  of  the  orijjinal 
eanipto  taken;  the  quotient  is  the  per-centaje.  This  per-centniie 
muUiplied  by  700  ;;ivea  the  number  of  grainri  uf  absolute  alcohol  by 
volume  in  the  gallon.  The  above  comprise  nil  the  calculations 
necessary  for  arriving  at  ibis  result.  The  following  U  a  staleoient  uf 
the  several  sums  :  — 

1600  gr.  by  volume  yield  1334*6  gr.  by  weight;  «p.  gr.  -9484; 

per-centa;je,  4I'6'2 

«  The  bulk  oftue  dL4tilled  spirit  is  obtained  by 

As  -9484    •     1-   ::   I334-i'.   :   A 

The  volume  of  absolute  alcohol  obtained  by 

As  100-    :    A  ::  41*67    :    B 
The  per-ccntagc  by  volumes  in  the  sample  by 

As  1500   :   B  ::  100-    :   C  =  syoy 

To  find  the  quantity  of  absolute  alcohol  in  a  gallon. 

As  100- C   :  700  D 
the  quantity  required. 

From  the  construction  ofTralles*  table,  the  per-centoge  of  alcohol 
by  wcipht  may  also  be  found  —  for  instance,  multiply  the  number  re- 
prpsentinji  the  volumes  of  alcohol  given  in  the  table  for  any  deter- 
minate specific  gravity  of  the  mixture  by  the  specific  gravity  of  the 
pure  alcohol  —  that  is,  by  7*039,  and  the  product  is  the  number  of 
pounds  of  alcohol  in  so  many  pounds,  as  the  specific  grnvily  multi- 
plied by  100  gives.  Thus,  in  the  mixture,  9510  specific  gravity, 
there  are  40  mciisurcs  of  ulcihol ;  hence  there  are  also  in  95*100  lbs. 
nf  this  spirit  7  939+40  =  31*7.56  lbs.  of  alcohol;  and  in  100  tbs.  of 
the  snirit  of  0*9510  specific  gravity  33  39  lbs.  of  alcohol  are  con- 
tainea. 

On  the  Presence  of  Sulphates  in  Gin. 

The  direct  method  of  determining  whether  gin  has  been  adulterated 
with  wat»r  is  by  ascertaining  whetlier  the  gin  contains  sulphates  or 
noC 

The  addition  uf  acid  nitrate  of  baryta  to  gin  which  has  not  been 
ailulterated  with  water,  should  not  occiision  any  precipilatiou  uf  sul- 
phates, Itecause  the  water  contained  in  the  spirit  is  all  ilistilled. 
When,  therefore,  on  the  addition  of  tlie  above  rt'ajient,  a  precipitiite 
is  thrown  down,  this  is  due  either  to  the  presence  of  free  or  combined 
sulphuric  acid;  if  the  latter,  and  there  be  no  sulphate  nf  Kinc 
present,  the  sulphates  arc  derived  cither  from  the  water  useil  lor  the 
dilution  of  the  spirit,  or  from  the  alum  employed  for  clarifying  and 
beading  it,  so  thai,  alumina  being  absent,  the  iiresence  of  sulphates 
atlortls  in  all  cases  a  certun  indication  of  the  adulteration  of  gin  with 
wnter. 

Out  of  Ten  samples  of  gin  to  whicb  the  barjla  test  was  added,  four 
u  M  4 


336 


GIK,    AND  ITS  ADULTERATIONS. 


turned  slighlly  opalescent,  but  scarcely  any  depoMtion  of  sulphftt 
occurred  ;  wbile  in  six  of  the  samples  there  was  a  decided,  and  in  three 
u  consMerable,  precipitation.  These  gins  were  likcwittc  evaporated. 
the  residues  dissdlveil  in  a  little  distilled  water,  and  the  solution  di- 
videil  into  two  [larts;  to  one  the  acid  nitrate  of  baryta  wm  added 
na  1>cforc,  when  Milphnto  of  baryta  was  thrown  down  in  every  cace* 
nnd  in  most  in  great  abundance.  Throu^'h  the  other  half  of  thti  »>Iu- 
tiun  sulphuretted  hydrogen  was  passed  ;  in  nut  one  intttniice  was  anr 
white  precipitate  observed,  from  which  tlie  absence  of  zinc  is  to  be 
inferred.  These  observations  are  iniporUuit,  because  tbey  afn>rd  U5 
the  iDcanM  of  judj^ina  of  the  adulteration  of  gin  by  the  addition 
wjiter.  Heretofore  ihe  presence  of  water  h:is  been  inferred  rath* 
than  proved,  trom  the  deficiency  of  olcuhul  iu  the  spirit  suppo««d 
cnntam  the  water. 

There  h  one  only  source  of  fallacy  with  which  it  »  nere«3«ry  ll 
wo  should  be  acquainted.     Supposing  sulphuric  acid  to  have  U 
added  to  the  gin,  a  prucipitutiun  would  equally  occur,  although 
water  had  been  adiled,  on  the  addition  nf  nitrate  of  barytii.     Thia  faM 
lucy  rriay  be  guarded  a^minst  by  ascertaining  in  the  first  place  wh<;th4 
the  gin  exhibits  an  acid  reaction  or  not  to  test  paper,  and  if  it 
we  must,  then  proceed  as  dirc^itcd  in  the  article  on  Vinegar,  lor 
determination  of  free  and  combined  sulphonc  acid.  ~ 


Method  of  determining  the  Amount  of  Sugar  in  Gin* 

This  is  readiJy  determined  in  either  of  the  two  following  ways: 
The  syrupy  liquid  contained  in  the  retort  after  distillation  should 
removed  and  evaporated  wii.h  a  gentle  heat,  until  the  water  has  beei 
driven  off,  and  the  sugar  crvstalli»ed.  Or  a  fresh  weighed  portion  a_ 
tfie  gin  may  be  evaporated  tn  the  snmo  manner,  and  the  weight  of  tb^ 
sugar  furnished  by  it  ascertained.  The  latter  is  the  more  accurate 
method,  l>eeause  tlie  heat  employed  in  distilling  off  the  spirit  unt  un* 
frequently  modifies  the  sugar  considerably,  su  that  in  all  cases  it  n-ill 
nut  crystallise  properly. 

Method  of  detecting  the  Pretence  nf  Capsicum^  Qraint  of  Paradi*^^. 
other  fixed  Acrid  Substances  in  Oiu. 

Tho  presence  of  these  may  usually  be  ascertained  by  simply  taal 
a  portion  of  the  syrupy  extract  left  ufter  distillation.  The  acrid  prm* 
ciple  of  oa[>jicum  is  a  fixed  one,  and  no  part  of  it  passes  over  during 
distillation.  Of  the  two  acrid  principles  contained  in  grains  of  para- 
disc,  one  is  volatile,  and  the  other  fixed.  The  taste  of  the  fixed  prin- 
ciple very  closely  resembles  that  of  Cayenne  pepper,  but  muy  be 
usually  distinguished  with  a  little  care.  The  plant  which  furnishes 
Malaguetta  |>epper,  or  graioi  of  paradise,  is  the  Amomum  Graaa 
ParadiMi. 


GIN,    AND  ITS   ADULTERATIONS. 


537 


On  the  Detection  of  Cinnamon  or  Cassia  in  Qin. 

As  the  flavour  of  these  flepen<l8  upon  the  presence  of  essential  oils, 
they,  of  coui'se,  readily  puss  olT  durin;*  distiUutiuiif  and  the  extract, 
therefore,  does  not  usually  furnish  any  evidence  characteristic  of  iheir 
presence.  For  the  purpose  of  detecting  tbe?c  oils,  tiie  spirit  sbuuld 
be  gently  evaporated,  and  at  such  a  temperature  us  does  nut  occasion 
the  vnlatiIii*a*ion  of  the  oiln,  and  their  pre*ence  judged  of  by  the 
smell  and  taste  of  the  extract. 

Oil  the  Detection  of  Cherry  Laurel  Water  or  Spirit  of  Almond  Coke. 

Distil  the  spirit  nearly  to  dryness,  add  to  the  distilled  liiptid  a  little 
caustic  potash*  evaporate  down  to  a  smnll  bulk ;  mhl  a  few  drops  of  a 
sol  itiun  obtained  by  dissolving  protosulphfitc  fjf  iron  in  water,  and  ex- 

IKisin^  iLe  M>-madc  solution  to  the  action  of  air  for  ten  or  twelve 
lours;  a  few  drops  of  a  solution  of  pota.sh  and  a  tittle  liydrochloric 
ncid  must  be  now  added,  and  if  the  liquid  aciiuires  a  blue  tinge,  the 
spirit  under  examination  has  been  Uuvuured  with  cherry  laurel  water 
or  itpirit  of  almond  cake. 

The  reactions  are  as  follow ;  —  The  bydroc_vat»ic  or  prus^ic  acid 
of  the  laurel  water  and  almond  cake,  when  tlie  spirit  is  distilled, 
passes  over,  and  on  the  nddition  of  the  potash  i:^  cunverted  into  cvanide 
uf  potassium ;  the  addition  of  the  salt  of  iron  and  hydrochloric  acid 
occasions  the  formation  of  pruasian  blue,  which  ia  a  furrocyuaide  of 
iron. 

A  more  delicate  metliml  is  the  following,  Cnt  described  by  Liebig  :— 
The  licfuid  must  be  distilled  as  before,  notasb  S'lded,  the  bulk  of  the 
spirit  reduced  by  evaporntion  ;  hydrochloric  acid  must  next  be  added 
in  slight  excels,  and  then  a  drop  of  sulphide  of  ammonium,  and  the 
whole  treated  until  colourless.  A  little  i»erchloride  of  iron  must  now 
be  adiie'l,  when,  if  prussic  acid  be  present,  llie  liquid  will  become  of  a 
blond  re<l  colour. 

The  reactions  are  as  follow :  — The  aulphocyanlde  of  ammonium  is 
formed  by  the  reaction  of  Bulphide  of  ammonium  und  hydrocyanic 
acid,  and  this,  like  other  soluble  tiulpUocyunided,  strikes  a  blood^red 
colour  with  a  persall  uf  iron. 

On  the  Presence  of  Lead  in  Gin. 

As  we  have  seen,  H  is  commonlv  statefl  that  acetate  of  lead  Is  em- 
ployed in  the  clarification  of  adulterated  gin;  in  order,  therefore,  to 
a/tcertain  whether  the  metallic  baw  of  this  »alt  is  to  be  found  in  gin, 
eight  ounces  of  Ten  diffrrent  sampU.t  were  evaporated,  the  resiiiuea 
dissolved  in  a  little  distilled  water,  and  sulphuretted  hydrogen  pur^sed 
through  them :  in  one  case  a  decided  brownish  discolouration  ensued; 
in  some  of  the  others,  slighter  discolourations  were  observed  ;  but  in 
none  of  the  gius  was  lead  discovered  in  the  ashes  treated  with  nitric 


S38 


GIX,   AND   ITS  ADULTERATIONS. 


acid  and  water,  nnd  tested  with  io<1i<le  of  potaj^siiim.      If  lead  tv 
therefore,  present  in  nny  oftlie  samples,  St  was  so  only  in  traces. 

The  absence  of  lead  mav  bo  expluined  in  some  cases  eren  wbcrv  •*. 
has  really  been  used.  The  lead  of  the  aeetate  would  combine  wiili 
the  aulphtitcs  of  the  wuter,  and  the  insoluble  ^ulpbnte  of  leaii  wmjU 
be  preeipituted ;  it  i.s  therefore,  only  when  the  quantity  of  lead  added 
15  in  cxcejt!<  of  the  ioilphates,  that  it  would  be  fuund  in  gin,  and  when 
sul^ihute^  are  present  in  gin  wc  may  safely  conclude  that  it  does  i»ot 
coutain  lead. 

On  the  Detection  ofSnlph/tle  of  Zinc  in  Otn, 

The  sugar,  havin^j  been  dried,  and  its  wtight  determined,  b  to  b« 
rc-dissolved  in  distilled  water.  Half  of  the  solution  is  to  be  tected 
with  acid  nitrate  of  baryta  for  sulphuric  acid,  and  the  other  half 
treated  with  «ulphuretted  hydrogen,  by  whi(!h  means  ihc  zlno  will  t<^| 
thrown  down  as  a  white  hydrated  sulnhuret,  from  which,  if  suiScient^l 
of  the  si)iril  be  used,  (he  nietnl  itself  may  be  separated.  We  ^vr 
lhe.He  directions  for  the  detection  of  tins  salt,  because  it  is  rerj 
probabli;  that  it  is  somelitiies  used  to  clarify  adulterated  gin. 

Gin,  ns  alpciidy  stiilcd,  is  mnde  hv  rectifyin;;  corn  spirit,  with 
addition  of  davouring  materials.      The  Kxcise  dury  is   paid  on 
corn  spirit,  now  Hs.  jier  gallon,   hydrometer  proof.       The    duty  i^ 
Scutliind  is  now  the  same  as  that  in  Kogland,  and   in    Irelami  *" 
tjs.  *2d,  per  gallon. 

The  quantities  of  spirits  manufactured   in  the   United  Kit 
charged  with  duly,  were  — 


la  ISM. 

In  1«&^ 

EiiKUiid  aliiiifr        .... 
Scotland      „           -           -           -           - 
Ireland        „           -           .           -           . 

Tetffll       . 

o*n.. 

8,440,734 

tMU. 
I0.M4.IM 
A341.3I9 

(Mta. 

a.nT,i»o 

M.MS,m 

11.997,174 

x^jntjm 

This  return  merely  shows  %chere  the  duty  was  paid^  not  w1»ere  the 

tfpirit^  were  actunlly  consumed. 

The  return  for  1655  is  six  davs  short  of  the  year.  This  is  the 
through  all  the  returns,  as  the  faiiancial  year  is  altered. 

The  above  quantiticB  ore  exclusive  of  exportation^  which  bos 
cently  been  very  large. 


RUM,    AND  ITS  ADULTERATIONS. 


539 


RUM,  AND  ITS  ADULTERATIONS. 

Rum  U  the  spirit  obtuineii  by  the  fL'nnuntatioii  and  distillation  of  the 
refuse  juice  of  the  suj;ar  cane,  chielly  mulaases. 

It  owes  its  distinctive  smell  and  taste  to  a  peculiar  volatile  oil. 

It  diflers  from  other  spirits  in  tto  tendency  to  cause  perspiration  ;  fur 
thin  reoAon  it  is  often  used  by  those  sufTering  from  colds  and  coughs. 

The  adnlterationa  of  rum  very  nearly  resemble  those  of  gin,  and 
they  consist  chiefly  in  the  addition  of  ira/er,  whereby  its  strength  ia 
reduce*];  of  Cayenne  or  cocadux  indicus^  to  give  the  adulterated  article 
ajipurcnt  strength  ;  and,  lastly,  of  unburnt  and  burnt  attgar,  to  restore 
toe  sweetness  and  colour  lost  in  conse<{uence  of  dUution. 


Restdia  of  the  Examination  of  Samples, 

Of  Twenty  samples  of  rum  eubjected  toanalTsU,  the  alcohol  ranged 
from  47  perceut.  the  highest,  to  27  per  cent,  the  lowest,  while  Cayenne 
was  detected  in  six  of  the  samples;  that  is,  some  of  the  spirits  did 
not  contain  half  as  much  aJcobol  as  uthers.  and  consequently  were  not 
of  half  the  value.  The  same,  it  will  be  remembereJ,  was  found  to  be 
the  case  with  the  gins  examined ;  some  of  them  contained  only  half 
the  quantity  of  spirit  that  others  did,  and  this  although  the  price 
paid  for  them  was  nearly  the  sfimc  in  all  cases. 

An  instance  leading  to  fatal  results  of  the  adulteration  of  rum  with 
coccfdu*  indicu4  occurred  some  time  since  at  Liverpool.  It  is  recorded 
in  Dr.  Tiiylor's  book  on  *'  Toxicology." 

Severitl  sailors  drank  a  glass  each  of  the  sophisticated  spirit;  one 
died  the  same  evening,  but  the  others,  although  made  seriously  ill, 
ultimately  recovered. 

Lewi  has  been  discovered  in  rum  in  some  cases ;  this  is  generally  tn 
be  r^arded  as  an  accidental  impregnation,  the  lead  being  derived 
from  the  worm  of  the  still.  It  is  m  new  rum  that  lead  is  chieily 
found.  Dr.  Traill  found  that  the  spirit  received  into  a  tumbler  us  it 
came  from  the  still  always  coutuine<i  lead,  but  that  it  diaappeare<l  from 
the  same  spirit  afker  having  been  kept  iu  an  oukcu  ciisk  for  some  time. 
The  explanation  of  this  curious  fact  i.s  that  the  spirit  extracts  tunnin 
from  the  cask,  and  the  lead  uuitiug  with  this  forms  an  insoluble  com- 
pound and  becomes  precipitated. 

There  is  a  kind  of  rum  termed  "  Pineapple  Rum,"  This  flavour 
of  pineapple  Is  communicated  to  the  spirit  by  steening  in  it  slices  of 
the  pine.  Recently  chemists  have  found  out  uetuods  of  imitating 
very  exactly  the  flavour  of  the  pine,  and  hence  this  artificially  prepared 
tlavouring  is  often  bad  recourse  to  in  this  country  to  convert  not  only 
ordinary  rum,  but  even  ordiwirj  spirit  into  **  Tincapple  Rum.** 


540 


BRANDT,    AND   ITS   ADULTERATIONS. 


This  fluvouring  may  be  prepared  by  distUlinj;  batter  with  sulphan'c 
ncid  and  iilcofaulf  or  bv  combinini;  umylic  or  potato  ether  wiih  butTric 
uciti,  nnd  then  dissolving  il  in  alcohol.  ThU  flavouring  is  uiucb  used 
in  sweetmeats. 

On  the  Detection  of  the  AduUendions  of  Rwtu 

The  methods  to  be  employed  for  the  detection  of  usder^  *^oi^% 
Cayenne.,  or  grains  of  paradixe  and  /rwrf,  nre  the  ^amc  as  thuFu  given 
for  the  discovery  of  the  correspontling  ailullenitionH  of  gin.  'ITie 
process  for  the  detooiiitn  of  eoccultu  inaicuM  is  destTibod  at  p.  513  ; 
11  ia  more  easy  to  discover  the  presence  of  thia  putM)n  in  runi  than  in 
beer,  owing  lo  Uie  smaller  qiiantily  uf  extractive  mailer  contuineil  in 
that  spirit.  A  very  eKcutltint  method  of  determining  the  presence  of 
cocctiius  indicus  is  to  evaporute  about  half  a  pint  of  rum  to  drjrnesi, 
to  dissolve  tlie  extract  in  about  ten  ounces  or  so  of  water,  and  to 
place  in  it  a  small  Live  G^h.  If  the  spirit  contain  picrotoxin  ibe  fi^ 
will  soon  exhibit  the  usual  symptoms  of  poisoning  by  that  deadir 
Bubsirtnce. 

The  Customs'  duty  on  rum  is»  in  Enghuul  and  Scotland,  8*.  2dl 
per  gall.,  Iiydrumeter  pnHjf ;    in  Ireland,  Gs.  Ad.  per  gallon. 

The  quantities  taken  for  borne  consumption  in  the  United  Kingvloai 
i\-ere,  in  1854,  3,227,J'J-2  gullti. ;  in  18. j,  3/224/292  galls. ;  in  nine 
months  of  1 856,  2,36 1 ,753  golU. 


BRANDY.  AND  ITS  ADULTERATIONS. 


Brandt  is  rhe  spirit  obtained  by  the  distillation  of  wine.  When  first 
distilled  it  is  quite  colourless,  but,  after  having  been  kept  for  s-ame 
time  in  an  oaken  cask,  it  becomes  of  a  pnle  amber  tint,  the  cfdour  bein^; 
derived  from  the  w<K>d  of  the  cask.  The  \Qry  dark  brandiea  owe 
their  higli  colour,  whereby  tbeir  flavour  is  much  injured,  to  tfunti 
rtugur.  The  characteristic  taste  and  aroma  of  brandy  is  due  lo  the 
presence  of  a  volatile  oil  obtained  from  the  grape. 

The  best  brandies  are  those  of  France  ;  they  are  hut  slightly  rec^ 
tifi(.'d,and  therefore  are  not  strtmg,  cnntaining  usually  nearly  half  tb< 
weight  of  water.     The  rensun  of  tliisls.  thut  the  rc-^listillation  of      _ 
Kplrit  injures  the  volatile  oil,  upon  which  the  excellence  of  the  br&nd/ 
depends. 

One  of  the  most  frequent  ftdaltcrations  of  brandy  is  witli  water. 


BHANDY,   AND   ITS  ADULTEUATI0K8* 


541 


Another  aduherfttion  is  with  tpirit  obtamed  irom  corrit  ngar 
■mola»$es^  beet  ruoi-,  or  potatoet. 

In  some  cases  one  or  other  of  these  different  spirits  oxe  substituted 
lor  genuine  hrandr»  the  flnvour  of  brandy  beint;  comnuinicAte<l  to 
thcui  by  artiHcial  flavouringn,  nnd  the  requisite  coluur  bc'ing  obtained 
hy  racfins  of  burnt  supiir. 

Mui'h  of  even  the  French  brandy  imported  into  Lhia  country  con- 
sists either  in  part  or  wholly  of  corn,  and  more  frequently  of  beet 
root  spirit. 

Strange  to  relate,  a  very  larjfc  quantity  of  corn  spirit  has  of  lato 
been  imported  into  France,  to  be  used  in  the  adulteraiion  of  French 
brandy.  Part  of  this  corn  tpirit  is  returned  to  us  in  the  fltrm  of 
brnndy,  this  adulterated  brnndy  on  its  arrival  in  this  country  under- 
f^oing  in  many  in^tunoes  further  adulteration  by  the  addition  of  more 
corn  spirit,  and  thus  it  becomes  doubly  adulterated. 

The  artirlL'  known  as  **  JJrrfwA  irwnJy "  consitts  for  the  most  part 
of  corn  Ppirit  lluvonred.  The  favouring  is  accomplished  sometimes 
by  the  adiJilion  of  a  little  {genuine  brandy,  but  more  frequently  by 
distillation  m\'  the  muric,  the  name  given  to  the  refuse  nkins  and  pips  nf 
the  grupe  left  after  the  distillation  of  the  wine.  "  The  llrittsh  brandy 
nioke^  Imys  up  this  murk,  and  imports  it  into  this  t'ounlry,  paying 
upon  it  the  same  duty  ns  upon  wine.  By  distilling  Uritiiih  molasses 
over  these  lees  the  manufacturer  ohtainti,  to  some  extent,  the  pecu- 
liar Havour  which  characterises  French  brandy."  * 

Dr.  Normandy,  in  reply  to  a  mieslion  by  Mr.  Scholefidd,  makes 
these  remarks  in  regard  lo  the  llavouring  of  brandy  by  means  of 
artificially  prepared  essences: — "brandy  is  extensively  prepared  in 
this  country,  cs|«cial)y  since  the  discoveries  of  modern  chemistry  of 
producing  essential  oils  nriificially, — oils  which  hare  the  (Sdourof  that 
particular  ether  to  which  brandv  owes  its  llavour." 

When  molasses  spirit  is  employed  it  is  necessary  it  should  be  pre- 
viously rectified  by  ditttiliution  over  freshly  burnt  charcoal  and  (puck- 
lime.  Indeed  it  is  essential  that  all  ?ptrit5,  especially  corn  spirit, 
emploved  in  the  adulteration  of  brandy  should  undergo  carelul  rec- 
tification, in  order  to  free  them  from  the  jHiculiar  tastes  and  (Hlours 
which  might  but  too  plainly  reveal  the  nature  and  origin  of  the  spirit. 

Receipts  are  of  course  not  wanting  for  the  manufacture  uf  spurious 
French  brandy.  Dr.  Ure  gives  the  following  formula,  as  one  which 
is  employed  for  converting  corn  spirit  into  imitation  brandy.  Pure 
alcohol  is  to  be  diluted  to  the  proof  strength,  to  every  hundred  weight 
of  the  spirit,  half  a  pound  of  argol,  wine  stone,  or  cream  of  tiirtar  pre- 
viously dissolved  in  water,  is  added,  as  well  as  a  little  acetic  ether, 
some  French  wine  vinecar,  bruised  French  plums,  and  (lower  stufi 
from  Cognac  (murk).  The  spirit  is  then  to  be  distilled  tiff,  with  a 
gentle  fire,  in  an  alembic  furni5hed  with  an  agitator.  The  spirit 
which  comet  over  is  coloured  with  burnt  sugar  to  the  tint  required, 

•  TriUivf  I'rftde.f-  110. 


M9 


BUANDT,    AND    ITS   ADULTEUATIONS. 


nnd  rou^liencd  to  the  taste  with  a  few  drops  of  the  Uacturt  of 
eaiouhu  or  kino. 

Oak  sawdust  and  tincture  of  grape  stones,  prepared  pur|i(«rlT  fram 
the  murk,  are  used  to  impart  to  uew  brandy  the  taste  of  an  old  tfit't 
which  bss  become  ripened  in  an  oaken  cask. 

'i'lie  author  of  a  work  on  "  Alalted  and  Uaoialted  Com,  coonedai 
with  Hrowing  and  Di&tilling"  gives  the  following  receipt  formakiffp 
an  adulterated  brandy,  suitahlu  for  retail  purpoites  :  — 


To  10  puncheons  of  brandy 
Add  Qavouring  raisin  spirit 
Tincture  of  j^raios  of  paradise 
Cherry  laurel  water     - 
Spirit  of  almond  cake  - 


1081  gmU< 
118       „ 

2       ^ 


1207  galloni. 
Add  alpo  10  handfuls  of  oak  sawdust,  and  give  it  complexwD  viik 
burnt  su^ar. 

The  cuse  of  brandy  aflurds,  (hen,  an  apt  illustration  of  the  pbefcrf 
refinement  to  which  the  art  of  adultcratiou  haa  reached  in  tbcKd^a 

liesuUa  of  the  Examination  of  SampUs. 

Ot  Eighteen  samples  of  brandy  subjected  to  examination'^ 

The  alcohol  ranguJ  from  30  to  50  per  cent. 

The  majority  of  tiie  j*amplca  ctmsisicd  of  so-called  Brituk 

Nonrly  all  the  brandies  were  coloured  with  burnt  rugar. 

Lastly,  in  none  of  the  sdraplcs  was  Cayt^une  present.  ThSg  is 
ticularly  w<irt1iy  of  note,  because  some  of  the  brandies  were  prae 
at  houses  at  which  bulb  tbc  gin  and  the  rum  were  found  to  w  aifait- 
tcTiited  with  that  substance.  This  at  lea^t  tbows  that  ao'id  sab- 
Stances  are  not  so  frequently  cmplored  in  the  aiiulierntion  vtfhntA^ 
as  of  other  spirituous  liquors.  This  result  la,  thereiure,  ii  ma* 
decree  stitisfartory. 

Brnmly  nnd  rum  are  seizabic  if  sold  by  or  found  tn  the  pnoraMa 
of  the  dealer  uiilcfs  it  possesses  a  cerluin  strength,  17  f>cr  cent.  (ida« 
proof,  by  S}kcs'  liydrometer.  The  following  arc  the  words  Mf  tli 
Act,  30th  Geo.  111.:  — 

"No  distiller,  rectiGer,  compounder,  or  dealer  shall  acrre 
out  any  foreign  spirits  of  a  lower  streu^th  than  that  of  oi 
under  hjdromoter  proof,  nor  have  in  his  |M>S5ession  uny  for*i| 
mixed  together  except  shrub,  cherry  or  raspberry  briuuly,  rfj 
stren;;tli  than  as  aforesaid,  upon  puin  of  such  spirita  being  fhHI 
and  such  spirits,  with  the  casks  and  vessels  contiiining  tlicnnie,Si^ 
he  seized  by  any  officer  of  Excise." 

It  will  be  perceived  that  many  of  the  brandies  examined  br  ■ 
were  sold  in  violation  of  the  act  above  quoted,  and,  u  usaal,  wf  * 
let  or  hindrance  by  the  Excite. 


BBANDYy  AKD  ITS  ADULTEUATI0N8. 


54S 


On  the  Detection  of  the  Adulterations  of  Brandy. 

The  metlioijp  nlrendy  pointed  out  umlor  the  lieadK  of  Gin  and  Hum, 
are  equally  apjilicnhle  to  the  discoYory  of  the  udultprations  of  Lrnndy ; 
the  Blrun;;lh  ciC  the  brandy  mui-t  be  ascertained,  ihc  kind  of  spirit  it' 
possible,  tbti  amount  and  nature  of  the  cxiractivCj  and  the  sulphates 
present  mu&\  likewise  be  determined. 

\Vc  will  now  inquire  as  to  the  capabilities  of  the  Excise  to  detect 
ndulleratiuns  iu  spirits ;  and  firnt  the  render  may  be  reminded  that 
udulterutiou  huM  been  found  to  be  rife  in  gin,  rum,  and  brandv.  Aa 
III  »o many  other  cjwes,  we  need  only  refer  to  the  evidence  of  iMr.tieorge 
Pliitlip!}  to  be  made  acquainted  with  ibe  state  of  the  case  as  respects 
the  Excise. 

Air.  ViUierx.  "We  have  had  evidence  here  to  theeffect  that  a  mix- 
ture or  adulteration  is  invariable  in  all  public  house*;:  what  is  the 
course  adopted  with  a  view  to  delecting  those  practices  ?"— "The  fact 
is,  we  have  abandoned  what  is  termed  stock  taking  of  the  retailers. 
The  trade  is  thrown  open,  and  they  are  left  to  do  pretty  much  as  they 
like.  At  the  present  moment,  so  far  as  8(04  k  taking  is  concerned,  we 
have  power  to  take  their  stock  if  we  think  proper  ;  the  goods  are  sent 
in  with  ft  permit,  and  the  trailer  enters  tliem  in  a  book,  and  when  the 
ofBoer  goes  he  tjdtcs  up  this  document  representinjf  the  receipt  of  a 
certain  syiirif,  and  if  we  think  proj>er  wc  can  take  the  stock." 

"  Is  not  the  revenue  defrauded  in  ibis  way  f  *' — "  I  think  not.  If  the 
public  wished  to  drink  gin  at  50  per  cent,  under  proof,  the  retailer 
eould  have  it  sent  to  him.  The  law  prohibits  him  from  putting  anjjthing 
to  it  himself.  He  it  not  allowed  to  add  sugar  or  water  to  hit  giu  ;  U  it 
(tn  net  of  componnditig  which  vre  do  not  recognige." 

*'Theduty  is  not  paid  on  gin  and  water?" — ''No;  it  is  paid  on  the 
tipirit.  Suppose,  for  instance,  the  publican  buys  his  gin  at  17  under 
proof.  That  may  be  too  stron<;  for  ordinary  tasie,  and  therefore  the 
publican,  when  begets  it  in  at  that  stren«rlri,  reduces  it  probably.  / 
caHHot  my  that  he  doeit  to  from  actual  hnotvledge^  but  we  moy  suppose 
that  he  doea." 

It  is  notorious  that  the  publican  almost  constantly  reduces  his  gin 
with  water,  adds  sugar,  and  often  Cayenne  and  other  injiredients.  As 
has  been  stated  by  Mr.  Phillips,  the  law  prohibits  this  net  of  com- 
|muiuling,  an<l  has  charged  the  Excise  with  the  duty  of  ascertaining 
whether  the  prohibition  is  observed  or  not ;  but  the  kxcise  leaves  the 
publicans  "to  dojprelty  much  as  they  like,'*  and  consequently  they 
lire  unable  in  speak  m  facts  in  regard  to  the  adtdteration  of  gin  which 
nre  notorious  to  the  public  ill  targe.  But  let  us  ubsen'e  what  further 
information  Mr.  Phillips  oflbrds  the  Committee  respecting  the  adulter- 
ation  of  spirits. 

Chairman.  "  Have  you  beard  of  Cayenne  pepper  being  mixed  with 
ginf"  —  "I  have  /iwira  so  ;  it  coaM  be  delected,  of  course.*" 

Afr.  Vdtirrs.  "Have yon  never  had  any  experience  of  the  adulters- 


544 


WINK,  AND   ITS    ADULTERATIONS. 


1 


/db 


tion  of  spirits  during  tbe  twelve  years  you  have  spoken  of  P  **• 
not  recollect  a  ctue.** 
"  la  bramly  ever  adulterated  ?" — "  If  you  view  colouring  matter  m 

adulteration  it  is  always  adulterated."  , 

*' Do  you  know  if  it  is  ever  reduced  with  water  and  then  madcl 
stronger  by  the  introduction  of  oilier  ingreflicnta  ?  " — *'  I  cannot  speak] 
to  the  use  of  other  ingredients.  I  have  no  knowledge  of  what  a  par-' 
tit-'ulur  trader  may  do." 

"Tlieevidence  wbirh  hiisbeen  given  before  the  Committee,  therdb 
has  not  reached  ibe  Excise  yel  ?  '  —  "I  have  not  seen  it." 

These  replica  ccrfuinly  evince  an  amount  of  ignorance  of  the 
adulteration  whtili  iictnally  occurs  in  the  articles  enumerated,  which, 
considering^  the  jio.sition  auddutit^s  of  tlic.  Kxiise,  is  really  nstoundin". 

Customs'  duty  on  bnuuly,  IS.t.  iier  pall.,  hydrometer  proof. 

Taken  Tnr  IionK*  consumption  in   1854,    1,863,622  gaits.  ;    i 
l,.Vi6,2-21  yiiUs.;  in  nine  iiionlhs  of  185G.  1,109,497  galls. 

The  quantity  in  1853  was  2^78,961  galls.  The  diminution  is  owing 
to  the  cost,  ex-duty,  having  been  more  than  doubled. 


in  1SS5. 


WINE,  AND  ITS  ADULTERATIONS. 

IK  is  the  furmented  Juieeof  the  gr.ipe  ;  it  is  distinguished  from  other 
fermented  nnd  dcoholie  liijuid^  by  conLaiiting  bitartrate  of  potash, 
or  cream  of  tartar,  commonly  called  wineatone,  a  coostitueut  of  the 

The  numerous  varieties  of  wine  are  occasioned  by  ditTcrcncea  of 
soil,  climnic,  season,  nnd  by  the  kind,  quiility,  and  condition  of  the 
grape  as  to  ripeness,  the  mode  of  fernientaiion,  the  manner  and  tem- 
perature at  which  thu  wine  is  preserved,  and  by  its  age. 

All  wines  pofscss  a  characteristic  taste  and  aroma  or  bottquelf  as 
it  is  termed.  These  varieties  depend  upon  dilTerencea  in  the  voliitile 
nnd  aromatic  principles,  mostly  of  an  oily  nature,  generated  during 
fermenlatinu  and  di^itillation.  Contrary  tn  what  nii^hl  hare  been  an- 
ticipated, the  wines  of  warm  countries  po:^scss  but  little  bon({uet  ;  {hose 
of  the  "central  departments  of  France  have  it  in  a  marked  degree, 
whilst  the  wines  of  the  still  more  northerly  situated  Germany  have 
the  most  intense  perfume.  The  grapes  which  are  gathered  before 
the}*  are  completely  rif>e  have  the  strongest  bouquet."  • 

The  tirious  odour  of  wine  is  produced  by  tbe  presence  of  a  volatile 
substance,  which  has  received  the  name  of  anattthic  ether ;  it  poa- 

•  Trkki  of  Trad?,  p.  IM. 


WIKE,   AND   ITS  ADULTERATIONS. 


545 


a  sharp,  disagreeable  taste,  bat  the  odour  of  wine  in  iia  most 
powerful  degree  i  it  is  proJuct;d  during  fermt^nlation,  and  seeniB  to 
increase  in  quantity  in  wine  bv  keeplitg,  oa  the  odour  of  uM  is  stronger 
titan  thttt  nf  new  wines. 

The  different  wines  may  be  classified  under  one  or  other  of  the  fol- 
lowing heads: — Stropg  and  lights  sweet  and  dry^  tparkling  and  still, 
vhite  and  reii. 

The  strong  wines,  such  as  sherry,  port,  Madeira,  &Cm  are  made 
^m  thnroughlr  ripened  grapes,  grown  in  southern  countries,  and 
which,  from  containing  more  (lugar,  yield,  when  fermented,  a  greater 
amount  of  alcohol,  the  ingredient  which  gives  to  wine  its  strength. 

The  amount  of  ab»oiuic  alcohol  usuuUj  present  in  wines  coiuuionlj 
xn  use,  is  as  follows  :  — 

7ti  100  Metuuret. 


Johnston, 


Port 

-     21  to  23 

Sherry 

-     IS  to  25 

Idudeira   • 

-     18  to  22 

Marsala    - 

-     14  to  21 

Claret      - 

-       9  to  15 

Burgundy 

-       7  to  13 

Rheuish    - 

-       8  to  13 

Moselle     -        . 

-       8  to    9 

Malmsey 

16 

Tokay      - 

9 

Charapsgne 

-       6  to  15 

Brande, 
Marsala    - 
Fort 

Madeira  - 
Cwpe 
Sherry 
Montollado 
Constantia 

Malaaa    .        .        . 
Buceltas 

liermitage  (White)  - 
(Red)       - 
Claret       - 
Malmsey 
Santeme 
Burgundy 
Tent 
Hock 

Champagne 
Viu  de  Grave  - 
Cote  Rdlie 
Tokay       - 


-  35 

-  23 

-  22 

-  20 

-  19 

-  12 
-  18  to  20 

-  18 

-  18 
■   17 

12 
15 
16 
15 

-  14 
13 
12 
12 
13 
12 
10 


From  Liebig*t  Letters.    Arranged  according  to  Price. 


Steinberger, 

Mareobrunncr, 

Hattenhcimer, 

Steinberyer, 

Rudesheimcr, 

Mareobrunncr, 

Geisenbrunner, 


1846 


1822 


Alcottol  per  Ccot.        He»l<ltw. 


1017 
1114 
10-71 
1087 
]2'61 
1160 
12-60 

K  If 


10-56  "I 

5-18  {-Freaeninfl. 
4-21  J 
994 

5-39 
510 
306 


MA 


WINE,   AND   ITS   ADCLTEUATIONS. 


The  per-centage8  of  alcohol  in  the  wines 
Dr.  Jones  found  lo  be  as  follow  :  — 


in  u&c  in  this   country 


Alcohol  br  Mfwure. 
Port-        -        -    from  20-7  to  23-2  per  cent 
Sherry       -         -  15'4  to  247         „ 

Madeira    -        -  1&-0  to  197        „ 

MarsaU     -        -  19*9  to  211        » 

Claret        -        -  91  to  11-1 

Burgundv  -        -  1 01  to  13*2        „ 

Rhine  Wine        -  9  6  tu  130         „ 

.    Moselle      .        -  87  to    9*4        „ 

Chanipngnn         -  141  to  14*8         „ 

These  results,  which  are  rather  high,  were  obtained  by  means 
I  he  alcoholometer  of  M.  Geisler. 

Some  idea  of  thii  relative  strength  of  wine  may  be  formed  when 
is  mentioned  thai  (^ood  brandy  ami  rum  usually  contain  Ironi  4S  to 
per  ctmt.  of  absnlute  alcohol,  poor  beer  about  2  percent.*  porter  rati 
over  3,  and  stout  about  5  or  6  per  cenL  We  thus  perceive  that  M 
Sftlfi,  port,  and  Madeira  contain  about  half  as  much  olc-ohul  as  brandy^ 

The  amount  of  alcohol  in  wines  is  maleriolly  affected  by  their 
it  beiji|*  iu  most  wines  ruduced   in  ouantity   by  keeping;,  part  of  ic 
being   toi't   by   the   evaporation   which  takes   place  even  in   lightly 
corkcil  bottles,  and  part  by  the  oxidation  uf  the  alcohol,  and  it£  con- 
version into  acetic  acid. 

To  this  rule,  however,  Madeira  and  sherry  form  exceptions,  since 
these  rather  increase  In  strength  for  the  first  five  or  six  years,  owing 
to  the  conversion  of  the  sugar  which  they  contain  into  alcohol. 

In  connection  with  the  strength  of  wine  iVsaciiiity  maybe  consider 
since  in  some,  though  not  in  all  casus,  the  acidity  in  part  is  dependen 
upon  the  strength.     While  the  acidity  of  beer  is  occasioned  mainl 
by  acetic  acid,  and  that  of  cider  by  lactic  acid,  that  of  wine  is  produ 
by  tartaric  acid,     In  the  last  two  liquors,  hftwever,  acetic  acid  also 
present   in   greater  or  less  proportion ;    it  is  always  fomie<l  at 
expense  of  the  alcohol  when  the  fermentation  proceeds  too  far. 

Wines  made  from  unripe  griipes  HoiuL'times  contain  citric  acid;  as 
the  truit  ripens,  this  acid  is  replaced  by  the  tartaric. 

Tartaric  acid  exists  in  the  juice  of  the  grape  and  in  wine  in  co 
bination  with  iiotash,  forming  what  is  called  bitartrate  of  potash 
cream  of  tiirtar,  the  sour  taste  of  which  i»  well  known.     When  win 
is  left  at  rest  this  salt  is  in  part  precipitated,  and  the  wine  become* 
much  Ihe  less  acid.     This  is  one  of  the  good  effects  of  ngc  upon  win 

The  following  is  the  order  o( acidity  of  some  of  the  chief  wine«  c 
flumed  in  this  country 


Sherry  is  the  leant  ofirf. 
Fort  comes  neat. 
Champagne. 
CUrcL 


Madeira. 

Burgundy. 

Rhine  Wines. 

Moselle  is  the  most  tfcitf^ 


WINE,   AND  ITS  ADULTKUATION8. 


547 


The  principal  sweet  vines  are  Toka^,  tent,  Frontignac,  and 
%!a)mscy  ;  they  are  made  from  p-apes  so  ripe  that  tbey  are  almost 
shrivellod  up  to  raisins,  and  wbion  therefore  contain  much  aug:ir,  the 
fermentation  also  being  arrested  before  all  the  suj;ar  is  converted 
into  alcohol. 

The  onler  of  sweetness  of  ctTtnin  winei^  or  the  amount  of  sugar 
present,  was  ascertaineil  by  Dr-  Bence  Jones  to  be  as  follows :  — 

Claret^  tiur<;und_T,  Rhine,  and  Moselle  wine?,  including  hock,  con- 
tun  no  sensible  quantity  uf  sugar. 


Sherry  contains 

-     4  to  18 

grains 

of 

sugar  in  the  ounce 

Madeira  - 

-     6  to  20 

91 

n                     vt 

Champagne 

-    6  to  28 

» 

Vt                             )* 

Port 

*  16  to  34 

n 

*t                     *i 

Malmsey* 

-  56  to  66 

n 

*>                     » 

Tokay-     - 

74 

11 

n                    tf 

SAmos     • 

88 

„ 

n                     ti 

PascareUe 

- 

94 

It 

n                     H 

The  siifrar  was  estimated  by  the  saocharometer  of  M.  Solcil. 

In  the</ry  wines,  as  in  some  kinds  of  sherry,  esperiallv  Amontillado, 
the  fermentation  is  prolonged  until  nearly  all  the  sugar  has  diaap- 
pearcii. 

In  effereexcing  or  sparkling  wines  the  wine  is  put  into  casks  or  bot- 
tles while  the  fermentation  is  still  progressing :  the  consequence  of  this 
is  that  much  carbonic  acid  accumidotes  in  the  wine,  cuusmg  it  to  efler- 
Tesce  when  unourked. 

Both  U-'hUt  and  red  winea  may  be  made  from  the  coloured  or  red 
grape.  The  colouring  mutter  is  situated  in  the  husk.  The  white 
wines  are  prepared  from  the  juice  of  the  grape  only,  while  for  the  red 
wines  the  whole  grape  ia  used. 


On  thb  Adultebatioks  or  Wisb. 

The  wines,  of  the  adulterntinn  of  which  we  propose  to  treat,  arc 
port,  tlierry,  Madeira,  Champagne,  claret,  hock,  and  Moeelle. 

There  are  no  manufactured  articles  Hubject  to  greater  adulteration 
thun  wines,  and  this  on  account  of  the  high  price  they  bear,  the  extent 
tu  which  they  are  consumed,  and  the  ease  with  which  many  of  the)n 
may  be  imitated,  and  this  in  a  variety  of  ways  which  altogether  ImOle 
the  cflorts  of  science  to  detect. 

Although  many  adulterations  arc  practised  upon  wine  which  cannot 
be  and  never  arc  discovcrcil,  yet  mui-h  evidence  has  been  obtained 
of  the  general  prevalence  of  ndulterai ion  in  wine,  and  science  has 
also  supplied  means  for  the  detection  of  many  of  the  Buphislications 
practised. 

V  B   2 


548  WINE,   AND    ITS    ADULTERATIONS. 


r 


PORT,  ANT)  ITS  ADUT^TERATIONS. 


Of  all  wines  none  u  Bubject  to  more  adulteration  thnn  port  wine. 

The  first  adulturntion  o(ten  pi-actised  upon  it  consists  in  m  ' 
hrmuiy,  sornetiuies  to  the  extent  of  twelre  gallons  to  Uie  pipe,  em 
while  leriuen ration  is  goin^  an.     This  practice  is  aaid  to  be  luost  in- 
jurious to  the  flavour  of  the  wine. 

Another  practice  \&  to  increase  the  colour  of  the  wine  hy  aPti- 
6cia!  meiins :  this  is  umiolly  efTecteil  hy  tlder  berry  coltmring,,  more 
brandy  beinfj  added  with  the  colouring.  So  common  is  thia  prmctKC, 
that  e!der  berrj  treea  are  grown  in  many  of  the  vioeyarda,  while 
other  prnprit'tors,  it  is  asserted,  have  been  known  to  pajr  as  much  tf 
400^  per  annum  for  the  tflder  berries  used  by  them. 

Before  thr  wine  in  5hip[>t'd  more  brandy  is  adde<),  and  aI«o  aome- 
Imies  a  mixture  denominated  Jerupiga,  This  is  a  compound  expnadv 
prepared  for  the  adulteration  of  port  wine  ;  it  consists  of  /A^  jmict^ 
elder  berries^  brown  tugar^  un/ermented  grape  Juice,  and  brtxnd^. 

Further,  this  article  is  extensively  imjwrted  into  this  country  for 
the  adulierntion  of  port  wine.  By  a  return  recently  made  to  tlie 
HoUMe  of  Commons  on  the  motion  of  Mr.  Oliveira.  Al.  P,,  it  appear* 
that  jerupiga  was  iniported  and  used  by  some  of  the  first  bouaee  ea- 
^aged  in  the  wine  trade  in  this  country. 

Another  substance  used  to  colour  port  wine,  both  in  Portugal  mm! 
at  home,  is  logwood;  large  quantities  of  this  dye  are,  it  ia  stac^Ml,  im 
jwrted  into  Uf*orto. 

Lastly,  jrnrt  wines  are  adulterated  at  Oporto  by  the  additiim  of  iit 
fenor  winea,  imported  for  the  purpose.  It  is  by  this  means  that  the 
supply  of  port  wine  is  maintained  at  a  trjlerably  uniform  average^  do 
matter  what  may  have  been  the  vintage. 

It  U  therefore  evident  that  port  wine  is  subject  to  a  large  amount 
of  adulteration,  even  before  it  reaches  this  country;  after  ita  arriTal 
here  it  is  frequetitly  Buiyected  to  further  adulteration. 

Sometimes  it  is  dilute4l,  braiidied,  and  then  coloured  by  the  idlx- 
ture  termed  jerupiga,  or  by  means  of  lo^ood.  The  briJIiancT  o 
its  colour  is  sometimes  incrert'ied  by  means  of  alum^  and  if  turbid, 
it  is  cleared  by  gypmm^  while  incrcHsed  asCringency  is  somt^times 
imparted  by  meauti  of  oak  satrdusi.  Not  unfrequentty  pei-uliar  Am 
voura  or  bouquets  ore  artificially  communicated  to  port  wine :  the 
principal  substances  used  for  this  purpose  ore  extract  of  sweet  briar, 
i/rrU  root-,  cherry  laurel  xvater^  &c. 

In  other  cases  the  true  fhivour  and  taste  are  given  to  foctitioua  port 
by  means  of  a  tincture  made  from  the  *ee<is  of  the  grape. 

The  resemblance  to  port  is  further  increased  hy  tuidinj^  salt  of  tnrtar 
to  the  winr.',  which,  it  will  be  remembere<l,  is  one  of  the  natural  con- 
stituents of  the  grape.  This  salt  after  a  time  becomes  in  part  de- 
posited in  a  crystalline  state  from  genuine  port  wine,  either  on  the 


I 


WINE,   AND  ITS  ADDLTERATIONB. 


S49 


Hides  of  the  cask,  or  even  in  the  bottle  in  which  it  is  kept,  it  oaiTTuig 
down  with  it  some  of  the  colouring  matter  of  the  wine.  The  fabri- 
cators of  spurious  port  have  not  forgotten  to  imitate  this  criterion  of 
a  ffooil  wine. 

For  this  purpose  a  hot  saturated  solution  ofcrenmof  tartar,  coloured 
red  with  a  docoftion  of  Brazil  wood,  i*  placed  in  tlie  cask  nnd  rolled 
about  in  it  until  the  aides  become  covered  with  the  crjstdlised  sub- 
ttance,  after  which  the  imitation  wine  is  poured  in.  Bottles  even 
are  treated  in  the  same  manner,  and  the  very  corks  are  also  dyed. 
The  crust  of  port  wine  is  nn  indication  of  its  age,  and  not  only  is  this 
produced  in  tlie  manner  just  pointed  out,  but  likewise  in  other  ways  ; 
one  of  these  is  to  put  new  jK>rt  into  warm  water,  the  temperature  of 
this  is  raised  to  the  boiling  tH>int,  alter  which  the  wine  ia  put  back 
into  the  cellar,  when  it  boon  aoposita  a  crust  which  might  pass  for  the 
growth  of  years. 

But  wine  not  unfrequently  cimtains  iead :  in  some  cases  this  ia  an 
accidental  impurity  or  impregnation,  but  more  frequently  it  is  to  be 
reffarded  oj  &n  adulteration. 

When  lead  is  accidentally  present  it  is  derived  from  the  ^ot  used  in 
cleaning  the  bottles. 

When  added  intentionally  to  wine^  it  is  so  for  the  purpose  of  pre« 
Tcniinff  ii  from  tuniing  sour. 

Dt,  Watson  *  states  that  the  practice  of  adding  lead  to  wine  was  at 
one  time  uommon  in  Paris. 

Dr.  Warren  t  relates  an  instance  in  which  thirty-two  persons  were 
made  Kriou!<lv  ill  by  drinking  wine  a<lulterated  with  lead;  one  of 
them  died,  and  another  became  paralytic. 

In  Dr.  UroV  **  Dictionary,"!  we  find  these  remarks  In  relation  to  the 
use  of  lead  in  France :  —  "  This  distemper  (excessive  acidity)  formerly 
gave  rise  to  the  very  dangerous  practice  uf  adding  litharge  as  a 
sweetener,  whereby  a  quantity  of  acetate  or  sugar  of  lead  was  formed 
in  the  liquor,  productive  of  the  most  deleterious  consetiuences  to  those 
who  drank  of  it.  In  France  the  rcguUtions  of  the  police  and  the  cn- 
lighfi^ncd  ((urveillance  of  the  Council  of  Salubrity  huve  completely  put 
down  (his  gross  abuse." 

Lastly,  Graham  in  his  ^' Treatise  nn  Wine  Making,"  published 
nany  years  since, under  the  article  "Secrets,"  belonging  to  the  mys- 
teries of  vintners,  recommends  lead  to  l>e  used  fnr  sevend  purposes. 
The  following  receipts  are  copied  from  that  mischievous  work :  — 


"  To  hinder  Wine  from  turning. 

"  Put  a  pound  of  lead  melted  in  water  into  your  caik  pretty  waim, 
and  stop  it  close." 


•  Chrmtral  BMaji.  vol.  vlIL  p.  3fjO. 
t  MedlcaJ  Tnna.  wL  II.  p.  Ml 


t  Vol.  H.  ^  11 


N  It  3 


S50  WINE,  AND   ITS  ADULTEKATIONS 


"  To  soften  Grey  Witu. 

"  Fut  ID  a  liltle  vinet^ar  wbtireln  litharge  bas  b««n  well  ste«peJ, 
and  bull  some  hontty  to  draw  out  the  wax.  Strain  it  through  a  cloth, 
and  put  u  quart  of  it  into  a  tierce  (42  gallons)  of  wine,  and  iAU  wiU 
mend  t/." 

To  cure  Wine  of  iU  MuddinesM. 

A  lump  of  sugar  of  lead  of  the  size  of' a  walnut  and  a  tablespoon- 
ful  of  sol  enixuui  arc  directed  tu  be  added  to  a  tierce  of  wine. 

Accum  has  the  following  rcmarkB  in  rcferencv  to  the  lue  of  lead  tn 
wine: — 

'*  Tbti  most  dangerous  adulteration  of  wine  is  br  aome  prepAratkntf 
of  lead  that  possess  the  property  of  aropping  the  progress  of  acei- 
cence  in  wine,  and  also  of  rendering  white  wines,  when  muddy,  trana- 
parent.  I  have  good  reason  to  sute  that  lead  is  certainly  employed 
for  this  purpose.' 

*'  Lead,  in  whatever  state  it  is  taken  into  the  stomach,  occasions  ter- 
rible d■^ea»l'v,  and  wine  adulterated  with  the  minutest  quantity  ofU 
becomes  a  slow  poison.  The  merchant  or  dealer  who  jiractises  tiiia 
dangerous  sophidticntion  adds  the  crime  of  murder  to  that  of  fraud, 
and  deliberately  scatters  the  Deeds  of  disease  and  death  amongst  those 
consumers  who  ctmtributeto  bis  emolument.  If  to  deface  the  current 
coin  of  tbc  realm  be  denounced  as  a  capital  ofience,  what  punishment 
should  be  awarde<l  against  a  practice  which  converts  into  ptiison  a 
li<(uor  u»e<l  for  sacred  purposes ! "  These  remarks  h;ivc  a  wider  applica* 
tion  than  to  the  subject  of  the  ndultcration  of  wine  with  leul. 

It  must  be  remembered  that  lead  may  be  present  in  other  wine*  as 
well  as  in  port. 

It  appears  that  no  real  necessity  ever  exists  for  having  recourse  to 
lead  to  remedy  the  more  usual  defects  of  wine. 

It  may  here  be  stated  that  the  muddiness,  and  especially  the  ropi- 
ness  and  vii^cidity  of  wine  is  due  to  the  pre»ience  of  an  aaotiMd 
matter  precipitable  by  means  of  tnnnin.  It  iif  in  white  wines  deficient 
in  tannm  that  this  malady  chiefly  «KXurs.  M.  Francois  recommends 
for  its  cure  the  use  of  the  bruised  berries  ol"  the  mountain  ash  in  a 
somewhat  unripe  state,  and  of  which  one  [K)UDd  well  stirred  in  is  suffi- 
cient for  a  barrel. 

But  we  have  not  yet  exhausted  the  list  of  adulterations  practised 
upon  that  much  abused  wine,  port. 

Accuni  state-s  ''uinny  thouE<and  pipes  of  spoiled  cider  are  annually 
broiiiiht  hither  from  the  country  for  the  purpose  of  being  conrcrtea 
into  factitious  port  wine." 

The  business  of  imitating  wines  is  in  many  continental  towns  a 
distinct  and  ucknowlcdgctl  occupation.  'Hie  author  of  the  *  Tricks  orf 
Trade  "  has  the  following  remarks  on  this  .*ubject :  — 

"At  Cette,  in  France,  those  following  this  trade  do  not  hesitate  to 


WINE,  AND  ITS  ADULTEKATIONS. 


551 


^ 


fasten  boards  with  *  Wines  matmfiiclured  here'  over  their  doors.  Lorpe 
shipments  of  spurious  port  iirrive  from  this  town,  most  of  which  <lo  not 
contain  one  drop  of  the  real  wine." 

Another  method  prnctisod  of  adulterating  port  wine  is  to  mix 
together  h  variety  of  cheap  red  wines,  adding  a  little  genuine  port. 
This  STstem  is  expused  in  a  work  enlitied  "Wine  aud  Spirit  Adultera- 
tions Unmasked."  The  author  states  that  large  vats  are  kept  bj  the 
manufacturer  in  which  diOerent  inferior  wines  are  mixed  to'^ether  in 
iinitalioit  of  [wrl.  These  are  fur  the  most  part  Beni  Carlos,  Figura*, 
and  KedCapc.  Heni  Carlos  may  he  purchased,  duly  included,  at  38/. 
fjcr  pipe,  Fipuras  at  45/.,  and  Rud  Cape  at  32/.  One  or  mure  of  these 
are  mixed  together,  a  proportion  of  common  norl  added,  and  a  small 
quantity  of  mountuin,  to  imparl  a  suftness  and  give  a  rich  appearance. 
salt  of  tartar  will  ensure  a  quick  and  firm  crust,  and  gum  dragon 
ffive  a  fulness  of  davour.  a  consistency  of  body,  und  auood  fuce.  Berry 
dye,  a  colouring  matter  imnorteil  from  Germany  for  tue  express  pur- 
pose  of  ailuheration,  will  increase  the  deep  piirpl-*  tint,  while  with 
washings  of  brandy  cjuks  the  whole  compoimd  is  mode  perfect. 
Wine  thus  ntode  up  would  cost  only  about  16«.  9d,  per  dozen,  every 
expense  included. 

Various  receinta  have  been  published  for  the  manufacture  of 
spurioui  port  The  follnwing  are  from  the  '*  Publican's  Guide:" — "The 
cask  is  to  be  well  sulphured,  and  then  twelve  gallons  of  strong  port, 
three  cf^Uuns  of  Coy:Tiac  brandy,  six  of  prt>of  spirits  of  wine,  and  forty- 
two  ofgood  rough  cider,  making  in  all  a  compound  iit  llie  rate  of  18«. 
|>er  dozen."  A  second  re<:eipt  is  as  follows:  —  "Take  forty-five 
gallons  of  cider,  six  of  brandy,  two  of  a  decoction  of  sloes,  and  eight 
of  port  wine.  To  increase  the  colour,  tincture  of  red  sandors  woofi 
or  cudl»car  mu^t  be  added.  The  wine  is  to  be  bottled  in  a  few  da^s, 
and  a  teas[HJonfuI  uf  powdered  catechu  aildetl  to  each  buttle  to  give 
a  rough  and  astringent  flavour  and  to  ensure  a  fine  crust ;  lastly,  in 
order  to  give  an  appearance  of  age,  the  ends  of  the  corks  are  to  be 
stainei!  by  soaking  ihcm  in  a  strong  decoction  of  Brazil  wood  con- 
taining a  little  alum.** 

Dr.  Recce's  "  Gazette  of  Health**  contains  the  foUowingreccipt :  — 
**  Take  of  British  grape  wine  or  cider  four  gallons,  of  the  juice  of  red 
beet  two  quarts,  of  brandy  two  quarts,  of  logwood  four  ounces,  or 
rhalany  root  bruised  half  a  pouu<l.  First  infuse  tbe  logwood  and 
rhatany  mot  in  brandy  and  a  gallon  of  grape  v;ine  or  cider  for  a 
week.  Then  strain  the  liquor,  nnd  mix  it  well  with  the  ingredients  ; 
keen  it  in  a  cask  for  a  mimtb,  when  it  will  he  fit  to  botf^lo. 

Ihc  fuUowing  receipt  for  the  mftiiufiu-ture  nf  '*  Soidhtunptan  Port^* 
is  from  the  some  work: — **Takc  cider  thirty-six  gallons,  elder  wine 
eleven  gallons,  brandy  6ve  gallons,  danuun  wine  eleven  gallons, 
and  mix.** 

It  thus  appears  thut  great  and  scandalous  tricks  are  played  with 
the  English  geiitleuiairs  favourite  ader-dinuer  beverage. 


k 


M  M  4 


5^2 


WINE,   AND  ITS  ADULTERATlOKS. 


The  consamptton  of  nort  wine  bos  recently  much  (loclmed,4Mb(lflA 
in  consequence  of  the  knowledge  of  its  adulteration  \mt\i  voan  ex- 
tensively dilTused.  Tt  is  to  be  hoiwd  that  this  result  will  le*lto» 
reaction,  and  teaeh  the  adulleraton*  that  Uiey  are  perilling  the  «»• 
sumption  of  this  wiue  in  this  the  great  port  wine  drioking  oonatr;. 


SHERRY,  AND  ITS  ADULTERATIONS 

Thefrrapes  from  which  this  wine  b  made  are  white;  thejr  trcgi*^ 
in  the  province  of  Andalusia  near  Cadiz,  in  Spain:  Uio*ewUnfiB^ 
nish  the  better  qualities  of  wine  are  cultivated  in  the  rineranliM* 
roundinn;  the  t^wn  of  Xeres  de  la  Fmnt<'>raf  and  b«^ee  the  vine  ii 
called  the  wine  of  Xerea.  The  vineyanlj  from  which  the  BnftA 
market  i^  supplied  extend  over  80,000  acres  of  land  :  the^  Aoafc 
ncLirly  half  u  million  pipes  ot  wine,  of  which  the  greater  qaaattl^li 
the  vnlue  of  4^0,000^..  is  exi>ort«d  abroad. 

The  ^reiitest  care  and  labour  are  bestowed  upon  the  colurttialf 
the  vinea  from  the  fruit  of  which  sherry  is  made. 

The  nrrapes  are  not  leathered  until  they  are  very  ripe»  and  na 
somewhat  ttbrirelled  with  the  heat  of  the  sun;  sometimea  the  friB 
after  beinj;  plucked  is  exposed  to  the  sun  for  a  day  or  two,  and  forlkl 
very  best  wine  the  finest  grapes  only  are  used. 

The  fcrmciitution  iii  continued  until  ue&ily  all  the  sugar  hM 
converted,  and  the  wine  is  often  not  drawn  oS*  for  four  ur  five 
after  the  commencement  of  feriaentation.  It  is  at  fir«t  of  a  pale 
colour,  but  darkens  with  age.  Sitmelimea,  however,  a  j>eculiar 
inj,'  liquid,  termed  "arrope,"  is  added.  This  is  prepared  by  hoiXtt^ 
sherry  down  to  a  syrup.  It  is  by  the  addition  of  this  substance  ihst 
the  diirk  sherries  are  prepared. 

Tiic  sherry  termed  Amontilladu^  and  which  at  the  praseal  tifltb 
so  much  in  tiivour  with  us,  iy  a  very  dry  wine.  A  singular  Ue^  ^fA 
rcfrard  to  this  wine  is,  that  its  peculiarities  are  not  due  xa  any  anh 
tained  causes  capable  of  imitation,  but  are  entirely  aL>ci(ieiitsl  so  far 
as  the  manufacture  is  concerned.  In  atleinptin^  tu  prcporv  it  ^ 
fruit  is  plucked  at  a  murh  earlier  period,  and  tnxlden  duwn  b«  thi 
peasania;  but  of  a  hundred  butts  of  wine  made  fiom  the 
and  by  the  same  process,  some  only  will  be  Amoikfcilhido 
onlinary  sherry. 

Sherry  bears  too  hi^rh  a  price  and  is  too  extenflvdy  tauaaatA  % 
escape  the  bunds  of  adulteratorb.  it  is  never  adulterated  bf  ^ 
growtjrs,  but  either  by  the  importer  or  by  the  merchant  at  b«nK- 

IVeviuus  Xa%  its  exportu(i<m,  a  proportion  uf  brmidf 
ahviivs  adiled  to  cherry.  This  is  a  very  unneceisary  mod 
practice,  ainoe  it  cannot  fail  to  injure  the  delicacy  otf  tht  flsvsars' 


WXNB,  AND  ITS  ADULTERATIONS 


ortivEaSHY 


561: 


the  wine,  and  to  retmrd  those  natural  chnriges  in  it  consequent  upon 
keepiniit  and  which  are  »o  improving  to  its  quality. 

'Ilie  chief  adulterations  of  itherry  coniiist  either  in  mixing  with 
ffenuine  sherry  of  the  first  quatity  inferior  sherriea,  in  adding  to 
Baerry  other  wine*  of  inferior  quality  not  sherry  at  all,  or  sotnetimet 
factitious  compouxdi^  not  contoiniog  any  grape  juicer  arc  substituted 
for  sherry. 

Low  iHTtced  sherries  are  imported  from  Spain  at  about  18/.  per 
butt,  expressly  fur  adulteration.  On  their  arrival  they  are  mixed 
with  cape  and  cheap  brandy,  and  the  mixture  is  flavoured  in  imitation 
of  gfKxl  sherry,  the  colour  being:  either  increased  or  diminished  accoxd- 
inff  aa  brown  or  pale  sherry  is  required. 

llie  author  of  the  "Tricks  of  Trade'*  states  that  at  Ceite,  in 
France,  ^rreat  quanlitiea  of  sherries  are  made  up  and  shipped  for  tba 
En^ilish  market^  the  composition  of  which  la  nothing  more  than  a 
cheap  white  irnur,  strengthened  with  brandy^  coloured  with  treacle^ 
and  tlnvoured  with  almontU. 

Lastly,  the  same  writer  srates,  a  kind  of  sherry  is  manufactureil  in 
thiti  country,  the  ba-sis  of  which  is  pale  mtiU  unci  trtigar  candy,  a  small 
ouanrity  of  French  bramly  and  inferior  wine  being  added  lo  flavour 
toe  mixture. 

The  practice  of  restoring  muddy  or  ropy  wines  by  means  of  lead 
is  also  resorted  to  in  the  cattc  of  sherry  and  most  of  the  otlicr  wines 

Genuine  sherry  is  a  very  wholesome  wine,  in  consequence  of  its 
freedom  from  acidity,  augar,  and  other  extractive  matters. 


I 


I 


MADEIRA,  AND  ITS  ADULTERATIONS. 

The  different  qualities  of  Madeira  arc  distinguished  as  south 
north  wines,  according  to  the  side  of  the  island  on  which  the  trees 
were  gjown  frora  which  the  wine  is  made,  the  former  being  three 
time^  more  valuable  than  the  latter. 

In  the  manufacture  of  the  better  qualities  of  Ma<lc-irn,  the  juice  is 
expressed  by  Irnmnling  on  the  grapes;  this  is  drawn  off,  and  a  further 
(|uuntit^  of  juice  obtained  by  the  aclion  of  the  press  on  the  murk,  and 
Iroin  this  an  inferior  quality  of  wine  h  prepared.  The  fcrmenuiion 
is  usually  continued  for  about  six  weeka,  the  juice  being  conatantlj^ 
agitated.  | 

For  the  ripening  or  mellowing  of  the  wine,  beat  and  motion  are  had 
recourse  to. 

One  plan  is  to  keep  the  wines  in  stores  lieoted  to  about  SO*"  F. 

Another  is  to  place  the  bottles,  well  corked,  in  heaps  of  fermenting 
mtinurc. 

Lastly,  in  some  cas«a  Hadeirm  is  sent  mie  or  more  voyages  to  the 


554 


WINE,   AND   ITS   ADULTERATIONS. 


Kant  Indic.%  the  heat  of  the  climate  and  the  constant  agitAtiaoin  vbirb 
tlio  wine  iH  kept  very  greatly  improving  its  qiiulities. 

TIte  adulterations  tti  which  Mitdeirn  is  subject  are  in  ike  nuin 
similar  to  those  of  Bbcrry  and  other  white  wuies.     Maiieirt  of  inliiv 

Jiiiulitj  is  mixed  with  and  passed  ofl*  for  the  bcft,  and  viaiB  vt 
abricaled  in  tmitatiun  ot  Madeira,  but  really  not  oontaiiiinf  adrof  ^ 
thut  wine  in  them.  A  spurious  Madeira  ia  aometimes  made  li<ciia  i 
Canary  wJne  called  VedtmiOj  which  somewhat  reacmbles  Aladeira,  aai 
like  it,  U  improved  by  heat  and  agitation.  Thin  ia  mixed  wilhafluU 
qiinntity  of  mountatn  part  and  cape^  '*  sweetened  with  nvor  aflMJft 
flavoured  with  biu^r  aJnt/tndji^"  and  then  subjected  to  a  boC  nkr 
proceaa  to  give  it  mellowness  and  aj?e. 

Of  course,  a  higher  price  is  ithar^cd  for  Madeira  which  hai  bcM 
to  the  East  Indies.  Much  tliat  is  sold  ns  baring  underpow  tk 
vfiyiiffc  ha#  never  been  to  the  East  at  all.  It  is  stated  that,  in  arte 
to  nid  thiti  deccptioii,  casks  arc  branded  and  fjalse  bills  of  Cr«ijbt<i- 
hibitc<L 

M.iny  ima^ne  that  wines  pTircha.4cd  at  the  docks  mtut  bf  pat: 
there  is  gooil  rejiaon  for  believing  that  thiit  is  not  always  so.  On  iftii 
Rubjetit,  we  find  in  the  **  Tricks  of  Trade,"  the  article  in  whicfa  wrk 
on  wine  ia  full  of  interesting  information,  the  following  renurks:— 
*'The  crafty  importer,  in  general,  orders  his  ships,  un  their  wyrtD 
En<;lnnd,  to  touch  at  Guernsey  or  Jersey,  when  the  required  adobe- 
radons  arc  praottscil." 

Some  idea  of  the  extent  to  wliich  Madeira  is  adulterated  ms;  hf 
formed,  when  it  is  known  that  not  more  than  '25,000  pipes  araaiibi 
of  these  not  more  than  .'),000  belong  to  the  &rit  growth,  of  wkicki 
about  one  half  reaches  this  country. 


CLARET.  AND  ITS  ADULTERATIONS. 

St.  Estiphe,  St.  Julicn,  Pouillac,  and  La  Rose  are  all  light, < 
able,  mid  aromatic  winc5,  exhilarating  gently,  without  amr  difia 
aion. 

The  celebrated  Cbnleau  Margaux  is  a  fine  wine,  haTin^  Uie  perftpBi 
of  the  violet.,  and  a  rich  ruby  colour. 

Haiit  Itrun  h  valued  for  its  peculiar  flavour  and  ils  yowtsfd 
boiitjuet,  which  resembles  a  mixture  of  violets  and  rasplierries^ 

The  much  esteemed  wines,  Latour  and  Lafitte,  the  foraer  hit$ 
the  stronger  wine,  possess  a  fine  violet  perfume  and  taste,  tbair  «altf 
alio  being  dark  violet. 


more 


The  greater  part  of  the  claret  sold  in  this  country  coosiaU  of  uuiWtf 
>re  than  the  cheap  red  wines  of  France  used  by  the  pT""*"  *' 


soi'l  ut  most  of  the  ordinary  wine  shops. 

"  Occasionally  a  cheap  common  French  wine  is  miaed  with 


WIXE,  AKD  ITS  ADULTERATIONS. 


555 


eider,  and  coloured  to  the  appcnrance  of  claret  with  eachitiealt  logwood, 
aiid  other  in«turial»."  * 

Burfptudy  may  be  classed  amongst  the  clnret  wines  :  it  is  f>erhaps 
the  finest  of  all  the  red  wines;  it  is  stronger  than  ordinary  Harets,  the 
8tren<;th  being  sometimes  increaaed  by  the  addition  of"  brandy.  It  pos- 
leiues  a  powerful  aroma,  and  a  delicious  and  lasting  flavour ;  it  is 
slightly  astringent,  and  hence  8ometim>'B  occasions  headache  and  in- 
digestion. It  must  t>e  rememlwred,  however,  that  as  it  arrives  in  this 
country  it  is  usually  brandied,  and  this  may  iu  some  instances  account 
for  the  eflectt  produced. 

The  addition  af  brandt/  to  Burgtindy  is  most  injurious  to  Its  flavour 
and  smell.  So  delic-tiU^  is  this  wine  thnt  it  is  eaid  thut  if  two  Biir- 
gun<ties  of  superior  qualitieij  are  mixed  tugetlicrf  the  bouquet  and  taste 
are  entirely  changed. 


CHAMPAGNE.  AND  ITS  ADULTERATIONS. 

The  grape  from  wliich  Charapaj^ne  is  made  is  black.  The  process  ol 
uiiuiufucture  is  mnut  carefully  conducted.  The  grapes  are  first  ex- 
uuiine<l,  every  bruised  or  unripe  grape  being  removed.  For  the  cxey 
or  white  Champagne,  the  grapes  arc  trodden  for  a  quarter  of  an  hour 
before  being  pressed.  For  the  pink  wine,  the  treading  is  prolonged 
until  the  juice  becomes  tinged  with  the  colouring  matter  of  the  husks. 
For  infLTit>r  Chainpugne,  the  colour  is  sometimes  artificiidly  produced 
by  means  of  a  little  red  wine^  or  even  by  the  juice  of  elder  berrUti. 

The  white  Champagnes  are  therefore  in  general  to  be  regarded  as 
purer  than  the  pink  varieties. 

Chamjiagnes  are  not  only  classified  according  to  their  colours,  but 
al.to  into  still  and  upurkling.  The  best  of  the  still  wines  is  Sillery,  a 
dry  Ciiumpiigue,  of  an  amber  colour,  rich  body,  and  powerful  bmu|uet. 

Of  the  Champagne  sold  in  England  a  very  large  proportion  is 
spurious. 

Sometimes  it  is  fabricated  from  cheap  white  French  wine,  tuguTf 
and  colouring  matter  being  added. 

At  others  it  consists  in  port,  or  even  wholly,  of  wine  made  from  the 
goftitetieny. 

Not  uufre(]uently  it  is  manufactured  aAer  the  followins,  or  some 
similar  reeeii>t  : — ''Take  of  white  sugar  eight  pounds,  the  whitest 
brown  sugar  seven  pounds,  crystalline  lemon  acid  or  tartaric  acid  a 
quarter  of  on  ounce,  pure  water  eight  gallons,  while  grape  wine  two 
quarts,  or  perry  four  tiuarts,  of  French  l)ran<iy  three  pints.  Boil  the 
sugar  in  the  wnicr,  skimming  it  occasionally,  for  two  hours;  then 
pour  it  into  a  tub,  and  dissolve  in  it  the  acid  before  it  is  cold.  A<ld 
yeast,  and  ferment.  Fut  it  into  a  eleun  cuifk,  und  add  the  other  iu- 
grcdienlM.     The  cask  is  to  be  well  bunged,  and  kept  in  a  cool  place 

•  TMcki  of  TradcL 


AM 


WIXE,  AND  TTB  ADTTLTERATIOKS. 


for  two  or  three  months  ;  then  bottle,  &nd  keep  i(  cool  for  •  month 
lonj^cr,  vhen  it  will  be  fit  for  use.  By  adding  one  pound  of  iresfa  or 
prc'scrred  strawberriea,  and  two  ounoca  of  powdered  cocUineol,  the 
ptiik  Cbampogne  may  be  mode.'* 

The  Champagne  sold  at  races,  fairs,  and  tea  gardeni  b  rarelj  erer 
genuine. 


GERMAN  WINES.  AND  THEIR  ADULTERATIONS. 

The  vine  ccncrally  cultivated  on  the  banks  of  the  Rbixur,  and  its  tri- 
buraric»  the  Alooelle  nnd  ibe  Mayne,  is  called  the  Resslin;;r,  The  grapes 
wbicb  it  beara  are  small  and  po98eR8  a  hartih  taele,  but  the  wines 
mufl**  from  ibera  are  rt'iuorkabtu  for  ibeir  aroma  and  pleasant  flavour. 

Tbe  chief  German  wines  are  JnhnHmHherg&r^  Steinberger^  Hmdt^ 
keimer  a  red  wine,  Horkheimtr  or  Hock,  and  Mttselle. 

.Johannisberp:er  is  grown  in  tlie  <*ourtyard  of  the  castle  of  .Tuhan- 
nisbere,  on  the  batiks  of  the  Rhine,  and  (he  quantity  of  thU  wine 
made  is  so  smiiU  chut  it  is  for  tbc  most  part  disposed  of  prirateljr,  ukd 
can  rarely  be  obtained  for  cither  love  or  money.  Wine  may  be  por- 
cba^^t-'d  in  Uennany  freely  enough,  but  nt  n  high  price,  under  the  name 
of  Jobnnnidberger,  but  this  in  rarely  if  ever  what  it  ii  represented. 

Steinberger  is  said  idmnst  To  rivid  Jobannisberger.  The  Tioeyard 
from  tbe  grapes  of  wbirb  tWis  wine  is  nindc  contains  only  108  aurea, 
BO  that  tbe  supply  of  this  wine  is  alwj  ejctremely  limited. 

The  vines  from  which  Hockheimer  or  Hock  is  produced  grow  round 
tlic  town  of  llockbeim,  near  to  Mayence  and  Frankfort,  on  the  bvika 
of  tbe  Mayne. 

Rudtshtimer  is  another  much  trstcemed  wine,  a  small  qunntity  (^it 
only  \i*i\n*i  made,  and  wUiuli  \»  soon  ull  bought  up  t>n  the  S|>ot. 

The  most  celebrated  Mvselle  wines  are  those  named  Scharsherger 
and  Orunhauxer,  also  culled  the  "Nectar  of  the  Moselle." 

Not  very  umcb  in  known  respecting  tlie  adulteration  of  the  G«rmiui 
wines;  they  ure  ]>robubly  confined  principally  to  hock  and  Moselle. 

"Cheap  light  French  wines  ore  perfumed  with  essences,  ]Jaccd  in 
bottles  ot  tbe  colour  and  shape  peculiar  to  the  Rhenish  wines,  and 
often  passed  off  at  enormous  prices  us  the  choicest  specimens  of  the 
GcrniuD  vincyiirds.  In  England  tbe  demand  for  them  is  small,  »o 
that  as  yet  it  has  not  been  worthy  tbe  attention  of  the  trade  to  8L<iul- 
terate  largely  ;  lor  as  the  consumers  are  few  and  far  between,  and  these 
sopbistit;»tion»  spoil  with  keeping,  tbe  loss  would  be  larger  than  the 
profits  gained  by  the  deceit."  • 

On  ike  Detection  of  the  AduUeraiioju  of  Wine. 
It  is  unforiunato  that  many  of  the  adulterations  practised  upon 
wine  do  nut,  in  ibe  present  state  of  organic  cliemlstry,  admit  oi  being 
discovered.     This  remark  appbes  especially  to   thoi^e  adulterations 

»  Trkki  of  Trade. 


WINE,  AND  ITS  ADULTERATIONS. 


557 


which  coDflist  in  the  mixture  of  different  kintls  of  wine,  and  to  the 
various  vegi'tablt*  subatancea  eniplo}-ed.  Neverthtiless  many  of  the 
atlalteratiuus  of  wine,  including  »ocae  of  those  which  are  iiiiurious 
to  health,  do  admit  of  detection,  and  we  shall  now  describe  the 
methods  by  which  these  may  be  discovered. 

The  strength  o/witif  depends  upon  the  amount  of  alcohol  contained 
in  it ;  this  may  be  in  exccs:)  from  the  wine  contuining  brandy^  or  it  may 
be  deficient  from  its  dilution  with  water.  It  is  therefore  frequctitly 
necessary  to  ascertain  the  quantity  of  alcohol  present,  llie  melhu<ls 
by  which  tliifl  determination  is  efl'ected  in  the  case  of  wine,  are  nearly 
the  aame  as  in  spirits  and  other  alcoholic  liquids.  They  will  be  found 
described  in  the  article  on  Gin, 

When  the  wine  contains  little  or  no  extractive  matter,  ita  weijtht 
may  he  taken  at  once  with  the  specifii:  gravity  bottle,  and  the  alcohol 
calculated  direct  from  it.  When,  however,  much  sugar  or  other  ex- 
tractive is  present,  then  the  spirit  must  be  separated  by  distillaliun, 
or  the  following  more  ready  method  may  be  adopted  :  — 

To  eiglit  partH  by  measure  of  tie  wiue,  odd  one  part  of  a  concen- 
trated solution  of  subacetate  of  lead;  a  precipitate  will  ensue coiuistiiig 
of  the  extractive  matters,  the  gum,  C4ilimring,  Albuminuusi,  and  acid 
matters  of  the  wine  in  combination  with  pan  of  the  lead ;  sepanite 
the  precipitate  by  filtration,  add  to  the  filtered  liquid,  in  small  qiiun- 
titicfl  at  a  time,  nure  and  recently  ignited  subcorbonatc  of  potash 
until  the  last  portion  added  ceasca  tu  be  dissolved.  The  potash  ab- 
atracta  the  water  from  the  spirit,  which  floats  on  the  lurfuee,  forming 
a  distinct  stratum.  If  the  liquid,  previous  lo  the  addition  of  the 
potash,  be  poured  into  a  glass  lube  graduated  in  per-cenlages,  and  the 
potash  be  subsequently  added,  the  quantity  or  per-centage  of  spirit 
may  be  ascertained  by  mere  inspection  of  the  scale. 

If  the  spirit  be  sepflrBte<l  by  dii^tillation,  the  smell  of  the  distillate, 
especially  when  worm,  will  fretjuently  betray  the  presence  of  volatile 
suustancea  —  as  cherry  laurel  watrr^  and  in  some  caees  com  spirit. 
Tbe  characteristic  odour  of  this  snirit  is  brought  out  especially  by 
rubbing  some  of  the  strong  spirit  briskly  between  the  puluis  of  the 
hands;,  and  then  smelling  it. 

On  the  Determituition  of  ike  Ertractive.  —  For  tliii  purpose  a 
measured  quantity  of  wine  should  be  evaporated  on  a  water  both, 
until  it  ccoMA  lo  lose  weight.  The  presence  of  a  variety  of  foreign 
substances  moy  frequently  be  detectetj  in  tliia  extractive  by  the  amell 
and  taaie,  especially  the  snicU  emitted  by  the  wine  while  hot,  and  ua 
the  evaporation  draws  to  a  close.  In  this  manner,  the  odour  ol  elder 
hirries^  of  cider^  gaosefKrries^  and  other  fra^ant  and  aromatic  sub- 
atancea may  frerpicntty  l>e  detected  ;  and  by  the  tuj^te  the  presence  of 
catechu  and  Cauenne  determined.  Tbe  taste  of  the  apnle  or  pear 
becomes,  oceoraing  to  Normandy,  more  evident  after  the  removal 
of  the  bitortrutc  of  potash. 

Om  the  Determituition  of  the  Su^ar.  —  The  amount  of  sugar  present 
in  wine  may  be  ascertained  in  either  of  the  fuUuwing  ways : — The 


55a  WINE,    AND    ITS    ADULTF.KATIONS. 

extractive  is  to  be  thrown  down  hy  means  of  subaoetate  of  lead,  tbe 
wine  filtered,  the  excess  of  load  removed  by  rulphiirHted  hydro- 
gen passefl  into  it  through  water,  as  in  a  Wootfo'a  appiLratas,  tbe  wine 
afcain  filtered,  and  then  evi^rated  to  dryness.  The  residue  cooaiaCs 
of  nearly  pure  suffar.  Or  we  may  employ  the  copper  test,  as  described 
under  the  head  of  Sugar.* 

On  the  Determination  of  the  Acidity.  — ^Tbe  process  is  detailed  under 
the  head  of  ISet^r. 

On  ike  Determination  of  the  Bitartrate  of  Potaah.  —  This  salt  is  also 
cAlle<l  cream  of  tartar  and  wine  stone.  5000  grains  b^  measure  of 
the  wine  arc  to  be  evn]>orated  to  dryness,  and  the  residue  limited ; 
by  the  igtiition  the  acid  bitartratc  is  converted  into  the  alkaline  car- 
bonate, the  umount  of  alkali  is  then  determined  by  means  of  %  M^vtioa 
of  ascerlainefl  i»trength  of  dilute  sulphuric  acid.  If  an  alkali^  aa  tbt 
curbonnles  of  soda,  potash,  or  lime,  baa  been  Added  for  the  purpose  oi 
correcting  the  undue  aridity  of  the  wine,  this  method  is  fallacious ; 
and  we  must  then  crystallise  the  tartrate  of  potash  from  a  conceotratcd 
watery  solution. 

The  solution  may  be  thus  prepannl :  —  The  wine  is  to  be  evapo- 
rated to  a  syrupy  consistence,  and  allowed  to  cool  without  stirring:  for 
twenty-four  hours  ;  at  the  end  of  thnt  time  the  clear  litjuid  sdiould  be 
decanted  from  any  crystals  of  cream  of  tartar  which  may  have  formed ; 
the  decanted  liquid  is  to  be  diluted  with  distilled  water,  and  evapo- 
rated as  before.  The  crystals,  if  any  have  fonued,  are  agtun  separated 
by  decantation,  and  the  operation  rc|>cated  until  no  more  crystals  are 
formed. 

Another  way  is  to  calculate  the  bitartrate  from  the  quandtv  of 
chloride  of  potassium  obtained,  ond  if  carbooatQ  of  soda  also  has  been 
added,  to  estimate  this  from  the  chloride  of  sodium  found.  Tbe  pro- 
cesses for  tbe  quantitative  detennination  of  the  chlorides  of  potassium 
and  sotlium  are  given  under  the  heads  of  Turmeric  and  Annatto. 

On  the  Detennination  of  ike  Presence  of  Foreign  Coiouring  Matters.—^ 
Some  of  these,  especially  tbe  colouring  matter  of  tlie  elder  herry^  may 
oflen  be  detcrmineil,  as  already  noticed,  by  the  odour  nf  the  warm  or 
hot  extract  of  the  wine.  Certain  chemical  methods  have,  however, 
been  described  for  effecting  the  discrimination  in  question. 

Method  of  M.  Vot/ei, —  This  chemist  has  recomuiendvd  acetate  of 
lead  for  the  detection  o(  extruiieous  colouring  matters  in  red  wine. 
With  this  reagent  he  statev  that  genuine  red  wine  gives  a  pvenbh 
grey  precipitate,  but  that  in  the  case  of  wine  coloured  with  the  juice 
of  bilberries,  elder  herricA,  or  Campvachy  trood^  tbe  jirecipilate  is  deep 
blue,  while  with  Bnizil  wood^  red  Jktndera^  and  beet,  it  is  red.  Wine 
coloureil  by  beet  root  is  also  rendered  colourless  by  lime  water,  bnt 
the  weakest  acid  brings  buck  the  colour. 

Mitchell  states  that  tbe  precipitate  with  acetate  of  lead  from  an  in- 

•  Wln«lwin|  aomeCinia  .iilullpratcNl   trUb  eamt  near.  It  \t  occaiiottallr  neccturr  la 
dlicHrotauUe  tietweeo  f M|w  And  c«ii«  (ugan .   tliv  tovtbiMt  »l)l  bf  louod    ilvMrlbtd 
ibe  onlcto  ZToMy. 


WINE,    AND  ITS   ADULTEBATION8. 


559 


Auion  of  logwood  is  purple  red,  and  that  if  the  colounnjr  mnttcr  be 
very  much  diluted  it  nas  a  leaden  or  bluish  hue.  With  the  juice  i)f 
beet  the  colour  is  puce ;  when  diluted  with  water  the  tint  becomes  a 
paje  galmuii  red. 

According  to  Berzelius  the  colouring  matters  of  reel  wine  giTC 
difierent  coloured  precipitates  with  diiicelute  of  lead,  according  to  the 
•gc  of  the  wine,  and  thnt  in  new  red  wine  the  precipitat**  is  generally 
blue.  If  this  is  correct,  the  value  of  the  teat  of  M.  Voyei  i«  of  couriw 
much  diminished. 

This  statement  seems  opposed,  however,  to  the  following  experi- 
ment of  M.  Voyel.  It  has  already  been  stated  that  the  colour  of  the 
red  wines  is  derived  from  the  colouring  matter  located  in  the  skin  of 
the  grupe».  In  order  further  to  assure  himself,  he  prepared  a  quan- 
tity of  grape  skins,  reduced  ihcm  to  powder,  and  treated  thoiu  with 
alcohol.  Ihis  took  up  part  of  the  colouring  matter,  and  when  acetate 
of  leail  was  added,  the  same  greyish  pr^'en  precipitate  was  obtained. 
Lastly,  ic  should  be  stated  that  the  wines  principally  cxf>crimentcd 
upon  by  M.  Voyel  were  new  wines,  and  were  made  by  himself  from 
black  grapes  for  the  purpose  of  his  experiments. 

Method  of  Al.  Cheptniier. —  Solution  of  caustic  potash,  ailded  to 
genuine  red  wine  in  such  quantity  as  (o  neutralise  all  the  acid,  causea 
the  colour  to  chunge  from  red  to  bottle  green,  and  after  some  time  to 
brownish  green,  but  no  precipitate  is  formed.  The  colours  produced 
when  tbreign  colouring  matters  have  been  employed  ore  dinerent,  u 
shown  in  the  following  table:— - 


Wine  coloured  with  — 
Elderlwrries     - 
Logwood 
Red  mulberries 
Brazil  wood 
Beet  root  juice 
Litmus    - 


Colour  produced  by  potash  — 
rurple. 

Keddish  purple. 
Purplish. 
Ued. 
Red. 
Light  violet 

Method  of  M.  Jacob.  —  The  colouring  matters  experimented  upon 
were  those  of  the  petals  of  the  poppy,  of  logwood,  and  of  Brazil  wood. 
Tlie  reagents  which  he  employed  were  sulphate  of  alumina  and  car- 
bonate of  ammonuL 

Normal  wine  furnished  a  slightly  coloured  grej/uh  precipitate.  The 
Sime  wines,  with  Brazil  wood^  give  a  carmine  red  precipitate  which 
Tsried  in  intensity  with  lite  quantity  of  colouring  mutter  added;  with 
logwood  the  precipitate  was  of  a  fine  deep  violet  colour,  and  with  red 
poppy  of  a  nliUt'grey  colour. 

The  reagents  were  thus  employed  :  —  A  solution  of  sulphate  of  alu- 
mina was  made,  containing  10  parts  of  the  salt  to  100  of  water;  about 
half  a  drachm  of  this  solution  was  added  to  an  equal  quantity  of  wine, 
and  then  a  few  drone  of  a  solution  —  usually  about  12  or  15,  H  parts 
to  100  of  water— of  carbonate  of  ammonia  were  poured  in.  A  prer.ipi- 
tate  of  alumina  is^  Immediately  producetl,  variously  coloured,  accord- 


560 


WINE,    AMJ   ITS    ADULTEBATIONS. 


in^  to  the  nature  of  tbe  colourint;  nutter  employed.    An  excess  of  the 

precipitant  must  not  be  added,  fur  in  that  case  the  ttnta  produced  ar« 
Dot  sufficientiv  marked  to  allow  of  ihe  discrimination  of  the  aubaCjutoe 
employed.  'Ihe  action  is  most  marked  ailer  tbe  lapse  of  seven  or 
ejgut  minutes. 

