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UNIVERSITY      OF     ILLINOIS     BULLETIN 


Vol.  HI 


AUG.  15,   1906 

[Entered  at  Urbana.  Illinois,  as  second-class  matter, 


No.  22 


FUEL   TESTS  WITH   ILLINOIS   COALS 


L.    P.  BRECKENRIDGE 
S.   W.  PARR 
H.  B.  B1RKS 


BULLETIN    NO.    7    OF     i      '      ] :"     VERSITY   OF   ILLINOIS 
ENGINEERING  EXPERIMENT  STATION 


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UNIVERSITY    OF   ILLINOIS 

ENGINEERING     EXPERIMENT    STATION 

BULLETIN  No.  7  AUGUST  1906 

FUEL 'TESTS  WITH  ILLINOIS  COALS 

BY 

L.  P .  BRECKENRIDGE,    .     .     PROFESSOR  OF  MECHANICAL  ENGINEERING 

S.  W.  PARR, PROFESSOR  OF  APPLIED  CHEMISTRY 

H.  B.  DIRKS, ASSISTANT  IN  MECHANICAL  TECHNOLOGY 

During  the  last  ten  years  a  considerable  number  of  boiler 
trials  have  been  made  at  the  University  of  Illinois.  Many  of  these 
have  been  made  under  the  boilers  in  the  power  plant  of  the  Uni- 
versity. Still  other  trials  have  been  made  with  boilers  in  use  at 
the  plants  in  neighboring  cities.  In  some  instances  experts  rep- 
resenting several  special  stoker  and  furnace  companies  have  been 
present  at  these  trials  and  operated  the  devices  in  which  they 
were  interested.  For  the  most  part,  however,  the  tests  have  been 
made  in  order  to  instruct  students  in  the  usual  methods  of  boiler 
testing,  and  the  boilers  themselves  have  been  operated  under  such 
usual  conditions  as  happened  to  obtain.  In  some  of  the  earlier 
tests  all  of  the  data  relating  to  the  heating  value  of  the  coals  were 
not  obtained,  and  for  such  tests  several  items  depending  on  these 
values  are  necessarily  omitted.  While  in  most  cases  these  tests 
have  not  been  made  with  the  object  of  making  a  comparison  of 
coals  or  of  appliances,  nevertheless,  it  has  seemed  wise  to  publish 
the  results  obtained  and  also  to  exhibit  these  results  side  by  side 
as  they  apply  to  various  forms  of  furnaces,  types  of  boilers  or 
kinds  of  coal.  It  is  entirely  probable  that  the  results  obtained  are 
equal  to  those  generally  obtained  under  the  varying  conditions  of 
plants  using  Illinois  coals.  Many  more  boiler  trials  have  been 

159348 


2  ILLINOIS    ENGINEERING    EXPERIMENT    STATION 

made  than  are  here  reported,  but  only  such  are  included  in  this 
report  as  appear  to  be  free  from  any  indications  of  errors  in 
methods  or  results.  For  the  purpose  of  this  bulletin  all  of  the 
results  of  the  tests  have  been  carefully  rechecked. 

The  work  of  the  department  of  Applied  Chemistry  has  not 
only  supplemented  the  work  relating  to  boiler  trials  by  furnish- 
ing the  composition  and  heating  value  of  the  coals  used  in  these 
trials,  but  it  has  also  examined  and  tested  a  large  number  of  Illi- 
nois coals  not  yet  tested  under  boilers.  In  connection  with  this 
subject  this  department  has  perfected  several  new  devices  very 
useful  to  chemists  and  engineers,  designed  for  making  the  ordin- 
ary determinations  of  the  heating  values  and  composition  of  coals. 
The  Parr  calorimeter,  one  of  these  devices,  has  found  ready  sale 
among  the  operators  of  many  of  the  power  plants  of  the  country 
as  well  as  among  the  consulting  chemists  and  fuel  experts.  It  is 
expected  that  a  separate  bulletin  will  soon  be  published  setting 
forth  in  detail  many  of  the  new  methods  which  have  been  devel- 
oped by  this  department,  and  giving  the  complete  results  of  its 
investigations  relating  to  Illinois  coals.  It  is  hoped  that  the 
tables  of  the  chemical  composition  and  heating  values  of  Illinois 
coals,  which  form  a  part  of  this  bulletin,  will  furnish  engineers 
and  manufacturers  with  useful  information  in  this  important  field. 

With  the  above  somewhat  general  statement  in  explanation 
of  the  character  of  this  bulletin,  it  may  now  be  advisable  to  refer 
more  in  detail  to  the  special  features  which  are  intended  to  be 
brought  out  in  the  following  pages. 

BOILER  TESTING 

For  many  years  engineers  have  been  making  "boiler  tests" 
with  the  object  of  finding  out  how  many  pounds  of  water  in  the 
boiler  could  be  evaporated  with  one  pound  of  coal.  In  order  that 
the  results  of  the  tests  might  be  comparable,  it  became  evident 
that  some  common  method  of  making  tests  should  be  agreed  upon 
and  also  that  the  tests  made  should  be  reported  in  a  uniform 
manner.  A  committee  of  the  American  Society  of  Mechanical 
Engineers  recommended  to  that  Society  in  1899  a  method  of  test- 
ing boilers  and  also  a  method  of  reporting  such  tests.  These 
methods  have  been  largely  used  since  their  recommendation  at 
that  time.  The  many  expert  engineers  who  are  to-day  so  familiar 
with  these  methods  will  probably  not  be  interested  in  the  pages 


PARR  AND   DIRKS 


FUEL  TESTS    WITH  ILLINOIS  COALS  3 


immediately  following.  Having  in  mind  the  owners  and  operators 
of  power  plants  as  well  as  manufacturers  and  young  technical 
students,  it  has  seemed  worth  while  to  present  somewhat  in  detail 
the  following  subjects: 

(1)  Observations  to  be  made  during  a  boiler  trial. 

(2)  Appliances  used  during  a  boiler  trial. 

