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HP MS sm15a19a.d: 


Medi ,i/13522/1T3522/sm15ai19a.d 
11-MAR-96 14:55 


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File: /chem/msdi.1 
tion Date: 16-SEP. 


AD 


CAML 


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scan 
hem/msd1 . 1/sm16.b/sm16009a.d 8 
16-SEP-96 20:27 


HP MS emi6a09a.d: 4,990 to 14,984 Hin 


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<i— ner 


<— DT 


2.0 12.5 13.0 13.5 14,0 14.5 


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m16.b/sm16a02a.d bi tao 
17:15 


HP MS smi6a02a.d: 5.012 to 15.006 Min 


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(Maisie les nies \e) || 


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b 


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Data File: /chem/msdi.1/em16,b/sm16a30a.d 
Injection Date; 07-OCT-96 18:33 


HP MS emi6a30a.d: 4,990 to 14.984 Min 


ze DET 


nun 


nino 


Y 


(1076) 
BAO PMA A SAS mnc mon 

tS 

mn 

Cs | 


Min 


rf eee Se SS ®) ee 


S10 S'S 610 615 710 715 B10 BLS 9:0 9.5 10.0 10,5 11.0 11.5 12.0 12.5 13.0 13.5 14,0 14.5 


! ABC 


Data File: /chem/msdi.1/am16,b/smi6a30a,d 
Injection Date; 07-OCT-96 18:33 


FP WS emiba30a.d: 11.017 to 13.997 Min 


(wet) || Oet) | 
ee) oe 


(x107*5) 

BRE NNNNUUUUSs sean 
sumeonuaonuaonuae 
> WS 

= 

5 

a 

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——— 


12 NU anee : 


2 11.4 11.6 11.8 12.0 12.2 12.4 12,6 12.8 13.0 13.2 


13.4 13.6 13.8 


HP MS smi6a30a.d. Scan 564: 11.772 min 
1.2 j se 


p86 


on 


Ore ee ENN NANNY UU 
: 5 ene 


S 
MI 


0.2 
| 7 
j 132 
o.1 
iy j BBS 5 25G. 21 367470 
plural Woe Wares) AWE ine ee al 
50 75 100 125 150 175 200 225 250 | 
m/z 
HP MS emibas0a.d, Scan 598: 12,229 min ] 


6 
A agke 
\@ 2.2 
| 2.0 
Xai: 8 
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4 

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K oe AB | 
| 0.6 | 
| ' 

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144 

) O.24) | LL | 216 229 316. 
ae Se ae Oy eer es pee ae 


50 75 100 125 150 175 200 225 250 275 300 325 350 


HP MS smloas0a.d, Scan S22: 11.208 min 


2.14 13077 
| 2.04 | 
ae. | | 
} 1.8 | 
|| sehsee | 
1.6 | 
1.5: | 
Ite! 
| tee 
1 
Sitses 
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|= 0.9. 
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| o¥e. 
0.6 7? | 
| 0.5 } 
} 0.4 160. 
| 0.34 | | 
| 0.2 ) rf 219 26 33 362g0 | 
0.1 S 
0.0 sbi alll stub aa ets adits nth baat omnl 
| 50 75 100 125 150 175 200 225 250 275 300 325 350 
P mn 622; 12.551 
| i HE MS eni6as0a.d. Scaq 622: 12.551 min | 
8. 


bono 


nam 
m ¢ 


me 
4.8 | 
4.44 | | 
4.0: 
3.64 152 | 
2.84 | 
2.44 

| 2.0 | 
1.6 56 128, 

| 1.2 | 

| 0.6 
0.4 
0.0 


HP MS smiGa30a 
| y 7143 


| 


d. Scan 627; 12.619 ain. 