Mfihod  of  Nets  Van  Esenb^ck. — Tbe  process  of  Nees  Van  Eaeobeck 
is  but  a  modification  of  the  preceding  method,  that  chemut  using 
alum  and  carbonate  of  potash. 

Tbe.se  reagents,  with  normal  in'nr,  giTC  a  dullish  ^rey  preopttate 
having  a  more  or  less  decided  red  tinj^.     An  excess  of  alkali  redi*> 
solves  part  of  the  preci pittite,  tbe  remainder  being  ash  gre/.     Il' 
wine  be  new,  tbe  residuary  precijjttjice  iK>Mie8a«s  a  gre«nish  tin^. 

Wine  coloured  with  the  culouriiig  matter  of  the  petals  ofredpop^ 
gives  a  brownish  grejr  precipitate  which  becomes  Dlack  bj  excess 
alkali. 

Coloured  with  privet  berriet^  it  zives  a  brownish  violet  preclpit&te. 

Coloured  b_v  elder  berries,  a  violet  precipitate;  by  Brazil  wood,  a 
greyish  violet;  and  by  logvfood,  a  rose  coloured  precipitate. 

It  thLTeforH  follows,  from  the  experiments  of  Nees  Van  Esenbcck, 
that  all  those  wines,  which  cive  with  the  rea:ients  above  named  bluish 
violet  or  rose  coloured  precipitates,  are  artificially  coloured  or  adults 
rated  with  foreign  colouring  matters. 

The  reagents  must  be  employed  by  meant}  of  solutions  of  defiuiUs 
strength — namely,  one  part  of  alum  to  eleven  of  water,  snd  fur  the 
other  solution  nnc  part  of  carbonate  of  {xitash  to  eight  parts  of  water  ; 
the  wine  and  the  alum  solutions  are  to  be  mixed  together  in  equal 
proportion?,  and  the  solution  of  potash  gradually  poured  in,  until  the 
whole  of  the  alumina  is  precipitated. 

On  the  Detection  of  Lead  in  Wine. — If  the  wine  be  of  light  colour,  a 
portion  of  it,  about  ten  ounces,  may  be  evaporated  down  to  one  ounce, 
and  this  may  be  divided  into  two  parts,  one  being  tested  with  sul- 
phuretted hydrogen,  which  will  ;;ive  a  black  precipitate  if  lead  is  pre- 
sent, and  the  other  with  a  solution  of  iodide  of  potassium,  which  will 
give  rise  to  tbe  formation  of  a  yellow  iodide  or  lead.  Or  the  saino 
quantity  of  wine,  either  re^i  or  white,  may  be  evaporated  to  drynesst 
luid  the  residue  incinerated  :  the  destruction  of  the  carbon  and  th« 
oxidation  oi'  the  metnl  U  rendered  more  complete  by  ignition  of  tbe 
residue  with  about  twice  its  weicht  of  nitre.  After  fusion,  the  residuum 
must  be  digested  with  a  little  dilute  nitric  acid,  the  solution  evaporated 
nearly  to  dryness^  the  residue  treated  with  distilled  water,  and  tbe 
solution  filtered  and  tested  with  tbe  reagents  above  named.  For 
fuller  particulars  refer  to  the  articles  on  Annatto,  Sugar  ConfcctioQery, 
and  Snuff. 

On  the  Detection  of  Copper  in  Wine.  —  Copper  is  sometimes  preaent 
in  wine  from  natural  causes,  being  in  such  cases  derived  from  tbe 
grapes  from  which  the  wine  is  made;  sometimes  it  is  purpoicly  intro- 
duced.     M.  Perctte  undertook  some  very  interesting  inTestigaticms* 


n 


WISE,   AKl>   ITS   ADULTERATIONS. 


661 


P 


which  will  be  found  rcponied  in  the  wnrk  "  On  the  FuUitlcntinn  of 
Aliini.Mitiir)'  Suba!tttK*es'*  bv  MM.  fJtimier  luiil  Harel«  in  <ir(ler  to 
tltilerniine  wbuUier  vvnw  iiiuthiKl  ini^lit  nut  b.'  iJuvisutl  by  whicli  the 
cases  (if  ihc*  prcscncv  of  ibo  iiicial  fr«»iu  mitural  cause!)  uiight  Iw  dis- 
crimiiiateil  iVimi  thofte  in  which  it  had  been  purposely  introiluofd  intn 
the  wire  ;  and  in  attaining  this  end  M.  Ferette  appears  to  have  been 
Mit'i-e^sful. 

M.  IVrt'tCe  took  10  Ihs.  of  perfectly  pure  red  wine  ;  this  lie  divided 
into  twri  parts,  one  was  de(-olourie**d  by  sninial  cliarcoal,  c'va[>o- 
raletl  to  oite  Hftli,  treated  ajriiin  with  chArcoal,  and  rendere<l  still  more 
mu(X*ntr:ited  by  eva|xiniriun.  To  a  little  of  ihu  liquid  poured  into  a 
te»it  tube,  a  few  drop«  of  ii  K^dutiou  of  ferrocrantde  ofpotasitium  were 
n<ld»l,  brit  no  change  of  colour  ensued,  neither  did  anv  precipitate 
take  plact*.  In  another  |M>rti(m  of  the  decolourised  liiiuid  a  plnte  of 
p()li(iheil  iron  woa  plunged  for  some  time,  but  no  dfposUion  nf  copper 
occurred. 

The  other  5  lbs.  of  wine  were  evaporated  to  dryness,  the  residue 
incinerated,  treuteil  wiih  nitric  aoidt  and  after  eTa[H>ration  to  drynus:s 
the  re*>iduu  WHS  dissoU'ed  in  water  :n  plate  of  irrtii  plunixed  into  a 
portion  nf  the  solution  became  rapidly  coated  with  copper,  and  the 
«(dutlnn  of  ferrocyanide  of  poUsnium,  added  to  another  [Mirtinn  of  the 
solution,  (;nve  an  immediate  iron  red  colimnirion,  which  after  a  time 
became  violet,  denoting  ihc  presence  ot  iron. 

M.  I'erctie  next  added  one  (nain  of  oxide  of  copper  to  another  3 
lbs.  of  wine,  and  treated  it  by  decolourisation  and  cvajKiratiun,  mid 
then  tested  it  witli  one  drop  of  utolution  of  fen*ocyanide  of  potafi»ium 
when  the  wliole  assumed  h  ru!>e  red  tint,  and  after  a  lime  a  preuiptiate 
of  the  same  rolour  farmed  without  any  indication  of  the  presence  uf 
iron,  as  shown  by  t)ie  formation  of  a  portion  of  prussian  blue. 

The  iron  nalundly  present  in  the  wine,  M.  Perotte  subdetpicntly 
prove«1,  had  been  removed  by  the  ehareoul  with  the  colouring  matter. 

M.  lVrett^3  further  a-^certJiiited  that  if  the  residue  obtained  by  the 
evaporation  of  wiue  be  carbonised,  and  the  carlK>naoeous  mutter  tieated 
with  wuter  conlainiD;*  a  little  uuinioni:!,  the  liquid  will  remuin  eoliuir- 
Icfs  in  the  case  of  normal  wine,  hur  will  he(*4>me  btne  if  oxide  of 
cooper  has  been  added  to  the  wine  in  the  pro[kortion  of  one  grain  to 
5  lbs.  of  wine. 

Liebig  ha«  the  following  remarks  in  regard  to  the  value  of  wine: — 
•*  As  a  restorative  or  means  of  refroshtnent,  where  the  jKiwerji  of 
life  arc  exhiiu^Ud;  of  giving  animation  and  cner<;y,  where  man  has 
tn  struggle  with  duys  of  sorrow  ;  as  n  mean*  of  correction  ami  com- 
pensation where  misproiK»rtiun  exists  in  nutriiinn,  and  the  or;runi^ni 
IS  deranged  in  jls  o{ieration;  and  as  a  means  of  protociion  u;::iii>st  tran- 
sient organic  disturbances,  wine  if-  surpa.'ised  by  no  product  of  nature 
or  of  art. 

"  The  nobler  wines  of  the  Rhine,  and  many  of  those  of  Bordeaux, 

0  o 


563 


WINE,   AND  ITS   ADULTERATIONS. 


are  distinguished  above  nil  others  by  producing  a  minimum  of 
jurioua  ftfter-cflecl.  Tlie  quantity  of  wine  coniiumed  oii  the  Uhine  by 
persons  of  all  ages,  without  perceptible  injury  to  their  raenuU  and 
bodily  healtli,  is  hurdly  credible.  Gout  mid  calculous  diseases  are 
nowhere  more  rare  iLitn  in  the  district  of  the  Rhinegau  so  hijEhly 
favoured  by  nature.  Iti  no  purt  of  Gennsny  do  the  Bpotheearies* 
estahlishmenCs  bring  so  low  a  price  ns  in  the  rich  cities  on  the  Khin«; 
for  there  wine  is  toe  univei>al  medicine  for  the  hedlihy  as  well  as  the 
sick;  it  is  considered  as  millk  for  the  ngcd.'* 

We  gather,  from  the  evidence  before  the  Commitfee  on  Adulter- 
ation, the  following  particulars  in  r^ard  to  the  proceedings  of  the 
Excise  as  to  wine :  — 

Mr.  VillierM.  **  How  does  foreign  wine  conic  within  your  province 
to  examine  ?" — '^1  cannot  tell ;  we  have  huii  two  samples,  uue  in  the 
year  1820,  and  one  in  18S2." 

*'  Are  there  any  tjisiers  appointed  for  the  wine  brought  into  this 
country  ?"  —  "  We  have  none." 

Mr.  Miiffutt.  "The  wine  is  under  the  Customs,  is  it  not?" — 
*'  Yes,  and  the  denlora  have  to  pay  a  licence  to  us." 

Mr,  Villiert.  "Arc  British  wines  much  ailultcratcd?*' — **  British 
wines  arc  made  up  in  a  variety  of  ways ;  we  do  noc  interfere  with  them 
much." 

So  much  for  the  efficiency  of  the  Excise  in  r<^nrd  to  wine  It  ap- 
pears ifaut  two  samples  were  examined  in  twelve  years. 

The  Customs'  duty  on  wine  from  lii-iti!>h  cnloiiie:!>,  certified  to  be 
the  production  of  those  colonies,  is  2j.  9ii.  per  gull.,  with  2  pt^r  cent, 
thereon  ;  all  i>ther  wines  5«.  6</.  |)er  gall,,  ntiJ  5  \iet  cent,  tbercoo. 

The  quantiti«a  entered  for  home  consumption  were  *— 


lBlS94. 

blHS^ 

t>WtwM«a. 

•riBsa. 

BritlthColonlM:  red        ... 
FotrtftTi:  t«d           -             -             -             - 
Britlih  Colunif  1 :  white   . 
Fordini :                   do.       -            -            - 
Vvfotu  Qilxed  In  bond  .red       - 
wblu    . 

Total - 

o«n.. 

1MI.-.79 
S,n9«i,(lM 

175.739 
3,511,  i  13 

ITT.IUS 
7«.4Mi 

<!•■■. 

l»-i.ll«9 

».7Mi7W 

111,1  IS 

Vn.iBft 

tSMilA 

KiTi.fln 

111847 

rj4»«ii 

f,S70,SU 

6,4»0,644 

I 

I 

I 


PART  ir. 


DRUGS,  AND  THEIR  ADULTERATIONS, 


Tub  vubject  of  the  adulteration  of  drugs  has  tlrend/  boen  briefly 
toucheii  upon  in  tlie  introduction  to  the  wurk ;  the  aj-Mtetn  uf  drug 
grindinfc,  and  the  efTecls  of  odulturarion  in  tiii)>airii)|{  tbe  unurts  of  the 
|ihvstcian  to  cure  difieoflc  wtTi*  e-^pc*  iaJly  alluded  tu. 

The  prevalence  of  adukt-rution  nmy  be  proved  in  several  ways. 

Kirstf  by  the  actual  amdvi^is  of  vurinus  drugs:  (he  refiulls  of  gome 
hundreds  uf  such  analyses  vrc  flhuU  ahortly  prucotid  to  record. 

Second,  by  the  testimony  uf  conipotcnt  witnesses. 

Third,  by  the  system  of  druj!  ^'rinding. 

Fourtii,  by  the  existence  of  what  are  knovn  as  compound  powders. 

Fifth,  by  the  prices  at  which  various  drug^  are  M>ld. 

Referring  to  the  evidence  given  Urforu  the  Parliamentary  Com- 
niittee  appoinletl  to  inquire  int4)  Lite  aul>ji-ct  of  adulteration,  we  meet 
with  much  vuluable  testimony  in  regard  to  tbe  fdaificatiun  of  drugs, 
and  »ontc  of  which  we  shall  now  quote. 

Some  idea  of  the  extent  to  which  adulteration  prevails  may  be 
formed  from  the  evidence  elicited  froiu  l>r.  E.  D.  Thomfion  by  Mr. 
Villicm. 

**  All  tlie  drugs  are  submitted  to  some  examination,  ore  they,  al  St. 
l*boiiias's  Hospital  ?" — *'  Every  one." 

**  Have  you  often  rejected  dru^  P" — "  Very  frequently  indeed.  I 
may  say  that  one  third  of  the  substances  I  h;ivc  examined  I  have  re- 
jected, either  from  impurity  or  adultenition.*' 

Mr.  Herring,  a  wboleside  chemist  and  dru^igist,  of  the  highest  cha- 
racter, engaged  in  the  drug  trade  fur  forty  years,  thus  dejjoces  to  the 
prevalence  of  adulteration  in  drugs. 

Mr.  SchoUfieid.  **  Wdl  you  favour  the  Committee  with  your  view 
as  to  the  existence  of  adulterntion  In  the  article  of  drugs  !*'* — **It 
exists  to  %  very  great  extent-" 

Referring  to  Mr.  Redwood's  denials  of  adulteration  before  the  Com- 
mittee, Mr.  Viiliers  asked  Mr.  Herring  the  following  Question: — 


564      EVIDENCE    BEFORE    PARLIAMENTARY  COUCITTKE 


"  It  iit  the  opinion  of  a  };eiit1eimin  connected  with  that  Scxuety*  tb«t 
there  i»  very  htile  impuritj  In  drugs  and  what  there  10  U  not  at  all 
injurious?" — **  I  ciinnot  ay:rec  with  that." 

"  Have  you  any  experieure  of  the  sttpply  of  drugs  to  Pf»or  Law 
Bonnli*  ?*' — "  \Vc  never  di<i  it,  but  I  have  9ecn  a  great  deal  of  it ;  aod 
there  the  powdered  ortirle  will  be  100  per  cenl.  cbenper  thtui  the 
Btajiiti  article."  fl 

Mr.  Scaiilan,  a  chemist  of  repute,  enp^aged  for  many  yenrs  in  tiie  V 
manufacture  of  drug's  und  chcfuieaU,  gave  the  folluwtng  evidence  as 
U>  the  peneial  ndnlieralion  of  drufjs  :  — 

Afr.  SchnirJirUt  "  The  general  <?tTei't  of  your  evidence  is  that  there 
18  a  considiTjlile  nniount  of  adullcr^ticin  in  di  uga  ?" — •'  In  lirugi  and 
oheuiicab  u&ed  in  medicine" 

"And  therefore  considerable  riak  exists  that  the  prescriptions  of 
phvsicians  will  not  have  their  intended  effect  upon  ilieir  patients?" — 
"There  is  no  doubt  of  it.  I  heard  Mr.  Uedwf»»d"j  evidence,  and  I 
do  not  think  he  admitted  adulterations  to  the  extent  to  which  theT 
really  exist." 

It  appears  from  the  foHowinj;  remark  of  Dr.  Thomson  m&de  to  the 
Committee  on  Adulteration  that  any  {Ktwder,  no  m.itter  what  it^  real 
value  and  original  cost,  might  tit  one  time  have  been  Imught  for  36r. 
per  cwt;  this  single  fact  of  itself  proving  tlie  exten«ve  practice  of 
adutlerution. 

Mr.  ViUiers.  *'l  BUppnse  there  ie  !«»me  diflerenoe  of  price  between 
the  lM.'st  dru<;;s  und  those  which  are  inferior  and  adulterated,  is  there 
not?" — **  I  have  boen  tulJ  ihul  there  are  drugirisls,  at  least  one  dmg- 
gist,  who  woiilii  fltll  any  powtler  von  pleajted  at  36*.  the  cwl." 

The  following  infoi'nmtian  was  cHcitetl  by  Mr.  Villiers  from  Mr, 
Wnringlon  in  reijard  to  a-iulteraiion  on  the  part  of  drujr  g-rinders  : — 

"  Vuu  say  you  generally  jrrind  your  own  drui!!*.  From  inqttirief 
which  you  have  nuide  in  the  trade  i<t  it  your  opinion  that  a  jrreftt 
deal  of  adulteration  takcB  phiee  on  the  part  of  the  grinders  ?" — 
"We  were  forced  t'>  grind  our  drugs  by  the  fact  of  the  adultera- 
tion. Kven  wht-n  the  SmTJi'ty  of  Apolhi-carii-s  ?»ent  a  man  to  the  dru^y 
mill  to  RUfH'rinlend  the  grinding  of  Uieir  own  dru<;.H,  he  wa5  taken 
down  to  dinner  or  (o  luni'b,  or  to  ftomethingof  the  kind,  and  all  kinds 
of  tricks  were  played  with  their  drugs.** 

Mr.  Brtstick,  whose  mnunmenta  in  pharmaceutjeal  chemistry  arc 
unequalled  by  any  other  chemist  in  iXxM  country,  furnished  the  Coin- 
raittee  with  the  ibllowing  evidence  in  regard  to  the  adulteration  of  the 
articles  known  as  ctuHptynml  jumnUrs : — 

"  There  is  a  cUss  of  bodies  1  aiiould  wish  particularly  Ut  draw  the 
attention  of  the  Comotittee  to,  which  is  a  senei>  of  powders  vended  by 
wholesale  druggists,  which  they  are  pleased  to  term  compound  pnw> 
dera.  Those  powders,  if  they  were  proi>crly  deaignated,  would  be  called 

*  The  Fhwiftccutlul  Soci«lf . 


ON   THE   ADULTERATION   OF    DRUGS. 


565 


tduitei'ated  powders.  They  are  obliged  to  use  a  term  in  contradis- 
tinction to  that  of  coin|x)un(l  powders,  and  ibey  employ  the  word 
*■  venuj  If,  tor  exuinpli^  you  wished  tu  order  genuine  aniseed  powder, 
you  would  n!>k  fur  puhit  anisi  vent* :  but  if  you  wanted  t  lie  adulteruled 
powder  you  would  uj*k  t'oT  puicu  anUi  compositug.  The  most  frequent 
in^tnncea  of  these  lululterated  pnwd»frs  are  aniseed,  carraway  seeds, 
fentigreek  .<ieedfi,  litpiorice,  gentian,  lurnieric,  and  starejiocrc.  The 
recipe  which  I  propose  to  read  to  the  Committee  fur  coinpoundin;?  one 
of  these  powders  is  onW  a  tyiK:  of  many  others.  It  is  in  a  bonk  which 
I  have  in  my  hand,  wtiich  belonged  to  a  person  who  used  to  mnnufac- 
ture  these  p»twders  who  is  now  dead,  and  therefVtre  I  feel  no  delicacy 
in  reading  it.  The  following  are  the  nmtermls  for  making  compound 
(tention  powder;  true  gentian,  1  ll>.,  linscetl,  5  lt>s.,  flour,  2  lh*t.,  cape 
aloe^,  to  ^ive  the  bitteme^is,  a  sulficient  quantity  ;  that  is  the  recipe 
employed  to  make  f:entian  powder  Mtnpnsitua." 

Chairman.  "  If  I  undereitand  rightly,  there  are  Tibs,  or  8  Ihs.  of 
niatt'ritil,  having  only  I  lb.  of  the  genuine  article  in  itl*"^"  Yes." 

Mr.  SheridaH,  "\VIjo  are  rhe  parlies  who  apply  f<)r  pidvis  compo- 
attu*?"  —  "  Tlie  retail  dru^igi^t ;  it  is  a  convenliuniil  term  between  the 
retail  and  tlie  whole^<kle  dru^igisl,  invented  to  avoid  the  disngreeuble- 
nc5S  of  talking  iibotit  .adulterated  articles." 

**Any  medical  man  u<iing  gcntittn  made  upacconlingto  that  receipt, 
would  find  his  expectations  totally  fail  ?"  —  ** Entirely." 

Mr.  Sheridan,  "  The  wholesale  druggist  compounds  the  powder?*'— 
*^  In  most  cases  it  is  done  by  bioDi  or  by  the  drug  grinder  on  hi« 
behalf." 

Chairman,  "U'hat  would  be  the  relative  telling  price  ofllie  true 
genliiiri  and  the  compotitut  f  " — "  A  wholesale  dnigffist  would  speak  to 
that  better  than  I  c^n  ;  of  course  there  is  a  considerable  rednclion. 
I  will  mention  one  oiher  instance  of  the  composition  of  a  c(mi[>oand 
powder,  that  is  turmeric :  common  ochre,  1  lb.,  true  turmeric,  1  lb., 
flour,  2  lbs." 

'*  That  is  in  the  ppop<trlion  of  one  to  four  ?  "  —  **  Yes." 

"Yuu  ullude<l  just  now  to  the  use  which  has  been  made  of  the  term 
'conventional  adulterution  ;*  *  do  you  consider  the  prnctiee  you  have 
ftuw  nrlerred  to  a!>  conventiomd  between  the  drugL'ist  and  the  drug 
grinder,  or  between  the  wholesule  druggist  and  ihe  retailer?"  — 
*'  Yes,  bctwet.*n  llie  wholesale  druggist  ami  tlie  retailer ;  certainty  not 
as  regards  the  public." 

*' The  drug  grinder  and  (he  retailer  understand  each  other,  and 
therefore  it  may  be  siiid  to  be  a  conventional  urrungement  Ijetwcen 
thvni ;  but  do  tlie  public,  when  they  purchase  these  pi)wders,  under, 
stand  thai  there  is  this  udinixiure  in  the  one  case  ot  four  tn  one  of 
furiMgn  materiul,  and  in  the  other  of  seven  to  one  of  foreign  m^ 
terial  ?  "— "  CerlAinly  not" 

*  Thii  renurliablc  nxprmiloD  wu  ArM  uDfilo)*!  by  Mr.  Redwood  ia  dsfaooi  of  idul- 
tOTMkm. 

o  o  3 


ftft6      EVIDENCE    BEFOKE   PARLIAMENTART   COMMITTEE 

**  Does  a  mcdioAl  man  who  prescribes  those  powders  expect  to  W 

those  proportions?" — "  Certninlv  not." 

"Then,  aliliMU^'Ii  this  may  bea  i-onvention&l  mntter  between » l**" 
tion  of  the  Irmle,  tiie  public'is  lilemlly  defrau'le*!?"— "  UiMJoobtodljl 
nor  do  I  believe  lliat  the  public  in  tiny  tnatance  are  ft  partT  to  1*5 
adullcrnlinn,  or  willln^^ly  purcliasean  article  which  is  adultcnitc^' 

Now  these  compound  powders  form  part  of  the  stAek  of  eetrlT  lU 
wholcMilc  druggists,  inchirlinfr  even  many  of  the  most  re»frrUblt 
Wo  have  now  in  our  p<»&<ession  suniples  of  all  thesv  ptwUffi  •ap- 
plied to  U8  by  one  of  the  first  houses  in  the  drug  trade.  Not»it^ 
8taiidin>;  this  notorious  fact,  that  tlii^y  are  tlius  coniuiuidy  kfpt  nA 
sold,  Mr.  James  fiaiss,  after  fencing  a  r>ow\  de^d  nith  the  Coanittec* 
gave  ihe  iinnexed  reply  to  a  question  by  Mr.  MnfTitt  :  — 

^*  You  are  not  aware  of  that  orllele  (compound  gentian  pa«4ir) 
beinjr  ont*  of  tlie  current  articles  in  the  drug  trade.** — "ll  n^ 
only  be  in  very  rare  inslanees." 

We  ttflirm  thiit  there  is  i*curuely  another  wholesale  c!iCB0st  a4 
dru;;«:iHt  in  the  kingdom  who  would  have  ventured  upon  a  lim^ 
statement. 

It  is  ur^ed  in  defence  of  the  manufacture  of  these  prtwdcrs,  tkal 
they  are  exclusively  used  as  cattle  medicines.  Tbis  fftatrntvnS  t>  ■«* 
incorrect,  in  proof  of  which  we  need  only  rel'er  to  the  wrticlee  oaTafr 
mcric  and  Litpiorice  powders.  Besides,  why  should  adtdti'ratsd  Mr* 
ders  containini  larpe  quantities  (»f  starch,  jeUow  ochre,  &c-,  lie  Uval 
down  the  throats  of  cattle  any  more  than  of  human  beings  ^ 

Mr.  Guy,  a  witness  before  the  Parliamentary  Oimutlttif,  bVB 
whose  eviflonce  we  have  before  had  occasion  to  tiuoie,  gave  the  U- 
lowins  answers  to  questitins  by  the  Committee,  Laving  nelocaeili 
a'lulteraiion  bv  drug  grinders; — 

"  I  wAA  etnploveil  a  long  time  in  what  is  cftlled  a  grist  miU,  aadac 
split  upon  tht*  average  sumetlung  like  60  or  70  ijUHrters  of  bMM  I 
day.  Egyptian  beans  contain  a  great  deal  of  dirt ;  if  a  cmn  ataim 
100  stone  of  Egyptian  beans,  when  we  w^ished  the  diil  out,  th«  w«aM 
be  reduced  5  intone,  leaving  9J.  We  asked  the  persoo  w^  ttt/t 
them,  *  How  much  do  yim  expect  to  be  relumed  out  of  th»  \^ 
stone?'  —  *'  If  he  said  he  wanted  1 10,  there  being  5  f!'-  r-  <  -•  —  ■*-♦ 
there  must  be  15  stone  more  sent  to  him  than  he  actn 
mill,  thiiiinh  it  is  not  injurious  to  health,  because  it  Is  1^  «.;.-.^  --.,— 
of  water." 

*'  You  added  ihe  weight  by  soaking  the  beans  in  water?** — "Tbc 
we  were  compelled  to  do  it;  he  sent  so  many  hundrcdweiglit  to  I* 
split,  and  told  us  he  wunted  so  many  hundredweii;Lt  Imi^  ;  iW  ■ 
done  by  what  Is  called  in  tlie  trade  '  washing/  with  a  virw  to  viA 
the  dirt  nm." 

^fr.  Sfierinan.  "  IlaTe  you  had  drugs  also  to  grind  to  Ut*  «K 
way  ?"— »  Yes." 


ON   THE   ADULTEHATION   OF   DRUGS. 


567 


my  nl: 


How  lonp 


as  burnt  iiown." 


Uint?"— "  I  think  it  is  nbont  three  years  since 

y  nhice  was  burnt  iiown." 

"  TiVlittt  kind  of  proportion  did  the  peraon  who  sent  the  dni^  to  you 
to  be  ground  require  back?"  —  "It  nepemled  upon  {hn  pnrlies.  Take 
the  cmse  of  rhubarb;  whatever  may  be  said  about  Kn^il^h  rhubarb 
bein^  sold  to  the  public  m  KnjiHsh  rhubarb,  it  i-i  mostly  ^-ohl  under 
the  iiutne  of  Turkey  rhubarb,  ijier^  Is  no  question  about  that ;  I  have 
had  5  cwt.  of  rhubarb  sent  lo  be  pround,  pcrhapi  2  cwt.  would  be 
Turkey,  and  3  cwt.  English  rhubarb." 

Chmmian,    "In  the  ground  stule?"  —  "  Yes." 

Mr.  Sheridan,  **  Su[»posin^  a  hundredwei;»hl  of  Turkev  rhubarb 
wore  Rent  to  be  ground,  would  a  hundrwlweight  be  returned?"  — 
»'  No." 

"Who  ffuflered  tlic  loaaP** — "The  proprietor;  perhaps  he  would 
make  it  up  with  inffrior  rhubarb.*' 

Chairman.  **  There  was  no  uttcmpt  to  supply  the  waste  by  any 
other  material  ?*'  —  "  Yvf  ;  I  have  seen  th:it  done  bv  satinwood  saw- 
dust. I  have  in  my  mind  mease  In  which  two  hundredweiKhl  of 
sarinnrood  sawijut«t  wert.'  ground  up  with  rhubarb,  packed  in  flint  l?ot- 
tles^  an<l  sent  abroad  " 

Mr.  ShrritLm.  "  Do  you  nieon  to  say  that  that,  is  the  custom  of 
the  trade?" — "I  do  not  say  that  it  ia  tlie  custom  of  the  trade.  I  have 
ground  but  few  thin;:!*  genuine,  as  for  as  my  experienrc  has  ^onc.'* 

Mr.  KtttNaird. ~ **  Wtixv  long  were  you  in  businessP" — "I  WM 
thiriy  years  a  inuniard,  chicory,  drufj,  and  «pice  prinder." 

"  Durini;  that  time  v*>u  very  seldom  sent  fortli  a  pure  article?"  — 
»  No." 

"  Can  you  say  whether  ndulleralion  has  been  rather  on  the  increase 
during  the  last  few  years  yuu  were  in  business?*'  —  **I  am  sureilhaa; 
new  t)un;:i<  huve  been  found  out,  which  years  ago  we  knew  nothing  of, 
to  aHuiteraie  with." 

Mr.  SfieHftan.  "Had  you  any  book?"  — "I  had  a  book  till  my 
place  was  burnt  down,  which  j;avc  the  detail  of  every  transaction 
from  the  time  I  went  into  buninesK,  [  made  no  i^cruple  to  sli'>w  il.  I 
huve  done  us  much  in  the  «ray  uf  ailulteralinn  as  any  man  in  the  trade, 
and  I  lutve  done  more  than  almost  any  other  mtin  to  cxfiose  it.  I 
have  done  it  in  defiance  of  my  employers,  with  a  view  to  orxish  it ;  and 
I  have  felt  exceedingly  jrlud  to  nave  an  opportunity  of  pivin^  it  a 
severe  blow.  I  believe  many  honest  men  will  thank  any  one  who 
will  putnn  end  to  it.** 

"i)nyou  mean  lo  say  that  it  was  a  general  instruction  you  had 
from  ihoiK'  hou>e*  to  mix  other  ingre<lient»  with  the  drugs?"— "  1  cannot 
say  thiit  1  hod  one  i;ust<imer  on  my  books  but  what  has  been  com- 
pvlleit  to  mix  more  or  ie.'S." 

"Still  your  experience  as  a  druy;  grinder  leaila  you  to  say  that  it 
is  the  prevalent  practice  with  the  wholesale  druggists  to  send  two 

o  o  4 


568 


EVIDENCE   OW   AOtJI-TERATION  OF    DBUGS. 


BubstAnccs  to  be  mixod  together,  to  be  sold  m  one  trticle?" — ^T 

haT«  lljuml  it  so." 

Mr.  Mnjfiitt.  "  A»  a  drug  prinder  were  \r>u  ever  called  upon  t« 
introrlucf  any  otiier  subtitanco  into  x  drtitr  before  you  sent  it  borne  ^** 

—  "Yes;  sfunelimen  the  adulterate  has  been  sent  to  me  to  n»ix,  awl 
sninetiines  they  have  sent  to  me  tu  suy,  *  Put  in  so-anil-so,  juid  charffv 
lor  it'" 

**  Were  those  instructions  applicable  to  a  great  varietj  of  dra«a  ?" 

—  "To  rhubfirb,  jalap,  and  cocculus  mdiuus;  I  hare  grounj  manjr 
cwts.  of  coceuius  "in  lie  us." 

"And  you  Imve  worked  for  a  preat  number  of  respectable  whAle- 
sale  druygists?"  —  "  I  have  worked  for  a  pTvat  niuuber  of  respectable 
whoIfSuK;  drupgists  in  thy  romitry,  wliere  iiiv  mills  were." 

"  Where  were  yfiur  mills  y"  —  "  Nenr  Leeds." 

"Have  you  had  iiny  experience  with  re"«rd  to  drug  grinJing  ia 
London?" — "1  have  ground  a  good  bit  in  London." 

"DotB  your  evidence  apply  also  tn  the  London  dnigjriaw?'"— 
"Yes;  thut  ca»e  of  the  rhubarb  being  mixed  with  Mtinwood  mw- 
du«t  ntx*urre<i  in  Loiidnn." 

Theevidenceof  Mr.  Bell, given  beforf'thePurliamcntnry  Commiltee^ 
in  regard  to  the  practice  of  druf;  grinders  13  ]tarli('nlnrly^  valuable,  as 
coming  from  one  whiL,  like  his  friend  Mr.  Redwood,  hoi  on  more  than 
one  occasion  sought  eilhcr  to  deny  the  cxislcnce  o(y  or  to  palliate  and 
excuite  ailulteraiimi  : — 

^  Are  you  of  opinion  that  n  ^eat  deal  of  adulteration  takes  place 
among  drug  grinilers?"  —  "I  think  Roine  adulteration  dot»,  but  not 
nearly  so  much  as  wa«  the  ease  some  years  ago;  it  was  fonurrlv  the 
cuitfom  t(i  send  fourteen  pounds  of  a  iirng  to  be  gmund  and  receive  a 
quarter  of  a  hundredweight,  and  gomelinies  Imlf  a  huiiilrednrclgiit 
bat^k ;  but  that  custom,  I  believe^  is  oniir**1y  di»M>niinuiHl. 

*Vr.  WUe,  —  "  Have  you  not  heard,  and  is  it  not  a  frcqui*nt  ftcrur- 
rence,  that  persons  are  sent  in  charge  of  drugri  which  are  t<»  be  pround, 
fO  as  to  wutoh  that  no  adulteration  takcti  place?" — "1  have  not 
hear<l  of  (hat  as  a  frecjuunt  occurrence.  I  sbould  be  very  surry  to 
employ  a  person  to  grind  drugs  who  required  looking  alter  in  that 
way  ;  it  may  have  been  done.  Till  very  recctitlif,  it  wa-^  always  t)ie 
rase  that  persons  expected  to  receive  fAtfyw// quantity  back  in  powder, 
without  any  allowance  for  loss  in  grinding.*' 

A  few  other  facts  may  now  be  cited  in  further  proof,  if  any  were 
needed,  of  the  extensive  prevalence,  till  within  a  recent  period,  of 
adulteration  in  drugs. 

The  Am(?rican8  found  that  the  drugs  iniported  into  (he  Union  fVom 
this  country  were  so  infamously  adulterated,  that  io  self-defence  iliev 
were  driven  to  appoint  inspector;)  and  examinei*s  in  some  of  the  placca 
of  Import.  Still  later,  tlit?  Spaniards  disf^ovore*!  that  they  were  snb- 
jected  10  the  siime  inqntsition,  and  were  compelled  to  adopt  nieamre* 
of  precaution  of  a  like  character. 


TOBACCO,    AND    ITS   ADULTKKATION'S. 


569 


The  qunntitie*  nf  damagetl  and  fldulteniUHl  dnigi  rojectod  by  the 
Americuim  is  rcnily  nmrvellnuo,  an  will  be  wen  by  reffrence  to  thv 
eTiilcnce  given  by  Mr.  Jiicub  Beli  before  the  i'arliamLMitiiry  Com- 
mittee. 

We  will  now  ntntc  nt  length  the  results  derived  from  tlw  microsco- 
pical exaiiiinstion  and  chemical  anaWsis  of  aooie  of  ibe  principal 
drug!,  under  which  head  we  include  lobaccu. 


TOBACCO.  AND  ITS  ADULTERATIONS. 

Tobacco  <<on»t»ts  of  the  dried  leaves  of  several  different  species  and 
varielii'S  **t  plnnt^  belonginfr  to  the  gt-nus  Aicotiavtt,  of  the  fanidy 
.Vrr/uftnrmr,  which  inrludet^amon;*:*!  other  tnediciiiu}  [)laht.shyo>cyanius, 
bellailunna,  and  stramonium. 

The  tobiicco  plant,  ueconHng  to  Humboldt*,  has  been  cultivated 
fnnn  time  immemoriul  by  the  natives  nf  Uronokn,  hut  it«  intn>diictic}n 
into  Kuriipe  apiK>iirs  to  huvc  taken  place  subrte«|Uvnt  to  the  discovery' 
of  America,  allfiou':h  there  'a  ruasun  for  believing  that  it  was  known 
to  the  jV^ialios  Iniig  bt^fore  that  tJuic. 

The  cTisiom  of  fluinking  cigars  was  beheld  by  Columbus  and  his 
followers  for  the  first  lime  on  their  arrival  at  Cuba  in  WO'i.f  The 
plant  was  introduced  into  Spain  and  Portugsl  bv  Hcmandoz  dc 
Toledo,  and  Joan  Nicot  about  1559-60  sent  the  seeds  from  the  latter 
place  to  France.}  On  the  return  of  Sir  Frani'is  Dnike  with  the 
colonists  fn>m  Virginia  in  1586.  the  practice  of  mioking  wa^  introduced 
into  England,  and  stkui  l»ecame  general,  bir  Walter  Haleigh  being  ime 
of  the  fii«C  to  adopt  it.^ 

Subsequent  to  it.t  introduction  into  Euro[)e,  various  nttempts  were 
made  to  prohibit  the  lonoking  and  use  of  t(»l»iici*o;  bur  all  tlie  writings, 
pains,  and  penalties  proved  incirt*ctual,  and  tlie  practice  went  <m  ex- 
tending, until.  IIS  al  present,  it  has  become  almost  universal.  One  nf 
the  most  celebrated  of  the  t real i»e4  written  ai'uinst  tobacco  was  the 
**Couit(erblaSte  to  Tobacco,"!  by  Kitig  Jjiim.'s  the  First. 

In  Great  Ijritain  the  eultivjiiion  dl  inbacro  is  still  restricted  on 
account  uf  iho  revenue,  nut  more  than  half  a  |>ole  (two  yunls  and 
threc-qunrtcrs)  l>eing  iillowed  **  in  a  physic  or  university  gardeti,  or 
in  any  private  gnrden  for  phytic  or  chirurgcry." 

The  generic  nppetlatiun  of  Nicotiatia  Is  evidenlly  derived  frotu 
Nicot,  the  name  of  the  imlividual  by  whom  ihc  plant  was  first  sent  lo 

*  Pertona)  NaftjiiU*,  tnl.  «   p.  tf*. 

t  lluliin  nf  Itie  Lib-  aimI  Vnyafr-v  ut  Ci^lutnbua.  W*ih>a(lon  trvlnff,  vol.  I.  p.  %?. 

t  B«uUlu'«  Viutx.  i  Ulosrsph.  Brit.  vol.  t.  ^  3471  ||  Work*,  p.  Sli.  f.  |«l«. 


S70 


TOBACCO,   AND  ITS  ADULTEHATIOKS, 


France,  while  it  is  probable  lh»t  the  specific  word  tefranm  pn%  to 
one  ot"  the  principal  specie*,  ia  derived  from  tnbac,  the  haiMofUte 
insfrument  useii  by  the  niitives  of  America  for  snioking  tnhamo. 
Some,  howi'VtT,  {Utivc  tlie  word  from  Tobago,  others  from  Tobuoov 
a  town  in  Now  Spain. 

The  print-ipal  Hp<>cies  of  tobacco,  and  alfio  that  emplored  in  nrii* 
cine,  is  Nicodnnu  Tabacum,  or  Virgittian  tof>ac€0 ;  it  i»  a  berbtceflB* 
plant,  reaching  from  three  to  six  feel  in  height,  with  a  viici'J,  S'Jn^T 
luiee;  the  leaves  are  aes^ile,  large,  pale  green  when  fn-sL 
lanceolate,  acuminate,  and  clutliet)  with  fhott  frlandulur  h^ 
extensively  cultivated  nearly  all  over  the  world,  but  chiefly  lu  ll<; 
United  States  of  America^  Virginia  being  tbe  most  celcbnted  ftaia 
growth. 

Of  tliis  species  several  varieties  are  cultivated ;  Virginian.  Kentucky, 
Maryland,  and  Columbian  tobacco,  are  all  obtained  from  it. 

The  leaves  of  A',  latistima  (Milter),  jV.  murrophylla  (SprciiltJX 
yield  the  large-haved  ur  Oronoho  tobttrco.  Tliia  i»  prubahly  nrrof  • 
variety  of  the  preceding  !>peeies;  it  likewise  presents  rertaia  mom* 
cations  or  varieties  di-pendent  upon  the  size  ainl  form  '•* 
also  upon  whether  they  are  sesnile,  or  fiirni;«heil  with  h 
cordinj;  to  l)on  the  lar^c  Havannah  cigars  are  prub;i: 
the  leaves  of  this  species. 

The  leaves  of  the  N.  rusiica^  common  green  toharr. 
tobacco  of  Salonieu  cir  Thessalonica;  also  the  Turkish  '■ 
on  the  coasts  of  the  Mediterranean,  so  hi*:hlv  valued  • 
probahly  alito  the  celebrated  Lutakio.  The  leaves  of  this  »{ 
peliolati',  ovate,  and  quite  entire.  It  ri|ien5  curlier,  aad  is  monthsrl? 
than  A'.  Tfihacum.  It  is  frequently  cultivated  in  gur<leuf  in  En<;is»l 
and  \!i  U!4ed  by  gardeners  (o  destroy  insects.  It  is  indigvaooi  is 
America,  and  grows  wild  in  Kuropc,  Asia,  and  AfricA- 

N,  Fersica  (Lindl.)  yields  the  celebrated  Shiruzor  Persian  tohaoiL 
Of  the  leases  of  jV.  repawla  (Willd.),  a  native  of  Cuba,  ne^at  Haranml^ 
the  sinnll  Hiivannah  nr  Queen'ts  cigars  are  said  to  be  mode. 

N.  fftiaclriculeii  (Fiirsh.)  grows  spontaneously,  and  is  also  obId* 
vated  on  the  banks  of  the  Missouri  by  the  Indians.  'I*he  tob«M> 
prepared  from  it  is  described  as  cjccellent;  the  most  dcUcaie  if  ms^ 
irom  the  dried  flowers. 

A.  nana  (Lindl.)  grows  in  the  Rocky  Mountains;  tlie  Indians  srt 
said  to  prepare  the  finest  of  their  tobacco  from  tbe  leaves  of  tkii 
species. 

The  last  species  whitdi  need  be  noticeil  is  N.  multit*alrUy  cultitslri 
by  the  Indians  who  inhatiit  the  banks  of  the  Culuuibta;  the  calti* 
which  is  very  foetid,  being  preferred  to  any  other  port. 

The  t4tbacco  plant  is  prupagateil  in  Virginia  and  Maryland  fftB 
Be.^^  These  are  first  snwn  in  turds  :  as  soini  the  young  plants  tia>« 
five  or  six  leaves,  exclusive  of  the  seminul  leavuM,  ihi^y  ore  transplaatsd. 
during  the  Diontb  of  May,  into  fiddSf  the  seedlings  bein^  placed  ivs 


1... 

I...^  u 

\- 

J'.^ 

rumi>ii  tk 

** 

M 

89 

KHja  «^ 

TOBACCO,    ATTD   ITS   ADDLTERATION8. 


571 


or  three  feet«spart,  in  rows.  When  nenrlj  fuU-frrown,  ihc  tops  are 
pinched  off,  to  prevent  the  fnrniation  of  flowor*  and  seetls,  and  to  pro- 
mote the  devf'lopmcnt  uf  leaves.  The  harvest  takes  ptnce  in  August; 
the  mature  pliints  are  cut  off  above  the  roots,  liried  under  cover,  and 
■tripped  o{  their  leaves,  which  ore  tied  in  bundles  and  packed  in  bogs- 
bead*,  &c 
T<il>acco  is  met  with  in  two  states ■» the  "  Raw  **  or  "  Unmanupac- 

TURRU,"  and  the  **  MAKirrACTtlKHD." 

Tobacco  in  the  raw  state  consists  merely  of  the  dried  leaves ;  these, 
as  imfKirted,  are  soinetiines  separnte.  and  pUced  one  upon  the  other, 
as  in  Turkey  tobaceo ;  at  others  they  are  striin;;  oit  8trin<|;s,  as  in 
German  tubucco  ;  but  usually  tbvy  are  iinportcd  in  "  heads"  or 
"hands,**  es  they  are  termed;  the  different  varieties  of  American 
tobacco  come  over  in  this  state. 

There  are  various  kinds  of  ilricil  leaf,  or  unmaniifiictiirccl  tobacco, 
distinguished  by  the  name  of  the  country  in  which  it  is  grown,  as  well 
as  by  differences  of  colour  and  quaiiiy,  arising  chiefly  from  soil  rihI 
climate. 

U.MiTKD  Stats*  Tobacco.  —  The  principal  supplies  of  lobncco  to 
this  country  are  derive^!  from  the  lJnit^»d  States  of  America,  the 
several  kimls  beinjt  name<l  after  the  states  in  which  they  are  prown  — 
as  Vir^iniaTi^  Kfutuchyy  Maryltind^  Misitottri,  Ohio^  and  other  descrip- 
tions all  cultivated  in,  atul  iin[)orted  from,  the  United  Srates. 

Virginian  Tobaeco  h  the  stron^fcst  kind  of  tobacco,  and  is  not,  there- 
fore, well  suited  for  cigars ;  it  is  best  adapted  for  smoking  in  pi|)es  and 
for  .snuff.  The  colour  of  the  leaves  is  deup  brown,  and  they  present  a 
mullted  appearance;  Ihev  ^eel  unctuou%  and  are  so  tough  that  they 
may  be  bent  d<iuble  wiihimt  breakina,  when  not  over-dried.  Sim;e 
this  tobacco  will  retain  more  moisture  than  almost  any  other  kind, 
and  since  iu  strength  is  much  greater,  it  is  extensively  use<l  by 
tobacco  manufacturers. 

Maryland  Tobacco  is  paler  in  colour  and  weaker  than  the  former; 
the  '*/Ki/e  CinmrmoH"  is  dm  best,  the  '*AVni6*"  the  commone»L 

Kentnckg  Tohocvu  itf  deH-rilK'd  ax  bein^e  intermediate  in  strcQigth  be- 
Iwei-n  these;  it  is  paler  than  the  Mrcinia. 

Carolina  Tobacco  is  less  frec|uent]y  met  with,  and  is  of  inferior 
quality. 

Ctfiumbian  Tobacco  in  much  esteemed  for  cigars,  for  which  it  is  more 
used  than  any  other  kind.  The  leaves  are  markeil  with  light  yellow 
spot^  Oiher  varieties  of  Oilumbiun  tnb.t<-co  are,  Varitias^  brought 
over  in  rolU  and  )ieajh<,  a  very  mild  tobacco,  and  Cumana, 

Oko!(oko  Tobacco  comes  over  in  separate  leave«;  it  is  of  a  yellow 
colour,  and  is  very  miM  aitd  delicate. 

CunA  Tobacco  iit  also  a  mild  loharco,  and  the  most  esteemed  for 
cigars;  tliat grown  neur  ihe  town  of  Hacaunfih  U  the'  finest ;  the  leave* 
of  lliis  are  yelhiwiah  brown,  with  a  mutiky  or  spicy  odour.  The  ordi- 
nary tobacco  grown  on  the  ialand  is  darker  iban  the  Havannub.  lioth 


67S 


TOBACCO,    AND   ITS   ADULTEHATIOX8. 


kin<l9  arc  imported  in  heotls,  and  are  remarkable  for  the  *]ij;1it  yeiloi 
spots  oil  tlie  leaves. 

St.  Domingo  Tobacco  come«  over  in  separate  Icavea,  and  is  of  In- 
ferior quality. 

fiB\ziLiAii  Tobacco.  —  A  very  small  quantity  only  of  this  tobacco 
is  iuiportetl  Ironi  the  Brazils. 

Dutch  or  AMEBsrooRT  Tobacco  is  very  milj,  and  deficient  in 
flavour ;  tlie  darlcL-r  kirnl  is  the  strongest,  and  id  mutU  used  for  snufiT; 
while  the  milde»l  is  employeil  fur  the  c'onnmnne<{t  cigars. 

Levant  Tobacco  includes  Turkey^  Laiakia  (a  Hvrian  roharco), 
and  Suhnica  tobacco;  thc^e  are  nil  the  produee  of  Nieotiana  nutiea; 
they  are  mild,  but  valuible  tobaccos.  Turkejf  tobacco  comes  orer  in 
broud  and  fifparate  leaves,  of  a  bright  yellotv  colour. 

Persian  or  Shiraz  Tobacco  is  al»o  a  Levant  tobacco;  it  is  tlelicftte 
and  fnijrrant,  and  is  the  proiluce  of  Nicotiana  Persica. 

Another  description  is  Kast  India  Tobacco,  of  whicb  a  small 
quantity  only  \a  imported  ;  it  is  not  mueh  estoenied. 

Mfwi/lii  'Johfifco,  grown  near  the  town  of  Manilla,  :n  Lucon,  one  of 
the  Philippine  Islaiid.s  is  u  dark-coluured  tobaecOf  and  ia  extensively 
use<l  in  the  manufacture  of  cheroot*. 

In  the  hiinds  of  the  nianutiioturer  the  leaf  is  converted  into  momt- 
Jachired  tobacco  in  the  following  manner :  — 

The  leaves  ore  unfolded  and  "  strip[>tid"  — that  is,  the  mid-rihs  or 
stalks  are  removed  ;  this  is  done  by  a  sudden  jerk  of  the  stalk  by  the 
hand,  holdimr  by  the  leaf.  They  are  then  sprinkled  with  "saace" 
or  *•  liquor;'*  thi*,  properly,  should  conMst  of  water  onlv,  bnl  in 
some  rases  it  eontuins  salt,  and  is  coloured  with  treacle  or  fiquorice; 
but  these  additions  are  adulteruliont.  After  the  sprinkling;,  by 
which  Um  leaves  imhibe  a  ^ood  deal  of  the  liquor,  and  therefore 
become  iuereaseil  in  weight,  Ihey  are  put  into  Urye,  Hat,  Mjuare,  iron 
boxes,  and  pressed  into  a  solid  cake;  durtnj;  the  pressure,  if  too 
nmch  "  liquor"  has  been  used  for  the  sprinkliiiir  of  the  Kavea,  some 
escft|>es,  deeply  coloured  with  extractive  derived  from  the  tobacco 
leaf.  This  mixed  with  the  washings  of  the  cloths  Uiiod  in  pressing, 
is  gold  as  ''lol'aceo  water,"  and  is  used  as  a  sbeett-wash,  and  also  by 
cordeners  to  destroy  worms  anrl  other  venuin.  The  cake  is  then  eut 
into  shrecls  witli  kuife-ed^ed  ch<»pping-stumps,  the  shreds  varying  in 
diameter  of  from  sixteen  to  one  hundred  to  the  inch.  IjOstJy,  the 
tobacco  in  this  state  is  li>:htly  dried  or  "  stoved"  in  a  flat  copper  or 
iron  tniy,  Iteated  by  sand,  and  freiiuently  by  steam. 

The  above  pnxrcss  of  course  applies  only  to  cut  or  suao  ronacco : 
in  the  manufaeturo  of  "boll  tobacco"  a  lolully  diiferenl  method  is 
followed ;  — 

The  leavBs,  or  rather  the  half-leaves,  ore  arranged  end  to  end  in  a 
line  down  a  long  table;  thii*  is  mostly  dune  by  women  or  boys.  One 
of  the  leaves,  having  first  been  twisted  into  a  kind  of  thin  rofie,  is 
attached  to  an  iron  hook,  which  is  made  to  rcvolre  rapidly,  by 


TOBACCO,   AXD    ITS    ADULTKRATION8. 


979 


of  a  wheel,  in  a  borizonltti  position  on  a  level  wiili  the  surface  of  The 
tftble.  The  "'  spinner"  thi'n,  wiili  u  <tinull  tHKinl  Hxcd  to  thi*  palm  of 
the  hand,  while  tlie  rope  \s  tiirniojr,  Mttat^ht^i^  leaf  at'Cer  leaf,  itiUing 
und  hiinietiiii^v  it  with  the  board  as  tho  length  proceeds.  When  Biifli- 
cienl  i-^  mauufootured,  the  rope  b  coiled  up  ^n  ns  tu  form  u  burrel- 
sbaped  pile  nr  mas?,  ench  layer  Iwing  well  oiled  with  »  hruyh.  In  pr«f- 
venl  the  uuilu  from  udbering  to  each  other.  Tlic  coiU  beiiijj  tJrmI/ 
I»*«jied  togelhtr  with  wooden  nailc^  the  whole  pile  is  then  steeiK*<l  in 
"  Tiquor,**  and  Grmly  prestied,  oilc),  ftnd  polished  with  a  bruiih.  It  is 
estimated  that  this  kind  of  tobucco  increaaes  in  weight  in  the  inanu- 
faciure  from  fifteen  to  twenty-five  |>er  cent. 

All  miiiiofactured  tobaccos  may  be  referred  to  one  or  other  of  the 
four  fnllnwing  f(^^m^  or  kinds  :  — 

In  the  Britl  kind  tlie  leaver  are  cut  into  shredx ;  to  this  all  the  dif- 
ferent varieties  of  cut  toitacco  belong. 

In  the  second,  tlip  leavi»s  are  twisted  or  (tpun  into  a  kind  of  rope  ; 
thi:3  includes  the  dilTrrenl  kinds  of  roU^  spun,  or  twist  tithacco. 

In  the  third,  the  stripped  leaves  are  folded  one  over  the  other,  so  as 
to  form  C'ffttrt  and  cheriMti. 

In  the  iburth  foruu  the  leaves  are  reduced  tu  powder,  constituting 
snuff'. 

We  need  only  describe  at  present  the  different  varieties  of  cut  and 
roll  IfibiiciMi ;  — 

The  chief  kinds  of  cut  tobacco  are  Sha^,  Heturus^  and  Bird't-eye; 
other  less  common  kinds  ore  Maryland^  K^NtuUr^  Orottoko^  Turkey^ 
Persian^  and  Variitaa, 
Shag  is  prepored  chiefly  from  Virginia  and  KenlucJty  tobacco. 
Returns  is  a  ligfat-colourcil,  mild  tobacco.  The  true  derivation  of 
its  name  is  said  to  be,  that  formerly  the  tobacco  known  lus  '■  shfrt  cut'* 
was  with  luucii  labour  rublwd  through  a  wii-e  sieve  ;  the  finer  j>or- 
lions  and  du»t,  lechnic:dly  called  "smalU,**  pii^^ed  t)irou};h,  jiiid  wirre 
j4U]ip<jsed  to  be  much  the  5tronji;e9t ;  when  no  mure  would  ^o  thmuj^'h, 
that  which  wos  left  upon  ihe  sieve  was  rtn'koned  tu  be  uiilder,  and 
■  •f  superior  quality,  and  called  in  the  traile  "  Returns."  Acoord> 
ins  to  I'ereira  its  name  **  derivetl  from  it*  Ivinp  formerly  pn'piircd 
br  ri'turninj;  shiiu  fi»r  re-cutting.  In  the  KefM>rt  on  the  Tobacco 
'1  rade,  bv  the  Select  Comtnittee  of  the  House  of  Commouft,  ntidu  in 
Au*;ust  1844,  it  is  described  ns  "made  up  of  the  :«mii11  pieces  uf 
broken  leaves,  and  the  dust  and  sifiings  ])ntduced  in  the  various  pro- 
cesses nf  maniifrtcture." 

Sirrf«-rytf  differs  from  the  other  Tarteties  in  containing  the  mid- 
ribs of  the  leaves,  ihe  imnsverse  slices  of  which  have  been  I'ancirully 


compared  to  the  eyes  of  birds. 
Tlie  principal  kinds  of  roll  I 


tobacco  are  Pigtail^  liogie^  AUoa^  Negro- 
ketid^  an<l  Cacertduh. 

The  first  three  are  used  entirely  for  chewing,  nnd  are  distinguished 


CavenfltMh  U  mftde  in  smsll  eqtiare  flat  cakes,  about  an  inch  and  a 
balf  wiile  by  five  inches  l(»iig. 

Structure  of  Tobacco, 
Th«  k'Hves  of  tobnofo  present  Bcvernl  well  marked  pecnliortHf  o/ 
'*,  by  wbicb  ibej  may  be  readily  diatinguisbed,  eren  in  their 


TOBACCO,   AND   ITS   ADCLTERATIOKB, 


573 


manufacfured  state,  from  tboiie  of  most  other  plants,  llicsc  pecu- 
liarities can  only  be  sutisfuctorilr  detertnincii  by  means  of  the  micro- 
scupe,  and  it  is  very  imporlant  that  they  should  be  clearly  undcr^jtood, 
fftr  without  a  knowledge  of  them  it  is  often  impftssiblt*  to  discriminate 
between  f^cuuinc  and  adulterated  tubacco  —  a  ptiint  of  the  greatest 
consequence,  since  no  less  than  about  four  millions  and  a  hulf  (joundfl 
sterling  are  derived  annually  from  the  duty  on  tobaceo,  and  since  it  is 
known  that  the  revenue  is  defruuded  to  a  large  extent  with  uom- 
parative  im^junity  by  the  adulteration  uf  tobacco.  MobI  leaves  may 
be  divided  mto  two  parts,  the  bruad  eA[>anded  part  or  lamina,  and 
the  mid'Tib  or  stalk  and  veins,  as  they  are  cuUe<i,  which  traverse  this, 
impart  in<;  t(»  it  strength  and  solidity  in  the  same  way  as  do  the  bones  of 
an  animal. 

I'he  Ituiiina  is  composed  chiefly  of  cellular  tissue,  and  the  veins  of 
woody  fibre  and  vessels. 

A  minute  fragment  of  tobacco  leaf,  viewed  on  its  upper  surface  with 

Fig.  IS». 

l^aOKR  SCKTACK  OT  IjUV  OF  To*«O0Q. 

Ikhcolled  820  dluncUn.) 


a  half  or  quarter-inch  object  glass,  is  seen  to  consist  of  a  num1>er  of 
cells,  joined  together,  and  having  smooth  and  waved  borders,  with 


576 


TOBACCO,    AND   ITS    ADULTEIljlTIOira. 


here  and  tbere  stom&U  and  numerouB  hn'tn,     Hk^c  liwnvrfivni 
liar;  itiey  iire  of  the  kind  icnned  pUndular  —  tfam  is,  tL^ 
in  u  roumlish  swelUD"  or  enUr^'oinent,  very  clearlj  seen 
dried  IcMif;  I'urtbtir,  llu'  ha'm  vurv  greatly  in  &izc^  and 
ihev  are  divided  or  compound,     /i^.  184. 

l*he  under  yurfoee  nf  the  li'af  presenu  a  nearly  similar 
but  the  itloiuata  are   much  more  numerou*,   and   tbe   hair*  ftinr. 
Fig.  185. 

The  veins  and  mid-ribs,  viewed  in  transrcrst*  sections^  ttt  4 1 
rresrentic  nr  horseshoe  form.  It  hat  been  cf>n?id»rred  bv«»BwtUl 
the  stulka  of  toVfarco  may  always  be  djstinjrulhh^-d  fnMii  ti»i»f  i>( C*^ 
pliiiits  hy  tbid  ehnroeter.  It  a|ipear<s  however,  that  «M-t:oni  ri  iW 
fttnlka  of  stramonium  and  byoxcviitinis  present  a  nearlr  MiitiUr  ««!• 
line ;  but  these  plunta  are  Rtrarcely  likely  to  bv  use«l,  uuiler  ui<  rir* 
cunmtances,  by  tlte  luanufactiirer,  for  tbe  adulteration  of  luljoirr^ 

Transverse  sections  of  tbe  suioller  veins  under  an  iucb  ot>irct-£rU.i 
present  the  appearances  shown  in  ibe  following  6«pire. 

F(f,  IBfi. 
TBAXirnsi  SffCTios  or  Mii»-iiii  or  LB4r  urn  TueuW* 


On  the  outside,  runninif  all  round  the  section,  jfy.  Ifttf,if«  Uy^^ 
the  cellular  tisstie  of  which  the  laiuinaof  tbe  leaf  U  iueif  luihil^av 


TOBACCO,   AND   ITS  ADDLTEBATI0N8. 


fir: 


poted,  bearing:  on  iu  outer  surface  the  gandular  bairs ;  in  the  centre 

of  the  section,  the  cut  extremiiies  of  the  elongated  cells,  woody  fibre, 
and  dotted  ducts  of  which  the  stalks  arc  chieflr  made  up,  are  seen, 
having  a  somewhat  radiated  disposition.  These  structures  are  more 
clearfj?  shown  mfg.  187. 

Fie- 187. 

Fosnov  or  TtAVfriBsi  fiicnos  at  Mio-kik  or  \^xt  o»  Tobaooo. 

(IfafnUcJ  WtUuDftan.) 


Fig.  188.  represents  a  lonjijltudinal  section  of  one  of  the  emnlW 
mid-ribs,  in  which  the  cells,  tibrcs,  and  vessels  are  still  more  clearly 
■huwu. 


p  p 


578  TOBACCO,   AND  ITS  ADULTERATION8- 

In  longitudinal  sections  viewed  with  the  qnarter-inek  objc 
a  few  smnll  but  well-formed  starch  coi'piuclea  majr  somtftameal 
Ijing  in  the  cells  situated  just  outride  the  central  part  of  tbeaM 

Fig.  IM. 

LoirarrvsiifAi.  Bwrtioir  or  Mjd-ui  or  ljt*»  ot  TovACVObl 

(MAff&Ua  to  dluMUi*. ) 


In   the  leaf  of  tobacco  re*iiiced  to  powder  all    the 
tures  may  be  rca<illv  detected,  —  of  course  much  broken  op.- 
haire,  cells  of  the  UmintL,  stomutn,  elnn<;ute<l  cells  wood;  fifan. 
portions  and  fmgnienl.i  of  the  spiral  ducts.     Fig.  ]h9. 

The  quantity  of  woodjr  fibre  present  in  the  central  part  of  the  i 


TOBACCO,   AKD   ITS  ADULTEBATXOKS. 


579 


rib  is  \>y  no  means  very  cunsiilerable,  it  being  made  up  to  a  pent  ex- 
tent of  the  spiral  duct3  ;  tbe  tibrcs,  in  general,  uro  more  like  elongated 
cells  tbun  ordinary  woodr  fibres;  nevertlieless,  bundles  of  undoubted 
woody  fibre  do  occur.  Tbe  fibres  are  short,  the  borders  slristcd,  and 
the  extremities  truncate. 


GuKViwM  Cvt  TntACCO 


Composition  of  Tuhncco. 

We  bare  now  to  constdcr  the  composition  and  propirties  of  tobacco. 
Tbe  principal  analyses  of  tobavcu  which  have  hitherto  Leeo  made 
are  the  following  :  — 

P  P  2 


TOBACCO,   AND   ITS  ADULTER ATIOHS. 


VtPiqueliua  AualpHM* 

An  acrid  volatile  principle  (nicotina). 

Albumen. 

ltd)  matter  soluble  in  alcohol  and  water. 

Acetic  acid. 

Supemialnte  of  lime. 

Oiloropliylle. 

Nitrate  of  potash  and  chloride  of  potusium. 

S)(l  ammoniac. 

Water. 

Ejrpressed  Juice  of  Ltcvta. 

The  /«ire#  contained,  In  addition  lo  llie  above,  woody  fibrf, 
and  phospliiite  of  lime,  oxide  of  iron,  and  siliea.  The  two  Uu<f1 
stancen  were  obtained  from  the  ai^hes.  ManvfaeturtH  tthoeeo  MK 
tained  the  same  principles,  and  in  addition  cArl>i>n;ite  of  anmumistti 
ehloride  of  calcium,  perhaps  prcMJuoed  bjr  the  reaction  of  nal 
and  lime,  which  are  added  tn  tobacco  to  give  it  pungency. 


Potxelt  und  I^etHmantu*  AnalffMJf 

Nicotina  .  -  -  .  . 

Concrete  volatile  oil        - 

Bitter  extractive  -  -  -  ■ 

Gum  wiih  malatc  of  Ume  ... 

Chlorophylle       -  -  -  -  . 

Albumen  and  gluten       -  -  -  . 

iVItiHc  acid  -  -  -  -  . 

Liunin  and  a  trace  of  starch        -  -  . 

Salts  (sulphate,  nitrate,    and   malate  of  potash, 

chloride  of  potassium,  phosphate  and  malate  of 

lime,  and  malute  of  ammonia) 
Silica      ------ 

Water  .  .  .  -  „ 


Q7SI 
IHIU 


Freeh  leaves  of  tobacco     - 

CtfnwtlCa  Anafytix.^ 
Gum. 
Mucilage  soluble  in  both  water  and  alcoboL 

Tannin. 
Gallic  acid. 
Chiorophjrlle. 

•  Ann.  df  Ctilm.,  vnt  l»l.  p.  iXt. 

■i  (imf-Un'a  Itanilb.  dv  Ctirm.  vol,  H.  f^  IJ 

I   Sllllmairi  JuiudjU.  voL  xril  p.  SOS. 


100 


TOBACCO,  AND  ITS  ADTJLTEEATIONB. 


581 


Green  pulverulent  maltcr.  soluble  in  boiling  water. 

Yellow  oil  having  llie  odour,  taste,  and  poisonous  properties  of 

tobacco. 
Pale  yellow  resin  (large  quantity). 
XicutinH. 

A  substance  analogous  to  morphia. 
An  oranu^e  red  colouring  mutter. 
jNicolionui. 

or  the  several  constituents^  tlie  presence  of  which  has  been  revealed 
by  chemical  analysis,  the  most  important  are  nicotina  or  nicntine,  and 
nicnriiinin,  as  ujjon  these  the  octive  properties  of  tobacco  mainly  depend. 

NiroTiNA  exists  not  only  in  the  leaveSf  both  fresh  and  fermented, 
but  in  the  roots,  seeds,  and  even  the  smoke  of  tobacco.  It  is  obtained 
by  digesting  an  aiiucnns  extrucl  of  the  leaves  in  rectified  spirit ;  this 
tukvs  up  the  nicotina  in  combination  with  acids;  the  tincture  is  then 
to  be  concentrated,  and  mixetl  with  solution  of  [KitJish ;  this  nets  free 
the  nicolina,  whiob  is  again  token  up  on  agittttinn  with  ether. 

The  aUcjdoid  ui;iy  be  purified  thus:  —  Oxalic  acid  is  to  be  added  to 
the  ctherlal  solution;  oxalate  of  nicotina  fulls  to  the  bottom  of  the 
vessel :  this  precipitate  is  to  be  repeatedly  aliAken  up  with  ether,  the 
nicotina  beinir  sepnruted  as  before  by  |MtJLsh  and  ether.  With  a 
view  to  its  still  more  complete  purification  the  etherial  sniuiiun  is  to 
be  disliltcd  in  a  saU*water  bath,  trunsfcirtMl  tu  a  retort  through  which 
u  current  of  dry  hydrogen  gas  is  ma<lti  to  circulate,  ex|iosed  in  an  oil- 
bath  to  a  temperature  of  284°  Falir.,  to  get  completely  rid  of  the 
water,  ether,  and  ammonia  ;  lastly,  the  temperature  is  to  be  raised  to 
n^G'^  Fahr.,  at  which  the  nicotina  distil?  over  drop  by  drop.  It  is 
stated  that  from  twenty-eight  pfninds  of  Virginia  tobacco  at  least  four 
per  cent,  of  the  alkaloid  can  be  obtained  by  this  process. 

Nicotina  is  a  colourless  lit^uid  alkaloid,  with  an  offensive  odour,  and 
an  acrid  burning  taste.  It  boils  and  undergoes  deeonipo.sition  at  4h2°; 
it  becomes  brown  by  exposure  to  the  air,  and  is  readily  combustible 
with  the  aid  uf  a  wiek.  It  Is  soluble  in  water,  ether,  alcohol,  and  the 
oils  both  fixed  and  volatile;  with  the  acids  it  forms  salts,  which  are 
fnr  the  utost  part  (Tystallisable.  A  solution  of  nicxitina  with  one  of 
bichloride  of  mercury  gives  a  white,  floceulf  nt  precipitate,  a  duuble 
chloride  of  nicotine  and  mercury,  and  a  yellow  granular  precipitate 
with  chloride  of  platinum. 

Scbloesing*  bos  given  the  following  process  for  estimating  the 
amount  of  nicotina  in  dried  tobacco.  Two  drachms  of  tobacco  are  to 
be  exhausted  by  ammuniacul  ether  in  a  continuous  diMilUtory  appa- 
ratus, the  ammoniaad  gas  is  to  be  expelled  from  (he  nicotina  solution 
by  boiling,  and  after  the  evaporation  of  the  ether,  the  amnunt  of  nico- 
tina is  to  be  estimated  by  the  quantity  of  diluted  sulphuric  acid,  of 
known  strength,  retjuired  to  neutralise  it. 

*  CboBlul  Cuutir,  vuL  v.  p,  41. 
P  P  3 


SS2 


TOBACCO,  AKD  ITS   ADULTERATIONS. 


NiraUiu. 

6-87 
6-09 
229 
2-00. 
7- 

7S4 
6-59 
629 
4fU 
321 
2-04 
bvdrocTtni 


The  follijwin?  fire  the  amounts  of  nicotina  eatimatod  bj  liua 

ces9  found  In  (litTtireiit  kinds  of  tobacco. 

100  PtrtaofTubacco  dried  at  Sl'iO. 

Virgina  -  -  .  . 

Kentucky       -  -  -  . 

Alary  laml        -  -  -  _ 

Havannah  (Cigarcs  primera)  less  than 

Lot 

Lot-et-O&ronne  ... 

Nord  -  - 

Ile-et-Vilaine  .  -  - 

Fas  de  Calais  ... 

Alsace  .  -  -  . 

Tobacco  in  powder      -  -  - 

Pure  nicotina  is  an  energetic  poimn  almost  as  active 
acid.     It  WM  employnd   by  Count  BiX'arine  for   the    luunler  o(  bit 
brotlicr-in-Iaw ;  and   bis  trial  at  Mons  a  few  years  since  created  a 
great  sensation  in  the  public  mind. 

NicoTiANi:*,  the  concrete  colatile  oil  of  tobacco,'  tobacco  errmphtr, 
is  obtained  by  distilliition.  Six  pouruls  of  leaves  yif  Id  only  abAut 
eleven  jfrains  of  the  oil ;  it  has  the  odnur  of  tobucco,  and  a  bitwr 
taste;  it  excites  in  the  tongue  itiid  tliroiif  a  sensatiun  simdoriothit 
caused  by  tabsicco  smoke;  applied  to  the  nose  it  causes  «ne«£iii£. 
Ilermbstadt  swallowed  a  grain  of  it,  which  produced  nausea^  cidduiak 
and  inclination  to  vnmit. 

Since  it  is  chielly  from  Tobacco  smokk  that  we  must  draw  ov 
conclusions  as  to  the  effevt  of  tobacco  smoking  on  the  syst^rn*  a  knov- 
ledge  of  its  L>ompo^ilion  U  of  great  importance*  It  has  beeo  analrM^ 
by  several  different  expmuiunlers*. 

The  constituents  of  ToImcco  ^tmoke,  according  to  Raab*,  are 

Carbonate  of  ammonia. 
Acetate  of  amuionia. 
Nicotian  in. 
Empyreuuiatic  oil. 
Carbonaceous  matter. 
Moisture,  and  several  gases. 

Unverdorben -[  obtainc<l,  by  the  dry  distillation  of  tobaccoi  the 
lowing  products  : — 

A  vol  utile  oil. 
An  oleat^tnous  acid. 
An  empyreumatic  acid. 
Resin. 
Traces  of  a  powder  insoluble  in  potash  and  acida. 

•  Zenlt^r  And  Seh»nk.  Valurff^cfh.  d.  TortUx.  Huulelwl.  Bd.  H    V  vs 
t  Paantlorirt  Aiiualrn,  till.  899.  ■  *  *•- 


TOBACCO,    AND    ITS    ADULTERATIONS. 


SS3 


OHorin,  a  small  quanitj. 

A  ha^i!  ftulutle  in  water  (Nicotin  P). 

FiiAcin. 

Kcd  nk:ittcr  <ioliil>lo  in  acids. 

Two  oxtratftivo  matters,  one  forming  a  soluble 
the  other  iin  insotublt:  coiiipoun<l  witb  lime. 
More  recently  Zaiw*  bus  niii<tea  i-artjlul  anulj'stti  uf  lubacco  emoke, 
id  gives  the  foUuwing  as  iu  cunstilueiila  :  — 

A  pvculiiir  urn  pareunia  tic  oil. 

Butyric  aciil. 

Carlionio  ucid. 

Ammonia. 

ParufBne. 

Emp^Teumutic  resin. 

Water. 

Acetic  acid,  probably. 

Carbonic  oxide. 

Cnrburettetl  hydrogen. 
Lastly,  MeUt^nst  lia»  HetecK'd  nicntina  in  tobacco  smoke.  The 
empyrcumatiL-  oil  of  loharoo  is  uhdiNtiiifpiifthable  from  that  of  fox- 
gloTc.  It  is  evident,  therefore^  that  tobucco  smoke  contains  the  more 
active  constiiucnls  of  t»>bncco,  and  that  it  con»c<picnlly  possesses  to 
sotno  extent  the  properties  of  the  leaf.  We  shall  herearter  enter  upon 
the  cjuejilioQ  of  the  eSects  upon  the  system  of  the*  liabit  of  timoking 
ti'biicco,  but  we  now  confine  our  reraitrks  to  the  physiuh^'ical  action 
and  elTects  of  tobucco  when  administered. 

The  foUowing  Tables  were  drawn  up  at  the  aulbor*s  reauest  by 
Dr.  Lcthcby  from  samplt-s  of  unmanufactured  tobacco^  furnisucd  him 
for  the  purpose,  and  were  published  in  the  "Lancet"  for  1853  :  — 


Table  A. 

Skatvittg  the  general  Composition  of  Six  Sampies  of  Leaf  Tobacco^ 
QM  imported. 


KxtTJU-lire  tulubl^  In  eold 
wjilrr         -        .        -        . 

EntracUve  Mlubl«  In  Iwlllnit 
water         .... 

Ligneout  natter  «nd  inxilu. 
bitHlu    -      *      -      - 

.u— ^ 

v^^^ 

ManXmA.  KnoKk;.     Ttakm,. 

(kntMB. 

IS-0 

<at 
<•• 

•0-8 

I1'4 

t-6 

45-1 

11-4 

484 

MO 

1*4 
MG 
10 
770 

10« 
49-0 
1-0 

lOOi) 

iiXN»       loa^o 

1000     ,    100-0     1    100^ 

•  AoMl  d.  ClinDl*  a.  Phwni.,  vnl.  sWII.  p  «|«.,  IH4I. 
t  Ann.  Am  Ctiim.  it  de  Pti/tJq.,  Sme  ««r.  i.  ix.  j^  483. 

r  r  4 


5S4 


CO,   AND    ITS   ADITLTESATIONS?. 


Tablh  B. 

Showv*g  the  general  Cotn^iosfti&n  of  tltn  Mxiractit*e  tnkeri  vp  bjf 

Amjitoniaail  Ether, 


HCWHAt). 

Vlq^dift.       IfiqtBBd, 

K«liiek7. 

r»TWy. 

1(K1 

HI 
l«-4 

CbNir«i>hjleUidr«t       . 

Nlcotiao       -       -       -       - 

la* 
I  ft 

- 

'4 

T 
1 

1^1 

in 

1^< 
1-9 

TqM  tpef  oait,]ioJLibl«Hil 
ethur                                       J 

iP-a 

.. 

IT-Q 

1B-G 

Shoteing  the  Oompositiffti  of 


Hot  AqneatiA  ExtPoctiM. 


iugir  -       -       -       -       - 
Gum     .        ,        -        ,        , 

Addin    chlflllir    niBUtr^    wltli 

Iktie  folnUTln^c  InAttrtr 
StVEb  -        -        -        -        - 
ColDurini  OMtter,  &c,  - 

i>«d. 

Ew«t^. 

r^. 

7-6 

4-4 

4-0 
ihl 

0-4 
lOrl 

11*9 

3-0 
44» 

ntmf 
Vi 

30 

*T'i 

43'JI> 

«-4    1    W-a 

O^ 

U-D 

Tablk  D. 
Showing  the  Composition  of  the  Ash  in  100  Parts. 


Carbonate  of  potash      - 

Hinnnah. 

Vibrate. 

Htfjlsnd. 

Kntoekj. 

T«Uf. 

O 

0-5 

a-0 

4-9 

4-3S 

S-0 

4-1 

Chloride  of  potuslum,  and  a 

little  *oda          .       .       . 

3-0 

0-6 

0-4 

0-M 

0-1 

Ore 

Sulphate  or  potash 

2-7 

a-0 

11 

l-fiO 

0^ 

1-3 

Carbonate  of  lime 

7-4 

52 

5-8 

4-40 

30 

7^ 

Carbonate  of  niHimefia 

2^ 

25 

a« 

1-60 

i-o 

8-3 

Pboiphate  ofUme 

1-6 

1-9 

21 

340 

1-8 

i-9 

Pboapbateof  Iron  and  alumina 

traces 

truces 

traces 

traces 

traeei 

traces 

Silica,  chiefly  tand 
Per  cent,  amount  of  aib 

0» 

7-4 

33 

0-W) 

08 

3*4 

I8« 

31 -6 

19-2 

t5D0 

10-6 

3a-« 

TOBACCO,  AND  ITS  APULTERATIONS. 


585 


b 


Taulb  E. 
Showiuf^  the  Compotiiion  of  ike  Tobacco  Stalk  in  100  Partt. 


CarbotiRCii  of  potuh     • 
rhlnrtdvor  polaiklum  ■ 

Sulphtito  or  pouih 

Alltn'iiM  i>li4>kphiUea    - 
£«'thy        ditto    I 
Iron  uid  Klumiiia 
HitlCA      .  .  - 

Per  cent,  ofuti     - 


lUlMBftk. 

fruBiid*. 

ft-2 

<•» 

C-& 

I'fr 

0-6 

O-l 

7il 

N-4 

a-6 

9-3 

SI 

1-4 

meet 

tracM 

o-» 

0-4 

ti*« 

197 

It  is  evident,  from  the  preceding  ftnidjses,  that  the  eomptwition  of 
tobacco  is  subject  to  vory  great  TuriaLioiiM  ;  reviewinjj  these  anulyseB, 
ve  find  the  Tafiutiuns  to  extend  —  fir<4t  to  all  organic  product!^  and 
compounds,  ua  the  gum,  sugar,  starch,  chlorophyle,  fat,  the  orgunio 
acids  nicotine,  and  colouring  mailer;  and  secondly,  to  all  the  imir- 
ganlc  eubstanccif  and  BallA.  including  u  variety  nt' soluble  oiid  InBiduble 
carbonate!*,  sulphates,  chlorides,  and  phosphaies. 

It  will  be  observed  that  the  ash  tu^ni^lled  bj  the  tobacco  leaf  is 
Tery  great,  amounting  fretjuently  to  conttiilerably  over  twenty  per 
cent.  This  character  has  letl  to  the  suppo:iition  thitt  it  is  possible  to 
detect  the  adulteration  of  tobacco  with  leuves  other  than  those  of  the 
t4>baceo  plant,  by  rae&As  of  the  riuantity  of  nsh  furnished  on  iuciiicra- 
tiou.  It  in  obvious,  however,  that  no  certain  reliance  can  be  placed 
upon  this  test,  since  the  tobacco  a^h  itself  varies  very  greatly  in 
weight,  as  is  shown  even  by  the  preceding  analyses,  in  which  there  is  a 
variation  of  from  lOOG  to  22  6  per  cent.     (See  table  on  next  page.) 

We  are  now  in  a  position  to  form  some  idea  of  the  extreme  diiH- 
culty  in  deterniinino:,  in  many  casc6,  the  question  of  the  adulteration 
of  Ipbacoo.  It  is  also  now  evident  that  it  is  qnite  possible  to  adnltc- 
rate  tobacco  to  a  large  extent  in  n  particular  manner,  and  with  certain 
vnbstancea,  without  the  possibility  of  detection  by  any  means  ut  pre- 
sent known  to  science. 

Mr.  George  Phillips  has  so  far  analysiKl  tobacco  as  to  ascertain  the 
relative  proftortions  of  extractive  and  wtuidy  fibre  obtaintible  from  dif- 
ferent vuiit^ttes  (if  tobacco.  In  tliese  expermient-s  the  extractive  was 
procured  in  tlie  following  manner:  — 

One  hundred  grains  of  t4ilHieco,  previously  dried,  were  placed  in 
two  pints  and  a  half  of  distilled  water;  the  temperature  of  this  was 
raised  tn  176"  Kahr^and  maintJiined  at  that  heat  for  fif>y  minutes;  at 
the  end  of  that  time  the  infusion  was  •tmined,  ami  thn  insoluble  p<»r- 

D,rctaiuedby  the  strainer  or  filtering  pupcr^  re-dried  until  it  ceased 


4 


5%B 


TOBACCO,   AND   ITS   ADULTERATlOKft. 


Table  Jthnwin^  the  Per-ceniage  of  MMHttre^  Extract,  Sahd^  ftpfaHf 
and  Total  Axh^  and  Glucose^  in  Eight  Samples  of  U» 
Tobacco, 


1 

"- 

riMtric 

Eunwt- 

1 

!a 

•XiT-l) 

VirirlTiIa     tear     -       - 

la-M 

MKt 

«iU 

tJlIC 

IG-W 

Ml 

Dittn       Icaf-iUlk     . 

.G-6IJ 

asift 

«-lft 

!>H0 

U-'Aft 

tTMH 

'1 

KrntiicJtf    ItMf 

JV70 

57M 

4-^ 

13  W 

ivia 

!»■■            , 

Dittu       Inr-tulk     - 

MJi 

»■« 

fl-00 

IS-M 

33  »R 

•*tdmUM^  ' 

s 

Mluouri     ■••ar     - 

11-  M, 

It  44 

9-«0 

Itrns 

IN-M 

MB        '  , 

Ditto       le>if.>talk     - 

i*-i<; 

Xfao 

11-44 

lA'M 

»»4 

Ml        1  ■ 

4 

CnUimlifa    leaf      . 

14-M 

«7*fi4 

7  Ifi 

MM 

lfr«4 

fMM        14 

DlUi»       lc«r.«»lll     - 

l5*m 

ar» 

»6(> 

14  40 

VVt 

iraM    r 

% 

1176 

n->^ 

S94 

10  V. 

I»fi0 

l(t-l^ 

«I*CM 

lOM 

KM 

»tn 

tr«»»      1   ,| 

r. 

Havaniifth  leaf     - 

'4-:io 

aom 

4-ns 

irto 

*I'T« 

**•          1 

Ditto      IcHr-iUlk     - 

11-fiO 

SAM 

9-t« 

1»M 

irn« 

I*       1  • 

7 

GflfRiAn      Lear      - 

1 1*3  i 

)£«O0 

4  16 

17-W 

«-M 

MM         '  J 

Diiii      Irar^iwlk     • 

If>l6 

s3-n 

J-M 

I4« 

rrm 

a 

Tu-k^r     iMr    -      - 

n-96 

44M 

l-no 

10  7S 

i>7« 

><«          1    « 

Ditto       le«r-lUlk     - 

16-74 

94-BO 

11*08 

ie« 

n-» 

4»         iP 

to  Inse  weight ;  it  was  then  weig:bed.  The  Iims  sustained  iliDveJ  ift* 
qiianiitv  ot' soliiMu  matUtror  extraclive.  The  resulta  obtMBfd  ly 
Mr.  FblUips  were  as  follow  :  — 

Per-eentage  of  Extractive  and  Lisnteou*  Matter  in  differtwi  Kiadt  ^ 

Tobacco. 


nrglnlj^  Hand 

SMraettv^ 

MP-— 

M- 

w- 

M- 

«» 

StrlppeJ 

Si- 

4»- 

SeaVuckj,  fland              -              -              - 

ns- 

e 

w- 

«»- 

,                                                                             •                                 ■                                 a 

441 

»« 

Stripp«sl          ... 

4^« 

»r« 

>               >               - 

4fi-7 

«M 

MaryUnd.  Lear 

Wl 

m 

*              •             • 

4S1 

»r? 

Ponolliro       .... 

M^ 

Ml 

» 

W 

Columbian         .... 

M^ 

n» 

,•                   .... 

»S 

»^ 

VIrKlala.  SUlki 

K1-4 

•»» 

KrnliKkj.      ^                   .               .               - 

r-s 

«41 

DM                              -                       -                       . 

»« 

.»« 

Mr.  Phillips  ftiitefl,  thnt  he  has  ox  peri  men  ted  wirh  bctwoca  Bit  tfJ 
six  Ininrded  Hfimples  of  tohiiceo,  fjid  that  he  never  found  anir  to  ftn 
A  liiglifr  Amount  nf  fxtrnotive  ihnn  ftfty-fivi*  per  iw*nt. :  ftUotbifb 
fnuml  it  made  no  difference  whether  be  cxperimcnfcd  with  the  )x^9 
with  tbo  out  and  nuuiufitotarod  tobacco. 


TOBACCO,    AXD   ITS   ADULTEBATI0N8. 


587 


The  onlj  other  MnAlviies  of  tobacco  which  have  been  made,  and 
whicli  are  at  all  iiiluutulL'd  to  b«  of  stTvioe  in  iluluTinininj;  the  (jiiestion 
of  ihe  adulltimtioo  of  tobacco,  are  lite  following,  by  Mes&rs.  tirnnde 
and  Cooper,  made  in  1845,* 


iktalMtlV. 


t.  Llfhl  Mluourl, 

IfAf  ami  tUlk 
%  UrIiI  Mluourl, 

loaf ontf 
t.  Dark    Mliaourt. 

Icmt An*  tUIll 
4.  Dxrk   MUiouri. 

Ii**!*  onik 
ft.  I.litht  VlrfrlnlK, 

Ir^if  «nd  italk 
6.  Light  Virirlnia, 

li^rtl  unly 
T.  D»tk    Vintlnla, 

Ir-Mf  Hnri  rtMlk 
a.  Dark   Vltglula, 

leaf  onlf 


50- 

so- 
ul- 

Hi 

M- 

tt-a 


Pa  r«m.<    FtrCmi. 
./  W.-I7        af  All) 
F<  brr.      aftrr  trvailnp 
air.,  til.        «.Ui  <'«r- 
■  iliiblr  tn        Imnit*  at 

Wairr.     !  AmmratM. 


477 
At 

Al 
46 
&l« 

49-9 


1  vhito 

fl  If  7 

4  I  white 

*   I  while 

•fi   J  W* 

•I  fl  "** 

f  grrco-i 

[ 
I 


PnCmt.  PaCvnI. ' 
PfvCnil.  if  M«ita!t       tiTlD. 

t<f  ^lM(«T  K'^tibklM'  Mdubto 
•n'lililr  In     ffjtlnt-      Mai<«T,» 


uT-tlcolMri 


]  217 

]  1*77 

I  4-1 

]  117 


Si) 


hllei 


2-M 


ll-Tl 
IS-U 
IC-U 

fCM 

OM 
B-40 


S-9 

Si 
i-u 

9« 

ft-U 
Sll 
IS 
1-7 


Q-7a 


0-U 


1-M5 


]-4C 


Maimt 
htini  ih« 


IM 


o-ji 


391 


1.  The  samples  were  dried,  and  the  extract  and  woody  fibre  were  ulao 
dritrd  ut  t^ltS'^.  Tlii:>  watery  infu^iutis  of  all  contained  ammoniacal 
sattt.  The  flidlfl  fntiii  the  o^h,  which  were  soluble  in  wuler,  COD- 
flidted  of  .Hijl|ihiite!t,  ejirbonate&,  [>lio:<phatcft,  and  chlnritle<i,  the  bases 
beinj;  |)otJi!tAa  und  lime.  The  aoliiiion  by  hydrochhiric  acid  con- 
taiiieil  lime,  aluminn,  phoBphute  of  lime,  and  oxide  of  iron. 

3.  Contained  oxide  of  manganese  in  small  rjnantity.  Sulphates  in 
watery  (mlutiun  of  a^h  abundant.  liydrochlono  solution  contained 
an  abundunce  of  lime. 

4.  A  trace  of  manganese  ;  a  trace  only  of  phosphoric  acid  in  watery 
solution. 

6.  Container!  abundance  of  oxide  nf  manganese. 

6.  AbiiniUncc  nf  oxide  of  manganese. 

7.  A  mere  trace  of  oxide  of  maogancsc,  and  a  trace  of  oxide  of  iron  { 
only  a  trace  of  alumina. 

8.  A  irace  of  oxiile  of  manganese;  quantity  of  oxide  of  iron  very 
great ;  only  a  trace  of  alumina. 

Propertie9  of  Tobacco, 
III  smaii  do*e»  tobflwo  prodnces  a  wnsation  of  heat  in  the  throat, 
•nd  sometimes  a  fevlinir  of  wnrmlh  in  ihe  Rtomnch  ;  it  also  frcr)uently 
excites  nausea,  and  a  peculiar  sL'nsation  of  giddiness,  mure  allied  to 


•  flvaodt'i  MniuU  of  CtWBUtry,  p.  1033.,  Ii4a. 


TOmM€COt  A3n>   m  ADirLTKKATtOlSraL 


I      Bmt  tfce 


^^■£««e  cwea.  there 

^^^Bpcfi;  Ik  ossraMnc 
Mid  oftmmar  wiM—ii 

Tfce  ipffif  linn  of  inhMW  l» 
pnctioe.    A  cbk  faai  beea 


^  p«raljai  wd  a 


vUcfc  prvfedfttel  in  three 
ami  a  kaU^  IB  wkic^  iWcxDiwed  ran  had  iMca  appGed  Ibr  the 
i^adhiUcMt 


j^anoitffi. 