(3)  Form  of  report,  methods  of  operation  and  explanation  of 
computations. 

I    OBSERVATIONS  TO  BE  MADE  DURING  A  BOILER  TRIAL 

In  the  report  of  the  committee  of  the  American  Society  of 
Mechanical  Engineers,1  1899,  on  the  revision  of  the  standard  code 
for  conducting  steam  boiler  trials,  two  forms  of  report  are  submit- 
ted, a  Complete  Form  and  a  Short  Form.  These  are  both  shown  in 
Section  III,  page  21.  The  observations  necessary  to  complete 
either  of  these  forms  are  given  in  Table  I.  An  explanation  of 
some  of  the  methods  used  in  obtaining  these  observations  and 
the  forms  used  in  recording  them  follow. 

COAL,  WATER  AND  ASH 

The  two  fundamental  points  to  be  determined  in  every  test  of 
a  steam  boiler  or  furnace,  regardless  of  the  special  or  specific 
purpose  of  such  test,  are  the  pounds  of  water  evaporated  by  the 
boiler  and  the  pounds  of  fuel  necessary  to  produce  such  evapora- 
tion. To  determine  these  two  points  it  is  necessary  to  know  the 
number  of  pounds  of  water  fed  into  the  boiler  and  the  pounds  of 
fuel  fed  into  the  furnace.  The  possibility  of  an  error  in  either  throws 
doubt  upon  all  the  indications  of  the  test.  Each  item,  therefore, 
should  be  ascertained  in  a  manner  that  proves  its  own  correctness, 
and  the  records  must  be  such  that  if  errors  are  made,  they  will  be 
clearly  exposed. 

Coal. — The  weight  of  the  coal  is  best  obtained  by  means  of  a 
barrow  or  car  with  a  capacity  of  500  pounds.  The  car  should  be 
loaded  uniformly  each  time  and  weighed  on  platform  scales  in 
front  of  the  furnace.  The  total  weight  and  the  time  of  weighing 
should  be  recorded  in  the  log.  From  the  car  the  coal  should  be 
fired  directly  into  the  furnace  and  the  weight  of  the  separate 


1  See  Trans.  A.  S.  M.  E.  Vol.  XXI,  p.  34. 


4  ILLINOIS    ENGINEEKING    EXPERIMENT    STATION 

TABLE  I 
OBSERVATIONS  TO  BE  MADE  DURING  A  BOILER  TRIAL 


Short  Trial 

Standard  Trial 

Observations 

1 

1 

Weight  of  water  fed  to  boiler 

2 

2 

Weight  of  coal  as  lired                  (sample) 

3 

3 

Weight  of  ash  and  refuse             (sample) 

4 

4 

Moisture  in  coal 

5 

5 

Steam  pressure  by  gage 

6 

6 

Force  of  draft:  between  damper  and  boiler 

7 

7 

in  furnace 

8 

in  ash-pit 

8 

9 

Temperature:  of  feed  water  entering  boiler 

9 

10 

of  escaping  gases  from  boiler 

11 

of  external  air 

12 

of  tire-room 

13 

of  steam 

11 

of  feed  water  entering  heater 

15 

of  feed  water  entering  economizer 

16 

of  escaping  gases  from  economizer 

17 

of  gases  in  furnace 

10 

18 

Moisture  in  steam  by  calorimeter 

19 

Analysis  of  flue  gases 

20 

Smoke  observations 

21 

Average  thickness  of  fire,  intervals  of  firing 

charges  and  time  of  firing  entered  in  the  log.  After  the  entire 
car-load  of  coal  has  been  fired,  the  weight  of  the  empty  car  and 
the  time  should  be  recorded.  The  sum  of  the  separate  charges 
must  then  be  equal  to  the  difference  in  weight  of  the  car  when 
loaded  and  empty.  A  convenient  form  for  recording  the  coal  fired 
is  shown  in  Form  I.  Prom  each  car-load  of  coal  fired  an  average 
sample  of  coal  should  be  taken  for  moisture  determination  and 
chemical  analysis.  The  sample  of  course  must  be  taken  before 
the  coal  is  weighed  and  should  be  about  two  per  cent  of  every  car- 
load, or  about  ten  pounds.  At  the  end  of  the  test  these  samples 
from  the  different  cars  are  mixed,  pounded  into  small  sizes,  and 
then  quartered  until  enough  is  left  to  fill  a  two-quart  jar.  The  jar 
should  then  be  sealed,  to  prevent  loss  of  moisture,  and  sent  to 
the  chemist. 

Feed  Water. — The  water  fed  to  the  boiler  should  be  both  weighed 
and  measured,  as  dependence  upon  measuring  alone  will  introduce 
errors  due  to  uneven  filling  and  variations  in  temperature;  for  the 
latter,  however,  corrections  may  be  made.  The  measuring  tank 
or  preferably  two  tanks  should  be  set  on  scales  in  such  a  position 
that  the  water  can  be  delivered  directly  into  the  suction  or  set- 
tling tank  as  shown  in  Fig.  1.  The  measuring  tanks  should  be 
filled  and  emptied  alternately,  the  time  of  each  weighing  to  be 
noted  when  the  tank  is  empty,  the  tanks  being  designated  as  No. 
1  and  No.  2.  In  no  case  should  a  simple  tally  be  recorded  for 


PARR°ANDBDIRKS] 


FUEL  TESTS    WITH  ILLINOIS  COALS 


Weighing  and 
Measuring  TanH 


FIG.  1    ARRANGEMENT  OF  TANKS  AND  SCALE  FOR  MEASURING 
FEED-WATER  FED  TO  BOILER 

each  tankful,  as  the  liability  of  error  is  thereby  increased.  When 
the  boiler  tested  is  of  small  capacity,  one  weighing  tank  will  be 
sufficient.  A  convenient  form  for  recording  the  feed  water  meas- 
urements is  shown  in  Form  II. 