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Uusseauna 


Y 
soo 


200 | 


115 


ood sda RITES or Sere om Sax SINS 


50 75 100 125 150 


175 200 225 250 275 300 325 350 
sich, MS smi6a30a.d. Scan 670: 13.197 min 


bKeNN ND 


ym 


183 


r] 


280 


ihn tt ca be cores 


foi | | 
AM ata anda adadte se elongates 
SO. 75 100 125 150 178 


1 175 200 225 250 275 300 


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af chem, 1/emi emi6a35a.d 


36a.d 


di. 1/9m16.b/sm16: 
OCT-96 18;08 


HP MS emiba36a.d; 4,99 


9:5 10.0 
Hin 


9.0 


tion Date: 14-OCT-96 17:48 
. i HP MS smi6a35a.d: 4.997 to 
4.4 
4.2 
‘ be) 
3.8 i 
3.6 
3.4 
3.2 
3.0 
8 
2.6 
o 2.4 
A 
1.8 
1.6 
1.4 
1.2. > 
Mg fies 
0.8: c 
0.6 
0.4 \ 
ig Saree rer eens = eps Ses See ee K A NLA 
5.5 6.0 6.5 8.5 9.0 9.5 10.0 10.5 11,5 12,0 12.5 13,0 13.5 14.0 14.5 
= oo er ee | - eS. = — = 
eee: HP MS smiga35a.d. Scan 673: 13.018 min. PS anidelseld. Sean 7e0r Tac 
| | al - 1147) 
4.24 | 1.6 
| 
4.0 | 1.5 e 
3-8 | 1.4 
3.54 | 1.3 
3.24 | 161 1.2 | 
Pi es S - u _ a 
ets G-Neo-WvPT | | i S-Vad- Die T | 
| 2.8 
| | 1.0. 
eee! | 
Bo | = 0.3 
52-2 | ie AR 
20 | || [eos | 
eB | | |= 0-7 7a 
1.5 | ~ 0.6 
1.2 | | 0.5 | 
1.0: | | 4 
7 | 117 | 
0.8 | | | ereess 160. 
0.5: | | 232 | 2 | 
0.24 I | | 219% 1 3 | | i 
0.24 || 21%, B16 33.469 | = = = 
<< || 1 188 257 274 33867 
eal in eee @ eae SWees| ret: g 
== aE Fy TS Sh BED Ea os 3D 0 -0- 2 = ey = — 
So 75 100 125 150 175 200 225 250 275 300 328 35 2s 150 175 200 225 20 27s 300 305 50 
| — {HP MS smi6ai5a.d. Scan 703: 13.409 min. FETS ealeain a Scan 750 TOS a ; 
3 it 
1.6 | 3.8 
1s | (ASy A) Se Cd) 
| | lees | 
| | 3.04 
| | 2.84 
oe S-Meo-Te “2 i 
| eae 
| | Ris | 
| & |P 2.0 
| we. 2 1.8 
| | | 2 tas 7 
| maa . 
| | 1.2 | | 
| | 1.0 
. | 0.84 
I as | 64 160. 
| 0.24 160. P | 0.6 
1 oa i | alas 355, ass | es | 21% 27a 275 3az0 
ane iba otal aie We et _ ~ | ang im | | iJ I ‘. diiaa 
50 75 100 125 150 175 225 325 350 = | —_ = a i a = 
oo a es = = 50 75 100 125 150 175 200 225 250 275 300 325 350 
- L n/z 


oA pus & 5 WH N\LO - 


(10°6) 


HELMS smioasea.c 


114- 


Scan 


765 


=a | 161 
ie | 
) 6.8 | | 
6.4 
6.0 | | 
5.6 | | 
5.2 | | 
4.84 | 
4.44 | 
4,04 | | 
3.64 | 
\> 3.2 
2.8: | 
| 2.4 | 
| 2.0 117 
| 4.6 | 
1.6: | 
xed 21% 232 
ee \, | | | 279 35t_ 370 
° | : 
0 Watt wud ee lle ateaihhesiad ~ os 
50 75 100 12 150 175 200 225 30 32 350 


| 
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1 


Injection Date: 