«f  nagwwM  lo  uie  feeaa  m  a  oMd  of^t  jtan  of  af«^ 

ToMooo  haa  aim  inatteaa^f  P*?**^  ^^"^  "^  *^  f<»m  of  m 
Dr.  Coplaad  mv  half  a  onchB  m  infiiwen  ptme  lataL 


The  operation  of  tobacM  R«ea»blca  ■am  ahii  that  of  L^fcefia 
iniUta,  both  bong  anodyiie  asd  iiifiwiaMiinitif..  In  it»  mf  chfin^ 
action  on  the  heart  it  agrees  whh  dijestat]i»  but  k  k  not  e<)aal  tft  As- 
glore  in  this  reipecc.  In  ia  power  of  canwag  rdaxatiaa  of  the 
Biucalar  tTftem  h  greatly  snrpaaee*  digiufit^  From  hrlliiViwna 
itramonium,  and  hjoacyamm.  it  is  diatingnaihcd  hj  caumn^  cootiae- 
tioa  of  ibe  pupil,  bcHh  when  applied  to  the  eye,  and  when  taken 
intemalljr  in  poisoiunu  dosn,  and  also  bj  the  a^^ence  of  ddirism 
and  of  any  affertJon  of  the  thruat.  From  ftconite  it  is  distnifiiahed 
by  not  prawwing  the  power  of  paraly^iag  the  sentient  nerrea. 

Ov   TBB   Al»tTI>TSBATI03V8  Or  ToBACCO. 

We  have  enumerateiS  the  different  species  frum  which  the 
rarietief  of  tobacco  are  obt^ned,  described  the  cultivition  of  th« 
bacco  plant  in  Virfcinia,  gi^en  the  minute  structure  of  the  lenre«,  th«irj 
rhemicat  composition  and  properties,  the  procetttrs  br  wlitcli  raw  or] 
unmanufactured  is  convened  inio  nunufactured  tobacco,  &0fl,  lastiy^] 
we  have  described  the  diflferent  varietied  of  cut  and  roll  inliaix-o ; 
these  particulars  were  necessury  in  order  that  ihe  subj(>ct  of  the  adnU 
leralion  of  tobacc<f  might  be  the  more  easily  and  fully  comprt bended. 

The  following  are  the  prineiiial  sub-lances  which  have  cither  been 
discovered,  or  have  been  fttaivu  on  g«tod  autliority  lo  have  !»««n  em- 
ployed, in  the  adulteration  of  tobacco,  principally  in  the  fiu-m  of  cut 
or  roll  tobacco.     They  may  l>e  diviileil  — 

Virst,  into  regetable  giibAtaReuM  not  titbacco^  as  the  leaves  of  the  dock, 
rhubarb,  coltsfoot,  cabbage,  potato,  chicory,  endive,  dm  and  ouk,  &!"..; 
moll  cummingtt — that  is,  the  roota  of  germinaung  mall ;  peat,  which 


\ 


TOBACCO,   AND   ITS  ADULTERATIONS. 


589 


oon»utfl  chiefly  of  decayed  moss;  seaweedt  roasted  chicory  root,  wheat, 
oatmeal,  bran,  cftteirhu  or  terra  jnponica,  oakum,  and  lo^o^ood  (]ye. 

Scrnndly,  into  tacrfiarine  subitancex^  as  cune  sugar,  treacle,  honey, 
liquorice,  beet  rodt  drops. 

Thirdir,  into  nalia  nnd  wrthi^  as  oUre,  common  saU>,  sal  ammoniac, 
or  h^'dnH'litorate  of  ammonia,  nitrate  of  ammonia,  carbonate  of  am- 
monia, ihu  alknliea,  nn  pntiisfa,  »odu,  and  lime  ;  tiutphate  of  mngnesin, 
sulpliiite  of  soda  or  glaubcr  »dts,  yellow  ochre,  umber,  fuUer^s  earth, 
Yenctiim  red,  sanit,  tiiilphnte  of  iron. 

The  following  has  bcfn  the  experience  of  the  Cxcise  in  regard  to 
the  adulleratioit  of  tubucco  ua  titaled  in  the  evidence  of  Mr.  George 
Phillips,  given  before  the  (^ommitlee  on  Adulteration:  — 

*'With  regard  to  lobacro,  we  have  found  in  cut  tobacco,  snf^ar, 
liauorice,  gum  catechu,  Bait,  8alt|ietre,  and  various  nitratea ;  yellow 
ocnre,  Epsom  salta.  glauber  saltn,  green  copperas,  red  sandstone, 
wheat,  oatmeal,  malt  combings,  chicory,  and  the  following  leayea: 
coltsfoot,  rhubarb,  chicory,  endive,  oak,  elm,  and  in  fancy  tobacco  I 
once  found  lavender  and  a  worl  called  niii<;iTort.  It  U  a  fragrant 
herb,  suggestive  rallier  of  the  nuliJie».  In  roll  tobacco  we  hare 
found  rhubarb  Inavfta,  endive  and  liocK  leaves,  sugar,  Hquorice,  and 
a  dve  maile  of  Ingwootl  ;ind  fulphalc  of  inm." 

l*he  adulterationH  of  tobacoo  most  fmjuently  practised  are  with 
waiert  sacchurine  matter^  as  trrade  and  mcar^  and  aoUji  of  Turious  kinds. 

Since  tobacco  cont.iina  all  these  substunoes,  and  since  their  umounc 
is  subject  to  considerable  Turialion,  it  is  only  when  they  are  present 
in  considerable  excess  that  we  are  enabled  to  stale  that  they  con- 
stitute adulleratiunft,  unless  indeed  the  original  leaf  tobacco  can  be 
procured  to  serve  as  a  slaridard  of  compariaon. 

Ileaultg  of  the  ExaminaHon  of  Ftfltf-nix  SampUt  of  Unmanufactured 
and  Manufactured  Tobacco. 

From  the  examination  ot£ight  samples  of  unmaRufacturfd  tobacco 
it  api>eareil  that — 

The  bvjrrometric  moisture  varied  from  11*25  to  22'96  per  cent. 

The  extract,  from  2a'20  to  51-20. 

The  »iolub!e  ash.  from  a-00  to  11*44. 

The  insoluble  ash,  from  i>  60  to  17  80. 

The  total  ash,  trom  13-60  to  27-90. 

The  sugar,  from  Iracea  to  A'iiX. 

From  that  of  Forly-eight  samples  of  manufactured  tobaccos  it  appeared 
that  — 

The  hygrometric  moisture  varied  from  9'80  to  6^*76. 

The  extract,  from  29  32  to  62  20. 

The  soluble  ash,  from  3'24  to  7-60. 

The  insoluble  ash,  from  9*20  to  16*J4. 

The  tolul  a»h.  from  U'OS  to  20*B0. 

The  sugar,  from  traces  lo  3*82. 


I 


• 


590 


TOBACCO,   AND   ITS   ADULTEEATIONS. 


That  in  the  BirtTs^Eye  Tohnccon  the  noluble  ash  wu  renr  ^jb.  ia 
conseijuence  of  the  large  qusntitj  of  mid-ribs  which  theie 

con  tain. 

That  the  extwct  from  the  Htf^roheadM  and  TiciUa  was  in 

unusiittlly  high,  n.i  was  also  the  quuntiry  <if  ^Iiic<»»e  ;  flieae  Uifc  et- 
tractii  were  probHbly,  in  part,  due  to  ibcoil  einplojred  in  the  mtn- 
fiiciurc  of  these  kinde  of  tohacai*  but  princijudly  to  the  um  of  noe 
saccharine  solution. 

That  in»t  one  of  the  Forty  SampU*  nf  munufauturvd  mt  tobaccp  »» 
adultvntted  with  any  Inreign  leaf,  or  with  nny  in^tlubte  or  nrpAic 
extraneous  substance  of  any  deNcrtption  other  than  with  ^ngv  or 
some  other  snocharine  matter,  which  was  present  in  sever*)  iusanoei. 
The  more  common  aduUemtions  of  tobaci?o  connist  in  the  adtiitjoa 
of  water,  su^'ur,  nnd  salts.  The  prejenoe  of  these,  in  uxoonni  luS- 
cient  lu  constitute  adulteratimi,  ran  only  be  < leclnreit  with  cm«mlt, 
however,  wht;n  they  are  in  ooii^iiicrable  exreaa,  <.>r  by  a  oompariwa 
of  the  unmanufacture<)  and  uianufuetured  leaf. 

These  results  are  very  diiVerent  from  tho«c  which  might  han  ben 
anticipated,  taking  into  considenitiim  the  notions  which  prevail  ,^nc- 
rally  aniongBt  the  public  with  re4p«-ct  to  the  adulteration  of  totncca 
and  also  the  high  duty  to  which  this  article  is  •ubj«<*t.  The  «Wnc« 
of  the  grosser  aiiulteralions  is  to  be  expluinefl,  we  apprcturnil,  by 
the  coriKinnt  i>upervisiim  exercised  over  the  manufacture  of  tubwc« 
on  the  pnrt  of  ihe  Excise. 

Although,  tiiking  a  limited  number  of  samples  of  tobaroo.  wt  ib 
not  find  iidullenition  to  he  by  any  meatis  so  common  as  wc  antieipiMt 
yet  we  must  nut  cotieluile  from  (his  th^t  t"bui-c«>  is  never  adoltexsiej 
with  foreign  leaves  and  other  solid  and  insoluble  substances  TV 
Kx<.'ise  returns  show  (hat  it  uccasionully  is  so,  (he  ortjvi^v  of  Cicii* 
making  from  time  to  :inie,  in  the  wttiehouses,  Stc^  of  tobacco  muM* 
faciurers.  seizures  of  iloek,  rhubarb,  col tMixjl,  and  other  leaTW^atni 
as  a  variety  of  other  vegetable  and  mineral  substances. 

On  the  Dttection  of  the  AihJtrratiotu  of  T^fhotm. 

Ttie  examination  of  a  sample  of  tobacco,  with  a  vinw  lo  dHTOAr 
whctluT  it  is  genuine  or  tiJuUerated,  is  of  two  kinds — thcoM  mttn 
seopiatlt  the  other  chemical. 

tAw\\  sample  must  be  examined  with  the  microscope  in  orJer  U 
ascertain  whether  any  f'>rei:;n  vegetiible  suhstaiicv  is  pr-'*--!)!      1' i* 
( ontnin  any  of  those  enumerateil  on  the  preceding  pi 
fine  a  stsle  of  |*ow([er,  and  evt-n  in  the  timnllest  quam 
be  deteoied  with  tht*  grentcst  c*Ttain(y  with  the  aid  of  \ 
since  they  all  present  [>eculiarities  of  structure  by  %\. 
be  readily  distinguished. 

Structure  of  ^ruven  of  Dttck. — Thus  the  structure  of  the  loiTwrf 
he  couimuD  dock  is  vtry  characteristic;  it  is  as  follows:— The  orib 


TOBACCO,   AMD  1X8  ADULTERATIONS. 


591 


the  Inniina  dn  not  tliffcr  mntcriallr  in  size  or  shape  from  those  of 
tubai'co  le»f,    nt'ithtT  do   ihc  ptomiila  pTescnl  uny  ^rcut   jjccu- 
rty  ;  like  thoM.*  of  tobarco,  ihey  ocour  on  bulh  Mirfaues  nf  ihc  leases, 
course  are  most  numerftus  on  iUa  uhdcr  siirfnce;  unlike  to- 
huwcver,  the  celluliir  part  of  the  kmina  is  wholly  deatitute  of 
Fig.  190. 

Fig.  190. 
Ttibnoii  or  UmvUm  BumrAca  or  m  lkav  or  tbs  Dock. 


thte«Il««B4«4offl>U.MBlK>lK«Junetion  of  thcMllulu  ptrt  of  (lie  Ittf 
vlUt  OH  of  tbc  ••TfttUr  r«liu.     MA^fniScd  23)  dJunrUr*. 


Tbe  alructure  of  the  mid  rib  and  veins  is  very  diflbrent  from  that 

"  Cob«eT(> ;  they  differ  in  ^hllpe,  in  the  form  and  nature  of  the  »pine« 

bAirt^  nhiih  arise  from  tlieui,  and  in  the  arranj,remt>nt  of  the  ve^^sels 

ro«M]y  fibre.      Transverse  Becti(ms  of  the  mid-rib  are  of  a  «ome- 

rltat  trtan^ulur  forui,  the  bii»e  of  the  triangle  bein^  smaller  than  the 

lido;  one  of  these,  viewed  with  uu  inch  object  glasa,  presents  mx 


voBAOOo.  jun>  rrs  adci^tkbai 


in  thoec  offlfnull  and  niLHlium  Mm  there  ore  usuallj  six  oret»ht  ftwd* 
euli.     fw-  HH. 

The  cclU  forming  the  riilgei  are  rery  characVeristic,  bcinj;  onaD 


TOBACCO,  AND   ITS   ADULTERATIONS. 


593 


Wm\  lingular;  those  coinpOMiif;  ibc  intemal  part  of  the  mid-riU,  ami 
'hicli  nre  truvcraed  by  llie  vascular  and  woody  tissue,  are  Inrger  and 
"tniirf  reticular. 

'I'he  above  structural  neiruliarities  are  clearly  shown  in  jfipi.  192, 


Ftg.  iw. 

PoKtiov  or  TiuvftTiux  Skctiok  or  Nficwnn  or  1.ur  or  Votx. 
(MasnlAnl  Wi  iliHDClvt.) 


=-.«»« 


Struftttre  of  Ltof  of  Rhubarb. 

The  structure  of  the  d*tck  leaf  being  m>  very  distinct,  we  will  now 
nhow  that  the  organiaation  of  the  rbubftrb  leaf  is  equally  charac- 
teristic. 

In  the  Dtrtmata,  and  in  the  form  and  size  of  the  cells  of  tiie  rhubarb 
leaf,  slight  differences  only  are  observable;  but  the  walls  of  the  celU 
nre  finely  striated,  a*  shown  in  the  wood-engraving;  nnd  thi^  is  a 
rharuoter  by  which  rhtibarb  leaf  may  bo  at  once  known  from  tobacco. 
Other  diffcrenres  arc  founil  in  ihe  characters  of  the  short  spines  or 
hriirs  which  chttbc  the  leaf,  in  the  form  of  the  tnid-rib  and  veins,  and 

•4  u 


394 


TOBACCOj  AND   ITS   ADULTKRATIOXS. 


in  the  presence  of  gland-like  bodies  scattered  tbroughimt  tk  faoin 
le 


of  the  leaf. 


LoaarrrmaAL  Smnm*  or  Mip*u>  or  Lcat  ov  Doc*. 
(M^nUad  H  dlumton-l 


The  bairfl  or  spines  are  sbnrt,  Oiick,  hollow,  stnato^l,  and 
in  obtuse,  rounded  extremities.  They  rusi'Dilile  closclv  in  fona  di 
of  ihe  dock,  but  diflbr  in  being  several  Times  larger;  io  thecbnMI 
and  fineness  of  the  striw  with  which  the/  sre  taaric«d»  and  b^  ifti 


d 


T0BA.CCOnfNI^ 


»ULTKRATION8. 


dislributiitn ;  for  while  in  !be  tltK*k  the  spines  spring  only  from  the 
mid  rib  und  vuiiw,  ill  thu  rhuburh  k'lit' thuj  nrisc  from  ull  parts  uf 
tliL*  leal^  I  be  lauiiua  as  well  as  the  mid-rib  and  veioa. 

Fig.  IM. 
FuBTiajr  09  Vitimm  ficsrACB  or  RnukAJU  I.tjir, 


.Jk 


f<7^^ 


tmoviuii 


luDiJ'JlLr  UpI 


'hiKt  (rliir*  or  hftln,  »Bd  lUe  OM  of 


The  mid-rib  and  vein<4,  iifl  in  dock,  consist  on  the  outaidv  of  imall, 
fni^ulur  rell?,  pucuccili^d  by  larj;©,  reticular  cells,  whirh  are  traver»e<l 
by  bundle*  of  wimmIv  fibre  luid  spiral  vesstrls  ;  ibe  differenci's  bctwe<.'n 
the  mid  ribt  of  tlie  leaves  of  the  two  plants  being  in  form,  nnd  in  th« 
nbwnce  of  distinct  ridges  on  the  mid-rib  of  ilie  rlmbnrb  leaf. 
Fig.  194. 


Strtieture  of  the  Lenf  of  Cttlttfwti. 
We  now  proceed  to  duK*ribe  ihe  minutu  organisation  of  ihv  Colts- 


596 


TOBACCO,   AND   ITS   ADULTERATIONS. 


foot  or  Tusstlnge  leaf,  which  hu  b««n  stalvtl  to  hn\e 
empltived  in  tlie  adulteration  of  tobacco. 


Fig,  19\ 

TBA.TflTXtM  6SCTID5  or  MiD-Bi«  or  lllir»4t>  t^At. 

(MiffnlBcd  40  itlUMKis.) 


The  i'plls  wbieh  form  the  upper  surfuce  of  the  leaf  of  eoteAii  I 

of  Miinll  Pize.  nrpular,  and  ttiintiv  striRfeO  :  there  are  bot  a  ^»  ^ 
inutHf  ami  no  buir.s  except  on  tlit^  mid-rib?  and  principal  tvid*-  i 
196. 

Tlie  structure  of  the  under  surfnce  of  the  leaf  differs  (-niin^T  fr 
that  of  the  upper.  The  cells  are  also  nf  smnll  size,  but  theimnrf 
are  waved,  ond  the  wtilN  are  not  striated  ;  the  stomata  are  f!Stm 
injjly  numeroiiR.  and  the  whole  of  thi*  surfnr.'c  is  clnihed  with  d*tin 
filamentous  hairs,  which  impart  the  downv  character  to  the  hi 
intemiixed  with  these  nre  other  hairs  of  much  latyer  siiOk  and  "h* 
beinfT  jointed^  bear  some  r«temblance  to  tho«e  of  tobarcOf  but  ll 
want  the  distinct  glandular  terminations.     J^tf^.  197- 

TransTer»e  aectiona  of  the  Ieaf-!>(a1k  present   tlu-  ,    fOti 

turc  ; — Externally,  there  i*  a  w«'II-defintfd  border  ci  j»|J 

cells ;  Irom  the  outcide  of  these  spring  the  two  kinds  ut  U*u#  dcfCW 
above.     The  central  portion  of  toe  section  is  made  up  of  looff  ttM 


TOBACCO,  AND    ITS    ADLLTEKATIONS. 


S97 


liMue  siiniliir  to  that  of  the  tni'Uribs  of  inaii^  other  leaves,  aiid  it  u 
traversed  bjr  from  about  »&  to  etj^Lt  bundles  of  wood/  and  vucuUr 

Fig.  196. 

Foitiujf  or  UrrcR  SuxrACN  or  Lsav  or  CotXirooj. 

(UagaUM  290  dlAimlcn.) 


iUmi?,  Ibe  number  usually  vnrying  with  the  niie.  The  large  ^m/- 
xitiikx  of  the  *■ll[r^^l)ot  woitUi  hardly,  however,  be  used  in  any  case  (or 
the  ttdulterAfion  nf  cut  tnbnccn. 

S*rction8  of  tlie  vein*  prKsunt  a  nearly  8unil.ir  conformfltion;  the 
principal  difference  is  in  the  numlfcr  i>l'  tlic  bundles  which  traverse 
iheui,  there  bein^  almof^t  invariably  but  three  such  bundle?.  Hy  thift 
obaructer  the  veins  of  the  leaf  of  eoUsfuot  are  at  once  di.^tinguished 
from  those  of  the  otlier  leaves  we  have  deaeribeil.     J^if^,  19iJ, 

Differenec*  eiiually  marked  ehiirjctorise  the  other  ve-^eUble  sub- 
ctaiuieji  which  have  been  actunlly  detected  en»ennji  into  the  iiiulterA- 
lion  of  titbacco.  Descriptions  tind  rc|>rt'))ontatioiis  of  ihe  uiajurily  of 
these  will  1)e  j^ivcn  at  some  future  periiMl. 

We  will  now  proceed  to  describe  the  pr<H?cs5efl  to  be  pursued  in 
the  chemical  examination  or  analysis  of  tobacco. 

The  pariieulnrs  to  be  ascertained  ore  the  jwr  centa^e  of  water,  of 
extractive,  of  sugar,  of  ash,  together  with,  to  some  extent,  it§  com- 
position. 

4Q3 


698 


TOBACCO,    AND    ITS   ADVLTERATIONS. 


One  buntlre45  grains  of  each  of  the  tobaccos  are  to  be  tmtcd  u 
follows:  —  They  are  to  be  dried  lor  twenty-tour  hours  in   a  walcr- 

Pi£.  197. 
FoRTiu.t  or  U.<<i>KM  StiiwACi  or  Iaxw  op  COLTtrvOTa 


SbowiDf  Ihc  numerotu  ttMnnlft.  u  slm  Ibe  two  kindi  arhkin  vlUi  vUch  Ihi* 
•urfuieof  tiM  kkf  UlnveitMl. 

bath,  and  then  re*wei(fhcd ;  the  loss  shows  the  amount  of  A^,^ome/n> 
moutture  which  the  samples  contiiiiicd. 

They  arc  then  to  be  iniicerared  fur  twenty-four  houpa  in  cold,  dis- 
tilled water,  by  which  means  the  extractive  is  obtained.  They  ar« 
next  boiled  fur  an  hour.  The  rcaiiliie  is  lifiiientm  vuttier^  yielding 
from  three  to  ten  f>er  cent,  of  ttsh,  rompnse*!  chiefly  nf  silica,  wiln 
earthy  earhnnales  nnd  phnsphntes.  7'lie  table  mnrked  A,  p.  585.,  re- 
preseiiti)  the  results  obtained  from  the  genuine  tobacco  leaf  by  the 
above  prreesses. 

One  hundred  grains  nf  each  tobacco  are  next  to  be  stibmilte<1  (ac» 
cording  to  the  process  of  M.  Scliloesiiip;)  to  tlic  action  of  ummoniaietl 
ether;  the  eiher  distilled  olT,  and  the  residue  neutralised  with  di]uc*s 
sulphuric  acid  of  known  saturating  power;  by  this  means  the  propor- 
lions  of  nicotine^  chloropkyhy  and  ftU  arc   delermine<l.     I'he  table 


TOBACCO,  AXD  ITS  ADULTKRATIONS. 


599 


taiarked  B,  p.  386..  represents  the  results  obuincd  by  this  process.  In 
ordinarj  ca»es  this  [Mkit  u(  the  analysis  may  be  omiiied. 

T«iMTt««  8w.Tio.t  or  ojri  or  tb»  Vmm  or  t.t*r  or  CoLrwoor* 

(MAgfillM  W  dUtDCien.) 


The  extractive  oblnined  by  the  first  operation  is  lo  be  treated  as 
foltom  : — 

It  is  lo  be  ilissoK'Cfl  in  illstilled  water,  and  ihe  nnbitinn  treated 
with  hftsic  nretattf  of  lead  and  fiUorcd.  The  filt<?rcd  liquid  and  the 
pret'ipirale  dcHHtmposed  by  sulphureitod  hrilro^jen,  and  evajwraled 
to  drynosH,  one  is  treated  with  a  mo'iificati'in  of  Trommer's  nr  the 
cnppt>r  lest  f)r!in^iir«  and  the  nther  with  <lilute  alcolirt]  for  malir  nod 
nnd  ;;uin.  'lliu  Utble  inark^^d  C.  represents  the  results  oblnined  by 
the  above  process. 

if  it  bo  suKpected  that  cane  ragar  is  present-,  instead  of  adnntin^ 
Fehlin^*!<  process  wo  mn.it  employ  the  fL-rinentation  test,  and  estimate 
eiiher  the  quantity  of  carbonic  acid  srna  evolved,  or  the  amount  of 
nlcnhol  penrrafcd ;  indeed  it  saves  time  to  cmp'oy  the  fermentatiou 
test  in  nearly  all  rase*  for  the  deterrninntion  nf  the  presence  of  sac- 
(•h;irine  matter,  whether  in  the  fumi  of  glucose  or  cane-Hiignr 

The  fertnentalinn  te!»t  la  used  in  the  fffllowing  manner: —  lOOOj^ini 
of  tobacco  are  to  Iw  placed  in  a  vessel,  and  a  pint  or  so  of  water,  at  a 
temperature  of  about  100°  Fahr.,  poured  ufwm  it :  the  infusion  is  then 
to  be  strained,  and  *250  ^oins  of  dried  yeast  added ;  the  mixture  is 
next  lo  be  set  aside  for  forty-eight  hours  to  fermenl,  at  a  temperature 

gQ4 


600 


TOBACCO,   AND   ITS  ADULTEKATIOXSu 


of  nboiit  60°  ;  lastlvi  the  liquor  must  be  introHucei]   into 
nU'ijljiil  iJt!<tilled  ovtfr,  aiul  lU  amount  efttimiUed^  or  the  (*arlM>ntc 
taay  hii  cuIluL'ted,  tuul  the  ainouia  of  siigur  calculated  tiiererniitu 

The  inathoi]  of  cftleulatinig  the  ttu^ar  frniii  the  amount  of  carhnnic 
aci'1  formed  (iurin<r  f'f-*riii«'iitntion,  will  hefouud  detuilcii  ut  some  length 
in  Bowiiiian's  "  ML-dicul  Cliemistry,"  p.  93. 

For  (Lo  detoriTiiiKitixn  of  ibo  salts  contained  in  tobacco  one  ortvo 
hundred  grains slioulil  Im  incinerated,  and  the  ash  te«te<l  for  the  rh\*i 
lu'ids  lind  bases  —  the  sutpfauric  acid,  chlorine,  lime,  soda.     It  is  well  ^• 
disjiolve  nut  the  soluble  from  the  insoluble  portion  of  the  msh,aQd 
test  these  separately. 

Hydroohlornle  of  nmmonia  and  the  nitrates  must  be  aoupht  far 

cold  tnfuKian  nf  tobacco,  iiit  the  fir^t  is  t*ntire]y  dissipated  on  iuclnei 
tion  oftlie  ash,  and  the  latter  are  dccompfised 

The  presence  nf  tin  ummuniflcal  salt  is  suQicicntly  indieati^i  on  tl 
addition  of  u  little  caustic  putash  to  the  tolutiun,  th«  amjuouia  beii 
evolved. 

The  following  process  may  be  pursued  for  the  detection  of 
nitrates. 

One  of  the  best  methods  of  detecting  the  presence  of  nitrates  is 
a<ld  to  a  concentnttcd  infusion  of  the  at^tietms  extract  a  fcir  drops 
sulphurii!  acid,  and  then  n  crystal  of  sulphate  of  protoxide  of  iron:  ft"! 
dark  brown  discoloration  immediatclv  occurs  around  the  cryuaU  if 

any  nitrate  be  preaoni.    This  generally  disap|>earB  ufwn  simple  agiu- 

tion  of  the  tluiu,  and  invariably  upon  tho  application  of  heaU  ^M 

For  the  quantitiitive  eslinmtion  of  nitric  acid  consult   Freseiiiui^H 
"  Quantiutivti  Analvsis,"  p.  274. 

The  proce3<(e4  for  tlie  detection  of  iron,  silica,  or  san<l,  and  chrontite 
of  lead  hiive  already  licen  de:*<-nbcil;  that  for  the  latter  substance 
under  [he  hc^mi  of  Coloured  Sujfur  Confectionery. 

The  amount  of  ex'racC  obtained  from  any  tobacco  vtiries  somcwbi 
even  in  dilK'ient  portions  of  the  same  leaf  treated  in  prei'isely  tl 
e^iue  manner,  buL  when  difierent  methods  of  cjctractiou  aix'  fidlowt 
the  results  ilitKr  stilt  more  considerably  ;  the  ipiantity  of  diatillct 
water  use<l,  the  temperature  to  which  it  is  raised,  and  the  length 
time  diirin;;  which  tlie  infusion  is  kefii  hot  and  niacerntion  allowed  u 
continue,  will  iiHcct  the  results;  when  therefore  wc  arc  deiiirous  ol 
oblniriing  comparative  results,  the  same  method  of  extraction  should 
in  all  cases  be  carefully  pursued. 

With  regard  to  the  method  of  proceedinjr  for  the  detection  of  grape 
sugar  or  glucose  in  tolutirco,  we  would  remark  that  we  tiud  it  neces* 
t»ary  to  add  a  conaideriiblc  excess  of  Fehling'tt  test  liquor,  in  order  t( 
precipitate  all  the  su<.'Hr,  and  hence  the  tpiuntily  of  glucose  present 
tannot  be  accurately  determuicd  by  the  amount  of  t<.*st  Hquur  used.^ 
One  of  the  best  modes  of  proceeding  for  the  quantitative  deterniiua* 
tion  of  glucose  is  as  follows  :  — 

Take  u  solution  of  the  extract  of  100  grains  of  tobacco  and  strain  it 


1 


CIGARS   ANU   3IIKIU   ADULTBRATI0N6. 


601 


through  miittlin ;  precipitate  with  a  slight  excesx  nf  basic  ncvtale  of 
leatl,  anil  tilt«r  ;  pass  Dulphuretli'd  bvdrofivn  tlinmyU  iIil*  tilteicil 
liquid  re-fiUer,  and  evaporate  neariy  to  d^ynL'^s  ;  di^s^lve  the  residue 
in  about  one  ounco  of  liquor  potniMie,  dilute  with  one  ounce  of  di:ii- 
tilled  water,  and  filter  aj>ain  to  remove  the  salts  of  lime;  then  add 
half  an  ouneu  of  Kehlin{;'s  jolucion  ;  put  the  mixtnre  into  a  lar^e  test 
tube  or  Hatik,  boil  for  a  few  minutes,  ami  observe  wlit^ther  any  yellow 
streaks  of  reduced  oxide  of  copper  make  llieir  iippt-aranoe.  i>K'"dd 
that  be  the  euse,  set  the  boluliou  aside  at  ^e^t  for  two  bour«,  nnd  col- 
lect the  precipitate  i  wei^fa  and  calculate  the  quantity  of  ^tuco^e  to 
which  ii  IS  eiiuivtdent.  One  grain  of  the  reil  oxide  of  copper  is  nearly 
equal  to  half  a  grain  of  jyrape  eujfur  or  glucose. 

The  following  is  a  more  simple  method,  tind  in  the  case  of  tobacco 
affirds  regulta  which  pre  for  the  most  part  sufficiently  arcurate.  Take 
1000  grains  a  of  solution  of  tobacco,  containing  two  grains  ul'  the  dried 
extract  Ut  tme  ounce  of  water;  adil  fuur  drachms  of  lii|Uor  ]kiU8s»  ; 
boil,  fdter,  nnd  then  add  about  400  grain»of  Fehlin;!'!<  teifl!  liquid,  and 
best  to  boiling ;  if  any  gluc<»se  be  prt- «ciit,  the  red  oxide  of  copper 
will  be  thrown  down  ;  collect  and  ihomu^hly  wa.di  the  precipitate  In 
onler  to  iTee  it  from  an^  albumen  that  may  l>e  present;  weigh  and 
calculate  aa  belbre. 


n 


CIGAR8.  AND  THEIR  ADCLTERATIOK& 

The  second  form  in  which  manufacturcil  tobacco  is  consumed  is  that 
in  which  the  leavoa  are  rolled  up  into  eigart<  and  cheroots.  The  use  of 
tobacco  in  this  fonn  has  bet^n  nipidly  advancing  within  the  lu5t  few 
yeartf,  the  cheaper  penny  cigars  taking  ihe  place,  to  a  gre»t  extent, 
of  cut  tobacco,  although  the  consumption  of  both^  from  the  growing 
ta»tc  of  the  ])ublie  for  tubacco-suiuking,  hu»  beun  fur  itome  tiuie,  and 
still  is,  on  the  increase. 

The  process  employed  for  making  cigars  and  cheroots  in  EnglantI 
is  precisely  the  same  as  that  adopted  in  other  countries.  It  in  m 
follows :  — 

The  leaves  are  first  slightly  moistened  with  water;  they  are  then 
"stripped,*'  that  is,  the  mid-ribe  are  rcmoveil  in  the  same  manner 
aa  described  in  the  description  of  the  ro^iufacture  of  Cut  Tohacco, 
by  which  means  ench  leaf  is  separated  int^i  two  parts  ;  the  hnlf-leaves 
are  next  smoothed  out  by  the  hand,  and  put  under  a  slight  nrea- 
sure,  to  remove  any  creases  which  may  havi?  occurred  in  the  parking. 
This  firat  process  is  generally  the  work  of  n  woman  or  Ixiy,  who, 
frcateil  near  the  eigar-imiker,  hands  up  the  half-leaves  as  fast  as  they 
are  reipiired. 

The  "cigar-maker"  is  seated  in  ftvmt  of  a  stout  wcodcn  bench, 
mode   somewhat  like  a  butler's  tray,  it  being  furnished  with  raised 


604 


CIGAnS,   AND  THEIR   ADULTERATIOK8. 


edges  on  three  of  its  niilefl,  but  open  on  that  next  tlie  wnrknun. 
lakvs  nne  of  the  hftlf-lcttves,  and  by  means  of  a  very  K>i.irp  knife 
it  intft  ihe  rnrm  of  a  seolion  of  the  riiul  nf  an  orange  ;  upon 
sufficient  qimniity  of  frainnents  anil  cuttiiig5  of  leaf  are  pli 
the  *^  maker*'  proceeds  to  roll  them  up,  and  fashion  them  into  I 
known  furni  of  u  ci^iir  or  cheroot;  over  this,  ug-ain,  n  lonj* 
(trip  of  tobuccu  leaf,  nf  rather  a  better  quality  and  app« 
tunned  the  **  wrapper,*'  U  spirally  rolled;  this  is  twisted  at  ihie  andsl 
end  into  a  kind  of  knot,  to  prevent  iU  becoming  loosened.  The  v^ 
ia  next  pliici'd  asainitt  a  ;;nuge  made  of  iron,  and  cut  from  its  tfai^ 
end  to  the  required  length.  Or(*nt  dexterity  is  requisite  in  iW 
mnking  of  ci^'am,  and  tlie  work  prui^eecU  with  the  titnjost  rapiiliti.fc 
few  sucouda  only  bfinjr  employed  in  the  nianufaeturo  of  each.  Afta 
the  eij»ar8  are  rein«ve<i  from  thy  maker:*'  hands,  they  are  (da£cd  -• 
open  tray 8  in  u  rooiu  urtificially  healed,  in  order  to  thortm;*bly  dry 
thorn  :  they  are  then  wei;:hed,  antl  packed  iu  boxes  of  varioiti  fii0 
for  sale. 

rii;arA  nnd  cheroots  are  known  in  the  trade  by  a  variety  of  differeal ' 
nntncfi,  taken  either  from  the  name  of  the  country  from  wbence  thet 
are  imported,  or  the  kinds  of  leaf  from  which  tlicy  are  niadt-,  whil^  ia 
iiihcr  eiises  the  name  of  the  maker  or  the  rnprice  of  the  inanufiuclurer 
determines  the  name.  Thus  we  have  Ilavannah,  St.  Lueia,  CuIh, 
and  Dneh  Clears,  and  Chinsurn  and  Manilla  Cheroots  ;  Columbia  aiu! 
Amenjf*M»rt  Cijrun*;  Cabana,  Silva,  and  Lo[>ez  Ci^^ars,  and  the  innu- 
merable fancifid  names  that  have  at  raiiouri  times  been  ^vcn  themi 
as  I'rineipef,  Fraguncia;',  Panetcllas  Kings,  Quoimis,  Imperials,  and  a] 
host  of  other  name»,  the  only  distinirui.ihing  rharacters  bein*;  tbi 
(^ize,  colour,  make,  and  form.  The  above  names  all  relate  to  furcij 
cigars  and  cherootJi. 

British  ciirars  and  cheroot?  are  most  frequently  made   in   imitatic^l^ 
of  the  most  lanious  and  saleable  varieties  of  the  above,  and  take  thcil 
names  from  them.     It  should  be  mentioned,  however^  that  neurW 
thecif^ars  i^ild  as  Cuban  are  of  British  manufacture.     Vast    number 
aUo  of  cheroots  peculiar  to  the  Kn;:lish  markets  are   tnanufaetm 
here;  one  sort  ii  termed  "  Bengal,*'  and  are  sold  usually  at    l^c/. 
2d, ;  the  uther,  "  Pickwicks,**  the  price  of  which  is  Id.  each. 

On    THE    AnWl.TBBATION»   or    CiG&BS. 

Although  it  is  commtudy  Iwlieved  and  stated  that  cigars  are  vi 
penerally  adulterated,  and  that  they  often  cmisist  of  anything  rather 
ihua  tobacco,  we  do  no'  find  any  precise  observations  recorded  re- 
tj>ecling  the  adulterations  alleged  to  be  practised. 


HesulU  of  the  Examhfotum  of  Sampiet. 

Oni  of  Fifti/ -eight  samples  of  cipars  and  cheroots 
amination,  three  onhj  were  found  to  he  uduUerated.. 


■  J 

subjected  ttfl^H 

J19 


C1GAR9,    AND   THEIR   AtlDLTEHATlONS. 


603 


One  of  thtstt  wm  piirchflfie<1  of  a  hawker  in  AVhiteolinpel  Koa*l ; 

le  cheroots  were  made  up  of  twisU'd  wmppera  or  Invera  of  ibin 

a/>fr,  tiiin.'d  of  k  bislre  oolour,  while  the  interior  consij-ted  entirely 

'A//J7.  not  a  pwticle  of  tobacco  entering  into  their  coinpodilioii. 

AnothtT  was  procureil  at  a  review  in  Hvdc  Turk;  the  cigars  ron- 
lisled  externully  of  tohneco  lertf,  but  interniilly  they  were  made  of  hiiy. 

The  third  sample  cone^istteil  ot*  penny  cigar**,  and  contained  inter- 

lly  apt>tf  paringt  and  other  rubbish. 

It  ap(M»nr8  thiir  about  the  neijfhboiirhorHl  of  VVhilechnpel,  the  sn!e 
»f  spurious  cberfmttt  const!tut4-(t  a  regular  bnsim*i»s.  Men  dressed  as 
liloni  Aod  appearing  as  thou;!h  they  had  junt  returned  from  n  lon^ 
anoonstantty  ua  the  Innk  our  lor  youii;;  ^entlentun  who  are 
supposed  (o  have  a  liitle  inuuvy  in  iheir  jiockcts,  :uid  lo  be  suuicwhiit 
inexperieuetf'l ;  to  suuli  thene  leHows  addrojis  the  in<iulry  in  a  myste- 
rious mnnner,  ns  though  thev  fvnred  beiiiji  overheard  by  the  polic-e  — 
"Do  you  wont  to  buy  a  box  of  real  Manillas?  I  hnve  pot  a  ffw 
boxes  'on  ihr  crotn;*  just  crjme  with  me  down  this  pa^$a;;e,  and  I 
will  show  you  them  ami  lot  you  (iisic  ihoin,"  at  the  i-aiivc  time  blinding 
out  a  fremiine  Mnnilla  cheroot,  as  if  taken  frnui  the  box.  for  the 
young  f(entlcmnn  to  try.  who,  bein;;  sntiplied  with  the  ^u.ility  and 
flavour,  close*  the  b»r<j:iin,  mid  walks  nff  home  with  a  hvx  of  bmwn 
paper  and  hay  undt*r  his  urni,  con^atulatinghim&clfon  bif  puichn*e, 
and  unticipating  tlie  pleasure  in  store  fur  him  from  smokinj;  his  ac- 
cpiisition  ! 

Twelve  sampler  of  Manilla  cheroots  were  te8te<l  for  OptrM,  but  that 
narrotic  was  not  detected  in  a  single  instance. 

7'Ae  atlulferation  of  ciffara  tnaiil  frtquenlly  practined  is  to  alcrp  the 
leamt  in  txirious  saccharine  and  taUne  infnsioiu  whereby  their  weight  it 
j^rrtUltf  iiiereaxefl. 

It  ihus  appears  that  cigars  and  cfaeroota  arc  subject  to  but  little 
adulteration  ;  the  cheap  fienny  ones  even  consisting,  in  the  majority  of 
cases,  entirely  of  tobacco,  though  there  is  no  doubt  but  iliat  it  i-4 
tobacco  of  very  inferior  quality.  This  is  again  quite  contrary  to  what 
might  have  been  anticipated  from  the  general  belief  entertained ;  and 
it  li  no  doubt  due  muiniy  to  the  great  difiicultT  of  6nding,  or  using, 
any  article  that  couid  be  substituted  for  the  tobacco  Kaf, 

In  t-onsequunce  of  the  high  duty  of  9ji.  (yd.  per  pound,  cigars,  like 
tobacco,  are  often  smugfjled  into  this  country,  as  is  shown  by  the 
evidence  of  several  witnf»s«^s  who  were  examined  before  the  Select 
Commttteeof  the  House  of  Commons  on  the  Tobacco  Trade,  in  August, 
1844. 

Another  very  common  practice  is  to  sell  Britisb'madc  cignrs  and 
cheroots  as  foreign  one?  ;  this  deception  is  carri'.'d  into  ciTect  by 
makings  brandinjr,  and  labelling  boxes  in  exart  imitation  of  tfae  difTe- 
rent  foreign  boxes  in  which  cigars  are  imjMirted.  This  pracllce  pre- 
vaiU  extensively  with  English-made  liavannah  cigars   and   Mauilla 


f1tJ4 


CI6AR8,    AND   THEIR    ADULTERATlOXi. 


rheroots;  altfaou|fh  in  tlie  case  or  MjniilU  cbernou  the  (r«oduci«lr 
ilotecteil,  since  it  is  scarcely  jioiisible  to  imitate  tbeK  chewto  •«• 
closely  as  not  to  allow  of  tbe  Jiscrimination  between  the  Briliifc  tui 
furei;.ni-tniMl(t  article.  So  gen^rallr  ia  thi»  fu-artised,  that  tirotaU? 
uot  cue  third  of  the  ci^arft  sold  in  boxes  arc  what  tbej  pruwtfWlit 
—  iiauielr,  forei<;n-iuade  cigura. 

There  is  n  kind  of  cheroot  called  Chingurah ;  (bis  w*»  canncal; 
sold  in  ih«  shops  for  some  years,  alihousb  it  was  known  that  Uittw 
or  thrt'e  eimes  had  Wun  entered  at  the  Custom  llou»e^  nod  paUdait, 
diinn^  (he  whole  tlnie.  In  one  year  alone,  twenty  thouwinU  jiott»k 
wci;»ht  of  tht'se  olieroois  found  their  way  into  tlie  ntarkct,  in  aiMilMi 
to  JVoiu  ei^'hteen  thousand  to  twenty  thuusuud  pounds  of  Maailii 
cheroots,  witboiil  havin<;  paid  duty. 

The  iiheroutM  known  as  Brugal,  notwithstanding  their  Eaal  ImbB) 
name,  are  till  British-made,  havinjr  originally  been  prepared  in  noiU' 
tion  of  Chtnsuruh  eheroi»ts.     Thus  we  see,  what  with  smu^linf  tad 

the  passing  off  inferior  Knglish-inadp  eigare  as  foreign.   ^  ■    ■'■  :!»• 

tion  of  the  fonn,  manufuclure,  branding,  and  lal»ellii>;;  •■  ^^''- 

tfaere  still  remains  a  wide  sco[ie  for  fraud  and  adult',  i^^ 'M 

articles  of  ci-'ars  and  clieroots. 


Oh  the  Detections  of  ike  Adult^rahotu  of  Cigan, 

The  cigars  and  cherootA  are  to  be  examined  in  tbe  fuUov^a; 
manner:  —  Very  thin  trnnaverse  vectiont  are  to  be  made  frow  J'- 
ferent  parts  of  the  whole  cigar,  so  ae  to  include  all  its  contrati. 
tfaei^e  are  to  he  aRerwanis  examined  under  the  micn*<«.'i»|>v  with  an  c^' 
ject-glfltfs  of  one  inch  focus,  and  the  second  eye-piree  ;  ea*.-h  rijftr  a 
then  unrolled  carefully,  and  every  leaf  or  fragment  of  lejif  Mlsosubjeclvd 
to  micrr)M'Opic  examination.  In  this  way  but  little  difficulty  b  »• 
perieneed  in  determining  whether  tbe  ciiiar  eon^ists  of  tobaca* " 
not,  the  structure  of  the  leaf,  and  especially  of  tbe  giaoduiar  )ua% 
being  80  peculiar  as  to  allow  of  ready  identitication. 

In  addition  to  microscopic  examination,  tbe  cigars  ^brndd  be  o* 
amiiied  chemically  for  »ugar,  and  the  ash  fur  extruneiitu  aaltoe  sal** 
stance  ;  while  Manilla  cheroots,  which  are  commnnly  rvpnrted  ^ 
contain  opium,  are  to  be  su1ijecle<l  to  analysis  with  ft  Tiew  Ifttir 
discovery  of  the  presence  of  that  dnijp. 

The  pmces?  to  be  adopted  for  the  dcleolion  of  opium  is  as  follows  • 

Four  cheroots  from  each  sample  are  to  be  cut  up  and  infawd  i^ 
twelve  hours  in  about  ten  ounces  of  cold  water,  slightly  adififia^ 
by  the  addition  of  a  few  ilrops  of  acetic  acid.  The  tii^uid  is  iWs 
filtered  off,  and  partially  pro.'ipitated  with  basic  acetate  of  IrtA 
by  which  means  i*  considerable  proportion  of  c^diturioc  mailtf  a 
thrown  down.  The  solution  is  next  refilterfd,  treatc<l  with  tbw 
drachma  of  animal  charcoal,  and  allowed  to  digest  for  tweidy-M? 
bourS}  frequcDlly  ftgitating  it;  bj  this  meani 


oigesi  i«r  iweitiy-ww- 
it  beoOMM /tmbcr  i^ 


J 


BNUFF,   AXD   ITS   ADULTERATIONS.  606 

ilorisci],  and  Jnsesit-"  hitter  taste.  The  charcoal  is  then  collected  on 
^a  filter,  and  boiled  with  two  portions  oC  rectified  8[nnt«  each  ot* about 
the  fame  bulk  as  (he  b't)uid  originally  employed.  The  spirit,  which 
ho*  Required  a  slight  (rreenish-Tellow  tint,  is  submitted  to  distillntlon, 
no  that  it  should  not  be  wnsled^  and  it  lenven  bt-hiiul  nn  (extract  i>f  a 
ycUowi§h  colour,  havin;;  a  hitler  tiist*';  this  i-t  purified  by  wiuibiii^  nii 
a  filter  with  weak  liiiunr  uminnniie,  then  with  ether,  and  IfiMtly,  with 
rectified  spirit ;  ihis  is  now  evaporat<Ml,  nml  the  residue  trcottd  on  a 
white  porcehiin  plate,  with  a  little  peroxide  of  manganese,  and  a  drop 
of  concentrated  sulphuric  acid  ;  und  ifmoi-phia  ia  present,  even  in  only 
very  itmall  c|utiiit)ty,  the  residue  will  assume  :i  rich  violet  tint,  ."luiilur 
to  that  which  occurs  with  ^Irychnin  when  treated  in  a  similur  way. 

It  floes  not  appear,  after  a  most  careful  analysis  of  numerous 
samples  nccitrdingr  to  the  process  aUive  given,  and  notwithsianding 
the  genendly  recfived  opinion,  that  Manilla  chcrooU  usually  contain 
opium.  The  diffieuliiea  attending  nn  organic  analysU  of  hm  kind 
are  very  great,  but  the  results  ohtaineil  appear  to  be  of  a  chiiracier 
to  be  rched  upon,  since,  by  the  process  above  given,  bo  little  as  one 
nuarter  of  a  grain  of  crude  opium  may  be  piiliMuctorily  detected  in  a 
single  cheroot  to  which  that  drug  has  been  purposely  added. 


SKUFF,  AND  ITS  ADULTEnATIONS. 

Tlie  thinl  and  last  f">rm  in  which  the  tobacco  leaf  is  employed  is  tn 
the  slate  of  a  more  or  less  finely-reduced  powder,  constituting  sniifl*. 

SnuflT  i<t  made  principully  from  the  stalks  or  "  jifri/*/>iii^*"  of  the 
leaf  which  arc  rejected  in  the  processes  of  manufacturing  cut  tobacco 
and  cigars ;  some  snu^  however,  coniaiu  a  proportion  of  leaf  as  well 
OS  stalk. 

Snutfis  met  with  in  cnninierce  in  two  slates — namely,  the  dry  and 
the  moist.  Of  each  of  these  there  are  several  varieties,  the  charac- 
ters which  distingui.ih  them  depending,  in  most  case*,  upon  difTerences 
in  the  pr<»ee*se9  of  roannfaoture,  in  the  relative  pro|K)rtton  of  the 
stalk  and  leaf,  in  the  <legree  of  moisture,  in  the  flavour  or  pungency, 
and  in  the  scenting. 

The  dry  snuflfs  are  in  general  much  more  finely  ground  than  the 
moist :  the  different  kinds  of  Scotch,  Irish,  and  Welsh  are  comprised 
under  this  head. 

The  moist  suufTt,  of  which  there  ar«  a  great  many  varieties,  are 
known  in  the  trade  under  the  following  names:  —  Bruwn  and  Black 
Rapjiee,  John  Bull,  Hardham's,  37,  Princerji,  French  and  Dutch  Car* 
rottee,  Masulapatam,  Prince's  Mixture,  Granil  Cairn,  and  a  great 
many  others,  which  derive  their  nojnes  either  from  the  fancy  of  th« 
maker  or  the  fashion  of  the  day. 


606 


8NUFF,    AND   ITS   ADULTEKATIOX8, 


Manufactitre  of  Snvff. 

In  the  manuracturc  of  the  difr<}rent  varieties  of  snufT,  the  proces.^ 
adopted  <if'pcu*l»  u|>on  the  kind  rt.'(iutred  to  be  made.  Scotch  snuiT. 
wbiidi  is  i^a'id  to  be  the  purettt  of  i\\\^  \6  miule  almost  entirely  from  the 
btiilks  of  tobiicro;  und  tbii>  bfiii^  ti  dry  snuU',  hs  little  moisture  as 
{K^ssible  is  added —merely  puffieient  to  prevent  the  finer  purticlefi 
i'mm  escaping  and  being  l(«t  in  the  act  of  [xiwdermg  or  grinding, 
vhieb  would  utberwiiie  ocimr.  The  stolkn,  cut  up  into  snudi  piecei*, 
are  inlrodueed  into  a  kind  of  iron  mortar  or  ^'mull^  as  it.  is  tenneil. 
This  is  furnished  with  a  pestle,  heavily  weighted,  the  handle  of  whieti 
is  connected  wltli  n  set  of  joint<;d  arms  or  levers,  so  adjusted  as  to 
pve  it  a  jHfculiar  njtary  and  grinding  motion,  this  being  the  best 
ealculat^nl  lo  effuct  the  reduction  of  the  stalks  to  powd«T.  A  K'Hes 
of  twenty  or  thirty,  or  more,  of  these  mortars  or  "  uuilU"  are  arrange*! 
anil  fixed  on  a  strong  oak  table,  with  similar  niuchinery  attaehetl  to 
the  pestles  of  each,  and  alt  of  which  arc  capable  of  huing  worked  at 
the  same  time  by  meatu  'tf  a  steam  engine  and  noitnectin^'  shafts  and 
wheels.  Aficr  the  snuff  hud  been  reduced  to  the  requisite  degree  of 
fineness,  it  is  removed  from  ihe  "  mullC  and  dried  imd  tlavouted 
according  to  n  procesEi  peculiar  to  the  different  manufacturers. 

Irish  and  Welsh  snulfj  are  also  dry  snuffs  ;  but  before  the  stalks 
are  reduced  to  [njwder,  they  are  subjected  to  a  roaslinj;  process  in 
ch>sed  cvlindcrs,  whicb  assists  in  imparting  the  peculiar  smelt  hy 
which  these  snofls  are  characterised.  Tlu-se  two  varieties  of  dry 
snuff  are  grnund  in  ntilU  of  a  similar  descriplinn  lo  thotie  employed 
in  the  jxiwdcring  of  Scotch  snuff:  linte  wnter,  and  even  powdererl 
linie,  frefjucntly  cuter  into  the  comp<>silifiu  both  of  Welsh  and  Irish 
snuff.  Indeed  the  uddllion  uf  the  formi'r  rs  idhiwcd  by  the  Excise 
laws.  The  mont.  celebrated  of  tht?  Irish  snuffs  is  lliat  manufactured 
by  the  firm  of  Lundy  Foot  and  Co.,  of  Dublin,  and  from  which  it 
takes  its  name. 

On  account  of  the  high  duly,  over  6*.  per  pound,  to  which  foreign 
manufactured  snuff  is  subject,  but  a  very  small  quantity  i.s  ever  im« 
ported  and  passed  through  the  Custom  House,  as  it  c:m  be  made  in 
Kiigland  quite  equal  in  ([uiiliiy  to  the  foreign,  and  for  less  than  half 
the  duty  ch^ir^ed  upuu  the  latter.  Indeed,  preference  is  in  general 
given  to  K^g]i^h-mAde  snuffs. 

The  different  varieties  of  the  rappees  or  moist  snuffs  are  likewise 
made  chiefly  from  stalks,  but  a  small  proportion  <d*  the  leaf  is  aUn  in- 
troduced, lis  well  as  the  finer  parts  and  sittings  of  cut  tobacco  called. 
"«mff//j|,"  which  are  Ux\  fine  lo  be  ctmveniently  smoked  in  a  pip**- 

The  pnicess  followed  in  the  manufacture  of  ntoist  snullii  diff«.T« 
somewhat  from  that  just  described.  The  stalks  cut  into  fragments, 
pieces  of  leaf,  and  smalls,  are  well  molstvned,  and  ground  in  a  mill  of 
the  following  construction  :  —  A  pair  of  very  heavy  cylindrical  stones 
(in  form  like  the  common  grindstone),  six  or  eight  feet  in  diameter. 


8XCFF,   AND   ITS  ADULTEKATIONS. 


607 


nml  a  foot  or  eighteen  inches  ihielc,  are  set  up  on  edge,  parallel  to 
each  nth(*r,  ami  a  few  indite  uparl,  oil  a  wooden  slab  or  hi'd  Nlinhtly 
bollowed  otil.  ThL'se  stones  have  a  twofold  motion  piven  to  thetn  — 
a  miary  one  on  ilieir  nwn  horizontal  axis,  and  a  traversing  roiary 
inntiDn  round  the  surface  of  the  bed,  similar  to  the  two  wheels  of  u 
carriage  ^oiiig  round  in  a  Mnull  circle  ;  this  motiwn  it  communicated 
to  thtrm  by  means  of  an  upright  shal^  driven  by  macliinery.  The  in- 
gredients for  !he  anurt'  are  placed  upon  the  bed,  and  the  broad  edge 
of  the  niiissive  stnnefl  pnnsing  reiM-atedly  over  tlicin,  combined  with 
their  nUary,  grrnrlinj  niotinnf  smm  reducfs  them  tit  powiler.  'I'lie 
con4truL>tinn  nnd  workin;;  of  this  kind  of  siiuirmill  is  thi*  ttante  an  that 
used  in  malsing  gunpowder,  or  for  cni^hln;;  the  apples  in  the  munu- 
fiicture  of  ci<ler.  After  the  snuff  has  been  reduced  to  the  re(|uired 
de;^ix*e  of  fi^ene^s,  it  is  bca[H*d  up  in  a  trough,  and  again  mui^tened 
thorou;.'hly.  or  "sauced,"  as  it  is  termed*  and  allowed  to  remain  ii  cuu- 
sidurable  lime,  by  which  means  a  cert^un  degree  of  fermeiituLion  i^ 
induced ;  it  is  turned  with  a  sliovel  from  time  to  time,  und  le-liijuored 
a?  the  moisture  evapiimlcs.  The  flavour  of  the  snnfl'  ilepencU  much 
upon  the  extent  lo  which  the  fermentation  is  aWnwcd  lo  proceed ;  ihia 
ferment  ive  process  also  adds  greatly  to  its  depth  of  colour.  At>er  the 
snufTis  thus  far  manufacturetl.  the  salts,  or  alkaline  saUs,  allowed  by 
the  Excise  regulation;',  are  added.  The  salt  is  faid  to  be  chiefly  em- 
ployed to  enaure  the  preservation  of  the  snuff  from  niotiidiness,  and 
to  cause  it  to  retain  its  moisture;  while  the  alkaline  salts  are  ueed  to 
increase  its  pungency;  at  the  same  time  they  ad<I  considerably  lo  the 
weight  nf  the  snuff. 

In  the  scenting  of  smiff^,  the  perfumes  used  —  either  the  efisential 
oil  of  lK»rgauu)t,  or  otto  of  roses,  and  in  some  cases  powdered  orris 
riKit  — arc  addcil  after  the  snuffs  are  munutacturcd.  The  priK'ess 
adopted  is  as  follows  ; — The  snuff  is  sprea«t  out  upon  lorge  skins  or 
sheets  of  pandiutent,  and  the  <iils  sprinkled  over  it  from  a  bottle  with 
slits  cut  in  the  ci)rk  ;  the  snuff  is  frequently  turned  over ;  and  laatly 
it  is  rubbed  with  the  hand  through  a  wire  ^leve.  The  only  snuffs 
that  are  ever  scented  are  brown  and  block  rappee.  Grand  Cairo,  and 
prince's  mixture,  amongst  the  moist  snuffs,  and  Scotch  amongst  the 
dry  snuffs. 

The  greater  port  of  the  snuff  consuincil  in  London  is  ground  in 
VDuff  millA,  eituate<l  near  Mitcham.  in  Surrey,  in  conscipience  of  the 
facility  affonied  for  working  the  mills  by  means  of  the  river  W'andle, 
which  runs  through  the  town.  There  are  several  of  these  otublish- 
ments  lo  which  the  London  mannfuf  turers  send  their  snutf  after  hav- 
ing undergone  a  certain  stage  of  preparation.  Beyond  the  prepara- 
tory ilryiiig  and  grinding,  il  is  snid  that  nothing  further  is  done  to  the 
snuff  in  the  snuff  mills;  the  proprietor  imt  only  prepares  it  before 
sending  it  tu  the  mill,  but  in  most  c[i:^'s  passi'.s  it  through  some  finish- 
ing openttiun:^  after  it  is  brought  from  the  mill.  Many  of  the  London 
manufacturers  have,  however,  Muall  mills  in  their  own  establishments 


COS 


SXrFF,    AXD  ITS   ADDLTEHAT10X5. 


for  grinding  sin»ll  qunntities  of  •tuuff,  or  for  pa$»injj;  the  raritius  kmilfl 
of  fancy  siiutTK  ikrou^li  any  parllculor  process  ;  but  there  are  very  few 
esliibliahmcitti  in  Loniion  where  thu  m&in  bulk  of  the  anutT  u  ground. 

On  the  Advlteiations  or  Sncrr. 

Fortif'lhree  Sfiniplea  of  snuflT  woro  nubjerJcd  to  microscopical  anrl 
rhemical  exaniinntitin  and  fiiuilyi^is  'trid  imni  ihefii?  it  appeared  that 
snutVis  subjeol  lo  n  very  lnr;re  iiniount  of  udultLTution. 

The  priiicipiil  rfsiilts  nrrived  at  were  — 

Th;it  comnum  suU  is  u(ld'.d  iii  large  i}uiintities  to  all  descriptions  of 
snuff. 

That  oxide  of  iron,  derired  from  diflerent  deitmptions  of  coloured 
femijrinous  earths,  a-*  r*d  ochre,  yelhjw  orhre^  iind  gnme  of  the  brown 
eartli4,    as   umber,    was   present    in    iipwunls    of   two  thirds  of    the 

!>Ulllple9. 

That  chromate  of  le<uK  a  verv  poisonous  substnncc,  was  detected  in 
nine  'd'the  .samples,  nmountiiitr  iii  one  instance  tonearly  eighl  percent. 

That  nxUle  of  tf^ii/y  an  ef|unlly  poisonous  substance,  probably  in  the 
form  of  red  lead^  was  disoovenrd  in  three  cases. 

That  bichromate  of  potash^  a  still  more  poisonous  substance,  iraj 
jtresent  in  three  cisi's. 

That  niiiny  of  the  samples  conTaine<l  pojedered  tilktt^  prt»bably 
potrdered  glass. 

These  as  well  as  some  other  less  important  results,  stated  more  in 
dctnd,  were  — 

Tliat  chloride  of  siMtinm,  or  salt,  is  ndded  in  Inrjre  and  very  variable 
qtinntilii'S  to  all  descriptionfj  of  snntT,  the  proporti<in9  riinjjing  from 
1-0  to  as  uiuch  as  VIS  per  rent.  Where  the  amount  of  ehloride  is  lew 
than  I'O  per  cent.,  it  is  probable  that  it  i*  derived  from  the  tobacco 
itself,  as  well  Ji.-t  the  water  used  to  mni.sten  it. 

That  the  alkalinr  and  earthy  carbniintes,  chiefly  the  earhonale*  of 
poUtsh  ofid  limey  :irc  likewiFe  udded  to  BimlT.  sometimes  In  considerabfe 
ijnantity,  but  ui«tially  to  a  le^R  extent  than  chloride  of  sodium.  One  of 
the  srtmple8yiehled3'9  per  cent,  of  carbonate  of  pntnah,  andanotherno 
less  than  10*8  per  ceiil.  of  carbuimte  of  lime.  On  lookin*;  over  tJie 
liible  of  annUses,  it  will  be  sofn  that  the  amount  of  earthy  carbonate* 
varies  considerably  in  the  diflerent.  sample^  as  was  the  case  with  the 
rhloride  of  sodium,  the  lime  being  present  in  somewhdt  larger  propor- 
tion in  the  dry  sniiffk,  as  the  Scotch,  Irish,  and  WeK-«h — to  these 
snuffs  the  law  allows  the  addition  of  lirac  water.  When  at  the  same 
time  carbonate  i>f  potash  is  adiled^  decomposition  takes  plu<?e,  jmrt  of 
the  carbonic  acid  of  the  carl>onate  of  potash  unites  with  the  lime, 
and  so  forms  carbonate  of  lime.  This  renders  it  diflicult  to  state 
exactly  the  rehiiive  proportions  of  lime  and  potash  employed. 

It  would  appear  id.-io  that  in  some  cn^es  the  alkaline  and  earthy 
phosphates  are  in  excess  in  Snutf,  ss  much  as  7  per  cent,  of  ihe 
former  having  been  detected  in  one  of  the  itmplea,  and  4*8  per  cent. 


I 


SNUFF,   AND   IT9  ADULTERATIONS, 


609 


of  ibe  liittcr  in  nnoiher.  The  stalks  of  tobacco  cnntnin  a  very  large 
■n<i  viiriiible  (|uantily  ofphotiphuteis especially  the  a[kaliii<>  iilioephates, 
and  it  is  pruUable  thai  they  are  rery  rarely  added  to  anuff  tor  the 
piirpo!tc  ol  adultfnuiiin. 

That  the  nlkulitie  guiphaifa  are  likewiao  slightly  in  excess,  amounting 
in  one  nainple  to  5*4  per  cent. ;  in  tlus  case  the  addition  nmy  Lave  been 
inieticionul. 

That  ozitie  of  iron  deriTed  from  diSbrent  descriptions  of  coloored 
ferru^riiious  uarlh,  as  re</  ochre,  yeilour  vchre.,  and  home  of  the  brown 
earlhSf  as  umber,  was  present  in  upwurdDuf  two  thirOitof  the  sumplets 
amountin;;  in  one  case  to  nolens  thun  five  per  cent.  It  is  especially  to 
beob^frveil,  that  while  all  the  Scotch  anuns  coutnitied  iron,  the  oxide 
of  that  metal  was  not  present  in  any  one  of  the  samptes  of  Wel.sh  and 
Irish  8nu0s  submitted  to  analysis.  The  presence  of  fcrrujiintma 
earths,  aa  well  as  of  some  other  colouring  [natters,  i&  freniienlly  indi- 
cated by  the  colour  of  the  ash.  Genuine  tubueco  invuriably  yielJs  an 
ash  which  is  more  or  less  (;reyt  whilu  the  ashes  of  snullii  coutaininj^ 
iron,  lead,  and  some  other  mineral  colouring  matters,  are  alwtiys  to  a 
P'eater  or  less  extent  coloured :  when  deeiiledly  n\  wc  may  safely  de* 
dare  that  some  aubatance  liaa  been  employed  to  colour  the  snuff.  In 
unadulterated  tobacco,  the  iron  present  amounts  only  to  traces  ; 
nearly  all  therefore  of  the  different  kinds  of  snufl'  examined,  except- 
ing the  Welsh  and  Irish,  were  adulteraleil  with  coloured  ferruginous 
cartlifi,  especially  the  Scotch  rujipees,  and  scented  nippees,  in  one  of 
which  the  inm  and  aliitiiina  amounted  to  five  piT  cent.  The prttenct 
of  ctUuttred  ferruginiiUM  earths  in  sHuJf  i$  uti  nduUerution. 

That  chronuite  of  Uad  was  detected  in  mue  of  the  samples,  amount- 
ing in  one  instance  to  4G  per  cent.  It  <>ccnrred  in  five  out  of  the 
nine  fuimple±t  of  Scotth  snuirexamine<l,  in  one  of  the  four  samples  of 
Welsh,  and  in  one  of  the  tiiree  samples  uf  Iri:>li  snuff  submilted  to 
analvriis.  The  preneHcn  of  this  meltUHc  comjHfund  in  tuuff'  cotutitutea  an 
aduUf  rattan. 

Thut  oxide  of  lead,  probably  in  the  form  of  red  Uod,  was  discovered 
in  three  cases,  as  mueh  lut  three  per  tent,  bein^  lound  in  one  of  the 
samples  of  ItjLnJham's  37-  7^he  prrseuce  of  thus  metaUic  oxide  is  also 
an  uduliendion  and  an  infraction  of  the  Tubacctt  Act. 

That  bichromate  of  potash  wiis  present  in  three  of  the  samples  ;  in 
two  of  the  cases  it  was  found  in  the  Scotch  snufK  amounting'  In  one 
sample  to  6*2  per  cent*  The  presence  of  thij  mU  Ukewi9e  coHstitutet  an 
adtdieration, 

'i'hat  many  of  the  samples  contained  considerable  quantities  nf 
siiiea,  nmounting  in  one  instance  to  no  leas  tbnn  b'-l  per  cent.  Jn 
some  of  the  samples  the  atidttion  uvm  uuqttrstionably  intcvtiomd.  Genuine 
tobacco  rarely  contains  more  than  3'4  per  eeiit,  and  usuully  much 
lens.  In  niobt  of  the  fitliceous  re.iidue3  of  the  allies  shming  jHirticles 
were  observed,  which  unuer  llie  niiun>ccope  presented  ull  the  »p|>ear- 
ance  of  powdered  glass;  but  since  earth  contains  similar  ]»riicfe8  in 


A   it 


^^ 


*k 


610 


8NUFP,  AND   1X8  ADULTERATIONS. 


large  quantities  we  are  not  nble  to  state  whether  in  any  case  pow*lered 
pinss  had  \i^en  uiMet^l ;  to  tho  miij()rity  of  tlie  samples,  however,  it  was 
manif'cjtt  from  the  vrtijiht  anil  apiMJuranei!  of  the  resi(lue<i  that  no  such 
addition  had  boon  made.  Theosiios  of  the  rappees  all  furnliib  a  nili- 
ccou?  residue,  wludi,  after  the  ai'tioD  of  the  aeids,  in  its  gelatinous 
character  renemhles  the  fiilicft  di-rived  from  such  a  silicate  a.i  glass. 

That  powdered  orri-i  root  was  detected  in  two  of  the  eample^.  The 
presence  of  this  in  xuujf  is  likewise  an  adtdivrtition. 

That  the  total  wtt^ht  of  ash  furnished  by  tlic  incineration  of  the 
preater  number  of  the  shufl*s  examined^  altboufjth  many  of  them  were 
very  moist,  much  exceeded  that  of  peiiuine  tobacco  after  being 
dried.  While  the  a>hes  of  snm)>le5  of  the  loiter  have  been  fuuitd  to 
vary  in  weif^ht  from  lO'H  to  TJ.'6,  those  of  the  snuffk  which  were  not 
drie<l,  and  many  of  which  contiun^d  very  large  per-centagea  of  water, 
were  in  no  ett.*e  under  I8;26  per  cent.,  while  in  one  instance  it 
Amounted  to  S5'54  per  cent.  Ilad  the  snufls  been  dried  before 
analyniftf  as  was  the  lob.-icco,  the  ditference  in  the  weight  of  the  ashes 
would  liave  been  much  more  evident.  The  average  proportion  of 
water  in  ihu  moist  snutfa  is  about  *25  per  cent. 


Cephalic  Snuff, 

Tliis  snufn  on  examination,  was  found  to  consist  almost  entirely  of 
tobacco  stalks  ground  to  a  very  fine  powder,  and  disgui5cd  by  being 
flavoured  or  scenled  with  some  essential  oil  or  oils,  most  probably 
that  of  lavender.  100  ;^ains  furnished  21*6  grains  of  ash,  o(  a  dirty 
brown  colour,  which  was  composed  of  chloride  of  itodiam,  2*0;  alha' 
Hue  carbonateB^  3*9 ;  eurthy  corhonnte$^  4*0 ;  alkoliiie  phoMphate*,  5-^2  ; 
earthtf  phoftphate*^  21;  alkaline  sulphateM^  09;  oxide  of  iron  and 
alumifuL,  TO;  and  5i7ica,  1*6  grains. 

Orimjttone*9  Eye  Snuff. 

A  prolonged  examinotion  of  this  article  by  the  microscope  si 
that  It  is  made  up  of  several  distinct  vegetable  substances.  Amoi 
these,  afler  considerable  trouble,  we  have  succeeded  in  identifying  tEe 
following  :  powdered  orrix  root^  savory^  rosemary^  and  lavender.  There 
are  probably  one  cir  two  other  vegetable  substances,  the  names  of 
which  we  have  not  as  yet  ascertained ;  but  it  does  not  contain  any 
hellebore,  assarabacca,  nor  tobacco.  100  grains,  on  being  incinerated, 
afforded  30  grains  of  ash.  of  a  light  reddish-brown  colour,  composed 
of  chloride  of  sodinm,  12*8;  alkaline  carbonates,  3'8  :  alhdine  phetS' 
phateM^  4  6 ;  earthy  phoxphates^  2  8 ;  alkaline  sulphates^  08  ;  and  BiUca^ 
6 '2  grains. 

Mr.  Phillips  furnished  the  Committee  on  Adulteration  with  the 
following  information  in  regnrd  to  the  adulteration  of  snuff:  — 

**  We  have  found,  in  different  samples,  conmion  peat,  such  as  you 
:et  from  the  bogs  of  Ireland ;  starch,  ground  wood  o{  various  kind*, 


SNUFF,    AND  ITS  ADULTERATIONS. 


611 


fustic  being  most  predntninant ;  extract  of  logwood,  chromftte  of  lead, 
bicliTxtniate  of  potash,  and  various  oclirefius  earthft. 

"We  !i«ve  also  had  satnpleA  of  Rpurimis  snutT  made  up,  aiul 
Ta^iou^Iy  scented,  to  represent  Scotch,  Wel.^Ii,  ond  Irisli  snuff,  and 
which  )ia.i  been  composed  of  ihe  following  substunces:  —  sumach, 
uml>er,  which  is  a  thirk  earth,  Spanish  brown,  und  common  salt.  In 
another  ca-e  we  found  peat,  unibur,  ami  common  salt.  In  imoibcr, 
ground  coal,  jwat,  and  extract  of  lojrwood.  in  another,  pruund  peat, 
yellow  tchre,  lime,  and  itand,  ihc  whole  of  tbvm  bein;;  more  or  less 
scouted.  I  have  no  di^ubt  they  were  made  fur  the  purpose  of  being 
mixe<l  with  other  snnflV 

Hesides  the  articles  above  enumerated  the  Excise  have  met  with 
eeriain  other  ^ubstance^. 

From  an  Excise  retuni  of  the  seizures  made  during  the  two  years 
1851  ami  1652,  it  up^^ears  that  fourteen  prosecutions  wt-re  innlitutcd 
against  [wrsons  residing  in  various  pnrtfi  of  the  United  kinjj;doiii,  for 
ndiilteraiin;;  snuff  with  vepetnble  and  earthy  matters,  or  for  Imving 
the  miiteriids for  adulteration  in  their  posi^e-tsion.  On  an  examination  of 
this  return,  it  ap]>ears  that  the  foHowinj:  subslatices  were  cither  de- 
tected or  seized  by  the  Excise  authorities  in  the  cases  itbovt*  referred 
to: —  Powdered  CoUnubo  root,  yellow  ochre,  qua.'-Ria«  red  ochre,  and 
gentian  rout,  in  one  ease  ;  f>eat  moss  and  earthy  matter,  in  two  caches  ; 
earthy  matt*T  and  ground  rhubarb  leaves,  in  onesiimple;  t2'l  1  [Hircenl. 
of  oxide  of  iron  and  (land,  in  onecuse  ;  iSO  percent,  of  vegetable  matter 
not  tobacco,  and  powtlere*!  leaves  of  tree*  each  in  one  caite ;  ^ound 
fuHtic  W004I,  in  two  coHe.^  one  cnntaininp;  *I5  |ier  cent.,  the  other  15 
)>er  cent.;  in  one  sample  wood  anil  earthy  matter  was  tbund,  and  in 
two  other  cases  the  materiob  u^cd  in  the  adulteration  were  not 
stated. 

But  it  is  not  only  with  udutteration  that  the  revenue  has  to  con- 
tend, but  alfo  with  nHUgf^fing, 

It  is  particiilarljr  woriliy  of  note  ihot  mention  is  not  made  in  the 
return  above  reterreil  to  of  the  owmrrence  of  red  lead,  chromate  of 
lead,  or  btchrtimate.  It  would  appear  that  the  Exci.-^e  only  became 
acquaintt^l  wiih  the  fart  of  the  use  of  those  poisonous  substances  sub- 
senuent  to  the  nulhor'a  report  on  suulF. 

Looking,  then,  at  the  whtde  of  the  results  contained  in  this  report, 
we  would  say  that  /Ac  nrtiele  tnujf  u  tubject  to  a  rerif  large  amttuiit  of 
adniferutmn,uttil  that  of  a  fiit,fi  which  is  not  oiUy  detrimental  to  the  reoenue^ 
but  excteihngly  tvjunotu  tt}  hralth. 

Such  striking  and  even  startling  results  were  hardly  to  have  been  an- 
ticipated; for  when  we  cotisider  the  enormous  revenue  derived  from 
tobnccG,  as  well  as  the  co^-^tly  machinery  employed  to  suppress  ndul* 
teration,  especially  in  ihin.,  and  al»o  in  otfier  exciseable  articles,  it 
might  have  oeen  expected  that  the  results  would  have  been  very  dif* 
ierent. 

a  B  2 


61S 


SNUPF,    AND    ITS  ADULTERATIONS. 


The  Exciiw  autliorities  are  numerous  and  powerfiil  ;  lliey  poMCsa  a 
staff  i>l'iinHlys!s,  ami  tliey  Imve  the  liberty  of  entering  upon  any  pre- 
iuise:«,  and  of  seizing  all  nuapeetcd  gmnU.  It  is  clear,  therefore,  from 
the  results  contained  in  this  refMtrt,  as  \TeU  as  those  of  several  previous 
oncts  that  these  autliorities,  includiiifj  the  analysis  employed  by  lliem, 
unt  by  no  means  up  in  ihcir  work.  We  say  it  witlmnt-  boiistinu,  but 
certainly  with  sonic  du^jree  of  satisfaction,  that,  aided  only  by  science, 
and  8Up|»<irted  by  a  firm  resolution,  we  have  done  more  to  discover 
and  che<'k  adullcmtion  than  the  whole  body  of  Excise  autlioritii^s  the 
maintenance  of  which  costs  the  country  some  hundreds  nf  thnusnmU  of 
pounds  annuallv.  In  those  rases  in  which  the  Excise  officers  have 
proeecutcd  parties  for  the  adulteration  of  snuff",  rhey  have  rarely  done 
soon  purely  scientific  jironnd*,  i'rtnn  i  be  results  (»f  cheinica!  and  micro- 
scopical examination ;  but  their  proceerlin^rs  uf  uoUy  have  been  based 
upon  the  scixure  of  the  artictefl  employed  for  adulteration  on  the  pre- 
mises of  the  manufacturer. 

That  forpj^  leaves  or  itlher  vegetable  Biil>slancc3  should  not  have 
been  found  in  tlic  samples  of  anulT  examined,  exccpiin*;  powdered 
orris  root  for  scenting,  is  not  surprisinir,  when  wc  con:*uler  the  latitude 
which  the  law  itself  affords  for  adulteration  with  sul*stances  not  vege- 
table, the  Tobacco  Act  pcnnitlinL',  without  limitation  as  to  quantity, 
the  addition  nf  water,  still,  and  alkaline  ealU,  and  in  the  caae  of  Insk 
and  Wcl(*h  snuffs,  lime  water. 

The  diwlosiircs  made  in  this  rejwrt  clearly  sliow  that  this  Act 
should  be  extensively  altered  ;  that  some  limit  should  be  xssigned  lo 
the  use  of  the  suttstjinces  just  named,  niid  that  the  prohibition  should 
be  extended  to  many  articles  not  specially  referred  lo  in  the  Acu 

It  appears,  then*  us  one  jn'eat  result  of  our  examination  of  »nuir, 
thai  tht)  uiajoi-ity  of  the  samples  are  adulterated,  and  ihis  iu  such  a 
manner  as  is  in  direct  viohitiou  of  the  Excise  laws,  the  parties  being 
liable  lo  very  heavy  pemdties  and  imprisonment.  Of  thy  injurioiia 
chanu-ter  of  some  of  the  adulterations  d«'l«:t«'d,  not  a  doubt  can  t»e 
entertained.  Chromate  of  lead,  red  Icnil,  and  bichromate  uf  potash, 
arc  all  highly  poisonous,  anil  when  applied  to  soh  mucotis  surfacex, 
such  OS  thoae  of  the  nose,  they  ore  readily  absorbed  into  the  sja- 
tern. 

Since  Government  allows  of  the  admixture  of  water,  salt,  alkaline 
salts,  and  lime  water,  without  any  Hiiiit  as  to  the  amount,  it  Is  ex- 
tremely difficult  in  many  cases  to  draw  the  line,  and  to  aay  where 
adulteratiun  with  theso  substances  begins. 

On  the  DtUctiou  <^ihe  AduUerationx  of  Snuff. 

The  method  to  be  adopted  in  the  examination  of  ihc  different  kinds 

of  snuffs  is  aj  foUows:  —  A  portion  of  each  is  to  be  spread  out  Ufkon 

aslip  of  glass  and  thoroughly  weiteil  with  water;  all  the  luriicr  iiar- 

tides  picked  out  with  a  needle-point  and  removed  to  another  slip ; 


I 


SNUFF,   AND   ITS   ADULTERATIONS. 


6t3 


tliese  carefully  pnllcd  to  pieces  nml  scrutinised  with  the  microscope, 
the  iiuHt  or  fioer  portion  being  tiiso  ihorou^jhly  cxiimined  under  this 
iiistruuiLMit ;  Mul  this  process  is  to  be  repcntetl  two  or  three  times 
wirli  4;uch  siiuipli*. 

PtHit^  woody  Jihre  including  yujr/ie,  as  well  %&  foreign  leatet^  are  all 
dirtcovemble  by  meAiiA  cifehc  mieroscojHj. 

100  gruiris  of  each  of  the  snutT^  ure  to  be  incinerfttod,  the  Treirrht  of 
the  iisb  flBcerininctl,  and  then  analysed  quantiiatively  for  chloride  of 
sodium  or  salt,  for  idkiiline  and  eurtby  carbonates,  sulnhiitcs,  and 
iiitrutes,  for  iron  and  uluniins,  chrumate  of  lead,  oxide  of  lead,  bichro* 
mnte  of  potash,  and  for  sdica. 

F(»r  the  detection  of /^a^y,  the  snutf,  afix?r  being  moistened  with  a 
solution  of  cnrbunate  of  soda,  is  ii>  be  incinerated,  the  ash  drcni'hed 
with  a  little  water,  and  the  residue  treated  with  a  few  drop:*  of  nitric 
acid,  an<l  tested  with  the  uttnal  reug>fntH.  The  qunniity  may  be  de* 
terniined  from  the  bulphurct  or  sulphate  of  leiul  formcii. 

The  following  is  a  good  method  i»f  proeeediiig,  and  by  it  wc  ascer* 
tain  whether  the  nietui  i>i  in  the  state  uf  cArvfrni/eor  oxxide :  — 

The  soluble  portion  of  the  ash  having  been  reuiove<l,  the  reinainder 
shiiuM  be  fused  with  a  mixture  uf  nitre  and  bi<iulphHte  of  potash,  the 
residue  well  washed  with  water,  the  solulion  filtered,  eva|>orated, 
treateil  with  hyilrocMoric  acid,  and,  while  at  a  boiling  heat,  with 
alcohol.  If  no  green  colour  be  prtxluceil,  the  absence  of  chromic 
acid  may  be  inferred;  if  the  colour  df>es  ap|>eur,  the  oxide  uf  chro- 
mium must  be  precipitated  bv  ainntonia. 

The  residue  left  after  the  hn^t  wo-^hing  is  to  be  treated  with  a  solu- 
tion ijf  amuiuniuool  tartrate  of  aninionta,  by  which  means  the  sulphate 
of  lead  is  talcen  up.  This  is  precipitated  with  sulphuretted  hydrogen, 
collected,  drie<l,  and  weighed. 

On  treating  the  sulphuret  of  lead  with  nitric  acid,  and  evaporating 
to  dryness,  an  insoluble  sulphate  of  lead  \&  again  obtained,  and,  on  fusing 
this  with  carlwnate  tii  soda,  and  treating  the  insoluble  residue  with 
acetic  acid,  aectatti  of  \ew\  is  formed,  the  solution  of  which  gives  a 
yellow  precipitate  with  imlide  of  |H)t3SEiium,  yellow  with  bichromate 
of  potush,  and  whiti:  with  dilute  sulphuric  ucid. 

If,  on  following  the  above  melhii<U  of  analysis,  the  green  colour 
is  produced  on  tUe  ad>lilion  of  alcohol,  but  no  lead  found,  then  we 
may  infer  that  chromate  or  bichromate  of  patash  bus  Iteen  employed. 

We  will  now  inquire  whether  the  Kxci»e  bos  succeeded  in  protecting 
the  revenue  from  loss,  in  the  aduiicralion  of  tobacco,  which  pays  so 
heavy  a  duty  to  the  state.  As  has  already  been  shown,  cut  and  roll  <p- 
6aci»i8suhjecl  to  ctmsiderable  adulteration,  while  «nv^  is  so  to  uii  euur- 
muus  extent.  Uf  forty-three  samples  subjectetl  to  examiualion,  nearly 
the  whole  were  ailulteraled,  and  in  n  very  scandalous  manner,  with 
stibttnnces  injurious  to  health.  So  much  f«ir  the  et^iuicncy  of  the 
Excise  in  preventing  the  adulteration  \i\'  tobacco  and  snull'. 

B  a  3 


»U  TOBACCO,    AND  ITS  ADULTE RATIONS. 

It  is  questiuiinhle  whether  the  Kxcise  really  possesses  the  rcquUite 
knowkMl^e  to  detuct  lunuy  oi'the  adulterations  of  tobacco.  Some  lime 
oinee  it  ctfriainly  did  not. 

We  learn  fium  the  Report  by  the  Select  Committee  of  the  HoiiftC  of 
Commons  un  the  lobjicco  tmdf,  that  so  convinced  were  the  ninnufuc* 
lurera  of  London  of  the  inHl)ilily  of  the  Excise  officers  to  deteet  ndul- 
terutionfl  in  tobacco,  that  they  *■■  proposed  to  the  secretary  lo  the  Kx- 
ci»«  iJoitrd  to  uend  specimen!*  of  pure  antl  of  adulterated  tobacco,  that 
the  Excise  officers  mipht  convince  the  manufacturers  of  the  power  they 
had  of  detecting  Hdulterntions. 

Under  the  authority  of  that  Committee  twelve  ump1e«  of  tobacco 
were  prepared,  und  ftiibmiited  to  the  Exrifie  to  be  oxamiticd  by  them 
and  reported  upon  ;  t}ke  exaniiiicn>  bein^  ilr.  Uiehftrd  riiUijts,  Pro- 
fessor Graham,  and  Mr.  George  Phillips. 

The  suWtaucc!)  and  artich-s  introduced  into  these  samples  were  as 
follows:  —  rhubarb  leave*,  fuxjzlove  leaves,  brown  paper,  syrup  of 
>U|2ar,  saltpetre,  alum,  cliicnry  root,  IriHh  moss,  carbonate  of  jmt&sti, 
sulphate  of  potash,  carbonate  of  magnesia  and  carbonate  of  lime,  terra 
japunicu,  refined  sugar,  conmion  salt,  nitrate  of  ammonia,  chloride  of 
puiudfiium,  and  sugar  of  milk. 

isoyr  the  only  subst^mces  detected  out  of  the  above  llht  by  ibe 
ex^nnners  vfem  ihij  rhubarb  leaven^  iTie  brown  pnpcr^  und  *vgar;  all 
the  others  remained  undiscovered.  Even  of  the  articles  actually  detectetl 
the  proportions  <>iven  wt^re  in  alt  cases  very  wide  indeed  of  the  mark; 
thus  the  16  per  rent,  of  rhubarb  leaves  iiitroduce<l,  were  set  clown  at 
3*3  per  cent.,  and  the  same  error  was  committed  in  regard  to  the 
amount  of  sugar  present. 

In  some  cases  tlie  samples  were  allejzcd  to  be  adulterated  with  sand, 
sugar,  and  crumb  of  bread,  when  either  these  substances  were  not 
present  at  ull,  or  the  samples  were  perfectly  genuine. 

Never,  in  fact,  in  the  whole  history  t>f  science,  was  a  more  hunentftble 
exhibition  of  incoiiifietenee.  'i'heie  i»  not  one  of  the  vegetable  sub- 
stances or  clK-niii-al  er)mpouiids  above  enumerated,  which  migbt 
not  have  been  readily  discovered  und  identilied. 

PROPEBTIES   AKD    EfrECTS   OF   ToBACCO. 

We  will  in  the  next  place  con^iiler  the  eO'ects  of  the  use  of  tobacco 
upon  the  human  frame,  whether  smoked,  chewed,  or  employed  iu  tiie 
form  of  snulT. 

Tobacco  owes  its  chief  properties  to  the  presence  of  two  active 
principles,  ternie<l  nicvfiiut  and  mcotiamn.  The  first  of  these,  nicutitux, 
IS  thus  chflriu-teriseil :  it  is  liipiid  and  vt>latile,  devoid  of  colour,  wttli 
an  acrid,  burning  taste,  and  p{>:t&esses  the  slrntkg  odour  of  tobacco;  to 
test-jtafier  it  shows  an  alkaline  reaction:  water,  ether,  alcohol,  and 
the  uila  dissolve  it.    It  combines  with  various  organic  and  inorganic 


TOBACCO,   AXD  ITS   ADULTERATIONS. 


615 


■ridii  to  form  salts.  1000  grains  of  tobacco  yield,  neconling  to  the 
kind  u^ctt,  Irotii  3'Bti  tu  11*28  grains  of  nicotinu.  The  action  of  nico- 
tinii  on  the  human  frume  is  tbut  of  lui  acrid,  uurcolic  iHiison^  causing 
giildincB.s  aud  voniiling,  and  in  du^es  of  a  few  grains,  ileath. 

The  properties  of  the  hitter,  nicutiamn^  are  as  fallow: — It  is  & 
toucrete  oily  substance,  hiivin^  the  smell  of  tobacio,  and  a  bitter 
tAStc.  It  i&  volutilo;  the  dilute  at-.itls  and  water  do  not  di^Milve  it, 
but  it  is  Boluble  in  liquor  pottiji.sa>  and  ether.  In  swallowing  nico- 
tioiiin,  tint  same  sensation  is  produced  on  the  tontfue  and  fauces  as  by 
tobaouo.  A  grain  udniinittlered  internally,  quiokly  cau>^ed  i^iddinesa, 
nausea,  and  retching.  It  also  produces  sneezing  when  applied  to  the 
nose*  Six  pounds  of  tobacco  leaves  furni&U  uhout  eh'ven  gruiuK  of 
nicotianin.  It  is  also  known  as  "  Concrete  Oil  of  Tobaccoj*  and 
'*  7ht/acco  Camphor."* 

Both  these  at;tive  principles  and  constituents  have  been  shown  by 
chemical  analysis  to  b^*  pre-icnl  in  thff  $make  of  tol)ucco ;  they  are 
therefore  undoubtedly  not  destroyed  by  the  combustion  of  the  to- 
bacco, whether  used  in  the  form  of  cut  tobacco  or  cigars,  but  in  the 
act  of  smoking  ihi-y  are  inhaled  aud  thus  drawn  into  tlie  mouth, 
fiiuces,  luugs,  and  even  the  stoma'  h,  especially  when  the  saliva,  im- 
pregnated with  the  tobacco  smoke,  is  swallowed.  Further,  that  ihesu 
active  constituents  ure  actually  aLsurbed,  and  makii  their  way  into 
the  system,  in  provi'il,  from  the  sickneis,  giddinw;!,  ami  death-like 
liitntncM  experienced  by  those  who  are  unaccusUHiU'd  to  smoking; 
ihnt  th'^y  are  absorbed  lo  some  degree,  if  not  to  the  same  extent, 
in  the  case  onmhiiual  smokers  of  tobacco  is  unquestionable,  the  dif- 
fercnce  in  the  cflecU  cxpericnceil  being  due  to  the  circumstance  of 
the  tiyt^teni  becoming  more  inured  tu  its  use,  and  therefore  leas 
susceptible  of  its  influence. 