To  guard  against  the  loss  of  all  data,  due  to  accidents,  it  is 
best  to  have  coincident  records  of  the  water  and  coal  fed  to  boiler. 
For  this  reason  it  is  well  to  have  a  float  in  the  suction  or  settling 
tank,  and  each  time  an  entire  car-load  of  coal  has  been  fired>  the 
time  on  the  feed  water  log  should  be  recorded,  also  the  height  of 
water  in  the  boiler  and  in  the  settling  tank.  This  will  also  pro- 
vide a  check  on  the  uniformity  of  operations. 

Ash. — The  ashes  and  refuse  should  be  weighed  dry.     The  time 
of  each  raking  of  the  fire  and  cleaning  of  the  ash-pit  and  the  weight 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 

FORM  I 
LOG  OF  BOILER  TRIAL  NO 


Made  at . . 

Date 

Boiler  No 


By 

Fireman 


COAL  SHEET 


COAL 

COAL 

COAL 

DELIVERED 

ON  SCALES 

FIRED 

TIME 

TO 

AFTER 

EACH 

FUEL 

SCALES 

EACH    FIRING 

TIME 

POUNDS 

POUNDS 

POUNDS 

Moist  coal  consumed,  pounds 

Moisture  in  coal,  per  cent 

Dry  coal  consumed,  pounds 

Wood  consumed,  pounds 

Coal  equivalent  of  wood  (=wood  x-4)  Tb 

j      Total  dry  coal  consumed  including 
1         wood  equivalent,  pounds 

Total  dry  refuse,  pounds 

Total  dry  refuse,  per  cent 

!  Total  combustible 


DESCRIPTION  OF  FUEL 

Commercial  Name 

Commercial  size 

Lumps,  per  cent 

Small  coal,  per  cent 

Slack,  per  cent 

% 

Appearance  of  coal 

j     Record   the  times   when  fires 
t        cleaned 

are 

TESTS    WITH  ILLINOIS  COALS 


FORM  II 
LOG  OF  BOILER  TRIAL  NO. 


Made  at  , 

Date 

Bv. 

Boiler  No 

Fireman  

FEED  WATER  SHEET 

TIME 

WATER 
DELIVERED 
TO 
FEED  TANK 
POUNDS 

TKMP. 
OF 
WATER 
IN 

TANK 

TIME 

WATER 
DELIVERED 
TO 
FEED  TANK 
POUNDS 

TEMP. 
OF 
WATER 
IN 
TANK 

REMARKS 

• 

Test  began  at 

o'clock             M. 

• 

Date 

Test  closed  at 

o'clock             M. 

Date, 

8 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 

FORM  III 
LOG  OF  BOILER  TRIAL  NO  .  . 


Made  at . . 

Date 

Boiler  No 


By  

Fireman 


PR 

ESSUR 

ES 

TEMPI 

iRATUI 

IES 

g 

TIME 

STEAM 
GAGE 

DRAFT 
GAGE 

BAROM- 
ETER 

1  BOILER 
ROOM 

EXTERNAL 
AIR 

FLUE 
GASES 

| 
IFEED 
WATER 

STEAM 

S  ,     o  o 
Hg 

REMARKS 

Test  began  at 

o'clock    M. 

Date, 

Test  closed  at 

o'clock    M. 

PARE°ANDBDIRKS]      FUEL  TESTS    WITH  ILLINOIS  GOALS 


FORM  IV 
LOG  OF  BOILER  TRIAL  NO 


Made  at . . 

Date 

Boiler  No 


By 

Fireman 


TIME 

CALORIMETER 

DRAFT 

HEIGHT 
OF  WATER 
IN  TANK 

gl3- 

1^ 

Ȥ5 

REMARKS 

GAGE 
PRESSURE 

STEAM 
DISCHARGE 
OR  CALORI- 
METER 
TEMP. 

WATER 
SEPARATED 
OR  CALORI- 
METER 
PRESSURE 

BETWEEN 
DAMPER 
AND 
BOILER 

IN 
FURNACE 

Be 

Hw 

/n 
•< 

i 

10  ILLINOIS    ENGINEERING    EXPERIMENT    STATION 

FORM  V 


Made 
Date 

at                               

Rv.. 

Boile 

r  No                                           .             Fireman  

FLUE-GAS  SHEET 

TIME 

C02 

02 

CO 

HYDROGEN 
AND 
HYDROCAR- 
BONS 

TOTAL, 

REMARKS 

FUEL  TESTS    WITH  ILLINOIS  COALS  11 

of  ash  removed  should  be  recorded  in  the  same  log  as  the  weight 
of  coal,  Form  I.  A  representative  sample  of  ash  should  be  taken 
at  every  cleaning  and  saved  in  order  to  determine  the  principal 
characteristics  of  the  ash,  a  proximate  analysis  giving  the  actual 
amount  of  incombustible  material  being  made  of  each  sample. 

GENERAL  OBSERVATIONS 

Although  the  main  points  to  be  determined  in  a  boiler  trial 
are  the  weight  of  water  evaporated  and  the  amount  of  fuel  burned, 
the  general  observations  of  pressures,  temperatures,  etc.,  under 
which  this  evaporation  takes  place  and  which  tend  to  secure  the 
accuracy  of  these  two  measurements  must  not  be  overlooked.  It 
is  necessary  that  all  available  data  be  obtained  and  recorded  in  the 
log  for  use  in  making  comparisons.  The  value  of  the  observation 
will  depend  primarily  upon  its  correctness  and  the  greatest  care 
should  be  exercised  in  obtaining  and  recording  observations.  Too 
often  the  observer  is  guided  by  personal  opinion  and  former 
readings,  and  the  value  of  the  observation  as  an  indication  of  some 
specific  occurrence  is  entirely  lost. 

All  general  observations  should,  as  nearly  as  possible,  be 
taken  at  the  same  instant,  the  exact  time  in  all  cases  being  recorded 
in  the  log.  As  a  rule  all  observations  should  be  recorded  in  dupli- 
cate, this  being  necessary  especially  where  several  persons  are 
concerned  with  the  results.  Duplicates  are  easily  obtained  by 
placing  carbon  copying  paper  below  the  original  log.  The  dup- 
licates are  then  obtained  as  the  results  are  originally  recorded. 
Forms  for  recording  the  general  observations  are  shown  in 
Forms  III  to  V. 