le: /chen/msdi . 1/06 
06-OCT-97 


7 .b/em18a87a.d 


Ss > ———F# WS enibaG7a.d: 4.136 to 16.706 Hin 7 ven HP MS eniBa67a.d: 7.995 to 11.932 Hin 
7.8 | 
3.4 
a | 
7.04 3.2 
6.8- 
6.5: 3.0- | 
6.24 
6.04 2.8 | 
5.8: ~ | 
Re 2.6 
5.25 2.4 
5.0 
4.8: 2.2 
4.5 
4.2 _ 2,0 
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g 3.8 <a 
x 3.5; ~ 1.6 \ 
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3.0: 1.4 i) 
2.8 ww 
2.5 ‘ W 
2.2 
2.02 1,0- 
1.85 
1s 0.8 
1.2: 0.6 
1.02 = 
0.8: 0.4 
0.5- | 
oe ee a ae cea ae = a PEWS Sicitig asSignah sigh ©. re es , | 
5 é > 8 3 10 ‘1 12 3 14 ts 6 810 6.2 614 8.6 8.8 9.0 9:2 9.4 9.6 9.6 10.0 10.2 10,4 10.6 10.6 11.0 11.2 11.4 11.6 11.8 
— = Hin = te eee < — —— he - = 
HP MS snlGaGva.c. 5 5: 5 min HP MS smlGa67a.0. Scan SM: 6.553 min = a 3 0.662 
po = smi6a873 Scan 386: 9.306 mi a smi8a87a.c. Scan 335 WS salGad7a.c, Scan 88: 10.662 min 
4.24 1. | call 
4.0 | 
3.8 o. 
3.6 0. 
3.44 0. 
3.24 
3.24 = 0. 2 
|= 0. | 131 be \- 25 
3-0} ls o | pS ts 
2.84 ree. | a! > \S 
|} 264 | ~ 0. | |= | 264 
= | 26+ = — 
j~ 2.4 7 ~. > 
Bee | : HI 
Ss | 0. | | | 
$2 e 314 
= 1.84 y wh | hie 
> 16 | o.oamet A a al ib Bed sins ah ab cnn a i ier so ee bd 
1.4 cel Sis Meet eet eee We See) eee ee 125 150 175 200 225 20 275 300 325 350 
1.24 He MS smiGae? Sean 337270 653) ain — 
oy | , a ea ae = Average Spectrum SOS to 10.623 min 
0.8) 8.07 = 
0.6} ? a 
0.44 | vf of see 7.01 
0.24 | 165 215 264 306 33 04 == eal | 
o.otib tuba tts = wee =i H 31 6.0) 225. 
50 75 2 150 275 300 25S - = = 
30 = 15 2 =| °] a 5.04 3 
— | 4.04 isenet 
| = 4.04 
o = | 
264 , 3-04 264, 
2.04 = 
1 | i 
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F l Lagi fiat \ 
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| So 75 (100 125 15 ae 225 0 275 3 so. 75 125 15 
326: 6.533 ain. (DIF HP NS selGa67a.c. Scan 468: 662 5 DIFF 
8.04 7 
| | 
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le 5.0 
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=10°6) 


HP MS smi9a35a.¢ 


Scan 317: 8.667 min 


“1074) 


eceooo ore ees 


5. 
Ps | 
| 4: ai 
| 
4. 
| 4 
|) 3: | 
sm19335a.d \ ASP 3 | 
nn si ae “GBT ghd + he” N39 zy | 
<== HP MS smi9a35a.d: 4 asso —y. a | 
1.3 A es | | 
(C=) [Sites | 
j= < 
1.2 E 2 
t a 
1a Wo 
(fy) 
1.0 z 
9 ° 1) ee ae 193 267 281 355, 57 
° (@) ch Aly Ti Se ea e- 
: | 50 75 100 125 150 175 200 225 250 275 300 325 350 
0.8 we 
| HP HS smSassa.c. Scan 452: 10.582 min z 
ou / e 
0.6 \ 0.34 207 
™h 
i We 0.84 | 
ss hd, | 
0.4 [ 
ae 43 
02h A a 
ray nel arm ym annientine cl nyatal Nonicrvat yriaelow ; 
415 5:0 5.5 6:0 6.5 7.0 7.5 6.0 6.5 9.0 9.5 10.0 10.5 11,0 11.5 12,0 12,5 13.0 13,5 
Se fee eR ES) \\, ED z See TRe Eee 
281 
267 355 370 
5 eae = eeeever eer a 
175 200 225 250 275 300 325 35 
d, Scan 495; 11.191 min E 
| 
| 
| 
| 
DSwALe eB O afer 1S Ry i> | 
\ > @: ro | Ke: 
0.85 
0.6} 
© 4 | a 235 281 
ltd = 
| o.otdd. BV eran] Coonernees eae eee 
| 50 75 100 125 150 178 200 225 250 275 300 325 350 
RA 
HP MS emidaa7acd | eee HP MS emiSaa7a.d. Scan 331: 6.668 min 7 
| | I geges |] eg 
| s.o4 | 
| | 7.64 | 
| | | 7.2} | 
| 6.84 | 
e-4| 
| =a | 
5.64 | | 
| 
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1 | 135 
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0.44 Ht | x 
ae | Fey ee eee ea ae 
u BS tie i ani cara eer ao he | 50. 75 25 150 175 200 225 250 275 300 350 
Min a 
EERE Senne RETESET ; | HP MS smig G. Scan 472; 10.581 min 
8.0: | BA DOT | E 
7.6 13 