In  the  case  of  confirmed  smokers,  the  eS*ect  of  tobacco  smoke  is 
that  of  a  narcifde  After  a  very  shnpt  and  almost  inappreciubie 
I>eriod  of  excitement,  the  eflei-t  begins,  and  its  tranqnillising  intluence 
IS  experienced,  pervading  the  whole  system  ;  the  fre<|uency  and  force 
of  the  puUe  are  diminislicd,  as  well  as  the  tonicity  of  the  muscles, 
p'lrticulurly  of  the  involuntary  muscles,  as  is  shown  by  the  readiness 
with  which  the  bowels  act  in  most  caites  after  sinotcing  tobaec*o.  The 
U'.lion  of  the  skin  is  also  often  iucrease<l.  but  there  is  nu  evidence  to 
show  whether  it  exerla  any  sensdde  elfeut  over  other  secretions,  us 
tlio<i«  of  the  liver  and  kidneys.  Hearing  in  mind  the  nature  of  the 
(>rdinai-y  anil  more  usual  symptoms  above  rei'erred  to,  produced  by 
the  smoking  of  tohaci-o,  we  are  in  a  position  lo  apiirei'riate  the  t-flects 
of  the  continued  use  of  lobatco  in  this  form  upon  the  human  system, 
in  persons  whose  circulation  is  brisk,  and  who  huvc  an  abundance 
of  re*l  blood  —  in  other  words,  in  the  ^aug^rne  and  the  plelburic  —  in 
whom  the  functions  of  digestion  and  assimiljtion  are  active,  w^  should 
say  that  this  habit  would  be  calculated  to  bo  productive  of  beneficial 

B  A4 


616 


TOBACCO,   AlfD   ITS  ADULTERATIONS* 


rather  than  injurious  consequences,  hy  lowerinji  Bomewliat  the  tonenl 
the  ciTculaiion,  and  hy  proiaotin^  the  »e(.*rflioii  ot*  the  sadivary  gtantU 
and  uf  the  skin  ;  nlso,  (Krhap.s  by  moderating  the  aetivity  ofdigcsiion. 

In  [H-'Pfinns  of  weak  circulation  and  digestion^  in  many  of  wbouj  the 
hubit  uTtubucco  Fni^kin;;  is  At1i>ntled  with  };reat  expectoration,  there 
is  no  (juestion  bul  thut  the  indulgence  in  this  practice  is  in  n  high  de- 
gree prejudiciiil  (**  healih,  for  it  Imvers  stdl  more  the  force  of  the 
cirnilatiiin  And  ihe  powers  of  iliue.>ition  ;  while  the  great  ex[>ei-toration 
of  saliva,  a  fluid  which  fxiniainii  a  lar}ze  portion  of  animal  matter,  Acts 
as  an  exhausting  drain  upon  the  system. 

There  is  another  class  of  persons  on  whom  the  practice  of  tobacco- 
smokinj;  may  possibly  exert  a  beneficial  effect  —  nunielvi  tliose  of 
nervous  and  irritable  temperament  —  espet'iaily  those  who  arc  00 
from  tbe  over-c.xcitemenl  of  business,  rather  than  from  disease:  tbiit 
would  apply  to  a  considerable  number  of  residents  in  targe  towns  ai\d 
cities. 

In  those  oases  in  which  smoking  ia  attendtnl  with  great  expectora- 
tion, it  is  probable  that  tbe  constitutional  eifecis  of  the  tobocco  are 
experienced  in  a  far  less  degree,  since  very  much  of  tbe  nicotin  and 
nicuiianin  is  ejected  with  the  saliva. 

In  countries  where  tohai'co  ig  vrown,  w  in  America,  the  peruiuioui 
efiifcts  of  extreme  ii)dul;;eiiee  in  smoking  are  i'uHv  known  and  rp- 
cognised.  In  America  it  is  no  uncommon  circumstance  to  bear  of 
coroners*  inifuests  on  the  bodies  of  smokers,  especially  youths,  tbe 
ordinary  verdict  l)eing,  "Died  from  excessive  tobacco  smoking." 

jiul  a  very  large  |)roporlii>n  of  tobacco  smokers  belong  to  none  of 
the  three  classes  of  persons  above  referred  m,  being  neither  pielhniic, 
dyspeptic,  nor  nervous  and  irritable^  but  arc  in  ihc  enjoyment  of  a 
goutl  and  sound  slate  of  health:  lo  such  pers<ms  we  would  ?ay  chat 
the  habit  of  tobacco  smoking  is  useless  and  exjiensive,  and  aiaipl^ 
panders  to  that  spirit  of  self-indulgence  which  leads  many  to  gratilj 
the  senses  in  a  variety  of  ways. 

The  habit  of  smoking  is  often  injurious  in  an  indirect  manner,  by 
its  acting  as  an  inducement  to  drinking,  and  thus  becoming  the 
source    of   intem^H^rance  and  its  attentlant    evils.     Indeed,   too   fre- 

3uently  these  practices  go  together.  "  Smoking  induces  driiiking, 
rinking  jaundice,  and  jiiundiue  di'ttth." 
Muny  of  the  above  remarks  apply  with  greater  force  to  tbe  practica 
of  tobacci)  chewing;  in  this  case,  no  doubt,  a  larger  quantity  of  ilia 
active  principles  of  the  tobiu'co  make  their  way  into  the  system  ;  and 
this  amount  woidd  be  very  much  greater  were  it  not  for  ihc  fact  thaW 
all  chcwers  of  tobacco  ex]>ectoratc  largely  and  often  injure  themselTefj 
thereby. 

The  constitutional  effects  resulting  from  the  use  of  tfibacco  in  th^i 
form  of  snuff,  when  this  is  genuine,  are  certainly  niuth  less  than  inl 
the  case  either  of  smoking  or  chewing  tobacco  ;  indeed,  tbe  eflVcts  nrft| 
in  most  cases  chiefly  local.    The  nerves  of  the  Schneiderian  muiubrj 


TOBACCO,    AND   ITS   A T>U ITERATIONS. 


617 


lire  over  stimiilatcfJ ;  l)ier<»  is  tleterminatlon  of  blooJ  to  the  pnrt,  nnd 
tliu  inerul>rane  becomes  titifkent^il  and  in^nsible ;  at  ilie  snme  time 
the  brnin  is  rouitcd  to  increased  action.  When  any  of  the  snuff  tnkcn 
make«  iu  way  int4>  the  faures,  as  it  very  often  does,  it  produces  a  cit- 
tHin  amount  of  constitutional  derangement,  and  often  pives  rise  to 
dyspepsia.  On  first  UHfifininp  to  talce  sniin,  .tieknessaitd  fuintness  iire 
induced  in  llie  same  way  a$  from  tobacco  •miokiug. 

The  chief  torul  t-flWt.-t-t  of  the  long-continued  use  of  onuff  are,  impair- 
ment of  the  8cn5e  of  smell,  and  lo  a  Ims  fxlent  of  that  ofta-itf ;  the 
voice  also  becMinieH  much  altered.  'Diose  effects  are  not  he  attributed 
entirely  to  tiie  tobacco  contained  in  the  gniiff,  but  arc  aUo  due  to  the 
irritatinn  action  nf  the  alkalies  and  sails  which  enter  into  the  coiii|K)- 
sttion  of  all  suuff,  as  well  u»  to  the  red  anil  yellow  ochre,  red  lead, 
chromate  of  lead,  bichromate  of  potoiih,  uml  many  other  iiijurioiissub* 
stflhcpi  with  which  snuff  in  etdoureil.  The  poisonous  nature  of  the 
chromtitcs  of  polnah.  e*peciiilly  the  biihicmate,  had  lonjj  l>een  his- 
pcclcd  frt»ni  the  diittre!>sin;^  sympfoms  produi  ed  in  workmen  en^jagcd 
in  many  of  the  operations  of  dyeing,  'ihi.*  led  MonR.  Duchatel,  of 
Paris,  to  institute  ex|>eriments  wirh  the  view  to  inve»ti(!ate  and  de* 
termine  the  effects  which  ihiR  salt  exerts  on  the  animal  economy,  ami 
the  dopes  in  which  it  ]irove8  injurious  or  poisonous.  He  found  that, 
even  in  the  small  doses  of  from  one  twenty-fifth  of  a  frrain  to  one  five- 
hundredth  of  a  grain,  it  destroyed  the  livt^s  nf  uninials  (do^)  on 
which  he  experimented,  cau»in<;  sickness,  vomiting,  and  severe  gas- 
tritis; ftnd  po<>t*nior(cm  examination  showe^l  the  mucous  memhrnne 
of  the  9tumach  and  prima  via  to  be  much  inflame<l  and  completely 
softened. 

Chromate  of  lead  and  red  lend,  although  not  poisonous  to  the  same 
extent,  are  yet  of  a  very  deleterious  nature,  even  m  exceedingly  minute 
doecs.  The  metallic  salt^  are  constantly  employeil  to  give  colour  to  a 
variety  of  articles,  e?]»ecinlly  sugar  confectionery  ;  and  many  instances 
have  been  recorded  of  the  fatal  consetpiences  to  children  who  have 
partiiken  of  sweets  in  which  these  dangerous  substances  had  been 
ut*etl. 

I'he  quantity  of  chromate  of  lead  and  red  lend  contained  in  snuff 
as  shown  by  the  annlyttes  is  ofiim  very  c<insiilcr«ble^  nearly  5  per  cent, 
being  sometimes  found  in  it  ;  ^ufficieIlt  —  a.*(  ap[>ears  from  the  follow- 
ing very  intcre^itin!!  and  highly  im|Kirtant  ciiJie,  tor  the  particulars  of 
which  we  are  indebted  to  Professor  Kriih'wn  —  to  give  rise  to  the  dif- 
ferent symptoms  and  effects  of  |K>isoniiig  by  lead,  as  colic,  paralysis,  &c. 


Cfi»€  of  Slow  Puisoniwg  b%j  Snuff  corjaimng  Lead^  by  Mr.  Erichten, 

"Whilst  on  a  profcprional  visit  In  tlic  country  Inpt  March,  I  wasrc- 
questetl  to  s«e  a  gentleman  who  had  been  invited  d«>wn  to  a  fnend*s 
country  scat  in  the  hope  that  change  ot  scene  and  uir  would  jnlluence 
favourably  an  attack  uf  pBraly&ii<,  which  was  said  to  be  of  a  rheumatic 


018 


TOBACCO,  AND   IT8  ADULTERATIONS. 


cliaracter;  b^  which  be  had  been  dlsahted  from  work  for  many  montlrt 
post,  and  of  which  he  despaired  of  reouveriiig,  having  reliiu|uUhed  all 
treaHnent. 

'*  I  found  the  patient  in  bed, and  somewhat  exhausted  by  thejnnrnej 
down  —  a  distAJicc  of  nearly  n  hundxed  nillea  from  his  usual  rcaideiice. 
He  was  peculiarly  sallow^  the  enniplexion  having'  almost  on  icteric 
tinge ;  but  the  couiileiiunec  was  lively  aud  exjirettsive,  and  the  intellect 
as  bri;;hl  ns  usual. 

"  Ah'.  A.  B.  could  stand  mul,  if  support^^d,  could  walk,  though  feebly 
and  with  mudi  diUiculty.  lie  coui[ilu)iitfd  uiucb  of  paina  about  the 
shoulilen*  luid  the  He-hy  \vdrUi  of  the  thtglu  and  legs,  and  espociidly  of 
buriiin*;  sensaiinn^  iii  the  sulea  of  his  feet.  The  at  lirulation!!  all  ap- 
])earcd  healthy^  no  swelling  or  looseneia  was  perceptible  about  any  of 
them. 

**  I  wa.%  however,  particularly  struck  with  the  appearance  of  the 
hands  and  arms,  which  were  lying  powerlesti  on  the  coverlid  of  the  Itcd. 
There  was  marked  "wrist-drop"  of  both  arms,  the  hun'ls  hanjfing 
Baccid  and  at  right  angles  with  the  forearms,  without  the  patient 
being  able  to  extend  or  raise  tlitm  in  the  sli^jlitei't  dejpve.  There 
was,  however,  sonie  iilight  p*iwcr  of  extension  left  in  the  fingers,  ejpe- 
cialiy  in  tho^e  of  the  left  hand.  Thou};h  unable  to  extetul  the 
fingers,  raise  the  hand,  and  Bcurcely  having  power  to  elevut«  the 
arm,  Mr.  A.  B.  couhl  Jlex  the  fingers  pretty  firmlv  so  as  to  j^ivc  % 
tolerably  go<Hl  gratp  to  wJiiiUiVer  was  put  into  hi<t  hand.  The  index 
finger  of  tliu  riglil  hand  seemed  to  be  the  moat  alfeeted,  and  was  per- 
manently flexed. 

•*  There  was  a  very  marked  degree  of  wastineof  the  whole  nias»of  the 
extensor  muscles  of  the  forearm,  so  that  a  longitiidimd  htdlow- corre- 
epomlihg  to  the  inloros:>vous  ajjuee  was  perui-ptihlt'  ilnwn  the  whole 
length  of  the  forfHrui,  and  a  very  tleep  and  mnrkL*d  depression  in  the 
interspace  between  the  first  atid  second  metacarpal  boues.  The  hands 
were  (juite  powerlesbi,  and  the  patient  was  unable  to  render  himself  ibts 
Blightest  assistance. 

**'J'he  ton{£ue  was  pale  and  flabby  ;  and  on  examining  the  gums  I 
found  a  de^p  blue- black  or  leaden-coloured  line  around  the  teetli, 
more  marked  about  the  mnhirs. 

"Digestion  was  much  impaired.  Appetite  capricious,  with  much 
fiatulcnce  and  oceasiunul  attacks  of  constipution  with  colickv  paioit. 

"•'  On  inquiring  Into  the  history  of  the  ca^e,  I  learnt  that  Mr.  A«  B^ 
who  is  much  devoted  to  literary  pursuits  and  habitually  led  a  seden- 
tary life,  had  for  *unie  years  previously  suffered  Irom  puins  of  a 
rheumatic  or  gouty  character;  that  in  Alay,  1853,  he  had  beon  at- 
tacked liv  constipation  and  colic  whilst  lodging  for  a  short  tiuiu  in  a 
Jiewly  painted  house.  In  Aujiust  of  the  s»ine  year  he  ha<l  first  bogus 
to  lose  power  in  extending  lils  arms,  finding  a  difliculty  in  ruining 
them  to  put  on  his  coat ;  and  from  (his  time  the  purulylic  s^'mntoiu* 
gradually  increased  until  they  hud  assumed  the  degree  iu  which  X 
ibund  them,  when  he  hud  become  reduced  to  a  bUie  of  complete 


TOBACCO,  AND  IT3  ADULTERATIONS, 


619 


]ihysIco1 1ic1plos5tK*ss,  tl)oii<;li,  as  I  have  already  obser%'ed,  his  puwcr- 
t'ul  und  clcur  iiiteltecl  vtha  an  perfect  na  ever. 

**  On  tfxuiuiiiinj^  Mr.  A.  U.,  I  wa.4  at  once  struck  by  the  very  marked 
*wrUt-dru])/  inuru  coiiijilete  than  I  hitd  ever  seen  before;  the  limi- 
tfltioM  oC  the  [mralysis  to  the  extensors^  which  were  preiitly  wasted; 
the  existence  of  u  blue  line  around  the  teeth ;  and  the  occurrence  ol' 
occasional  attacks  of  cunntipation  and  colic,  together  with  Hying  pains 
in  llie  fle:diy  ports  of  the  binly,  with  absence  of  all  articular  infljim- 
nnition.  Ihese  syniplouis  led  mc  to  the  conclusion  that.  Air.  A.  B. 
wua  suffering  from  saturnine  paralysis,  uud  that  tiu  had  been  slowly 
puiMmed  by  lead. 

"The  ditHculty  wan,  however,  to  ascertain  how  poisoning  by  load 
could  have  been  elFected.  With  th»  view  1  nmde  diligent  inquiry 
into  the  putient*s  habiu,  the  water  he  ilrank,  the  utensils  he  used,  &c., 
but  could  not  detect  any  st>urce  to  xvhioh  the  presence  of  the  mineral 
in  the  system  could  be  traced,  except  that  the  first  attack  of  colic  and 
constipation  had  occurred  whilst  temfK)rarily  Iod;;ing  in  a  house 
which  smelt  of  fresh  piint ;  but  >i»  he  mmmi  left  this  1  ihouj^ht  it  very 
insullicient  to  explain  his  continued  and  inci easing  sullerin};!;.  In  the 
course  of  my  inquiries>  however,  1  found  that  he  look  suutf  in  consi- 
derable quantities.  I  &ccordin;.dy  emptied  his  box  of  its  contents,  and 
tfMtk  (hem  up  to  town  with  me  with  the  view  to  further  examinalitm. 
The  snuiT  was  unalvBcd  by  i'rofe^sor  Williamson,  who  imnieiiinlcly 
detc<:ted  in  it  a  considerable  ipi.iniiiy  of  letMl;  and  another  supply 
having  been  procured  from  the  shop  at  which  Mr.  A.  B.  wa«  in  the 
liabit  of  purchasing  it,  whs  subjected  to  analysis  by  Dr.  Garrod.  who 
readily  detected  large  i^uu(ititiv:t  of  the  metal  in  it. 

"Mr.  A.  h.  was  n«tw  put  under  treatment  for  saturnine  pamlysis. 
The  sniilVw:u  left  olV;  the  bowels  were  kept  o|>en  with  the  acidulated 
••niphate  of  ma^ncMa  ;  iodide  nf  pulas-sium  was  tVeely  ^iven  in  con- 
junction with  &trychuiii«  which  wo-t  uiiplied  topically  to  blistered  sur- 
f.ices  as  well  as  a*lministered  by  the  hands;  und  galvanism  was  assi- 
duously employed.  Under  thjs  plitn  of  tieatmunt  he  •rraduully  im- 
proved in  all  respects;  the  colicky  syuiploms  rupidly  disappeared,  the 
niuscuhir  pains  subsideil,  und  the  purulytic  condition  of  the  extensors 
was  gruduidly  removetl,  until  at  the  end  of  Julv  iie  was  able  to  resume 
and  to  discharge  public  duties  of  u  very  onerous  character  with  his 
n>ual  ability  and  energy." 

Witli  the  above  sketch,  wc  rcwivcd  frtjm  Mr.  Ericbsen  a  sample  of 
the  snutf  which  was  the  occiisi<Mi  of  al]  the  mischief.  On  analysis  it 
was  fnund  to  contain  1'2  per  cent,  of  red  oxide  of  lead;  that  is  very 
much  less  than  some  of  the  other  samples,  the  analyses  of  which  have 
already  been  j^^iven. 

But  the  case  reported  by  Mr.  Knchsen  is  by  no  means  a  solitary 
one  ;  we  have  already  been  mf'ormed  of  others. 

One  of  these  casf-s  was  that  of  Mr.  Fostiroko,  surpcoii,  of  Bidford, 
Alecster.  The  particulars,  as  kimlly  furnished  by  Mr.  Fusbrokc  hiui- 
selil  «re  as  follow ;  — 


4 


(80 


TOBACCO,   A5D   tTS  ADULTER  ATT0K8. 


"  In  the  latter  pnrt  of  the  year  1852.  I  suflercd  from  an  attack  of 
what  was  at  ilie  limo  rojranleil  as  simple  coiistiptttinn  of  the  Ixiwelo, 
but  attended  by  eoiisiderablc  pain,  efpecinUy  about  the  umbilicu*,  of 
u  iwititiiig  chnraeter.     A  luetliuul  friciul  who  visiteil  me  nrdered   a 
dose  of  morphia,  followed  bj  an  active  aperient,  which  relieved  all  the 
symptoms.     In  the  course  of  a  short  lime  my  jzenorHl  health  bepan  to 
fail ;  I  eonatanlly  experieneed  a  wdsation  of  sioklii"^  about  the  t'pijjns- 
trium  ;  the   t>owels  became  irritable,  and  I  invurmhlv  pa£So<l   ii<iuid 
motions.     After  spemlin:;  a  short  time  from  home  iti  ^lay,  18^4,  1  was 
suddenly  attacked  by  similar  svinpionis   I  hud  before  suflenMi  tVoiu, 
but  of  a  more  severe  character.     The  puin  was  most  excruciating, 
the  bowels  more  obstinnte,  au*l  were  niuny  diiys  before  they    were 
relieved,  upiio  which  all  the  »yn»pt»>m!i  jiubiiidud.     I  now  noticed  sonic 
trembling  of  the  hands,  which,  however,  aoon  pn??ed  oH";  but  fr*>in 
this  time  every  thin);  1  did  wju  by  an  effort  most  painful.     The  appe- 
tite Jailed,  I  became  much  thinner,  had  palpitations  of  the  heort,  con- 
stant jmins  in  the  lower  extremitie«i,  and  was  little  relreshed  liy  sletfp. 
MatteiTi  continued  in  this  state  until  October  15ih,  when,  being  en- 
gaged in  writing  late  lit  the  oi^ht,  I  vrm  suddenly  (in  a  moment,  in 
fact)  surprised  to  find  that  I  liad  no  command  over  the  ring  finger  of 
the  right  hand,  tliat  it  dragged  on  the  [>aper;  and  in  a  lew  days  the 
other  tingers,   as  well  of  those  of   the  left  hand,   became   similarly 
affected.     The  extensors  of  the  thnnibs  and  wrists  cacapetl.      1  wna 
then  fully  impressed  with  the  iilca  that  it  niuat  arise  from  lend,  and  I 
consulteil  Or,  Thomson,  of  Strattbrd-on-Avon,  who  haa  paid  much 
attention  to  the  subject  of  lead  poisoruug.     He  at  once  toUl  me  tiiere 
could  be  no  doubt  on  the  subject;  the  blue  line  whs  well  marked  on 
the  edges  of  the  gums.     In  the  cour.«e  of  the  same  week  I  had  a  third 
attack,  much  more  severe  than  either  of  the  preceding  ones  ;  the  in- 
tensity of  the  pain  was  indescribable,  and  1  was  only  conipanitivelj 
easy  when  in  a  bath  of  almost  boiling  w^tor.     The  bowel?,  as  bef< 
did  not  act,  and  renuired  varioufl  aperients  tor  forty-eight  hours  be 
Bny  effect  was  j)roducod.     Ciuitor  oil  with  laudanum,  in  large  doseSi 
and  the  use  of  irtjeclions  of  turpentine,  at  last  gave  relief  to  them.     T 
WHS  then  for  some  time  tormented  by  a  fixed  pain  in  the  small  of  the 
back,  and  extending  to  the  lower  extremilics,  caused  {K)s9ibly  by  the 
action  of  the  turpentine  on  the  kidneys.     Dr.  T.  saw  me  at  this  time, 
when  parulysia  uf  the  upper  extremities  hail  gone  on  so  far   th«t  I 
was  unable  to  turn  in  bed.     He  most  kindly  interested  hini»eLf  in 
my  ease,  and  ini>tiluted  a  most   minute  iiitpiiry  as  to  what    1   took 
ditfercnt  from  my  family,  and  at  once  fixed  «»n  the  article  of  ttnutf 
as  the  probable  source  trom  which  the  M'stem  had  been  inipre<;TioltNl. 
Subse(juent  investigation  fully  cunfirnied  his  view.     My  health  is  now 
perfectly  restored,  nothing  remaining  but  a  Irltiing  weakness  of  lb( 
ext'^iisurs  of  the  lingers. 

*•  Tlte  treatment,  in  the  fir?t  instance,  was  iiuliihuric  acid  and  alks- 
linc  aulfiJiates.     Iodide  of  potassium  produced  uo  very  murkud  b«ur6( 


I 


TOBACCO,   AND  ITS   ADDLTERATIOI^S. 


6SI 


unlil  gulviinisin  wa§  cnnjo'intly  tried  with  it^  under  which  plan  X  wns 
in  n  few  months  I'liUv  restored  to  hfulth." 

In  the  ItittLT  vrhicli  aocoiopitniod  ihc  sketch  of  the  cascabnve  given^ 
Mr.  F<tebr'»ke  remarks:  — 

"  Perhaps  il  may  bo  intcrestinj;  in  some  degree,  in  iidilirion  In  whnt 
I  stated  rfspeclinjj  niy»eir,  if  1  inform  you  lliiit  my  father,  who  is  now 
between  70  mtd  HO  veurs  of  a'je,  took  the  !<nme  snufT,  und  linx  l>een  in* 
rurnbly  piinilvsed  for  many  ycira  past.  No  opinion  was  given  by  any 
tnedical  man  he  consulted  u.«  to  its  origin.  He  Imd  ilisK'ontinued  the  use 
ol'snutV  for  several  yearn  previous  to  my  case  occurrini;,  and  hiis  now 
miii-h  better  heallh.wiihcxtreotion  of  the  pow(>rh^s  condition  of  the  nruLS." 
in  a  sei^nul  communieaiKmf  Mr.  Fosbroke  furni&hes  the  tollowing 
further  information  :  "  I  t'orgtft  to  say,  respectinj;  my  fatlier's  cjwe, 
thiit  ub'tul  four  years  u<:o  he  sulfervd  most  lireuilfully  from  seiutiea, 
whieh  eonfined  hiui  lo  bed  lor  ^everid  ninnthi,  und  that  Dr.  Thomson 
then  visited  him,  nnd  pointed  out  thiit  lead  baij  occasioned  »ll  the 
mischief,  but  that  from  its  insidious  introtliiction  intn  the  svstein  from 
whatever  Aource,  and  tlitt  lon^tlt  of  tiino  that  hail  elapsed,  littU-  rould 
be  done  beyond  relievin;:  his  present  suiTerings,  wliieh  fortunately  was 
ctl'ected  by  sulphuric  ucid.  r  nun  distiiste  lie  gave  up  snuQ-taking, 
and  has  hud  no  return  of  a  similar  attack. 

*' A  j^enilemnn  in  this  neijxhb(»urho*xl  took  the  same  snuflf  (Itolon- 
piro,  from  'iVhiy's,  L<>n<lon),  an<l  com)>lnine<l  of  inability  to  raise  the 
leO  arm  for  some  time  previous  to  his  death." 

A  sfiniple  of  the  snulf  taken  by  Mr.  Ko.-»broke  yie1de<l  on  nnalysic 
disLinet  rvidenees  of  the  presence  of  lead,  but  not  in  amount  nearly 
so  great  as  the  previous  and  many  other  of  the  snuffs  exnmined. 

Another  ease  was  refeired,  about  a  year  since,  \o  Dr.  Letheby ;  it 
was  that  of  a  ;^enllemau  who  presented  all  the  symptoms  of  luad- 
p4>isoning.  An  aiiulvMs  of  the  snull',  brown  rappee,  which  he  took, 
led  lo  the  (tiscuvery  of  the  source  of  !h«  poison. 

At  the  la>t  meetin<;  of  the  British  Asvoclution,  it  was  stated,  in  a 
discussion  on  jMti-tonin^  by  snutT,  that  mnny  persons  hud  been  injured 
by  the  leati  reueiveil  iiilo  the  sy.^tem  through  the  «nutr  taken.  We 
have  thus,  in  the  catte  of  sniitT.  another  striking  example  of  injury  to 
the  pubtiu  health  arising  out  of  (he  praiuiec  of  njlulteraiitni 

Itut  the  practices  of  snioknigr  »nd  chewing  tobacco,  and  of  smufT- 
taking,  are  objeclitmable  on  other  grounds  than  Ukmc  relating  to 
henilii.  Tlio  dwelling  and  clothes  of  the  smoker  arc  impregnated 
with  the  heavy  nauseating  iHloiir  of  the  tobacco,  particular! v  oHen- 
aive  to  thotie  who  have  a  niL-e  sense  of  smell.  nn<i  who  are  not  them- 
selves tobacco  smokers.  Imleet),  the  uiord  and  duiueatio  ol>j*:ctionfl 
to  smoking  are  of  the  strongest  kind. 

In  the  ease  of  the  chewing  of  tob:icco  the  practice  U  rendered  dis- 
gusting by  the  ilark,  unn.iturul,  and  disli-iuriag  ataiu  which  an  indul- 
gence in  this  liabit  im|):irts  to  the  UsKUi^  and  by  the  character  of 
the  liquid  which  is  con>tai)l]y  ejeclud. 


89d 


TOBACCO,   AND   ITS   ADTTLTERATIONS, 


SniiiT-tnkinrr  m  an  ennntly  dirty  habit ;  for  not  only  are  the  nosUiU 
constantly  filled  with  tlic  brown  nnd  earthy-liwkinp  powOer,  but  the 
Ittucea  at  weH  as  Ihe  atomnch  come  in  lor  their  >hQre  nC  it ;  Uic  fiice 
19  often  !inieari'<l  with  it,  tlii'  niiilii  filled  witb  it,  aud  the  sliirt  and 
clothes  nUo  sluined  and  dirtied  br  >ti*  tue. 

Other  views,  which  may  l>e  taken  of  these  practioea,  are  the  ex])«t)0« 
and  Inss  of  time  which  they  involve.  With  record  to  the  expense  and 
loss  of  time  sacrifired  in  sniifl-takingf  the  fullowing  curious  ealifuate 
has  been  idikIu  by  Lord  8tunhr>pe  :  — 

"Every  professed,  inveterate,  :md  incurable  snuff-liiker,  at  a  mode- 
rate coiiipututionf  taktit  one  j>iiicii  in  ten  niinuteit.  Kvery  pinch,  with 
the  Egreeiihle  cereinuiiy  of  blowing  and  wiping  the  nose,  und  either 
inci(lent:d  circuiuHtiinees,  con.sunie^  a  minute  and  a  half.  One  ttitnute 
and  a  half  out  of  every  ten,  nllowinjf  sixteen  hnurs  to  a  pnuff-takin); 
day,  imtituntit  to  two  himrs  and  twenty-four  minuter  out  of  every  na- 
tunil  day,  or  one  day  out  of  every  ten.  One  day  oui  of  every  ten 
amounts  to  thirty-six  days  and  a  half  in  a  year.  Hence,  if  we  sup- 
pose the  practice  to  be  persisted  in  for  forty  years,  two  entire  years  of 
the  snun-tstker's  lil'e  will  be  dedicate*!  (o  Tickling  his  nuxe,  and  two 
more  to  Mowing  it."  The  ex|>enfie  of  snuff,  snufT-boxcs,  and  hand- 
kerchiefs is  also  nlliided  to,  and  it  Ih  calculated  "  that  by  n  proper  titf 
nlicntion  of  the  lime  nnd  mom-y  thus  !o?t  to  the  public,  a  fund  uiigtit 
be  constituted  f<»r  the  diH'harg^e  of  the  nntionnl  debt." 

It  should  also  be  remembered  tlmt  such  unclean  and  diitgusting 
practices,  although  thev  may  lose  much  (tf  their  itd*ensiveness,  from 
reiH'tition,  to  the  parties  who  ihcuiselies  practi^e  them,  yet  in  mo«i 
cases  they  are  most  disagreeable  to  ibo^e  who  do  nut  pjirttcipate  la 
tlH>in,  and  who  are  forced  lolw  s(jeclatnr»  of  them. 

For  much  interestinj:  and  curious  detail  relating  t*>  Ti>baicn,  the 
render  is  referred  lo  "  A  I)issertation  on  the  Use  and  Abuse  nf  To- 
bacco," by  Adum  Clarke.  These  remarks  occur  near  its  t^mehision  :  — 
"To  those  who  are  not  vet  incor)>ornted  with  the  fashionable  com- 
pany of  tobacco  consumers  I  would  say,  Never  enter.  To  thooe  who 
are  entered  1  wouhl  gav,  I)i.>si9t.  Firpt,  for  the  sake  of  your  health, 
which  must  be  muterially  injured,  if  not  destmyed  by  it.  Secon-lly. 
for  the  sake  of  your  property,  which,  if  you  are  a  pcior  man,  must  bi; 
considerably  impaired  by  it.  But,  supposing  you  can  afi'iird  thi«i>xtr« 
eipcnse,  consider  how  acceptable  the  pence  (to  go  no  f.irther)  whirh 
you  spend  in  this  idle  and  unnecessary  employment  would  be  to  manjr 
who  arc  often  destitute  nf  bread,  and  to  whom  one  pcnnv  would  same* 
times  be  a?  an  anpel  of  God.  Thirdly,  for  the  sake  ot  your  time,  a 
larjre  portion  of  which  is  irreparably  lost,  parlicuUrly  in  smoking. 
Have  you  any  time  to  dispose  of — u*  murder?  Is  there  no  need  *if 
pruyer,  readini;.  study  ?  fourthly,  lor  the  sake  of  your  friends,  who 
cannot  fail  to  be  pained  in  your  company  for  tlie  reasons  befure 
aS9i|;ned.  Fifthly,  for  the  «ake  of  your  voice,  which  a  continuance  in 
snutr-lakinr  will  infalliljly  ruin,  as  the  nasal  possaj^  are  almost 
cutirely  obliterated  by  ii>    Sixthly,  for  the  sake  of  your  memory,  th^c 


i 


TOBACCO,   AND  ITS   ADULTERATIONB- 


639 


it  may  he  vi)?nrou»  nnd  retentive ;  and  for  tlie  sake  of  ynur  judgment, 
thut  it  nwiy  be  cluar  and  rett'iiiive  to  tliti  end.  La^tl^,  for  tlie  sake  of 
ynur  soul.  Do  you  not  think  that  God  will  visit  you  for  your  loss  of 
liiuu,  waste  of  money,  and  needless  9ulfinilul;»cnce?  llave  you  not 
■een  thut  the  use  of  tubacco  leatis  to  drunkenness?  Do  you  not  know- 
that  hiibitual  smokers  have  the  drinkin<;  vessel  often  at  hand,  and 
fretjuenlly  npply  to  it  ?  Nor  is  it  any  wonder ;  for  the  ifrent  uuiuitily 
of  necehsary  moisture  which  is  drawn  ojffrom  the  inouth»  &c.  oy  these 
means  must  be  9up|)lie<l  some  other  way.  You  tremble  at  the  thought : 
well  you  may,  for  you  are  in  great  danjjer.  May  G»hI  look  upon  you, 
and  f>ave  you  before  it  is  toi>  late!  It  was  this  view  of  the  subjeet 
which  led  Mr.  Sylvester  to  imagine  that  the  plant  derive<I  its  uame 
from  Bacchus,  the  heathen  i;od  uf  the  drimkards. 

"  •  WtiJch  cif  ihflr  WMpnnii  litith  thif  ronqunl  sot. 
(l«rr  thiMr  wlit ;  the  plp«,  or  rlif^  tlie  |iot  ? 
For  r*rn  thr  (Irrlrnlton  n'  Ihf  ruiiu' 
SwTTif  lo  ailiirii'  tn.  ari'l  tiitluilr  ihr  lamc  i 
Totuu-(*(i,  A»  Tm  Bui>_«  OQO  would  lay  ; 
To  i-iip-gu<t  Burtrhiu^cillcatctl  ay,' 

**  It  is  with  pnin  of  heart  that  I  am  oblippd  to  say.  thnt  I  have  known 
«evernl  who,  tlirouph  their  imni'Mk-rnte  atlarhnicnt  to  the  pipe,  hove 
become  vile  sots.  ^I'here  arc  olhrrs  who  are  walking  unconcernedly 
in  the  snroc  dangerous  road.  I  tremble  for  them.  Shnuld  this  foU 
into  their  hands,  may  they  receive  it  as  a  warning  from  God  ! " 

Thu  Kovnl  author,  King  James,  concludes  his  celebrated  "Counter- 
blaste  to  Tobacco "'  in  these  words  :  — 

"  Have  you  not  reason,  then,  tn  be  ashamed  and  to  forbear  this  filthy 
novelty,  so  basely  groundwl,  so  f4>olis))ly  r**eeiv<?d,  and  so  grossly  mis- 
taken in  th(.'  rij^ht  use  thi^reof  *'  A  custom,  loathsonie  to  the  eye, 
hateful  to  the  nojte,  harmful  to  the  brain,  dangerous  to  the  lungs,  nnrl 
in  the  black  stinkini;  fume  thereof,  nearest  resembling  the  horrible 
Stygian  t<moke  of  the  pit  that  is  botUimless !  * " 

Customs*  duties  art:  — 

Unmanufactured,  stemmed  or  stripped,  35.  per  lb. 

„  unstemnicd         -         3x.       „ 

Afanufacturcd,  or  Cigars       -         •         9f.       „ 
Snuff  -----         6<,       „ 

And  5  per  cent,  on  all. 
Stalks  and  flour  of  tobacco  prohibited. 

ThcTC  were  entered  for  home  consumption — 


!■  IIS4. 

rsiuA. 

In  Hliw  VMite 

■rflKM. 

Sinnrnfil       .... 
Unab'mmMl  .... 
Manantrtured  «tul  «nuff 

lT.030.fiST 

»,anrs40S 

3I9.&U 

ii.ri4.7n 

m.flis 

624  OPIUM,   AND    ITS   ADCLTERATIOXS. 


OPIUM,  AND  ITS  ADULTERATIONS. 

We  liave  in  the  present  article  to  tietai!  the  results  of  an  extminitiJi 
of  numermis  samples  of  opium,  one  of  the  most  iin|ior1ant  anidc! 
contained  in  the  whole  materia  iiietlica. 

The  substiince  known  ua  opium  'i$  the  milky  juice  of  the  lawuU  •» 
seed  vessel  ofjHtpuner  sontnifernm,  evn|>ornt«l  and  in«pi<t^t<^  hTti* 
posure  to  the  nctioit  of  li*:hl  iind  ulr,  during  which  it  acquires  it*  tloi 
t'oloitr  Hnd  piimmy  consiatenc^e. 

The  opium  poppy  ia  iin  annual  herbaceous  plants  atlAlolBg  AbB|tt 
iisuully  from  fuur  to  six  feet;  there  iiro  two  well-inai-ke«i  \Bh«t«t  «f 
it,  und  wliich  by  nonie  botauiMs  arc  even  oonAicliTeil  to  be  divUDCl 
speeies  —  namely,  tin:  bfuck  and  ihe  white.  By  i'&r  the  larptftproiv- 
tion  of  the  opium  of  commerce  is  obtaine<l  Irxtiii  the  Inttcr  »r  vmtt 
variety. 

'Jh«  lilnck  varit'ty,  ptipiwer  nomtti/trum  niffrumj  derives  its  aaoK 
(rnm  llie  colour  nf  it,s  see<ls,  whii-h  are  hhu'k. 

Tho  linhiiat  of  the  opium  poppy  is  Asia  and  E'^rpt,  but  it  ii  «ci» 
aionnlly  fimnd  growing  wild  in  some  parts  of  Kngland,  haviasivth 
bably  escaped  from  gardens  in  which  it  ie  l'rei|ut.'ntly  growm  nt^ 
sake  of  its  tlnwurst.  It  i*>  cultt\-ated  for  the  piirpofses  of  coanwrot  ia 
Uiudaytan,  Persia,  Asia  Minor,  including  Turkey,  and  in  lif^lp^ 

AeconUiig  to  Dr.   Uoyle,  the  bljck   variety  i»  cuUiTatwl  io  4« 
IliiualAVii*!.     In  Kuropi*,  the  opium  poppy  is  likewise  ir^wo  lo  as 
cxtL-ni,  but  for  different  purj>o9c-4 —  nnmely,  for  the  aakc  of  tbcoi^ 
sulcs  or  poppy-beads,  and  its  i^eeds,  which  yield  a  sweet 
oil,  much  employed  in  pniniin>!  and  wntch-DiakiDf?,  m 
ilti  being  legs  liable  than  other  oiU  to  oxidise  or  to  become 
Lundnri  market  is  chietly  supplied  with  poppjr  heacU  friHn  ihc  noigb 
biiurhood  of  Mitchum  in  Surrey. 

Puppy  beads  or  cflp5ulc5  are  ordered  in  the  I^mdon  and  DuUb 
Phannacnpa'iaa  to  be  ;:alhcred  when  quite  rip*',  while  the  Edi 
Collejre  directs  tliera  to  be  collected  whiUt  &tilt  ininrnturv,  2a 
state  lliey  are  murh  mt»re  active.     A  dL-cociion  of  iS.-  drit^l 
capsule  is  rendered  brown  on  the  addition  of  sesijuii  !  n«. 

owing  to  the  formatinu  of  a  meironate  of  iron  :  while  »      .  aiai 

8  slightly  orange  tinge  is  developed,  indicativa  of  tbe   pravEBM  iC 
mor{mia. 

Structure  of  ihe  Poppy  Cuptule, 

Since  tbe  poppy  capsule  is  employed  somewhat  fxtcnsirelyv 
wilt  np(}ear  hereancr,  in  the  adulteration  of  opium,  it  wiU  be  "^ 
to  dcscribti  its  minute  organisation   or  intimate  ■traoliir^  •• 


raacid. 


J 


OrtUM,   AND   ITS  ADULTEUAT10N8, 


«2S 


by  the  microscope;  uo  that  the  ohserrer,  in  subjecting  ony 
Munple  of  opium  to  a  niiernscffpic  exsniiimtion,  mny  be  uble  rendily 
to  identtfr  tlioae  tiMues  frequently  contained  in  it  wliich  are  referubic 
to  the  poppy  cnpaule. 

The  poppy  capsule  U  of  a  ninrc  or  less  plobone  or  ovntc  i^lohove 
form,  it  varies  in  size  from  a  hen's  egg  to  an  orange,  »nd  is  of  a 
light,  spfingy,  end  papypiicetius  texture.  It  is  one-celh'd.  conMir^ting 
fif  numcrniis  earpeU  endofted  in  a  membranous  prciiueticin  of  the  tha- 
lamus, uud  furnisIiL'd  with  pliiirentte,  wiii<-h  form  di^sepime^t5  in  the 
interior  uf  the  ciip<<ulc*  tlte  number  ami  ]>osiiion  of  which  correspond 
with  the  eavpels.  Thin  sections  of  the  ^xtvrnal  lurface  cf  tbo 
cftp*tulL',  examine*!  tmder  the  nuLTnsrope,  are  »een  to  hn  composed 
of  small,  an;»ular  cells,  hnvin^f  exceedltijjly  well-marked,  broud  walls 
or  parictes,  wirh  here  and  there  a  few  rounded  stomnta.  It  U  ncce!<- 
gary  that  the  microscopic  examiner  shuuUl  lie  tlioroujihly  acquuiiiCiKl 
with  this  structuref  ^iitce  it  is  chielly  the  cxtemnl  portiun  of  the 


Fig,  I». 


rattloa  •#  Um  €rUr»nl  miHmw.  'f*^^'!*^  "f  *^  Porn  CArvrLc.    Dnwa  wlUi  Um 


capsule  which  enters  into  the  adulteration  of  opium.     The  resem- 
Uaikce  uf  this  membrane  to  the  celh)  of  the  membrane  forming  the 

8   8 


OPITM,   AND   TT8   ADULTERATIONS. 

surface  of  the  jfrain  of  wln-at  is  vt*rj  ;:real,  «o  that  a  person  migbt 
ensiW  inistiike  tlie  one  lor  the  ntlier.     fig.  191*. 

The  slructure  of  llie  niembrnne  which  lines  the  interior  of  the  cap- 
sule, and  which  is  s*itunt*'(l  hctivei?n  the  dissepittienls,  is  very  •iifTerent: 
it  conBists  of  very  lar^c  cells,  of  an  eloripiteil  and  irri.*2ular  fonn,  but 
mostly  becominjr  narrow  towni*ds  either  extremiiy ;  their  pariere^  xrt 
very  thick,  anil  beoled  ;  this  iiicmbrnnc  is  iiUo  furnished  vrith  a  few 
»nguUr  sluuiata.     Fig.  200. 


Fit  aw. 


VortiuN  of  uMn-MulMCof  Ibc  rorrr  CAP*uui.nMfiKai3n.    MasBUhMinr) diun^i^f^ 

Tn  loncitiidiiinl  sections,  pnfisin^  throiii:h  the  entire  thickness  oftlM 
capsule,  weohtnin  a  side  view  of  the  cells  'n'hich  form  the  outer  And 
inner  portions  of  the  cupsulc,  the  space  between  the  two  being  oom- 
poM**]  of  a  hiose  and  open  cellular  ti.<ijue,  whiuh  iinpaitH  the  sponn* 
ncsii  to  the  capsule^  anU  wliich  i$  traversed  here  and  there  with 
bumllea  of  dotted  ductn,  spiral  vesHub,  and  woody  fibre. 

The  Htriiclure  of  the  diBt^jumcnt?  or  pluceutje,  aj;uiii,  differs  ent4relf 
from  thiit  of  the  internal  wnll  of  the  ciipsule.  The  surface  of  each 
disaepiuieul  ou  both  »idcs  presents  nuuicroiis  dark  points  or  ^peck*: 


OPIUM,   AND   ITS  ADULTERATIONS.  e«7 

these  consist  of  short,  ruJscd  projoctions,  sperinopliores,  each  of  which 
originiUjr  guvs  vup(>urt  to  a  distinct  AUtui,  whiuh  iix  the   ripe   cap- 
Fur.  901. 


Fortloa  of  mrfK*  of  otM  of  th«  placaMr  at  dit^fpim^wiM  at  0\*i  Turn  CArntftM. 
•howtogobt  of  th«  apmno^lMnM.    M«cnU)c<l  flit  and>W«Uunc(cn. 

9ule  is  found  to  be  usiinlly  detached.  Those  portions  of  the  Kurfaoc 
of  the  dissepiment,  lying  between  the  spermnphorea,  aro  made  up  of 
celU.  whii'h,  thouj^h  riiher  hirgc,  arc  aiurh  smaller  than  those  form' 
ine  the  internal  surface  of  the  cjip»ule;  thev  are  somewhat  elongated, 
Iteing  usually  nurrow  at  each  end;  their  margms  or  parietes  are 
doited,  and  there  are  no  btomata ;  the  s|)eruiophorcs  or  projectioiu 
supporting  the  secd»  are  composed  of  simibr  cells.     Fif;.  201. 

In  transverM!  section*i  of  the  diwcpiment  viewed  with  a  two-inch 
object  glniM,  the  projections  or  sperniophores  aru  well  (teen,  as  also  the 
manner  in  which  the  iiceds  are  supported  and  dititributed.    J''ig.  20*2. 

In  sections  uf  the  !<ame,  viewed  with  a  hull-inch  objeet  glaas,  the 
intimate  structure  of  the  dissepiments  may  be  fullKwed  out.  The 
central  or  9pt>ngy  piu-t,  which  swells  greatly  when  inimeniL>d  in  water, 
con^ints  of  tubular  cells  running  in  uU  dir<.*ctions,  so  airuuged  as  to 
leave  considerable  interstices  or  areolie   between  them,  together  with 

§  a  '2 


«Jt  OPIUM,    AND    ITS    APULTERATIOKg. 

bundles  of  woody  fibre  and  vessels,  one  of  which  bundles  passes  up 
through  the  centre  of  each  spcrmophore.     Fig.  200, 

Fig.  K7. 


IVaww'ai'M  mMoo  throqeh  thu  (NkktiTM  of  &  dt<*ephn«at  of  Pt^rrr  C«r<tt-t.r, 
•bowlnf  ihr  t{«nnnplinrei  with  the  •vwl  atUeihcd.     Mx^nlflnl  in  diunctcr*. 

The  Structures  which  enter  into  the  composition  of  the  popper  wc\i 
are  shown  in^^jr.  303.  and  304. 

Colifction  of  Opium. 

The  process  by  which  opium  is  obtained  from  the  poppv  capsole  is 
»irailar  in  principle  in  all  countries  although  subject  to  various  mcxti- 
fi cations ;  it  consists  in  making  incisions  inlo  ibe  hnlf-ripe  capsulei^ 
and  in  collecting  the  juice  afler  it  has  becitmc  hardened  and  darkened 
an  colour  by  exposure  to  air  and  light,  Mons.  C.  II.  Texi«T  •  thu« 
*  Jhih,  de  Phjum.,  tnU  IK. 


OPIUM,   AND   ITS  ADULTERATIONS. 


est 


describes  the  proccHs  <if  obtaining  opium  followed  in  Asia  Minor :  — 
*'  A  few  iiaj'8  aftur  tla*  iWwer  biu  tuLIuu,  laeu  aiid  women  repair  Cu  the 


•MtiAO  of  diNt^lmciU  0/  Pom'  CMfVPlMt  •tiowinf  twouf  Uu  tiKUiiM- 

fieldii,  and  cut  the  head  of  the  ponpv  hnrizontnUy,  takinfr  rare  that  the 
incisions  do  not  penetrate  the  internal  cuvit^  of  the  ^heJl.  A  whiti* 
Hiib(>tance  inimediutolv  floivs  i>ut,  iiml  c«iltt^rt»  in  teurs  on  the  edges  of 
the  cuts.  In  ihtBaiulu  the  iield  i^  left  fur  twenty-lour  hours,  and  on 
the  following  du}*  the  opiuui  is  collecteil  bv 'urge  blunt  kiiivc».  Each 
head  furni&ht,**  upium  unee  only,  and  that  to  the  extent  of  ti  few 
finiinti.  Thus  collorted,  opium  hiiA  the  I'onn  of  a  nlutinoufl  and  grn- 
nuhir  jelly.  It  ia  defio.-titfd  in  sntull  curthcn  vessels,  und  beaten  up 
with  saliva.     When  oijkcd  why  water  woa  not  employed  in  place  of 

a  ft  3 


630 


OPIUM,    AND   ITS   ADUKTETtATIONS. 


sulivttt  the  answer  was  that  water  caused  it  to  spoil.     It  ic  aftcrwai 
enveloped   in   dry   leavot^  and  in  this  state  it  is  sold.     The  see<l 


Fur.  3M 


Frmfmcat  of  Forrr  Rrxn.  ahnwlng  pnrtloiu  of  thr  itirtw  m^mbrkDM  which  eonpoM 
tbfi  bojk  af  arrtl,  ■■  wett  u  the  cell*  eontalninf  Lh«  vU  lii  gliibulw,  which  &rtn 
Uw  nibitanee  of  ttut  •ccd  iUelf.     HflCniCeil  IM)  dlKrucUn. 

ihoae  poppies  which  have  yielded  opium  arc  equally  good  for  sowing 
the  fidlowmg  year." 

In  Persia,  according:  to  Ktempfer,  the  incisions  are  m»de  crosawiae 
hy  fk  tiiie*ed}:ed  knife;  while  Kerr  slates  that  in  tht*  ftrovince  a( 
Bc'hur  **  two  longitudinal  double  incisions  are  made  iipnn  eacli  haU- 
ripe  capsule,  postiin^  from  beh>w  upwards,"  rare  being  taken  that  tht 
internal  cavily  of  the  capsule  be  not  penetrated. 

A  Tery  interesting  and  impurtant  account  of  Uic  cultivation  mod 


OPIUM,   AND   ITS  ADULTERATIONS. 


6Sl 


mnnufacture  of  In<linn  o])imn  has  been  published  hy  Dr.  Eotw*?!!,  mid 
friMu  which  we  much  regret  that  our  vpace  (iues  not  ptniiil  us  to 
qiKitt?  ]ari,'el)-.  A  Ion-'  abstract  of  the  cnnmiitniration  refcrre*!  to 
will  bi*  Ibund  in  the  author's  Ueport  un  Opium  puhlnbed  in  "The 
Lancet." 

Anuly$u  of  Opium. 

Thf  iinite<l  Ubours  of  varidu.t  eliemUtii  have  shown  timt  opium  in 
line  of  the  ni(>?t  complex  of  vegetable  7ubstuueea  with  which  we  are  at 
prewDt  aequuinteil.  To  give  anything  like  u  cumplute  aeeouiit  of  the 
luiulysis  of  opiufUf  andof  ihe  labours  which  huve  bi^en  bestowed  upon 
it,  would  itself  occupy  a  volume;  we  must  therefore  cuntent  uuraelvea 
with  ?>iich  a  description  of  the  eoni|>t>9ition  of  ihal  drug  as  iia  necessary 
to  enable  the  inquirer  to  ascertain  tor  hhiisetf  its  strength  iind  ])urity. 

Cbeniisis  have  succeeded  in  detecting  in,  itiid  isolating  Ironi,  gum 
opium  the  following  active  principles  and  conflittucnts  : — morphia^ 
uarcotina,  cndeia^  rtarceta,  mvconinc,  thehia  or  paramorpbin^  psewiff 
mtfrphia  ?  mecomc  aciti^  brnint  acitl  rj^tractive^  Jtuiphunc  aclil^  reshi^ 
fat,  oil,  gummjf  uuitter,  caoutchmic^  iilhumen^  (ttiorom  priticijtie,  (volatile 
oii  ?)  and  li^iuu ;  to  thcae  uiav  be  added  another  suhsLtnce  not  in- 
cluded, so  lar  as  we  ore  aware,  in  any  of  the  anulvftes  of  opium 
yet  given^  alihough  it  is  fre4[uunlly  couta'ineil  in  it  in  large  amount; 
we  refer  to  glucune  or  grape  sugar. 

Of  the  more  aclive  principlL'ft  of  opium  the  most  important  belong 
to  tho  class  of  alkaloidft,  as  morphia  and  lu/reohua,  and  furm  buses; 
while  others  readily  unite  with  oxygen,  and  play  ihc  port  of  acid^, 
soDicuf  which  enter  into  conibinuliuu  with  the  allialoiil».  'Vha  muiit 
complete  analyses  of  opium  which  have  as  jret  beeu  published  ure 
those  by  Mulder,  Sebiudler,  and  tiilu. 


1.  Morphia 

2.  NdrriHiDJi 
a.  CwUli 

A.  NarcHne 

5.  M«c(intiM 

6.  MccoDic  •ckl    • 

7.  K« 

A.  ra'-uU-houe      - 

V.  Kvtiii     • 
ni.  Giimrn*  r&lradve 
II.  Cuni      - 
IlL  M'Kua  - 
13.  Witter   • 


T«tal 


teftM0|4«. 

10^1 

A-m 

o-Ma 

1-M3 

S-MO 

6tMI 

SIM) 

0-360 

7/t» 

(>*M6 

0-OTS 

(IM4 

0-MB 

0-8SS* 

0-cso 

fi«n 

TVif. 

7-6ai 

9  903 

ia"j40 

Oi«M 

OM6 

0-31 1 

|>-M0 

0-WM 

ftlM 

!■»« 

7  6W 

Tiht 

6-f»l 

IIW 

13X1 

l-fllfi 

4-«M 

i-Mm 

6fll7 

5  (r>. 

3  671 

a7S4 

3106 

a>w2 

XIW 

Ml* 

M-O" 

I'lHH 

iB-tOO 

JUTfl 

SI -Ml 

»c« 

23-740 

l-Ml 

3A96 

IrlJM 

I'J'.ih 

0-890 

I9V« 

17  VJ** 

ai-w»« 

IviliS 

is-osa 

»N«fl 

HlV. 

II  471 

I1IM4 

14  on 

100«00 

a-4»6 

(COM 

9-sn 

OO-tRiS 

lOODon 

10(KOOO 

«  Phiira.  C«ntnil-BUU  fOf  tUT,  t.  674. 

B   9   4 


H^^^^^H 

^m                           6S9                    OPIUM,   AND    ITS    ADULTEUATTOXS.            ^^H 

^m                                                                     SchindlerM  Anaiy§t4*                             ^^^^| 

-«ji 

Morphia      -             .             .             .             . 

uSST*^ 

sssr 

10  M 

450 

T-OB 

NuTutlna    ..... 

1*30 

a-47 

Itt 

Codttta         ..... 

(1-35 

oaa 

NiTcdne     .              -              -              .              . 

0-71 

(I-4V 

Hccoiiine     ..... 
M«contc  acid               .... 

<-70 

010 

4-3A 

I 

Itriln             ..... 

lOM 

•  10 

Ila.fortn.  r«Dvtchow,  ru,  Uid  Kfnln     . 

aeas 

17  lA 

S»IU  ami  volatile  oil - 

z-m 

»-f« 

V    n-a 

Lime  and  miiKiir«iii    -                .                 •                 . 

047 

t4» 

Alumiua.  cxi.eof  Iron,  silica,  and  phoiphale  of 
hmw          .               -               .                .                . 

(^S< 

0-M 

I 

Bro»n  acM,  solublr  In  attnliti)  ami  wairr 

1  IH 

0-4O 

Urowu  acid,  toluble  id  waicr,  gum,  and  low 

49  la 

66  «» 

Toul        -               -               .               - 

100*00     1     loo-uo 

BiUz*s  AnahjKt.^                                      ■ 

iMlilt-MtM  Ctptum. 

Orivnial 

OlMMk 

frtmt 

rroM 

Morptita    .               .               •               ■               - 
>*arcoUna                 .... 

*KWniin 

f*  **>^^ 

9W 

rao 

aooo 

■ 

Mrronio  tuciA  (Impure) 

1*7.1 

\tift(l 

i^H 

m 

Bltt«r  fUtraciWp     .               -               -               - 

3»-(iU 

A-50 

*^H 

M 

Drpoiit     ..... 

T-7S 

4-75 

f^^H 

m 

Albumrti  ..... 

10-f* 

irM 

(f^H 

m 

Bali^inlc  matter     .... 

UK 

7-eN 

^^^1 

m 

CAuutitiai-r             .... 

tm 

10  Ml 

J^H 

I 

Cum,  «lih  hioe      -               .               -               . 

lis 

OK 

^^H 

<■ 

Siilphnl"  of  pniash  .                ... 

■i-'fi 

9-aa 

'^^H 

I.iini'.  Iron,  aliimioA,  and  phosphoric  acid 
\V<KMl)i  libra            .... 

3-7IS 

D-80 

^1 

Animtiiiia,  (otallteuil,  aitd  loaa 

Total     -            *            .             .. 

3H)0 

I-IO 

f^l 

10000 

imao 

l«Mi 

I 

Of  the  numerous  constituents  of  opium  it  is  only  nece^ary.  fq^l 

purpo-ie  we liuve  in  view» — nuuitly,  iLt-  Uftee-lion  of  »iciullernti».ii,^r^ 

we  ^lioultl  be  ncquaiiiied  with  ihe   pri^j 

crtics  of,  uiitl  methods  of  i^ 

luining,  uinrphia,  nurLoiina,  and  mcciui 

^l  acid.                                    ^H 

Morphia  exi»t&  in  o]>iuni,  eliiell)*  in  c-tuubinution  with    mcconl^H 

•  PUam).  rriittal-Bljitt  flir  \^M,  t.  7IM.                                      ^H 

t  I'horm.  Leou^UBUtl  liif  ll»31.  ».  7V7.                            ^^^H 

OPItm,    AND   ITS   ADCLTERATIONS. 


631 


fulphuric  acids.  Vure  morpliia  presents  iUilC  in  the  form  of  tmna- 
parenr,  right  rhnmbic,  priMiiatic  crystals.  It  has  an  alkaline  rowtion^ 
OS  shiiwn  by  tnrm<-ric  nnd  reddenvd  litmus  papers;  it  is  nearly  in- 
boliibte  in  cold  water,  to  wliiib  it  imparts  a  degree  of  bittenicari; 
boiling  water  di^isolves  n  little  more  tbun  one-hundredth  part  of  niur- 
pbitu  It  in  soluble  in  forty  parts  of  c«<td  absolute  alcohn).  and  thirty 
parts  nf  builin<;  ak-ohtjl,  but  ic  is  insotublef  or  nearly  so,  in  etiier.  It 
lA  soluble  in  [heoiU(n.\ud  and  volatile),  in  solutions  of  s<Kla  and 
jKitasb,  and  ulso,  but  in  uiueh  smaller  cniantity,  in  solution  of  am- 
nuiiua  i  lustly,  it  readily  dissolves  in  sulphuric,  hydrochloric^  and 
acetic  arids. 

Tiio  Dublin  College  now  ailmits  morphia  annmcst  its  pharmaccuticai 
preparations.  It  directs  the  morphia  to  be  preuipituced  by  the  addi- 
tion of  ohlnride  of  ealeium  to  a  concentrated  aqueoui  infusion  of 
opium  ;  the  precipitate  is  dl.^^olved  in  boilin;;  water,  and  a  slight 
exce!>.«  of  solution  of  ammonia  added  ;  the  preeipit4ite  which  is  now 
thnmn  down  is  to  be  collected  and  washed  with  distilled  water,  and 
finally  dnei). 

'I'lto  followin<r,  perbapSf  is  on«  of  the  liest  methods  of  obtaining 
moriihia  in  a  state  of  purity;  it  is  a  nit^dificntion  of  the  proci'ss  re- 
cininiK'nded  by  Thiboutnary.  To  the  watery  extract  of  opium  solu- 
tion of  nmmonia  is  ti»  be  added,  care  being  taken  that  it  is  not  in 
excess;  the  precipitate  thus  thrown  d<iwn,  after  being  washed  with 
water  nnd  proof  Fjurit,  is  to  be  builed  with  animal  oharcotil  nnd 
rectified  spirit;  the  «olulioo  is  to  be  61tertMl  and  evaporated,  by  which 
means  mui  phia  in  crystals  is  procured.  The  mor|>lua  obtained  by  ihu 
above  prtness  is  n<it  alisolntcly  pure,  but  contains  nanotina,  which 
nmy  be  thus  got  rid  of: — AlYcr  the  pretMpitate  on  the  filter  has  Ijeen 
wa.>^hcd  with  water,  dried,  and  mixed  with  proof  sntrit,  nceiie  acid  is 
to  be  added  tlrop  by  drop  until  the  solution  slightly  reddeivs  liimus; 
the  morphia  will  be  taken  up,  but  not  the  nareutina  ;  the  former  ts  tu 
be  n^ain  precipitated  by  ammnniu. 

Mnrphiuand  itssnltsarercildencdby  nitric  acid,  with  which  they  form 
an  orunge-red  solution  ;  this  is  darkened  by  adding  excess  nf  amntonia, 
but    becomes  yellow  aft^r  a  time.      Neutral   sesquichloriile   of  iron 

rnured  on  morphia  retidors  it  blue,  as  also  its  salts  if  concentrated. 
f  un  excess  of  water,  or  acids  or  alkalies,  be  adtled  to  this  blue  com- 
pound, the  c<»lour  becomes  destroyed.  The  most  delicate  lc»t  for  the 
pieitence  of  morphia  or  iu  salts  is  chh>ride  of  gold,  the  ndtlilioii  of  a 
lew  drops  of  which  to  the  solution,  thrown  dnwn  a  yellow  precipitate, 
which  i«  re<lisftolvc<l  on  shaking.  If  &  little  litjuur  pHassie  Ik;  nnw 
ad'led,  it  be<'omes  tirst  greenish,  then  blui*h  violet,  and  lastly,  purple. 
Narnttiau.  —  The  greater  port  of  nureotina  i«  suid  toexi^t  in  opium 
in  a  free  »tute,  aa  it  la  removable  by  ether  without  the  aid  of  either 
acids  or  alkalies.  The  properties  of  nnrcoilna  do  not  appear  to  be  us 
yet  fully  and  aalisfacmnty  determined;  but  there  is  reason  to  believe 
that  in  tt«  pure  btate  it  is  pcnsesscd  uf  but  little  activity.      Dr.  Hoots 


OPIUM.    AND    ITS   ADULTKKATIONS. 

adtninint^red  it  in  dofcn,  gradtiAlly  iiicreued  to  ascnijJe,  without  aay 

ill  constMjueiictfs  ensuing;. 

Narcotin.i  i»  di»«tntved  by  nitrio  acid,  with  wlitch  tt  foruts  an  oranjE^ 
cciluured  solution,  an<i  U  turned  vellow  by  sulphuric  acid.  Vege- 
lablc'  colfiura  are  not  affiHted  by  it.  by  which  il  is  easily  dislin- 
guishtnl  from  morpiiia.  It  does  not  di&.-<ulvc  in  cold  water,  but  \i 
fohiblc  in  400  parts  of  boilincr  wutLT ;  cold  ulcobul  takes  it  up  apar- 
iig'/i  but  it  dissiilvcs  in  tWL'nty-futir  parts  of  boiling  aluuhol ;  it  b 
Itke^ri^e  sululih;  in  ctlier  iitid  rbe  vnbitile  oils. 

Mccojiic  Avid.  —  Til  is  h  usually  j)repitrfd  by  heriling  meconat«  of 
lime  in  hot  wntcr  wlih  lijdrnLhlorie  arid,  wltirh,  on  rnnlinjr,  de[io9it5 
erystuls  of  meiMmiL'  atid.  When  pure,  it  occurs  in  while,  trunspareiil 
miwit't'oits  scales,  wliich  are  Knluble  in  (nwr  times  their  weijfht  of  bt«l- 
ing  water,  but  at  this  tcnipcrulurt^  water  deci)nip"scs  it.  ilolii  wotef 
disholve.-*  u  Hmidlcr  qiianlity  of  inccunic  acid,  but  it  is  entirely  soluble 
in  alcohol. 

Mfconic  aoid  reddt-ns  the  neutral  {ie5(]uisalt^  of  iron,  furminff  me- 
oonnte  of  sesquioxirlu  uf  iron;  but  tit i-*  red  colour  is  destrovetl  ly 
alkalies,  prot<"eliiorido  of  tin,  and  nitric  acid  aided  by  beat.  An»- 
munio-sulphate  of  copper  throwH  down  a  ^reen  precipitate  (mcomuu 
of  copper),  and  it  furniithcft  white  iirecipitaios,  which  are  soluble  is 
nitric  acid,  with  m-etate  of  h>ad,  nitrate  of  silver,  and  chloride  tt 
barium.  Mci-miirui  id  i»not  rcddeni'd  by  chloride  of  gold.  It  $hoa)*l 
be  remembered  ihaC  ihe  acetatof,  siilphnrynnides,  and  ^ome  otbtrrtuI>- 
Btanees  eijuully  with  meeonic  uciil  pa^JieKS  theptjwerof  coDiniunicatilg 
a  red  colour  lo  the  ^e>'qiiii'tiUi4  oi'iiun. 

^'(ir  a.  furthtT  nceouiit  of  ihe  ehnrncters  ami  propertied  of  the  f»- 
inaintng  constituentfl  of  opium,  the  remler  ia  rffcrrcd  to  the  cn»* 
eluding  part  of  llie  third  edition  of  Pereira's  '*ElemenU  of  >iAt«i« 
Medica." 

Varietie*  of  Opium, 

Several  varieties  of  opium  arc  imported  into  this  country,  and  art 
met  with  in  commerce.     Of  these,  the  foliowinp;  arc  ihc  principal:— 

Smyrna,  'I'itrket,  or  Lkvamt  OnuM. — Thin  occurs  in  irrvguUr, 
rounded,  or  tt.itteneil  nuiflseH  of  various  sizes,  hut  rarelv  excee<lin<{  tve 
pounds  in  weijiht,  enveloped  in  leaves,  and  with  runiex  carK*<ules  ad- 
Iierinj»  to  the  surface;  some  of  the  (lat  cakes  are  not  furnished  with 
capsuleft,  mill  in  ihia  state  somewhat  reiienibk'  ConntantinopW  opiun. 
Wneii  lirst  imported,  the  masses  nre  sol't,  und  of  a  i'e(ldisli*browii 
colour,  hut  by  keeping  they  become  hard  »nd  blackioh ;  il  breaks  witk 
a  waxy  lustre;  its  o< lour  is  strong;,  it^  tiute  bitter,  acrid,  tinuaeoui. 
and  fHfrsist£nt.  M.  Guilmurt  considers  the  masses  to  bu  made  up  crf^ 
af!>:lutinutcd  ^anules  or  tears,  and  he  rei/aid?  this  cliaraetcr  as  n  left 
of  purity.  It  viebis  more  viorphia  und  mfconic  acid  tbtin  either  Con* 
stantinople  or  ^gvpii^n  opium;  the  average  quunlity  of  morphta  ob- 


OPIUM,    AND   ITS   ADULTERATIONS. 


035 


tainable  in  from  it  is  about  eight  per  cent.  The  narcotine  muv  l>e 
estiinatc'il  at  soiiiewbere  about  four  per  eenL  Murck  *  oxaniine<l  five 
kindii  nf  Smyrna  opium  ;  from  the  worst  he  obtained  three  to  four  per 
cent.  r)f  morpliia ;  from  th«  bejit  Kl  to  13*5  pr.r  cent. 

CoNSTANTMopLfc  OpiuH. — Of  tbia  Icioil  of  optum  Professor  Guibourt 
»lvi?s  the  following  description: —  "There  are  two  sorts  of  it — one 
III  very  large  irrej^Inr  enkcit,  whirh  are  flattened  like  the  Smyrna 
opium  ;  ihii*  is  of  wry  ^"od  (pndily.  The  oilier  Ja  in  small,  flattened, 
ri'iliilar  cakes,  «f  a  lenlicular  funn,  front  two  lo  two  inches  and  a  half 
in  diameter,  and  covered  with  the  poppy  leaf,  the  median  mrves  of 
which  divitle  the  disk  into  two  parts.  It  has  nn  rulnur  Himiliir  to  the 
precedinjf  kind,  but  more  (eeble;  it  blackens  and  dries  In  the  air.  It 
18  more  muciln<!innus  than  Smyrna  opium.**  The  cakes  arc  never 
covered  with  rumcx  capsules.  Constantinople  opium  i»  inferior  to  the 
Smyrna  kind,  but  superior  to  the  Kgypllnn  opium.  Guibourt  states 
that  it  yields  only  hulf  the  morpliia  procurable  from  Smyrna  opium, 
but  it  furnishes  more  morphia  than  the  Kgyptiau  opium.  This  state- 
ment does  not  agree,  however,  with  the  experience  of  Mr.  Duncim, 
of  Edinburgli,  Dr.  Cbrislison  and  Merck,  all  of  whom  obtained  very 
large  quantities  of  hydrochlurate  of  niorfihia  from  it ;  these  ddfcrences 
probably  depend  upon  the  uneniial  <|uality  of  the  opium  produced  in 
various  portions  of  the  TurkUh  emjiire,  an<l  which,  being  exported 
from  thence,  bears  the  name  of  ConstanUnopIe  opium. 

KoynrMTf  Oi'iuM.  —  It  occurs  in  round  dnLteneil  cakes,  of  about 
three  inciies  diiimeler,  covered  externully  with  the  vestiges  of  some 
leaf;  it  is  ustually  very  dry  ;  it  is  diKlin^uished  from  the  two  preceding 
varieties  by  its  reddish  colour.  unah>x»us  U*  that  ol'  Socotrine  nr  he- 
patic ahtes.  Some  very  inferior  qualities  nre  sometimes  offered  for 
sale,  and  which  np]>ear  to  the  sight  and  touch  to  he  larjjely  adulterated. 
It  does  not  bhickcn  by  keeping,  and  iis  odour  is  less  stronr; ;  by  ex- 
posure to  the  air  it  usually  becomes  sotl.  £<;vptian  opium  is  for  the 
most  part  inferior  to  either  Smyrna  or  Constjmtinojtle  Dpium,  but  its 
strentrih  and  quality  are  not  uniform.  Guibourt  states  that  it  yields 
only  five  sevenths  of  the  morphia  procurable  from  Smyrna  opium; 
tlie  murphlu  obtained  ie  purified  with  ^eiit  ditficulty.  The  watery 
infusion  ot'this  opium  possc>ses  a  distinct  othmr  of  atetic.  acid. 

TftEBizoNO  OK  Pkrsian  Opiiim.  —  Somc  years  sinc^-  a  quantity  of 
this  opium  was  imiMtrieil  into  this  (K)uniry  from  Trebizond.  It  was 
in  the  form  of  sticks  renilered  somewhat  angular  by  pressure,  about 
■ix  inches  long,  and  half  an  inch  in  diameter,  enveloped  in  suuHith, 
shiny  puper,  und  tied  with  cotton.  Its  colour  is  similar  to  that  of 
Socotrine  aloes ;  its  odour  i<  stronger  than  that  of  the  Egyptian  kind, 
but  less  than  Smyrna  opium  ;  it  ii  very  inferior. 

InoiiN  Opium.  — There  are  three  varieties  of  this  kind  of  opium 
met  with  in  commerce,  under  the  names  of  Maiwti,  BenarcM,  and  PaiJUt 


*  Fharm.  Ccolral-BUtl.  36. 


636 


OT'JUM,    AND    ITS   ADULTERATIONS. 


opium  ;  the  \f\nt  two  ate  not  to  be  distinnuiahed  from  each  other,  ami 
mar  bo  iiirluiiiMl  under  the  nno  heud  of  Bena;:il  opium. 

Rengal  Opium  is  brought  into  this  oountpy  in  bolls,  each  of 
lliivc  and  a  halt'  pounds  in  weigin ;  ami  which  nre  packed  in  chest 
v&cli  htiliJin<;  nbout  forty  bnll^.  They  are  hard,  glubular,  and  aboutj 
OS  lur;!e  as  u  chilli's  head.  TUe^v  iire  conted  externully  with  the  |>euU 
of  the  puppy,  fusteited  together  by  uieuns  of  a  paste  calle<l  IriniM; 
this  covering,  tliough  disposed  in  layers,  is  6rm,  and  wei;>b8  about 
fourteen  nunres.  On  removing  this,  the  opium  iu  finnnl  to  be  of  tin 
cotisistence  of  a  soft,  bomor^cneous  extract  of  a  blackiuh  brown  ciiluur: 
its  odour  and  taste  ure  stron;^,  and  it  rapidly  huconics  inoubW  on  e&- 
f>ostire  to  air.  Benares  and  Patna  opiums  are  exportcil  fi'oni  Cideutta; 
the  former  h  mn«t  esteemed  by  the  Chinese.  Dr.  Suiytttin  *  procured 
(•Illy  '^ft  or  3  )K'r  cent,  of  moi'phiu,  from  Uen^al  opium;  but  it  W 
Vjeen  e^liiuniled  l>v  Mr.  ^Inrsoii  that.  Uunares  opiuDi  contHiita  ratluff 
more  ihan  hjilf  the  cpianlity  of  niorphia  nmtaincfl  in  gotxl  Xurke* 
ifpium;  wliili',  from  a  table  jiiven  in  Dr.  KarwfU'a  work  on  Opium,  il, 
apnejirs  that  the  averaRe  quantity  of  ninrpbia  yielded  by  BeniMi' 
opiiiin  iu  the  seur^n  1845—46  was  2*48  per  ceni.,  and  of  nareotina,' 
5*26  per  eent. :  in  1846 — 47,  morphia,  2  38;  nurcutina,  452  i>er  ctou: 
in  1847 — 48,  nKir]>hia,  2'20;  nureutina,  5  68  per  cent.:  und  jo  ikj 
season  of  1848 — 49,  the  average  per  cent,  was  3'21  morphine, 
406  uarcutine.  The»e  reitultj^  show  tliat  Benares  opium  is  soiuewltfj 
deficient  in  morphia  but  rich  in  niLrcotinu. 

Garden  Patna  Opium.  —  This  kind  of  opium  is  Jmporte*!    in  »(ittart' 
cake.s  of  about  tlirec   indies    in  diameter  each  way   ami    one    iiwi 
thick,  and  wrapped  in  thin  plates  of  mica.     Profe>sor  Guibuurt  de- 
scribes it  as  "  Imvina:  the  ap]>enram'e  of  a  well-prepureii,  ehinv,  drf. 
pbarmaeeutieal  extract;  its  colour  ib  blackish   brown,  and   itaodkiiirj 
uoL  so  strun<;  as  that  of  Smyrna  opium." 

Mtiliea  Opium.  —  There  uru  two  varieties  of  ALdwa  opium.  Il 
was  formerly  considered  lo  be  of  inferior  quality,  but  it  is  ut  the  VK' 
gent  time  much  esteemed.  One  variety  consists  of  round  flaUeMi 
cakes  of  ubnut  ten  ounces  in  weight,  and  irt  jiacked  in  coarsvtv-po** 
dcred  {>nppy  petaU.  It  is  of  nioilcrately  firm  consinienee,  and  ofi 
homogeneoiiji  texture:  itji  colour  is  dark  brown,  and  the  smell  reseo' 
blei*  somewhat  that  of  Smyrna  opium.  The  other  variety  i«  met  will' 
in  flattened  cakes  without  any  uutuide  coatin;;;  exterindlv  it  is  o(ij 
dull,  opatpiK,  hl.ii'kish  brown  coKmr,  but  the  interior  is  soft  and  iImP* 
in  colour  ;  its  odour  i«  »nmewhut  similar  to,  though  nut  so  p<kwerrii 
as  Sinynia  opium.  It  yields  only  one  tViinl  the  quantity  of  morfikal 
tiirni!«ht>t|  by  Smyrna  opium.  Dr.  Smytten  obtanied  nikly  from  Jttj 
5  per  ci'Ul.  of  murphio,  but  from  liner  sunqtics  as  much  fls  7}  to  H  ya\ 
cent. 

Cuieh  Opium, — This  occurs  in  small  cakes,  rather  more  thanOtfl 


•  I'nuu.  of  th«  Med.  and  Phy*.  Soc.  of  Calcutta,  vL 


OPIUM,   AND    ITS  ADL ITERATIONS. 


6.17 


inch  in  diameter,  and  app<»ara  to  be  enclosed  in  fragments  of  leaves  ; 
its  cwlonr  ij4  not  fo  strtdir:  a?  that  of  Smyrna  opium. 

Knnfirixh  f)pi«m  is  imported  in  round  flatit-ned  rakes  fthnut  half  a 
pound  weight  enrh.  It  is  bard^  brittle,  nearly  hlnok.  and  breiiks  with 
a  grritly  or  prniiular  frneture.  Accordinj!  to  Mr.  S'lUy,  100  grains 
funiipht'd  7*2  «;rain5  of  soluble  matter,  and  alxmt  7  sraitis  of  nior]iliiM. 

Kngmsii  Opivm.  —  This  opium  is  met  wiili  in  flat  cakes  or  batls^ 
covered  wiili  leaves.  In  appearance  it  yiore  resembles  the  best 
Egyptian  opium  than  any  other  kind  ;  it<  colour  is  like  that  of  hepatic 
aliK's,  and  it  pfvssesses  the  peculiar  smell  of  opium  niodi-ratfly  stronjr, 
I'roni  one  sample  of  Enplnh  opinm.  Mr.  Ilennoll*  nbtainod  as  much 
fts  707  percent,  of  morphitit  while  from  'J'uikey  opium  he  only  pro- 
cured 70  per  cent.  Mr.  Morson  f  obtained  4  4  per  cent,  of  morphia 
and  2'fi3  of  narcotina  from  another  sample.  Mr.  Young  %  stales  that 
Hnjilish  (tpium  is  stronger  than  ordinary  commercial  opium,  six  ounees 
of  the  former  being  equal  to  eight  of  the  latter. 

Krb^cu  OrirM.  —  This  kind  of  opium  is  described  by  M.  Pellelier  § 
as  being  of  h  deep  retbiiih  brown  colour,  and  brittle  when  dry.  Its 
taste  wua  somewhat  ditferent  U*  that  of  Smyrna  opium  ;  it  left  a  less 
insoluble  residuum  than  Kastern  opium,  antl  he  procurmi  more  mor- 
phia from  it  than  from  Smyrna  opium.  In  an  experiment  on  abtmt 
two  ounces  of  each,  he  obtained  about  10  38  per  cent  from  the  former, 
and  only  7"08  per  cent,  from  the  latter.  It  contained  no  norcotina. 
The  disappearance  of  one  principle  (narcotina).and  the  augmentation 
of  nnolher  (morphia),  caused  bv  climate,  are  interesting  ami  im]>or- 
lunt  facts.  Petit  II  gut  from  IG  to  18  percent  of  morphia;  and 
Cavcnton  obtained  fmm  2*2  to  28  per  cent,  from  French  opium  ;  but 
in  the  Utter  ease  the  morphia  was  probably  very  impure. 

Gkhhan  Oritm.  —  This  opium,  when  obtained  inmi  the  PapaTer 
somniferum  (a)  nigrum,  furnishefl  under  the  analysis  of  Blitx,  of 
Krfurt,  from  16^  to  20  p-r  cent,  nf  muq)hia,  and  troin  G|  to  94  of 
narcotina;  while  from  that  pro<Iuce(l  by  the  P.  somnilerum  (b) 
album,  and  on  which  he  proturetl  ccmversely  6  8  per  cent,  of  morphia, 
and  Hii  per  cent,  of  norcotina. 


On  the  AotjLTKRATioss  or  Opium. 

Opium,  like  most  other  articles  of  a  costly  character,  is  sobjectiid  to 
oonaiderablc  and  varied  adulteration,  as  proved  by  the  ronrurrent 
testimony  of  nearly  all  writers  on  this  important  drug,  and  us  well  by 
the  results  of  the  analyses  nf  numerous  samples. 

"The  first  sophistication,"  sayt  Dr.  Perciri,  "which  opium  receives, 


•  Trsm.  Soc.  ArU,  ilUI.  H. 

i   Duncan,  StiM.tntliffKd.Dlip.  p.  fli. 

I  Joum.  dr  I'hATtn.,  %\l.  nO. 


t  IbM.  1.  3&. 
I  IbM.  alU.  I 


89S 


OPIUM,   AND   1X8   ADULTERATIONS. 


M  that  prnctispd  by  the  peasants  who  rollert  it,  nnrl  who  ligbOrK?^ 
the  epidrrmis  from  the  shells  or  c:i]Kule.«  to  augxneiit  the'weiitt 
This  openition  aiMs  abnut  one-twelfth  of  forei;jn  matters.'*  In  fqrtiw 
proof  uf  tht:  practice  uf  this  adulteration,  we  hiive  likewiye  ibv  >»• 
tbority  of  Mr,  Ini|Mjy,  who  states  :  "  U  is  during  the  operatinn  ofKn^ 
in^  ihut  the  tir»t  »ophtnifntion  oc<;urs,  the  sH:raper  being  cantrl 
hemvily  over  the  capsule^  takln;^  with  it  a  couE^iderabie  part  of  thehcsrt 
or  pubeseent'e."  , 

AeturdlnfT  to  Dr.  Eiilwell,  whose  Report  on  Indian  opium  « 
have  ulrondy  referred  to,  "the  grosser  iinpuritii?*  usimllv  mlxti 
with  the  Uruj;,  to  incrciiae  its  weight,  tire  mud^  nand^  pou^derrd  okir 
ccio/,  soof^  cntc-dung^  pnuiuit'd  futppy  p^luU^  und  ik>iiu»]c<I  trtd*  o( 
various  (icscriptinns.  All  uf  these  substances  are  rcnililv  iliscnvermMf 
in  breakin^r  up  the  drug  in  eold  water,  reioovini^  U/c  ttuJiibte  and 
lijjiiter  portions  of  the  diffused  mass  by  decantation,  ami  4'arefullT 
exHiiiining  ihe  sedlinem.  Hy  tliis  means,  impurities  of  the  obow 
nature  usually  bet^mne  physically  apparent.  Fl-nr  \»  a  verr  fiiviianir 
article  of  ndulleraLioii,  but  is  readily  detecte<).  Opium  so  ndiiltenitcd 
speedily  becomes  Eour  ;  it  breaks  with  a  peculiar  frhnrt,  rtigu:eil  fr»c- 
ture,  the  t<harp  ed^t^s  of  which  ure  dull,  and  not  pink  ond  tnin&luccDl 
tut  ihfy  shouid  be  ;  and,  on  squeezing;  a  mass  of  the  ilrujr  af)cr  imnj^r- 
sion  in  water,  the  starch  iiiiiy  be  seen  oozing  from  ila  surface.  Tht 
application  of  the  iodine  lesT,  however,  furnishes  conclusive  evtd*fnf« 
of  its  ])re>enoe,  or  at  least  of  that  of  some  aniyUceoua  coomound.  The 
farina  of  the  boiled  potato  is  not  uDfrei|uentlv  made  use  nf;  ghee  atxl 
pftor  (an  impure  treacle)  are  also  ocrasiomdly  useil,  as  beinff  artiela 
at  the  couiinnndof  most  of  the  cultivators.  Their  prcAci^cc  is  reveded 
by  ilie  peculiar  odour  and  coni^istence  which  ihey  impart  to  (he  dnic- 
][i  addilifin  1o  the  above,  a  vaiiety  of  vegetable  juiceti^  rxtmcU,  puip^ 
anil  coloitrivg  matter*  are  occasionally  fraudulently  mixed  wirli  the 
opium,  such  as  the  inspissated  juice  of  the  common  prickly  juvr 
{CactHK  dilrnu)^  the  v-xiTocis  prepared  from  the /I'/wcca /jM»*f  (_ViM- 
tiana  fabftcum)^  the  Dahtra  stramoinum  and  the  Indian  hemp  (^Ctat' 
h/jhiA  itidica)^  &c.  The  gummy  exudations  from  various  jdunts  are 
frequently  used  ;  and  of  j)ulps,  ibe  mo?t  irc«juen(ly  employed  are 
those  of  the  /wmariW,  and  of  the  Bad  frvit  {JEgU  tnnrmrUts).  To 
impart  colour  lo  the  drug,  various  substancet:  ore  entploTed,  u 
catechu^  turtnerte,  the  powdered  flowers  of  the  motcka  tree  {BataM 
lati/ufia),  &c." 

"  From  one  sample  of  Smyrna  opium,"  irrites  Dr.  Pereira,  **weiffh- 
ing  ten  ounces,  I  obtained  frn  drachms  of  stones  and  praveL" 
Speaking  of  Ei»yptinri  u[iiuni,  Dr.  iVreira  writes: —  *'  Some  very  in- 
ferior f|un!iiies  are  sometimes  offered  for  sale,  whirh  apftear  to  the 
sight  and  touch  to  be  largely  adulleruted."  And  further  on,  the 
same  author  goes  on  to  state: — *'Opium  is  brought  into  the  markpt  of 
unefpial  degrees  uf  purity,  inconsequence  of  itg  having  been  f^ubjei'ted 
to  adulteration,  and  partly  perhaps  from  the  empluymtmt  of  diifureol 


OPIUM,    AND    ITS    ADULTERATIONS. 


631 


leUioils  of  preparation.  Furthennor*?.  opium  from  whirli  the 
morpliiii  li!M  been  uxtmcted  \ui»  bcon  tVauilulently  inlrocliict:!(l  intn 
Coiumt^rcti."* 

LanikTL'rf  has  dc!scribeii  an  ndulturation  of  a  smnple  of  npiuni  ob- 
taine'l  lUrect  from  Sniyrnii.  whicih  ht:  (liMjovcred  in  liie  pn-puraiioii  of 
a  tincture.  Ah*;r  wvltiiI  liours'  digetsiion,  the  tincture  a^.sunlcrl  a 
slimy  or  iiiucihi^innus  cunclition,  nnd  in  the  course  ol*  a  tew  days* 
became  so  •/cljiliniform,  tlml  it  could  not  be  i>oured  out  from  the  glitiji; 
by  a  ciireful  examtnntion,  gtiltp  jMitder  in  large  pi-oportion  \ta*t  dis- 
cuv*;rod  in  the  opium;  nntl  Landerer  w.os  afterwards  informe<i  lh«t 
this  is  a  very  common  iidulterniion,  prst-ti.sed  in  order  to  make  the 
opium  lijinlLT,  and  to  hawien  the  pioeess  of  drying;.  Dr.  Pereira  also 
9peuk(t  of  ail  opium  whi'.'h  contained  n  gelallnirorni  substance^;  and 
Mr.  Murson  has  met  with  an  opium,  in  which  an  appnrt^ntly  aimiiftr 
RubifLinee  wiis  prt»ent. §  Lunderer  abo  states,  that  the  extract 
olitaiiH-d  liy  boiling  the  poppy  planta  is  commonly  added  to  Smyrna 
opium.  II 

In  lh\  Normandy*8  work  ("Commercial  Tlnndtionk  of  Chemical 
Aiudysis")  we  nice!  with  the  fuUowinjj  siatcmet>ls  reluiin^  to  the  iidul- 
Icrati'tn  ol' ihif*  dru^  :  "Opium  is  often  met  wiih  in  urHnmcrce  fn»m 
which  the  luorphine  hw  been  exlrnctcd  ;  on  tlie  other  hand,  tliis 
V)duu)ile  drwjr  is  *>l'ten  found  adulterated  with  sttirvh^  initer^  Spaniah 
liqiwrice,  lactnairiuni^  extract  ofjhippi/  learei^  of  ^iauv.inm  luttrum,  and 
other  rti^ctahle  extracf.%  mucilage  of  ^um  trm^ncmdh^  or  nthrr  gam/i, 
ciat/^  stintly  gravel ;^  often  the  opium  ia  mixed  in  A*ia  ami  Kgypt.,  when 
frehh  iiutl  soft,  with  finely-brmsed  grapes  from  which  the  fltomrs  have 
boen  removed  ;  scmieiimes,  als<>,  a  mixture,  fabricated  liy  bruisinj;  the 
exterior  skins  <tt  the  eapsuiea  and  stdks  of  the  poppy,  to^ethi^r  with 
the  white  of  eg;.'s,  in  a  stone  mortar,  is  a-l-led  in  certain  prop'irtions 
tu  the  npium,  In  fact,  ihiii  most  valuable  dru};,  certainly  cue  uf  the 
most  important  and  most  frequently  UM*d  in  tuedicine,  is  also  one  of 
the  ntiMt  r-xlcnsivcly  adulterated." 

Ilia  abundantly  Aliown  by  the  fore^joinir  quotations  and  extracUi, 
that ^um  opium  la  very  exti-n.sively  adulterated;  it  doefl  not  uppoar, 
however,  tuat  any  obMirvations  have  yet  been  made  rcKoectin);  the 
adultL'ration  o(  pourdered  nptum  ;  whether,  for  ingtance,  like  so  many 
other  vefcelable  iKiwders,  it  U  ^ubjectcd  to  sophiMiculion  in  the  pro- 
cess of  jirinding. 

The  niajnrity  of  observations  found  in  works  treating:  of  adulteration 
are  nearly  all  uf  a  general  character,  and  fail  to  show  the  condition  as 


*  Jotirit.  df  rtiHrrn.,  sil*.  33-^.  44Q. ;  x.x>.  Id7- ;  a^Ki  Jaurii-  J*  Ctilni.  Mi'U.    I*.,  liitle 
8ftr..  |>ii.  3}V  iVt. 

t  BMC>Mi<r'*  K<*»*rtnrli|m.b(J.  ♦!.,  h»ft  S.,  p.  349. 

I   Kirnirnii  nf  M«)orU  MmUr4.  ?mI.  tL.  p.  )7«1     S«coail  KdttlOU: 

)Kh>rim.  Juiirn..  fOl   tv.  p.  An?. 
Archlv.  d«r  Tdann..  .Scftemttrr.  ISM,  p.  SM- 


(140 


OPIUM,   AND   ITS   ADULTERATIONS. 


to  pnrit;  nf  the  articles  ns  they  actually  reach  the  oonvqacr;  tim 
j;rt?at  object  of  tbe»e  inquiries  ia  to  supply  thia  cbipf  d«f«t  n  »xt 
tixi-tting  intormalion,  ii  work,  in  many  cases,  of  e\Ci>:iiii*  Ubiiar  vhI 
difficulty,  but  it  is  upon  this  feature  that  the  value  aiul  intoRAor 
theM*  articles  mainly  depend.  Wc  thusoArertntn  what  are  th«amacn 
and  prevailiii;;  nduU^iratinriR.  what  the  more  unmmmon  and  rmrt.  Mil 
lastly,  we  are  enabled  to  reject  a  whole  ht»8t  itf  iiul>:4lancc4  ukI  out^• 
rials  from  the  list  of  alleged  sophistications. 