For  convenience  it  is  best  to  have  the  log  sheets  tacked  to  a 
board,  which  may  be  suspended  on  the  wall  at  some  convenient 
point.  This  avoids  the  accumulation  of  dust  and  dirt  when  the 
sheets  are  lying  around  unattached  in  a  horizontal  position. 

Sufficient  time  should  elapse  between  temperature  measure- 
ments if  only  one  thermometer  serves  for  taking  several  observa- 
tions, in  order  to  allow  the  thermometer  to  assume  the  new  tem- 
perature. TvVhere  the  range  of  temperature  is  large,  however,  this 
should  never  be  practised,  and  it  will  be  preferable  in  most  cases 
to  take  only  the  most  important  of  the  readings,  being  certain  of 
its  correctness. 


12 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


Determinations  of  the  moisture  in  the  steam  are  necessary  to 
make  corrections  in  the  amount  of  water  evaporated,  and  should 
be  made  at  regular  intervals  and  entered  in  the  log. 

The  analysis  of  the  flue  gases  is  important  as  it  indicates  to 
some  extent  the  progress  of  combustion  in  the  furnace.  Notwith- 
standing, the  general  use  of  this  analysis  is  still  very  limited,  al- 
though in  some  instances  a  record  of  the  CO  in  the  flue  gases  is 
regularly  kept.  The  value  of  the  analysis  consists  in  its  being 
an  indication  of  the  amount  of  excess  air  being  used.  The  flue 
gas  to  be  analyzed  should  be  an  average  sample  taken  con- 
tinuously over  a  considerable  period  of  time.  This  is  necessary 
as  the  composition  of  the  gases  varies  from  minute  to  minute. 
Under  ordinary  conditions  an  analysis  every  half-hour  is  sufficient; 
special  readings,  however,  may  be  taken  more  often.  The  ap- 
paratus for  sampling  will  be  explained  in  the  following  section. 

II    APPLIANCES  USED    DURING  A  BOILER  TRIAL 

Since  the  corrections  to  be  applied  to  the  weights  of  fuel  and 
water  fed  to  the  boiler  are  dependent  on  the  general  observations, 
the  appliances  necessary  for  their  determination  must  be  consid- 
ered. The  correctness  of  the  observations  will  depend  primarily 
on  the  instruments  used  and  their  location.  In  the  following  para- 
graphs these  are  discussed  to  some  extent. 

DESCRIPTION  OF  APPLIANCES 

A  list  of  the  apparatus  necessary  to  take  the  observations 
given  in  Section  I  is  shown  in  Table  II.  The  apparatus  required 

TABLE  II 
APPLIANCES  FOR  OBSERVATIONS  GIVEN  IN  TABLE  I 


Short  Trial 

Standard  Trial 

Appliances 

1 

1 

Measuring  and  suction  tanks  for  measuring  water 

2 

2 

Platform  scales  for  weighing  water 

3 

3 

Car  or  barrow  for  handling  coal 

4 

4 

Platform  scales  for  weighing  coal 

5 

5 

Standard  calibrated  steam  gage 

6 

6 

Draft  gages,  U  tubes  or  otherwise 

7 

7 

Thermometers  according  to  observations  made 

8 

8 

Flue  gas  thermometer 

9 

Pyrometer  for  furnace  temperatures 

9 

10 

Throttling  or  separating  calorimeter 

11 

Orsat  apparatus  for  flue  gas  analysis 

12 

Smoke  charts 

°  ANDRmRKs] 


FUEL  TESTS    WITH  ILLINOIS  COALS 


13 


in  the  determination  of  the  weights  of  coal  and  water  was  discussed 
in  the  previous  section  and  needs  no  explanation  other  than  that 
the  scales  used  should  be  calibrated  so  that  a  correction  may  be  ap- 
plied if  necessary.  The  suction  tank  should  also  be  calibrated  so 
that  the  contents  of  the  tank  are  known  for  all  positions  of  the  float. 
For  measurement  of  the  steam  pressure  an  ordinary  steam 
gage  calibrated  by  comparison  with  a  standard  gage  or  other 
means  will  suffice.  A  good  recording  steam  gage  carefully  ad- 
justed and  compared  at  frequent  intervals  with  the  steam  gage 
provides  a  good  check.  Various  forms  of  draft  gages  are  used  to 
determine  the  draft  pressure.  The  ordinary  U  tube  is  the  most 
common  form  and  gives  very  satisfactory  results.  A  gage  of  the 
type  shown  in  Pig.  2  has  been  extensively  used  at  the  University 
and  gives  results  which  can  be  read  with  greater  accuracy  than 
the  U  tube. 


FIG.  2     DRAFT  GAGE 

In  the  choice  of  thermometers  care  should  be  taken  that  the 
range  of  readings  will  fall  within  that  of  the  thermometer.  Where 
thermometers  are  likely  to  be  handled  constantly,  a  metal  casing 
is  desirable.  Where  temperatures  within  a  pipe  are  required,  as 
in  steam  or  water  pipes,  thermometer  cups,  as  shown  in  .Fig.  3 
will  need  to  be  used. 

Either  mercury  or  a  heavy  cylinder  oil  may  be  used  in  these 
cups;  the  former,  however,  is  preferable  both  for  cleanliness  and 
accuracy.  For  the  measurement  of  flue  gas  temperatures  a  spe- 
cial mercury  thermometer  is  used,  reading  up  to  1000°  F.,  with 
nitrogen  compressed  above  the  mercury. 

The  thermometer  should  be  calibrated  from  time  to  time  to  in- 
sure its  correctness.  The  location  of  the  thermometer  will  be  dis- 
cussed in  the  following  section. 