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Data File: /chem/modi .1/04May1998,b/am19a55a.d 
Injection Date; 04-MAY-98 15:08 
aie: in "HP WS ami9aSSa.dn 4,136 to 16.701 Min oe age 
} 
1.6 Uh 
1.7 
1,6- 
FL 
1.4 
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0.9 
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0.6- (> \ 
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one rea pene lh ayer ner sais BPE Oe oO, edi ites anor) aay Ness. 
6 8 : 1c 11 12 13 14 15 16 


HP MS smi9a55a.d. Scan 573: 12.034 min 


Oey 
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re) 


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N- he - S-G40-T 


an pe ere er men wer 


ttl | a ae 


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h -74ah: Saget wn | ww ar rmnne 


700 min 
2.502 min 
+ 
-041 min. (DIFF 


13.084 min. 


n S56 


Ne 


‘wre 


avy 
snida 


Sean 579: 2 


Sa73a.d 


Scan 
212 
HP MS smlSa7la.d, Scan 633: 1. 


HP MS sm19a72a.d. Scan Et: 12.50; 


HP MS sml9a73a.c. 


AP MS 


0 -0-LdL cde disoabe tbh 


6 
3 


JIM 666°GT 93 gff'¢ 


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MIN B02'9T 03 ger'p u ‘9 ° 9 91 P'ecves 
= u 
UIW B02'91 03 ofysy MIN BO2*91 09 ofp tp “IW B02*91 01 gy 
ee = “IH 802*9 SEI*b  tp'eevecrus 


njection Date: 13-JUL-98 17:5 


4 

7.0 

6.8 

6.6: 

6.4 

6.2 

6.0: 

5.6: 

5.62 

5.4 

5.2 
8 
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3.4 Z 

3.2 0 

3.0 F 

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2.6 2 

2.42 2.2: 

2.2 2.0- 

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a. \ “a 


hem/mad) . 1/13Ju11998,b/em19a66a.d 
54 


ee = _ - = —TP MS smiSaGéa.d: 9.057 to 11.067 Min 
HP MS emi9a66e.d; 4.136 to 16.702 Min 


\ 
df ga phicnionypntmaertt 
10.8 11,0 


10,6 


| 


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125 150 225 250 275 300 325 350 


i 
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t | 264 278 350. 368 
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aor itu) 
25 HRB-PRULYL-NDNA 


i! 
SLYL-MDMA 1 
‘ 


NaHCC 


~MDMA Ft? 
mcm le) ee eed NUM 
fiw (tint 2 Leg i VNVGL2d 


ML, DMAP 


32 MIPT UR 
33 PRYIDINERETIC ACID B 
zd Ok CAP PLANT NICH 


}VINERLEI 
QIDINE ACETAMIDE ({MARYBE) 
SIC ALKALO]N FRACTION MATUCANA MANTSANTI 


2S J Wsik 
40 BASIC ALAALUIL JANA GLAUCA ex 
41 NICOTINE 

CHN/Me2S 


Peon re f IPTV 
SLL \ Web dts 
44 METHYLATED T FUR RETENTIVN TIMES 


REPEAT 


ha 1 bir 


Ac narcenrciice 
Th Wis Wk 


WL 


DVETHYL WR 


VW Sv) hog a eee 1iCLTe oD 


t fe 
. 


7 


Yaitlbn tas 


Wt 


ri ee 


mF 
ebb YS 


OH Jang 


c 


(HE-TAHLAWIA-2°T-AKOHIAWIA-2°Q ShT 


4 ZUN-US 4d 
oUN-S ay 
MAY MAN TM 


riot 
2 


TH WOM4 St 1 


» 
' 


oy MOLL 
oh MUL LIHd4 NOLASLL iz 
W9bT# 3NY-OH 
ACh 3NF-rlW 


ni 
See Us) 