"We  will  now  prnceeil  to  <;ive  the  resultft  of  the  analysb  of  Tan^ 
three  aampfes  of  the  prinetpul  kinds  of  Qum  Opium  in  tlw  lUlta 
which  it  is  imported  into  this  country,    Tiie-te  were — 


Tbflt  out  of  the  Tteent^'three  samples  of  gum  opium  analfsed, 

were  atliilterated,  and  four  only  genuine,  many  of  thc«<-.  a*  A"'* 
by  the  micToscopc,  being  Adulterated  to  n  large  extent ;  thr  5»r>«i3 
ing  nduUerations  being  with  pofpt  capsblh  and  wncat  ri^>i» 

That  the  amount  of  alkai^ids  varied  from  2"7  to  14-0  per  (vuunr 
in  the  proportion  of  nearly  one  to  five ;  that  is,  some  of  th**  Mmple* 
were  five  times  as  strong  as  others.  This  variation  otfrtraifda 
partly  due,  no  doubt,  Ut  the  adulteration  to  which  lo  naof  rflW 
Mmples  were  subjected,  but  partly  also  to  the  rarring  aoiiTtlTvf 
the  opium,  determined  by  natural  causes,  such  a«  diflvmKacfM^ 
climate,  and  mode  of  preparation. 

The  above  analyses,  therefore,  inrontestahly  prore  that  npiam,  nlW 
state  in  which  it  is  imported  into  this  country,  ta  Tery  extenaritly*! 
commnnly  ndulternted. 

Looking  Ht  the  results  of  the  chemical  analyses  of  the  opium  «ffC- 
ceive  thut  the  different  samples  vury  in  the  nio»t  reittsrkable  uoatt 
in  their  composition.  To  such  an  extent  is  this  the  c«m  tktf  flM 
would,  in  several  in^tiinees,  be  led  to  >iu«pi>ct  the  fjct  of  adullwrfw 
front  ihe  chemical  anulyites  nlone,  wiiliuut,  however,  beiiuf  ahlc  !■>* 
lively  To  affirm  its  existence,  in  conMequence  of  the  dcf^ivc  la  vwk 
in  extreme  cases,  the  composition  of  gum  oiuum  of  undoubted  o^an 
is  itself  found  to  vary.  Making  all  due  allowance  for  aucb  var»liMi 
however,  we  are  still  enabled  to  indicate,  in  addition  to  lliowt  alNMh 
enumemled  ns  being  adulterated  with  {Hippy  capsule  and  «b«asfl(Nr. 
»9  undoubtedly  itiluUcrnled,  two  sampler  of  Suivrna  opium,  aailtviKif 
Kgvptiun  opium,  which  were  adulteratetl  with  mtntt,^  'Wor.  andf^* 

(^'om  the  analyses  instituted  of  Porty  tfrmptes  of  vju^ijd  ipa* 
it  npfK^arod  :  — 
That    Thirty-one   of  the  samples    were   adulterated,  and  m/  tisif 

genuine;  the  principal  adulterations,  as  in  tlie  previous  ease,  beaf 

with  porrr  capsuxje  and  wukat  rtovm. 
That  /our  uf  the  vamplefi  were  further  adulterated  br  the  wUbas 

of  POWDERED  WOOD,  intToduced  no  doubt  in  the  pracva  of  M^ 


OPIUM,   AND  ITS  Al>ULTEBATION8.  Ml 


That  (he  nmount  nf  aOudouit  varied  from  23  up  to  13*2  per  vent.,  or 
in  the  pniportion  ofotiarlv  one  to  %\x — that  i.i,  the  iitniplefi  difTcred 
in  slren^lii  in  thnt  rnlio.    fbe  lowest  sniounte  ufalkulnids  lumitihed 

►  bv  the  p«twdered  opiums  wijre  2*!$  and  3  2  per  eent.;  tliefe  wt-re,  in 
all  prohabilitv.  exiiuiisted  Dpiiiniii,  which  \vm\  heen  previounly  em* 
plojred  ill  the  preparation  of  lincture. 

We  helieve  thut  it  id  not  an  unfre<)nent  practice  with  dniffptsia  to 
employ  tiic  insoluble  residue,  whec  dried  «nd  pulverised,  left  from 
the  pri-panitioQ  of  the  tincture  nf  opium,  in  the  adullerntion  of  pow- 
dered iipium.  We  have  ulno  knuwn  it  to  bv  ui^^ed  for  making  the 
titi;.'iientiim  ;:allGe  cora[icH«iluin. 

"  I  have  known."  9tatc9  Dr.  Tliom»on,  in  hii  evidenr-e  before 
the  Parliumentarj  Commitlre,  '^extrjiet  nf  tipiiim  mixed  with  extract 
of  senna,  and  froto  30  to  60  per  cejit.  of  water." 

From  all  thi»,  then»it  fdllowu,  partly  in  oonsequoneo  of  adulteration, 
thut  LTude  opium  varies  to  a  great  extent  in  strength  and  activity, 
BO  much  »o  ihat  m»  certain  reliauce  can  be  placed  on  the  efleoU  pro- 
<]uced  hy  this  remedy,  administere^l  according  to  any  fixed  or  uni- 
form scrtle  of  doses. 

It  further  follows  that  all  those  preparations  made  from  opium,  or 
into  ihe  eompositiun  of  whirh  opium  enters,  are  of  equally  uncertain 
6lren<rtli  nnd  power  —  as  tinctmu  opH^  tinct.  Cfimphonr  compoMtta,  vi- 
wMwi  /i/ifi,  pntptx  crefft  comp.  mm  opio.  puh.  ipecaruanho'  comp,y  pule, 
kino  emup.,  piMtt  saponix  romp.y  runfeciin  o/n'i,  ertntctnm  ouii„  enema 
opii^  liiiimeiitwn  opti^  and  tmftiwttrum  oph\  of  the  Loiiiluii  i'hiirmaco- 
|K£iii;  tinctiirti  opti  amtntmiuUi^  ufttum  opit,  piluto!  opii,  pd,  eutomelanos 
ei  opit^  pd.  plumbi  npiata,  eUrtuarium  opii,  and  trochiMci  opii^  of  the 
Kditibur<;h  and  Dublin  PhamiacopcetH!i. 

The  fact  that  even  ;ce«Mi»«  f;um  opinm  is  possessed  of  very  diffe- 
rent dcgreea  of  itrcngib,  has  been  clearly  shown  by  various  analysts 
and  ex[>erimentali«iU:  — 

Cbevallier  found  in  six  samples  of  choice  Smjma  opjum  the  fol- 
lowing proportions  of  water  —  viz.,  33 5,  35*0,  40*5,  42-32,  525,  and 
53*0  per  cent. 

(TShaughneur  found  from  25  to  21  per  rent,  of  water  in  Indian 
opium  (Bfehar  ageney),  and  13  percent,  in  Patna  njiium.  Dr.  Eat* 
well,  the  opium  examiner  in  the  Benares  diitriet,  findt  thnt  the  pro- 
[>nrtion  of  water  varies  from  30  to  24*5  \kt  cent,  in  tlic  opium  of  that 
diitriel. 

With  respect  to  the  propttrtion  of  mor[>hia,  Cbevallier  states  that 
Smyrnu  opium  contains  from  A*6  to  6  4  pir  cent  of  that  alkaloid ; 
Constiintinoplc  opium,  from  2'8  to  3'2  ;  and  Egyptian  opium,  from 
2*0  to  2"4  per  cent. 

The  subject  of  the  strength  of  opium  wns  dincusBed  nt  the  Pharma- 
ceutical Suiriety  of  Paris  on  tbe2na  of  April,  1850.  Miuihe  stated  that 
the  proportion  of  morphia  in  coonDercial  opium  varied  from  I  to  10  per 

T   T 


642 


OPIUM,    AND    ITS   ADL'LTERATION& 


MurphU. 

NaroMiM. 

248     - 

- 

•     A-26 

2-38     - 

- 

'     4-58 

2-20     - 

- 

-     6M 

3  21     - 

- 

-     408 

cent.,  ami  this  trail  confirmed  by  Snubeiran.  Giiiboiirt  9a\<\  h^tihlaintd 
frnm  15  to  17  i>«r  cen:.  from  Sin^rrita  opium.  b»  uIoo  diil  MM.  CanatOB 
and  Aulier^er.  Dublaiic  affirmed  that  it  cuniMin«  at  m<>«t  MptfoeML. 
butAomeiiines  it  isevona.*  low  as  1,2,  or 3  percent.  Guiileiurtteranur 
obtained  more  thim  14,  while  good  spocimcns  rieldvfl  from  }OMt$ 
per  cent.  Do  Vry  analrscd  21  ttamides  nf  coniinrn.*M]  t-; 
found  the  {iro])orlion6  of  niurpliia  to  vary  from  mere  trwc?  : 
cf-nt.  (but  his  pr(>ce59  was  not  a  good  one).  Keii'h  gvt  from  Ifiu 
1*2  per  cent.;  utid  O'Shuujfhnffsy  ubtniuetl  from  tlie  o|nun]  aftk 
Behttf  agency  frfini  175  (o  3-5  |»cr  rent,  of  morphi.i,  -•      -■ 

of  narcoiinn;  in  that  tn>m  Hnzflrecb:iti^h,  4'5  of  timrp 
cent,  ofnarcotina ;  and  in  Paina  garden  opium  he  e^:; 
»^ent.  of  morpliiii,  and  6  0  pep  cent,  of  narootina.     l>r. 
in  the  onium  of  ihe  Beuiires  dislriet  the  following  prb|K.4  ...^....  v. .... 
phia  and  narcotina,  in  the  ycara  1&45  lo  1848  :  — 

I84o 
1846 

1817 
1848 

Thc^  fucts  f>hiivr  that,  even  if  wc  could  succeed  in  obtjiinin<:f  a  ifl 
ca^es,  gum  opium  of  undoubted  purity,  yet  we  couhi  not  rvU  u{b« 
iti  prt>ducin<r  uniform  efferts.  'ilm  consideriiiitm  shnwi  liiRtUn 
the  neceraity  of  employing  in  medicine  prcpurntioiis  maile  frm  tU 
drug,  of  us^ertuiiiud  strength  ;  these,  to  some  extent,  we  pomven  '» <W 
salts  of  morphiu ;  and  no  doubt  it  is  far  better  to  prescribe  ihflff,  ii 
the  majority  of  ra.-ses,  in  preference  to  crude  opium. 

But  it  15  prubtibli*  that  u  piepanition  miglit  be  obtained  foriBadif 
more  than  one  oonslituent  ol'iij>iuni,  and  wbieh  would.  Uier«A>f«,Bff* 
neiirly  rcsumble  the  complex  and  original  drug.  One  mfthttj  hj 
whicl)  an  iip[iroxim;ition  Id  uniformitv  of  stren;:th  could  be  aliti»a«d 
in  the  lin<:turo  ot  o[>iuni,  h  by  a  previous  analvsis  of  the  sruin  'hmu'W 
from  which  it  is  tn  be  prepared,  and  a  rcgulatMtn  of  tU*-  <. 
to  the  fllrer.jTth  of  ihtit  opium  ;  or  the  alkidoicU  utighi  ' 
ihcy  were  ileficient,  so  ua  to  ensure  as  near  art  approach  tu  uitiuiriui:* 
a?  proetienble. 

It  nhould  be  c»bservcd  that,  of  the  samples  of  powdered  ofink 
the  results  of  the  examination  of  which  have  ju«t  bfron  £ircfi«  tk** 
whiuh  were  found  to  contain  the  lari^v&t  {•er-e<^ntr(«:e9  f»f  watrr  kal 
been  kept  in  a  (in  Cii^e,  and  thus  the  moii^turc  prctcnted  f rao  0^ 
faping;  while  mo^tt  nf  ttie  samples  which  cimluincd  the  sKutler  K^ 
<?entagea  of  water,  had  t»een  exposed  tu  the  atmospbeie,  and  90  w 
lost  part  of  their  water. 

In  reference  to  the  varying  quantity  of  raoi*^ture  cont«ift*d  •> 
opium,  we  find  thj  following  ruutarlu  by  Mr.  C  V.  Uogner,  of  I^J** 
delphia  :  •  — 

*  riuripacfUliOBi  Juarnsl.  9«|**  )•  IMI,  toI.  la.  f.  lU- 


OPJUM,    AND   ITS  ADULTERATIONS. 


64S 


"We  sometimes  receive  Tegetnble  Bubslances,  roots,  bnrks,  (Znmd, 
hc.f  tJirect  from  llie  hultl  of  a  ship,  or  from  tluiiip  Cfllim;  at  other 
times  we  receive  the  same  ifliclcs  from  the  j;arrvt.  of  a  store,  where 
tbej  way  have  been  fur  a  jear  or  more.  It  is  ridiculous  to  expect 
the  same  loss  in  both  caw^.  Most  of  the  articles  we  jwwiler  contain 
more  nr  Il'»h  wiiti-r,  which  we  an;  obli;'e«l  to  ilry  out,  ami  if  we  did  not 
dry  them  artifieiully  when  we  rcducx*J  them  to  ».  ch  minute  ptirticlea 
as  cnnBiiiuie  n  tine  powder,  the  water  wouhi  in  a  {;reut  uieiuure 
escape  by  evofwralion.  '1  his  cuniitilutes  the  hms  in  nowrJering  drugs, 
at  leaitt  the  greiit  amount  of  it.  Some  time  btick,  I  received  u  lurce 
lot  of  barberry  tmrk  fnmi  a  bouse  iti  this  city,  who  hud  lH>u^bt  it 
without  Hutlicient  ex:iuiiniitioti,  for  it  hud  been  completely  saturated 
with  water,  purjKjsely,  I  suppose,  by  ootne  *  financier*  to  increase  the 
weijjhr.  When  I  opened  it,  and  saw  the  condition  it  wns  in,  I  rulled 
the  tittcntion  of  the  owner  to  it,  but  he  had  unfortunately  already 
paid  for  it.  1  dried  it,  and  it  loet  over  thirty-tive  per  cent,  in  the 
drying  alone.  Now  what  a  position  1  would  have  bcfn  in,  had  I  been 
refltricrted  to  a  loss  of  two  or  three  pi^r  cent.  It  would  have  taken 
a  considerable  fiuantity  of  what  Mr.  Uedwood  fncelinusly  calU 
'  veritable  powder  of  post'  (sawdust)  to  have  made  this  matter 
fctraiffhi. 

"  Twenty  years  bark,  I  attempted  to  unite  to  my  other  operniiomt 
th&t  of  cliipping  »n<l  drying  dye-woods,  and  ground  in  all  from  fifti'ca 
to  twenty  lens  fur  diflerenl  parties  ;  and  although  the  woo<l  appeared 
to  be  dry,  it  lost  over  two  hundred  pounds  un  each  (on,  caused  by 
evaporation  on  lietn^  cut  into  line  chip»  across  the  grain  of  the  wood. 
Of  eoursc  I  nrceiv«:d  ihc  usual  amount  of  'rowinu  up'  fur  making 
such  losses  ;  si>  ninch  so  that  I  became  heartily  t<tck  ol'  the  buitness, 
and  ftold  at  half  the  cost,  the  app»iatu»  I  hud  erected. 

"  It  is  customnry  to  remedy  this  dillieuhy,  not  with  *  powder  of 
post,'  but  *  uouajunt."  Under  tne  pretence  that  it  improves  the  quality, 
water  is  fieefy  u^ed,  not  unly  to  n<ake  jjood  ihu  hists,  bnt  a  little  further, 
and  the  consumer  is  inudu  to  pay  a  pretty  hi^h  price  for  water.  I 
hnve  seen  bai  rcla  "f  chipped  wood  that  have  luid  si>me  time  in  n  store, 
fall  short  from  fifteen  to  twenty  poumls  on  the  mnrkft  w«ij»ht.  I 
think  it  is  a  fraudulent  and  nsfle^s  custom.  If  the  nrtlclc  is  really 
improved  by  the  operuiion  (which  I  very  much  doubt),  there  i*  plenty 
of  water  in  every  ilye-houw ;  let  the  coi»sunier  water  it  as  much  a^i  he 
chooses — let  Ihe  dealer  sell  him  wood,  not  water,  and  chiirj^e  occord- 
'mgly,  and  let  the  chipper  be  a  '  hewer  of  wood ;'  but  have  9'Mne  com- 
passi'm  on  him,  and  do  not  also  make  him  a  *  drawer  of  water/ 

"  The  imporliuit  article  of  opium  cimies  to  iis  in  very  different  rnn- 
dittons.  I  U-lievL-  it  is  the  (iciieral  custom  of  the  dru;;gitits  to  keep 
this  article  in  their  cellars  lo  prevent  it.H  <lryin^  iiml  losiiiir  ifeigbt ; 
»omc,  however,  do  not,  particularly  when  it  is  inicnde<l  to  be  pf>w- 
dered ;  of  course  the  Umb  in  the  former  must  necessarily  be  greater 

T  T  a 


644 


OPIUM,   AND   ITS  ADULTEHAT10X8. 


tban  in  the  Utter inBUnce,  tnd   it  would  be  perfectlj  nvr»i^<^      ., 
under  such  circum5tanc«8,  to  bind  the  powdercr  to  a  regH*  P«*      1| 


F(g.m, 


Sunplt  of  OriCM  kduUcrsUd  «1U)  i^vvir  cnpfwtM^    M«CBt9td  lOD 


centuge  of  loss  in  powtloring  opium.  I  have  Imjcii  inftmisdi 
believe  correctljrt  that  thure  uxistA^  in  -lome other  places  aeon 
rule  of  six  per  cent,  in  powdcrinj;  npiiim  ;  so  far  a*  I  reaembs,  I 
rarely,  if  ever,  powdered  it  at  a  less  toss  tbnn  ciiiht  |t«r  ceni^aki 
Bomctimes  OS  greitt  as  twenty  per  cent.  I  have  exHrniiiMJ  my  bwto 
in  refereni.'e  to  the  Inst  twelve  lots  of  opium  powdered,  and  And  thij 
amount  to  165  lbs.  12  oz.  received,  ftnd  U!21bft.  2  oz.  rviuraeil;  iW 
least  loss  ei^hl  per  cent.,  and  ihe  greatest  near  twenty  pcf  oeaL,  t&a 
average  being  14  lbs.  5  ox.  per  cent.  Mr.  Kcdwoixl  jnTca  ihm  mm* 
ug;e  lo5.i  in  powdering  this  article  in  London  at  14  lh«.  I4  oc.  «■  dkl 
1 12  lbs.,  the  greatest  ei<;hieen,  and  the  leiist  six  per  cisfit. 

"  It  would  be  a  very  easy  matter  for  any  <1  rtia  iW 

loss  in  dryinf>  any  particular  lot  of  oiiiuni,   i  tjoa  lali 

very  small  pieces,  and  drving  it  sulliciently  u>  mu*.'  a  nm^  m*4w. 
Yet,  notwiihyUinding  this  simple  methiHl  of  ascertainin}!  tW  tet,I 
have  met  with  instances  (not  many,  to  be  sure,  and  none  lalclv)  when 
persons  have  sent  their  opium  elsewhere  to  be  powdered.  Cor  noxAti 


a 


OPIUM,   AND   ITS   ADULTEUATIOXS. 


645 


rewon  than  that  of  the  loss  being  less  thnn  I  made.     Porhnps  t  might 
bave  satisfied  lliem  had  I  made  use  of  the  *|M)wder  of  post,'  or  some- 


Maftilftvd  !!S0  dUmclCf*. 

thinj;eUe,  whti-h  i ft,  and  must  be  done  by  every  one  who  powders 
orditmrj  opium  al  a  lo«s  of  only  six  per  cent.  This,  however,  I  never 
have  dutie.  and  never  will  do.  I  do  nut  profess  more  hnriei^t}'  than  my 
neighhours  ;  but  if  1  had  no  scruples  on  the  subject,  1  can  iuiu;i;ine  a 
casti  when;  I  niii:lit  make  mvrclf  uuvnalile  to  juoiire  fu  a  jmrlicipant 
in  cau!ting  the  death  of  a  fellow  being,  whoue  life  might  be  lo»t  for  the 
want  of  a  pmiwr  article  heing  aduiiiiistered.  I  repeat,  if  Ihore  were 
no  other  motives,  I  would  not,  under  any  cirrum-ttjint'Cft,  make  myself 
liable  to  nuch  a  charge.  Opium  is  one  of  the  most  importaut  of  the 
dnijFS  that  pass  ibruugh  my  hands.  Kvery  physician,  dru*;gist,  and 
apothecary,  knows  tbt.  importance  of  having  it  ri^ht,  and,  t^o  far  as  it 
depends  on  me,  it  shall  be  right,  be  the  loss  in  powdering  what 
it  may. 
'*  With  a  conventioual  lo«s  of  six  ]>er  cent,  there  can  be  no  uniformity 

J  T  S 


646 


OPIUM,    AND   ITS    ADULTERATIONS. 


in  the  article.     A  powderer  receives  a  lot  of  opium  no  dry  that  it  only 
loses  six  per  cent,  in  powdering,     lie  receives  Another  lot  that  Ium* 


SorrrtAjr  OnvM,  >4aIUt«fed  wfth  turn,  iMMtfy  jOn.  taa  m  UUlc  nAMi^bMr. 
HflcnUcrd  un  diwnctcn. 


twenty  percent.  To  bring  the  lo^s  on  the  latter  to  the  same  as  the, 
former,  ne  must  put  in  fourteen  percent,  nf  Adulieraiiun,  imd  Uie«| 
you  have  oik*  article  fourteen  per  cent,  less  in  efliciency  than  the 
other.  Fruin  sijuie  cause  unknown  in  me,  the  ootisuinplitui  of  pow- 
dered opium  hfis  {;i*eatlv  inL-reiised  ia  the  last  five  jeurs,  and  soens 
to  be  increasing  annually,  if  1  may  judge  from  the  (juimliiiei  I 
powder." 


8CAMMONY,  AND   ITS   ADULTERATIONS.  617 


On  Me  Detection  of  the  Adviteraiioju  of  Opium, 


The  arlultenitions  of  gum  und  powderoil  opium  with  poppi/  cap- 
sule (jf^.  205.),  wheat  Jifntr  (J^,  HOG.),  or  other  vegetable  auhstanceis 
may  Ijl*  ri'iuliFy  ilistcovercd  by  simply  exiuninin^  a  minute  portion  of 
the  opium  under  the  microscope.  To  estimnte  the  quantities  oi'  these 
present,  a  dried  nnd  we)*'lied  amount  of  the  opium  must  be  dissolved 
in  water,  the  insoluble  residne  I>ciny  dried  Hnd  weighed. 

Saati  or  other  insofuhle  iiutrganic  nthsttiuce  which  may  he  present 
mur  he  dIiu:overed,  and  It.t  amount  t'nleutate<l  In  the  trame  mnnner. 

'Phc  gum  mny  he  calruhited  from  tlic  residue  of  the  tillered  watery 
extrncl  whieh  is  insoluble  in  nloohol. 

Lastly,  it  is  well  in  mL>st  cn^es  to  delermino  the  amount  of  alkaloidt 
present  by  the  procfMcs  alrea^Jy  described. 

Cufltonifl*  duty  on  Opium,  \s.  per  lb.  Qunntities  retained  for  home 
conitumptinn  were,  in  IN.14,  6J,43*ilhs. ;  in  1855}  56,067  lbs.  ;  in  nine 
munlhs  of  1856,  35,354  ll>s. 


SCAMMONY,  AND  ITS  ADULTERATIONS. 

The  adulteration*  diseovt-rod  in  drurrd,  like  those  in  food,  are  prac- 
tised by  three  diff-rent  el»»se<i  of  p»*rfiona  —  the  preparers  or  manu- 
facturers, the  whoU*t<aIe  and  the  retail  dealers.  In  si'ioe  co^es  the 
adulterations  detected  are  exclut^ively  the  work  of  one  or  other  of 
these  rlasses;  in  olher?,  each  does  its  jmrt  in  the  deterioration  and 
sophistication.  In  the  course  of  our  invesiij^atiuns  we  have  met  with 
many  examples  prnvinj;  the  truth  of  l!if  above  classification,  and  (he 
article  scsmmony  afiord^  an  illu.«tration  in  iMiint. 

Scammony  U  the  ^um  resinous  exudation  obtained  by  inci!fton<i 
into  tlie  roots  of  Conroirultu  scammonia.  The  rwits  are  perennial, 
tulictous,  tapering,  three  or  four  feet  long,  and  ronlarn  an  acrid, 
milky  juice,  which,  dricil,  constitutes  scammony.  It  grows  iu  heilges 
and  bu^hy  places  in  Greece  and  the  Levant, 

Sorimmony  was  known  lo  ilie  ancient  Greeks.  Dioscondes  thus, 
accordinjj  to  Pi-reirn,  dejcfil***  the  mode  of  procuring  it :  — 

**The  head  beinj^  separated,  the  root  is  to  he  excavuicd  in  the  form 
of  a  dome,  or  vault,  by  a  knife,  po  that  the  juice  mnv  flow  into  the 
cavity,  from  whioli  it  i?  to  lie  token  *)ut  in  i^bells.  Others  excavate 
the  earth,  and  having  incised  the  root,  let  the  juice  ruu  into  the 

TT  4 


fi48 


SCAMMONY,    AND    1T8   ADULTEKATION8. 


cavitTi  which  has  been  nrevtously  lined  with  walnut  leAVea.     ^V! 
the  scammiiny  ia  ilrv  it  is  removed." 

In  1 770.  the  nieihut]  of  proeurinj?  frcunmony  ntlopted,  nnd  whicb  « 
piubablv  ihiit  followed  in  the  prescDt  day,  was,  ftccording  to  Dr.  Uu»- 
wjl  *,  nsftillows:  — 

TUm  earth  being  cleared  away  from  the  upper  part  of  the  roots,  the 
peaaanta  cut  otf  the  tnm  obliquely  about  two  inches  below  where  tlte 
«ulkfl  arc  ^iven  otf  Under  th«  nimt  dependin;;  pnrt  of  earh  inciaioa 
a  shell,  nr  ntliGr  suitable  n^ccpUcli^  1.1  placed,  into  whicii  tiie  juioe 
slowly  flows.  The  shell  is  left  for  about  twelve  buurs.  when  thm 
whole  of  the  juice  baa  exuded.  The  ci«atiiiiy  vieldcMl  hy  each  root 
doe«  nut  exceed  a  few  dnirhmit.  The  milky  juice  frmu  (lie  several 
roots  is  {lilt  lo;rethe^,  often  iiiLo  the  Iv^  of  an  uld  bout,  wb«*re  il  gra* 
dually  becouiL's  hardened,  and  forms  scummony. 

ScHiiinionv  ia  usually  imported  from  Siiivrnu.  OecaBionally  it  comes 
by  way  of  Trieste,  and  still  more  i-arfly  it  is  brought  from  Alexan- 
dre! ta,  tiie  port  of,  and  ro:td  to,  Alep)>o.  It  comes  over  in  boxea  and 
drum9,  which  arc  fre^jucntly  lined  with  Lin. 

The  ditfi^rcnt  kintjit  of  scammony  of  etnnraerce  are  arranged  hy  Dr. 
Perciru  under  ilirce  beads — pure,  uduitrratnl,  ami /actttiimA, 

Tlie  purif  scaiumoni(;s  arc —  Vtrgin  JScammonj/^  the  only  pure  kind 
known  in  Knglirh  commerce ;  scammony  iu  calabaBhes  or  sbcUv,  and 
probably  Trebizond  or  Sumos  scammony,  which  diflVrs  very  much  in 
appearance  from  ordinary  itcummony.  Virgin  scaramany  occurs  usually 
in  irregular  plceei*,  covered  with  a  whitisu  jjrey  powder,  wbit'h  clTer- 
Tcsces  on  the  additiim  of  a  Ktrtmg  acid,  showing  that  the  pieces  hare 
been  rolled  in  clialk  ;  it  i&  friable,  the  fmctured  eurfacci  being  reoin- 
ouA,  ibining,  and  greeidflh  black ;  they  prt'seiit  tmall  air  cavitic^,  and, 
examined  with  a  ma<j;nifying  glasst,  nuineruus  ^rey.  9cmi-tMins{»a.n;nl 
splinters  or  fragments  are  seen;  the  |ii>wder,  viewed  with  ;i  uimrtur- 
iiich  object  gla^,  is  observed  to  conni^it  ol'  numerous  anguiur  and 
resinous  frajimenl^  of  a  ;;reyish  brown  colour  and  of  variable  Hixe 
(Jig.  208.);  intermixed  with  ihc^c  other  fra^menl«  Bometimea  occur, 
which  are  bliickish  or  even  quite  black  :  these  arc  best  seen  when  ibe 
powered  scammony  U  viewed  as  an  upnqne  object.  It  has  been 
(iup];e»ted  by  l>r.  Uutael  ibat  ihiit  <lilferenre  is  the  result  uf  dif- 
ferent melhodt  of  drying,  an  ejKplanation  which  is  certainly  not  cor- 
rect. 

The  black  pieces  in  question  undoubtedly  consist  of  broken  massea 
of  vegetable  liMue,  in5Urated  witli  the  resin,  »&  may  be  fihowii  by  the 
action  of  sulphuric  ether,  which,  by  diiuolving  out  the  resin,  reveala 
the  tissue.  Although  even  the  best  scanmtony  usually  cimtuiua  u  »ma]| 
number  of  these  fru^iuente^  yet  we  have  observed  that  they  are  mua( 
abundunl  in  the  inferior  or  adulterated  sorts  In  the  residue  left, 
after  the  removal  of  the  rettin  by  sul]iburic  ether,  cnnsiderable  quau* 


I 


Mnl.  Ob*,  lod  llH).  tol.  (.  pt  18. 


SCAMMONT,   AND   ITS  ADULTERATIOX8. 


649 


titles  of  vegciahle  tissue,  oyllylar  tissue,  woody  6bre,  frajnnents  of 
spirul  vesseb,  and  stellutu  ci'll*.  uiuy  ri-et|iiuDily  be  detected  by  ibe 
microscope. 

fig-  3M. 


Pun  or  ViMtii  SCAMJtoar  In  powdrr.    JtUftiiSM  Un  dlamcttra. 


Character*  and  CompontioH  of  Scammvny. 

With  water,  or  laliva,  scammony  yields  a  milky  fluid ;  it  readily 
txkes  6re,  nud  burns  with  a  Tellowish  llume,  leavintr  a  minute  |>ortioii 
of  a!«h  niily  when  incineruled  in  a  crucible  —  rarely  ex(«edinn;  three 
percent.  Its  odour  h&s  been  compared  to  old  cbee^te  ;  ila  tn»le  is 
sli<j!ht  Hi  first,  but  atierwanis  aorid  ;  it  is  not  rendered  blue  by  io<line, 
nor  does  it  eflervesce  witli  hydrochloric  ttcid.  Sulphuric  ether  ^huuitl 
eeparutt^  not  less  tliun  78  |H.'r  cent,  of  e.\lrnrt,  rouMAtin};  priiieipnlly  of 
revin.  Pufx-r.  wetted  wilh  atietlierial  or  alcoholic  solution  of  seunimuny, 
•hould  undergo  no  change  of  colour  when  exposed  to  the  orange  fumes 
of  nitriu  ai*i<l. 

The  lollowing  are  the  r^uUs  of  the  analyses  of  three  samples  of 
scamtuDoy  by  Dr.  ChrisCtson :  * — 


I 


*  DtApcoaaUwy. 


Os   T/ 

*^'cfa  do  not  1 'f?P'«* 

a  hn,.„..         " /"^"""num.  _   ' 


BCAMMONY,    AND    ITS   ADULTBRATI0N8. 


651 


'Phnrmaceuticiil  Society  is  a  ftpccirnen  orMfimmnny  which  is  puppoaed 
to  be  adultcralcd  with  tri^ai:iuiLh  ami  some  resin. 


llc«iitii»iT,  Umlf  kdaltfnitnl  with  «riW<ir.  and  probablr  Irutit  Bmrert.    q  «, 

hrnkrn    (tikifntwiti*   uf   •rainniiiiiy  i  h  h,    •Imrrh  >iir|iu«:lr*  of  vrlMSL  |  r  c,   bladl 
fra^menu  of  ctlluUr  Umuc.     Mafuiflril  £!U  tliuntUri. 

**  Indian  St^mmony.  —  From  ray  frii'iid  Dr.  Royle  I  have  receiTcd 
a  snmple  of  sciiiinKiny  met  with  in  fhe  Indian  baxnnrs.  It  U  lijfht, 
porni»«»  nf  a  preetiinh-jfrey  rnlimr;  pritty  nn<1er  the  t<*eth,  a«  if  con- 
tainin;:  n  i-nnHuKTublu  rjuHntily  of  sunfJ,  anil  bavinj;  a  huNamie,  oil- 
banum-lilce  (xlonr. 

"  FncUtumH  Setimmony.  —  To  this  dtvieion  belongs  part  of  ihe  90* 
callt'«i  Smyrna  $aimmony  of  coiitinent4il  fommerre,  as  well  as  Freitch 
or  Moiftpellier  scammony.  I  have  met  with  three  samples  of  fnctiiious 
•cammnny, 

"  Unrlvr  the  name  Smyrna  Mcnmmony,  I  purchasc<1  of  a  London 
dealer  a  »nrt  of  scanimonv  in  the  furnt  of  L-irciiliir,  flat  oiikcs,  n1>nat 
hmtf  aninch  thick.  It  is  blaikrsh,  and  hiL%  cxternnllv,  a  Fliittr  appear- 
ance :  it  breaks  with  diffii'iilty;  iis  fra'.'tiirc  itt  dull  rind  bhu'k  :  int 
specific  gravity  is  1*41*2.  Moistened  and  rubbed,  ic  evnivea  the  smell 
of  guaiacum.     Boiled  with  water,  it  yields  a  tarbid  liquor  (which  is 


8CAMMONY,   AND   ITS   ADULTERATIONS, 


not  renderetl  blue  by  iodine),  and  depoflita  a  blockish  powder:  (b« 
Utter,  boiled  with  alcohoi,  yields  a  solution,  wbich  becomes  nreenub* 
blue  on  the  additiun  of  nitric  acid,  showing  the  presenei;  of  ^aiacuoi 

**  It  is  probably  the  common  Smyrna  tcummony  (Scmunioniuni  Siuti- 
nense  fnctitiiim)  of  Griiy^  who  directs  it  to  he  made  with  Aleppo 
»cainmony,  one  pound  ;  exirnct  of  jalap,  five  pounds;  guaiucum  refill, 
ten  pounds;  sugo,  ion  pounds;  and  ivory-blafk,  four  ptiuDdit. 

"  Under  the  name  of  Scamntonium  Smynicnse  medicinale  ocmdt,  II. 
Batka  ha>  presented  tu  the  Hmrninceutiual  Society  a  spurious  acan- 
inouy,  said  tu  be  made  up  of  gum,  bread,  scamoionjr,  guaiacwB, 
benzoin,  wax,  sand,  and  wood. 

"  French  or  Monfprliitr  ScammoHy  (Scainmonium  Oallicum  »ru  yiont- 
ptliacum).  This  .substance  is  mwle  in  the  snutbt-rn  parts  of  France; 
with  the  expressed  juice  of  Cynnnchum  Monspeliacum^  mixed  wii^ 
ditTerent  reiiins  and  other  purgative  &ub&tjinces.  It  occurs  in  aemi- 
circulur,  blaukish,  Imrd,  compact  cakes,  which  frequently  bave  the 
amell  ut'  balnam  of  Peru." 

RetuU$  of  the  Sxaminatiotu  of  Samfdet. 

The  following  conclusions  were  deduced  from  nn  examinfttion  ft' 
Thirty  suuiples  of  Sc&mmony,  as  iui[>orted,  as  vended,   and   as  wU 
injiowder. 

That  out  of  the  thirteen  samplefl  ol'  Resin  of  Scammouj^  a^  imported, 
submitted  to  examiniition,  one  only  vrii^  gmuine ;  it  yielding  70*60  per 

It.  of  reitin,  the  active  prim  iple. 

7hat  eleven  of  the  sainjites   were   more  or   le«a   adtdterat^  i     H^ 

louni  of  iiilulteriuion  varying  beiwetn  8  and  75  per  ccnl^  and  tbe 
pHMHirtion  of  rcain  between  13-^0  and  72"00  per  cent. 

That  vne  ftaiiiple  was  entirely  factitiuuM^  beiiiii  composed  of  tlie 
resins  of  ^Hoiaaun  and  jalaps  with  much  woody  jSbrt,  celiular  tismt^ 
and  other  insoluble  vuttter. 

That  the  adulteratin);;  ingredients  delected,  consisted,  for  tlie  most 
port,  of  carbonate  of  lime  or  chalky  iind  wheaijiuury  witli  sometiiaea 
taiul^  or  other  enrtJty  mbHtance^  gfUfn,  and  c*onaidcrable  quantities  of 
Kootiy  fibre  and  cellular  tisittie. 

That  of  the  seventeen  *ianiples  of  Powtiered  Scammoyy,  purchased  of 
various  chemists  and  dru;i;:i»t»,  unaly»ed,  oite  only  wits  genuine^  it 
alTordiJig  7(!*40  per  cent,  of  resin. 

That  the  whoU  of  the  retnainin<r  snmples  were  adulterated^  frequently 
to  an  enormous  extent;  the  iLdulierating  in^^redient-s  cnn.Mituting 
from  18  to  (>5  [ler  ccnL  ofthc  entire  arliite,  and  the  it'sin  varyiiij*  from 
27'20  to  Go  60  per  cent.  —  that  is  to  any,  Kome  of  tlie  ftamples  con- 
tained little  mon^  than  one  fourth  the  projier  quaniity  of  hcaininony, 
and  of  court'e  were  deficient  to  that  extent  of  the  active  pruptjrties 
which  they  should  pOMiess. 

That  the  adulterating  ingredients  in  these  samples  consisted  pi 


8CAUMONT,  AND    ITS  ADCLTEBATIONS. 


653 


«ipa)Ijr  of  enommus  qunntitie*  of  wheat  Jlovr^  with  fre<]UontIy  much 
chalky  and  occasionnlly  sand  or  ullicr  earthy  nubslnnce^. 

Mr,  Eli^rrin;;,  !!<{H.*akin^  of  the  afluhcTHtion  uf  scainiuony.  sUtes 
in  his  evidenre  heCore  the  Parliiimfntiirv  Coinuiitluo,  **  We  have 
9nmc  iniporteri  wliieh  hns  contained  from  80  to  90  f>er  cent,  of 
clmlk."  Mr  Herring  nUo  stnU'ft  thut  there  is  ten  or  Iwcntv  times  lu 
«rreat  demand  for  the  spurious  and  cbeap(.T  article  fl»  fur  the  other, 
riie  priee  in  the  market,  he  observes,  is  one  great  erilerion  of  purity ; 
scaiumuny  varies  from  Ha  to  40«.  per  lb.,  aud  opium  frou  9«.  to  26j. 
per  ]b. 

We  have  now  to  ascertain  who  are  the  parties  that  practise  th«e 
atlulteraiions. 

Fmm  the  fact  that  the  majority  of  the  samples  of  gam  resin  of 
scamnmny,  a5  impurted^  contain  chalk,  and  sometimes  wheat  (Inur,  &c., 
it  is  evident  that  these  ailultcrutioiia  are  practised,  to  some  extent, 
before  the  article  is  brought  into  the  Kn<;Iiflh  market.  In  reference 
to  this  point,  we  meet  with  the  following  information  in  Pereira's 
"  Materia  Mwliea";  — 

"  Of  thit*  entirely  pure  soammonj,  says  Dr.  RusscI,  but  very  little 
is  hrou^rht  to  market^  the  frreatcr  part  (»f  what  is  ti»  be  uiec  with  being 
adult4>rat4?il,  if  not  by  those  who  gather  it,  by  those  wlin  buy  it  of 
them  nbroiid  ;  fur  the  chief  part  of  what  is  brought  hither  posses 
throu'.'h  the  hands  of  a  few  people,  chiefly  Jews,  who  make  it  their 
business  to  go  to  the  villages  of  anv  nnte  near  which  the  scammony  is 
etilh'CtwJ  (as  Antioeh,  Sho^jre,  Elil),  Maraash,  &c.),  and  ihere  buyin;^ 
it  whrle  it  is  yet  soO,  they  have  an  opportunity  nf  mixing  wilh  it  »iich 
other  things  ta  suit  their  purpose  best  —  as  wheat  Hour,  ashes,  or  fine 
sand,  all  of  which  he  found  it  niixei)  with.  But  there  seem V*  he  adds, 
"some  other  injn*edient  (possibly  the  expressed  Juice),  which  makes  it 
so  very  hard  and  indissoluble  that  be  was  not  able  to  discover  it  to 
his  satisfaction. 

"  I  have  been  informed  by  a  Turkey  merchant,  who  formerly  re- 
sided at  Smyrna,  th^it  scamniony  is  brought  into  Smyrna  in  the  soft 
state  on  cumels.  Here  it  is  mixe<l  wilh  various  impurities  by  persons 
(«Tew!i')  who  are  denominated  scoiumony  maker;!,  and  who  a<iulterate 
it,  and  thereby  lower  its  value  to  suit  the  miirket." 

It  is  equally  evident,  from  the  analyses  given,  that  scnmmonv  under- 
goes further  adulteration  affcr  its  arrival  in  this  eountrr — ihi.s  eou- 
sisting  principally  in  the  addition  to  it  of  targe  quantities  of  wheat 
flour. 

We  may  here  observe  that  in  some  cases  it  is  qiiile  possible  to 
determine  whether  (he  ofldition  of  the  flour  has  been  made  "(iiHwquent 
to  its  impnrttition  or  not  by  the  condition  of  the  starch  granules. 
When  starrh  in  added  to  scamnmny  abroad,  it  is  mixed  with  it  while 
the  re»in  is  sof^ ;  the  granules  thus  become  embedded  in  und  coated 
with  the  resin  in  a  manner  from  which  no  subsequent  powdering  can 
entirely  free  theiu. 


654 


8CAMMONY,  AKD  ITS   ADULTEBAT10K3. 


On  the  other  bnnd,  when  the  starch  baa  been  added  after  iki 
bns  hetMi  reduced  to  powder,  the  grnnutet  and   mawei  of 
retain  their  usual  appcuram-e  and  chnmcters. 

Tht^  Incl.i  brnii^ht  out  in  thi:i  nrlit  le  are  calculated  to  give  rvt  to 
some  {t<^n<mH  i-efl(>rtinns  ;  tor  if  )idult4.'nitions  exiifL  in  <<lher  ttnfcflnt 
arlick's  of  tlie  Miituiia  Mcdicfi  to  anything  like  the  same  eiVftL, 
iben  thire  is  inlrtiduced  into  the  treatment  of  di»ea?«9  eniflos  na* 
ceriaintieft  and  diH'ereiices  through  the  varying  strength  and  atuoa 
of  rentedie«. 

The  jirivper  doses  of  rfmedios  are  usually  determined  }  •■•  •*  ■  —■■ 'tii/ 
repejited  und  rarcfulJy  lOiidiicted  experiments  with  <tr  ^ui' 

cuH  of  ascertained  purity.    Tlieae  resulta  are  re(i>;niiM?d updB 

by  the  p^oft•^9lon  at  largo  ;  but  whai»  in  the  face  of  such  fncii  u  ir 
referred  to  in  ihls  und  the  preceding  article,  is  ibe  pruc-tii'sd  lalneitf 
such  results?  for  we  see  (bat  the  slrengtli  of  tbe  aauic  reiucly.  trm 
adulterutiim  only,  sometimes  varies  oa  one  to  four — ttii:  i',  fonj 
grains  in  some  cases  will  not  be  stronger  than  ten  of  lli'  'as. 

No  wonder,  tlirn,  that  the  phyRician   is  so  often   di^-:*!'  tb* 

effects  prnihiceil  hy   his  pret*cripti(tn,  and  that  the  patient  e*-      *     j' 
aonictiirii>i»  Umk  with  di^triiEtt  on  his  metlical  iidviser,  who««Ni..i.  i.<:. 
xnd  cxpectitiioDA,   with  retpect   to   the   action  of  fats  miii.4ici^  s> 
fro(iueinly  fail  to  be  realised. 

Here,  loo,  we  meet  with  an  explanation  of  the  extraordinary  doMl 
in  which  certain  remedieA  are  reported  to  Ite  u^ed  by  different  fnoi- 
tioners ;  some  teUint;  us  that  tbey  prescribe  enoi  iiMmt)  ilnevs  of  cahml, 
cluterium,  opium,  sianinmny,  &c.,  und  find  only  tbe  ordinary  etft«t»; 
hence,  such  phv.oiciunM  are  feil  to  conclude  (hat  tbe  reiiivdv  ts  rwal  l» 
at'tive  118  described,  nverhxikin;;  in  gciiend  llie  exi'itcnce  4>l'  adulters 
lion,  and  arc  even  imluoed  to  entertain  serious  doubts  with  ropettt* 
the  general  efficacy  of  medicine.  Under  5ucb  circuut5tani1^s  it  « 
useless  for  the  physician  to  consider  carefully  the  a;!e,  streu*:iiu  lAJ 
condition  of  his  palient  ior  the  purp<)?e  of  apportioning  c-ornsnJ?  tk* 
doses  of  the  remedies  contained  in  bis  prvBcription  ;  loti  otl«B  (^ 
adulterator  ^tep!l  in  and  renders  all  attempt  at  cnlcuUtiun  fiiiilc 

Neither  with  safety  can  the  prescriber  venture  to  net  on  the  pcf- 
aumptiun  that  certain  medicines,  being  ordinarily  ndultcralctl.  iMiyU 
■dtninisiered  in  more  than  the  lecojjnised  do»e>  for  as  it  i«  ju«tpM> 
sible  that  lie  may  secure  a  genuine  article,  as  great  an  error  wotil/ he 
cuniniitted,  perhap.",  by  such  a  proceeding}  as  by  an  adhervnof  to  tibc 
UBiiid  practice. 

The  ffiim  resin  and  powder  of  scnnimony  being  sn  extct\»irrU  vfail- 
terated,  it  of  course  follows  that  all  ibe  other  articles  of  ibe  Malerii 
Medicu,  into  the  compoaiiinn  of  which  scammony  entcni,  aa  cvrnfrtAt^ 
of  ncammotiy^  scammony  tcitfi  caiomel,  and  compound  aem 
powder,  are  similatly  adulterated,  their  properties  and  ttrcngtli 
thus  rendered  very  uiicertaiiL 


SCAMMONY,  AND   ITS    ADULTERATIONS 


653 


On  the  Detectitm  of  the  Adulteratum*  of  Seammony. 

The  Adulterations  most  frequL-nilj  prnctised,  anil  the  detection  nf 
which  is  therefore  most  iroportaittf  are  those  by  chalky  sandy  »Utrehy 
guaiantm,  ntitijaLip. 

riie  chalk  may  Im; deleft e<!  hy  the  efTerveicence  oocoAloned  on  tire  ftd- 
ditinn  oC  jiL'L'ticor  hyiJrochloric  arid.  The  di»en;»ageinentof  the  curbnnic 
acid  i?*  wrll  seen  in  unnute  r|iiantitit's  of  ihe  powdeieil  scainniony, 
wetted  with  the  a«:iil,  nnd  watched  under  the  niicr(i>i'0[>e  wiih  mi  inch  or 
half-iiiehohjept  j»lasH.  The  per-cemnge  ot'ehulk  cnntaincd  in  any  8«inple 
tttny  be  det-Tiiiinod  in  severul  wiivii.  C'hiiik,  well  incinonted  ac  a  red 
heat>eynei;talivin  combinution  williorpmic  mutter,  is  reduced  to  caustic 
lime.  The  uvh  of  well  burned  s''»ininoiir,  adtilteratetl  with  clialk,  must 
therefore  be  bmuyht  tuick  intocurlKinnteof  linieJOOpitrtit  of  which  con- 
sist of  56'29  of  lime^  Bfui  43  7 1  of  carbonic  acid.  The  lime  iont«ined  in 
tlie  scjimm*mj,  when  inriiterated,  nuiy  be  moistened  with  n  drop  or  two 
of  n  saturated  solution  of  carbtiniite  of  ammt>iii;i,  and  a^ain  it^nited  just 
helow  rednezis,  by  wluch  meuns  the  caustic  lime  is  convertcii  into  cor- 
bonaie  of  lime,  the  ummoniu  bein^  driven  off;  or,  lastly,  the  ii.irlially 
decomposed  cnrbonaleof  liine,  prekioiis  to  incinerntion,  may  be  con- 
verted, by  the  iidditum  of  a  little  dilute  sulphuric  acid,  into  ttulphatu 
tit  lime,  whirh  is  not  dicomposetl  by  heiit,  and  the  carbonnle  cidculiited 
from  it.  When  Mulfifietff  of  time  is  piettenl,  this  must  be  di<«MiIved 
in  a  ttmall  quantity  itf  hydr(M*hloric  acid,  dim)  the  sulphuric  acid  precipi- 
tated ty  means  of  ch>ndc  of  barium  or  nitrate  ofbnryla,  and  the  lime 
hy  oxalate  of  ammonia,  the  precipitatca  being  calculated  fur  sulphate  of 
lime. 

\[ garni  be  present,  it  is  in  general  Ruflicieiitly  indicated  by  its  inso- 
lultility  in  tiydrochluric  ai-id.  Where  sulphate  of  lime,  sand,  or  other 
earthy  matters,  are  employed  separately,  ihe  weight  of  the  ash  suffi- 
ciently inilirntes  the  per-centage. 

The  xtnrch  is  detectefl  by  the  addition  of  iorline  fo  the  cold  decoc- 
tion ;  but  it  is  only  by  the  micniACojH;  that  the  kind  of  starch  emfihiyed 
con  be  determined.  The  presence  of  dcj-trine  is  rcvcale<l  either  by 
the  microscope  or  by  iodine.  Gumaaim  is  discovered  by  its  smell, 
when  rubbed  down,  or  by  a  piece  of  j>;iper  niiiislened  with  the  tincture 
becoming  blue  when  ex[)iiSL*d  lu  nitrous  hcid  rinne'*.  Jalap  rexin  is 
iniuilubje  in  ether  and  oil  of  turpentine  ;  di^'e>te4l  in  u  watch-glass,  with 
oil  t)f  vitriol,  a  crimson  cutourcd  solution  is  obtained. 

Siammony  i:^  tree  of  duty,  as  are  nl^o  all  drujr^  unenuroerated.  and 
among^t  titcm  those  treatetl  of  in  the  following  articles,  namely^  julnp, 
ipccacuunha,  rhubarb,  eolocynth,  and  squills. 


656  JALAP,    AND   ITS  ADULTERATIOX^ 


JALAP,  AND  ITS  ADULTKHATIONS. 

The  true  julap,  Exognnium  purga^  belongs  to  tlie  natural  order 
Conpolruiacetc,  nnd  is  clngL'lv  allied,  both  in  its  botanical  relations  and 
nropertitfiif  to  CoHVoloudts  scamnutnia,  ]t  is  n  climbing  plant,  with 
Drancbcd,  annual  ctcnis,  and  tuberous,  perennial  roots.  It  );rows  in 
the  woods  of  Mexico,  near  Chicanquiuco,  at  an  altitude  of  nearly 
6000  t'eet  Hl>ove  llie  level  of  the  8*?a. 

The  part  of  the  plant  euiploved  in  medicine  u  the  tuber.  When 
recent,  the  tubers  are  irre^rularfy  ovate- conical,  are  covered  by  a  thin, 
blackidb  epidcnniti.  numerous  rootlets  or  nulicles  si>ringin^  froni  their 
lower  flurluce;  while  iiilerually  tiiey  are  ileshy,  wuite,  and  obvcureJ/ 
laniiniited. 

The  dry  tubers  rnry  in  size  from  a  nut  to  on  omnge,  the  largest  oc- 
casionally exceedinjr  a  pound  in  weight.  When  entire  they  are  usuaUy 
oral,  the  extreinitifB  bein{»  more  or  less  pmlonjred  or  pointed;  they 
are  wrinklci],  anil  covered  by  the  blarkish-brown  epideruiip.  The 
larger  tubers  frequently  exhibit  several  incisions,  made  for  the  pur- 
pose uf  fucilitaiing  their  exsiccatiun.  InTernuily,  Ihuy  present  nume- 
j*ous  concentric  rings,  arising  fmui  tli**ir  tutiiinaied  structure. 

Tubers  of  good  quality  should  be  firm,  solid,  and  heavy,  and  when 
broken,  of  a  deep  yellowiBh*gi-ey  colour,  with  a  somewhat  resinous 
fracture.  When  very  light  they  are  usually  hollow,  from  defective 
trying  ;  when  white  and  triable,  they  contain  cxcfss  of  starch,  and  are 
of  inferior  quality.  Sometinies  (he  tubers  are  imported  in  Alices, 
which  appear  to  he  quarter  segments,  according  to  Fereira,  of  trut^ 
▼ersfi  slices  ;  this  vaiiety  is  (M'tniiionutly  called  fpunoua  jalap,  or.  from 
its  >h ape,  ct}cktd-hat  Joltip;  and  like  tlie  tubers,  when  while  aiid 
friable,  the  slices  are  niferior.  The  lubi-rs  are  very  liable  to  b*»  at- 
tacked by  worms ;  as  the^c  do  not  touch  the  restnt  it  is  to  be  obtaiued 
from  such  tubers  in  nrprmal  quantity. 

The  only  market  for  j:ilap  is  iTalapa,  a  town  of  Mexico,  from  which 
jalap  takes  its  name,  and  from  whence  it  is  imported  by  way  of  Vera 
Cruz. 

Structure  of  the  Jalap  Tuber, 

The  minute  structure  of  the  julap  tuber  is  very  characteristic,  and 
it  is  ni>(-(>^ary  that  tlu'  ubi^erver  should  be  thoroughly  acquainted  with 
it  bi'fort:  he  will  be  able  to  detect  the  adulleralious  to  which  jalap  in 
powder  is  liable. 

Tlic  e[)idermis  dnes  not  differ  materially  from  the  same  structure 
IS  it  occurs  in  many  other  plants,  it  consisting  of  what  we  are  in 
Ike  habit  of  denominating  stellate  cells,  of  un  elongated  form.     It  is 


JALAP,   AND   ITS  ABULTERATIOKS. 


fl57 


but  seldom,  however,  that  these  cells  can  be  detected  in  the  dried 
tuber. 

The  lamellEB,  viewed  in  transverse  sections,  are  seen  to  be  conipoeed 
print'ipiUty  of  cuiln,  witli,  along  the  iU8r;;in!i,  occaaionitl  buniUus  of 
dutttid  vessels  onJ  woody  fibre.  The  cella,  of  which  the  inber  itstilf 
is  almost  entirely  composed,  are  not  ail  of  one  kind.     First,  there  are 


Tiuwrcnc  hmIob  of  J*LAr  Tcitu,  iliovlni  ike 


ftpMumaot  utd  dtfttlbvtioa  of 
■  iuAmI  M  ilUnietcn. 


numerous  well-defined,  dark,  and  sooiewhiit  angular  celU  lying  here 
and  there  in  the  uiidsi  of  the  other  celU.    Fig,  tiilU. 

u  V 


658 


JALAP,    AND    ITS   ADULTEEATIONS- 


The«e  cells  appenr  to  contnin  resin  ;  but  since  tbey  ore  slowly  uied 
upon  by  water,  so  that  frnm  beiiij;  ilark  and  opaque  tliey  become  cUar 
and  transparent,  it  ia  evident  that  tfaey  also  contain  some  soluble  nt^ 
stance. 

Of  the  remaining  ceUs,  many  arc  apparently  empty ;  tbne  cOMth 
lute  cliiefly  the  outer  luinellse  of  the  tuber.    F"*^,  210. 

Lastly,  other  cell»,  crowded  with  ttturcb  corpuacleii,  occur  in  gifit 
abundance  ;  the  innermost  layers  of  the  tuber  nre  chiefly  coukjpoteAii 
these  cells.     Fie.  211. 

The  resin  ceUa  are  scattered  throughout  the  wh»le  of  the  tab«, 

Fig. i\l. 


■Tnnwnnt  •ecHoo  of  Jtur  Tcbki 

crlh.m%t:aiRt4  lOU  dUmrttrra 


;■.  abovlnf  the  ((on*  ndfc.  M4  •!»  *•  "■* 
In  U.e  lo«»f  P*rt  n#  llit  Ofun  tte  te«  aH 


dlfttiivif  n. 

occurring  indiflercnlly   in  the  raidst  of  either  the  tt^pntnUjf^^ 
ceUfl,  or  those  filled  with  fitjuxh. 


JAJLAP,    AND   ITS   ADULTERATIONS. 


Go9 


The  stu*ch  corpuscles  are  of  considerable  size,  and  possesi  well- 
niArkcd  characters.  Some  are  circular,  but  »oniewhiit  rtaftenpd,  while 
o:]iers  are  muUer- shaped.  Thesp  last  are  occasionally  united  in  tnos^ 
ihrees,  and  fours  ;  whenever  mullcr-^bapcd  starch  corpuscles  are  met 
will]  in  Hni^  vegetable  tissue,  it  is  to  be  understood  that  they  were  all 
orijTinQlIy  united  in  this  manner,  and  it  is  to  such  union  that  their 
f*irm  18  chiefly  due.  Thvy  are  all  furnished  with  a  distinct  hlluni, 
nround  wliirh  one  or  two  concentric  rings  may  sometimes  be  seen 
(yfj^ji  il  1,  21i!.).  Many  of  the  corpuscles  in  every  tuber  have  become 
expanded  and  tuis^hapen  from  the  hjat  employed  in  the  process  of 
drying. 

In  f^nuine  powdered  jalap  all  the  structures  above  described  may 
be  dcteute<i :  the  stellate  ccUs  of  the  epidermis,  the  resin  cells,  the 
empty  cells,  those  filled  with  starch,  numerous  free  starch  corpuscles, 
anti  occaaional  fragments  of  dotted  vessels  and  woody  fibre.  The  oc- 
currence of  single  cells  completely  filled  with  starch  corpuscles  is  very 
characteristic  of  powdered  jalap. 


KtiiMta  mil  Htm  ■trantaw  moA  tUMfto  faoad  In  Oawrms  Towvmucp  JaLaf.  o. 
)«  WHl  mwmn  of  0»  mm*  slMrcd  by  he*!  i  /.  fracBMB*  «  dotted  dtut 

It  should  be  particularly  remembered  that  the  tuber  of  jalap  is 
a  0  S 


uo 


JALAP,   AND   ITS  ADULTERATIONS. 


made  up  almost  eatirely  otcelltdar  tutnte,  with  but  few  dotted  veneh^ 
and  extremely  little  woody  Jihre^  tbe  Bbres  being  hur^e,  coarse^  and 
dotted,  closdj  roscmbling,  in  fact,  except  id  size,  tbe  ducts  them- 
selves. 

Conpotition  of  Jalap. 

Tbe  jalap  tuber  owes  ibi  activity  as  a  purgative  principally  to 
resin  whirh  it  contains. 

The  following  arc  some  of  the  principal  analyses  ofjalap  which  hai 
AS  yet  been  made,  that  by  Gerber  being  the  most  complete ; 


Oerber's  Analyns,  • 

Hard  resin          -            -            -            .            -  7-g 

Soft  resin            -             -             .             -             -  3-2 

Slightly  acrid  extractive              •            -            .  17-9 

Gunim^  exiraetive          -            -            -            -  1 4*4 

Colourinff  matter            ....  s><| 

Uncrystalli  sable  sunr   -             •            -            -  1  -9 

Gum,  with  some  salts      ....  15*6 

Bassorin    -         -             -             -             -             -  3*2 

Vegetable  albumen        -             •            -            -  3*9 

Start'h    ------  6*0 

Water    -----            .  4-8 

Malic  acid,  and  malatcs  of  potash  and  lime          -  2*4 

Chlorides  of  calcium  and  potassium        -             -  1  *4 
Phosphates  of  mnffnesia  axHl  Umc             -            -17 

Carbonate  (?)  of  Kme     •             -            -            -  3*0 

Loss      -            -            -             -            -             -  4-6 


Jalap 


1 00-0 


Henrifi  Analyiu.  f 


Rmln       -             .             .             .              . 
ExtracUve             .... 
SUrch      ..... 
Woodyfibra           .... 

LKCM. 

SMBd. 

—         II    MM 

11 
lb 
10 
M 

9-6 

I0-4 
42-0 

14*4 

Ift'O 
SOI 
40-0 

IM 

100*0 

1«M 

- — 

•  Ginelin,  lUndb.  d.  Cbnnir.  bd.  fi.  1.  IM. 
t  DaU.  de  Phvm.  t.  U.  ft.  97. 


JALAPf  AND  ITS  APULTERATIONS. 


661 


Ledavoiis  Analjftit.  * 


Resin  - 

Gummy  extract 
StJirch 
Albumen 
Woody  fibre    - 
^Vftter  and  loss 


M&lo  Light, 
Fukliorm  J«Up. 

-  8-0 

-  25-6 

-  3-2 

-  2-4 

-  56-0 

-  28 


Julap 


100-0 


Nee$  D.  Esenbeck  and  Marqnarfs  Analyses,  f 


Rutractlre    .             .             .             - 
R«in             -               .               _               . 
U«Ucr»  liuolable  In  alcohol     . 

J.top              -              -              . 

i^JSl.-.™ 

■ 

rate 

t7-ao 

I«f33 
75W 

100-000 

100-00 

KKMtO 

Guihourft  Analyna, 


LlquM  ittfar  hr  alcAhnl 

Brawn  McchsHiw  estrmct  obtained  bjr  wsur 

Gam  ..•-.. 

Stanh              ..... 

WMdrMre 

Uwi                 ..... 

Jalap                   .... 

«^.^ 

SMtt 
10-lt 

m-7* 
a-f)o 

4600 
1-81 

100  00        1        lOO-OO 

From  the  above  mnalyies,  some  of  which  are  not  very  complete,  it 
is  evi'lent  that  the  umuunt  of  rosin  fuunil  in  jfilap  is  Hubject  to  con- 
•itlerable  variation;  further  analyses  of  the  tuoer,  in  different  states, 
are  still  much  needed. 

It  wilt  l>e  noticed  thut  the  womly  6bro,  in  some  of  the  ftnolrseSf  is 
put  down  at  a  very  high  fiirure.  The  u^ual  practice  is  to  consider  all 
matters  not  soluble  in  ether,  wau^r,   or  alcohol,  except  starch,  as 


■  Jouni.  dr  Cbim.  Mrd.,  t-  t.  f.  MM. 
t  Fharm.  Outr<l-SkU  lUr  IBM.  a.,09A. 
U  U3 


662 


JALAP,   AND   ITS   ADUI-TERATIONS. 


woolly  fibre.  This  practice  is  as  objectionable  as  Ute  one  wc  bre 
already  had  occasion  to  comment  on — namely,  the  use  of  thcnnl 
**  traces**  to  designate  all  the  organic  matter  eonlaincd  in  water.  la 
the  present  case,  the  actual  quuntity  of  woody  fibre  rarely  arootabUt 
one  per  cent.,  tl^e  tuber  being  mainly  composed,  as  alreatty  putnttii  «at, 
of*  cellular  tiisue. 

Jalap  resin  may  be  prepared  in  the  following  manner : — Tbc  rm 
together  with  other  extractive,  is  tlissolvod  out  by  alcohol;  to  ili 
alcoholic  solution  water  is  added,  which  preeiphates  the  resin;  ikiib 
washed  in  warm  water,  and  re-di»8oived  in  alcohol ;  or  the  alcukfr 
solution  may  be  at  once  decolourised  by  animal  charcoal ;  tbr  M 
methoJ,  however*  is  the  best,  ns  by  it  all  the  sugar,  &c„  whidi  an 
be  present,  as  well  as  nio^t  of  the  colourinj?  matter,  U  got  rid  of. 

Jalap  resin  is  charaeterised  by  the  following  propertir* : — It  ii 
soluble  in  alcohol;  insoluble  in  water,  ether,  the  6x<*«l  ami  voliA 
oiU,  including  oil  of  turpentine;  triturated  with  milk,  it  doeanoCim 
an  emul&ion  ;  dig&Hed  in  a  watch-jtlass  with  sulphuric  arid,  a  cnaMi 
coloured  solution  is  obtained,  this  being  a  very  distinctiya  t«*t.  Fnm 
scammcMiy  resin,  it  is  distincuiahed  by  its  not  forming  an  OMiUh 
with  milk,  and  by  its  ins<»Lubility  in  oil  of  turpentine.  It  ia  aoij  labc 
sometimes  adulterated  with  guaiucum,  which,  unlike  iah4i  rain,  il 
soluble  in  ether ;  and  paper  moistened  with  the  alooholic  »alalid% 
exposed  to  the  fumes  of  nitrous  acid,  turns  blue. 

According  to  some  obserrera,  aa  Buclmcr,  Herber^cr  *,  and  K45* 
serf,  the  so-called  jalap  re&in  is  a  compound  body,  and  caraila«f 
two  rcsina,  the  one  soluble  in  ether,  the  other  insoluble  in  that  H^ 
atruum.  In  relation  to  these,  we  meet  with  the  following  partiodBi 
in  the  third  edition  of  Fereira's  "  Materia  Medica :"  — 

^"•Jalapin;  rhodeoretin  (from  ^-r'l.if,  ruse-red,  and  onrir^,  nma), 
C^     H,j  O  jQ.     This  resin  is  insoluble  in  vther.      Kav-        '  ,1  it 

by  boiling  purified  jalap  resin  in  ether,  which  took  up  t  ,id 

and  left  thejahipin.     According  to  Huchner  and  Uerbvn^'vr,  u  w* 
stitutes    not    quite   nine  tenths  of  jalap  resin  ;  it  ia   a  traiMpatatlt 
(colourless,  odourless,  and  tasteless  resin,  very  soluble  in    " 
insoluble  in  water  and  in  uther. 

"  It  does  not  possess  basic  pro[)enics,  as  Buehner  and  H 
suppo^d,  but,  on  the  contrary,  possesses  acid  f^roperties,  reddens  Ik- 
niu>,  and  is  soluhle  in  ammonia  and  acetic  acid.  If  tbe  salt  whidi  it 
forms  with  oxide  of  lead  be  decomposed  by  sulphuretted  bydj  qgi 
the  resin  is  then  found  to  have  combined  with  the  elements  of  waMT* 
and  to  have  l>eccune  converted  into  hydrorhoti^yretan^  C,,  U,,  0,,. 

^*Jahpic  urid^  odorotui  nrincipU  0/ Julap  (f)^  con»t'tium  thirtvOI 
per  cent,  of  jalap  resin.  It  is  a  brown,  soft,  and  frreasy  substase^ 
which  reacts  as  on  acid,  has  the  odour  of  jalap,  and  an  acrid 


•  Ann.  dcr  Chen.  u.  Ph«»..  U.  ti  p.  SU  !•«. 

t  Ftium.  Criiual.BlAU  fUr  IfQI,  &.S84. 


i  aod  rtMim.  Joant.  vvL  H.  f).  atk  i 


JALAP,    AND    ITS   ADULTERATIONS. 


663 


By  long  contact  with  water  it  crystallises.  It  is  soluble  in  ether,  in 
alcohol,  nnil  in  alkaline  sulntioiis,  but  is  insoluble  in  hydrocblorlo 
aciil.     It  i^  cither  a  cryat&Ilij^ulilc,  «ift.  rcsin^  or  a  fulty  aoid." 

Parurhodeoretin^  C^^  H»^  0,ii  w  obiaiiioii  from  ine  male  or  fusi- 
form jalnp,  Ipomaa  OrizabemU  :  it  is  soluble  in  both  alcohol  and  ether, 
unil,  witli  Hufphuric  acid,  exhibits  the  saiue  characteristic  reaction  as 
true  jalap  resiQ. 

On  TBI  Adultsbatioms  or  Jalap. 

Having  now  tn^ated  of  the  structure  and  properties  of  jalap,  wC 
in  a  poaition  to  enter  upon  the  consideration  ol  it*  adullerationt. 

Exogotmtm  purffa^  or  true  jalap,  is  not  the  only  kind  ofialap 
which  grows  in  Mexico;  there  is  a  second,  a  spuriotu  jalip^  touiid 
there,  commonly  called  rtutle  jalap,  and  which  is  sometimes  exported 
mixed  with  the  genuine  sort.  By  Uuibourt  it  has  been  called  light  or 
/tuiform  jtilap ;  m  English  commerce  it  is  sometimes  known  aa  troody 
jidap  or  jalap  wood;  while  in  Germany  the  term  jai^ip  Mtaiks  haa  been 
lipplied  to  the  upper  section  of  the  tuber,  embracing  the  comiuenoft' 
ment  of  the  stipeXy  or  stalk.  It  is  the  tuber  of  fponura  Ohzedftwrig, 
(Ledanois.)  **  As  met  with  in  commerce  it  is  in  slices  or  sremeota, 
which  are  raoro  tibroua  or  woody  than  {genuine  jaUp.  Tlte  cut 
surface  i^  ofcrn  darker  from  exposure  to  tlic  air,  and  uneven  from 
unequal  sbrinklnj;  in  the  drying  process;  internally  it  ii  whitith,  du? 
odour  and  taatc  being  siniilar  to,  but  feebler  thnn,  true  jaJap,'* 

Guibourl  has  deiicribed  u./aLie  rosC'KCenied  jalap,  the  characteni  of 
which,  according  to  Pereira,  are  as  follows:  —  "It  is  in  tubcrclea 
which  are  not  so  dark-culourcd  as  the  genuine  druR  Tbi-y  are  *Uxp\y 
furrowed  ;  the  prominent  parU  of  ihe  furrows  bein;r  white  from  lh« 
friction  of  the  pieces  against  each  other;  the  depressions  htAiij^  datk- 
coloured.  The  pieces  are  but  slightly  resinous,  arc  amylaceous  and 
saccharine,  and  bare  rather  an  a^eeable  swectinh  odour,  which 
Guibourt  compares  to  that  of  oil  of  rhodium  or  of  the  roee.  It  |k«- 
Besses  scarcely  any  purgative  action ;  it  is  probably  the  kind  known  iu 
the  American  market  as  orergroicn  jalap." 

We  have  here  then  important  aduU^ralions  of  the  very  root  ittclC 
one  of  them  at  all  events  practised  in  Mexico  by  the  dealers ;  wc  shall 
presently  see  whether  jalup  is  not  subject  to  further  adulteration^  th« 
work  of  parties  nearer  home. 


I 


RetuUs  of  the  Examiuation  of  SampltM. 
From  an  exanjination  of  the  analyses  of  Thirty-three  samples  of 
powdered  jalnp.  it  npfMiared — 

That  no  leas  than /'wr/^en  irerr  adidtrrnted,  or  nearly  "»e  half. 
That  this  adulterutinn  wits  in  all  the  sanij)li.'s  of  ilic  same  kind,  and 
consisted  in  the  addition  of  large  quantities  of  wood  in  a  minutely 
dirided  slate. 

c  D  -t 


664 


JALAP,   AND   ITS   ADULTERATIONS. 


That  the  wooH  emplnyorl  in  twelve  of  the  samples  iras  of  the  sat 
kind;  in  the  other  two  snmplra  a  ilifTcrcQt  duscription  was   used,  m 
was  evident  from  the  characters  of  the  fibres. 

That  this  adulteration  amounted  in  some  of  the  samples  to  at  least 
one  third,  the  properties  and  strength  of  the  jolap  being,  of  coan6, 
impnircd  to  that  extent. 

That  one  of  the  samples  yielded  only  6*37  per  cent,  of  extractire; 
and  there  is  therefore  niuoh  reason  to  believe  that  the  resin  hftd  been 
previously  extracted. 

Mr.  Scanlan  gave  the  following  evidence  before  the  Committee  on 
Adulteration  respecting  the  sophistication  uf  jalap  with  giutiactun  shav- 
ings :— 

"  I  discovcre*!,  by  accident,  an  adulteration  of  powdered  jalap  to  a 
great  extent.  1  wtnt  into  a  druggitit's  warehouse  one  day  in  WoWer- 
hamptoiu  and  saw  a  numl>er  ot  powders  ready  folded  in  7  lb.  or 
14  lb.  parcels.  There  was  one  I  did  not  know;  I  :isked  the  wwre- 
houseman  what  that  one  was.  He  lold  me  it  was  powdered  jaJap. 
I  said  it  was  not  ptiwdered  julap.  He  insisted  that  itwu&  I  saiil  *Ic 
IB  not  the  ct)lour  <tf  jidnp.'  I  took  u  comer  of  the  paper  and  movetl 
the  po^ider,  and  I  saw  thiit  tlio  muss  of  pnwder  had  a  dilTerent  colour 
from  the  surface,  I  said  to  him,  'That  is  a  very  curinus  thing.  It 
Ujoks  vt!ry  like  the  effect  which  rays  of  light  prmiuce  upon  guaiacum.* 
The  mail  bt'^nii  to  lini;;h,  and  lold  me  it  was  jnliip  root  and  guaiacuoi 
shavings,  ^ont  m  equal  wt^ights  to  the  mill  to  be  ground  and  void'  oa 
jalap  powder." 

Mr.  Villicra  put  this  question  to  Mr.  Herring,  in  regard  to  the 
adulteration  of  jalap: — 

"  Is  it  true  that  lalap  powder  is  frei|uenlly  adulterated  with  rasp- 
ings of  guaiacum  ? — "  Yes,  latterly ;  even  last  week  the  merchontd 
have  been  imjiorting  an  article  culled  jalap  tops,  which  is  merely  the 
cuttiiigsof  the  tree,  not  the  root,  and  which  has  been  sold  at  "Itl,  per  lb." 

We  have  now  t'>  inquire  who  are  the  parties  guilty  of  adulterating 
an  imjinrtunt  article  of  the  Materia  Mu<Iicii  in  sn  seandalouA  a  manner. 
It  is  evident  that  the  retail  chemists  and  druggists  arc  not  the  parties 
who  practise  this  adulteration,  since  the  aid  of  a  powerful  pulveruinj; 
opperatus  is  required. 

From  the  analyses  we  have  made*  it  is  also  evident  lliat  jalap  is  not 
unfrequently  supplied  by  wholesale  chemists  and  drupgists  in  the  adul- 
terated coudition  in  which  it  is  afterwards  retailed  ;  but  we  are  not, 
in  the  majority  of  cases,  to  conclude  from  this  circiimstance  that  tliejr 
arc  the  partitas  who  practise  the  adulteration. 

As  one  of  the  great  results  of  dur  invt'stif^ations,  we  have  ascertained 
that  a  large  proportion  of  the  adulterations  met  with  are  traceable  to 
the  pn'purers  or  manufacturers  of  the  ditferent  articles  of  Food  and 
Medicine. 

It  hu  already  been  shown  that  most  of  the  vpices  are  lorgelj 


I 
I 


I 


JALAP,   AN©  ITS  ADULTERATIOrrS. 


6G6 


ndnlternted  in  a  variety  of  tnyn.  There  is  no  dotibt  that  many 
of  the  adtiltorntions  delected  were  perpetrated  by  a  class  of  persona 
known  a^i  spice  GRi7iDER<t  Now,  m  the  dru^  trade  there  exists 
a  bimilur  class,  ealled  nnuo  obikdrbs.  It  is  perfectly  evident 
that  an  adulteration  of  tlie  kind  pointed  out  in  the  case  of  jalnp  can 
only  be  practise*!  by  such  grindera,  who  alone  (>omgm  the  luacliinery 
necessary  to  carry  it  into  operation,  'llie  drug  grinders,  then,  would 
appear  to  be  the  parlies  guilty  of  the  adulteration  described  in  this 
report.  The  wholesale  chemists  and  drufigists,  however,  must  not 
be  entirely  acquitted,  for  in  many  cafieft  tney  arc  thenisolve«!  cither 
druif  grinders,  or  they  direct  the  finders  to  atld  certain  adulterants 
to  the  nrtictcs  which  they  send  to  be  ground. 

That  the  drup  grinders  arc  in  the  habit  of  practisin;^  many  adul- 
terations with  various  nrttcles  of  the  Materia  Medica  is  a  matter  of 
notoriety  amongst  chemists  and  druggists,  and  many  members  of  the 
medical  profession ;  and  various  are  the  statements  related  of  the 
practices  to  which  they  have  recourse ;  thus,  it  is  said  to  have  been  b 
common  thin*;  to  send  a  certain  (|imntily  of  an  article  to  be  ground, 
with  a  reiiuest  that  it  should  be  returned  of  a  weight  greatly 
excvoding  tnat  of  the  article  sent. 

In  the  evidence  of  Dr.  K.  L).  Thomson,  given  before  a  Select  Com- 
mittee of  the  House  of  Commons  ap[K>inte(l  in  1838  to  inquire  into 
the  "Administration  of  Kelief  to  the  Poor,"  &c.,  it  is  stated^  in 
answer  to  a  (|ue9tion  by  Mr.  Wakley,  "  that  it  is  common  to  send  to 
the  drug  grinder  eighty-four  pounds  of  julap  to  bo  made  into  a 
hundredweight." 

We  have,  then,  clearly  established  the  fact  of  a  scandalous  adultera- 
lion  in  another  ttnyst  important  medicine, — an  adulteration,  moreaver, 
to  which  no  reference  is  made  in  works  on  Materia  Medica,  not  even 
in  the- most  complete  work  un  the  subject  in  existence — namely,  that 
by  the  late  Dr.  Pereira. 

Whon  to  this  fact  we  add  certain  other  considerations,  we  shall 
perceive  how  great  must  be  the  variation  in  the  strength  and  proper- 
ties of  this  remedy  as  dailr  administered  in  hundreds  of  cases. 

Thus,  as  will  be  presently  tibown,  the  genuine  jalup  tuber  itself  varies 
very  greatly  in  strength,  while  this  again  is  commonly  udulteriited  with 
the  spurious  or  male  jalap,  the  purgative  properties  <»f  which  are  much 
inferior  to  those  of  genuine  jalap.  The  remwiy  for  this  last  adultera- 
tion is  to  prohibit  its  importation. 


Ou  the  Detection  of  the  AdulterationM  of  Jnlap. 

Male  jalap,  jalap  sulks,  and  rose-acented  jalap,  differ  cnnsiderubly 
in  their  microscopic  characters  from  true  jalap,  and  also  from  each 
other. 

In  male  Jalap  the  resin  is  not  confined  to  distinct  cells,  but  occurs 
in  masses  of  irregular  form  aud  size,  of  a  bright  yellow  colour.    The 


666 


JALAP,   AND    ITS   ADULTERATIONS. 


starch  granules  hare  the  same  form  as  those  of  trae  jalap,  but  ore 
smaller  iint]  not  so  abiiii<lant. 

Jah^  Btalka  coiisihI  ohitlly  of  very  beautiftil  dotted  ducts  of  large 
size,  with  dotted  woody  fibre,  mid  a  small  i|uatuity  of  atarcb  of  toe 
same  size  and  form  as  thut  uf  lasiforni  julap. 

In  rosc'Scented  jtdup  nu  distinet  resin  cells  or  masnea  of  resin  occur, 
but  veins  or  streaks  of  coloured  und  jippurently  empty  cells  traverse 
the  tuber,  sections  of  whiih  („-shihit  a  mottled  appearance,  owing  to 
the  intermixture  of  the  rnlnured  and  colourleda  celU.  Ko  starch 
corpuscles  were  found  in  the  single  Bample  of  tbis  descriptioa  of  jaUp 
submitted  to  examination. 

The  autount  of  exLrat'live  obtained  from  powdered  jalap  by  diges- 
tion in  ulct*boi  doea  not  indicate  with  any  certainty  tbe  extent  of  the 
adulteralion ;  since,  alUiough  tbe  adultemted  samples  of  jalap,  aA  a 
rule,  furrtish  much  less  extniriive  than  tbe  genuine  drug,  yet  there 
aro  several  exceptions  lo  ibis:  thiijt,  in  one  genuine  jalap  the  extract 
amounted  Xii*ll-'M\  \>ct  cent.,  and  in  another  to  only  19-32  per  cenL ; 
while  in  uno  adulterated  jalup  it  was  xxa  low  as  iJ  37.  in  another  tt 
reiM.'lied  a»  bigli  as  2jS-84  per  cent.,  these  b<:iup  tbe  extremes  of  voria- 
liun  in  tbe  quantity  of  extrict.  This  difference  is  due  cbietly  to  itiree 
causes : — 

First. — The  quantity  of  resin  and  other  matters  soluble  in  alcohol 
▼artea  very  p-catly  in  different  jalap  tubers,  as  is  apparent  from 
following  analyses :  — 


Firtt  T\iber. 


the   I 


Char.  —  Soft,  resinous,  and  dark  coloured  ;  not  very  heavy,  and 
slightly  worm-eaten.  It  yielded  32*66  per  cent»  of  aieokoUt 
extrocL 


Second  Tuber. 

Char. — Firm,  hard,  rather  whitish,  and  friable, 
per  cent,  of  extraet. 

Third  Tuber. 


Furnished  10-^4 


Char. — Taken  from  the  same  parcel  as  the  above,  the  characters 
being  similar.     It  yielded  17'80  per  cent,  of  extract. 


Fourth  Tuber. 

Char.  —  Heavy,  very  hard,  and  of  a  jrreyish  colour. 
1 1  '08  i>er  cent,  of  extract. 


It  furnished 


The  extracts  obtained  from  powdered  jalap^  although  the  restilts 
vary  considerably,  are  yet  much  more  uniform  than  tbuse  from  the 
tuber,  for  in  the  cai^e  of  the  powder  we  obtain  the  average  extractive 
of  many  different  tubers. 


JALAP,  XifT>   ITS  ADULTERATIONS. 


66: 


Second. — If  llic  alcohol  emplored  contain  water,  u  portion  of  the 
watery  extract,  includicig  even  gum,  is  likewise  taken  up,  and  so  aflecta 
the  pcr-centaKes. 

Xliird.  —  The  adulterating  ingredient  used,  it«clf  yields  a  portion  of 
extractive. 

Willi  tlie  viev  of  determining  the  kind  of  wood  so  extensively 
used  in  the  adulteration  of  powdered  jalap,  we  have  compared  it, 
ainon;;st  other  woods,  with  that  of  liquorice  rooty  lignum  vita  or  guaia- 
cum^  tatin  and  box  wonHn  ;  and  it  is  probuble  that,  in  thi*  majority  of 
case«»  the  wttrxl  employed  is  that  of  lignum  vittp,  which,  being  a  highly 
rt^sinouB  wn<id,  yields  to  alcohol  a  lurge  amount  of  extractive;  thi^ 
wniilil  account  for  the  high  pcr-oentjigea  of  extract  obtained  from 
mtiny  of  the  adulterated  aamplcA  of  jiilup. 


f.>.2U. 


PovrascD  Jauf,  lufltlr  MluUtnUCd  wllti  woo4.  pnbAblr  Ihrt  of  I^wmi 

Mto  tr  gmamctmt.  ■  a  a.  eclli,  ala-nth  carijiuelM,  Ac,  ut  fftlap  i  bit,  Tnt- 
■mto  Mid  Abna  uf  the  vwd.     UafDlStd  XPi  dUinttvn. 

The  characters  of  the  fragments  and  fibres  of  this  wood,  and  the 
api^arance  of  u  sample  of  jakp  thus  adultei-atod,  are  shown  iny%-.  :iia. 


666  IFECACUAKHA,  AND   ITS  ADUI^TERATIONS. 


IPECACUANHA,  AND  ITS  ADULTERATIONS. 

Ipecacuanha^  Cephaelis  Ipecanmnhn,  is  n  somewhat  shrabbf  ploR. 
the  stems  of  irhicli  rcnch  two  or  throe  feet  in  height,  thmvin^M 
runners^  and  are  t'urniehed  with  leaves,  seldom  more  thtn  wax  m 
six  In  nuinbt^r,  placed  near  the  extremities.  The  moU  wkick  as* 
stitulc  the  i|)ecuL:uatdia  of  commuroe  are  perennial,  four  or  six  iaeba 
long,  simple,  or  stirnL'tiinos  divided  into  a  few  liranclies,  and  *U  pw» 
seating  the  strongly  annulated  character  by  which  they  arr  so  reuly 
recognised  and  distinj^uished  from  all  other  medicinal  rooto.  u 
habitat  is  Brazil,  it  Hyeinj;  found  Iwitwcen  8®  and  20°  S.  Ut>  Xlgrovi 
in  moist,  shady  situations,  as  valleys.  The  following  aeeottBt,likci 
from  Martins  of  the  collection  and  gathering  of  tbe  roots  i>pvna 
Pcreira'a  "  Materia  Medica"  :  — 

"  The  roots  are  gntheriul  at  all  seasons  of  tbe  jear.  tliough  laon 
freimentty  from  January  to  March  inclusive  ;  and  as  no  cane  ii  tabl 
in  the  ctdtivatinn  of  the  plant,  it  has  become  scarce  around  tb'*  pfifr* 
cipal  towns.  7'Iiofle  Hrnzilian  funnrrs  who  reside  in  th«  nvjjhtioiir' 
hood  of  the  plant  carry  on  confiiderahle  commerce  with  it  Tk 
native  Indians  also  are  very  assiduous  in  the  collection  of  it.  'Wtm 
called  by  the  Fortuffucsc  the  Corf>ai]os,  who  live  near  tbe  rirer  XmoCi 
in  tbe  province  of  AKnaes,  as  well  as  their  neighboum  the  Pun.  v% 
the  grciilest  colUetors  of  it.  They  sometimes  leave  rbeir  vilU§«  Ut 
two  months  at  a  time,  6xing  their  habitations  in  tbos*;  pluxs  in  viiid) 
this  plant  abounds.  Thuy  cut  the  roots  from  the  st«:(us,  dry  llicrni  ic 
the  nun,  and  pack  them  in  bundles  of  various  sizes  and  forms.  Ipen* 
cuanha  is  imported  into  this  country  from  Rio  Janeiro  is  btlci^ 
barrels,  and  ba^s." 

Three  varieties  uf  ipecacuanha  nre  described,  distin^i^bed  by  tMr 
colour  —  namely,  brown^  red,  and  g^rry  annulated  iiiei'airuatiba. 
continental  writers  ipecacuanha  is  denominated  anmuuiied  \\ 
to  distinjfuish  it  from  the  roots  of  T'jfycAo^na  eirwAica  and 
jico^a.     These  ore  not  known  in  English  commerce. 


StructHre  of  Ipeeaevanka. 

The  Bubatancc  of  the  root  of  ipenacuanha  is  divisible  into  two 
—  an  outer  ct>Wi«x/  portion,  and  an   loner,  iibrous.  and  ir«»»i 
botanically  termed  medititUiitm.     These,  in  the  dry  rttut,  s«pan 
easily  from  each  other,  and  their  intimate  structure  may  b« 
with  facility  from  transverse  sections. 

Examined  unrler  the  microBCoi)c,  the  cortical  part  u  i 
sist  externally  of  cells  of  a  deep  brown  colour,  tbe  pari«l 
are  but  indistinctly  visible,  and  which  form  tbe  epidenaia  r 


IPECACUANHA,  AND  1X8  ADULTERATIONS. 


669 


the  cortex  h  matle  up  of  ailonrlesx  ceU.s,  tlie  cavities  of  which  arc  Bllcd 
with  minute  but  excemliii^ly  distinct  starch  cor|)U»clcs,  many  of 
which  are  unit^  in  twa",  threes,  and  even  fours^  and  con6e<juentl)r 
are  ruther  luuller-shaped,  while  thejr  ire  all  furniuhcd  with  a  very 
dtstioct  bilum.     (See  j^.  214.) 


Fii.  214, 
iMCACOjutu  Boot. 


Trsmrme  wclton  ot  the  rcrttx.  tna/n)<l*d  l!9i  dUmrlfn.  J .  Starch  cor- 
puKlrs  (ir  the  Mine,  PMfntlKl  fSO  tlUnict«ts,  w  mlaa  eaxttia  ueieoiMi 
cr/dal*  -,  rrnetimt  (T)  oDaubnd  in  ifaki  purtkin  orth«  root. 

In  tr&narerae  sectioiu,  the  central  part,  or  mefHtuUium^  appears  to 
coDuit  of  a  number  of  tlighllj  angular  cells,  of  different  size*,  having 


I  of  Uw  oentral  prnti  or  maiHt^imm,  nagnltad  fl» 
A,  iruuvuii  MMtok  I  a,  lODittudliiai  niiUok. 


Hcmbling  ctos^y  those  of  the  cortex.     In  lonrritudin&l  tectimu  « 
becoinet  evident  thai  what  uppeared  in  transverse  sections  to  btodk* 


J 


IPECACUANnA,  AND  ITS   ADULTERATIONS. 


67 1 


itre  really  wood/  fibres  which  had  been  cut  ncross ;  the  fibres  arc  all 
strongly  dolte<l,  and  are  remarkable  for  cnnuin'mg  in  their  caviliea 
an  abundance  of  Rtarch  corpuscles.  This  is  tlie  unly  instance  irhich 
has  as  yet  fallen  under  our  obitervation,  in  which  the  cuvitiea  of  uii- 
duubted  vroinly  fibres  have  contained  starch  corpuscles.     Fig.  215. 

In  genuine  powdered  i{>ecacuanha  the  whole  of  tlic  structures 
whieh  enter  into  the  foruiution  of  the  cortex  and  meditulliutn  nmy  be 
detected  on  c&reful  exauiiDation,  variously  broken  and  cujuminuted. 
Fig,  21G. 

OsanvB  Qrovitd  IrmcACVAtimA. 


a  tt.  rrBffmrnbt  ot  lb*  brow  9%M*rmi»  t    &  A.  wUi  of  tb*  eortcs.  cDBtalcliif 
'  itkTch  t  f  c,  looM  •urth  aety imuU ■  uid  njiUU  t  (f  <<•  VBody  flbrw  of  tlM 

The  Structure  of  ipecacuanha  root  is  therefore  exceedingly  cha- 
racteristic. 