14  ILLINOIS    ENGINEERING    EXPERIMENT    STATION 

Thermometer 


Mercury 
bath  ~ 


FIG.  3 


THERMOMETER  CUP,  USED  TO  OBTAIN  TEMPERATURES 
WITHIN  A  PIPE 


The  measurement  of  furnace  temperatures  is  very  difficult, 
and  no  especial  form  of  pyrometer  has  proved  to  be  entirely  satis- 
factory. The  Wanner  optical  pyrometer  is  being  used  at  the  Gov- 
ernment Coal-Testing  Plant  at  St.  Louis,  and  seems  to  be  giving 
fair  results. 


B-/n  holes   Gfr///eaf 
/7e//c0//y    a/ong 


FIG.  4      SAMPLING  NOZZLE  FOR  STEAM  CALORIMETER 

For  determining  the  moisture  in  the  steam,  as  long  as  the 
moisture  remains  below  three  per  cent,  any  one  of  several  forms 
of  calorimeters  may  be  used  with  good  results.  Above  this  point, 
all  calorimeters  are  inaccurate,  owing  to  the  inability  to  obtain  an 
average  sample  of  the  steam.  The  sampling  nozzle,  Fig.  4,  should 
be  made  of  i-in.  pipe,  and  should  extend  across  the  diameter  of 


BRECKENBIDGB.  ~] 
PABB  AND   DIBKS  J 


FUEL  TEST8    WITH  ILLINOIS  COALS 


15 


the  steam  pipe  to  within  half  an  inch  of  the  opposite  side,  being 
closed  at  the  end,  and  perforated  with  not  less  than  twenty  i-in. 
holes  equally  distributed  along  and  around  its  cylindrical  surface, 
but  none  of  these  holes  should  be  nearer  than  i  inch  to  the  inner 
side  of  the  steam  pipe.  The  calorimeter  and  pipe  leading  to  it 
should  be  well  covered  with  felt.  When  a  separating  calorimeter 
with  attached  gage  for  determining  the  amount  of  steam  passing 
through  the  calorimeter  is  used,  such  gage  should  be  calibrated  by 
taking  readings  over  twenty  minutes  in  length,  and  condensing 
the  steam  passing  through  the  calorimeter  during  that  time,  the 
weight  of  condensed  steam  being  compared  with  the  indication  on 
the  gage.  This  should  be  repeated  for  the  entire  range  of  the  gage. 
Superheating  should  be  determined  by  means  of  a  thermometer 
placed  in  a  mercury  well,  inserted  in  the  steam  pipe. 


Hue 


-/n.  gas 

One  for  every 
.  eross- 
of  f/ue 


/ron  recever 


box 


-/n  pipe 


FIG.  5     FLUE  GAS  SAMPLER.  ADVISED  IN  THE  A.  S.  M.  E.  STANDARD  CODE 
FOR  CONDUCTING  STEAM  BOILER  TRIALS 

For  determining  the  composition  of  the  flue  gases  a  sampling 
tube  for  drawing  the  sample  of  gas  from  the  flue  is  necessary,  also 
apparatus  for  analyzing  the  gas.  There  has  been  a  great  diver- 
sity of  opinion  regarding  the  method  to  be  used  in  obtaining  the 


16 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


FIG.  6      ORSAT  APPARATUS  FOR  ANALYZING  FLUE  GAS 

sample,  due  probably  to  the  varying  conditions  in  different  boiler 
settings  and  at  different  points  in  the  same  flue.  In  the  trials 
carried  on  by  the  United  States  Geological  Survey  at  St.  Louis, 
both  the  sampler  advised  in  the  A.  S.  M.  E.  code,  Fig.  5,  and  an 
ordinary  pipe  closed  at  the  end  and  perforated  with  holes  equally 
spaced  along  its  entire  length  have  been  used.  The  results  indi- 
cate the  advisability  of  using  the  latter,  and  it  has  been  adopted 
for  use  in  all  future  trials.  To  get  a  uniform  flow  through  all  the 
perforations,  they  are  made  of  such  size  and  number  that  the  sum 
of  the  areas  of  the  perforations  is  less  than  the  cross  sec- 
tional area  of  the  sampling  tube.  The  Orsat  apparatus  is  the  one 
mostly  used  for  analyzing  the  flue  gases,  as  it  is  simple  in  opera- 
tion, and  with  a  little  care  gives  reliable  results.  To  insure  the 


PBABBCANDBD?BK91      FUEL  TEST8    WI 

17 


No.  1. 


No.  2. 


No.  4. 


No.  3. 

FIG.  7    THE  RINGELMAN  SCALE  FOR  GRADING  THE  DENSITY 
OF  SMOKE 


18  ILLINOIS    ENGINEERING    EXPERIMENT    STATION 

total  absorption  of  the  various  gases,  care  must  be  taken  that  the 
absorbing  solutions  are  in  good  condition,  and  they  should  there- 
fore be  renewed  from  time  to  time.  If  the  flue  gas  is  to  be  col- 
lected over  water,  a  saturated  salt  solution  should  be  used,  as 
water  has  a  tendency  to  retain  some  of  the  CCte  when  a  consider- 
able quantity  is  present,  and  to  give  it  up  later  when  there  is  a 
smaller  quantity  of  this  gas,  thus  causing  errors  in  the  results. 
Fig.  6  shows  the  type  of  Orsat  apparatus  generally  used. 

If  determinations  of  the  relative  density  of  the  smoke  are  to 
be  made  during  the  trial,  the  Ringelman  smoke  charts  shown  in 
Fig.  7  may  conveniently  be  used.  These  are  placed  in  a  horizon- 
tal row  about  fifty  feet  from  the  observer,  and  as  nearly  as  con- 
venient in  line  with  the  chimney.  At  this  distance  the  lines  become 
invisible  and  the  cards  appear  as  different  shades  of  gray.  The 
observer  by  glancing  from  the  chimney  to  the  cards  determines 
which  card  most  nearly  corresponds  to  the  color  of  the  smoke  and 
makes  a  record  accordingly. 