UIAv ett tl 


SN(OL 1S WHS AKLSW-f -- SN iWiL 
“O"d -- SNIWIL 
JH =| -ASHA MM 


SN Ie 


“hit 
Le 


Anas SWidi 


on 7 f in 


ons te Ln 


HLNAS 20-3 [NYON 
IH1FH NYY HEN HEA TODATI/SAEYAdA-Ad 
U 


SULRUds Ad 
90-4N [109 [NAOM 
3S4H~3N (WH 


NAG 


Jane mise 
wrk mL 


“O"N 30 NOLLYTAHLSW NAAT 
FIMNTIQTIN VAHL 


SN(UL 
IN IOL 10S WSosdAH30 10 
(MHANHIS AQtWHNT | 


1onf 
1 sk 


t- 


WY "IU WOYs SLYALSANS 90-3N1LOIINAON 
AMHANHIS 3 


, Wt 
aut 


JiLSHLAAS ~SUTWHNT LOST 


eek lowe 
= —————— ene 
uy eae ee ive eee MM aetat LM 
Ree: sk er 
mn \ é | bs = a4 | | 4 
149 | [ (o i | 
(te | | | 
| | | 
| | 
{ | 
& is is is i _ 
. MS : m™ WS fi 5 Wr< im Ms 
i ieee | 2 (2 ) S re 
le: ee VG = 
| re 


a T io 

aA ISS) Aras @ 

ean et aaa | ee Bae Blin 
207 hon se ie 
\T%G QP| 


197 193 
gos 


| 


Pipe. : 
75 §-ATLAS 2 Crneha. 
ATLAS We | 


pan 
Arty 173, \18 


a de i 
D HS Fla 4 > 
4z Se a eee 

= ——— 


\ 


SN 


tes 


wi 


; 


J 


( W)] 
ees (B0y ~ wt Ow = co Ic 
eeeee Ob) T- Wu dW et Cw) oe led ap ¥ tf 
Bae 2 z elas jee y- Wwe “o_o MLE Up | 
eas Ss Cw Vv -A QW Wy) yp -WWaw | ey ~ acre L ; - Je 

(yi Xe - HA aw ae | © gam >-vuwd Bh, 
— wT) (snl 2-YuGw | Ly) ¥ -dAWC le 
| é “Dov wo 

ee H9Lie ylife Ly 14) 7 
b\ | Ne 

) \ 


ty \| 
BI \ 
ey 
ak 
fos) 
= 
z 
S 
— 
=x 


eS ] 1 
ee bo Ne 
a errereey. ror | Ga) t-wwwa Fe 


ba UNS |) P 
pea &@ OD : 
\L-2 SY COW ap Vom ) I> 
802 (i Bi hee eae ce | ao ae npr V2AWd § 
Ez care 2 if 
vee ea | HE am -L9 my om LY | |i 
4 pasa | 

py SAAwn t vy NOW - 22 >) wm °5 a 


Oy 


wy 


™ A f 
ae MeN AD © 
. ie. v eee = Toate oa 
63 i 4 MA N\ \ H I 

=a dhe A = Crown 

ipa eat: Jou 144 

Ao 

(0 ‘| 


A Be 
Rie 
<e = Z T 12) 
MLAS @Q3} ATLAS By = Arias &) 
/ BRN Wile ce es |p ” oe 
ra oOo 143 Pee 
Rel gos 
is 1B ws 4a ee ¢ 
| 20 \ IGA aor 


| Sar pmmGla 
i) MLASQ) (17 


MLKSQ4) 


\q 


PALE -tm man 


14 M\ 199-201 ¢ 
Moy 


MA 4ecier)\ aay San | MM lor-204 GF 


| mu) 0) 


hea Mw 22. 
cr 

yea = 
e 
a ee 7 
a ¢ 
49:53 

SS) ae) on 

& £) 

‘ eo Ie 
REgE 


Sorte cemnetane mereerees 
y pegs ' 


Me 
Mare 
vevieer 2 oulthy. 


er ee uae 
~ ae woe 


one agp ORE 


mcpere dig, NT 4 os sae z J 5 7 : a < -- ee 2 2 
pa tetegn 1 (Me regs aah 2 “5 } 5 ‘ : Z ts ie : 5 : ames J exe ; 
¥ » ‘i e be ~ ae a * * ; ~ - z 5 > ms n= ~ Yan % es re 
i 4 - Ate poe ; ip ‘ - Z : See are z 
2 f : 2 7s ey spn ibe Pair ie - Jan re 
wee - & * 2 > = a a . . : 4 . r +
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