Composition  of  Tp^caenanha, 

The  most  complete  analyse*  of  ipecacuanha  which  have  as  yet  been 
made  are  those  of  Pelletier  and  Bucholz. 


e72 


IPECACUANHA,  AND   ITS  ADCLTERAT10K8. 


p£U.ETl£K*t   AnALTBia. 

Srown  Antmlaled  Ipecacuanha. 


Km«clM            .... 
(VLirotu  bttr  nullar       . 

Gum                     .... 

SUrch                    .... 

LlffnvcHU  nctUr 

Naa-«mccic  exinctlve    . 

Lou    •              -              .              .              . 

lt>r(W!iwi)>ia 

CoRM. 

HadltuUlMi. 

cmT 

16 
S 
6 
10 
41 
ID 
0 
4 

trAcct 

8^ 
KKMl 

S6-IR) 
S45 
4-BO 

14 

u 
It 

m 

"i 

m 

100  00 

100 

BocHou^'s  Ahaltsis. 

Emetic  extractive  (emetina) 

Soil  resin         ,  .  .  - 

"Wax  .            -  -  .  - 

Gum  -            -  -  -  - 

Slarch              .  .  .  - 

Woody  fibre   -  -  -  - 

Bitter  cAtr&ctive  -  .  - 

Sugar             -  -  .  - 

ExiTHctive,  gum,  and  ttarch,  extracted  hj 

potuh         -  -  -  - 

Loet  -            -  .  .  - 

Ipecacuanha    ... 


4*13 

2-43 

0-7tf 

2517 

fi-OO 

10-80 

1012 

2-00 

34S0 
0*80 


100  DO 


The  only  constituents  of  ipecacuanha  which  require  to  be  partkm- 
ItLrly  noticed  are  the  odorous  fatty  mntter  and  emetina. 

'llwj'otty  matter  w  extmctctl  from  ipecacuanha  by  ether  ;  it«  odour 
is  verv  strong,  and  rcsemblea  that  of  the  essential  oil  of  horiieTadialt. 
Notwithstanding  its  acrid  taste  and  ]>ungent  smell,  it  does  aoi  exert 
any  considerable  effect  upon  the  stomach. 

Emetina  is  iucHlort>us ;  has  a  slightly  bitter  taste ;  is  fusible  at  122" 
Fahr. ;  very  ^liglilly  sofuble  in  com,  but  more  so  in  hot  water  ;  verr 
soluble  in  alcnhol,  but  scnrcety  so  in  ether  and  oils.  It  forms  sddu 
with  acids,  including  tannic  acid,  by  which  emHiMui  is  {urecipitated  & 
its  solutions  as  a  tonualc 


On   TUB   Al>ULT£XATION8   OF   IpECACCAHHA. 

From  the  examination  of  Thirty-three  samplct  of  powdered  ipees- 

cuauha,  it  appeared  — 


IPECACUANHA,  AND   ITS  ADULTERATIONS. 


673 


rlicratetl  with  a  vegetable  anbstance 


That  eighteen  were  aduiteniied ;  or  more  than  one  half. 

That  of  these  one  coutaiuvd  a  very  hirge  quantity  of  tartar  emetic. 

Two  of  the  8iunple«  were  adulterated  with  Urge  quantities  of  car- 
honnte  of  lime  or  chalk. 

Two  were  adulterated  with  wheat  flour^  one  of  these  also  containing 
A  proportion  of  extraneous  woody  Jitre. 

That  one  of  the  samples  wm  adulier 
containing  much  starch. 

That  iwetre  sauiplea  were  adulterated  with  mriouB  and  often  con- 
siderable proporiiomt  of  extraneous  looody  jibre  of  more  thun  one 
kind. 

We  have  now  shown,  that  powdered  ipecacuanha,  like  the  other 
dru;js  we  have  re|)orled  upon,  i«  aubjeet  to  very  extensive  aduU 
tcratinns.  The  miwt  prevalent  nduUeration  delcct^tl  i^  that  with  ex* 
traneouB  w(HH)y  fibre;  it  will  he  remembered  that  the  pr{nci[)id  adul- 
teration of  jalup  was  of  a  similar  nature.  In  our  report  on  that  dru^ 
we  expressed  the  conviciiim  that  since,  for  the  reduetiun  of  woody 
Bubfltonces  into  powder  in  uny  quantity,  a  |>uwerful  ^rindin;.'  ajtparatus 
is  required,  dru^  grinders  were  the  purliL's  wh<j  practise  this  mluhera- 
liuii.  The  eorrespimdenee  whieh  ensued  on  tlie  publicuiiiui  of  that 
report  \\^a  afforded  abundant  evidence  of  the  correctnesa  of  that  con- 
viction ;  tiiL're  is  no  doubt  that  in  the  caite  of  ipecacuanha  also  the 
parties  chiefly  e<mcorned  are  drug  grinders. 

I|h?oaruanha,  then,  one  of  the  most  important  medicines  in  the 
whole  Materia  Meilica,  is  now  proved  to  be  adulterated  to  nuch  an 
extent  a^  tt>  render  its  cHt'etn  w]ien  administered  must  un^ati.sfactory 
and  unct?rtain.  This  unceitainly  yiay  be  shown  by  reference  to  the 
action  of  two  of  the  sanqjiea  nf  ipecacuanha  anrdysed. 

Une  sample  supplied  tn  a  public  hospital,  and  ailullerated  with  a  verj 
1ari;e  quantity  ot  chutk,  whs  repeate<llr  administered  in  do^c:«  two  or 
thrct'  times  as  large  as  thuse  ordinarily  prescribed,  without  the  usual 
effects  being  produced  ;  in  facl  the  dru^  was  almost  inert,  ami  it  was 
this  marked  inciHciency  of  the  remedy  that  led  to  the  detection  of  the 
adnUeration. 

Another  contained  nearly  fourteen  per  cent,  of  tartar  emetic.  Now 
the  t'tfectj*  re^ultiiifT  from  the  ailminiiitralinn  nf  i^fecaeuunha  thus 
adulterated  would  be  twice  as  severe  and  violent  as  thosie  which  eiuue 
from  iri'nuitJie  ipccncuaiiha  of  good  quality. 

It  if*  alitu)<4t  in  vain  that  pliysiutogisla,patho)o<;ifits,  and  chemists  ore 
oonstaittly  eoiitribuiinj;  to  the  advancement  of  the  aciene_'  of  medicine, 
since  the  reetults  of  their  labours  nre  pruciitiUly  defeated  and  set  at 
nou^liL  by  iidulterritionssoscaiMbdousas  those  revealeU  iu  these  articles 
on  *^  Dru^fs  and  their  Adnlierations." 

The  lime  must  come,  and  that  ere  lon(f,  when  oflfences  of  this  de» 
scrap'inti  will  be  viewed  in  their  projrer  lij^ht.  ami  men  guiltr  of  theiu 
will  tind  themselves  pinceil  where  they  ought  to  be  —  at  the  feloD*l 
bar. 

X   3t 


674  IPECACUANHA,  AND   ITS  ADULTERATIONS. 


To  adulterate  medicine*  which  »re  so  frequentJ/  the  salration  fl/l 
is  not  a  Bimplc  act  of  liishonestj,  but  it  amounu  to  a  crime  of  tfaf 

CoLocTsra. 
fig.  217. 


deepest  dve, 
able. 


COLOCYNTn,   AND   ITS    ADULTERATIONS. 


675 


Since  llie  powiler  of  ipeojicuftnlia  is  so  extcnaivcly  Atlullenite<i,  it 
follows  that  all  ihe  other  phumiaccuiical  prcpiinitiona  into  the  compo- 
Htion  of  which  This  (1rii}»  cnloi*s  are  niso  adultorntcti,  as  Pulv,  Ipecac. 
Co.  PiL  Conii  Co.,  Fil.  Ipecac,  c.  Opio.  and  PiL  Ipecac,  c.  Scilla. 

On  the  Detection  of  the  AduUeratians  of  Ipecacuanha. 

Tbc  oflultcrations  of  ipecaL-uanba  with  wheat  floury  woody  flhre^  or 
oXhtr  vegetable  substances^  are  tU»c<)V(*rab)<*  by  invaiis  of  the  micro- 
scope; those  with  chalk  uud  tartar  emetic  by  cht'iuical  methods  of  re- 
search. 

Presumptive  evidence  of  the  presence  of  chnllc  is  obtained,  if, 
un  a4ldii)^  a  little  acid  to  the  powder  viewed  under  an  inch  object 
,i:1a85,  effervescence  occurs.  In  sucb  cases  a  driven  quantity  of  the 
powder  must  be  incinerated,  and  the  ash  weighed  and  tested  for  car- 
btmate  of  lime  in  the  manner  already  fn-quentty  described, 

For  the  discovery  of  ohe  tartar  emetic  we  may  pnn.ced  tbus  ;  tlie  salt 
must  be  dissolved  out  of  the  |>ow(ier  with  distilled  water,  and  the  so- 
lution, after  being  acidulated,  tested  with  sulphuretted  hydrogen  ; 
wluMi,  if  tartar  emetic  be  present,  the  yellow  sulphurct  of  antimony 
will  be  formed. 


COLOCYNTH,  AND  ITS  ADULTERATIONS. 

*•  PowoBREU  colocynth  frequently  contains   large  quantities  of  the 
seeds  of  colucynlh,  and  those  ought  never  to  be  present ;  in  the  direc- 


Fwtloao/Hirfkeaof  QoviO.      M4AIIM  ISUdltnclcn. 

X  X  a 


676  COLOCTNTH,  J^ND   ITS  ADULTEBATIOKS. 

tions  given  for  prep«in;r  powdered  colocjnth  it  is  « 

thftl  the  seeds  abould  be  rcmoveil.     1  have  mlto  met  wit£  tribntf  jb 

Tin.  II*. 


Sccttun  of  flKfto  of  CutorruA.    ItafnUUd  UO 


bolh  tn  tlic  povder  and  in  the  extmct  ofcnlocynt]! ;  ami  in  ifctfadH 
I  have  detected  chnlk,  CoIm'Tiitb  is  one  of  the  most  valuable  ya% 
live  mcdii-inca  crmt^tined  in  the  Pharniacnpaia.  nnil  ita  adoltcnM 
therefore,  is  a  nuttrr  nfcondiiienible  inip4irt»nre."* 
As  it  15  impos!<ible  to  detect  the  adullcraliona  of  coloc/otll 


*  Evideoc*  by  (be  tutlior  befor«  Ptfllamtour/  ComwHit « 


RHDBABB,   AND   ITS  ADULTERATIONS. 


677 


a  knnwicdjre  of  the  structure  of  the  gourd  and  seed,  we  append  some 
beuutiful  and  cUoractcrulic  iltuslralious. 


RHUBARB,  AND  ITS  ADULTERATIONa 

"  Akothkb  (Irijfj  which  I  have  found  sometimes  to  bi;  adulttTntfid  IB 
powdered  rhubarb.  I  have  met  with  samples  of  pt>wdercd  rhubarb 
adulterated  with  turmeric  \  and  there  is  a  sample  upon  the  table  which 
contains  a  considerable  quantity  oC  wheat  Jluur."* 

Another  adulteration  uf  Turkey  rhubarb  in  powder  is  with  Engluh 

Fii.  S». 


rhubarb;  the  medicinal  aotiim  and  the  commercial  value  i>f  which  li 
9<)  much  inferior  lo  that  of  Anialic  rhubarli. 

The  dotted  dueti,  cellular  tittuet^  starch  euMjuucIet,  and  groupt  ijf 
rnphides,  are  all  clearly  exhibited  in  the  figure. 

*  £»!<■■»  bf  Ue  Mtbor  br(br«  pKrlUmt^Urjr  Comnlttw  oa  AduluraUoo. 
X  X  3 


67^  SOUILLS)   AND  ITS   ADULTEE.ITIOXS. 


SQUILLS.  AND  ITS  ADULTERATIONS. 
"  PownsmBD  squilU   I  have  found   to  be   udulteratrd   witb  vlMf 


Fovi)crt4  Sqriu.1.  ■^■llanltA  wMi 


The  Jarge  eelU^  miral  vesteit,  and  groupi  vf  t^dUAAt 
characteristic  of  the  bulb  of  xjuills,  are  all  delineate*)  in  Ibc  eagnfiiC- 


COMPOUND  SCAMMONY  POWDER,  AND  ITS 

ADULTERATIONS, 


"AnoTHRB   mnst    importunt    medicine   \%  the  rmnpoond 
pnwdtT.     This  consist!"  of  three  in^eilients,  nAmelv,  Mnunoooir, 
extract  of  jnlap,  and  ginger.     Now  two  nf  Uiuk  in^re4i«ttta  ate 

•  Evidence  hy  tlt«  authvr  bcfurc  PvllMtMUrr 


^ 


LIQUORICE,  AND  ITS  ADULTERATIONS.  679 

liable  to  ailuUenition,  namely,  tlie  eoammony  &ntl  the  powdered 
ginger;  wli'ile  the  powder  of  jalap  U  very  rpetpieutly  FulisliUiled  for 
the  extract,  althcMigb  it  is  not  more  than  about  one  luurth  strensth 
of  the  extrnot.  Of /*«  sample)*  y}(  [lowdt-reil  scainmony,  I  fouml  chtdk 
in  trreater  or  less  proportions  in  ftU,  wktut flour  in  three,  and /jourf/cred 
_/(i/rfn  in  four,"* 

The  ^ubstilutinn  of  powdered  jalap  for  the  hard  extract  u  a  most 
scandalous  odulteratiou. 


AROMATIC  CONFECTION,  AND  ITS  ADUL- 
TERATIONS. 

"  The  last  medicinal  preparation  of  which  I  propo»e  to  speak  i« 
aromatic  confection,  a  very  valuable  renjcdy  in  tlie  tTontiiient  of 
diarrbtca.  This  should  conifisC  of  ciniiauioii,  cloves,  nutmegs,  carda* 
moms,  safTron,  prepiired  chalk,  and  «n;rar,  and  it  is  conseijuently  a 
somewhat  expensive  preparation.  I  find  that  the  more  expenMive  in- 
p-edtents  are  frcfjuently  omitted,  and  others  sometimes  substituted; 
as  tuntieric  in  place  of  the  saffron,  euenee  of  cattia  for  the  cinnamon, 
and  chalk  for  part  of  the  fiugar.'f 


LIQUORICE,  AND  ITS  ADULTERATIONS. 

LiquoBlcB  is  an  article  lar>;elT  eonaume<1,  and  furnishes  an  illustra- 
tion of  a  syotem  of  adulleriiiiun  which  extends  to  a  variety  of  other 
Uru*;s  and  pharmaceutical  preparations. 

Liquorice  i<  met  with  under  various  forms  and  namea:  thus,  there 
is  stick  liquorice,  the  [xtwder,  the  Phnrmaoopffiial  extract,  the  foreign 
extract,  pipe  liquorice,  and  Pontefract  lozengea. 

Stick  liquorice  consists  of  the  umlerground  stem  or  rhizome  of  a 
plant  belonpn^  to  the  genus  GlycyrrhizcL,  usually  in  this  country  Gly^ 
cyrrhiza glabra  :  the  powder  is  tlie  r<>ot  ground  and  pulverised,  while 
the  other  prepnrationf  named  ennsist  of  the  extract ;  this,  in  the  case 
of  pipe  li<iuorice  and  Pontefract  lozenges,  is  said  to  he  reBned. 

*  Rvltlenc«  br  th«  author  tMlbre  PkrlUmeiiUrjr  CofaaUlt«c  on  AdoltcraUon. 
1  IMO. 

X   X   4 


680 


LIQCORICC,  A^'D   IXS   ADULT£aATIOX8. 


The  foreign  extract,  known  as  Solazza  extract  or  jiuce,  in 
the  best;  aiidiiccoriiingBS  it  \t  prepared  in  Spain  or  Icalr,  HUoUed 
Spanish  or  I UiUan  juico.  AVe  learn  tVora  Pereira  Uiat  the  SM&tsk 
extract  is  prepared  in  Caialuiiia  I'rfim  Gltfcyrrhisa  gtabra^  mhm  Uf 
Italian  extract  is  obta.int;d,  in  Calabria^  Irom  G.eckinata.  Ot'UtcTcm 
thf  lionoricc  plant  has  been  cxlensivclv  cultivated  in  this  rountrr  taf 
iiK'dioiniil  \\%i.\  CBjieciitlly  nt  Miteham,  where  so  many  dificreot  tisnli 
of  niedii'inul  phmis  are  j^own. 

The  constiluenta  of  the  rot^t  of  Glycyrrhiia  glabra,  according  to  tie 
analysis  of  Kobiquft,  arc,  liquunce  iUgar,  or  t'^"  ■"—■'"*'«.  jivci, 
Qsparagiity  reatnmts  oil,  nlbutiwn^  woodi/Jibre,  and  ^  dly^ls** 

phate  and  nitrate  of  lime  and  m(if^ie»ia.     Tlicquantt     -  .•evrvctii 

constituentK  are  nut  given  by  Uobiijuct,  nor  duel*  he  inenuunna' 
oxaliite  of  lime  as  constituents,  altbougb  them:  abound  in  the  juicrof 
the  root. 

As  before  entering  upon  the  consideration  of  the  chemical  aduJtev 
tion  of  nny  article  it  is  necesMiry  tliat  wc  «hoiiM  he  acquainted  «it^  Ik 
proportions  of  tlie  principal  ingredients  of  which  that  articte  if  M^ 
]M>sed,  we  instituted  in  the  first  place  certain  analycea  of  ihe  roue  Ik 
jtotcdevy  and  the  extract. 

The  following  was  the  composition  of  100  part«  of  the  frtA  rMf.'— 

The  Fresh  Root 

Glycyrrhizin          ....  9^ 

Gum          .....  25-M 

Matter  soluble  in  alcohol,  chiefly  resin       •  -7$ 

Albumen  -              -             -             .              -  -OT 

Slarch       .....  22*91 

Woody  fibre          ...             -  |S-M 

Moisture     -----  S6*ftl 

Ash,  3  07  per  cent.  1 

Total         -  ]<MMN> 

The  analysis  of  100  parts  nf  ihnimffrrri  fi'rnfnf  jiiiirifiir  fiiriiwhni 
following  rosultd : — 

The  Powder. 

Glycyrrhizin          ....  10*40 

Gum          -             -             -             -             -  43-30 

Matter  soluble  in  alcuholi  chiefly  resin       -  1*09 

Albumen  -             -            -            .             -  r50 

Starch       -             -             -             -             .  24-41 

Woody  fibre          ....  l5-i0 

Moisture  -----  4*10 


Total         .  100^)0  

The  analysis  of  the  decorticated  pawdtr  fumiahed  nearij  tiflubr 

results: — 


r 


LIQCOKICE,   AND   ITS  ADULTERATIONS. 
Thi  Dicortieoted  Powder. 


631 


Gljcjrrhiziu 
Guni 
Re«in 

Albumen  - 
Srurch 
Wt.ody  fibre 
MoiBturc  • 


130 

371 
•8 

1*80 
29-52 
16-5« 

102 

10000 


Fire  hutiHrcd  partsof  the  fresh  root  furnished  175  parU  of  extract; 
while  the  Bomc  qiinntity  of  thopnwder  of  thedried  rot)t  pnve 'J75  ports 
of  extract.  Ldstly,  100  parte*  of  this  extract,  dried  to  a  temperature  of 
212°  Kahr.,  yielded  19-3  purU  of  liquorice  sugar,  aiid  80'3  purts  of 
matter  iiiwduble  iu  aicubol,  and  which  consisted  ehieUy  of  gum  with  a 
little  albumen. 

When  pur«  and  genuine,  extract  of  liquorice  U  entirely  soluble  in 
water 

As  will  be  shortly  apparent,  the  above  analyses  furnish  nomc  useful 
data,  by  which  the  quality  of  the  different  kinds  of  liquorice  may  bo 
judged  of. 

Structure  of  Liquorice. 

The  general  structitre  of  liquorice  rout  is  very  distinotive;  the  ele- 
ments uf  which  it  consists  are  bundles  of  iruuc^jy  ^^r^,  re/^n/nr  /ujHf, 
doUed  ducts  or  oesseli,  and  starch  corpUMcles,  Xbc»e  elements  are  thus 
arranged. — 

In  transverse  sections  of  the  root,  a  linear  zone  is  observed, 
asoally  distant  from  the  circumference  about  tlie  third  of  the  thick- 
noM  of  the  nK»t.  The  piirt  of  the  root  irithoui  the  stone  is  Ira- 
Tersed  by  bundles  of  woody  6bre,  united  togetlicr  by  cellular  tissue; 
that  within  tlie  zone  is  traversed  by  numerous  dotted  ducts  or  vessels 
as  well  as  by  bundli>it  of  wiH>dy  fibre;  while  tlie  cells  of  the  cellutur 
tissue  which  forniii  the  basis  of  the  root  are  tilled  with  starch  cor- 
puscles. 

These  tiarch  corpuscles  are  very  charjiclerlstic  :  they  nre  ov«I  and 
small,  and  in  many  uf  them  the  central  cavity  of  an  ehmgated  form  is 
vi«ble- 

Tbe  \coodtf  fibre  does  not  present  anything  remarkable  in  its  struc- 
ture ;  the  central  cavity  is  well  mirked.  In  sections  of  the  older  roots 
medullary  mys  may  be  seen.  The  several  structural  peculiarities  uf 
Uq^riee  root  are  ull  clearly  exhibiteil  in  the  accunijmiiying  drawinnrs. 

The  yellow  colouring  matter  of  the  rcK>l  is  situale<l  almost  entirely 
in  the  bundles  of  woody  fibre,  and  in  the  walls  of  the  dotted  duels. 


LIQtrOBtCB,  AKD   ITS    ADOLTEBATIONS. 

Pig.  33Bk 


CS3 


Xw^ffii^ftMl  mcUm  or  ijQDosiCTi  Root.    HmiiUM  40  dlanwtcn. 
Oh   THB   AsULTBRATIO^fS   or    LittUOBirB. 

Havin;;  thus  dcficrlbefl  tliv  chemical  composition  and  the  slruclurc 
of  lifjuDrlee  rotit,  the  subject  of  the  adulteration  uf  litiuorice  luu^  n«ct 
be  considered. 

On  tonsulting  the  works  of  differont  writers  on  ftduUeralion,  we  h»Te 
met  with  the  followinj;  nbservutions  rvlatin;;  to  liquorice:  — 

Accum  *  st&tes  that  Spanish  liquorice  ''1:1  frequently  nothing  else 
than  ft  mixture  of  the  worst  kind  of  ^m  arabic,  Ciilled  Indian  or 
Btirbaru  f^um^  im|wrled  chii.'fty  |ur  the  tibe  of  nmkin^  thoe  hlackinj;;. 
A  solution  of  the  genuine  Spanish  liquorice  juioe  is  mixed  with  a  su- 
lutiuu  of  Barbary  gum;  and  the  mixture,  after  b«ing  inspissated  to  a 

•  Tr««UM,p.S48. 


]nY>perconsuitencef  is  ngnin  mide  up  into  cylindrical  rol^  which,  whilst 
still  moist,  are  covered  with  bav  leaves,  iind  repncked  in  chettts  to  re- 
tiemble  in  every  respect  the  genuine  Spanish  liquorice  juice  imported 
from  Catalonia.** 

Brunde*  in  his  "Dictionary  of  Materia  Me<lica  and  Pharmacy,** 
published  in  1936,  remarks  as  f('>1lows:  — 

*'Thc  eliiet'consumpiion  ot*)iqmtri<:e  is  in  the  preparation  of  the  ex- 
tract, which  is  imported  Irum  the  South  o(  Kuro[ie  under  the  name  of 
Spaimb   Juice;    it  is  usually  burned  and  utherwibc  ciuelc»fily   pre- 

*  Ticalife,  p.  362.  . 


LIQUORICE,  AND  ITS  ADULTEUATIONS. 


6S5 


pared  and  itdidtcrAted,  and  of>en  conlftinfl  copper,  derived  from  the 
jHiiiH  in  wbi(  h  the  dfcm'lioii  of  the  root  is  evHpnrMlt.'d." 

M.  Chevollicr*  states,  tbnl  **liiiuoric«U  ofK-n  fulsifiod  by  W/ircA,  and 
A  largo  proportion  of  inert  powders,  it  hua  also  been  falsified  hy  an 
extract  which  gives  it  the  uwte  of  hay. 

"  It  coutaiiifl  likewise  mernllic  copper,  removcfl  raenhftnically  from 
the  pans  of  that  metal  in  which  it  i»  prepared,  liut  it  docs  not  con- 
tain saltA  of  copper,  a  conclusion  which  results  from  tuany  experi- 
ments made  by  M.  Villain." 

"  Liquorice/' writes  Pereiraf*  "m  met  with  in  commerce,  however, 
is  rarely  pure.  It  contains  the  soluble  principles  of  (be  root  with 
some  copper  scraped  off  tlic  iMiiler  hy  the  spatula  employed  to  stir  the 
extract  during  its  preparation.  Fee  says  thai  four  ounces  of  this 
extract  yield  two  dmcbuis  an<l  n  half  of  Dieullic  copper  ;  but  there 
must  be  some  great  uiisiuku  in  tbi:*  statement.  If  the  foreign  extract 
be  dissolved  in  water,  and  llie  sulution  filtered  and  inspijisated,  we 
obtain  reined  fttftmriee.  But  I  am  iiifurnieil  thiit  the  tape  refined 
liqimrke  is  a  very  iiduUeraled  article.  The  Pontefract  loztnget  are 
made  of  refined  liquorice,  and  arc  much  Gstecmcd." 

Jiestdtn  ttf  the  ExamhuUioH  of  SampUt. 

We  will  now  prrtceeil  to  state  the  rei>ul(s  of  our  own  examinations 
ami  analyses  of  litjuurice,  premising  that,  genuine  extract  o{  liquorice 
should  di!«»olvti  in  water  without  leaving  any  residue,  and  tberefiiru 
ought  not  to  contain  starch ;  that  it  should  yiehl  from  about  90  to 
nearlr  100  parts  of  extractive  utatter,  according  to  the  state  of  dry- 
ness m  which  it  may  happen  to  be  at  the  time  uf  anolytfis ;  this  ex- 
tractive matter  should  lurninh  from  7&  to  8.S  per  cent,  of  matter  in- 
soluble in  aicolml,  chiefly  gum;  and  from  10  to  \5  per  ceuu  of  sac- 
charine matter  or  liijuoricc  sugar. 

The  aualysvB  of  Thirttffnur  samples  of  liquorice,  including  the 
different  varieties  of  roll  »wi  pipe  liqtuirice,  and  Ponte/raci  loxenges, 
carefullv  considered,  tiiriii><h  ••oine  iiu|Kirtant  results. 

Thus  it  ap|H!ara  thai  the  ^um  of  the  difftrenl  k'uuU  of  roll  liquorice 
varied  from  65  5  to  335  grainsi  |H!r  cent  ;  of  the  ticcharine  wetUrr  from 
14"9  to  8*9  per  cent,  p.irl  of  ihie  in  some  cuscs  con&iftiing  of  vane 
sugar;  of  the  extractive  from  759  to  47  1  per  cenL 

Of  the  pipe/'yuoricr  ihat  the  gum  varied  Irom  22*7  to  45*9  per  cent.; 
the  sugar  from  l^H  to  1 1  0,  the  greater  part  of  tliis  consisting  of  cane 
jntgar;  and  the  ettractice  from  57*1  to  437  per  cent. 

Of  the  ronlefrota  h^zengeit  the  gum  ranged  from  31-5  to  25*7  ;  the 
tngar^  partly  ctine  ntgar^  from  18*1  to  13*1 ;  and  the  extractirt  from 
45*9  to  43-8  per  cenu 

It  further  anf>enrs  from  the  analyses  that  the  whole  of  the  rt^l  li- 
quorice furnisuetl  insoluble  residues,  varying  in  »m'?unt  from  1$'50  to 
4200  jwr  cent.     In  twtlct  ca«es  tJie»e  residues  cimsisted  of  boiUd  starch, 

*  DlctlonnRlre  dei  AU^raltmis  M  FalalAciiliniM  dei  SutMlincM  Alin«DUlns.  p,  304. 
t  U«lerU  Medlca,  vol.  U.  p.  1035,  llilnl  odltiuo.  '^ 


686 


LIQI'ORICE,   AND   ITS  ADULTERATIOKft. 


prohalily  n>«  (the  starch  present  in  the  difTerent  samples  of  Saksa 
und  Htirttccu  extrnct  was  alwiivs  uf  this  kind):  in  etfren  anplBlcf 
wheat  Jfour^  in  one  o\' pi>(ato  ntarcht  hiu\  m  one  of  u^heatjbmrnnrm, 

Tbiit  iUe  pipe  lUjuoricef  likewise  rurniehed  in^duble  residues  (orlk 
mosi  jiart,  in  siill  liu'ger  ainounta  thnn  iW  roll  liqunrJce;  thu*  tkn 
snaallest  re^^idue  wei^ihtMl,  after  being  dried  on  u  wuft^r  tiRlh,  34^S  mA 
the  l]irt!usl  41*0  ^rA.  ptT  cent.  In  five  CiiAef  ihia  cfin^isttMi  of  lete 
Jiuur^  in  one  of  rye  flour,  and  in  one  of  potato^  rice,  And  arAarf^lan 
In  tivu  viiscn  A  sniall  part  of  thitt  residue  coiifiisted  of  gtJitUuti,  dK 
pi|)e6  being  furni9he<l  with  a  distinct  tubeof  thm  ftubstancc 

Lastly,  thut  the  Povt^fraci  lozenges  funiisbed  residues  O0DaiM)i|tf 
VDheat  flour  (;tiibject  to  ihi*  uclioD  uf  beat),  wbich  varied  in  ttMMl 
from  i^(y^ti  to  39*0  (irs.  per  cent. 

The  ash  of  the  different  siimpiesof  roll  and  pipe  liquorice  and  IW 
lefnitt  U))ten^ea  varieii  from  ^50  t()  16  per  cent.,  and  eonsittrd  is 
severnl  cases  of  fon-ii;n  niincnti  matter;  tl>i;<  in  one  in.^tAnceanioavlfll 
to  13  percent,  and  was  composed  oi  carbonate  of  lime,  or  rhalk.  TV 
ashes  of  the  pipe  lir^uorices  in  two  or  three  cuse^  were  ao  *!«■(; 
coloured  iifi  (u  lead  to  the  suspicion  tbat  Mime  coloured  mineral  vuWf 
Bubstiinee  hiul  been  enipluyed  to  iitcreu»e  Ibuir  weiifhl. 

It  h  tim.t  evident  that  the  different  kinds  nf  ndl,  pipe  Itijuorice,  tad 
PoiiLefraet  Kiieenges,  are  subject  to  very  extensive  adidteratitfQT  lim 
in  fiuiiie  instance.''  auumnlin^  to  nearly  one  half  the  article. 

Aa  a  rule,  the  pipe  liiiuorice  and  Pimtcfruct  triKeni;esronlainal 
amount  nf  fureign  starchy  matter  than  even  the  inferior  detet 

nf  roil  Itqnnrire.    Many  of  the  pipe  liquorices  are  in  addition  funiii    

with  a  thii'k  rnuun^  of  |;etanne  :  this  is  sometimes  of  the  wont  qt^ 
lity,  antl  but  little  bunenur  to  plue.  The  best  way  to  exhibit  the  tabi 
of  gelatine  tinea^ing  llie  pipes  is  to  place  them  in  coUl  water;  the  fi|Na 
will  swell  up  and  increase  Co  two  or  three  times  tbeir  orijfinAl  liff: 
when  in  this  state,  the  gelatine  may  be  easily  removed. 

The  ingredients  employed  in  the  adullenilion  of  the  kinib  of  Uqv^ 
rice  above  referred  to  consist  then,  of  stan-h  of  various  kinds,  as  wbist, 
barley,  rye,  and  rice  flours,  ;ind  potato  starch,  either  separat«-lT  cr  » 
combination;  cane  sugar,  gelatine,  and  fureign  mineral  matter, as ar^ 
bonatc  of  lime. 

Although  not  immediately  connected  with  the  object  nf  ibia  artkk 
vfii  yet,  when  en^juged  in  the  analysis  of  liquorices,  thought  it  dttSrMt 
to  determine  how  frequently  and  to  what  extent  the  samplci 
contaminated  wilh  copjter.  We  deteeted  that  metal  in  thirteen 
twenrv-one  roll  liquonces  examined  in  greater  or  lesser  amount;' 
quantities  in  three  of  the  samples  were,  for  the  100  grains,  •»,  "iSj 
of  u  grain.  Traces  of  co|t|ier  were  found  in  only  one  of  ilie  pipe 
ricesii  and  in  none  of  the  Pontefract  loxen(;e». 

We  will  now  pa^  on  to  state  the  results  of  the  cxanunatioo 
extract  of  liquorice  of  the  Fharmocopiria. 

Ten  xamplex  uf  extract  of  liquorice  were  exvniiiedt  Untii 


alaifff 


I  LIQUORICE,  AKD  ITS  ADT:LTERATI0N5. 

iliMolvet!  nearly  wiUiout  rp«tHue»  and  were  f^ehuitic:  the  remalntJer  of 
the  samples  dep(»3itc(l  inaaltibic  residues  Ainountin":  to  3,  13,  17,  9,  7, 
XH'S,  uid  33  per  ccnU  rcapectivcty.  In  four  cases  thi^  consisted  of 
btnletl  starchy  maiier^  and  in  one  instaucc  of  4Uirchy  matter  aiid 
gelnth*e. 

The  sample  containing  the  gelatine  fumisbed  only  65.5  per  cent. 
of  extrnct,  and  tlie  insoluble  residue  amnuntcd  to  17  per  cent.,  lbu« 
leaving  18  percent,  fnr  moistiiPe,  which  liirjje  qiinntily  the  liquorice  whs 
partly  enabled  to  retain,  in  consefiuence  of  its  admixture  with  ftelatine. 

It  ia  evident,  from  ilio  nature  and  (]iiAntitIcd  of  the  in:»ulub]c 
residues  that  the  ndidterated  Mimples  of  cxlracl  of  licjuorice  consisted 
ofthe/orei^  extract  melted  down. 

The  compilers  of  ihe  FhammeopcEia  were  doubtloM  le<I  to  prescribe 
A  form  for  the  preparation  of  a  genuine  extract  of  liquorice  by  the 

Ilcnowledge  of  the  fact  of  the  mlulleration  of  the  foreign  extract.  We 
ibu*  perceive  to  whatnn  extent  the  rcj»ulationsof  the  Pharmfti'opcritt  are 
•vadeil  in  this  casf>.  In  further  illiif'tration  of  the  extent  to  which  the 
Pharniaco[Kcia  in  this  and  doubiless  in  m»ny  other  articles  ifl  disre- 
^rded,  we  may  mentttin  that  we  were  only  able  to  procure  the  Pharma- 
(•(cpeal  extract  at  about  one-third  of  the  chemists  shops  at  which  we 
inquired  for  it.  In  one  coac,  although  we  particularly  requested  to 
be  furnished  with  the  true  extrnct,  »<>me  of  the  foreiun  extract  was 
CfHirsely  powered  while  we  waited,  nnd  handed  to  us  as  the  Article  we 
innuireU  for,  and  fur  which  we  were  mode  to  pay  twice  the  usual 
prux*. 

In  the  next  and  lost  place,  we  will  proceed  to  state  the  results  of 
the  cxuminalioii  of  uumcrou.H  <iai»ples  of  pouniered  linutjric^. 

Of  Ticei\ty' eight  numfileii  of  rKpnirirc  in  p<nc(/er  suojected  to  exami- 
TiHtiftn,  eli'vcn  icrre  aduUcratrd.  Of  these  mir  consisted  chicily  of  irheat 
flour,  another  contaiiivd  a  large  quantity  of  irAw/  Jiifvr^  tivo  contained 
much  (nreiiin  tniotfy  JiOrr^  two  KiUMh/Jihre  and  tnmieric^  another  woody 
Jiiire  nnd  wheat  flitttr,  </«e  was  made  up  chielly  of  Indian  cont,  potato 
«nd  Mgo  flovrx^  arid  turmertc,  another  of  soffo,  ttihnJy  Jibre,  and  much 
turmeric,  anttther  of  Kojit  Indian  arroxtroot  and  a  little  turmeric^  and 
anitiher  consisteil  almost  entirely  of  potato  Jiour^  a  Uitle  vhent  flour^ 
and  turmeric.    Some  of  the  BamplcK  likewise  coniained  cane  ruear. 

We  stated  at  the  commenceroent  of  this  pa[>er  we  believe*!  it 
would  be  found  tliat  li(piorice  ntl'orded  an  exam])Je  of  a  system  of  adul- 
terMion  wliii-h  extcnde«l  to  other  and  more  important  articles  of  the 
Mnicria  M*^lica.  We  will  now  adduce  some  evidence  to  show  that 
this  it  really  the  ca«e. 

It  has  bc*-n  ascertained  that  some  wholesale  dniggtsts  prepare,  and 
they  nearly  all  keep,  what  are  known  in  the  trade  as  compimntt  rwuf- 
fierH.  One  of  these  is  linuovice,  the  genuine  jxtwJcr  bein^  dintin- 
guishe<l  IIS  Pulvia  Olycyrrliiztt'  Verus. 

Other  comimund  powders  are  those  of  turmeric,  gentiaOi  fenugreek, 
MttUced,  cumin,  and  elecampane. 


6sa 


LIQtTORICE,   AND   ITS  ADULTERATIONS. 


Tbrae  of  tnnnerir,  ^nlian,  and  renugroek  are  avuiiUy  pr«p4i 
after  the  following  receipts,  or  aome  modifications  of  them  :  — 


Turmeric  Powdfr. 
Ytfllow  debre     -   1  lb 
Turmeric 
"Wheat  flour 


Gentian  T^mrdtr, 


lib. 
2lba 


G«ntian     -  -  I  lb. 

Linsoe*!     -  -  1  lb. 

M'beiil  Hour  -  2Ibi.J 

C&|)e  iiliivs  >      en.' 

Feiivgreek  Powder. 

Fenujjrcek,  Ih.  \%t. 
TuriHeric,  3  xii. 
^Vhcat  flour,  lb.  iii. 

This  custom  is  defended  on  the  plea  that  nn  deception  ia  pnutacd 
anil  that  those  iwwtlers  are  sold  as  comptiuiid  arlrclca.  TTiu  lua^  be 
flo  as  between  the  wholesale  and  retail  dealers  in  drugs,  hut  it  a^anredlr 
is  not  the  case  as  between  ibe>c  parties  and  the  medical  profttuoo 
and  the  public  :  the  liqiioiice  powdeis,  llic  extensive  and  vAtied  adul- 
teration <»r  wiiich  we  have  just  dcKTibed,  were  sold  simply  a#  liquo* 
rice,  and  no  acknuwlednnicnt  wlmtover  was  xuaile  even  tn  a  •in«Ie 
instance  of  tia'ir  cdinpoumi  character. 

It  15  eviilcnl  thtit  the  nni'-tice  of  making  and  selling   the»e  <'/uii- 
pound  powders  is   most  nbjectioiinble ;  il  indicjites  11  luxity  <>f  priocj* 
pie,  both  nn  the  part  of  the  wlioleside  and  retail  denier*  in  druEn,  and.* 
It  is  clear  that  the  medical  praf!::ssion  and  the  public  are  hy  H  seriouslrf 
imposed  upon. 

It  13  aflirined  that  it  is  as  cattle  medicines  that  these  compoumli 
are  used.  Althou;;h  this  is  the  case  to  iconic  extent,  yet  it  is  vurv  cvt' 
tain  that  they  are  nut  thus  yxcluaively  entpli»yed  ;  besides,  why  ahould 
these  adulterated  powders  be  thrust  down  the  throats  of  cattle  ? 

We  have  now  sliDwn  that  liquorii-i*  in  all  its  forms  and  varictiea  ts 
subject  to  an  rnorinous  amount  of  iiduheratlonf  and  that  rarious  sub* 
stunces  are  employed  fur  that  purpose. 

Thus  il  bus  been  shown  — 

That  the  whole  of  the  fbreif^  extracts  or  roll  liquorioea  wer«  mdul- 
tcmted.  yume  lotbe  extent  of  neurU  ;}0  per  cent. 

Thnt  the  whole  of  the  pipe  liquorices  examined  were  also  atlid* 
tenited,  same  of  them  not  containing  one  tbinl  their  weight  of  li* 
quorice. 

That  the  Pontefracl  lozengea  likewise  contained  hut  little  liijuoric^ 

That  of  the  samples  of  the  extract  of  Itquurice  of  the  Ptuiriuacopaio/ 
one  half  were  adulterated  ;  these  for  the  most  pari  conaittting  of  |j 
foreign  extract  melted  down. 

Lnsily,  that  a  large  pro[>ortion  of  the  powdered  liquorices  exnmiDcdl 
were  adulterated,  muny  uf  them  containin^f  only  as  much    liuuoi 
us  was  necessary  to  impart  the  Bavi>ur  of  the  geimine  powder. 


) 


UQtfDHIC£,    AND   ITS  ADULTERATIONS. 


699 


Of  the  aduUcrBtionH  discovered  in  roll  li({^uoricc,  some  are  practised 
by  tlio  fortjigii  preparers  of  the  extract,  while  others  are  the  work  of 
pnrties  nearer  homo.  It  is,  we  believe,  not  uncomDion  for  the  foreien 
extract  to  be  melted  down  after  its  arrivnl  in  this  counlrjr,  for  tie 
purpoiie  of  fiubjciHin^  it  to  further  adulreration.  In  some  casex  the 
adulterating  ingredients,  as  flaiir  and  chalk,  arc  so  clumftily  mixed 
with  the  liquorice,  that  particles  nnil  masses  of  these  substances  mvf 
be  detected  by  the  naked  eye  alone,  aod  may  be  picked  out  with  a 
penknife. 

The  adulterations  of  pipe  and  powdered  liquorice  described,  were 
no  dnubt  effected  in  this  country. 

Of  the  ingredients  cmployeil  in  the  adulteration  of  liquorice,  some 
ore  themselves  liable  to  adulteration.      This  is  the  case  with  the  tur- 

P/g.  aM. 


meric  used,  which  we  have  found  to  be  adulterated  to 
nearly  20  per  cent,  with  yeltow  ochre. 


On  the  Detection  of  the  AdwlteratioriM  ofLigmono0» 
Since  most  of  the  adulterations  of  liquorice  consist  m  tl 

T    T 


69U 


LIQLOniCK,   AND   ITS  ADULTKBAT/OW^ 


of  vegetable  Dulintanccd  of  diflfcrcnt  kinds,  the  mirrnscope  sfloff^  Ar 
ol lief  means  udnpted  Air  their  discoverjr* 

Tbe  cbaractors  of  irfieut  Jlotir^  htrnteric^  and  Kowi  Indian  orroirTwA 
have  already  been  deHcribed  and  'iijlineated  in  wcioOcufs;  tb«  i^ 
[lenrttnoea  pr^ontud  hy  liijuoricu  {Xiwder  adulterated  with  iketnowl 
n:irned  siibstancrs  are  also  exlnbiud  in^^.  "225. 

Tiio  chief  t'heinical  adultvrntionji  practised  arc  these  willi  flfv 
utid  ckaiit^  the  procc^  for  the  det^'ctiun  and  estimation  of  the  List  il' 
I»)inted  out  under  the  Iicad  of  tL'a,  wblle  for  the  detection  of 
xiigar  in  li<jiiorice  powder  we  may  proccL'd  as  follows  : — 

Add  nboui  two  ounces  of  cold  waier  to  200  grains  nf  the 
filter,  evaponitc  on  a  water  bath  at  a  yentie  beat.  i(  cane  i 
jircM'nt  it  wilt  cry»tallist)  as  the  evaporation  drnws  near  to  an  endLtnJ 
if  now  a  ViMXm  ^iilpliuric  ncid  be  addud,  the  retiidual  inasis  will  inuac- 
diiilelj"  hecome  clnirrt^l.  Sulphuric  itcid  does  not  carbonize  liquorice 
sugar  or  glycjrrhizin  but  forms  with  it  a  chemical  compound  or  tut- 
phiile. 

GIvcyrrhizin  and  cane  sugar  may  be  thua  separated  ftom  each 
oillur  :  ndd  excels  of  baaiu  acetuto  <<f  leud  to  a  elrong  filtered  infusJoQ 
of  tbe  powder,  remove  the  loud  lield  in  sululion  by  means  of  sult^u- 
retted  liydrojien,  filter,  evaporate  un  a  water  bath,  and  wli^n  dry  weijji 
the  residue,  which  consists  ol  cane  sugur. 
Ciislnm:^  duty  is  on — 
Liquorice  paste 

Of  and  from  British  possessions 
Litiuorice  powder 

Of  and  from  l^ritisb  possessions 
Liquorice  root  until  -Sth  April,  1857 
Thenceafier      -  -  - 

Liquorice  juice 
Until  lB4"2  the  oppressive  duty  of  3/.  15«.  per  cwt.  was  levied 
ibrt'iun  extract  of  li(]uorice ;  ibis  was  reduced  in  ibiit  year  to  ]/  7«. 
and  in  1653  tu  HOs.  [>er  cwt,,  at  which  it  now  remains. 


20*.  i»cr 

cwt. 

10*.    „ 

« 

20*.    „ 

11 

15*.    „ 

n 

5*.    „ 

V9 

free. 

20*.    ^ 

Artld«. 

Invomri. 

lalUL 

llll«»^ 

I^ttortM  Ftato 

JUIM 

Cvu. 

4.150 

7,»8a 

Cw. 
2l>S 

B<>«»^  Co.  u»nw 

IB  IftH. 

■.C4a 

«33 

C»u. 

7,Tn»t 

4Q0 

Liquorice  not  onl^  being  adulternied  as  imported,  but  bein;r  sttbj< 

to  furtlipr  adulteniUon  ufter  its  arrival,  it  is  clear  that  the  Revcm 
KufTcrs  a  considerable  h>S!i  through  its  sojibistication.* 

■  T>ie  prlnt-tpAl  r^rt  nf  tItU  article  WM  r««l  bj-  the  author  licfvrc  The  Mt4i<Ml 
hamdit*  hjia«  titmuhi  flnct. 


LIST  OF   DKUGS,  AND  THEIR  ADULTERATIONS.     691 

Afl  want  of  space  prevents  us  giving  r  Hoparate  article  on  each  drua-^ 
we  hare  compiled  tlie  roUowuig  tabic,  which  exhibita  many  of  tlie 
lululterutiuiu  to  wbith  the  more  important  drugs  and  phanimceutical 
preparations  are  subject  : — 

LIST  OF  DRUGS  AND  TIIEIR  ADULTERATIONS. 


Aincits. 
Cmloael 


While  prrciplUln 
R«d  prrclpllatp  - 
Mercurial  uIuUdvdU 

Nrnrurr 

ImUua       . 

lnJt>li>  nf  |Mitu*lain 
irhfomate  or  ]v«d 

iJlhiarRr 

Su'i'hKle  Qf  copper 
AceUit*  at  copper 

CartKHMttf  of  l«ad 
C«Uraln(>,  or   carbons; 

of    llltC 

Kltrat^oriltfcr 


C«rlM)Ul»  of  WMlA 
Nitrate  at  potaili 
BlUrtraU  of  poUJi 

Tarlarlc  ictd 
Lemun  Juice 


AOCLTRBATtoHI. 

Chklk.  flul|rfiat»  of  barytM  and  whtto 
Itad  I  fine  pipe  clay  i  white  prtx-lplute, 
with  ■nlptule  or  Umo 

Cbiilk  ;  corrotlve  luWImalv,  chalk 

Redlrad 

OnllnarT  day  tnlicd  •Ith  pnuaian  blue, 
aud  o(ner  tiibitaucn,  blue  cla/ 

I.t«d,  tin,  blimiiih  ■  -  .  . 

Wai^,  blarli  lead,  rnide  lalphaUt  of 
antltnoiijr 

Carboiut  e  of  potni  h  -  .  . 

Sulphate  of  baritea,  cjubonale  of  lettd, 
chalk 

Earthy  matter  -  -  -  - 

ttulphate  of  trim       -  .  .  - 

Cbilk  ;  lulpbaie  ot  copper  and  acetate  of 
Ittad  mIxM 

8ulph.tte  or  barjtM.  tulptiale  of  lead.rhalk 

Sulphate  of  larj tea,  chalk,  ocbre,  earbo- 
TiAte  of  lead 

><liral«  *^  potaih     .... 

Sallcllir.  Qiiiiiidtiie  and  CtDuhoDlor ;  (ilDi, 
tUnli.  clulk,  lulphAlcuf  Iwrtlei.  tten- 
rlnr;  rhalk :  •nlpliatriir^tii(ildltir,ch-tlk, 
aulpliAtf  o[  lime,  killceuut  mattrr,  car- 
bonate n(  niagttrtla,  lulpbaie  ol  Itia^f- 
neit,i.  kiiluhnti*  of  Mda 

Kiilphale  or  wida,  Ulaubrr's  lall    • 

Common  mK  .... 

(^halk,  alunt.  ttdphale  ot  potaih  -,   alun  f 

nuulpbatr  nf  tnda  ^  alum  ... 
lArftequaoiitlM  lA  water  ;  aiilphiirlc,  tar- 
taric, and  amir  arlda 
Idmo,  chalk,  kauda,  tulphate  of  barytct . 


AUTQOaiTY. 

Normandy,      filnglejr, 

Waklf^. 

Thnnikon,  Baitlck. 
Hattick. 
NellCiin,  Pottgaiu- 

Kormandf. 
Ditto. 

Haaiall,  Binglar 
Normandy. 

Ditto. 
llAttlrk. 

Nurmandf,  Wakley. 

Normandy. 
ThomtoD. 

NofinaiMly. 

HaaudI,  Warlnrtna, 

Normandy,  Mir  J.  (>or. 

(Ion,  Lclbrby,  Binglejr. 


Nonnandy,  Scuilaii. 
Normandy. 
Kormandy,      l'o<(galf, 

Cilwrn. 
ILulirk,  Pattjtate. 
Kaaauil,  Blufley. 

Normandy. 


l^lrlti  of  nitre    . 

So.  ntnmoiil*  fori, 
'1  r.  t^crrl-M'aqul 
H«dr»ryank  acid 
>fi    »mini«Qir  nra 

Mili.r.iirl.-  eiher 
llN.w-'hloncarld 
S-tnr^ld 
Alcubid    - 


Contaminated  or  adulterated  with  alcohol, 
rhlurtni-,  hjdrochlDili;  nrid,  hydroi'liln- 
r>c  ettuT,  «ih]  compoundi  of  miihyle, 
Utidf*  Maier  aitd  liked  iutMianc^t 

Water ;  alcohol       .  ■  .  . 


Dhto 
Ditto 
Ditto 
Ditto 
Ditto 
Ditto 
Dicio 
Ditto 


Blyth, 


HuulLThonaon.  Blt-di, 

Buli<k. 
BIylh.   rhrt  I  raa. 
Dlilu,  thttn. 
Ditto,  Ditio. 
Haiuill.  Biytk. 
Calvert. 
Haaiall,  Ac 
Dttio. 
Dllta 


Rhubarb  - 

Squilla     . 

tfcmia 


EnKliili  rtmUarb  ;  wheal  douri  tormerlc,  Warlnvum.         Ilaudi, 

Douf  Thompton. 

Wheat  flour             ....  UawalL 

(.lAitt  (if  c-ynatH-hum          ...  VervUa,  Bell,  Sic 

T  r  2 


692 


CONCLUDING   BEUAKKS* 


lAnttHtd  itiral 
SaAVoii      - 
Aronudc  ooaloctlan 


Sperm  oil 
0)lta  otl 
Castor  4iil 
Iha 


I        VSHOTQI 


olb 


Burnt  tponge 
Mtiik        - 


Cochineal 

AMafstM* 

Copal 

Wu 


Apt-XTBKATIOM. 
Ilr«n,  rlav,  utwdutt  .  .  _ 

SttflVflowcr    .  -  -  .  - 

Tiirmerir.  catiia,  pxrpa*  nf  rhnlk  —  the 

iDore  rKpentlfc  iDuriMtcntklifilDg  ionic- 

tlmei  omlltrd 
Whitle  MDil  olbcr  otl*  .  -  . 

Nut  itrul  po|>p;  oDi  .  .  -  . 

Croton  oil      -  -  -  -  - 

l.lusrt-d  oil     - 

Tur[irnllnr.  flx<Ml  and  TuUUIe  oU* 
CorbiHili:  arid  .  -  •  . 


Prfpnrnl  cbtrconl,  rommnn  tn\t   - 
r«ti«  bARi  filled  with  dhrH  blood  ^   Irad, 

drlnl  blood,  inabogAiiy  dutt,  luid  hitin 

nf  Uli  or  hitrsc 
Siilplitri*  of  iMrvtM,  V«nett«ii  talc 
Chalk,  land,  Mtiil  cUy  .  .  . 

Gum  aiiitne,  gum  dammar,  and  coinman 

r«la 
SpemiAcetl        .        .  .  - 


AtrntoMTT. 
Nftrm*nd». 
HuMaU 
Ditto. 


Sininnoii4a^ 

L>ltfa. 

HjumII. 

Bnhtirlt. 
I>lttu. 


WakUy. 
Quckrtt,  Bwtia. 


Normandy. 
Ulttv. 

BMUek. 


Many  of  the  adulterations  enumerated  in  the  above  list  will 
found  rcL'ordcMl  in  the  evidence  recently  iiiven  before  the  Parluimes*' 
lury  Committee  on  Adulteration.  It  might  liavo  been  grtatlr  tx* 
tended, eapccially  by  n-feroncc  to  Pcreira's  "Materia  Medica,**  andlhc 
"  Pharmaceutical  Jounial/* 


CONCLUDING  REMAUKS. 

In   various  parts  of  this  work  vre  have   dwelt,  influenced  solely  b; 

public  considerations,  with  some  severity  upon  the  shortconiin^»  and 
incompelence  of  the  Analytical  Department  of  the  Excise.      The  ft 
lowing  remarks  by  Mr.  Simmonds,  extracted  from  hia  evidence  b«fa 
the  Parliamentary  Committee  on  Adulteration,  ]>oint  out  eleulr  an 
of  the  chief  defects  of  the  Excise  *  — 


"  Tlie  Excise  regulations,  as  respects  articles  of  much  consiimptic 
appear  to  me  comparatively  obsolete,  and  fur  behind  the  rer|iiirt'nit: 
of  the  age.     There  is  too  much  laxity  and  injustice  on  tlie  part  of 
;Treasury,  which  sanctions  admixtures  and  adulterations  in  a  varr 


ADULTERATION    AND   THE  REVENITE. 


693 


of  instances,  u  in  tlie  cases  of  chicory  and  coffee,  canaia  and  cinna- 
fuoDf  wild  and  cullivatcd  nutmcgii,  and  other  articles,  but  ia  most 
virtuously  indignant  at  ndultvruted  tea,  tobacco,  snulT,  and  other 
heavily  taxeil  articles.  The  officers  of  the  Customs  are,  generally 
speaking,  (extremely  ill-infornicd  as  to  the  quality  and  purity  of  various 
articles  imparted,  such  us  starches,  oils,  dru^s  &c.  I  contiider  it 
would  contribute  greatly  to  check  adulteration  if  scientific  and  tho- 
roughly competent  examining  officers  wore  appointed  ot  each  of  the 
principal  ports,  whose  duty  it  would  he  to  examine  and  report  upon 
the  quality  of  all  articles  introduced,  whether  for  manufactures  or 
food,  but  especially  the  latter,  instead  of  submitting  samples,  as  is  too 
fre<piently  the  case  at  present,  to  interested  parties.  In  most  of  the 
principal  States  of  Europe  there  exists  a  Boaril  of  Health,  or  Conseil 
de  SAlulirit^'  (somewhat  difTcrently  constituted  to  our  Metropolitan 
Boaril),  composed  of  eminent  phyuiuiouB,  chemists,  and  engineers, 
appointed  to  watch  over  whatever  way  affect  injuriousty  the  public 
faeatth  and  comfort.** 


A  very  important  bearing  of  the  subject  of  adulteration  is  ita  rc- 
lattoii  to  the  Revenue,  This  hns  already  been  considered  to  some  extent 
iu  the  Intro<luction  to  the  work.  Altlmu^^h  no  duta  exist  by  which 
the  exact  extent  of  the  loss  suflercd  by  the  Revenue  through  adul* 
tcrntion  may  be  estimated,  yet  it  is  very  certain  that  this  loss 
amounts  annually  to  an  enormous  sum  of  money ;  in  fact,  to  several 
mUliona.  The  accuracy  of  this  statement  «ill  be  rendered  very 
obTioufl  by  on  examination  of  the  following  table :  — 


■ 

■^H 

■ 

1 

p^^^^l 

^I^HI^^^^^BB 

^V             694                                  CONCLUDING  REMARKS. 

Rmm. 

Konif  C«iwunt»- 

ttMiUilaU. 

Dull, 

Rtrten  ov. 

Aduiu 

1 

■.    d. 

€            •.     '■ 

<           •.    *■ 

Tm        -          .           •  ai.4M.(ltS  lb*. 

I    9 

S..'i&S.?M    1     9 

5 

277.4111    8    < 

CoAm    • 

ti,wnjm  ibfc 

0    S 

448,453  11     9 

40 

I79,isa    4    •  1 

StigartUDreaaed] 

7,WC.0S9  cwU. 

la  a 

SJSM.im  18    9 

6 

XM.«Si    »ll 

ChleocT  - 

34»llM. 

0    ft 

T    5    0 

30 

a  s  1 

Cdd«  them      - 

fl.9C7  vwu. 

a  0 

Ciiroa  |Mut«  or  cboeoUM         nM^  i^-     \ 

0    s 

Cocoa      ... 

4.471.501  Ibi. 

0    3 

lft,r*3l  10    1 

W 

»,aift  i»  1 

Kluur 

14M0,-119  cwti. 

0     4k 

3B,»4  IS    « 

Id 

»,«4     4    4 

Buiht     .           .           - 

4«(l.W»  cwt». 

a  0 

113,0(17     0    U 

A 

A.ma  9  • 

Ariowrool 

13,(MM  cwts 

0  a 

24a    9    R 

40 

M  a  1 

S«BO        -           -           - 

lM.49ftcwti. 

0     4i 

2.0CM    C  iri 

5 

109    4    « 

TapiocA  -           -            - 

iJM  rwii. 

0     4i 

su   9   a 

S 

4    «    4 

Prpppf    - 

3.C4T.«OH>». 

0    G 

'9l,l<Jft    1     1 

40 

S6,47«    0   f ; 

]-oi¥lRn  *)»rx«r 

94,10A  Rail* 

0  ^J 

4AI     t»    4 

30 

90    8  11  I 

<iinK*r    .           -           - 

»,4l3cwU. 

a   0 

Ji,s^   n  r 

W 

1,070  la    Bi 

Cintiaman 

42.M3  Ihi. 

0  s 

157  ir  5 

SA 

lor  y  tl 

Culia      • 

110,9191b*. 

0    1 

4»    5    tJ 

W 

01  If   • 

i 

Nutm*»g» 

imjueawM. 

1     0 

9.194  16    0 

16 

M»   »  T. 

! 

M»CH        . 

mflraib*. 

1     0 

1,428    2    C 

10 

ua  •  t 

/ 

ClnTM       . 

3S0,«4»lbi. 

0  s 

l,H3H  U  l< 

' 

Pimento- 

a,u6cwti. 

a  0 

»rt3  J5    (1 

Mixed  .Spica      . 

1     0 

CMiircctioocrr  .        .1     63,aflaibi, 

0  si 

629    fl    1 

30 

ins  14  1 

MaU        .           -           -  ;n.879.38l  tHJih. 

4    0 

6,77J.S:fi    4    ( 

30 

i.«ar769  IT  8 

Hop.       . 

SI.MA.»Mltiii. 

0    1 

686,402  It    * 

20 

aos,9aQ  n  i 

Hop*,  foreign    • 

19,030  rwtfl. 

»    D 

K.7W    0    0 

20 

i7.h&a   a  8 

SplrlU    -           .           . 

ll.ga7,17ABali». 

B    0 

«.782.906    0    i 

35 

1.1  ^\7«    8  8 

1 

Rum       - 

9.n4,KHIgalU 

4    S 

i;iifi,«n  9  H 

2a 

320.148     a   l' 

) 

Br«ndjr   .         •         . 

um»i  gmlU. 

Ift    0 

I,l44.<i60  1ft    C 

la 

ITI.M»    t  l| 

! 

Anoano  - 

336Gf:«U. 

14,703    0    C 

so 

7^a  10  • 

' 

Wine,  roreigii    - 

6.1803aAgmlto 

&    6 

t.aw.7ft7  a  € 

2& 

4V4.030  a  t 

Tobafco  - 

ao,s7S,oeii  ibi. 

a  D 

4,&4t.l50    3    t 

20 

9oa.9(io  f  r 

Oitlci.  inviufftcturtd. 

and  »nufl 

SlS.USIlM. 

:  c  0 

C6.K74  IS    t 

20 

la.114  19  T 

Ophtm     .           -           • 

A6.ofirrbi. 

]    0 

3.800    7    4 

30 

R4I  a  t 

! 

Uqiiorkv  iwUlB  . 

MTVcwtB. 

30    0 

I.H7!l     0     < 

30 

ft6a  14    8 

niltojuite      - 

MMScwu 

20    0 

8,643    0    C 

40 

a^93  u  a 

Ditto  root       - 

323  C»U 

6    0 

S,01»    0    0 

to 

16  a  •< 

ToUl            -            -  7 

►078.268  9  4> 

! 

ADULTERATION  AND  THE  REVENUE.       695 

ll  appears,  tTicrefore,  that  the  total  luss  to  the  rereniie  arising  oat 
of  luliiltoration^  ainounbt  to  tJic  unormuus  stun  of  7,078,268/.,  on 
eshniiit*!  which  in  the  main  is  doubtless  currecl,  und  which  is  amiily 
frufTicient  tu  detnunstrnte  that  the  subject  of  adulteraLion  is  one  of  hijjh 
intirejit  to  the  statesman  uml  tho  tinuiu-ier. 

Tbc  per-centages  given  represent  very  nearly  the  extent  of  adul- 
teration prevailing  in  the  years  1851,  lttJ2,  and  18^3;  at  the  present 
time,  in  the  case  ut' some  ol'  the  articles  enumerated,  it  is  less  in  eonse- 
<)ii^nee  of  the  exp(»sure!i  and  denuneiationsof  udukeration  made  in  our 
Kepurls  published  In  **  The  Lancet/^  and  iu  the'  evidence  Iwfore  the 
rarliameutary  Oimuilttee  on  Adulteration.  Ou  \\in  other,  the  calcu- 
lalinnd  are  based  u|K>n  the  returns  for  the  year  1H55,  the  conMunptinn 
of  mi>st  articles  in  tlwt  year  being  greatly  reduced  in  conset)Uence  of 
the  war.  It  should  also  be  remembered  that  (;^eat  rcduettuna  have 
been  made  of  late  years  in  the  duties  uptm  most  articles  of  consum[>- 
tion,  fo  that  it  may  be  fairly  u»!>umed  tbat  a  few  years  ago  the  propor- 
tionate \o**  to  the  revenue  woti  much  greater  than  at  present. 

Tlie  adulteration  uf  Mali  is  put  down  at  30  per  cent. ;  this  is  in- 
tended to  tncluile  nut  only  its  direct  uilulteration,  but  mainly  to  re- 
present the  diminished  consumption  of  midt  arising  out  of  the  adul- 
teration of  mult  liipiors,  so  generally  and  cxtcuttivcly  practised.  The 
same  remark  applies  to  Hops. 

llie  adulteration  of  Su^ar  is  set  down  at  5  i)ercent.  ;  this  includes 
ihe  Hugar  use<J  ^o  extensively  in  the  nninufucture  of  sugar  confec- 
tionery, aud  which,  as  has  been  shown,  is  liable  to  considerable  adul- 
teration. 

Fur  the  increased  revenue  yielded  the  lost  three  or  four  years  by 
many  articles,  Government  is  assuredly  indebted  to  ourselves,  to  Mr. 
Wakley,  and  the  Committee  of  the  llouse  of  Commons  on  Adul- 
teration. 

The  calculations  of  Mr.  P.  L.  Simmonds,  given  to  the  Parliamen- 
tary Committee  on  Adulteration,  establish  the  same  important  fact. 
It  may  be  observed,  however,  of  these  caleulaliona,  that  they  are 
certainly  on  the  aveni^  much  too  l>w.  He  made  the  loss  to  amount 
in  the  year  18^4  to  upwards  of  three  millions. 

If  the  loss  of  the  Kevcnue  is  so  great,  what  must  be  that  of  the 
Public  ? 

We  cannot  more  appropriately  conclude  this  work  than  in  the  fol-> 
lowing  words,  taken  from  a  very  able  article  on  the  author's  book 
entitled  "Fvod  and  its  Adulterations,"  contained  in  the  Quarterly 
Keview : — 

**We  have   now  shown  enough  to  convince  the  public  that   the 

grossest  fraud  reigns  throughout  the  IJritish  public  commissariat 

It  remnins  to  be  seen  irhetber  the  Government  is  able  and  willing  tu 
btay  this  gigantic  evil  luid  national  dishonour/^ 

K  T4 


INDEX. 


xlwrf.  or  lufar  iotvct,  ilffcrlptloD 
n,  Ar«.,  190,  l'J\.  Vj2i  MAblpl.  or 
I,  193;  riuliMt,  ur  int«l  lulU,  'JAM, 
no  I  tiro,  or  cta«eH  »<te,  t»t.  j^i., 

Hilr,  luliilmrkc.  and 
I,  107 ;    CAfTclc,  In  cot 
Xtwuic,  an<l  plioiphoHc.  In  chlcorr 
■Urttfir,    |iu()rt>lrtr.    liuiyriL-,   rji. 
riK,  ar>d  rapric,    In   buttpr.  ',£1*G ; 


nhnfpliorlc,  in 
)ffc«.    I  Ob;    lUl- 


sr 


OMOUf.  and  luliihurlc.  In  rlnegnr, 
Ito;  m  flOO(iMtloD«r)r.  «)»;  Milphiulc, 
UrilQ|lll.B2». 
A«r  btaiiUft*.  45G. 

in  <-otru«.  1)7.     DfltectloQ 


mdpouaA,  W,Jtg^  121). 
IOli«HAnUU)o  uf.  1.     lu  prcTalence. 
M  urf«d  tn  vxtcnuAlloti  uf,  4.     Rral 
tk«  prcTAlcnce  of,  S.     Who  are  lite 
tiltjol?  ft.    CUa«lflc«lion  of  adul- 

0.  Importaticv  of  ihe  i(i)i^*.-ct.  IT. 
§rj  beanun,  17.     Il*  unttarjr  bvAt- 

|u  moral  urarinfca,  tl,  Rrrnvdlv* 
lie{M  rrconim»Dd(-.i  by  ibc  Fatlla- 
.onitnittee  for  tt*  dtwN>iprv  ar>d  iu[>> 
B.  On  the  mejuu  br  whirh  it  may 
Ml,  U-6S.  Apiitlcatlon  itf  tbe  im- 
to  ttt  drtvrthin,  44.     A(iptlratluii  of 

lo  the  latno  |Hirt>u»c.  ^^.  K«a«enit 
In  uidor  to  dlirowr.  Kl.  ei  uq. 
ino>  o(  Tm.  IV'<-I(<4;  Coffer,  lU^^— 
orr.  130— |v^:  Co<o«,  ii\— !•«; 
1  —  10%:    HuiH-),   I'lK.-.i)!;    Mtlk, 

rioiirdiidUf  .  l)uU«r, 

Lanl,  aui—V*  —111; 

t.aia-3V3;   S.  .   Tapl- 

•S9;    I'  V  Frcu 

KW^  .141: 

ma  «it  :  I  uur<l, 

t&lM.  4' 

1,  «!«*_...;,    . 
fUuri'*,    iii.'  - 

!«»,,  4ji>— 4<.| 
k6ft-i:7L     CI-... 

t|ftr  CoorvctluMr^.  4M— 4i«i  iW- 


tM.  490-516;  AI&M&-A34;  GiO.  &'^4— >40  ; 
Kum.  Ml— ii2;  Braiidy,  M'J— i44j  Wt»«, 
.%44— Affi.  Or  Daix:a,  Kvtdriire  brforr  Par- 
llament*ry  Cutnmittee  upon,  56}— 5ffi.  LUl 
of  drugt  adulterated.  6flB~B93.    Sn  Drufi. 

Al>i:iisn.  Tcgctablt,  In  flour*  S39. 

ALcuHMLoHKTta,  rmtrilnut,  Gaf  Luinu'fl, 
SM.    M.  (i«ltler'i  alcnhuliiia^trr.Mf^. 

Alk,  bitter  or  pale,  iitti  \  .Mctiri.  AII(opp'»  am] 
Bjlt'l.  A16.  Quunlon  or  iirycliiiliu>  In,  AI7. 
RxatninaCloa  itf  «aiDpl«4  bjr  tbe  AnAlyUcal 
Sooltarr  CorouilMlou,  Ml,  SaLisracloiV  r»- 
•ult*  ol  the  aiia]/>b.  h\K  r.x<tminatt:>n  by 
Hr>»rf.  Graham  and  HoffiAMn  with  •hnitar 
TMulu,  MN.  Origin  uf  tlit?  ai'cututiuii  aKaiuaC 
thf  Ijoadou  pair  alo  breweri,  MH,  ^19.  Impro- 
b4bility  of  vmrloynifnt  of  itrtchnini;  in  al« 
drmonu rated,  MO.  D«trrt(itit  of  itryclinloc. 
ALK);  itMtt  far,  by  Marcttaud,  M«<'k.  Uttu.  ana 
I'linrnptnn,  .'Vll  ;  Mr.  Kodavri't  pntcru  for 
it*  di-t(srtiou  HI  the  animal  tl»iu«*,  tlA  ;  pbf- 
*iul')|[ica.l  leit  for,  SH. 

ALilKuimtKa,  Mr.  HnlaDd'i,  lor  the  detrnol- 
nallun  o(  rluivn,  MO. 

AlIlaLI  Iq  aruiBltu,  -Ifjti. 

ALKALiMBTia.  Mr.  <jilinity  SCO. 

Aiuru  (L     See  I*Jitirnto. 

All  M  Ui  bnsid.  Its  aClloQ  on  h«»alth.  MS— Kl  ; 
tnlariJ,  3U3;  mpwiteriMTi  In  ctn,  A^fft  ;  In 
pcjrt  wine,  Ah|4. 

AtrMlM*  Id  oiiDatto,  470. 

Amhunu,  bydtucblurtiu,  nltrat*.  and  carbo* 
uale  uf,  lu  ti>b«cu.  ^>iU. 

AMUMTiLi4Do.    Sft  Wtnn.  &&*J. 

Ami  iiu\iha,  ItennU' characters  uf,  acmrdlii|tta 
Yarrcll.  336.  Drawtac  of  true  Kngr^utU 
cncraalcoliii,  336.  Uetchpllon  of.  3.17-  Lar^ 
apeclmen  captur«d  near  \  armrw_ith.337.  \tr- 
acripiioi)  of  thebottl-  '  "   "  i^ 

TkK  4  1111  Mi  ilf.    «jlh  I  >  -   it- 

U.U1  Citt),  «Aidine«,.*|  'iij 

.   »( 


tm 


k 


«98 


IND£X. 


•CV}  Leblnnd'i.  4r.<:.  Stncttire  of  th«  rr«d 
466,  J^.,  4fi7  Itt  ifrMt  uie  in  manudirluHiig 
trwln,  4(ki.  CompM'/iun  nr.  >lfi7.  Adlltua- 
TloMi  oti  orgamic — lurtncrir,  rye,  bMrlrr, 
whrAt,  and  uijta  Hoar*.  4^  i  inornanif —  »ul- 
nhalr  add  tarbonair  tkt  hmr,  mU,  alkalt.  km|i, 
VftiPllan  r»l.  red  Inut,  and  copfwr.  46&.  Jtc- 
«it/<j  iif  Exam.  u(  ThlrtT-fuur  Munplra,  as  Im* 
porlpU,  nj  <ibtiim«J  from  KnjlUh  montirM:- 
luTrn.  a<<tl  a»  (iiirrhaki^l  frnin  ilvalrrf,  46k,' 
4S3.      Ana\yte*,  liy  Ur.  Uernay i,  ol  Qve  lam. 

Sle*  uf  anniiUo  a>h,  46^i.  Lt'Ml  In  ann4[lD 
rtrct>^  by  Accum.  MiU-hi^II,  Hern*}-^,  and 
Kormnndr,  47).  Iiuutiicr  o(  Iti  iiijurloui 
•OHti.471.  MaveiiU  In  annattn,  471.  I^irl- 
Avncr  of  Mr.  WakTry  on  Uie  adnltentiMA  uf 
aniintio,  t7'J.  Kxtmordhuirjr  ct  tdvnn  of  Mr. 
Jlrdwitnd  t ctprcting,  47S  t  of  Mr.  Draw.  473- 
Ul  cini'lormrnt  to  colour  mllli.  butler,  and 
rhecvc.  mnarkt  upon,  473;  Mr.  Stt-p|ivii*'i 
oplnioD  A»  to  ill  lu^lMinnt.  473.  Uetcfiivn 
t^  tke  ndHUemti'tiu  of  ann>(Uu  wilh  lurmrHc 
{Jfi  .  47'^),  wlicat  lUrih.  Tft.  bATiey.  and 
siij^o  flotir*,  47-1  i  *ii\.h  iiilphate  4ml  carbnDAU 
of  limi'.  ciirtitjnair  (if  pi>t«tt>,  rhlorlilc  tif  (o- 
dlum.'rcHl  WwA.  and  roppcr.  t74— G77.  Mr. 
Wnrlnfltnu'i^  proci'vt  for  d«lfctlMg  oxide  of 
coptirr.  47<!.  Quantities  ai»d  ralttn  Imjiortrd 
inl'^HAifl  |K%n,477.     Annatto  in  cheese,  479. 

AnrivtHi'  lUi  K  hi  riwif<t"l!iiiiery.  4*i. 

.ArptK  in  marmalade,  4l&.^.,  417;  parings  lo 
clffarv,  003. 

*'  Agti*  FuNT,"  fi4a. 

ARWRfiUf  IluLK  in  cocoa.  160  i  Id  MiehofW, 
33*4;  inpoitrd  innittaiid flfh, 341 ;  lriuucM,4>0> 

■*  AmorK."    Sfe  Wim-.  JWMI. 

ABaowBntiT,  March  granuln  of  Maranta.  or 
Wc«t  Indln,/^.,  4S  ;  <*urrtim;i,  or  KaiI  Iitilia, 
M.,  40;  Pouto,  or  BrItUh. /if.,  M;  Eait 
lit>ila    in  cocoa.    169.     Origin  of  the  naiiM 

i  **  arrowroot,"  ;II2.  Co^intrtct  whrnce  ot>- 
IAin«d,  ni-i.  PUiilji  vlfMmfi  It.  :II3.  Ma- 
aA>TA  arrttwrmit,  mmU'  of  tirp|iarAttaii  in  J«- 
makn.  Bermuda,  and  St.  Viiirrnt.  313.  Clia- 
ractciiitk-*  and  ■tnictiirc  of  p<irc,  j^jf..  SH. 
C*HP««,ar  l\>t'iiteA  M<j|»  arrow  root,  iiructiire 
of,  31%.^-,  31li.  Ci  ici-HA  arrowtoul.  ttro 
^uolilirs  Ol,  316.  Prcptiralinnof.  SIR.  SCrur* 
tureandcbaradrrtor.  Af  ,317.  Tacca  irruV' 

^  root,  lourrr  of,  Jl7.     IVrvira**  account  of  lu 

[' prefiarallon,  3lK.  Structure  and  charactiT* 
vt,jig..J,\h,M^j.  Mamiiot  Arrowroot,  called 
**  iirullUii,"  tourii*,  ctiarai'tei ft,  aiid  itrirp  uf 
319  (««-  l«plora,8'/7).  PofATO.  or  ■•  faritUh  ^ 
arruwruot,  iiow  prntarrd,  21!).  Cturarterf 
■ad  structure  of,  ii9.  Jig..  330.  Its  price, 
'S3l.  AatM.or  "  TonUnd.  arrowroot,  wbrripe 
OblaintHl.  3%).  Mode  of  iti  prepataTlrm,  3!l1, 
tru  Charartnri  and  tlnirtute  of,  3X3,  Jif., 
3'il,  Gt>ncral  .-i|ipllcalir>n  oftlie  term  "  arrow- 
root." 3W  "OtwcKo  IVrpArct  Carn,"  ladtan 
corn  arrowroot,  .TiV.  AmiLi(iM*Tio«t«  of.  with 
arrow  roota  of  inferior  i)Tt.illiy.  |M:>talo  Atujr, 
■acamea],  mid  tapioca  itarch,  [ri*.'.  Hc*viU<xf 
Ktttm.  ot  ViUy  aiimiiitt,  ytL  Drintion  of 
Mlilltvr.itin(M,  32^1.  StroiiK  inducrmrtitA  to 
•du'lcraie.  .V.M.  Duly,  323.  QiuintltiM  im- 
ntcd  .nnil  rr(aitird  fi»r  tic/tnr  rcnt»uin|f(lon  In 
lUi  ^nd  \*sy,  3'J3.  Eau  tndlA,  Id  cinoMDon 
powdrr,  4.171  In  cuofiivtiauvrT.  4«S  j  In  llqtw- 
rtee.  «»?.jV*.  <■■*».  •       -  -• 


«rar. 


AirH,331. 

AnsKMr  *n  vlnrjjar.  •» 
CO- ■  .  3ST. 

Al»i.-  -Jr  rl 

boucv  'a>t.iiitr<J  irom.  \9X. 


IluiL  KKtrr.  pulp  Kf.  In  opwi 
BAiDAnyCvM,  lufrriuf  cttmi 

Barlet  Fldcb  in  wh«M 

4(M  ;   In  liquorlcw,  «t«. 
BASiOHth  in  aramnaor,  ft.V). 
"  Ba»t  *»!>». "*     Set  SuV^r.  H 
BAf  Li^vrv  in  tra.  Tit. 
"  BlAOl.-xi;."     St<  Gin,  IW, 
Bl-tK  Flo(  ft    In   coAw,  l37.j|f,IVj 

**?./««•.  *^.  5"*-     *^  FW«a 
Baim.letrof.  ill  Ira.J^..  Mi. 
Bur,  potted.  »4f.        ^ 
Btm,  lasUace  of  Iheir  «m««li 

«rt. 
Berr  Root  in  chicory.  1411 

cow*,   913;    vntplcH*^   lo 

bottl*^  red  ft-tilta,  411}  in 

of.  tn  tOt'KCO.  MU. 
Bkllu*.     Sec  UinsLaav  4&T. 
BlX«  ORltLAKa,  ibr  aiin«lta 
"  Black  Jack.."  caramoi.  or 

nlujnl  tu  ml'iiir  ctiSr*,  114) 

tn  TtDC|ar,    99t>  i     Iti 

441. 
Black  JAru.    SfV  Ruit«r,  B«. 
Blavk  Lud  in  tK«.  xl.  39. 
BLdiiHAUDK.      ^r  laincLaM,  id 
BLOATftU.  poUei.  Ui. 
BtnwN  Malt.      Sirt  Porlia*,  VV. 
BLtra  Stook.     5(V  Ptrhlwa,  407. 
Hoik  AIimknian.     fl^  AnoflMiB] 
B^'LO^CAKo.     Sr.'  ^mtif, 
HoHftnrtT  li    ■ 
Bf.fcii.    .Srf  I 

BllTAVItAL    t  J 

BuTAhV,  tUilt  iiirA      Uk-1 

Of.  N3. 

BiAiM*  (abrrp's)  Id  nilfc.  ^\,Jig^T 
Brak  ill  oaliocttJ,  a«»  ^  tal  MMrt,  I 

Bt  i*»H\  usnl  bf  M.  Parcm  Ia 

milk  aui 
diktlU 

Aixltrb^i  .     H««tr,Mfj 

spirit,  sugir.  [n.>U*M  j.  iMal  w^k 
M3  "Brttlth  hraiMjy."lw««H 
ri<>UJ  Krt'iich  tir*n*lir,  lorw«|^ 
roct-rc  of,  MS.  »4f.  U4ft  M 
brandr.  541.      iTrjMAi  n^  Xm^  « 

Act  rr>ri^ 


Irtf,     ! 


samp'r 
itr> 

rat 

Km 


Ml. 


Ill  1,1 

llaAeiu«H  • 
"  DaawtRN 
"  BimiH  ><• 

BrI'MWICK,   « 

t\ttn«ry ,  4s5. 


IlLlR 


^-■•■aum   tJitfJOVa 
Brsndr  HI  fOTf 


INDEX. 


6*» 


Mte  wiw.  aaa. 

I,     At  ■■  BUrk  J«ck." 
Bilk.  VOC.     M-'thorti  nf  pr^pftrlnic 
Mhllif*  of,  VOS.  i<j6.    Cotni^a»itt«i*i 
■if    111    ("hnrnil,     Brom^i*.    And 
•    Ani'LTBRATtow*  or,  with  w-urr 

pnf.  CnUrrt'*  tividrnrn  r»*ri<^ll<i)t, 

^>t>io  riaur  and  «nlmiil  fata,  277. 
Jtrttitj    nf  Ktnm.vl    Yot\\-r\tht 

Itiillrr,  •gfi'  letter  from  Mr. 
luitrratrd, 'ilMi  fTiwn  "A  Stinlcnt" 
mpulitan  mNniiraL-titrr  ol    Kpi'trif 

iMr.  iMfn  o(  the  aduittrfAlkixi*  "1 
Willi  water,  twfi nirtliod*.  'JM. MO  ; 
I,    l^rd   (fig.iOA.].    NijJ    ttlt.   -WO. 

ImMit*.  IK.^4— ImV.,  301.  Au. 
Ui  culuur  Uiltvr.  473. 

I )  l««f  nt.  In  tobacco,  8M. 
I  In  co(fr«,  IW. 
CoOw.    1(6.     Procea*  for  lU  n* 

•. 

'■roouuk  oil.  to  rofTpA,  107. 

UM«tLA  uwd  to  aditllarate  t««,7a, 

portpr.  MT. 

14  M.  AV. 

«  In  Nailvlra.  Kti, 

haftr,  and  Confvctlonerj.)  Snnr 

Wo*  MM  MoU  •rrovropt.  316,  Jig., 

ffOWrooC* 

pilas.  or  t«n|M)w4cr  te&.  j<f ..  ao. 

r  Ctuititn.  M. 

Mi   la  port«r,   007 i    In  ftn,  UG. 

•. 

reira'i  arcount  of,  319. 

pit  iiiir&r,  or  "  Black  Jack,"  iih4 

»ffrr.  IH. 

■0*.  Inftulon  o1.  In  porter,  607. 
to.    ^n-Avid. 

lH^fJk:  381  (Mr  Cttrry  Powder) ; 
17*  Itoif  M,  and  on  cklraet  of, 
i  bokie  eottiuwpClon  In  IMI  and 

utod,  |»  ci>lfr«,  117:  In  cblooTf. 
■a  food  for  cawi,  Ills.    Di«oeU«n 
bUr,  In  milk.  Sll,  motff   Jotcfl  cT 
IM.  «79. 
ik.  WM. 

tafiit-ra  pltatt  S19  1  rarlotia  aperlM 
IT  l'.itp<nct. 

fMuiltiiit  am!  •tritr(ur<>  tit,  4%3L. 
»<lh  rliinaninn,  433.  f ./#.  »h««- 
Wpntut  rhamctprt,  Ol,  4XV  O^ 
lapuwdrr.jlff^  436.  lu  um  na  an 
Of,  and  fVvqiamllr  ••  a  lubaituto 
Min.  and  lorthMa  tor  drircilog, 
Viitf,  and  aUMilHr  iniarml  lor 
Bioptlon  Id  ISM— INM.  f»».  (5<v 
)  Oil  fi(  cataU  In  fin.  AM).  Ea. 
.  aromail<^  w>nf«ti<>r>,  (iTH. 
pa  AaoMarirrt,  444. 
•m,  it7 :  dM^cUdti  01;  lOVi  la  lo- 
in np1«m,  fiM. 

iDluOird,  Ml;  In  Mpprr.  MB. 
HoUn.  and  dHcription  oT,  SOI. 
k  of,  MM.  Durbolt  aiid  Bracnmvt'i 


umlftn, 
at. 


MB,  309.      Capslrin.   Perdra'a  ae^ 
369.     Struetmrf    nt   the   npalcum 

*wT.>^f» .  **.  3'o.  ^'.  ST*.  -^Ts.  2?*.  arft. 

AlH>lTTkATIOl>l»  o(  Ca^cnnr,  3Ti.  Httuilt  of 
Exam  of  Twmty>cl^lil  aampli'*,  37i :  rod 
Uad,  371,  373 ;  Venwiao  red.  rH  «Khrr.  rwr. 
tnlllun,  or  Dltulphur^t  of  m'*rcun'.  Krotind 
tier,  lurmrnr,  utll.  and  niiiatard  hiitk,  37-1. 
liUUoci!-  of  polaniijiiff  by  rrd  Ifad  lii  fnyrliw, 
37fi.  E'Mfrcc  I'T  Mr.  Scfirtlaii  ncu"  *ulitb1f> 
Cayran*.  .V-b.  37^:.  Uetetttvn  •>(  adujlrralwm* 
wllh  rice  flour,  turin«rlr,  Mnd  tnu*Litid  huak, 
fig..  376;  uf  ri^l  kaJ,  377, /Ijf..  37rt;  of  tiliul- 
pliiirpl  of  mcrcurr,  »77.  Diiy  un  ratciine. 
STKt  lu  rmpld^rn'til  In  the  adiilt^ratlou  of 
Blnfcr,  496.  In  gin,  hVn  Itt  mm,  Ml. 

Cbcioomvia  Tkitrki,  or  wlioat  nild|i«,  2<^7. 

CKHKtra  fur  cloalinr  the  urlla  i>f  mtcroM-ii|>ra  : 
Gnadby'c.  Qiiekptf'a,  Hr<H>kf'«.  uid  Hctl'i,  M. 

Ctrtiaaut  IfirMf  TAKna.,  f-'S. 

Ciaa^lNi,  or  tuiiar-r<inc  wax,  IHI. 

CniBBAL  MATTiia  In  milk,  ',^1. 

CflALR  ill  «uitar.  jHM  ,  III  hfHirr.  V03;  In  potted 
mrati  and  flah.  Ml  j  In  anria'un,  *i^ ;  in  coB- 
twt'i l»n<^ r .  4'jN  ,  In  Mmniiiiniy,  G.i();  In  Ipeva- 
cuaiiha.  Oii  i  In  cuNtcynlh,  (>7ti  ^  to  c-rniKiund 
aranimvny  iMtwdrr,  fl(H :  itt  aruniatic  coufK* 
Hon.  (7711,  In  hqtioiicv.  tiM. 

CuftHraoffB.    Sf€  Wln«,  AU. 

CNkRi'oaL.  pxwilervd.  h)  opium,  G3B. 

Chauam-k  In  BMittard.  3I«,  Jle.Sfet. 

Ciiti«t  tn  niilk.  'Jt>6  I*ri-cl|inat"Mi  aiid  pre- 
(laration  of  lh<*  ciiril,  4*7, 17**  MnUui  operamdt 
of  r«aDM,  47**.  ReaAou*  iirgrd  ammtt  it«  uk, 
474.  Profkortlmti  of  catrin  and  buti«>r  ililTtT  In 
CiMcae,  47)1.  Sailing  In  Scotland  and  Cltfthlrr, 
47^.  AoirLT>ii4Tioivior.  wltb  Riaflgtlld  floMeri. 
MffT'in.  julcc  of  ml  carrota.  tnd  aonatto.  4)9 1 
«llh  Venrtlui  rnl  and  ffrcjue,  4ltO.  KUviiitr- 
Infi  o^  with  paral^y,  aaa r,  and  f<niujirr<'k ,  4Tt*. 
Potato  cbeea*  la  Thuniif1«  and  SaKony,  llio 
prociTM  nf  Riana'aclurr  ilricrlbrtl,  479.  Rf- 
tmH»  qf  itxtfit.  »f  Tuvnly  aumjiln,  ISO.  Ac- 
cum  and  MI*clH!ir«  reioArka  apon  iMd  in 
chraav,  480.  Cauac  of  premi  i-nlmir  In  ninuMjr 
cboraa,  tM;  how  produced  In  n<rw  rliraar, 
4SI.  Aearua  ciro,  or  chrraa  mlio.  4*1.  j||x.. 
41)3,  4A1.  nnpbtU  otx-l.  or  cb«««o  fly.  a(-c>M.oe 
of,  by  Mr.  Duncan.  4MI.  "  Jutnp«ri."  their 
mvtfaad  of  aprlntcknfc.  4p1,  4A3  DriKtitm  ti$ 
ike  a^mitrmtioMi  of  chrvif.  4K3;  wlib  Venr* 
lUn  rt^,  4>M.  Import  duty  ana  hooi*  «oa- 
auniptina  Id  |bM— ilvSC,  444. 

CHlMiarBT,  H*  appllraiitrti  fo  the  dr(prti>»n  ol 
ad<|ll«r*t-l"0,  M  —  h'i.  Chrinlcal  app^raiua 
rr4)iilrcd.  Sft.  Chief  prrlimtnury  rhrtnlr.al  ofw-- 
ratloni,  A7.  litiofrnta  rnjuirwil  for  drtivllny 
adii Iteration.  CI.  L'tcful  laurka  un  th«  auttjcct 
nf  chniiiatry,  03. 

CflCttav  LAHaaL  walrr  li}  gin,  UO. 