LOCATION  OF  APPLIANCES 

Of  prime  importance  in  taking  observations  is  the  location  of 
the  apparatus  used.  On  account  of  the  variation  in  different  types 
of  boiler  settings  it  will  always  be  necessary  to  describe  clearly 
in  the  report  of  the  test  the  location  of  all  apparatus.  This  is  best 
done  by  indicating  on  drawings  or  diagrams  their  position  on  the 
setting. 

Feed  Water  Temperature. — As  the  methods  used  in  supplying 
feed  water  to  a  boiler  vary,  so  does  also  the  location  of  the  ther- 
mometer for  the  temperature  measurement  of  such  feed  water.  If 
an  injector  be  used,  it  should  receive  steam  directly  through  a 
covered  pipe  from  the  boiler  being  tested,  and  the  temperature  of 
the  feed  water  should  in  this  case  be  taken  from  the  supply  tank 
furnishing  the  water  to  the  injector.  It  is  here  assumed  that  the 
heat  of  the  steam  operating  the  injector  is  returned  to  the  boiler 
from  which  it  was  taken,  so  that  the  supply  pipe  between  the  boiler 
and  injector,  if  long,  should  be  covered  to  prevent  radiation.  If  a 
pump  be  used  for  feeding  the  boiler,  the  temperature  of  the  feed 
water  should  be  taken  by  a  thermometer  in  the  discharge  pipe  as 
near  the  boiler  as  possible.  If  this  is  done,  the  water  may  or  may 
not  be  pumped  through  a  feed  water  heater  after  leaving  the  pump. 


BBECKENBIDGE 
PAKB  AND   DIRKS 


s]      FUEL  TESTS  WITH  ILLINOIS  COALS  19 


It  is  always  essential  that  the  heat  carried  into  the  boiler  by  the 
feed  water  should  be  known,  and  it  is  well  to  record  its  temperature 
before  and  after  it  passes  through  any  kind  of  heater  or  economiz- 
er in  order  that  the  effect  of  such  device  may  be  given  proper  credit. 
The  location  of  thermometers  for  the  determination  of  boiler 
room  and  external  air  temperatures  should  be  such  that  drafts  or 
heat  rays  will  be  avoided.  The  flue  gas  temperature  should  be 
taken  at  a  point  where  the  gases  leave  the  boiler  and  pass  into  the 
breeching  on  their  way  to  the  stack.  As  the  temperature  in  a 
transverse  section  of  the  flue  will  vary,  several  readings  should 
be  taken  at  different  points  of  the  same  section.  Observations  of 
the  draft  are  usually  made  at  several  points  of  the  setting.  The 
one  between  the  damper  and  the  boiler  is,  however,  the  more  im- 
portant, and  should  be  taken  at  a  point  close  to  the  flue  gas  ther- 
mometer or  possibly  in  the  same  transverse  section.  The  force 
of  draft  in  furnace  and  ash-pit  may  be  taken  through  the  firing 
and  ash-pit  doors,  but  is  preferably  taken  through  holes  left  in 
the  side  walls.  The  calorimeter  and  the  thermometer  cup  for  de- 
termining superheat  should  be  attached  to  the  vertical  steam  pipe 
as  it  leaves  the  boiler.  The  sampling  tube  for  the  flue  gas  was 
explained  in  the  last  section.  It  should  be  inserted  in  the  flue  at 
the  point  where  the  flue  gas  temperature  and  draft  are  obtained. 

Ill    REPORT  OF  THE  TRIAL 

Forms. — The  data  and  results  of  a  boiler  trial  should  be  re- 
ported in  the  manner  given  in  Form  VI,  which  is  the  complete 
form  advised  by  the  Boiler  Test  Committee  of  the  American  Soci- 
ety of  Mechanical  Engineers,  Code  of  1899.  The  items  printed 
in  italics  correspond  to  the  items  in  the  "Short  Form"  of  report 
recommended  for  commercial  tests.  For  more  elaborate  trials  the 
code  recommends  that  the  full  log  of  the  trial  be  shown  graph- 
ically by  means  of  a  chart,  Fig.  8. 


20 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


02     91    91     fl      21     01      0     9       f" 
SflNHOd    0001    HI      NOIldWnSNOO    "WOO 


os    gf  ofr     gs     o«    s«    oz    ci     oi 
SONOOd  0001  N|    NOIidWnfiNOO    U31VM 


0022         0091         OOVI          0001 


001     08    09     Ofr      02       0 
13J    Of 

gajsj.no 


pABB°ANDBDiBKsJ      FUEL  TESTS  WITH  ILLINOIS  COALS  21 

FORM    VI 
DATA  AND  RESULTS  OF  EVAPORATIVE  TESTS 

Arranged  in  accordance  with  the  Complete  Form  advised  by  the  Boiler  Test  Committee  of  the 
American  Society  of  Mechanical  Engineers.    Code  of  1899. 

Made  by of boiler  at    to 

determine 

Principal  conditions  governing  the  trial 


Kind  of  fuel* 

Kind  of  furnace 

State  of  the  weather 

Method  of  starting  and  stopping  the  test  ("standard"  or  "alternate") 

1.  Date  of  trial 

2.  Duration  of  trial hours 

Dimensions  and   Proportions 

(A  complete  description  of  the  boiler  and  drawings  of  the  same  if  of  unusual  type,  should  be 
given  on  an  annexed  sheet ) 

3.  Grate  surface width length area sq.  f t- 

4.  Height  of  furnace in. 

5.  Approximate  width  of  air  spaces  in  grate in. 

6.  Proportion  of  air  space  to  whole  grate  surface per  cent 

7.  Water-heating  surface sq.  ft- 

8.  Superheating  surf  ace sq.ft. 

9.  Ratio  of  water-heating  surface  to  grate  surface — to  1 

10.  Ratio  of  minimum  draft  area  to  grate  surface 1  to— 

Average  Pressures 

11.  Steam  pressure  by  gage Ibs-  per  sq.  in. 

12.  Force  of  draft  between  damper  and  boiler in.    of     water 

13.  Force  of  draft  in  furnace in.    of     water 

14.  Force  of  draft  or  blast  in  ash  pit in.    of     water 

Average  Temperatures 

15.  Of  external  air deg. 

16.  Of  flreroom deg. 

J7.  Of  steam deg. 