CHiruRY  UMTd  lo  adult^rati!  <-ofl^,  flg^  47. 
gu#M)oo  nf  lla  adinixturo  with  cmi'i!  ron- 
aldrrml.  MR.  r-riniraa(r<l  wllh  rttlfcf.  Mti. 
119.  I'll.  Hoteiilon  of.  In  coffrv.  \%l.  Apr,. 
134.  IV7,  I3<  romniUtlOfl  of  Clirnil*la'^upi> 
nlrni  upoit.  114.  M'lluUarh'a  iU-*rflpl)iNt  of 
Uia  chicory pUnt  *ni  iia  u»c«,  liV),  l.l|.  L^rgr 
cnttiratlan  prinripjilr  dui?  to  Govrritmrnl 
patrooai^i  Ul.  Foreign  luperlnr  to  KngUah, 
131.     Anaifaaa  of  the  root  t^  autlmr  an  J  Ur. 


rth) 


INDEX. 


L«thH>y.  131,  l»,  IA3^  by  MMtrt.  Graham 
aotl  Co.,  lU,  IM.  Strufturr  of,  134, /<*  ,  47. 
laft.  136,  137.  141,1  ia.  tnpfrtift  ol,  ftreir*'* 
nbipnriiliont  iipiMi.  I3fi.  IS?.  Vmfcunr  Ji>hn- 
stnti'i  rctaatka  r««pfi:tlnit,^l37,  HB.  I'liwholr- 
tatnrnetiur,  u  an  aritclFoffUpt.  intunrvt  of, 
i:tH.  Um  of.  Aft  an  anerlLMil  In  FranCf  aDit 
GrrnMny,  199.  Bltndnou  a  letiilt  of  Ut  roa- 
timied  itM*.  139.  Amii.'rpR«Tin>t  of,  140; 
with  llambrd' poittlcr,  coffee  Highu,  romsUHl 
vlieut  ijig.,  141],  ryi?,  tK>Jn>,  M-orni.jff.  14?, 
cirroti.  ^rinipi,  maii^oltl  u-unrvl,  bccl  root, 
■awctu«i,  b^ktMl  n«era,  HO;  with  burnt  lugar 
or  hiark  ioik,  V<-iirii%n  rrit.  Ami  otiier  red 
eartbt,  uak  bark  Ian  i.fii.  143),  and  rxhaiutnl 
tan  oxrtiMtiJig,  Ul),  141,  Mr.  Gay'*  rv|. 
dmce  rM|i«ctlnff  ihc  mrtiiuracturr  of  carrou 
and  pnrinip*  inmchlcorj'.  I4l.  IVrvlra't  d*- 
Kriplioti  of  llambru'  pnwdor  and  rnfTnf  ni|;hta, 
141.  HiH  retnarUon  Vtnitytlait  r«d,  Wi.  Re- 
ttUlM  Iff  Eram.of  Thiiti->four  iMiiploi,  143; 
ot  Thirty -rlgbt  additional  tainpicft,  144. 
I^rgfe  profit*  of  iht  rvtiiilfrji  ti)>uii  ilie  ial«  of 
tilt*  .idultjrtaled  article.  14'>.  Det^iltou  of  the 
ttiiutUTalion$  of  chicary,  14.'^.  Ita;  tdrntidva- 
titiQ  dlAcult,  f&crfft  bj  rncani  of  tlic  micru- 
•copr.  IIA.  Wa(rr-t»t  for  detn-ttny  ill  i^re- 
stmce,  M'*!,  I4C  ;  »rn*lfic  gravity  aod  kugar 
Cnta.  I4fi  CompokltlitD  of  coflW  and  cbicuff 
a»b,  117-  QuMUItJiUva  Mtlmation  of  >Mqul- 
cikidt!  nl  iruti  lu,  149.  IBA.  Reaine  qf  reamtM 
urflrd  bath  for  and  againtt  tbc  admixture  of 
chicory  ulth  coffee,  IM— IA9.  Rruoni  In 
favour  :  ■uminiod  iirprovnnrnt  in  flavour, 
1^1  :  nll•r|:*^n  increased  coDiiiDiptioa  aod  mure 
^Fri»rnt  i-xtftiolrin,  IVi  ;  Ifgal  (ttnrtlon,  and 
fi-lf  proietrtiHK  )>uwit  of  ihr  public,  IM:  fal- 
lacy of  aFfiampiiti  ibown,  I.VJ,  |.%3.  RcaMina 
ag«lntt  :  niTctBary  commlkilitn  of  moral 
fraud  — fupp(>»vd  lutal  effccli  reiiiUi[ig  (rotn 
poiaon  owing  to  tin'  »u|>hi»ticat)uH  of  Ittaiiti- 
dutc.  ift4  i  lniu»tn-e  to  the  coBcp  p-owcr,  in- 
jury to  the  revrtiuf.  p«<uniary  fraud  upuo  ttte 
pilbUc  :  rfioed)' piopoinl,  154,  \bh.  Frvftrut 
and  pro«p«ctlirv  duty  un  roasted  and  ground 
chicory,  ISA.  Chicory  kaf  in  tobacco,  SM; 
ro-iatcd  root  in.  WJ. 

Chilis  In  p*p|Mrr,  36A  ;  in  vlnvfar,  40S. 

ChikaClaV  In  tea.  Kl.f)9. 

Chikmr  Botanical  Powdri,  uied  to «dalCera(c 
ten,/!);.  93. 

CMINaLDAIl.  chonXPl,  604. 

CMLoaA^Tdti*  I^coNsnctJV*,  ui«d  Ifl  tbc  Keat- 
ing ofuu.  Ot.Jig.'9. 
Chlounk  in  ath  of  coffee,  107  (  )n  ehleory  lab, 

1.14. 

CHcx'oi.tTi.  itk  mode  nf  prrparAtloa,  171.  Re^ 
Kultt  tff  Kfom.  of  Twelve  •.unpki,  171  ij^.  of 
adiiltrratPil,  177. 

ClIKuHATB  or   LXAU.     fitC  LcAi). 

Citaoita,  Uraan  and  orange.  In  oonfectloDBij, 

CiMR  In  port  wine,  MO  :  In  ctarvt,  AM. 

ClOAH.     Ste  Tobacco.  QOI . 

CurwAMDM.  where  cullWated  and  how  ot>tjilDed, 
4!0.  PpTclvari  arcifunt  of  II»p  procesi  of  bark 
peelinit,  430.  Ci>i*fp^«i7rvfi  of,  430.  Strucfure 
uthark.^g,  431 :  nr  i>o«der,  433,^.  43V.  Sub. 
atltiltlon  of  CMikia  for,  433.  ComparlMtn  of 
vAula  with  cluMHmoii.  and  jd.'j.  li(u«irattne 
Ibclr  dLTfrcncrt,  434,  43.V     /{fmUs  i^  A»0f.  uf 


Tblriy-two  •nspica.  KT.  kz 
with  cAiala.  baked  wmmI  floor 
IndlM  arrowroot.  Mi4  »Malo  ^mt,  { 
terttoa  of,  137,  iM.  CuMMKa' dH||. 
tUT  pnierrd  fur  botao  ea 
I  ■A.,  43*, 

CiraoN  Fin,  candled.  4|A 

CUBBT.       S^   Wll><>.  hft4. 

Cut  in  moatard,  AM  :  io 

Clovm.  d«rlvat»aci  of  ib«  M«««  MC 
KBthirrtog,  441.       Caiy a wWaa  aC 
thranalytra   of  Tto«n«Bd<W#«a4  IS 
.Stntrtmrf  of.    44^.    44t^  *U>^**V 
TiaATlOM    of.  with  cUivm  mialk^, 
and  water.  ilR.      t>.i.  ^t^m  af  (r 
ho«D«C<IDftU'' 

Coal,  btoudu 

Cobalt  In  c> 

CocccLT-a  1n'  f 

extrarC  of.  .  4 

home  cout<  .  l| 

culm  iDdicu*  in    ■ 

Coccit  OAcn.     *< ; 

COCHINCAL    iu     £m*.  ■ 

uuieei,  4101    Ui   vu..;..-;^.^—. .    .t.  .  J 
wiue,  MS. 
Cocos  r&Alted  origin  of  Ifta  bmb^ 
wrlption  of  cocoa.  lU,  tlC  VvtiM 
and  mudca  of  jpi  eporWUcn.  U^  W. 
fwn  of,  honrding  to 
IS7.      lu  iropnriMi 
eoaihtueoiB,  lU.  IM»      T^ifcai  rfi 
lM.rtC*-  l>9.  1^1.  IM.Itt.  li 
prfUrt  of.   It^.      ConiMrlMm  ^  ■ 
coffee  atMl  (««,  166,  tsi.      AaCUl 
Ifiti.    Horalit/  ot  i»f  «iMona  OM 
lloneit  courts   fo)l<t«ir<4    by  0t  I 
uth«r  Coiiti'  .  MUe%mm» 

maiki  or   ''[  >    •»«  pi. 

UjpOfilUraj  .    c^iOalAl 

IbT.  Attt-it:|  .>ii  iic-iviicv  of  Ua«M 
ttarch  And  itigar.  Its.  Adtalninri 
with  whrai  Ouur,  rvlala  ilMii^ 
Eaat  Iculla  arr%<wrt>ol.  T^»  te 
■u(ar,  Ifli  i  with  Vntcttaa  ral  a«tf 
olAD.  Its.  Bvktoopw  of  Mr.  n 
109.  IM.  Re  mtia^  JCmoa.  afa 
iTn.  AdulirrotlMi  wiih  dUnaTfli 
cucoa.  Dr.  Vn  «ad  Prof.  J«ta^ 
DOHA  coocerninff.  170.  /)<««—■  a 
trrattomM  of  cocoa,  in  ;  W'  t^V  < 
173;  of  whaatSottr,  MatoSiNar.aM 
173;  Indian  corn,  Marsatx  cr  VC^ 
CiuTuniA  or  Emk  ' 
ftrmwrooU.  IT4  ;  ij 

of  adulirratnl  r>"  ,3 

CeU  for    dJli-OTMKIf.-    j-r-i- rr.L'.i-. 

COCOA  by  flubkidence,  I7f.  -  by  u*e 
chnnitirf.  177  ,    lf>Al,«tn'«  pr 
Icdton    of    ror«4Kn    r«t4y    m^ii 
faandr't  mrthod,    I7«.    17V  (   *d 

ataace*.  I7if.  iw.     Uwtf.  «iid  ^ 

tloo  in  lH\4  — iK'ft    l«a 
Con-f  ■ 

CoFKt 

W'i  ')ik«ry<ue4 

nf.y^-.  tr.  IkactlpCioactftM 
berry,  lOV  L*av«a  pci»»ew< 
In  Suaatra,  IQi.  <!^<i—iarf  i 
propertia.  106— 1 1&  tteki^ 
rawandfoaatadcajha.iat.  P^oa^ 


INDEX. 


roi 


•e.  IOC.  rer-rtituitei  of  tujiar  in  raw 
•t«d,  106.  ftraban  wul  atmhuiifrr>'i 
loftheaih.  107.  Ciillbinc. rAffpone.  and 
Bid  th«  moit  Impoilant  ronititiiei<t«  ot 
rj,  107.  UrMcmal  fnptrlift  oT  the 
,  acrordltif;  lo  FervirB  anil  Johniton, 
t'nffiT  and  tm,  ni  brrcmuM,  com- 
IB.  I'er-cenLnie  of  iflulrn  In  mSrc, 
DnmnriiUvc    *ni)y»ii    u(    t^a.U!»r  b^ 

xikI  "(  coffrc  iMfrjr  by  Psfcit,  111. 
•e  or  cofT'^r   H-r<1,   111.   Iiat^*..ll3. 

Aul'LIt-NATioHit  ftf.  113;  «llhi.'lilcnn, 
■Icki  of  tr«(le«mrn,  Mr.  DurVwotth  • 
IH.  Cotfc*  motflj  (tcftijlin' in  h'rjinre 
m^ny,  ll'S.  tiuctiion  urailultprxtiiiD 
*ory  coii«ldrr«l,  110.  Onvprntnrnt  r»- 
I  tr»|n-cflii|C  ciiffi-r  tnual  »Mh  chhfrv, 
ttrv  AUfl  f  hif orjr  1-ontrjutfd.  1 117.  Adiil- 
wlth  rtMutnl  RrAtii,  r(x>ti,  itctini*,  i;i<r- 
(Un*.  tMk-lMiK  (an,  cxbatiitrd  txii  or 
,iul  tMki-d  h<>r*i'i'  and  bulli'Cki'  llT«r*, 
Ijiritf)  imimrUttiifi  ol  lujiln  wrtd* 
tgn  acomi  for  purpiMi-i  of  Mlultera> 
r.  bifurtiirrt  [nnrMl  hi  ctttRnUt  Jig., 
olouHng    miillrr*    «m[>lnyt-d ;     burnt 

"  UUfk  Jock,"  lis.;  WneiUn  rvd. 
■nUtt  cf  yftcrot.  Fsam. of  rhlrijr-rnur 

of  coffr*.  ni),  IW.  Impri'tcnicm  In 
trattnr.  I VI.  Krutttrd  orn  rxttrnilwly 
k  kubtlitutc  lot  cvltev.  1)1.  Deiect'un 
auUfrati-jm  of  coflMi,  131,  \TL     l*tr- 

uf  (ugar  III  roa»t«d  cutTro  and  Iti 
Dp  root*  u*ed  In  It)  AJult«iatiim,  IJ». 
nation  of  t^f  vuitar  iti  «lult(>ratnl 
a.  Detccttnn  uf  chicory  In.  I  :^,  Jiga., 
,  138 ;  ai'lninn  of  ('{iminUiion  of 
■  upon.   \iA.     I>p(prtlini  of  tnmn^ld 

VH.   fit*:   ISA.    )S6.  i    l>r  carrot   and 

\ih;  ot  whvat  llour.    139,  136,  Jlg^ 

brnii  floitr,  IST.^jf  •.  I'Ji)  i  i^f  r«aited 
ind  MCOm.  1*iT,/l^  ,  !'£);  of  uwdiut. 
;  of  raiamcl.  nr  tutrnl  %i\g'\t,   Wi,  l'i!i ; 

Ian  riHl,  tao,  Homr  mnaumptHHi  aid 
iM— I9.V.,  i>o.    Co(r«  rligiiu  UMU  aa 
Btani  of  cfalciirr,  140,  I4i. 
I  cotfiw,  117.     ^ructurM  detectMl  In, 

n,  figa.  S}b,  QG,  ADirtTaiATIONI  of, 
mdB,tf7&i  wKti  wheat  flour  and  tbaJk, 

«.  or*-bwu<lRfi,*'lll. 

'  IB  fiorlvr,  filO. 

r,  iMf  of.  In  lobAcco.  M8,  «M.  AT**  W, 

■,Parlianvnur7Jnn  Adiiltrrailnn.  Ifit 
vmtwn  c<imni  Ump.  37-  E«lilc>pr«  be- 
(Mt  lb«  adulteration  of    drugt,  £>€3 — 

I  ScavMcMv  PnKDBa,  Its  pri>|)«r  mn- 
I.  ft7ll.     AntxiKKATioxftof.  with  chalk, 
HIT,  and  p4»w>lrrrd  J^Up.  679. 
ira.    Srt  Kldur.  a77. 
»*,    Afofi»«ln*.    cry.      Ingrrdlt^ili    of 
ifinuld  conmut,  fit'j.     AnvLTkRATionn 
(urnipflr,  cKAiIti,  iind  chxlk,  f!?^*. 
iMtav.culouird  fuxar,  l>r.  O'Shaugh- 
rrsutrki   U|>un,  4d4       AuiLlkKATMina 
with    Irmon   and    OMnit<>    rhrmnr. 
e  of    lead,   nmbocv,  cwhlnrAl,   rrd 
mtUlon,  umuCT',  liidl(ri.  Antwerp  and 
I  blue*,  iiltrunartuc,  aiMl  Bruniwick 


flTftn,  411.%;  with  carltonatr  and  anrnitf!  of 
rojiper.aod  whirf  Ipd,  4i^i ;  with  inlphat«  »f 
llm<-,  whmt,  and  pouio  aniir>.  iu>d  K.nt  [tulla 
arrowroot,  4W*,  Rctuits  ./  Eiawt,  of  tanipliii 
|iurtliiurd:  tugar  treiU.  Uii|t  and  Karc,  4"'!  * 
nilXMt  auirar,  «nd  twrljth  rake  tiTiMmrnta, 
4*(7.  Dr.  Thmnion'i  nldrnce  rrffanliiiR  th** 
rmplnimml  of  terra  alba  in.  4KH.  Mr.  iiny  on 
tticadultvtnUonofcaniwny  comfitaatidpepitrr- 
mlni  loirniit-a,  4K^.  Iiijiirlntti  ai.il  |H(Uu*tuu» 
**M»iicc«*^'  uv^  in  fl4tourine,  4^!*.  Jlirir 
iiicprfibibllMt  in  Francr,  Helfcium,  Atid  Swll- 
xrriiind.  ^*i.  l.i»ti  of  cului.rv  tlir  \\tc  of 
wlihrh  may  b»  [wriiiltKhl,  nn-t  ibruirof  whirb 
(tinuld  b«  prohtMird,  490.  i'J).  1'hr  Uftvr 
wiirmlly  emjiloyi-d  Uv  iii.«nur(irtUTrr».  4dl. 
iMrttwM  nf  ailutteraiiunt,  A[<'l.  I'rgftiiM^, 
mnnnal t  anti  ttnntTcU  tfiU  :  ci>chinra)  and  rnl 
lvHd,4!#*;  vvrinlU.Mi,  494.  IV/Zaf  (WtJirrf  .* 
mlnrraJ^  Winon  aud  ijrainj(i'  rhrompa,  chnv 
inatpuf  Irail,  Niiplf»  yi'ilow,  and  riA.iJcrtt,  4'H. 
AVt.  VcKrl-iMi-  —  turnirrir  ulfron,  and 
f  (UDbotE«-.  40S.  iiivcColo*ii$:  VrB«*talil(t  —  III- 
muB  and  indlfcn,  4it^.  Mineral  —  l'n)«ilau  and 
Anlncrp  blurs.  arliQcial  uliramxnnc,  cDbalt. 
and  •malt,  4S6.  Grten  CvUrurt  :  \rif<)t4bl« — 
■ap  grt^u.  MptAllir—  v*r<ti|[r>*  or  jiirt.iti'  of 
coj'P*'.  ar»enlit>  of  ctippcr.  eniprald  grrrn.  and 
Kniiiiwlrk.  or  («m|touiid  gru-nt,  4ii7.  Brown 
Colours:  Irou,  4'.it«.  t*ttipic  Vviumt :  Mta. 
tun-  nl  Antwerp  blue  and  ruic  pink,  thtr  Ukr*. 
or  oirhiiif-al.  4!!'*.  Sronxr  t'owdrra  i  Copper 
nnd  ainr,  \^t.  Dctrctlon  of  chalk,  pUntrr  of 
pjirlt,  and  clnv.  41)8  ;  of  dtflV*!!-!!!  klndt  of 
itarch,  irr*.).  Uuty,  prrtrot  ami  iirnk|i*>cii«p, 
Importaand  quantltirt  r«>lainrd  fur  hoiQccon- 
ttlinptioa  in  )H.t4  and  KM.  Vy}, 

ConVOLVVLt*  :k-ANMOI«IA,M7. 

CorpRa,  rarbonatr  and  irafnltfl  nf,  in  tm,  ^7  t  lul. 
phat«  or,  In  bread.  W.;  iul(thatK  and  MCrtatn 
of.  In  picklp4,40ft,  ft  iri/.;  In  bcitl*?.!  fnilta 
and  vr9ft»t>lp«.  41ft,  ei  n-^  ;  in  pr»-»civf«  and 
Jrlllra,  41A,  4irii  in  tnucd.  4W  ^  •ulib.Uanf. 
in  annatto.  46)1 ;  carbo.'iAt«  nnd  arwnit*  of,  In 
confectlnnory.  4fM! ;  in  wbir,  ^G(),  Ul. 

Copperas  tn  tobacco,  H9. 

CoauNDH,  3714,  JV.,  S79;  infuilon  of,  In  wrtcr, 

Cuao,  mastvd,  titad  aa  a  lubitllute  for  coflcCk 
HI. 

Cnao  SrimT  In  bmnily,  Ml. 

CiiaaoiivaSriiLiuAT*  m  vln«gar,397. 

CowDl'AC  In  upluiii,  €38. 

f'RBAM.     Xre  Milk. 

CaoA-ri.  or  rxhxusfed  Un.  In  eoArt^,  I  IT. 

"  CrrEoo  Plirr,"  3?l. 

CrMi^.  -i^l.Jiff.,  .W*.     Xrr  Cirry  Powder. 

Ct'UMiMUH.  malt,  lit  IoImcco.  'Vw. 

C'rnci'M*.  or  E««t  Indu  «rroN'root,  174.  310, 
>li;fr..31T.  4'^     Ser  Arrowroot 

Ci  arvMiM.    Sft  Tiirnerli.  3«7. 

C'can.    See  Milk,  and  ClieMi>. 

Craa4wi-«,  411. 

I'i'HKV  PottUHR,  niimwrona  ln|rTx>dl^nta  <>nt»r- 
lug  lnlo(Jbvc<Knp<)iifi''in  nl,3;i3.  Cuauaiiia, 
•triK-tufpof,  STt.jfff  ,  S7t>.  t'jiKnAMOM,  «(rui-- 
lurr  of.  3AU,  Jig  ,  yn  ,  ii.  Schli  Idrn'i  KUtc- 
tnoiit  rvaprctlKi;.  .M).  ('liMl.ii.  ttructurr  of, 
341,  M;,  rfjf.,  3-'^  Mint  im|tarUnt  con- 
atthwnl  of  cnrry  powd«T,  Mi.  haMOoaaKK , 
%lruciUro  of,  }<<3,  A{i.,  4H4,  3M.     AuuLTtK/  • 


k 


703 


INDEX. 


I 


TlON*  orcurrjr  powilcr.  3<13.  ftfimtti  of^jmrn, 
uf  Twrtitj-alx  lamplfi,  :t'^,  Adulterated 
wttli  ftroiiitd  rii'6,  ^xmo  farina.  Hilt,  niid  red 
IpmI,  3MJ.  D«l#cllun  of  [K»t«I(»  aUrrlt,  3bi>. 
rnitnmi'  diit>-  fm  curr;  imirdnr.  3WE, 
CrcihiKit'M  iMrtuui,  I3U.    ^rcUhlcorjr. 

Dai'-iL,  bcArdH   or   poUonoiii,  Ki.Jig-,  V7, 

Inltiincei  of  U*  f-iUl  cnVrit.  VA. 
ncn>iMrrni  of  M.  Coliftrd^au,  329 
PciTHihi  In  •tiRtir,  IM:  ill  •c^mtnony,  ii-W. 
DiL4TUliRTSIl,ucolialomvtrlc.  M.  SUbermann'i, 

DwK   I.KAr  Ui  tnlMurca.  M».biQ/ig*.,l>'Jl,fm, 

■W,  KM. 
'  I>ocTi>K.  Thi.*    or   corrotirff  tutjllmatr,    In 

vltifK^r.  .V47i  in  via.  ft29. 
P'lLh  iios  StiJi,  or  4'MrR,  419. 
•*  |U»»»N"dorri.<<9. 
Dni  u«.  Mltilleriillim  of.  rvhimM  birforc  Pirlla- 

mvntitrjr  C'mniiil(t<N;  uimxi,  MA—f>€ff.   AorLTft- 

iiATioNsof  rnlMrco.fi£!i— r.iS^  Ojiluin.fiM— THti; 

Srimmoiiy,  M7— C.V%;  in\n\\  ii.yi— 667  j   I)*- 

ricuBiiha.    f)fiH—fi7f>  ;     Culocjinth,    fi76— 677  ; 

Ithubub.  G77;  8(tiillU,C78  ;  Compound  Scam* 

moiiy  fowder.  fi-^O;  Atnmatic  Ci>iifi'ril(m.67!* ; 

Liquorice,  <>7*J — G*«u.  TAbulatnl  Liii  o(  Urug* 

and  their  Adulleratttin^t^OI,  r»-i. 
■■DraKA**  ht  wlieat  flour,  W^,Ji^.,  39S.     An 

Inxredlcot  of  Whanon'i  ErvalritU,  S30. 
Di'TiH  Pma  in  tpa,  «7.  100. 
DvKs  usimI  Tor  colouring  teat,  U. 

Pa«  CocaLR  in  wboiit.  'H^.jlg,,  36S, 
>:urLLio9corif,  or  ebullition  nicoliilometer.  B3-I. 
Euiea,  Ivaf  of,  in  irHfJIg-,  *>8.     Hldvi^rry  ci>- 

hmrinp  tri  ptjrl  mIiif,  MH. 
Klh,  leaf  ur.  In  lea./f-.  *9  i  In  tobacco,  fmti. 
Enoive,  Wtld,    130.     {Set  Cliioory.)      Hnilirp 

In  tobacco.  ASH. 
ENoKAi'Llt    Bhchabicoluk.  the  Uw  •niUarj, 

Kl•l>l^o  BCTTEi,  Iftivr  on  maaufactore  of  fftc- 

lillutJt.  'Ml. 
Hrvalkkta,    WhAftoD't.    roTPpoiition  or,  390, 

fifi-.  ZAt.    Kecelpit  for  making.  331,  332. 
Ervil,  nr  baitard  Icottl,  flour  ol.  tii  opium.  GM>, 

yv.,  (>5l. 
"  KaABttco,"  liijurioui  and  polfonoui,  Hi<rd  In 

i1ii*oiiriin(  coi«rci:ii(Miorr,  A^. 
Kksk.hiia  Ui>a  ill  [turtcr,  M)D. 
KtiCK'tiA  ^tM•^TA.  449. 
E»ri»B,  taefficl«i)cy  of,  S3— 36.    tlluttntlotil  oT, 

in  llir  CAsoQf  iPa,l(M;  cblcory,  KStandnofr  ; 

oiM-oa.  190;  p(-pprr,  3AS  ;  vlnvgar.  4<M;  laalt 

and  hon>.   515  [  gin.  .'ai  -,  brandy,  044— M6; 

wiiir.  MiS  i  tobacto,  614. 
KxocuNitm  ft  aoA,  or  true  JaUp.  6%. 

Fabi*  Ah*ii«.    Ste  Strychnine. 

Favtitiuus  Saou,  325;  priipcrenmt,S6S  ;  nut> 

inrgt,  441  i  port  w  Inc.  V)0  ;  tcAmmony.  CM).     , 
FAKtKACBiHW      FOOUM,     SSi.       CotDpOlltlon     Of 

l^ardliier**     AliiiinntaTy     Preparation.     JXX; 

l^dih'A    Allmnttarv    Carina,   333,  ^f..    334; 

t»miullnn,  .13:1 :  Eliitl(irk'»  SpmoU.  ^-M  ;  Trlnce 

Arlbur'»  ai<d   fnticp  uf  Wuin'k   Ftiud*.  334 ; 

llarflt'  KarinacruiK  Klonr,  MAldnmn'*  NuTn- 
;    iliMii     FArlna.   Brwlrti't    Farinacrout    Fimh), 

Ittuttr'i  Soojle  and  C'^mpoundrd   Farlnii.  and 

JuCMt'k  Patent  Fluur,334  ;  Plurabcft'  Improvrd 


FarlnMeous  FmmI,  and  PdMTtl 

.tS.V      Drtrctryn  ul  tb*ir 
FkUPaH  In  Cfi.  99. 
FiaLtiNtUL,    >trui-tur«    of. 

(AriCurrr  Ti'viIptJ      UwOftDI 

47'J.     llec<r>pt  r»r  in«klBx< 

pawdnr,  &HM. 
FcaME'iTtM    (KAVIflAI.  MX. 

Fmiii.  wo.)dy.  In  tu^r.,^.,  W; 
111  kAiicrs,  430-     in  Anuff.  A|3i  i 

In  Jrtlap,  r.ti3  ;    in  kfwcMMttu 

quofirf,  6*7. 
•*  FiNrvo*  "  ol  jMirlpr.  VK. 

Fiji.  rr«|fmrnl  of  •' ^- '-^brti 

Fuoin*.  com-c.  >i«<J 

Ftovt  on  Oil.  > 

of  OoUTt  U*«ll   I  i 

apKicA  oC,  n¥. 
tor  of  fvouBd 

ffliiten.  Ttrt*Xt\': 
alboinrn,  vns-  ■ 
water,  and  Aal-' 
of,  by  D<inia»  I '  >  ij, 

Md.  .Slrnr^nrrot  ihe  jijriin  of  < 
342,:t43.  Starch^mntjlf^oC.  it>i 
Jif,,  2A6.  BlRLIiV,  •.■*or..I 
tlUtHicai conrpoatttoti  ■■'■ 
than  ttbeai,  *i4S.  A.- 
«'»./ir*..  244.  ?4.>.  I; 
conitltufntt.anU  itrurturc  7it^jl^ 
U«hI  aa  aq  adtilteraiit  of  ccMbC* 
ipnir*  of.  V4(.  Ir*  *nlii»  a*  as  dtM 
24*1.     SlntctUfr>''*-       -'  -'   '^  J 

a4'J.  2M.  (.V.'i'.  «] 

HItur-niA  And  ^: '  .-^l 

Com|K>tltiOD  of     1!  .  (f 

grain.   2^  fig*-,    ^--i  ^ 

opinion  ai  to  Tea  Tio»>.  .  -^ 

prnpwtin.  IWi.     M    r      ■      .    X 

potitloti  or  the rhitrf  crtt:^  rramA.S 
iMtor  Jahn*ton'i  analt  •*>«,  Mg,  ^ 
tinn  of  ihr  ■Idlrii  nf  wh 
thr  CURIpOtltl'Kl  of  Whc^t 

cnrr**i 

jf^lhfcf 
for  di-icmiliiliifi  ihe  ph< 
in  dilTcrcitt    corn*.    'lY*. 
CuitAL  Crauu,  UAO.     K 
Bunt,  tmiit  ImiIIa.  or   pvp|>nj 
a»  tf,   l>ii»t  brand,  'JMJ.^..  " 
rBd-roblii,  n*d-|tiini,   MSO. 
3ff4,    tjf>:i.     I'ruli-illuni    glar 
drvUlM,  Ac,    »?■      Brai 
dAHi*'!.  :f63.^..-J'r7.   FuriKMil 
In  Atalc  bnudj^., 'JW^. 
or  pcpprrcofn,  vS&.ji}.- 
S67,     AraruA  Fariac.  ' 
3GB.  U70.     MAM;rACTr<  i 
•nuV  or    frnnenl^d.    tfW,        1 
pllJlt,a  lUii^U*. '2fiV:/i)r  .  371  .  -IM 
ui<*d   in  hrt'iKl   niitkii^,    i/jn 
potter,  tinall  U\  < 
DlK>itfry  of  d's  |,| 


licnii  mrAl,  f  K-«*,  barley,  ry*.  |r 
poUto  flottrt.  '/7ft:    wilh  a  _^ 

termed  Uaii.  ibc  RMyor  of  Cofi 


Tabit*   rcpTr««ntUiv   the   ti 
thcAti)  of^lhv  chief  cvfr.il  gi 


]XDKX. 


703 


f76:  Mlih  alum,  intnrni  vhtttr. 
C*>ni|«li  vltj:  274.  Adull^ral>»n* 
»r. *m.  Jim.,  tf 0.  arnttU  ^  Etvm. 
n^oMmplctorronn  fluur.lT?.  STi. 
■)■  uf  hrrod  :  wl(li  Alum  atidtklt. 
fftkrrs  "barili"  ftnd  "ituff,"  and 

BTl.     ';«l        I>OtitlTff    «t1ll     nrgRllTC 

Bg  tli«r«rroad,  tMt.  Wbitrnpia  no 
br  th»  |r4*nuliimriift  ftf  Irrail,  VRlt. 
|w>  oil   Ihr  u**  I't  Ilium  tti  brvail, 

Kktymrtit  tlrfrnilrd  bjr  i  thrmkol 
Lftifp  profxtrtlKD  III  iirillniry 
Adullrmlion  of.  with  Witrr. botic 
\oa*  due,  2^) ;  ahlt^  I'lty,  CNr* 
|Dda«Dd  aiajmuU.  chiik.  gti^oni, 
Votcopf^r.VK.  Hr*iiUM  iif  Btam. 
Mftit  Munplm  of  brmd.  »0.  >horI 
|T«Ji-Dt  tD  Londnft,  tM ;  ru«rd«d 
Ibi-  EdtiilHirih  PoIlc«  *«,  >f«fi. 
1^  /Ar  advUtraUonu  i>f  Bour  and 
'  Organte:  bmi  eour  aiid  iiHrrh, 
IT,  WN  :  twrlrv  Hour.  SM  :  riet.JIg., 
k»9./(r..  »];  '•durra."  vet.fyr^ 
mK.  290.  tmorgantr  :  wu^,  v9l : 
U*  ur  Irtra  alba.  Ctilnaor  Comlth 

Rboiiatr  of  nafTDCtU.  TH  ;  alitm. 
>  f»f  copper,  Wft.  I)«ty  on  B'trr 
Wd  qutnllllt^  nttrrcd  for  bumr 
%\n  |H%4— ItitM,  19fl. 
IT»atl»p,  for  iiiic({i«ropf«  (.bjrrli, 
ff«rlr>flon'«,  ait4  tioMb;'*.  63. 
hlKkclt'i,  M. 

Iir'*(*t  of  artlriM  of,  M. 

k^,  or  Mupaton^,  in  fa,  i7.  101. 
I^Arttrte  In  •■  lloiurbAM  Hnrd*" 
IplnjtnrnI  (if.  t«T . 

EKTAktU.  f'  I  .1.409. 

il.  of  Thlri\  .    <m. 

an  and    iro-i  '  i  i"  ;    In 

«en|i|ri,  aDd  ullv.'.  41 ;  ;  cam- 
^•ni'r  u(.  In  curr«itU.  rx*pb«rM«^ 

V,    V  g,tn.     D*^ 

'•[   brrl  rrH>t 
1.  ..!..  4I».     ZV- 

iijili  I     in    |«jiiiiii'ii   iiiiU   n«l,   41i, 
loruh.  lU. 
[TH  ill  tobncco,  MS. 
|ar,    1<U.  /^..   IM  ;    in  brrul.  /«., 
HflHc.J!/  ,S76 

I  raw  )|»ttlli.  Dr.  fru'i  rpmarkt 
^.  Tajlur')  sUvrtnciit  rcaprcUnf 

^Croaod,  In  inuB;  CD. 

fec«Itc»Ima^  of  M,   Dlnunjun, 
,»11.«— i.-i,  ^r-.  2.3. 
iM>rf>t-tlt>nrrv,  4M.  i'j6. 
MiOA,  UM'd  lu  adullrralp  Im.  OK, 
I 

^wmtUe  of  mlcrotcopjc  nbjwu. 
bail  adiillrr-jnl  of,  and  'tfirn  :••  ■ 
iiirglwt.  lyt,  P)fr»rMt<r* 
itotj  tKffii,  _/fjr  .  ICA 
war 


It*   u«p  hi 
i»oi  mT.  With 
4A».  <;rl«Une  i 


«KhM  of 

*6.*. 

I  "m't 

lie  t%t 


cnrnAM  in  portn.  sdij  -.    powdmd  In 

fill      lUc^pt  for  makuii 
(Miwilrr.  Ot^ 

GiitK  til  (.'plum,  €3$- 

Gil,  manuEartan*  of,  tn  Htdland  am)  Briuto, 
ftH.  AS&.  Lift  <^f  subattiucrs  rnlrfili|[  toil 
"gin  fl4*ourii>i:.''  nn*.  At>i  ltkration*  of, 
wiih  HXcr,  atom,  •iitx-»T*wT-i«(r  cf  fyntaab, 
acttau  of  iMd,  md  •«  1  '  *n\% 

■nipr,   OaywuM',  and  -i>, 

&36.    Two  rwedpift  i'  .  m 

fiatourtnf ,  4tis.    Mr  .^  "* 

rcdurinf  ut»«ertri»  ii  :<( 

and  t«c«t*aln|[  Briii  <   >- 

lK>nable   adTlov   tu    <<  ; 
JUwniU  of  AuaL  of    I 

Sii,&M).     &oIpluil"  "f 
I  rair  iplriU.  Dr.   I  < 
tog,  &31,   »1      IV.     1 
Ita   Uupifyhii;     rflWt> 
i^f    tfdtilcrrw/idiu    of    . 

Indirect  mtxhod,  bi  ntunaiwit;  {rr'^xn.^m  iii 
alnluilfUa.  litatrumMiU  «tn|ilt>)«i] :  %ji,0m't 
EhXl  'tar  t.K>i.tr'(  r«nt*ttailA 
<  «r  HiulU- 

Ikn  a>coliolon'i  iitona  of. 

Ml;  SllbamaiM. 
rail  fpKiSC  fr<<IM  OCMfIr   <-«> 

trtealubl«o«Tr«llM.M(k    IMrcctapUiDdi  t^ 


■hv 

for,  107  •.  I«i  f 
icmlnbif  «■<- 
«f  ca^lrasi,  * 
fli«4  Krt4  tu) 

MMta.  M»i    or 

filci  cm«d  Air  • 

duty  Ml  gin  1 1 
land.  MO.     Q„ 
In  Ihr  I'fltfs) 
In  IBM— 1^^: 
•*r,in   Ki-*v.     1.1, 

CiDKfKK.   In     :.]:    i 

and  in'>ri.  ■  '  i  - 
drl*rviir.i-iL<  I  . 
ftcMuf.  MM.  !'■ 
4SS.  JifrMriw' 
4M.4V.     Aim  I 


(  fin,  tha  karna  tM| 

.AM.    Uructtoa 
"IIm.  afid  uCh»r 


!'•.      Kttif'i*    (Ifk^llj.llfNi 


'.    MBMft- 


tu. 

,iij»7. 


Quwots  or  frai  i  •««■  IM 

tko  daNcttM  "' 
nLtrmi  tn  lea,  74 . 

ffi.iraiit'^a,    Ita    uaa  ts  a  (•(i.M.(»>(i»ti,  M|    Ml 

liutlrr.  7M. 
Clii  vK»uit.A    GLaaa*.    f<71' i    itMiitUal    »imi 

•litiirnli  lit.  IMK 
Uuoftiafcaaiu.  Iio^  )««.  4l«j  I  liMfit(«|liK  UlUil 

rut  '•■!»  filfl*-*'*.!  fr  im    -rWi 

r.... 

tin- 

OlaiM,  I. 

r^Baiaa  "f 
nsavu.  Ik 
iSaMiaO*' 

'■OotWi- 


ii    iiifti  lit  lb« 
'tiDwti',  itiiKlH*'**  (lf|  II 
~.  •  I  HffUmimt    *•*•> 
<  in 


f(M 


INDEX. 


GKiHrronirt  Btb  Skcpv.    Stv  SouflT,  610' 

GsukTi.  347. 

0<-4(4(r(M   III  tcamcnonjr,  6M;    Ln  JtUp,  6G4. 

Jit.,CSJ. 
Gi'M  In  t««,  Cl>:    (It  tiiitar.  IW;    tngnuDlh,  Is 

milk,  331  t  RUin  In  porter,  Mtf ;  trniRCJuitli  In 

ti'Mtninoajt  050. 
GVMl'M  to  tea,  81 1    in  polled  mcAU  «n«l  flilt, 

S4I ;    In  nutUrd.  34B :    lu    rrpprr.  JH>i ;    In 

ccafedlonnry,  *7i ;  lo  |H)rt  wiiir.  6*tt. 

IIax,  potted.  343. 

Hambrp'  Fowuer  In  rhkorf,  141> 

'' VlAnnLiKr«"  tuxu.  ISS. 

"  Hanih  "     Sf*  TOIMCCO,  Ml. 

•■H«m>»,"  Wl. 

H4WTHUBN,  lr»f  oT,  In  tea,  iVr-)  6S. 

Hav  In  cl)tar».  «M. 

"  llttniMfi  "  topfirter,  MO. 

"  HsAiw."    Set  Tobneco.  MI. 

Hmr.  Indian,  Julrr  <ir,'in  o(>iuiii,  fiSK. 

HoCRUBIMBB.    Sfr  wine.  S-Vi. 

•*  HoLLAMIM."     A*v  Butirr,  W*  ;  Gin.  AW- 

HoNBT.  rofiktilutioii  i'(,  Vi.  How  pruducfd, 
19(1,  IW.  CimitKUcnIl  ju>d  prui-^rtifn  of,  \'M. 
PmfHirtlon  of  Milld  -iiiit  ll<i<ttd  tiijcar  in,  IMi. 
Folaououi  lionrjr  d*'*'""'*  ir.in  o.p  Duwerk  of 
tharhododeudron -k  iw     Cry* 

tall  of  booey  with  «  >  n  franiifri, 

JIgM.,  WO,  101.     \Jii'.-  . .  1  himry  dli. 

ting'tUhnt  lij'  th<<  iMillt  n,  .ixi.  Anisxing  iiKt<it< 
Crynrttpriiit  iticollixtiiiti. tUKtuncr fit,  2fH.Wt. 
AMIkxIi  M  otitalnlDK  tl***  fallen  for  micro- 
•oopical  jntrpotet,  3tlV.  AiirLT&R«Titm«  n|,w)th 
jwtaio  md  wtMMt  ktiirrlirt,  w-tili  itarch  Mid 
caue  cugan,  rhalk,  |iU>lrr  of  Pam,  jind  ptnr 
rlny.  'JOt.  Ih-itftivn  qf  adttllcritiumt .  Wit  i 
With  cjne  mitar.  »►<,/(»..  J"3  j  »ilh  grape 
auftar,  :fit4;  br  the  (i'^^'^*'^  "f  ^\^'  BW>(. 
IVllgiut,  and  Pajrefl,  3M.     Hon<-y  In  lolwcco, 

Ilurs.  rarr  nt^ceuary  tn  prrpartnt,  &00.  Gfeat 
«-ariall«n  tn  rrop*,  i*ri.  LUbtlltj-  of,  lo  In* 
Jury  fnjfn  fli(*«,  mf^iiM,  «nil  rtitt.  AiG  I*ro> 
fvu  of  pir|<d"itinn  Mloiilrd  in  En)|l>ind 
and  Brislum,  h<iS,  In  UavariH.  &04.  Stmt- 
turr  of  Iraf,  glaiid*.  atid  seed,  flgt.,  MH. 
MA.  Rxi'-nirvi'  idull^railun  of,  Ml.  Iff. 
tvflion  o\,  514.  RiclM'  duf>  on  humr  (ruwii 
ho|-ft,  Cn*tf>n<a*  du(v  on  torelitn  hu|M,  atul 
qiiantltm  tliat  pntrl  tjirlM-  itutjr  and  wrrr  rr. 
tali>i-d  for  huine  coii>unip(l(.>N  in  IH\^18&&, 
&ir>.     Sre  I'orler. 

tfiiaotiiit,  yifi. 

lIuiiuKi'M  Dl:kTKHO>(.  t<JL 

lIuaiK  I'liikfovr.  leaf  of.  \n  tra,  91. 

i1)iK<trLa-it  Mddr<l  m  |>oit«d  mrats,  MU^afM, 
iH^loiiir*,  Ac-  Mr.  It'cliaidMii)'^  «tldriic«  r»- 

lliiiMttt*  tff  c<jW«,  Mr.   Run'*  rvmarha  upon, 

■iHi. 
llYiiuoMiTva.  rrMnmnn, 'ill*.  Jig..  :tSl)  Syh.*-*'*, 

lor  rttimaltnit  nlrahul,  &X>. 

Im...*.  (.,.,%  >iv.  .•i.vftiiirnManU  HrudnrrjI^s.. 

-«mI  111  4«liilt«Tat«  O'lm 

I  ■•m\,a*K.>,    li4|UQnce.  GH7. 

■■       1, 

iMMtin  in  (ra,  HI.  itj.  'JH;  laconrKUonrrj-,  ^MA. 
iMramrtXTion.  GeueraJ,    1 — 41.      'iMUnMMi|    of 


leocr  of  •diillctatloft.  4.    Ol 

Uon  to  Incrraa^  btilk.  impfiH 

part  Itatotir    4    to    <')*Mita4 

drlecie<!  •      -    " 

II.    Ll>t 

be  uarti  '  og^  1^ 

BtatMl  (..    ,-.    .wTlori 

th<;  uA^of  whicii  t.u  poatUm 
adduced,  lU     l.i.t  «<  arucVni 

l)>«-r-Ili|'I>i»  IIK  :m    .   t    ahw-htal 
h' 

h. 

If,, 

A' I  I   ^141 

«ilollrr;i(i(.n,  V'J        >Ufl||««Ual 
Rieritary  Cnnimittm  lor  tei  i 
preaciofi.  aa      UaettctracT  of 
Li*t    of  (hf!    gvfitUvMV 
mroury      Coii.mlClaa     «• 
Ontttt'dt  nn  wlilvli  aflk*^f< 

r«-'' '■    *-  - *-'  —    41. 

loi 
Iri' 


fiTii.  1.7."       c— -■ 
Bdi'lioix'*  Hr>4>' 
Uilr(*.thie«  »... 
G;s.f.7X  Am  I  .  . 
t-tlMlk.    WlliNit     I 
n(>rc.  (,71      IVu. 
drug  grtDderm.  rr.l    /if^..  r»^^, 
rt7V 
iao^r,  •iilpl'iire  w^f    tn  tea.  •? 


lAtt>>  !.•*■ 


>1  Co  A. 


J.; 
>. 

lit  .li' 

Ibr     - 


INDEX. 


Ivnlort.GbS:  r»  IdcDC*  of  Dr.Tl)or»«m  rrtpecT- 

fi'A  hftfch'tm  nf  aduUnatiofU  of  Jalap 
Kh  tnal'-  J<iU|>,  fi'V** ;  with  Ji(la[»  ((•ilkt  and 
riiiKl  i'llnp,  liofi.  VarlMliiiH  In  qiunlli; 
nl  rc*Ui  ii>  lUlfrrriit  lubrrt,  VJfAx  Dftettlun  of 
llfiriiitii  >it#,  iir  piiHUu'um.  in  \%\i\>.  Jif.,f'*tt 
1'Mwdi'tt-il  i^lap  u-iil  ,<*  :in  NtluItt'rAtit  of  vom- 
lioutul  i<-»<iimi  ny  puMilor,  tW'J. 

iniiv  S4MM«i-  ttii|i)i>)'nll»fl<lultirrAl«lea,SA. 
JkacriCA  "  H)  itort  win-.  M". 
<Ml*M»l«bia'*Kii.     $rr  W|ur,  5&C. 
JrwrBM"  in  chc«*c.  491. 
VKirKR.     Jirv  C>ili> 

iiKOHv,  ion. 

UiMAUM,  the  t«A  M  lUllvd,  9S. 

LAi-Tt>ME.TEK.  115,^.,  MC.  Experlnwati  with 
•In  larti  mrtrr*.  Vt'. 

Laci.  «:).rr,  M.  1>.  iinc'i,  til.  Jig.  MS.  Tultle 
n(  riclDit'M  nfintlh  a>  ilumu  I15,  Vi».  330.  It* 
itit|ic«lU)n>  tiut  nt-frttAnlv  corrrct,  230, 

LAlii>iit  liiittrr.  W7.  MX>.  l'ri>cri(  of  nmnufac- 
luriHK  \(ktA.  3ti|.  BriirtMinrt'*  pfOxliDAtennA- 
\\%\t  111  irrtli,  ;<0i.  Fxp»ttiiia  rountitp*,  ati:/. 
Ant  i.iF«ATioN«.  Mr  \Vliip)>l«>'t  rmtark*  c**n~ 
rFr<  hit,  ^H.  Mr.  talvcrt  on  Ami'ik^n  lArd, 
502  I^Tit  .tiJulifrjUnl  wtlh  fatty  matters. 
■tjirri),  jiluin,  (jukkllinr.  CiUlHiiiBtf^  of  notath 
unci  to<U,  puutoflotir  (/^x.,.Ki.^|,Rnd  Mil,  303. 
Rcntltt  vj  Ktam.  uf  uii«  hunilritl  uiDi(jle>, 
3(Kt.  A'luller*ti'>n  nf  Unl  oaly  proBtjililr 
«i«ti-r  rrruiii  r4n-un>»tii)rt-*.  J***.  Dr/rriMH 
»r  w  «trr  am)  itAicti.  3''1  ^  dllDcuUf  In  llir  cak> 
uf  kf'itrh.  3»^.  ^tci-  Dflf  inm^lkun  of  inltnc 
n-ii'trT'<  tT<  |^irH.3()A.  l><-tn'tlun  nr  iilidii,  *Atl, 
■>  •'.     Imporu  In  IliM  — H^iCi,  »r«, 

I.*  .iCCl>.  >1>, 

Lt  .   <•!,  In  tra.  87  ;  in  mufttmrd.^M; 

frO.  Ill  .i<Mi.(  |..,  471  ;  In  clie««)>,  4W ;  rh'omiie 
of.  In  omlertionrry.  4AA  ,  ml  aiiij  viblto.  In 
ditto,  4M0i  Bcvtal*  of.  Ill  Kill,  (V'iA;  in  ttnn. 
Ml  ;   in  i>-rl  «>ln<-.  MX  ;    !>•  ■tirrry.  -lU  ;  chin. 

maif  iiihI  oMitc  <i(,  in  iiuir  uw. 

Lli)«Tll.i,  vjriiiiH  Ktti<ii  of,  their  nxtpnilvt  rtn- 
plo^initmttn  riittnanoui  fiKxlt.SSJ)  t(tt*i..Jie»,, 
TKl  31):  b«*ur<].  in  K-ainnion>.  ^'.Jlg..  ^hl. 

]jlk  TlA,  a'lultfraliMn  Hf  tr-a  niih.  I'lul  di*rrl|»- 
lion  of.  77.  KnoriDutit  liil|[HirUtlua  qI.  79.  HI, 
Aft  7\17. 

].HiMiiM  Vn«.     See  Gutiaeam. 

LiMK,  MTlMinRte  nf,  in  iva.  n',  10I-,  lulphate  nf, 
90.  t.ini»  111  «»h  of  rtiffrr,  1tl7  ;  in  aitt  tif  rlil- 
Cory.  IM  ;  in  Lird,  3it3.  3(4i ;  xilfhate  and  L-iir- 
b<)iiAt«  !•(,  In  animtH).  it  8  ;  *ulphat«>  of,  in  con- 
ItK^liinrrf,  4»C:  In  tubacco,  SHa  ;  in  vnuff,  611-, 
in  iCdinmnnv,  dWi. 

LiMi*.     Sre  I  ruiU.  410.  416. 

LiMiniD  MKAk  tn  fftip^r,  3&t.  Struclare  of  Un- 
M^  tnoil.  ^6*,/^.,  3'-f> 

Liui^oKiea  tn  iMjrdr.  I('7  :  In  tobacco.  •'■M  ;  In 
DVtun),63U.  V4riiMi»d*icrlr'»1o'i»of  Ihiu-rk-r, 
6Ti».  «iinl;»r»  <if  (Mir  liiiDdrrd  luarli  nf  thp 
tttiii  u.K)t  Muil  01  til**  iindt-cnrtifAlc^  |«t«(*pr. 
tUti;  ni  ilif  itvcofttcatcil  powder,  691.  Sttitc- 
Imre  or  liaiiorm  n>of,  f>f(<,  >S^i.,  Ga2.  fKI,  CM. 
ADi'i.iKR«Tii>T<a  of,  wiih  HartHry  fum,  UH^. 
liituitM  iif  Anal,  of  Ihtilt-fuur  uii>plr«  of 
Ii4|u»rlrr,  iA^.  Adult'*rA<i^  wHh  canv  aiupir 
and  rirn  fluur,  CH.1 ;  with  hnrlry,  r}c,  md 
wheat  Bouri.  i^iUto  Maicli.  cluUi,  ud  c*t»> 
tine,  696.     HeimilB  ttf  B*am.  o(  Ten  anptei 


of  llaunrlcr  nlrati,  Wk  Adult«ru«l  with 
■larcli)'  ii'Aitur  UkI  ftvUthie.  GB7.  Rf*vlUi^ 
S*am.  of  rurmy-riwlit  Miiip'f-  of  llqnnrlcvJ 
putttUr,  6K7.  Adiiltrr:itrd  with  whfat.  Iiidiiui 
I'om,  po'Alu,  ami  tago  llcjuri,  wmKlj-  filiri?.  tur* 
mi<rlr,  Kut  India  arrowroot,  and  ronr  »a)tar, 
6»l7.  C«inpmind  iK>wdi'r».  rw:<'lpl»  U'r  ni«li- 
iuK.  CK)!.  /Vf/cfiOM  Qf  nduilrraiioitt  of  llquD* 
lire,  fi>'i  ;  wHh  whmt  llour,  chalk,  arroMr>iot. 
lurmitrtc,  and  cane  tfigm.  f-'i^i.  CuMiMnt* 
dtiiy,  iMut  And  |irr»eri(.  t>Di>.  Qtmntlt-fi  im- 
poi|r-it  and  i-nlcred  for  home  coiiiumpUon  to 
iKMaiid  I8S\'KN>. 

LliTTflf  druifk  and  thrlr  adoltcrMl'ini,  Cfil.  093. 

LlTVl.*H  pArEiu  iSre  Vinepar.  40(J.>  Lilmua  hi 
cnnlrctktnprv,  49A. 

LiVKAs.  bilked  bor»*^'  and  bultoiki',  UM»d  to 
Ailiiltrratc  cottrv,  lit. 

iMW^ThU;  i-tftcnrc  ol,  49IX. 

LocwuuDln  tva.  10V.  Inchtcory,  149 (  In  bocilcd 
rrtl  Iriiiii,  4l3iia|mrt  wtnc,  648 ;  lo  claret, 
t^i^  i  dvt*  in  ioii«ec<',  SW. 

LoLii'M  TKMui.Cf>TUM.  or  dnmrl.  169,/f .,  '.'tSi. 

hirny  fredf  tiiported  for  tbe  purpuiv  01  adults 
rating  coffee.  117- 

Uaci.  two  kind*  of.  trie  and  Mtr.  443.  Com* 
potiiunt  at,  accordii'K  tu  Mr.  N,  E.  Henry,  1 
44).  Stryetwrt  of.  441,  fia^  AM.  Ani'LTtKA- 
TtoMS  uf,  by  addiliott  ol  nitd  innrf,  44J-  iltm' 
ttdis  nf  E»aMi,  ot  Twrlte  laniiiUift,  441  Im- 
port I  uly  and  hoine  cuniumptluu  la  IS&4 — 
U'<6.  444. 

MAuaikA.    Sff  Win*.  1^. 

MA(inK«t4.  carb«nai«  of.  in  tea,  87.  101  ;  *lllrata 
uf.  litlRA,  lid.  Uag^itrslainaAhofroflrv, lliT;  m 
chl  ory  a^h,  IM  -,  *u1phati*  of.  In  lolMccOi  dW. 

Maowmmt  In  tiihaiTo,  hn'j, 

MAH'ti^NT  du*t  lhchlru?7.  14}. 

MAturoi  1m  conft-citoiierf.  49S. 

UaiXK.     .'hv  liuluin  Com,  and  Flour  ar>d  Brend. 

Malt,  r^ro  r«qalrM  lit  prrpnnriK.  and  nit^Kle 
of  prrjMrAlioti,  Mil,  WH  .S»vrr-1  (arirtin  of: 
p,ilt-  tuAlt,  anil  aiobi-i  nult,  .M«l  :  bro*n  or 
blown  mult,  and  pMtvul  mnlt,5>'9.  (Jm-itloii 
wtirilirr  Ibr  Mt|inr  >•(  inult  ■■  formrd  ai  the 
expruw  of  iliv  ■tarcb.  conilduration  uf.  by  Mr. 
Wr*n.  ao-i.  Ani.iTiia«noni«  itf.-Ml.  SI2  /)*- 
IctiWi  of.  h\b.  hvidrtK-r  ol  Mr.  Phillip*  «llh 
re(p4*rt  to  malt,  -'•1^  Earlte  duty  on,  j**H  jind 
preaent,  ■M^.  Qiutnliti'*  rplHlnnl  fin  home 
contuinption  III  Ibi'  V.  Kingdom  In  11163— IH.%, 
Al\     Pai«?  malt  In  ^hnrrr,  .V\3, 

M^Nuoij)  \>riixeLlnri>ffL-c,  Ul^JIga.,  IID,l36i 
tn  cliicory.  14f*. 

Manihot  nr  Taniora  Arrowroot  Av  Arrow- 
rnot,  313,  and  Tapioca. 

Marauta,  or  nVa  India  arrnwroDt,  174.^., 
314.     StT  Arrowroot. 

MAVNLa,  fvwdrrrd,  In  lugar.  IM. 

MAkQAHc  Acid  Id  butter,  tX. 

MaHHtLADt,  <iraiigr.4l6,/^..417. 

MawrtrNT.  Iiitulpliiitrt  of,  la  Cajrrnrw,  37t1. 

Nil  Hm»copk,  tbc,  >u  creal  um  in  the  detection 
of  MlulteTHtluii.  4n.  et  te^. 

MitMiB.  whcot,  S€7. 

MiLDsu  In  wheat.  •:f,\,Jigi.,  S64.  36». 

lUiLK.  It*  gTu«i  and  vdij  Kvucrsl  adulteration, 
20).  Ita  importAnce  «■  ati  arlklr  of  dirt,  ^s. 
ComfatitUm  ol  :  fklm-mllk,  butlrrmllk,  anil 
cream,  906;  Inilirr,  rurd*^od-wbey.  iiirtfm- 
cfaevK.uid ordinary cbttMe.KK^  ConaUtuiHi 


XX 


"06 


INDEX. 


i>rcow'«  milk  In  U»  nortn«l  it»tc  nreonlinp  !o 
MM.  O.  Hf'»rkpiin4  ChrMlit-r.Wfi.  H*-tm  of 
trti  aiuilrsfi  nf  piirr  milk  liy  I'ruf.  Ptigpidlf. 
SUC^  Moilra  ot  ratlntatlnK  the  qiiantttT  of 
tnicitr,  iUfiBr  or  milk,  b&Itt,  nnd  »n);-tr  lu  |C'<«xl 
milk,  007  ^  nr  (Kline  tiiatttrr  and  cn^ctn,  fiw  ; 
ol  augar  In  the  «hej-,  M.  I*oK}{ialf't  mwhM, 
aW.iKW.  Sprrllic  uravltj  of  mlK,  taWohow- 
imiTiiriatiimi*n,«fiil  U-  rrUtioti  to  fto|>oftl'.n 
of  crram,  'iW,  210.  Tablf  or.ti-nnity  nf  M-nrm 
JincI  jti  rcliillon  to  i|K^Qc  tcraviir,  310.  la- 
riJiJiotniw  comtKHttkin  or  in  ilk,  31 1.  Inflr)pnr« 
ol  ngf  Nitdnf  condition  on.  211,213.  iDlliiitirc 
ol  food  an,  21V.  Cnnatiiiirni*  of  milk  wht-n 
rnwi  fpil  on  Iw^l,  and  vhrn  on  rarrnct,  51?- 
VahmltHf  condition  of  Lundun  cowi,  913. 
Mr.  IlMrlvjr'i  rcmarka  on  •roUtnir  cons  wtlh 
hif  M-rrs'  and  dlitUlrra*  prftin*  and  «»a*h,  3f3. 
MM.  Boutilnvnull  and  Leb(^i'l  >*«]M*rtrnriiu. 
SIS.  liillurncL*  on  tnllk,  of  U''>'(irr.iltJr<>.  and 
of  lime  anil  frequency  oTmt.klnit.  313.  T«ble 
thnwlnji  dillvrence  in  quality  uf  Brit  and  la^t 
milk  obtoiDcd  at  each  nillkidf,  ^14.  Table 
allowing  spM.  grav.  of  pure  mnniliiit  and  aftm* 
nitOD  mUk,  and  pcr^cistiinfttn  ol  rrram.  tmm 
Hlchmond  and  London  cowi,  21  is.  Iteiulti 
dnluewd  from  the  tablci.  !t1&  HouiIhk  uf 
rowi,  Mr.  Rujtb'b  reroarkt  upon,  'iUi.  Ctalcu* 
latlon  t>y  l>f.  Tlioni*on  of  iIm?  Amount  of  purt 
air  ]M'r  dtt-m  nrceiiary  for  one  ci»w,  717. 
Vharatlfriitic*  o[  good  milk,  ^  .  J17.  tlHi 
poor  oiilli,/^.,319;crrHm,2t«./l(l{..SI9;  cord. 
^\^,fig..'ti(\;  colfritrmn,  511.  iVi,  fig.,  121. 
Av;>arnlu«  f-ir  drtermlnlnic  purity  and  quality 
of  milk  :  >pcrlllc  ymyUy  bottip  and  common 
hfdromrler.  St9.  jl^.,  SSS ,  M.  DbiDCiHirl'a 
cen(e«lmal  v4liictoinet>>f,  de«cr1p(lon  of,  31'J— 
^Cta^  ftg.,  vSk-,  drn«im«-trr  of  M.  Collardr*n, 
Yt%.  Mrlhmla  of  dftcrmining  the  TBOtn, 
*25;  the  lartoweter,  'n\  flg.,  2W.  Rxp«>rt. 
nientl  wilh  »lx  Inrt'metrr*.  2V7.  M.  Dmmt'i 
t«etOM!ni>e,  with  dlriH-tiont  for  Its  HpvltcitMon, 
M7.  fig.,  »«.  TBblp  of  rirl.n.-**  <i  dtfTi'Teot 
kindi  ul  milk  at  shown  on  tne  Urtiftropi-.  Xfil, 
a-m.  Probabk''  fHllnry  I'f  It*  liidkatloiit,  »». 
Ai>t'LTERftTtnN«  of  milk  «lth  water.  irrKl*. 
ult,  aoiiattn,  cerobrMi  mnut-r,  March,  tnr- 
Bierlc,  gum  tr<ixacAnth,  rarbtiitAtn  of  tirda,  and 
KUm,  191  ;  with  drrocllou  uf  botlrd  wliltr  car- 
roct,  mi,  motf.  Abairactioa  of  tlir  crmtm, 
JXi.  Proportion  of  milk,  wcrr  it  aupfillod 
IfDUinr,  to  f>jich  1ndlridii;il  tn  London.  232. 
lUtulU  i^  Eeam.  of  T»pnly>*li  »ainple«  of 
Ixindon  milk,  ^i.  tlrt^rhnm  tf  adatttrtUiami 
with  watiT,  hy  ip«T  praT.  t«*»t  of  mOre  milk, 
'  Imraed  milk,  and  Mrruni.  233.  'Af.  TtMc  of 
drattty  of  ihi-  icrum,  :t34.  Dcl<^  ion  of  luf  ar. 
30I  i  of  cane  *U)nr  rr  dt-CMCtion  of  carroi*, 
04 :  of  *rarch.  jtiim  «r.ibfc  and  gum  rran- 
cantli,  and  cerrbml  mi»tti-»  ipf^..  iafll.  rli«lk, 
■ait,  and  annalto,  'IZS  ;  of  tinm'Ttr.  %Vi,  8ln- 
tlnilcB  tif  milk,  mohidinp  cht*f«'',  hnlteT,  *r., 
ronauned  annually  in  the  l^.  Kingdom,  '<a6. 
DdatU  of  its  coal  aril  cnn\r)'Rm-«*  lo  lunidon, 
'OHm     Annalto  ijted  ti>  colour,  I7:t. 

MotAMEi  (»*r  .*Huar) ;  m  brniHljr,  M3. 

MiMELLL     .^1-  Wine.  Jttfi. 

Mould  in  hopi.  K03. 

MowiiA  flower*,  powdered,  In  opium,  638. 

"  Mi'LTim,"  M». 

Mtait,  Ma, 

JdL-tTasD.  two  apedr*  of,  Skiapla  olln  and  nfffni. 


dilTereacea  In,  M4.     nut.*—  nf  ka 
lure  di'irrlbvil.   M4.       C^m^mamm  «l 
iDuaLatd    tfMKl.    Pviwlr^'a    rrwaart^ 
X44  :  ol  wliltr.  S4».     Htrm£t»»r  0 


Urd  •«• 
fit'  .  '■ 
wtl- 

jell..-  .■ 

XMiU     i\J 


I     Mfc     figT  ,    M'l.    M7 


7& 


............. ,.^  ^llM^M     ^ 

t:tamt.  nr  Ki>n*«i««  tcnfli*,  IK 
^dtiUuralioni  with  vtilpfMf*  «f  ••*.  |m^, 
potato  itarcti.  and  itc«,  Mram.  WaTwM 
and  Uay'a  gridanga  conc**i>*m.  »#.M*  w 

qualities  of  mnatanl.  **  SMqaia,"  "  tm^ 
"  Sii|irrriTir  ''  nod  -'l>ou*<le  *>a|i^ftB«.~  ■•• 
thd'  '  --niibtrl  Tr  W 

niai  !.,  Jti.     Jh^ 

tio;  .  '  -a»or.>l.Bai 

with  ••)<  •  »Ni.  vOk  rwvwal 

1^^.  A'-  -tn  ci^  arf 

4.V>i  Mtth  \ 

3.V;.     Duti     ATi.l   qiiaii|4lM» 
tallied  for  home  eaBMMi|iCMa  li 
^bf^,     Mtiatard  huaH  MiMM«r, 
finin,  »n  ;  lu  ginger,  49*  t  •■  p 
t|rlre   459. 

MtatvTK''*,  lhre«t  «p*«-|f^  of,  4tM. 

Mymocvmi.     Hix  Aiuslasd. 

KkPiia  Vklluw  In  miiriifli— j 

Nl<OTl*?ij«.  drrlratiDn  of  llM  fwa 

NicuTlkNiiw.^H. 

NiTBk  Id  totui«n.  Sfl9l. 

NtrTWlc«,    dr><Ti|>lJOU  nf, 
true  or  female,  and  «Htl  ori 
nf  cropa  and  mcde  «f  (Mtb^Wf,  aA    Cik^ 
llaUilily    tn    attack*    of     uul 
Ciim^iti' ity*t    nt .   fl\c^  cod 
nn*tre'<    anatyala.  tl9.     db-«rAvTa(Jk» ' 
AntTTt  RtTi«iv<    nf,    Mitk    wtM  fliri  lk% 
niitrr.  ''  ierMrta  aC,  Ml.   laMKt 

or.  *uimiifc»iaiii||    iw^i 

ant     ii'iTiir     moi, 

A16, 


Oak.  1'-'    '■■ 

MA 

Oat  I  < 
Uatm&ai..    it 
prnpertlea.    arr 


roA     II. 


t:'-Mt^«wMkr<«i, 

Fl*Hjr  iai4  BirwMi 


AtiaJy****    '-■f    ITi-'.'*t< 
Meaar*.  .V    1 
of.  Wi7. 

Anrniit'  ■ 

win 
aiiil 
Cfv- 
mr«l    Mi;.  ., 

tmtiii>n  •  ■■ 
arw.  Imi . 
food.  ai^. 

Tooting  » 

lllfl'*  Alld  ■ 

rice,    and    ::-i_:. ,    _i..       .,~,_Hi    -^ 
QtianlUiM  tMaiMripd  te  i«M— 4»Mk  Uft 
maal  la  eottaa.  MH 
Oena«,r«d.tiic«M*.  feVt  r^Ov* 
aw;  fwl.  In  C«}««»ff*,  »r»j 
nirttc.  VM;  III  lobacco,  US; 

■HUff.  tiML 


lM«t«7     1-rrtA*"^ 
>•»      liaf  ^^H 

w«wl  ■•  a* 


INDEX. 


707 


.N«  ui«d  to  ftduU«r«l«  tat,  GA. 

tor.  .V>7.  8)>ttrr«  •ntl  v^ri-tir*  of 
<-niiiitrk«  whrrc  e«i)Ur*lnl.  6H. 
if  tlif    p'»i'pf    l*40*iiIp,   GJ4,  Jtg»., 

r,    ftA.  ("ivn.    ro/Zr^riiM  or  t<|.(iirii. 

lUiMruliiK  ihu  uriirtiiri*  of  IIik 
I  CMb  AmiiLftct  uf  rt}jliiia :  lij- 
aiiym*.  Oft  Iv  S4<h>n<ti«-r.  '>r 
■iUnttnnftU,  «nd  ffffixun.  fiSi  ; 
r  nrlrttttti  ftlMl  tili1<|K?nou>,  'itV. 
T;  SmTrnA,  Tufk»-f,  or  Lfftant, 
Mitlnopli*.  Ksiyp  ioa,  Trrhtintul, 
~  B'*nf ill,  n<'Q>r*-4,  FAlna.  M4I. 
eh.ri3<i.  KaiKlrtiii.tkir :  Kitaiuti. 
1  G«ritiiui.  diSU  Ant-i.rKiiATioM* 
Kh  |ioppi-  c^ikiiIp.  mud,  lanJ, 
I4re«>«l.  MKit.  rnwilims.  lour,  |mi* 
ctioo.  KO'ir,  tlt«  tnipu»-it«it  jtitrttt 
y  Msr.  tub4cco  plant.  utH  IntlUn 
Wlim«rlnkl  «nd  B*'-)  (tuU.  cm- 


niraui')i[  upon  tlH<  xluUiratinn  nf 
I.  blflrrrnt  itrenftht  nf  grfituUic 
iiml  hr  mriniti  Knalyiu,  lift.  Mi. 
»  renurk*  iipoo  i»oi«ltirc  In  opium, 
itiMof"  ■Miutront"  and  "powder 
^416.  Sitniptr*  uf  onixtn  mIiiU 
poprr  CApiiil"  411)1  whrAl  R"ur, 
it       S^inptt-   »f    KtffpltMl   <H>tutn 

vMh  ffutn,  woody  Abra.  utdwhtM 
D*ttetim   9f  mntiura$imm$,  M7> 
If.  Mid  •  MiMUlM   MCjUiwil    for 
ipclMi  tolBM-ISAe.  M7. 
4Ltll«.  4l(,J|f,,41T. 

ric*.  au. 

l-i    mirvnaUde,    4I>,  jtiff.,    4|i  t 

nuir,  fvyj. 

I  Btoil  to  riiojver  MUf  be«r,  AQO 

Obkira.  <M 

nt  of.    An*  CirtUmiim . 
>f.  Inl|-<ftry.  ami. 

;u  A^TiHir  rhee»«',  4711. 

jnl,  m  c>nfl»<*.  1 3ft ;  la  chlcorjr,  140, 

,  Juie*  of,  Ih  e|4u«i,  6M, 

I    Ma 

AtrCDIi.  »».  4Wk 

>a*lv(t*«  of.  ttirlr  variou*  u»v*, 
qrkft  an  tlir  croHlh  nf 
"I   \Uf    in>-l*  rtf    rf..ii.  f  ■.>»    II..' 

HUrk     |>rpptr 

Itim?   Lln«U  nf  — 

,  ■ml    I'liitluh  }>i 
(TjpBpfHT   1.*.     A- 
d,l'^H.    l>M«-ripti'    < 
inr  of  tbe  b#rn-  x^^.  JV'*  ^U^'- 
-lA.    Dif. 


of  ground  t^VV^f^Ai- 


frr«tic«a  obt#rr«bl«  la  the  partlclM  of  Mack 
nnA  irhlU.  yVI.  3M.  ffnai/li  1^  KMam.  of 
Flirt  J- til  rw!  utnplfa-  ar>4.  Aut>tilJlATlofi>  of 
|>vpp«r  with  lint^ihl  xnvaX.  muttard  hutk, 
wlii<*t  lltiiir,  |>4-4  flottr,  ug<).  rit'e  flour,  pt<p|HT 
dusc.  and  wiMMtf  Q)iro.  'JfA.  EviUrncv  of 
M«»«r*.  Plilillp*  4IhI  Cvf  upon  tha  diseoTaif, 
in  addlltoa  lo  thff  Utt-^uoknt  ■iitiktanm,  of 
potiitn  tiarcti,  ChtiU,  (•ran,  ground  grpiun* 
ra^  mmI,  aiiiJ  buiii^  tlutl.  lti&.  ArttAcIal  pap. 
parcoTDt.  c<tir>i>o«ili'>n  of,  365.  IMecthm  ^ 
orfkattrrffftrm*.  wirli  the  klarrbptofwbm,  rlcv, 
prtiaio.  aiMl  I'tc  >,  with  miutjinJ  and  rap«  »Md, 
CayvDiifl,  and  ffjpiiim,  Ji'A.  Strurtura  nf  Itn- 
k*^  ror«l,  3fi5,  ##■.  Strf*-  Stntdura  of  pftn 
dour.  S*!?.  Ilftfctioa  of  pt'yjfMT  liu*ka,  IaT' 
Itlioua  pritpt^r  Urrri>i,  and  hone  diitt,  MT. 
Duty,  and  quaullttr*  Miti^rt^  Tor  bonto  cuu- 
•aiDption  lit  l-i^^-l— IM6.  3ti7. 

PiKllMX  Dacti  LiVBia.  ntia 

pHoaVMORic  Acid  to  oofTtfcaib.  107j  la  rblcory 
a«b.  134. 

Pickup   "  gr»eD*i»jr "    i>f.   Accom'*   rvmarki 

t<.   rm\ik  Inn  to.    4(t5.       Kaial  r<r«ult   of  Mlhlg 

,.,.  I'-  -  t...r....    ,.  ,fy-.1  «ii|,  cnpp«r,  4Qfi.  ktod^n 

>pl<-*,   4'>ri.     iitlecliuH  nf 
.    iiij'itiUUlvc  »*tiiti«llua  of, 

4-f.'      iJutv,   uiip(^>ri<,  and  hotnv  coniumpllon 

In  IVIlAoil  H1\4ti!t. 
PiurKi'u.  or  AlUpIC",  growth  and  prrparalion 

of,  4t!).     C-Mtpuintam  of,  acrordlug  lo  Perolra 

449.     CbcmlfAj  aiiaiiMi  uf,  liy  Buojutrv.  fOT. 

Xirurtvrrnf,    450.  J(/a.,    4-'>l.    O'J,    4M,  4iW. 

ADiTLTrakTloM    of.    wuti  tntiatord  lui(k,  iSC*. 

Dfifciivn  ol.  4^.     Dolr.  wlioiriaJf  pric«.  sfKl 

qo^itUtv    enlcrvd    fur    liuiuo  t:oii*uiu)Hltm    Ui 

ISM_I-V>,4M, 
**  Pi«K.%rrLK  RuH,"54l(  how  fUvovrad.  Mt. 
PiocMVLA    Ca>u,  or  chrcaa  fl|,  acoMtot  oT,  b/ 

Mr.  lhifican.481, 
Pirs  Clat  In  hnwj.  90t. 
Pifnursju  US. 
PmcMiHK,  desrrlptton  of,  A**. 
Plavk,  Irarof,  In  tra.yf*..  H7. 
pLtkiKR  or  P(Ki4.    AVv  Gypcun. 

Pm;«,  Iraf  of.  ITi  l»>iv  76.y^f..  74. 

Pmlknta,  Indian  r«>rn  flour,  3A|. 

Poio^toi  a(luli(*r4l>^  wiib  hor»rflnh,  343. 

Po^rarNArT  I.oxaKacs,  179,  W  a^. 

PuriAli,  Iraf  of.  In  LtA,^.,  IM*. 

Purrif,     Srr  Oiouin,  I'.'t. 

Pl*aT.     Srr  W  tor.  '^■•. 

Poaiva.  4f>4,  Prt'p^rallon  of  lh«  ingratl'eMl 
lor  brewing,  AOO.  Spmifti-  Knrity  of  good 
■Vio.  M4LT.  dNrriplton  o(  ir.4>  Kra>n  01  hur- 
ley  bHorii*  aivl  afcr  iiiiiUtni;,  ^'1.  Svvftral 
TarWilci  of  initlt :  p4la  aod  amber,  UtI  ; 
krown  or  blown,  nod  patvot.  Vnl.  Stalvmrnt 
Ihu  tb*  augar  of  malt  !■  fuiaiad  at  ttie  «x- 
ptow  of  tho  ttarch,  cootKlvrcnt,  AtTJ-  Hum, 
•racarhMianMa  ni  (lir  rroti.  and  lu  liability  tn 
■(ot.  mould.  i«"  '  '•"'  'I*  sif,,ji.,L,,.  .,„•,( 
Ia««urable  lo '  %>h 

•od  Bc'litUfl  >  llt- 

T.irhii  mrih "'        ;  .  ,      i.iji. 

'■'1,/fj;a..  .'lOl,  .'rtj.V  SiilpLui  u*ril  til  rv- 
plr  coloor  wbpomuiljr,  wn  HMStoa  1 
m  In  |-orlpr,  >K.  AniLTSKaTiuiia  of 
(•"rt'.-r,  «tlh  water.  Irtvtclc.  tiigar.  and  aalt. 
6or,.  HftfH*  nf  £iamM(  Fi<ly>t«ro  ■amplra,  &06. 


Z  K    S 


DiffVtrpnt  uppfifli:  grariU«i  of  thotc  obulned 
fnim  Ihf  bri-wer*  aiKl  ihn**  fr«tTn  lli*>  tmb- 
lican«,V>C.  A<)iilU>r.illon  with  «iilphKlcorirnn, 
bitten,  nnd  i  arraliiativn,  tu  iti-iitl«n,  quaiaU, 
camoinilv,  icirigtfr,  corUml*T  and  ciif*w4y 
■fr^lf.  caiJticjni,  irrami  u[  pimdlftc,  llq<iorlcp. 
alum,  iiilf>liiirlciictd,  ialtl  oriArUr,  carttonate 
of  kOtIa,  cnrciilna  Indinii,  And  tobarcn.  %a7. 
Erlrlciu-e  or  Mi-iirt.  PhdIltM  imd  Wkktum 
upnii.  ft'tl.  RffliM!  in  iitp  nmoti^  putilicxni  Tur 
ndiiltrrating  »urt«?r.  W'?.  Kruicnn*  at  M<-««r<. 
Slnimonrti,  Cav.  Rotltmn,  and  \Vn  khiim,  W"t. 
O'liiturnplioii  ft(  malt  and  liutu  ilatlunary, 
tlinugti  that  of  U«i*r  lurKHjr  Incre^iTHl,  ifm, 
M<-ttiorl  of  iiil'liii^  >aU  lo  pnrEnr.  50^1.  Mr. 
Worrl*'*  lilt  or  ftit'dtt-ranti,  and  advice  to  piil>- 
llrnni.Sfrt.  Mr.C»ii|>t't  leclp**  for  poriiT.AiiO  : 
two  rM:i|>r«  by  Mr.  Morrla,  filO.  "  Brcw«T»* 
drufK^liU/'Accii-n'*  (CatemMilconn'minK.  MO; 
Dr.  Norma  id)**  remark*  upon,  ft|l.  M't'ul* 
loch'i  cvldmi'Q  as  tn  the  rxirnilvr  a/ltiltrra- 
tli>ii  of^mrter.  At)(t  the  conapiiii<Mit  enormoui 
l0l»  tolhe  rfyrmif.  All.  A4titUraJiim  o[  hnpi 
and  mnlt.^ll.  J'ropoawl  reiri'tlr,  ft\1.  Df- 
tex*ion  nf  tk<  attttUn  atnmi  of  porter  and  ttaut 
witli  wotcf,  iMKitr.  aiiil  rum.M'i;  wtth  bi«<Ti. 
(-■arininatliv*.  Ac,  513 ;  wilh  rcicculua  iiidU'ut, 
Dr  H<-nipatli'»  tn-thod.  ■•la.  dl4j  M.  Kat- 
utunc't  method,  M4.  DrtiTtlnn  of  adul- 
teration of  hop(,AM  .  of  malt.  31 1.  MS.  Isn<>< 
raiice  of  Ihf  Kxcltc  wl'h  rrffrvnc^  to  rra't, 
hofn,  and  bf^r.  ihnwn  In  PTidenre  of  Mr. 
PlilIlipt.MS.  EkcU»  duty  pa<t  and  prrtrut. 
■m  trait,  and  qu>rtitip»  r*-tjiii»d  for  bofoc 
roriautriptlon  in  tb«>  V.  Kln|[dnni  In  IViS  — 
18V>,  &1A.  An4lriU  of  porter  for  Urrchnln*-, 
tit. 
Potash,  chrnnutte  of.  In  t<>a,  A7  ;  notath  In  aih 
ofcoffi*^,  107:  in  aBb  of  chicory,  131 :  carb'>fi-it« 
of,  hi  lard.aiB;  in  turtoprtc.  3HM ;  biUrtnLn 
of,  In  vtni-sar,  VH ;  ttibcurbnnatt*  uf,  in  uln. 
fi2S  :  bitartrdto  of.  in  wino.  ^^f(  -,  In  tobacco, 
M9  :  birhromnle  of.  in  »n>iff.  ti(H. 
Potato  St^vch  in  cocoa,  M'^.jtsi..  MX  t'A.  177  ; 
In  Irmey,  ?0J ;  (n  liutttr.  •£>!  ;  U\  lanl.  3f >3 ; 
arrowroM,  or  Dritlih./^,.  4-.  3lO,  /ftf.,3»; 
flotir  in  arrowrrmt.a  i;  in  uitiln''a,  3'<!1*:  *tari-li 
Id  mutta'd,  'M'J;    in  ]wtTr><'r,  Sfih  ;   in  rurry 

aiwder,  3»i\3»fi;  flour  In  dinnntion  ikO»'<lfr, 
7;  In  mtxrd  tnicr.  4.U1;  <-hf-f««>  in  Tbiirlnftia 
Mid  MaxiKiv.  l79  ;  flour  In  cnnfrcrloncry,  41*6  j 
leaf  III  lotuuTo,  f<M»  }  tariiia  In  opium,  (t3^  ; 
»t.irrtl  in  hqitotlri'.  r>H.'^. 

PonKi>  .Meat*  ajch  Fiiw,  Adult«>ni'lon  of,  with 
flour.  I'liallL.  uUittT  uf  Pml*,  sprnt*  >ind  other 
ch(?ap  U»b.  v«iii*tliiii  rv^  and  bolf  ArmcnUu. 
841  HftulUtif  F.tam.tn  r«<>niy«cUht  ■utn- 
>)vs,  M.1  I'nnwturnl  colnar  rommunlcatrd 
ijr  tlir  rpd  earihi.  3ia.  ETidence  of  Mr. 
KtrlmrdfOD  in  fi'irard  to  addllinn  of  horTRoh 
to  ptittfHl  tnf.1l*,  »4i|t->r''«,  r>-'loril<>i,  AC  .^13. 

"  Pin* nil  or  Pn^r  "  (lawdnit}  In  opium.  (>IA, 

)'owiiiiR4,  CD'rpnnnrt.  •(■•'l. 

r«tfr*a«-tio!»«i,  Pr'^prtctary  Alimentary  :  Wtiar- 
toii'»  Krvalcnta,  romim-lium  i»nd  arpparnric* 
of,  JJd.  jfi..,  33/.  ••  liarl"  or  "  durra**  oo#  of 
H*  prlitrlpal  inttrrHllt-litl  XU).  I)ii  Barry's 
RrralrtiU.  roni-.duiMili  of,  ^SO.Jie  .  333.  Re- 
Cplfit*  fur  makiD^c  KrvMlriitat  .iiid  Ri>«ali''il^'*, 
331.  U2.  t'ompiMllion  of  Butler  and  M'Cul- 
locti't    Pr*p«r«d   I^ntli    Puwder.   Edwards 


Ki 


Brolhen'    Arablea  'R(»val<tita.  and   S* 

Patent    Flour   of   Lenlllff.    33).     lUltai 

tlieir  rnnipoiition.  33'>. 
PttEvERVU    tND    JrtUCIi,    414.        .^•l«ilt«T'«t>»  «' 

oranKr-m-inn^Uiln  with  tMe«-t  t^r*ng^t,ft^ 

aniliiHi'cd«>,IIA,./Iir..4l7  ;  nf  rh«T»ttrm  )HIt»»- 

current  Jollf  :(nd  i>rrl»  tf-  -     \--     - 

idOiilaitand  ('.ilf  '•  f<H>    ,.- 

Jt^tuttf  1^  Anal     of    (nil 

]*ri'>i'u<'4>   iif  c'ippor    In    )n-|iii-iii   kii,j  «'• 

hvtry  lamt  Atid  oninpie  m<irinal*doa.  <11; 

pmervrd    gm-nx^e*     and     )ti>vncag« 

limr».  and  camll'^l  r(tr«" 

Hot  qf  the  a<i<*U/T-,%ttim  *■ 

dill'Ti  of  a  f  lit'M'cr,  of  or. 

npplo  or  turnip, anil  J-ll) 
"  Panor."    Sif  Cm.  S33. 
Pmi'wuk  Blue  to  tea,  81.  S7.  97  ;    la 

lloner-y,  4M. 
Paniair  Acio  In  confectlnDery,  4*9.. 
in-rctNiA  ORAMiMt,  or  mildew,  t«  whoabl 

jS|<.,  S&4,  ^6S. 

QcAMU  III  fOTter.  V17  ;  po«d«fc«l,  tn 
'■  Ql'icx.  rineitnr  proctn."  Jfil. 

R«Dl<il  Sciitln  miiitard,  A.V>. 

Kin  Stau  In  iniitt^rd.  M\  >^.,  353,  CM.  la 

p^i'p'T,  S'i\ 

riAi'PEr.    .^i-  Snuff.  COfi. 

KA«rtitRBrH,  111  1  jrlly  and  jam.  417. 

Ilin  I.KAn  in  Cayenne. 'S72,.%TA-  In  mrryi- — ™- 

SAA  :ii>  aiiDiitto,  4fM;  In  cnnf«ci|iiitM«.  AVt^i 

snuff,  OGtl. 
n  ifiNBT.  i(t«  of.  Lit  prrcipltate  tb»  rnr4  of  cal 

477.     J/r>tf«M  (ifhTafHff  '>r.  47».     Sty  Ckr««r.J 
Rkpacks.     Sff  Butter, 
KBTAtEnr*,   Dti    Burry's,   rompcMfClMi  of. 

Af..  W- 
nkvnncK.  Table  ibowInK  tba  nioani 

lots  tiiflVrcd  by  the.  o«rlng  to  Che 

or«dult>'rii[iijo,fi94. 
Rbvet,  a  •pc'.'i''*  of  whCAt.  777. 
RuAMNiis  (.'ATKARTit-i's,  i/r  t>w:bll*orfi.  4tfr< 
KHrB»RD,  411  ,  lr.if  of.  inrrtb>^-<i,  .'Jld.  AM^j 

aVi,  .VKb      rowdnreti,   adoltrrated   w4lft 

merle  and  triiejt  Buur.^.  <i77. 
Riii-»TvrHt«r»,  WO. 
Kirt  hLora  in  whrat  flour 

31)9;    In  rnuttatd.  34!)  , 

('avrnne,  373  :  111  cnrry  \\u    _   , 

43f>  ;  In  mlxnl  •plci*.  4AC  ;  tii  lt«|tMMUr.4iaf.  , 

Hour  and  Bread, 
Bosh  Plf»a  In  fe:*.  *^.  10^. 
RouNu  t>An)li:AL.    .■('•- 4 i>iTToml.  9(17. 
''  RlUDLa."  orUtrlev  li<i>t;.  Dl  iMtmnil, 
Ki'iiLsnttMiR.     Set  \Vi... ,  '.*.r,. 
HiN.  mfd'Tlnal  pr.ii 

iw»%vi,  Willi  w.ii 

liitnil  and    iiiibi.i 

J-lMom*  of  Tw"*?.! 

of    Mdiiltorat'nn    ■ 

LendarcidrmlaHt  , 

apple  Hum."  M    :  mfv    mi 

fliM  uf  a^iillrratii'ni,  M'J. 

for  ri>cciiliic  inditn*.  ^43. 

roiB   III  Kn|[land  Add  Si-'-f 

W2.    l^uiirittt'r*Uk<m  f.K 

the  Umie'l  Kutfilom  id 
Hrrt  III  wheal.  /Sn  ;  in  Lu; 
Kti  Fl^otmln  coflBsv,  II7 


4 

1 


[tltCit' 


rwaalMl,  In  ehkMry. 


INDEX. 


719 


M't;  in  iinnAttCL'4C»i  In  Itquoilo*,  ON. 
Huur  ami  Urviiif. 


Sfit 


S*muii'w  iimriMkiK,  or  ftgir  rnn^,  ISI. 

Sfcrmuw  111  fhM-M.  47^  ;  in  cimti^-tit-Mrrf,  49i. 
Sack  u»r>l  lo  iLtvour  elisor.  4T1>> 
»A<iu  Ms*L  in  coroj,  l«.  «  j,y,,  ^i.,  174.  17ft ; 
In  •rru»ro<it,  37i.  SonroAf  •uy>'.  ila  «prrlrl. 
and  hitbllAti,  3',c3,  3itt.  MmW  tH  prururtnit  raw 
*Agit  mml  III  t)i«  MDlitrt-m,  324.  Mc-iIumI  uf 
rri-(»arltt(f  itr4tiulitiF«l  la^o  and  •afo  rliiiir.  371. 
V4(le4ici  nC,  Hitd  dllT'^Teiit.'Ct  ill,  grMnuli(la>l, 
I'M.  At»l  LTKHATidNX  of,  with  ptrtjito  ttarrh, 
m.  Frx*.  lllu*trAllv»  of  lOfo  •tJiri.-h,  JI3\ 
SSA.  F«ri)liuuB  •■gii,  wlUlf  uiid  clournl, 
»ev«T»l  f»r-rHrt  of,  Hrrvira'i  rrmarki  upon, 
33W,  3i»'».  RnntU  of  F.ratm.  n(  Thirty  ■amploft 
t>(  tagn.  Sill.  iM.tiiom  nf  piriain  fltnir  iD.  3^i. 
Diiif.aiid  qiiiuitiltrk  linportrtt  amt  rrulnMl  for 
home  cim>uinp<loit  In  ia'<4iiml  IKA'),33ii.  Sii|[o 
>Urrli  ii»m1  loaJuHorAlc  Uplnra.  939  ;  prpi'^r, 
364;  Klop«r,  4ilt ;  ctnnamoQ  |K)iVil«>r,  437  ; 
mixed  ipicv.  I.Vi;  dnnolto,  4Uft ;  Hour  In 
|(qtlortc^  &I7. 

SAGOKaui.  323:  urrharthr,  au. 

S«ar«  LsviM  and  Omlna,  m  Importance  of 
S.  fif-tntna,  ai  fooil,  to  ihr  MaUyi,  3'J4. 

9aLKP  PuwDii  In  nfiHiin.ftXi. 

Salt  In  atiKM,  IM  ;  in  milk. 331;  ID  hfail,  3HA ; 
In  butter,  197.310^  in  Iinl,3(j3;  Int'iyimnc*, 
3T3  :  In  curry  |>owti)T.  ^*i\  .  In  uuc*.  420 ;  in 
KwUtlnv,  4&I ;  to  anitatln,  VA  ;  lu  port«r,  ftU> ; 
In  lo(i.rco,  ft\i9  -.  In  *niiir,  AM. 

StLTPfcTRI  hi  I'lharrtt,  3tfV. 

Sambicu*  S'iukr,  tiUO. 

SaHrHiac  CtcatKi,  putionoui.  f^ta]  cfliccU  of 
vailMK.  40f). 

Sanu  In  a«btffctilrnfj,  lai:  In  ■U|[ar,  |f  A  ;  In  to- 
bacco, S1l>;  In  o|tluia,63b;  to  ftcaiumauy.  RSU. 

Sarmku.    S0e  AnFr»o*let,S3A. 

Savcu.  419  Gr««t  varictr  of  >ub*Uocrft  Mi'er. 
Inc  into  ihHr  eora|to«tuoii,  419.  Hrtmiti  qf 
Anai.  of  TliiTtj>tliTra  •Mtrifl'^  of  Inilli*  <'if , 
toiit«t*i,  ai)(l  ih«  rs4i  iKf*  iif  (ot»t|i'r«,  *lirim|it, 

«ntl      nn-'iKii  k(>-       1?m  A  iki.  t  i  >I4  i  i..<aii      uilh 

trr.tl    'r-     f.tit,     C  IIJB- 


MX        L  M-  "^  r<:L  >i)r  11^:  uia11< n  jUtiid'^iM  1  by 
>U-.ir>    (.  ru<tr>  Ant  lti.irk«vll,  4.'l.     ObttquJty 

y.  (Ik   t'liltli.   I  •<(•'.  4.-t.4*;i 
V  *.  ..i^iH.  ...l.tiit^.n  .>l  l:<>ri.'lli-.ti  (".313. 
^\«'r..  .1   1 1  u,   i.hii'Tf.-   .-..iTf.-,   117,     Ma- 

i.-i>i  111*.  Ill  1 1 i>.  I  (.'    SuK'titu  (*'  ptfw*U-r  i>f 

|k>>it  "  I  ii>  iipi'irr,  »t\\. 
Ki  4MII4SY,  v3*»T<ff  i.f,  ij*7    Ant-ii-iit  r;r»*li  miMfe 
ofproeurtns  *f .  '^■■''     ^l.^i.^fl^^^lfll(  .tt  AMtx't^nX 

ilrtCrli  t"  ■      .  .    f        'r  ,     -■:■--        '■  :      .  .iOi. 

mmiy    i  ,.«-l 

^orM/ a- 


1.,    I',  1        .  .  .    o( 

'1  tilrly  tAJ»(-U'*, Cm^.      Mr.  Ht'r;:iit;'«  dvuldnrn 
upon  the  adulufrNtktni   «f   Kuitstntonj'.   CM. 


Dr.  Riitwl's  Inrormailo'i  rrfpMtiiin  lu  «l>il. 
Irralion  bpfnn*  It  rcwtiri  ibli  countri^,  (Ka. 
Scriom  •IT.ctf  likriy  to  mult  frrtni  tupliiiil- 
cati'Ki  of  (Iriijft  an<l  rliomk'aU,  (i-M  Driee* 
luM  '^  aitmUrrtUtoiu  of  •cammnny  with  chalk, 
lanil,  ilarch,  Kualacuit),  Jalkp.  tulphAtv  ol 
limr,  aiMl  iirKtrln«,  &VV. 

StAWi-MD  lu  tobacco.  •V«0. 

HiiALK  t:kiKALI,S4e. 

SrMriL*.  334. 

SCHOLtllA,  333. 

SKMt'U  lit  m'lk,  'J10. 

"  stuirs,"  or   «h«ai  hutk.  In   oatmeal,   SOt 

310. 
SmaaT.     Sfe  Wine.  W2. 
SuRiMn,  ^l»rncf  of,  490: 
SHcrpa  BaAi^«  m  milk.  tH.^V-  ^^ 
Silica,  powtlcrrd.  In  iniiff',  MW. 
SiNAri*   NiuaA  iml   Alba.  Hi;     nrirniU,   or 

rh-«rlork.  .Vi3,  Jig..  3.'.1 
SLok,  or  "tld  plum.  Iraf  nf.  In  t<a.^.,  H*. 
Sm«lt  In  c»iij'f.-ti-nrTy,  4.'>fi. 
"  SMAL.L3."  klKlDf*  or  lulMCCO,  '>0& 
Smut  iit  whiNii,  'jfift. 

^oAl•  t!i -"■■  4'-.'<. 

Soi>^  134  ;  riTttuniitr  of.  In  milk, 

23i  ,  III  tnrnii-ni'.  344  ,  In  porter, 

6<>7  .  ^  -in  tnlMCCo,  Vy 

9«tk>ii  M  1  UHbKUfiiM,  3t'>     Srr  I'aploca. 

Ainu II.  334. 

Soor  ID  opiitm   G38. 

ftilBGIIVM    V|i|.«ARK,  2*(!l. 

8i)t;r.  in  ParU,  pirpArod  from  MOtttUIUTlaq 
Iwne*.  4fi3. 

•'  SoitTiiAwm-Mi  Pout,"  ^Al. 

iiPBCivic  crnrUy  bivllk,  .M**, 

SriL-ttk.  rtiuin<-f.-ttlim  of  •arlctIM,  4)1.  Mtxrd, 
4S4i  «l(urlurr  i>f, Jig.  *^\  AM'LT1llt*TioN» 
or,  wtlh  wtimi  B-Mir.  (trniKi'l  ilc-,  p<njitn  Aovr, 
and  t'liC'i,  |.Vi,  RrmHa  <>/  KjOtit.  i)f  T«e<ity.iiK 
•ainpir*.  4A&      Deiaiiom  u(.  436-     Duty  un, 

Si'MATfi.    ,S«r  Anchov|ea,nL 

SgriLl*  ••liillrrjlrfl  «Uh  whrnl   Aour.jff.,  GTS. 

Ataim'M  lit  cxtfcc.  Uiilln- IfSi  for.  I2'>,  IJC ;  |xi- 
Ulii  III  foi'ua,  li(H,  *■/  u^.  ;  lit  kuir^r,  IM.  ly;  • 
Atid  tiarch  aus'ir  in  honry,  IIU ;  iltrcli  Ilk 
milk,  23i  1  in  tiutt«r.  .*Mk»:  in  l^ril.  Hit,  Hi 
airowroirt,  ■iti  i  in  n  iK<>,  1i^  ;  uitfn  aixl  pO* 
Utoln  latitttra,  i'i!) :  miHtnfrt-lluniTy,  41>'' :  In 
oplam.CaOi  tn  •cAmiDuO),  iiM>;  in  IhjiumIc*, 

SrtitinaiiOKa      Sft  Hioe.  ^Vl, 

Sru»'T.     Wr  Portrr. 

8iatc>l«i»R  I'l  IHXICT.  WT  :  qu^Uon  of.  In  Ut. 

ter  air*.  Mfi.  w»rY< 
"Srifp."  VHI. 
St'CCuKV.  13"     JtfV  Chl(Tti7. 
SiiiT  m  l-tnf    '    ' 
St'OA*   In   •  ■    Burni,  or  "  Bkrk 

Jar«."    11  (,  iM   rfci"-  •*     "* 

Tw"-'  ■•  ..  _.ji.»,  — — ^ 

I  >.  1  it-  u"    - 

n^    (. ^-  "• 

IUl<S  l*>i.  f«» 

ma.  AiiAir' 
Plyr»f,  »• 
and  cum 
Pervira  i 


10 


.  kugar,  lt>  mineTMl  cnnfUliienUuNl  JmpurUlM, 
lft:i.  Cryaulllivd,  burnt,  or  eju-«mt>l,  ivioLum 
•rk,  ami  trr.v-fr,  IN^.  Cr^Blnl*  (irr4ur  •upAr, 
Jii.,  IBl-  Strui-turt!  of  tlic  CAi»e.  nnd  prMrtiri- 
or  frasmcnt*  ot.  in  sugnr,  IM-lMft.  jteji.,  IM6, 
197.  IHA.  Knr<|iii-tirf  Rnd  abundanrv  m  Mtu- 
covadn  lUKxr  ftiiU  in  "  tuturdc,"  and  atMenca 
^ront  loaf  •HR*''.  rrmluMl  tiiinp.  ■iiyarcatidjr, 
iind  crrtitn  K«it  India  auffsri,  l^^S.  PkytioiO' 
tieal  actum  and  fri-perliei  o(  rnneiufiar,  197. 
LartiT  lioinr  (-••iioitiiiption  in  lUtW.  147.  Advl- 
Ti;aATit><««  of,  olth  pollen  «u|iar.  lUrcli,  huri 
i»r  lU-Kirliir,  fini-ly  (Hiwdernl  m:irl>lf.  rlulk 
or  vrludug.  Mnd.  buneOmt.  Aiid  cum'iion  Mlt. 
lao.  i>r.  Pfffeira'i  rL-m-irki.  nnd  Ur.  L.ethv- 
by'i  evidence  nii  itic  iitnnuCacture  of  lUgaT 
from  poutii  •UTh.  1H9,  "MIkIdi"  or 
"  Handling. **  Ib^  ^uncptt  dcwriU^,  111$.  Dr. 
Sotifftftn  un  the  manuriirture  of  »u(ar.  19S. 
Prrcence  of  trends,  gluccwe,  rraKiiHinu  oC 
kUftar  cjutf.  t|Kiriilft*  of  funcut.  and  Iniaru 
lit  brown  «iifiar  expUtned,  l!Kl.  Acarui  *«e-' 
rhnri.  or  *iiir><r  nii[^,  d<*wri]ittnn  o(,  IS*) — I9I, 
A^.,  I'JO.  191.  I'JV.     MrthtKl  for  Ur(»rtt(iK)U 

iir*>-kenc(>  In  atmar,  190.  Nuiiib<?r  of  thr  ai-arl 
D  iitfiar  a  trat  at  Ita  (lurity.  1^.  Grocer'a 
Uch  probHhIy  cauiMl  by  augnr  Iniecti,  it 
lM>ii);>  itf  thi'  lainc  cpnu*  a»  lh«  aCiiruft  acatilri, 
or  itch  [riircc,  l*J3.  iK'Of  ul<-«  Of  funirl  la  romtnon 
>u|[ar.  r.K),  yf-%  104  i  Vfiody  flbre  tu  luiup 
augar.  Id.1.  y%.,  lUi.  RentlU  nf  Kram.  a( 
SrvrnCv-two  aairplri  tif  bronn  auftar,  ISA, 
1!*4;  of  Flil^en  a4ini*li>i  of  lump.  IW.  Ad- 
vice  In  luii^r  rrfluprt,  j'j.l.  uetteliim  of 
otlultrraUemM,  Iffj ;  vlih  aalt,  pcum,  farlna- 
*r«>us  »ut»'anrea,  Jmlilnv.  n-nl  ttarcb  »u- 
Kar,  iU7.  Tciti  lor  llip  di-let-tton  of  cr«p« 
•ugar  :  Triimrnvr'a  ur  th?  copper,  Moiirr'i  or 
Ibf  potath.  and  tVhlinic'a  tr*t,  197.  Mod- of 
Vr»iKirlnK  FohltnK'a  teu  liquor,  197.  Duty 
u.i.  VArliiua  qiialitint  or  aiifAr,  miiitiFratnl  up 
In  |ii.vi,  i*!^  C^tiiflumpiiun  of  all  sorO  In 
IHM— Ig'tC,  lti8.  Employm'Dt  of  boih  cans 
and  [|ra|>«',  aa  luiiiltiTanlt  rtf  hon^jr,  'A%  2flS, 
'i()-(.  Siiftar  In  milk.  Vtr?,  •.•i.m  ^  m  ireUllnn, 
^li-i ;  in  pon^r,  tAtd  ,  in  rId  hSd  \  In  rum,  Ml ; 
in  brandy.  Mi;  randy  In  ativrry,  U3(  caae 
BUjtar  In  toluitfco,  .VKf  i  tn  lUiuirlrv,  6i&.  GR7. 

SCMMAKY  (if  Mr  Sliiiim>ndt'*r<[rutAtloiianrthe 
p'T-WiilMifea  of  adullPr^lKiti  lit  Tea.  I'cpprr, 
Sftiwi,  Tobai-cu,  Sii'itlti,  Wiiip.  onu  Heer,  0)8. 

SrLTiiaTK  ol  ll>fi<<.    Sef  T«rra  AlUt. 

SrLniu-iinAi*aiiK,  34^. 

SuLPilua  uipd  lo  rvatorr  colour  of  inuaty  bopa, 

St'LCHDRii-  Ai-in,lnTlnoffar,296;  iDportar,  A07; 

1u|iiii..hJi    .^rtfArld. 
St^VtCH  inaniifT,  till. 
Stcamoie.  k'Mf  of.  In  tna,  91. 

Taaar,  TalMcuni.  VO. 

TaccA  AiiiowaooT,  317. 

T*u-,  or  niicji,  in  tra.  W, 

Tamvbimi,  piilpiif.  In  upliin),  ^}».       • 

T*''MN  ill  It-a,  ■.». 

'rariucA  or  M-inihnt  Arrowroot,  17-t  \  itarrh  in 
arrowfool,  331.  Caaaara  meal,  or  llraJtllian 
arrowfioi,  Brrpr^l  rarirtluaof,  .ia7.  M-hI*  of 
i;rrp;(r  Kion.  ;ci7,  yy"'.  Strufimrr  and  matin, 
faciorf:  of,  Si"),  ^arrli  granulM  of  crmlrand 
lUanulaciurt'd  tafilora,^/*.,  S'A,  3:^.     Adul- 


IXI)£X 


nimillla  aasanqoa,  TT,  yfi. 
\ta{,fifi.,  71*.     Lie  tea.  %. 


f^r^^ 


TnannuAf.  wltto  mco  and 

3a-i.     JUtuitt  t4  lumm.  ol  TvnMT-Cfarati 

ulca.  3£(.     thuctiim    ^   n^m/teTMUgm. 

Duty,  and  quintlti'^i   lmr-<rT><!   and 

for  boin«  romumii 

Tat>l<K.'aatarcli  In  . 
Taitai,  aaiia  of.  ii>   . 

MR  ;  emetic  in  i(Hf.u-i».irin.i,  i  ,  j, 
Te».  )r">*tl»  and  pr«)>aratlon  of,  fift.      Vi 

of,  ^^.     Ita  6rM  iotrodiictlon  ii>l->  Fur«fa. 

l^oaTM  oTtartou*  drirrlpCiuna  i-t./fg*^ 

71.  7'i,  73.     Si-*>ntlnr  of  lea  *1U)  rartnoa 

grant  Onwrrt,  S'*.      Anitraia  nf  tea,  Ira  i 

cal  coiiitiiurnta.  r.s        \T..i.i-,'.      ..ii,,i,  ^i 

Btmriiir^of  (•-a  I" 

mcrHr$  of  tra,  IVi . 

on,ri,72,  73.     (  I  : 

74.     AiitiLTEntliii.i*  .ii    u« 

Irtr  the  Chloral,  with    forHitn  lna«ea.7&,  )^ 

7o.  77:    with  chioranthxt.   in'-,.'  yiortnii  ^j 

i-xirnaive  aav  ai  an  adtir  vVun^ 

lon'a  rrniArktOfi.TTl.     Iinkiri.ui  i4j>rrcvgi». 

powdor.Xf..  W.     Ani6rlKi  coloMnt^ft  mI 

ndiillrfHlion,    Rl.      CnloiiriMg- 

oth«>r     itibauncra     rmp'oyM,     61. 

wHiera  on  (liv    anbji*!:!.,  rvtrarta    fr»a  fthi* 

work*.  HI— H-V.     Te4   <l.vr>a,  A-V      .UmUrr^^-^ 

prirtttrd   in    ihU    (N><iinr>- :    «tih    liM»«a  if 

willdw  anrl   puplar.  ^^»..  •*« ;  wiih  |mv*<i  W 

plarr  nnd  '  ak.  >|;i.  tf7  :  with   lMar«  of  ka*- 

titorn,  alo*",  bffwrh,  elM<**     -■'  •   -• 

InjurliHi*  mbiiirinp  mat- 

Dulcti  ptnk,  caKrha.  cl  * 

p<itAtb,t(llp)Mli*iir  irnu.  ^  ' 

cli&lk  or  toaptt>inp.  PniaaLiti  iWuf^ 

vhromalaa  o<  Itnic,  mannr^la,  and 

the  ar»«]itr  of  Dippei,  a7        Haha 

If^vn.  Wt  analraU  of  tJ  >tiMyt  jind  Mth« 

black  tra,  by  rmnk  aud  PlillhT**.  9(1.     F< 

Ira-c*,  aycatfi fir*-,  bora*  ch>^iiut, 

96.     iLa  Vttio  Bifno.  ^\,    yfe,    >j%. 

batonlrAl  powder,  .die.,  93.     Itewwittt 

oftampleftai  BoM  to  tbf  piibiir.  *%4. 

maim  and  Aflaam  t^a*.  'ir- 

Ch  iIah.  arrntMl  oraiiir-   r 

HfJthtitfrntiimt.ltSi  »tci 

with    tuhiCaiii'ea    uanl    Im    i..,  <iiic 

131  ;   ft'frocyatiuir  of  Irnn.  nr  Pnta 

1)7;  ttidicu.  tunurric.!)!!;  bUrk  l^'ad.i 

or  kaolin,  talc   or  mlra.   frlapa*-,    ai 

Umc    ifi ;    Dutch  [tnk,   ro-c   pink. 

wimmJ,  |(V1  ;  i-^flMniiUF   of  limp  or   « 

bunatc  of  mafni^ta,  I-'rt*mii .  »,..(•.    . 

or  fll'itait!  ol  maeni-aiii,  I" 

hauaipti  ten  li-a»».  lul. 

bv   PbllU|»,    lOf.      />./. 

tulphata  of  Iroit.  I 

fHiubie  and  ari>i 

lot.      Hoinr  cun>ii>. 

1854— HWf,,  HM. 
Thha  AiJiA  In  eonfKtlonfry,  Dr.  ThcaBMn'i 

«vli]tfncr  roDcerntng,  4I1A. 
TaaiA  JwroMCA.    <S^  (^lerho, 
Thka   .SiNKima,  or  lea  ptant,  SS:   Bobai  Mid 

rtridia,  (iV 
ThijxI!  tnlra  0*. 
Thkoiiroma  ('ACMt.    .ftv  Cnroa. 
"  Tiliniia."  irfuac  of  wlicat,  eni|iloy«d  la 

(«rat«  oiiti»«al,  HfJ. 


ind 


Warfa 


INDEX. 


nt 


ToflAOeo  iB  porirr,  MI7.     Anllqutly  of  tt»  culM. 

valfoa  by  lUv  Ati«tlrm   AG9.     Cmaade  ii|rslnit 

lU  UM  In  EnnUnd.  M  hy  mrKltjr,  iutfffcciual. 

An.    Dvrlvatum  of  the  unn*  Narcotluia  mtwl 

T*taeoo,  MVJ.  i7').     IVlnclpnl  Bpertei  and  «a- 

rlMIM  KIUini>m«d,  570,      •■  Raw  "  M<l  "  m«- 

nufwtimd."    SH  I'liifMl    StAtM,     Virlaut 

IllDils  f<  OronolLo,  and  Cvtu  to(HCCu«,  571  : 

St-  Domteim.  Braiiltan,  Uulch,  Lfinl,  and 

Em»t  iDrtU.  A7a.     PruoeMM  of  minutactuHiis 

••  f  irt  •'  iiml  •'  roll  '*  b>4Mi«-eo.  in,  .S73-     Ulffrr- 

eiit  hlml*  of,  miiiTMratad,  ATI,  AT4.    Strwcturr 

ot.JIft..   ^7I,  A7fi.  It76.  Vn.  ATS,  379;    preu. 

lUrlli*^  c)i  itrvture,  iT4,  Va-     t'ow^wWrttW 

of  tubMro.  ATTi.      VaiMjudkt'i,    I*nM«>ll     and 

Nfflnma/m'i.and  CvmmelVt  analr«r*,  »f)0.  tHI. 

*l  ablr  ahuM  iri|t  (irnpitrtlon  ol  nicotinn  In  varU 

out  ktadt  at  laliAt-ro,   Mt.     C<Mi«t)tHrirti  of 

lobacco  fmnkc.  a*  (•aitraal'd  by  Haali,  Utivfr. 

dorben   hn  .   Zcitr.iuid  MfilM->i«.  Mt.    Txblv 

abowlng  the  f>in)crnl  crnipoalllon  or  Six  larn- 

pl««  or  Iraf  uibacro  u  Impnrtprf,  W3.     Tabfcv 

•hnwlnir  compoattliKi  of  vUrat.1l*o  lakrn  up 

bjr  elhur,  iKal  of  tli«  cold  aod  hot  aauroui  ex- 

tr^diYc  and   Uiat  o(  iba  aali.   Mi.      Tablp 

■iwwiojr  th* eo«|»otllioo  oTlhr  tobarm  »(Hlk, 

M&.    Table  aliowlug  p«r<emUMtP  u(  ni«<Ut(ir«. 

extract,  •oltiMe,  tnt»lubl«,  and  taul  uK,  and 

gturoi*,  In  Riff»t  >ainple«  of  unniaBufarTurvd 

inliai-ro.  SM'i.     Par-rrnlaf»  uf  #iiractl*e  and 

hcnrou*   maitvr   In  diSrrent   kind*,  bjr  Mr. 

PbiiUpa,  MC     Mmifi.  Co"per  and  BrMMla*! 

analjrMW,   AM.      /'ropetttr*   of    tob>uN»,   MT. 

Ita  «flhau  upon  the  human  Bvf  i«ib  tn  MBkll, 

larnirr,  and  HbMlaicljr  brfa  (k>M«.  W7,  Wt, 

ratal  moMqiMmcM  fMnUlaf  from  ch«  an. 

plleailoa  or  tobwco  Jatc*  tn  rlofvom,  SM. 

AbctntBATiuMa    of     tntMcco     viih     l«aT*i 

nf  dork     rhub4rb.  rolUfoot.  r«bba«»,  pota- 

iwt.    rloruf»    »,Mll*«,    vim.    and    o*k,    wUh 

mah    riimnilng*    and    jMirt.    IVix ;    «jih    •««- 

wrMt,  rn«.i«^  chiociry  r*>«>i,  whmt.  oalincul, 

b*«n.   r.tlrcliii,    iMktim.    lofvmd    dj-^,    rane 

•«t«r,   lr<^ci«.    hitoi-y,   llt^unrlrc,   tMvt    ri<  t 

dr«fn.  Rlira.  ult;    h>'drr>clorato,  iiltr»lf,  aixl 

cartiniut«  of  ammonia;    potaih,   u-m|.i,  limr. 

•uI|4m|»«  of  mwgnriu  .n'l  «Kta,  fr»lo»'.iclire. 

umb-r.    fullfn'    r^rth,    WnrtUin    r»d,   laitd, 

iMlfih^U-  i>f   Irtin,   •allp'-rrr.  eojitxra*,  (.iri-n- 

dvr,  rosf wort,  axd  *lth   «iat«r.  M9.      UctHit* 

qf  Ktam.  of  Flftj-^iU  larnpir*  a(  mxnufac- 

lurnl  and  nnBaniifoctnrvd  io4>«cco,  nw.  B'^. 

JUtfttiom    (/    tutmitfTMioms   wilh    dork    leaf, 

•irunnre.  tKJO,jlft..  .191,  R»3.  ASO,  KH  t  *llh 

rhubarli  Icjl.  ttrunurf,  IVBl.  Afi.  BOA.  Mffi  i 

ttiib  rolitfuit  l«>4l.  ttructure,  ^.  ^t.,  MT, 

i'<^.   >"-<-      DoKitptlon  of  procMao*  lor  th« 

1  ;  ftii  .  ,tl     aniily«U     of    lobwto,      IV*/7 — flOI. 

r<.\n>.    in.miif^irture   of.    In    Kofland,  4e- 

•.•riKfl,   lioi         Vatirijr    of   namr*    Blvrn    to, 

I.  J.       AinrLrtMAiio^*   ut,    Wi.       RftUta   ttf 

Ij.fii      lit     Fiit>-<l(tl)l    •amplvi.    nra,    MO. 

y*\H!r.    l)Nj.    a|ip(c    iwdnx*.   flrr..    >n   riKar*. 

iVJt.     Mt-*t-pMiK  fti,  lit  tftcchartiic  or  aaline  w>- 

Ittttnna.  fyu.       >lf»l«-rloua  |tf*ntiibu1a(orf  lo> 

tMrcniiliiB  of  Wlatrcliaprl.  fKU.     SiiiU«iell»K 

oldft^ri.  aitdileeepuoa  [xactlard  t>y  kabvihng 

brtiUli    aa    r<>r«ifn,    rU3,    6m.       Jirtrrtttm   i/ 

uiiM^/cmfiMl.  Ml.  fiM.     Shvrr.  ranrllM  of, 

and   na-itra  Blvm  to.  MH.       Nanufactura  of 

dry  (tiuRa  — &c<>ECh.  Iriih.  and  WeUh  — de> 


ftcribvd,  CUii  t  of  motti,  or  rapiwei,  with  d»- 
arrlfriloM  of  t)i«  af*|<*'*><ua  for  grinding,  fKMt, 
fUn.  Proerai  adi<pt«d  lor  »c«ntln)r.  GO*. 
AtM'LtK«ATtofh»  of,  with  aatt,  ml  and  rdlow 
oclirv,  •i.iibcr.  rhmmaita  of  l«ad,  rod  Irad, 
btcfariimai«  of  pouab  arwl  powdemi  tillca. 
&«  ]  with  po«d*f«d  Arria  mot  and  «.atfr. 
rAPj.  ComptHttton  of  cephalic  anuff.  and  of 
Cirimatonff'a  ij»  tnulT,  6l(t.  Kvldroca  o'  Mr. 
I'lilllipa  rrapcctlns  lhc  iwlnttrriitloD*  of  fouff, 
Gio.  Gil.  N<>CMil<y  for  ait«rAilnii  in  the  Tn- 
tMmt  Act  f>l4.  liHraian  fiflkr  athttlrratHtnM 
of  tnnir,  614  ;  wtth  pfHi.  wooclr  Ut>re  Inrlttd- 
ft)g  diitic,  Ivad,  ttiid  |K)CH*h,  diS.  Inatance  of 
Inrtttclfncj-of  the  Kxcikt-  In  reUtton  toadiiltrr- 
atktliaoftobaccft.lil'l.  J^vp^rtirt  AiuWri'cfi*  of 
liHiacru,  1)14.  Nk-uiinaaiid  niriHiaiiln,  itctlvo 
trrtniMplea  of  tobacco,  th<:-lr  inllii<-iirr  iiikmi  tli>i 
nxman  frame,  GU,  ti|^.  Tl«f>  iiiit-ttloa  uf 
IiiIhc<u  tnmktng  i;ou*Mcr«l  aj  a  iiixlivr  nf 
health,  tilA.  f>lti.  Kffpct*  of  toltacru  ebewlnfc 
and  bumIT  taking,  til^,  (>IT.  r««<<  of  aUrw 
VOUonmg  by  anttrr  ctxiUlntnit  |p4ii,CJ7 — 91!*. 
Throa  caaM  o<  pat^ijilt  r<-«iilttn(t  frcirn  i(« 
lUC,  630,  Oil.  Inclranlinra*  ncccnltatcd  \*f 
tka  UM  of  lotMn-n  hi  aiijr  form,  titt.  Q3'j ; 
Adam  Ctaiktr'i  and  L^ird  Statihope'a  lemaika 
apoo,  SSI,  631  ;  Kinx  Jamr*  ).*•  ricwi  ujion 
lh«  subject,  Si3.  Vuttomt'  dtitica  upon  ti^ 
hacco,  clgara.  and  anulT,  and  qujuituiira  «>ii. 
tcrcd  for  home  rnniuropttun  In  IHM — If'iG, 
6X1.     Tobiirrn  Jiitce  In  optuin.  631. 

Tot»  LM  Sloia  In  ctxoa.  I7&.  Jig.,  176. 

TiuaACAMTt4,  icum,  lo  milk,  ^1. 

TatacLa  m  Migar,  IW;  li>  milk.  Hi  ;  hi  aaucM, 
430;  In  portar,  M6;  la  ■borry.  H3 ;  la  to* 
bacco,  Sm. 

Taith  CM  rijlgare,  «flttvun,  and  hjibernuKt, 
>p*rie«  ol  «b>iat,  US. 

Ti'MMLiuc  mteR.ll.1Nli  <»  milk.  33)  ;  tn  mti*. 
tard.  34H  ;  In  Ca»«in»  S7J.  t'-ifpotitti/H  of 
uirmTlc,  3*7.  iohn.  Vojifl,  and  Pfllrflrr'* 
■i>al7M>«.  an'.  SlrwUtrr  of,  .V-T.  fian.,  ;j«4, 
S»i6,  AUfLTiKATia-'**  Willi  Vi'Uim  tHhrc,  cor- 
hoiialf*  of  toda  Ami  pol.iah.  i^.  tti-ltrtum  of, 
3Mlf.  ltn|>i>rt«  of.  In  <»fil.  Hint  XSitt.  3tf».  I'ur- 
mrrlr  pnwdi-r  In  irti)|t*r,  4i7  ,  In  aonato*, 
4C6i  in  cmiTrcttotWTT,  WV  ;  In  ofilutn,  f;iN;lM 
Turkey  rliubarb,  67< :  in  arommlc  conft^iUm, 
079  ;  In  Uqiiorlco.  <JiN7.  Jig..  Mv.  necri|«  for 
nukinii  oompouiHl  linnet ic  puwder,  688. 

Tuanir  In  marmalade,  4in,^.,  417. 

I   I m  conf*rttoi»e»y.  AM. 

.rucilooefy,  4)U;  In  tfibarao,  MO  g 

1. <  ^iii>->,7ao.Jlt^ieii  katida^tfOi  Mgr- 

luoi,  VUt.Jtg;  f'ik  rublRU,  IkMHrla,  MO, 

VtnoMU.     &rr  Wine.  JiM. 

Vr-iimAJ*  U»Min  lfa.»7  ;  in  icronnd  coffee,  ||>J  j 
In  rhtC'»rf,  144  ;  In  tinnm,  iU't ;  iii  atichn«||ia, 
aW:  iiiptiit>>4lnieatiandlbb,94|  Jn  raymne, 
173:  hi  aiinaiio,  4lUi  la  eliaaw.  4j*0  ;  in  to- 
b«cM.  !>*9, 

VtsM  Hinu  o»ed  In  adnlterate  tM,  9i,Jlg..  Ol, 

Vaauiuaia  In  cititfvcllonery,  497. 

Vta^iLioM  in  Citjrmne,  J7;i;  Id  iatM«>,  4SI  j 
111  coofectlooflry,  4*f', 

Viaaio  1  iiTici,  wt.jfr.  SGB. 

Vl.<itcAa,  exJaieiicu  off  Ui  evftaln  platitl,   3^ 


712 


INDEX. 


Mftdrt  of  prrpAration.  3&0.  Clmnwi 
li  arid.  ISl.  'Quick 
.Acttliirrmo<l'l  of  Mi*Hft.  lllit 


hoi    Inln 


rinmr 


1- vanb,  nnd  Co., j«r..  Wi.  "  Vint-par  ni"iti»T,"' 
»iS.  Difli^rriit  kind*  of  vino^ar.  And  tl»«lr 
niMixititciure,  :itij.  DotlllMl,  witip,  malt,  nnd 
tilgnr.XM.  Thc"riri<>iinr  plnnt."  liArtlctiUri 
)n  rKerrncp  to.  hy  Mr.  Mt-tflifr.  3W.  3^. 
DifTermt  itn-iiKltt*  or  ()iiaUltf>  itf,  :t^.'»  Aot<L> 
TkRATloNHBir,  with  wntrr,  suifihtirK-  nrid, burnt 
■uKiir,  irr^lufc  or  |»ittftii)H<.  p>r«)M|nii^ui  And 
MTfiir  Actili.  39');  with  iir*fiilc,  Mr.  .Scan)an*« 
c»nl*ncc  rMl»ccilnpr.  SWi,  3*17  ;  wtth  corroilrc 
Mihiimatr.  nr  '■  Ttic  Doctor,'  Mr.  f^ray'i  ^*1. 
dencp  concrrninir.  397.  JUMuilt  </  F.tam.  of 
I'hlnt'-threr  •Atnplrt  of  ilncfpir  piirrhiumi 
in  l^^ndon,  7D7  ;  and  or  a  Mvuml  s«>ii<>«  of 
Twrntv.plsht.  ,r«.  SulpbuTir.  and  acf*lc 
MCtili  In,  394.  DrUcliim  qfnauiuraitoni,  199  ; 
with  K>*itc  acid,  3W.  Mr.  Griflin't  alkall- 
mrter,  3W.  Dctcvtinn  «r  (iiiphurtc-  acid  lo 
Tlnegar.  401  ;  Mr.  L^'wIk  Tliommii'*  rrmATk« 
upon,  Knt ;  tvntnX  mrthodi  of.  40'i.  40S. 
])<rtettioil  of  Cliill»  and  nihrr  arrid  Mib- 
BUnres,  of  burnt  o'iKAr.  and  of  acvtic  and 
PJToMrikw.u*  arid*,  (Ofl  :  of  bhartrnlf  of  pouih 
and  mciallic  tm|ittritlfv  4''4.  Evldi-iirc  nf 
Mr.  I'M  nipt  on  the  adulfratloni  of  vincor. 
4IM.  DiiiT,  import!  and  liunie  contumptloo 
tn  II^M  and  IK-Vi,  101 
'iTANVDiWtMT,   ^aS.  ' 

ViTTJi,  oil  rccpptNclet.  STB. 

•  Wakx  HoBiN,*'  311. 

WaTU,  in  mltk.  £11 ;  fn  bittt»r.  IST.  9M;  In 
Urd.  :'(i-l  {  In  rlnrgar,  396 :  hi  rotter.  MG  :  in 
(Hn.  ft7S ;  hi  rum,  A4I  ;  in  l>raMd«,  MS;  in 
Inbacco.  ftHD  (  tn  ionfT.  fil"  ;  In  oitlunn.  CW. 

Whrat  Klouii.  In  colTw,  \t!t,fig..  Iv?;  faHncjr 
nfiCMltnt  N*  A  tvvt  for.  ('i.**.  I>.'<i.  RoailtK}  whfaC 
fn  clifcorv,  \A(\.  fin.  141  I  flour  in  cocna.  II^M. 
Whfflt  Mur.  Ii  tn  t.onry.iM;  In  pticlctl  mt>«ti 
and  llih,:mi  in  mustard,  348;  m  pri>|irr.3G4  ; 
tn  vnnc*-*.  A'iO  ;  lu  fcnifrr,  43^^  (biknl),  tn 
ctiinainon  fviwdcr.  437;  In  mlxml  tpicr.  4.V); 
In  annatto,  4l>'<i  In  cnnfprtlon''n  ,  486 :  in  In- 
baccii,  !3lif.\;  In  npium.  fDfi;  In  tcaromonj,  r>Aa, 
ftr-.Wj,  In  ip-anrnanhn  (JT;i ;  in  rnltwjrntb. 
6"6i  tn  Turkt^  rhubarb./?/;., 67;}  lo  powdpri^ 
M)UiH*,  Jif..  674;  in  rofnnound  •camitiimy 
pqwdrr,  *»;<» ;  III  liquorire,  6^t. 

Wittow.  ifnf  of.  In  tta.^..  Kf». 

Wise,  M4.  Cbnnicid  conftllupnU  and  vorlrtW 
of,  .^44.  ClaHification  of.  H-"*.  Anmuni  of 
nb«oiute  alrohol  prr-^rat  in  ordtnar;  wtn«>>. 
catlniatcs  of,  bjr  John>tnnand  Brands,  MA; 
in  Orrm^n  winra.  hj-  I.lr-Iifx,  %ift.  Ppr-r^nt- 
Af e«  nf  jlcohul  In  ordinary  vtnr*,  ncroridlnft 
In  Dr  Ji>nt*«,M^;  nint(>rtidlf  afr(-ct«>«l  by  affO 
M-V  Ord'-r  of  acidity  of  litP  ch\ri  wln*^.  he- 
llnnlniii  with  \hr  Icait  acid,  Mfi.  Principal 
•W»K  Nnir*.  ordrr  nf  twrrtiii***.  ."^7.  Aui'L- 
TlliaTiKNi  of  win«,  M9.  PuRT.  with  brandr, 
eldorfoerrj:  colouring,  Jernplga.  Kigwood.  and 


Infrrlor  wtn*«,  MA;  «ttk: 
Warren,  anil    l'r»-'»   rr^i 
64&;     Mr       <.r.  ..*< 

tlw   Ua«  Mf     Ir^'  \« 

lloilft    cu[ic«rr  <4i 

■poilf^  culrr,  v»>  ;  w  itb  tli<a| 
Vartoui  rrcvipla  (Vir  C|i«  m^mk 
r»o«»  i>ori,  Ml;  of  "  AcrmmB) 
Dvclinr  of  tx»>'-  ■ 
*brro  trrown. 
leriatlc*  of,  !>:■■■. 
tiont  of,  with  )> 
rln,  and  « iii*- 

wlillr  winr-  »J>-\ 


ct.l.  r..  .■  . 

Biaoi  V 

out  to  ii  ■    ' 

itirr  nf,  yr^       \  in-  (•*■■ 

chaTni>a|n>«^,  MS.    ('Abi 

Kr»^rh  tiln^.    «t»(r»r.  wnd 

and    fninptlii  f    . 

f-V..     ltpcvi,.t    : 

Kudcahr ,  ,  ,„„ 

Cti«a|)  I 
C«rfiMn 


11^ 


dUCT-J      I 
Tartoua   - 

Dciicc> 

M-    PpreU.*    1 

offop|»cr  in,  '• 
«alu?  of  mint- 
thr  t^iH.r 

on  eulor;  1 

mt«red  ii>< 
WinkfTTD.tK      ,'.. 
Ti- 


tJmm^  4 


«* 


97X    JV4N#Na  (ipc-r«n«f  »4  fragi, 

pe.llea.  V7J.  * 

Zta  Hat*,  or  ImtUn  corn.  Ml. 

ZiMc-  ta  conrvcibtfwrr,  • 
ZiNktuaAcajfe,  43L 


a 


LoMPOJi:  PriDtwl  by  Spematruooc  and  C«^  N««<«lr««(  Sf^v«. 


§,bbcriiscmcnls, 


ELEGANT  PERSONAL  EEOFISITES. 


Under  the 
The  Conrts  of  Europe, 


Patronage  of 
the  Aristocracy. 


and  the  Upper  Chsses. 

ROWLANDS'    MACASSAR    OIL, 

For  tilt  (JUOWTH,  RESlOUAl  (()>,  •n.l  for  IMPROVING 

AND    BEAUTIFYING    THE    HUMAN     HAIR. 

It  nrevrnti  IUt  rr^n  fallifiz  off  or  tiiriiirii:  (rr«v.  ■trmethi'ni^  weak  IIAIK,  rlransft  it  trota 

?«fiirfin'I  lUnilnfT,  iin<l  nuke*  il  »K\t' I  I  KIM.V  SOKT,  CIMII.V,  mul  UUWSV. 

In  th«  Growth  of  the  BEARD,  %VHI8KGRS,  and  MUSTAOazOB, 

it  i»  uiifailinic  III  it«  »nmiiiiitive  opfrndoii.     Kiir  iM  H.DKKN    it  I*  t'siw-cntly  recoiumcDileU, 

a«furii)mi{  ihfl^sttof  A  IIBAU  1 1  hUL  ili:M>  Of  HAIR. 

Price  3i.  M. ;  7». ;  Patiiily  lk>ll)r«.  rqiia)  to  (Our  imall,  I0«.  M. ;   and  double  Ibat  kite,  iU. 

HEW    LABXL.—I'n  prvvml  llie  subilltution  of  tipvHotui   ImitatUtms  for  Th«  gvioine 

■nirk.  x><f  uiipnnripifHl  ahnfikpeprrB,  n  Nkw  Lapkl  from  rtfel.  hy  Mntn.  Perkiiit,  lUcoiu 

■nd  Co.,  l«  iHiw  u«r<l,  whtch  CAM'iOt  lif  f\^fsi^i\.     It  i«  rom[^>«ci]  of  a  «ectiuii  uf  un  entrlne- 


'    tomni  rirde,  re|iriitr<l  our  htinttfrJ  amt  tktrlif  timet,  ami  funti*  an  oriKinal  lac«.work  Krounit, 
f    upon  vrliich  ii  cnx'kvrij.  m  wln'c  Ictu-ra,  itir  norUt, 

(  "ROMTLANDB'    MACAaSAK    OIL, 

PORTUfiGttOWTlI,  RKsr..|{AlHiV.AM>KOi{  liKAl' I IFVING  THE  HUMAN  HAIR." 

Uadfr  «li)cb  IS  the  ?<<irtittiirr  of  Ibr  I'mpriftdrs  m  Knl  Ink,— 

"A.     KOVVLASI)    A    SUN8." 

The  nbolr,  with  Ibc  rxrrptiim  uf  Ihr  |<ruA'r  uf  tier  Majciity  ttte  Qiircti,  beinj;  covered  nilb  ■ 

I  lac«  work  pAlterD,  In  traiwpareni  cok)uil««a  ink. 


K  A  LYDOR, 


ROWLA  N  DS' 

AN    ORXBNTAli    BOTANICAL    PREPARATION 

FOR    IMPROVING    AND    BEAUTIFYING    THE    COMPLEXION, 

Kradiralrs  CUI  ANKOUd  UKKELTS  and  OlSCOUmAllONS.  and  render* 
THE    SKIN    SOFT,     FAIR,     uid    BLOOMING. 

it  otiviatea  atl  the  elTtfcis  of  triimift-  on  tbe  fikiti.  wtietbtir  *f ith  rtriTt-nct.'  to  cold  and  incit* 
m«ttcyt  or  int-nsr  volar  ht^i,  and  nfTorda  iinnirdiate  relief  in  ca*n  n(  i>unt)urii,  attnta  of 
lOiet'i*.  cr  <nri'l6t)Ul  IfiflammatiDii.  GetitlrTiiPU  after  thavtoK  will  ipprcclatc  ita  aofteninf 
albd  aioeliorat'iis  prcjcerltco.     I'rice  4>.  6«l-  ami  H*.  tid.  per  Irotll*' 

'Tlie  words.  KowLAKDk'  KAtvooiir  >r«  u«  the  wrapiMrr,  and  tbelr  aifpitare, 


CAUtlON. 

A.  UovLA  91  o  &  Sena, 


in  rvdiuk.at  foot. 


ROWLANDS'    ODONTO, 

QDBpOttftded  ol  tb<  choiceal  and  tnuat  nvhcn-lM^  Inicredlenia  of  the  ORIENTAL  HKRBAl , 

■nd  urinc*timab  e  value  in 

PREBCRVING    AND     BGAUTIPYINO    THE    TEETRf 

STRENGTHENING    THE    GUMS, 

And  ill  rrriderinj; 

THE    BREATH    SWEET    AND    PURE. 

Pricp  t%-  ad.  per  box, 
CALTTIO^'.— The  worda,  Kowt\Nii"'  OhosTO,  Nreoit  the  label,  and  A.  Rowlaxo  IkSoir, 
Ml  HaltOQ  Oardea,  engraved  on  the  Gi>vcrtiii>eiit  :«tiitnp  affiled  on  earh  box. 

Bold  by  A.  ROWLAND  &  SONS,  20,  Hatton  Garden,  London. 

AND    KY    CMMMItTf   ^HX>    rKHrUM  8 -<«. 

Deware    of  Mpuriooii    ImltAUoiiMVW 

3    A 


u 


PURE  AND  UNADULTERATED  FOOl 


"The  preparation,  denominBtod  bjr  the  MaTTufacturer*  "Osvrsoo  Pbta 
CoKir/  po«5oe0ca  both  novcltv  and  raorLt ;  I  am  iUerefore  induced  to  comply 
the  requMt  nf  tbo  Agentf,  Mesars.  Kirsg  and  M^csr,  and  to  eertifj  lo  tbe] 
and  exoellenoe  of  the  article. 

**  It  consists  almoat  trboUy  of  tlio  focuU  or  staroh  of  ladiui  Corn,  ukd  it  tia»^ 
fore  possesses  all  the  properties,  plijiioal,  physiological,  and  dietetic,  ofaa  JLisvl 
riot.     It  is  light.  oasOjr  digestible,  and  of  dt^licate  flaTour." 


(Signed). 


ARTHUR  H.  HASSALL,  HD, 

Author  of  **  Food  and  its  AdoltOTmti^ 


B,  BcDKtt  Street,  St.  Jain«s% 
ISlta  July,  18M. 


Tbo  Importers  arc  desirous  of  bringing  thu  recently  introtluc^  Mid  vaii^fe 
article  of  diet  under  more  public  uotioc,  oouvinoed  that  it  baa  only  to  be  fcll 
to  be  appreciated  and  cj^ttiusivcly  used.  It  is  prejiared  from  Jodion  Con  ff 
Maize  witbuut  fenneutatiou,  is  perfectly  pure  luid  unadulterated,  and 

equalled  as  a  recipit*nt  of  Uavuurs. 

It  is  the   roost  delioale  preparation  knovn  for  Puddings,  Custaids, 
Creain,  filancmangc,  kc,  and  con  be  used  for  all  tbc  purposes  for  which 
is  employed]  being  at  tbc  same  time  of  a  lighter,  yet  more  DutriLioos  bat 
ei,  Kins  WiUiam  Stroet,  Citjr. 


May  be  obtained.  aC  lOd.  per  Packet,  of— 

WORTLBV  and  HAlfBCRY    M,  Upper  Baker  Si 

Messrs.  FOBTNUM  and  MASON Piccadilly. 

DE  CASTRO    Piccadilly. 

MART    130,  Oxford  8l«set. 

PHYTUIAS     430,  Strand. 

COOPER Oanabur^h  Street. 

FRESUWATER  end  Co Po«ltrv, 


ADVERTISEMENTS. 


HARDS' 

[  EARINAOEOUS    FOOD, 

■  rOK    INFANTS,    ZirVAI.II>S, 

AND    PERSONS    WITH    IMPAIRED    DIGESTION. 

MANTTPAOTURED   BT 

JAMES   HARDS,   Dartford, 

MILLER  TO   HER    MAJESTY. 


COPY  of  I  TESTIMONIAL 

orrnr  bt  thb  uti 

JONATHAN    PEREIRA,  M,D.,  RRS. 

A8SIITAKT  TUYBICUX  TO   THl   X^VDOZf   BOftrlTAL. 


**  I  luTe  canfuUj  eumtQed,  and  rapMtedly  prvwribed  '  DabD6*  FABrvAOBOUl 
TOOD.*  (tee  Porora's  TreatUe  on  Food  and  Diet,  pagm  309  and  473,  Slg.)  which 
is  prepared  from  the  most  nutritious  of  tho  Cereal  grains.  It  combines  boUi 
nitrogeniscd  and  non-mtrogenised  alimentary  principles,  and  forma  a  tctj  raluablft 
Food  for  Ohildren  and  Inralids." 

"JON"-  PERETRA.  M.D..  F.E.S. 

"  AsfilSTUTT   PUTfllCIAS   TO  TOE   IfOVDOH    HOSFITAU 

•*47,  FiDsbiu7  Square.  July  1, 1843." 


Sold  at  all  respecUbla  Chemists  and  Paiont  Medioiu  Vandors,  Tea  Dealora 
and  lUlian  Warchousei,  in  Packets  at  la.  and  2s.  each ;  also  in  Tin  Cases  at  7a.  6d. 
for  Familiea  and  Exportation  i  and  as  a  Canlton  against  spurious  imitations  it  if 
nsoassBij  to  observe,  that  each  Packet  is  signed  . 

"JA3.  HABD9." 

8  A  2 


4DVERTISEUENT8. 


CIjc  Snibcrsal  |1urbfi)or  OToiiipaiii 

(LIMITED,) 

(Established  for  the  Supply  of  Articles  of  Domestic  CommnptiM  tf 
Use,  free  from  Adnltemtion  and  Fraud). 


TRUSTEES. 
SIR  THOMAS  TANCRKD.  Bart..  TUlin^on.  Siwsex. 
TUOMAS  UAIKES.  Esq ,  14.  Lower  Berkcloj  Street.  Fortnsn  6fW« 

BOARD  OF  DIRECTORS. 
STR  THOMAS  TANCREI>,  Burt.,  CUairmaru 
REAR-ADMIRAL  DUNTZK,  Woolwich, 
ALFRED  HANSON,  Esq.,  2U  Old  Bqusn?,  Lincoln's  Inn. 
ROtlERT  RATKES.  Kiiq.»  Treberfyd,  Crickhowcll. 

J.  L£  CUEVALIER  ST.  ANDRE.'  Esq..  S3,  King  Wmka  StMt, 
Charing  Cross. 

SrCTftary,— Mr.  T.  E.  OURNKV  QORB. 


TA*  Ctmipanjt  are  ready  to  appoint  tt  Itmitrd  nmmher  nf  Agtmi9  X^  '^  M^^ 
m  LcHtiot  and  tAe  Province*.  Vmejr^plional  r^crtnctt  mm  I0  rA«r«rt(r.  «b 
mHpff  sKxtriiyt   vi/I  be  regbired,     JpjjUcalions  tn  be  made  mt  tieC^ 

*    83.  Canmof^  Street  ITejt,  London,  E.a 


I'ROTECTION    AGAINST   ADULTEEATIOJi 

■ 

FRAUD. 

AIiL  FAMILY  SUPPLIES,    GROCERIES.  WINK,    SPIRITS,    Bl 
PROCURED   THROUGH  A  SINGLE    HOUSE    OF   BUSIXJ 

LONDON. 

THE  UNIVEESAL  PUEVEEYOR  COMPAH 

(LIMITED.) 

Im  wmx.  orxnATiOK  fbom  Ibt  Jcri.r,  IftOC. 

83.  CANNON  STREET  WEST,  CITY;  23.  KINO  WILLIAM  SFBEIT 
CHARING  CROSS. 

Where  Lists  of  Prices,  and  Prospectuses,  may  be  obtaiaed  tm 

.    ,  application. 


AOVBRTrSEMBNTS. 


STEVENS'S 
DOMESTIC    FAMILY    BREAD 

It  maJe  from  the  l>*8t  counlrv-drr^sml  Floor,  llic  (iiiMl  country-tircwrd  Harm,  Filtered 
Water,  iind  Talile  Salt,  nml  nitt  the  xmnlfml  atvm  of  nny  nth«r  jii|;m!irii(  i«  ^vrr  umtiI.  It  IB 
U|rl)tt  )*'■"■!.  uttcxcitinKt  tii^l'ly  iiutnitoua.  anil  readily  (tifrefttcd,  and  ita  awKirrftKBs  will 
IBCOMMKNP  tTSKtr  H^  vaM  of  proof  and  U*t,  B. -TKVHKt  invitet  a  fri«l,  and /ivbUcIf 
ekaUfnge*  ti  Chrmient  Analvtit  p/  the  iMUveM  tent  from  kU  EgtabluMmfnt,  uU  Of  wliicli  are 
•tamped  with  bis  natov  lu  mil. 

Address -5,  6,  and  7,   CAMBRIDGE  ROAD, 

Kbib  the  Eastibn  CouvTiia  Rmlwat. 


From  ARTHUR  H. 


TESTIMONIAL 

HASSALL,  EBq.  M.D. 
Adulterations." 


Aatbor  of  "  Food  and  tU 


Anafyst  of  the  "  Ltneet "  Sanitarf  CommiasMn^  and  Jutkor  of  the  Beporis  qf  tk^i 

Commiinou, 
"  I  harr  twice  sul>ject(d  l>ot)i  tbr  whitt>  and  brown  llrrad  maniirartured  al  yotir  eatabliah- 
mrnt  to  riiei»rou&  iiiiL-ruftrortIc  •!  and  cliciiiiCNi  an>it>biB,  and  on  racti  occisinn  1  have  ^oimd  it 
to  tie  xeniiiitr,  cur»i«ti<ii;  vniirfly  ut  wlieut  Hotir.  yratt,  water,  and  a  )itt>  aalt.  and  con le- 
quextly  nnl  cDntniuiiii:  a  particle  of  alum  or  any  othi-r  admixturr.  FitrtSpr,  tlie  Urrad  la 
care'udy  leaveneil  ami  inaitufaclureil.  in  L'(iii«e<iueii<  e  of  wbtcb,  a«  wril  as  of  the  purity  of  tba 
niiterfal*  from  Hhich  it  is  prepared,  it  is  ItfAt.  digeatible.  and  aweet  and  pleasant  lo  Ibd 
ta-ste,  like  Hoitie-Made  Uread- 

iSimtdi  *'AHTIIUR  H.  HASSALL,  M.D." 

-Mb.  E.  i'TiTKKa." 


COCOA 


Of  all  artidps  of  food.  Cocoa,  from  tb«  fact  of  Ks  being  espcniolly  the  diet  of  tli« 
Inralirl,  ahould  be  above  siupicinn  of  baring  deleU-rioun  admixturrs  :  and  jet, 
what  bare  pooplc  been  drinking  of  lato  vc^rfli  under  the  name  of  Cocoa  ?  What  is 
the  fact  as  rvrvalifd  br  tba  Analytical  SHnitar^v  Cotnmiaaioiiera  in  iliirir  analvais 
of  thai  article?  Whj',  that  out  of  the  wIidIl-  of  the  pamplee  purcha-H-d  at  the 
different  dmlcrs  in  London  onl/  four  were  genuine  ; — our»  being  the  be«t ;  being 
not  only  gi'iiuine,  out  freu  front  hunk  nod  dust,  and  prepai*cd  with  great  caro.^ 
Vide  TAf  Lancrf,  Mnj  31»t.  1831. 

Id  roosting  the  nut,  Ore  is  not  allowed  in  imirediitte  contact  with  the  ojlinder) 
but  simply  uaed  to  generate  hot  air,  with  nhidi  tlie  nut  is  roasted.  Thi»  ia  moftt 
important;  prerenling  the  nutfi  bfing  scorched,  which  is  often  the  caw  in  the 
ordinary  method  of  roosting,  rix.  placing  tlio  cylinder  on  a  coal  or  roke  6rr,  and 
thus  prcrciiting  that  rancidity,  ao  unwholesomL*  and  diaagrccabio,  and  >o  frequently 
met  with. 

Sold  in  ]iound.  half-pound,  and  qturter-pound  Pocketo,  at  Is.  2d.  per  ponnd  i 
by  moii  Grocors  in  the  Coontry  ;  and  of  tho  HonafaclurcrB,  at  the  adoreas  below. 


HANDFORD  and  DAVIS,  61,  HIGH  HOLBOBN. 

3  A  3 


ADVERTISEMENTS. 


TEiS  AND  COFFEES  AT  WHOLESALE  PRII 

TO  THK  VALUK  OF  30*.  AND  UPWARDS, 

Delivered  Currmge  Free  to  all  Parts  of  England, 


2,   BUCKLERSBURY,    CHEAPSIDE. 


liONDOli. 


TniB  KUabtishment  wAa  rommcnceil  in  the  jear  1830.     It«  BUCCKSSfUl 
PROGRESS  durir.g  90  years  has  elevated  iU  po»tiou  to  one  of  the  lATgM' 
in  the  Trade.  

Our  innin  object  ha«  been,  and  still  is,  to  supply  the  Public  on  ^TKAM 
TKKiflM,  Grcnt  and  lusiiminft  as  »uch  an  undertaking  appear*  to  be,  it  » 
obTtous  that  to  do  6US1NKS.S  ON  A  WHOLKaALE  SCAIiB  it  ia  nnnmnto 
liave  wholemle  applbnoea.  In  conformity  willi  thew  ideoa,  our  IX>CAUIT 
WAS  CUOSKN  in  a  byc  thoroathfare,  ivUerf  SPACE  and  ACCOMMO- 
pATION  am  sufHciont  to  carry  on  1>uil<?  to  any  MtenC,  but  witbool  t^ 
inerci/en  anti /ntormout  i'jp''NJ-'^  u)fi"pnra.h\\  utttwtied  to  retail  sliopa  in 
aituations,  whereby  an  dtravajKant  |»roflt  in  rcndere<1  ncxreasary. 
it  will  be  <wn  thnt  we  arc  IN  A  t'OSI'l'lUN  lo  supply  the  Public  on  thp  baM^ 
and  nioHt  o(M»iioinh'al  terniH  — in  Tact,  tu'oupply  at  Amt  taaaAt 
by  wliLch  all  liiteriiirillatc  profitiii  are  itaved. 

The  Bubioinnl  List,  aa  a  cuido  Iv  the  Publio  generally,  wc  tliink  will  b« 

useful,  and  the  qualities  at  the  quotatious  will  give  satittfaction  (o  tho  PurrfaaiV. 


BLACK    TEAS.  >■  d. 

Commoti  Con[;ou  •  •  3«.  8d.  to  3  in 
Sonnd  ConscoD  •  •  •  -  3  0 
Good  StroQif  do 8    4 

A  Koo«i  uMful  T«B  for  ManamkBl  and 
latft  ooamuntn. 

Fine        do. SB 

Fine  Sonclionic       •        -        •  -    S    8 

Vtkac  na,voor,  strDnclr  recnmmcnilM.  1 

riNfidT  PKKDE  SUUCHONO  ■        •    4    0     ! 

nUa  IW  b  tn  ytrj  hlch  irputc. 
Lapsanc  itaacltonip  4a.  3d.  to    4    4 

JtiWAt  Assam  Sowcbony  -    4   • 

TbU  Tea (tta«  Aiisal  Importadl  toMBwii 
ritnonUiury  flavour  and  nnnitfUi. 


GREEN    TEAS.  •■- 

Common  Grven    •        -        2s,   lOtLto  I 

Yonntf  Hyson  •        -3a.  9d.le  1 

Ottehaln    -  .      .  9  \ 

W«  reccmmeiKl  thts  to  mix  wUfa  Uw 
a*.  «d.  black. 
Sapfrflne  do.        -       -        .        .        .4 

FiiiF  do.  buld  l^af         -         -         .        .  « 

Fior-At 4a.  ad.  to  S 

Common  Gunpowder  -        -        .        .  f 

Canton  klud  -  8a.  Od.  to  I  4 

FtVlid...  «nmtll*ar     -         - Sa.  fkt.  w  4  • 

t-'inr  I'tiirl  lipaf  do.       -         -  4«.  ad.  M  ft 

TilK  fi.NKsrrdo.      .       -fta.  M.  10  I  • 


PURE  AND  UNCOLOURED  GREEN  TEA, 
Imported  bv  o«  direct  from  China,  in  ii«  Dnrv  <ittiXf,  and  perfrrtly  free  from  thai  arttfcMf 
eolcnrlrs  which,  after  inslyiii  hy  our  most  enitii«t>t  chcmtita.  the  irot  itttuallv  impoftedafr 
[irovrd  to  be  CO»rred  by  the  Oinirwr.  Theirforr.  io  addition  tn  our  onJinary  lea*,  «e  W 
preparMi  to  aupfily  the  Public  with  teas  lu  Ihi-ir  pure  and  uucoLourrd  state,  at  :u.  4(1.,  Sa.  ai, 
10  fta.  Od.  per  lb< 

COFFEES. 
s.  d. 


Ceylon  Coffee  -  .  .  . 
&>0(1  Ce^  Ion  f'offee  -  -  - 
Plna  Jasaaiea  (recommended) 

Fine  Plantation    .        -        -        - 


flNEST     COSTA    HICA 

t»lroti|tly  r«rnrnm«nriedl  - 
Fine  MocliK  Cuffee 
IHneat  Moetia  Coffee 


Our  CfiffM  ii  Ruattgd  by  the  Patrnt  Drtiecnfing  Proresi. 


a.  A 
OOPFBB 

-  I    « 

-  I   « 

-  I  m 


»«  respM^fkllr 


,    HsTtne  brieflr  altadcd  to  the  nrinripir  on  wMrh  we  cotMliirt  our  husines*, 
MlidCiheatient'ionor  HOTKL  KKEI'KH!^.  SCllooL'i.ai.daU  I.aKG<-,  KVl'AHLlSMMUil^ 
wlio  will  derive  considerable  adTantacrea  from  the  aboTe  arrancemmtA. 

HORNE,    ROBINS  «c  CO. 

2,  BUCEJiERSBURY,    CHEArSIDE.    LONDON, 


PURE  AROMATISED  GOD  LIVER  OIL 

WITH     QUININE. 

PERFECTLY  SWEET  AND  PALATABLE. 
Mannfactured  at  KEWFOUNDLAND,  by  Steam  at  a  Low  Temperature. 

The  QrnrnrK  bmne  ohomit^lly  CDmbined,  and  the  Aromatic  properties  diffused 
during  the  pn>ec«e  of  MBnaficture— thus  prcwrving  the  »weetneu  and  purity  of 
the  Oil— while  the  natural  fl«>hy  flaronris  perfectlj  covered,  and  rendered  palatable 
•a  an  agreenble  and  nntritlous  tonic. 

Do»e  for  an  adult. — One  teafpoonful,  gradqallj  tncreaaed  to  a  tablespoonfu], 
ttirre  (imci  a  day,  in  a  little  pnro  wnl«r  or  milk. 

Children  may  take  a  small  teaspoonful,  gradually  increaaed  to  a  deasert  spoonful, 
two  or  three  times  a  day. 

DUNCAN  nOOARTH  &  CO.,  PBorstsTOBfl. 


To  pKvent  impoattion  and  adu1t«ration  th«  Cork  of  ucb  Bottle  ia  aecarftd  by 
"Patent  Metallic  Capttile,"  with  Dirptcji;*  Uooabtu  A  Co. stamped  tbertMn, with- 
Qoi  which  none  it  genoine. 

Mjhssbs.  1IEAK05  McCCLLOCIT  A8QUTKE.  Biihopggnte  Street,  London, 

lOEIfTfl     TO    THS     C03f8ltiNEX8. 

Sold  in  Bottles  at  2s.,  3s.  6d.,  aud  63.  each. 

TESTIMONIALS. 

iRTHUR  HILL  HASSALU  Eiq..  M.n  .  F  I.S..  Author  of  "  Foori  and  iti  Adulteratki&a,*' 

■*  Adtilttrmtioiii  Drlccteil."  (kc.  ftc. 

"  I  hiTP  antlyird  KTcral  Mini)t»  vf  ti^c  Pm-p  Aroniatis^d  Cml  Ltver  Oil  with  Qalittoe  of 
Me**r«.  Duncnn  Hovftrth  *nUCo..  malw  tbcOil  with  wliicflitik  nia<te.  Thr  nainplt^  were  w- 
lectedby  mysptf  froiaalmrs^itnck  in  ffie  WMrphauw^of  Messrs.  Hearon  McH'ullorb  and  Suuirr, 
the  Bfcnts.  I  bare  fiuntl  Ttir  (hi  iis-^if  to  be  i>«Trprttv  crnuii»e  aad  ot  tbefirni  iiualitv.  bland, 
aad  etttirety  rrc«  frotn  rancidity,  an  J  the  co.i  po'ind  pi  r-|)arittoa  to  coiiiUt  of  Oil  of  th«  lanw 
quality,  holdinir,  diuoltrd,  TPry  ncfirlv  I  wo  era  ns  Qt  Quinine  lo  itie  oiincr,  ia  «ell  ■«  ■  unall 
>|uintity  ot  an  arittristtc  |irinci|ilr.  The  cufnliinatn  n  of  Cud  Lixr-.T  Oil  and  Quinine  thii*  aroma* 
tise«U  a'n<l  rarerully  manurartured  fioiu  ttie  thieal  matcrialaj  undaubtcdl)'  forma  ■  valuable 
Iberapeutic  a^ent. 

'■  B.  U.Diictt  ^Areet,  St.  Jamea*!,  Septemlier  lOlb,  isM.** 


"  Medical  Collenre.  Loodou  HoiptUI,  The  Lahenilory.  Get.  lOth,  I6M. 
"To  Meaira.  Duncan  Hofarthand  Co. 

•MJenllpnien,— I  have  rarefuliy  analysed  Che  aample  of  Arofrtaitfted  Ccd  Liter  Oil  with 
Qtiiitiiir.  and  I  And  thai  Hie  pfoprrlirt  oftheUil  arp  Miinewhxl  (leruliar.  11  bat  an  aromatic 
odciir,  and  it  tattn  n(  cjuk^tne  ao'i  vuUlUeoll ;  and  it»  reaction  with  concrntraletl  tiilpbnric 
ariil  I*  very  ren'aikable.  l%r»e  jieculiaruie*  are  Ju*  to  the  ptraenre  of  qQiiunr  and  volatile 
iiil.  both  of  which  are  iatttnaiely  rotnbmei)  with  it,  for  t)ie  •atiiiilp  of  tvriftiital  uil  duea  not 
exhibit  any  «uch  reactions.  It  cootaina  very  nearly  two  crams  nt  quinme  in  the  Aind  Duncci 
tbil  rrfimeaia  about  two  fnina  snda  half  of  the  thr>iralli9<d  tnlphaie.  It  la  my  o[»nion 
the  Oil  has  lieen  caretally  |<re|  ared,  and  Ihnt  it  runiairift  Ihtr  u>ual  cliulnic  coni|v<uii>U  winch 
are  preaerit  in  itood  Cod  Liver  Oil  \  and  I  have  no  do'ibt,  wb^'ti  iIhs  alkaloid  ta  mdic-atcd  as  a 
remrdy.  thisauitarewUlbefouiidanadranUgeouaiberBpcotLc  agent.—!  rcmiin.UcatleincD, 
voara  truly, 

•*H.  LETHEBY.  M.B.. 
L  *•  Profeaaor  of  Cbemiatr«   anil  Toiiculucy  in  lite  Medical  To'lejce  of  Ibe 

L  Ixindon  tlovpiUl.  and  Officer  o(  Health  to  llie  L'lty  vf  LAmlun.'* 

•,•  Other  TestlraOBlala  from  eminent  sclentitic  g^entleinen  msy  be  aeen  on  a|)pltcation  to 
tbe  Affenta. 

BEWARE  OF  SPURIOUS  IMITATIONS. 


ADVERTISEMENTS. 


CROSSE     AND      BLACKWELL, 

^urlicBors  in  (OrMnars  to  ^er  5Slaj«ts, 


RssrKrrrirLLY  jQvitcatteniiou  to  tlir  followinir  niCH  SAUCK9  and  CONDI SlIBNTS 
with  llie  varioni  otb«r  delicftciet  tb«y  tiave  for  many  yeutt  enjoyed  «o  liig-h  m  ^rvfttrti€»  Im, 
can  be  obuincd  of  most  resprrUble  Satire  Vrndorii  and  ItaUau  WBrphouienirn  in  the  UaiM 
Kingtlom,  and  at  the  principal  Store*  tbrou;;hoiit  the  world. 


Royal  Table  Sauce. 


A  newSnnrc,  of  a  pecotinrty  dtliclnuii  ntrd  pi'iannt  flavoHr.  0r»t  introdticM  In  IA17.  Ill 
recPlvtHJ  uuivcrsal  rotuiiicnilatioii  from  Lht*  bcftt  jmlgps,  Riid  i*  in  v«ry  ircn^ral  Mar  M  U* 
tablra  of  the  noliility,  anil  the  prinnpal  cluba.  To  thou  vrlio  prefrr  »  ricb  fiarm  «aac».  k 
may  faecoundrnliy  recominc-nilfHl  at  thf  be»t  evi-rvft  produced.  S»M  in  lioUlca,at  la.li 
ana  3s.  fiii.  encli ;  and  iu  haiidiOtne  Cbina  vaM».  to  bv  placed  on  the  tabic,  ml  Mm.  ^cIl 

Soho  Sauce. 

Tbe  flatterltiir  riTfptian  tbii  sauce  li«a  in?t  wiili  trom  the  moat  diatinruish«d  v^ctn*, 
wwranta  thr  propHt-tors  in  n^i-ommmdinff  i1  ai  tbr  best  of  ita  kind  rAtant.  It  i«  cim>|kJMi 
of  a  varirty  of  iiiirr(-dicnl4,  wliicli  arr  all  lothnroucbly  ainal)raitiat<^l  i*iBt,  wbilr  iu  pt«i^Mn 
is  extnordiiiary,  tm  dt>cidt-d  flavonr  can  he  said  tu  predominate.  For  Aah.  (raoie,  trmki,  tm 
made  di»he«,  tliii  ia  a  tnoit  dniriLile  uuce. 


Essence  of  Anchovies. 

To  produce  thii  trrll-known  oiid  jiiftlly-rstfTrnf  d  Haure,  C  and  II.  use  none  Ituf  lb* ' 
ptcke<l  Gonr^inu  Anrlioviea.or  s*hich  Ihey  ■nniiill)  iniport  larirc  quarititira  fur  thia  1 
purpose,     (t  is  ncceaaary  to  slate  IhU,  as  thr  fact  i%  noloritiiis  llint  much  of  tbe  sahCc 
anOi<r  thiik  name  ift  initdr  from  Snrdin*^.  and  an  inferior  description  of  Siciliao  fUih, 
which  purchaaers  cannot  b?  too  itriclly  on  tbcir  j^uard. 

Dinniore*s  Essence  of  Shrimps. 


Tbla  Sauce  is  of^eil  for  tbr 


inip  purpo'Mi  n«  til*?  Ktisenre  of  Anclmvie«,  l> 
irniny.     U  if   preparcil  by  i.'.  aiut  U.  ut  tlipir 


rably  mililer,  I.*  preferred  **}         . 

tbe  Kea-C'>BLt,  and  tbe  true  flavour  of  tbe  »l)niii|i  beiiif;  retained,  tbe  .Saucr 
ilelicmuB. 
It  it  an  eicellcnt  reliih  with  boUcil  and  fried  flab  of  every  deicriptlOD. 

Sir  Robert  Peel's  Sauce,  for  General  Pujrposi 

Vjirb  bottle   ia  labelled  witli  m/metimiU  of  tbe  Rlrbt  Honourable  BaronrtS  Ivtter  vf 

approval. 

Strasbourg  Potted  Meats.  J 

Thia  delirioua  prefiaralion  fur  Burpa'urft  every  dpapription  of  Pott'-d  Meat  yet  inVrMne«dC*^ 
public  notice:  th^  fluvonr  )«  full  and  rirb,  at  the  tianietitne  lieinitaoniild  and  bUr<d,  th«t  tiM 
moat  delicate  and  hstidiooa  palate  is  pleaied.    It  ii  alao  very  cuy  of  digestion,  and  adaiilcA 
to  weak  stomacba. 


&DVBATI8RMBWTS; 


CroMe  and  BlacktorWa  Sauct»  and  CondimtmU — contioaeil. 

Calves'  Feet  Jellies. 

CoMiittnror  Onne-p,  Lfmon,  Noyiti.  Punrli,  Maileira.  anil  V.ttW*  Foot.  ThFK  ire  rcrid  in 
ivemrnt  aixp<l  boHlpn.  aiirl  their  luf  is  attvixkd  witii  a  lerot  Bnvmir  ot  truultif  and  incoD- 
ilencc  ;  iintdf*  which,  Ihey  iuiun-ihc  ccrtaiutjr  of  the  Jell)  BlMftyi  being  of  uuiform  e»cel- 
ce  sad  flavour. 

Tbey  are  now  Id  ilmost  daily  coasumptioa  in  many  famUlei,  lod  are  Tcry  hiKUyapprorcd. 

Pickles  of  aU  Descriptions. 

n«  luprrioritT  of  these  it  too  well  known  and  appreciated  to  need  uiy  reiaarlt. 

Fruits  in  Bottles. 

Preserved  |>tirr  for Tarta i  availiUle  when  fresh  rruiia  are  not  in  teaaoo. 

Syrups  of  Various  Kinds,  for  Flavouring  Ices. 

Or,  which,  if  dUuted  with  iced  or  ipnn^  water,  produce  a  cool  and  rrfreshinf;  t>everaj;e. 


r.and  B.  ronnider  it  imimrtant  to  state,  that  the  whole  of  their  tnannracture*  are  prefiared 
with  thenioct  acrupnloui  attention  to  eleanlinna  and  purity.  The  utmost  precaution  ia  taken 
In  every  tnatsnce  to  prevent  cuntacl  w  ith  copper,  or  any  other  perulctouB  metal ;  and  to  en- 
•arc  thia  en<l.  tbey  have  at  a  ffreat  expcmtc  fitted  their  factory  at  ^o\kO  Siiuare  with  a  numbor 
of  Earthenware  Steam-pani,  aod  in  addition  liive  bad  a  large  Silver  pan  made,  in  which  (d 
Itrepare  the  moat  delicate  of  their  prodoctioua. 


M.     SOYER'S 
SAUCES  AND  CONDIMENTS. 

Tho  roUowing  maj  be  had  of  M.  SoTEii's  Wholcaab  Agents,  CROSSE  atiil 
BLACKWKLL.  2t.  Soho  Square. 

Beyer's  Aromatic  MustarcL 

A  moht  rxqultite  romlmiatton  of  the  rfnuiiie  Muatard  aeeil  with  variotia  aromatic  avW 
•tancea :  loflnitely  auperior  to  all  other  preparations  of  MuKtard. 

Soyer's  New  Sauces. 

One  of  a  mild  deacription  for  the  ladiea,  and  aoDtlier  of  the  aame  iSavmtr,  hat  warmfr, 
fenlleiDea. 

Soyer's  Belish. 

with  reference  to  thia  ?aace,  the  Otutrvrr  remarki:— 

"  M.  Snyer  It  n  culinary  aitiit  aa  profound  a«  he  la  vertatilr;  nolblnir  eomnanii««  to  Inn. 
No  fnrri^ti  cwfWn^rr  cvfr  tirkird  ilx- ^aion  palal«  M)  iurrr^atully.    lie  la  a  f-'  <l 

theill-fuirkeil  tnuiton  rhop«,  I'lat  loat  Napoleon  the  bitl!e  of  l-c>l,>«ir,  nould  ha'. 
very  llilfcrrni  rffrrt  tf^\rr  had  dialml  Hit*  m  up  in  hti  Ma^c  Htuve,  and  reiidfi' 
rouxbly  light  and  digeatible  by  hi«  npprtiaing  Heliab." 


WnoLK8Ai.a  Waekuocbs,— 21,  SOHO  SQIJABE,  LONDQ] 


10 


AiyVERTlfiBMENTB. 


EDINBURGH 
ALE. 


PALE   ALE, 


DUBLIN 
STOUT. 


ROBERT  MTI.LEK, 

6,  CROSS  STREET,  FINSBURY  SQ.UABE, 

Agent  to  Meeen.  BASS,  RATCLIFF.  und  OREITON,  Bre<rerv.  Bortoi; 
McMra.  ARCHIBALD  CAMPBELL,  and  C/O..  Breirers  to  Her  Majntv.  Edb- 
burgh  ,  McuRi.  A.  QUINNESS.  SON,  and  Co.,  BrevrerH,  Dublin. 

The  Pale  AJe,  Kdinbur^h  AJe,  and  Stout  of  the  aboTo  ilrma,  supplied  in  ooa- 
dition  for  present  use,  in  Casks  and  Bottles,  to  all  parts  of  Xx>ndoD  and  the  ncigb- 
bourhood  free  of  expense. 

Eprry  aUemtton  fwid  to  Comntrjf  Order*. 

A  Ui^o  fttoek  of  Ales,  Stout,  Cyder,  Ac.,  alwajs  on  hand,  adapted  for  cxpofta* 
tion  Km  all  part*  of  the  norlJ. 

mETROPOLITAN  BREWING  COIVIPANY, 

''  LIMJTKl)/^ 

CAPITAL,  tM.OOO,  IN  10,000  SHAECS  OP  £fi  EACH. 
Dtrfttort—JoHM  Francih  BnNT«MH,  Chakl»s  Hknuv  Edmanp*.  Euwaro  VavarTTac* 

Nkalb,  L.  W.  THtiniciirM,  Charlk^  Tknnant  Wklu*. 

>BaaA«r«— Thk  Loni>ok  and  Coi'nty  Bank,  Lombard  f^trfel.  City. 

A"o*icJ/or— Cmarlb"  Mo95I)P,  fo,  Moorgate  Street,  Citr- 

0r«Acr— RoHRHT  ALi.iur,  t,  Kuyil  Ejtrhxnifp  Muil<Unci,CitT. 

ttfficiiM—i,  Iloynl  KxrliatiRf  EluililincK,  City. 

.S7tfr«— IS,  Upper  WrllinRtoii  Slrret,  (ovrTit  Garden,  Vf.  C. 

Thu  Corapatiy,  Mlahlitilied  to  fxlcnd  thpaperatimia  of  the  Metropolitan   antl   Prorincial' 
Joint  :>tock  Urcmery  Cowpiny,  commenced  In  1851,  iu  order  to  lopply  the  public 
Genuine  Beer. 

The  practicv  of  sdulteraiin*  Ber  bai  h»cn  H  fully  exposed  In  the  InniUtare  and  by 
nent  scientific  prartitionrra.  that  the  public  cannot  tr  iicnorant  of  Ibe  fief,  or  of  its  Injg, 
efferu  upon  the  central  brittb  ;  andthr  inrrrasinr  inptiort  in  thia Company,  which  ia  foi  _ 
eapresily  to  lupply  tbnn  with  a  pare  beverage,  affords  aatikrartory  proof  that  with  Increcntf 
neana  ■  lane  and  profitable  irade  may  be  done. 

An  im^orttittt  nnp  feaimrt  m  tkia  Cumfnaif  ia  an  nliawancr  to  .SkarehaidcTt  «/  a  tfiac«^tf  ^ 
^i  ptr  etml.  an  all  their  pmreka-ic.  TMm  t>  ill  «»/w>  iaHy  rfnmmeHti  it  to  inrgt  e^m^mmtTK 
wkc  MW/d  thus  re<fite  a  coHniderable  banut  ttpon  tkfir  iHrMfamf*. 

Applicatiutia  rnr  tlir  Ibarra  reinaitiitiK  to  bt>  isaunl,  may  be  made  to  Mr.  J.  NawLiMo,  tkf 
Secreiai  y,  at  the  Company's  i^tom ;  or  to  Ctic  broker,  at  lite  Company'n  DOtcea.  Apptlesau 
will  lie  rriiulml  lo  pay  tlif  nuni  u(  2a.  60.  per  Share  tm  the  itbarpa  npptml  (or.  In  part  pKf* 
SMnt  of  thr  firat  rail  uf  lOs.  on  the  tiamtirr  of  Sbarei  allottxrd,  the  rrmaininic  7a.  ft«L  bdw 
payable  one  month  irom  tbedaieoraltotnicnl. 

In  the  event  of  no  allotmeol  being  made,  the  deposit  will  be  retonied  forthwith  wiQMil 
dcd  action. 

'file  fbllowini^  are  the  prices  «f  the  CMnpany's  Unadnlterated  Alen,  Porter,  and  Stoat.  fW 
VtuhMlMirrry:-  ^' 

«.    4.      *.  4.      «.   d,      9,    d,      §.  d. 

Sthomo  Alss 10       13       14       1    •       IB    pernn. 

Bi-rraa  Alks —         0  lO        l    0        14        19        — 

PoBTha —  —  —         0  10       10        

Stoot —  12        14        1    C       II        — 

TasLR  Baaa  —  —         04       0tt0t.~ 

In  BotClea  of  the  Standard  Imperial  Meaaure. 
Fef  doien  ;— QaarU,  6a.  6d. ;  Piute,  3a.  9d  ;  Half-plot*,  %,  8d. 


ADTHRTISBVENTS. 


11 


EXETER  HALL  VAULTS, 

STRAND. 


BASS    AND    ALLSOPPS     PALE    ALES, 

AND 

GUINNESS'  DUBLIN  STOUT. 


Iv  tlie  aboTA  B«Tcregea.  which  hare  been  »o  continiuUy  recommended,  and  have 
prorrd  90  eminently  benc6cial  to  thoee  who  suSei*  &om  weak  digeitioo,  PurUjf^  of 
ecnine,  is  the  great  poiiit  to  insure. 

The  ANJtTTiCiX  SiJfiTABT  C011MI8B1031  of  "  Tbo  Likcit"  hiB  proTided  for 
the  Public  a  wfeguard  in  thi«  mott  iroportjint  particular,  bmtging  to  light  the 
rarioua  admixturM  in  all  article*  of  food  and  bereragM  in  common  connumption, 
and  hare  denounced  all  those  where  adaltcration  haa  been  difloorered,  and  alio 
gJTen  publicity-  to  those  home*  where  a  genuine  article  ia  to  be  procured.  We 
ihcrefure  beg  to  refer  the  Public  to  tlie  annexed  Bejx>rt,  and  upou  ttpplicalioo, 
vQl  be  gUd  to  furnish  a  list  of  thoae  Wine  Merchants.  Taverns,  and  Uotels,  which 
are  supplied  from  the  abore  Stores  in  Casks  and  Bottles. 

DAUKES  AND  RODICK. 


BepoTt  of  the  Analytical  Sanitary  Commission  of  "  The  Lancet,** 
ISth  May,  1854. 

"ANALYSIS" 
FROM    THE    STORKS    OF 

DAUKES    AND    RODICK, 

3,  Exeter  Street,  Strand. 

"nie  prodaei  of  Malt  and  Hops,  and  the  constitoeota  of  pure  spring  water 
Bot  any  other  kind  of  ingndients  found,  either  organio  or  inorganio." 


12 


ADVERT  1 8CUENT8. 


BASS'S    EAST    INDIA    PALE    ALE, 
BARCLAY'S  PORTER  AMD  STOUT. 

In  IH-Galion  Ctuki.  Bottha,  nuIf'hottUn^  and  Imperial  PuU*. 


BERRY,   BROTHERS,   AND    CO^ 

3,  ST.  JAMES'S  STKEET,  LONDON,  S.  W. 

SOCIETY   OF   ARTS    PRIZE   ffllCROSCOPES. 


R.     FIELD     &     SON 

Continue  to  manufacture  their  MicroBCopes,  uiuTcr«aUjr  acknowledged  the  I 
ever  mode  for  the  price. 

Compoiintl  Acliromatir  Micro!»copc,  with  Two  Objective*  and 

Two  Eve-pieves,  Condenser,  Slo.,  in  Muhogau^  Cabinet £3  S  0 

Ditto,  larger,  No.  2 4.  10  0 

Ditto,  larger,  No.  3,  with  Three  ObjectiTM    6  10  O 

Ji.B.  These  instruniunts  are  Mpedally  Adapted  for  detecting  ■iluUnnitifTg, 
are  recommended  b;  the  Apothettriea*  Coaipanj. 

113.  NXW  SritlBT,  BlBMIXOUAM. 


1.  PILlEiSGHER'S  ECOKOffllCAL  niCROSCOPE. 

For  which  a  Prize  Mn-dal  luas  bueii  uwnrUetl  to  him  nt  the  rariaicn  £xhibit>9il, 
1855,  eonsi^ta  of  a  firm  Stand,  free  from  TibratioD,  having  course  and  Am 
Adjustments,  an  cillfit'nt  Stage,  with  DiaphrDgtn.  one  and  one-quarter  iiioh 
Object  Gla^sen,  the  formrr  Iti^  and  the  latter  75°,  augtdar  Aperture,  an  Kj9 
Piece,  and  a  Mahogany  Caso.     Price  £7  7s. 

tiABaER  HIOHOSCOPES.  of  most  elaborate  workmannhip,  and  evovy  modflra 

improTcuieot,  at  equuU}'  moderate  Prices. 

*a*  ifiero4copie  PreparAiioM  m  ffteet  waritty. 


UAVUTkCTUUMR  0» 

PHOTOGRAPHIC  APPARATUS.  AND  EVERY  OTHER  DESCRIPTtOJ 

OPTICAL  INSTRUMENTS. 


A  List  of  Prices  sent  free  on  application  to 


ABVBRTISKMENTS. 


SPECIAL  NOTICE -THIRD  DIVISION  OF  PROFITS. 


13 


THK  unusual  succcas  which  has  nttcntled  the  cautious  yet  energetic 
operation*  of  this  Company  Itfts  enablod  the  Director*  to  odd  lievcnionuy 
Jionusea  to  Polieica  on  tlii'  pa rticipn tins'  clftS9,  areraging  nearlj  2  I>^r  cent,  per 
■nnum  on  tho  eum  insured,  or  frum  30  ^^  100  pci*  (^"1-,  ou  tbo  Premiumi 
paid. 

Part  ii-s  iniuring  with  this  Compinj  do  not  incar  the  risk  oF  Co>piirtnonhip,  aa 
ta  the  case  in  Mntual  OffloM. 


Est ahlviked  nearly  a  Qnarter  of  a  Cmtury. 


AWWCAI.  I^'COSIE  VPW^ARDS  OF  £13!H,000. 

The  Fund*  op  Property  of  the  Cornpinj  as  at  Slit  December,  1855,  amounted 
^  £566)124  2b.  Gd,f  invatod  in  Qorommcnt  and  otiier  approved 
Securities. 


Itnitctr  pingbom  i^ifc  f^ssuraiuc  Compann, 

8,  Watkbloo  Pi^ce,  Pill  Mali.,  Londom. 

CHARLF^  DOWNES,  Esq.  Chairman. 

HON.  FRANCIS  SCOTT.  MP,  Vfpvfy  CSmirmMm. 

A.  n.  HASSALL.  Ekj.  M.D.,  Physician, 

8,  Bennt'tt  Street,  St.  James's. 

(Bj  Order),    P.  MACINTYRE,  Secretary. 


CHRVATtTRE  of  the  SPINE. -SPINAL  STATS.— Of  all  the 
Supporti  yiUWh  ihe  MnrUanictRn  bis  contrived,  thit  's  one  of  th*  mo-*!  iniportant.  By 
tlir  linirly  uppliration  nf  Kailrv'm  Lioht  SrrrtAL 
9iiFfonTKN»,iii»iivyonnyperton»hsvolif«i  rescuetl 
fnnn  that  wntmt  nf  ill  <uiiiplaintt,  Oitisuniplian. 

Pktirtttft  from  tit'*  C'^iiDln  crtii  Up  iirrommoilsl«d 
St  Mr.  Itailcy'fi  I'nvBi*-  K-diiMitlintrnt  n^ir  lx)n«1on, 
wi  llmt  )if  rtmy  (N?ru>f>«lly  supvrliitetid  the  sppliri- 
lioiiuftltc  Inatfuiiirnt. 

Bxprrienred  Fewtatet  in  attfUftaHee. 

ELASTIC  STOCKINGS,  KNEP.-CAP9,  anb 
SOCKS,  for  Varicose  Vrhis;  TriiMi>«;  Knifmsi  or 
every  ileacription ;  Sptintt.  lUiley'a  lllu-tnt«<l 
f'«tal'»guf,  containiin  «  l-Ut  of  e*ppy  clc»rnption  of 
Siir/iral  liitlriitnrnt^  u*r<l  liv  n  Suprf"",  iiirluitin; 
Miiiwifrry  F«irrcp«,  I'lHikrt  ('aae  liiktruwrntt,  lt£., 
may  be  bad  free  bpun  appllcattou. 
Befort  Treattneot.    After  Treaimvat. 

W.  H.  BAILEY,  418,  Oiford  Strwt,  near  Solio  Square,  London. 


ADVBwrioiESires. 


SOVEREIGN    LIFE    OFFICE, 

49,  St  James's  Street,  London. 
ESTABLISHED      1845. 

fruslcii. 

B.  BOXD  CA.BI1ZXX,  Kk].  M.P. 
Hbnbt  POWWAIX,   £•<). 


The  Earl  Txlbot. 

Sir  CXAUDB  Scott,  Bart. 


Tlie  lut  Bonus  added  four-fifthA  of  the  Premium  p&id  to  Mine  of  lh«  pufia> 
pating  Folioie*. 

ProTtsion  can  bv  made  for  tlio  payment  of  a  certain  lum  on  attaining  mnj  fifca 
age  (aa  50,  66,  or  60j,  or  at  death  if  it  occur  previously. 

By  a  small  annual  payment,  £100  inajr  be  aeoured  to  a  child  on  mttMaiag  tfas 
age  of  14,  18,  or  21.  H.  D.  DAVKNPOKT,  SetrtUrj. 


J.    H.    SANDWELL, 
OPERA  ANB  RACE  GLASS  MAEEB, 

9,   WYNYATT    STREET, 

GOBWEbL     ITREET     ROAD,     B.  C. 

PRIVATE    WORKMAN. 

OPERA  AND   RACE   CLASSES    REPAIRED   ON   THE  SHORTtST    NOT1CC. 
Optitial  TuMlntmetita  o»  RfOMOHiibU  Terms. 

PLUMBE  S  GENUINE  ARROW  ROOT, 
Is.  6d.  per  lb.. 

Should  be  used  in  preference  to  any  other,  being  considered  hy  the  first  &Iv01eal 
Men  in  London  the  best  imported ;  their  Ti'»timoniob  aceompanjr  each  Packet* 
which  is  signed  \.  S.  Plombe,  3,  Alic  Place,  Great  Alie  Slivet,  Loudon.  whvsU 
can  be  obtained  Wholesale  and  Retail. 

Sold  aim  by  Skow,  Paternoster  Row;  J.  K.  Fokd  and  Soy,  l4UiigCoo; 
WnxiAMB,  Moorgato  Street;  Mobgajv,  Sloeno  Street;  MsDjta,  Camberacfi; 
Whittikohav,  39,  Piccadilly  ;  Pavltok,  Uackneir ;  Elus  and  Llotd,  72,  5ev- 
gate  Street ;  Udopeb,  London  Bridge  ;  Stkoud,  Blaokfriars  Boad;  JirfBisol. 
Stoke  Newington ;  Bkale,  Mission  HousO)  BtomJleld  Strvet ;  Weathkbxt, 
Peckham  ;  and  olber«. 


i.v*:  MENTAL  i!::n.w 
.  ..;.'o::d  rrrosiTX 
:..  pa:v:u!?  drive 

f /vLO  ALTO,  CAUf, 


N^ 


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