18-  Of  feed  water  entering  heater deg. 

19.  Of  feed  water  entering  economizer deg. 

20.  Of  feed  water  entering  boiler deg. 

21 .  Of  escaping  gases  from  boiler deg. 

22.  Of  escaping  gases  f  rom  economizer  deg. 

Fuel 

23.  Size  and  condition 

24.  Weight  of  wood  used  in  lighting  tire Ibs. 

25.  Weight  of  coal  as  fired " Ibs. 

26.  Percentage  of  moisture  in  coal per  cent 

27.  Total  weight  of  dry  coal  consumed • Ibs. 

28.  Total  ash  and  refuse Ibs. 

29.  Quality  of  ash  and  refuse 

30.  Total  combustible  consumed Ibs. 

31-    Percentage  of  ash  and  refuse  in  dry  coal per  cent 

Proximate  Analysis  of  Coal 

Of  Coal.       Of  Combustible. 

32.  Fixed  carbon percent  percent 

33.  Volatile  matter percent  percent 

34.  Moisture percent 

35.  Ash per  cent 


100   per  cent  100  per  cent 

Sulphur,  separately  determined per  cent  per  cent 


•"The  items  printed  in  italics  correspond  to  the  items  in  the  "Short  Form  of  Code.' 


22 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


Ultimate  Analysis  of  Dry  Coal 

Of  Coal.  Of  Combustible. 

37.  Carbon  (C) per  cent  per  cent 

38.  Hydrogen  (H) per  cent  per  cent 

39.  Oxygen  (O) per  cent  per  cent 

40.  Nitrogen   (N) per  cent  per  cent 

41.  Sulphur  (S) percent  percent 

42.  Ash . .' per  cent 

100  per  cent          100   per  cent 

43.  Moisture  in  sample  of  coal  as  received per  cent  per  cent 

Analysis  of  Ash  and  Refuse 

44-    Carbon per   cent 

45.  Earthy  matter per   cent 

Fuel  per  Hour 

46.  Dry  coal  consumed  per  hour Ibs. 

47.  Combustible  consumed  per  hour  Ibs. 

48.  Dry  coal  per  square  foot  of  grate  surface  per  hour Ibs. 

49.  Combustible  per  square  foot  of  water-heating  surface  per  hour Ibs. 

Calorific  Value  of  Fuel 

50.  Calorific  value  by  oxygen  calorimeter,  per  Ib.  of  dry  coal B.  T.  U 

51.  Calorific  value  by  oxygen  calorimeter,  per  Ib.  of  combustible B.  T.  U 

52.  Calorific  value  by  analysis,  per  Ib.  of  dry  coal B.  T.  U 

53.  Calorific  value  by  analysis,  per  Ib.  of  combustible B.  T.  U 

Quality  of  Steam 

54.  Percentage  of  moisture  in  steam per  cent 

55.  Number  of  degrees  of  superheating deg. 

56.  Quality  of  steam  (dry  steam  —unity).  (For  exact  determination  of  the  factor 

of  correction  for  quality  of  steam  see  section  on  computation  of  results.) . . 

Water 

57.  Total  weight  of  water  fed  to  boiler Ibs. 

58.  Equivalent  water  fed  to  boiler  from  and  at  212  degrees Ibs. 

59.  Water  actually  evaporated,  corrected  for  quality  of  steam Ibs. 

60.  Factor  of  evaporation Ibs. 

61.  Equivalent  water  evaporated  into  dry  steam  from  and  at  212  degrees.    (Item 

39  X  Item  60.)  Ibs. 

Water  per  Hour 

62.  Water  evaporated  per  hour,  corrected  for  quality  of  steam Ibs. 

63.  Equivalent  evaporation  per  hour  from  and  at  21 2  degrees Ibs. 

64.  Equivalent  evaporation  per  hour  from  and  at  312  degrees  per  square  foot   of 

water-heating  surface Ibs. 

Horse-Power 

65.  Horse-power  developed,    (34  H  Ibs  of  water  evaporated  per  hour  into  dry  steam 

from  and  at  212  degrees,  equals  one  horse-power.) : H.  P. 

66.  Builders'  rated  horse-power H.  P. 

67.  Percentage  of  builders'  rated  horse-power  developed per  cent 

Economic   Results 

68.  Water  apparently  evaporated  under  actual  conditions  per  pound  of  coal  as  fired. 

(Item  57+Item  25.) Ibs. 

69.  Equivalent  evaporation  from  and  at  212  degrees  per  pound  of  coal  as  fired. 

(Item&\+-Item  25.) Ibs. 

70.  Equivalent    evaporation    from    and    at   212  degrees  per  pound  of  dry  coal. 

(Item  61^-Item  27.) Ibs. 

71.  Equivalent  evaporation  from  and  at  212  degrees  per  pound  of  combustible. 

( Item  61 -H Item  30.) Ibs. 

(If  the  equivalent  evaporation.  Items  69,  70  and  71.  is  not  corrected  for  the 
quality  of  steam,  the  fact  should  be  stated.) 

Efficiency 

72.  Efficiency  of  the  boiler;  heat  absorbed  by  the  boiler  per  pound  of  combustible 

divided  by  the  heal  value  of  one  pound  of  combustible per  cent 

73.  Efficiency  of  boiler,  including  the  grate;  heat  absorbed  by  the  boiler,  per  pound 

of  dry  coal,  divided  by  the  heat  value  of  one  pound  of  dry  coal per  cent 


BBECKENBIDGE.  ~] 
PARK  AND  DIBKSj 


FUEL  TESTS  WITH  ILLINOIS  COALS 


23 


Cost  of  Evaporation 

74.  Cost  of  coal  per  ton Ibs.  delivered  in  boiler  room ; $ 

75.  Cost  of  fuel  for  evaporating  1 ,000  Ibs  of  water  under  observed  conditions $ 

76.  Cost  of  fuel  used  for  evaporating  1 ,000  Ibs.  of  water  from  and  at  212  degrees $ 

Smoke  Observations 

77.  Percentage  of  smoke  as  observed per  cent 

78.  Weight  of  soot  per  hour  obtained  from  smoke  meter ounces 

79.  Volume  of  soot  per  hour  obtained  from  smoke  meter cu.  in. 

Methods  of  Firing 

80.  Kind  of  firing  (spreading,  alternate,  or  coking) 

81.  Average  thickness  of  fire 

82.  Average  intervals  between  firings  for  each  furnace  during  time  when  fires 

are  in  normal  condition 

83.  Average  interval  between  times  of  levelling  or  breaking  up 

Analyses  of  the  Dry  Gases 

84.  Carbon  dioxide  (CO2) per  cent 

85.  Oxygen  (O) 

86.  Carbon  monoxide  (CO) 

87.  Hydrogen  and  hydrocarbons 

«8.  Nitrogen  (by  difference)  (N) 

100  per  cent 

HEAT  BALANCE,  OB  DISTRIBUTION  OF  THE  HEATING  VALUE  OF  THE  COMBUSTIBLE 
TOTAL  HEAT  VALUE  of  1  lb.  of  Combustible B.  T.  U. 


B.T.U. 


Per  Cent 


1.  Heat  absorbed  by  the  boiler  =  evaporation  from  and  at  212  degrees 

per  pound  of  combustible  X  965  7. 

2.  Loss  due  to  moisture  in  coal  =  per  cent  of  moisture  referred  to   corn- 

bustible-MOG  X  [  (21-2—  0+966+0.  48  (T —  212)  ]  (t  —  temperature 
of  air  in  the  boiler  room,  T  =  that  of  the  flue  gases) 

3.  Loss  due  to  moisture  formed  by  the  burning  of  hydrogen  =  per  cent 

of  hydrogen  to  combustible- 100  X  9  X  [  (212-^+966+0.  48 ( 3T-212)  J 
4.*  Loss  due  to  heat  carried  away  in  dry  chimney  gases  =  weight  of  gas 

per  pound  of  combustible  X  0  .24  X  ( T—t) . 

CO 
5,t  Loss  due  to  incomplete  combustion  of  carbon  = 


per  cent  C  in  combustible 
100 


C02 


CO 


Loss  due  to  unconsumed  hydrogen  and  hydrocarbons,  to  heating  the 
moisture  in  the  air,  to  radiation,  and  unaccounted  for.  (Some  of 
these  losses  may  be  separately  itemized  if  data  are  obtained  from 
which  they  may  be  calculated.) 

Totals...  


100.00 


*The  weight  of  gas  per  pound  of  carbon  burned  may  be  calculated  from  the  gas  analyses  as 
follows: 

11CO2    +80  +7  CO    +  (N) 

Dry  gas  per  pound  carbon  = —  — ,  in  which  CO2,  CO,  O,  and  N  are  the 

3  (CO2  +  CO) 

percentages  by  volume  of  the  several  gases.  As  the  sampling  and  analyses  of  the  gases  in  the 
present  state  of  the  art  are  liable  to  considerable  errors,  the  result  of  this  calculation  is  usually 
only  an  approximate  one.  The  heat  balance  itself  is  also  only  approximate  for  this  reason  as 
well  as  for  the  fact  that  it  is  not  possible  to  determine  accurately  the  percentage  of  unburned 
hydrogen  or  hydrocarbons  in  the  flue  gases. 

The  weight  of  dry  gas  per  pound  of  combustible  is  found  by  multiplying  the  dry  gas  per  pound 
of  carbon  by  the  percentage  of  carbon  in  the  combustible,  and  dividing  by  100. 

+CO2  and  CO  are  respectively  the  percentage  by  volume  of  carbonic  acid  and  carbonic  oxide 
in  the  flue  gases.  The  quantity  10,150=  Number  of  heat  units  generated  by  burning  to  carbonic 
acid  one  pound  of  carbon  contained  in  carbonic  oxide. 


24  ILLINOIS  ENGINEERING  EXPERIMENT  STATION 

STARTING  AND  STOPPING  THE  TEST 

Standard  Method. — Steam  being  raised  to  the  working  pres- 
sure, remove  rapidly  all  fire  from  the  grate,  close  the  damper, 
clean  the  ash  pit,  and  as  quickly  as  possible  start  a  new  fire  with 
weighed  wood  and  coal,  noting  the  time  and  the  water  level  while 
the  water  is  in  a  quiescent  state,  just  before  lighting  the  fire.  At 
the  end  of  the  test,  remove  the  whole  fire,  which  has  been  burned 
low,  clean  bhe  grates  and  ash-pit,  and  note  the  water  level  when 
the  water  level  is  in  a  quiescent  state,  and  record  the  time  of 
hauling  the  fire.  The  water  level  should  be  as  nearly  as  possible 
the  same  as  at  the  beginning  of  the  test.  If  it  is  not  the  same  a 
correction  should  be  made  by  computation,  and  not  by  operating 
the  pump  after  the  test  is  complete. 

Alternate  Method. — The  boiler  being  thoroughly  heated  by  a 
preliminary  run,  the  fires  are  to  be  burned  low  and  well  cleaned. 
Note  the  amount  of  coal  left  on  the  grate  as  nearly  as  it  can  be 
estimated;  note  the  pressure  of  steam  and  the  water  level.  Note 
the  time  and  record  it  as  the  starting  time.  Fresh  coal,  which 
has  been  weighed,  should  now  be  fired.  The  ash-pits  should  be 
thoroughly  cleaned  at  once  after  starting.  Before  the  end  of  the 
test  the  fires  should  be  burned  low,  just  as  before  the  start,  and 
the  fires  cleaned  in  such  a  manner  as  to  leave  a  bed  of  coal  on  the 
grates  of  the  same  depth  and  in  the  same  condition  as  at  the  start. 
When  this  stage  is  reached,  note  the  time  and  record  it  as  the 
stopping  time.  The  water  level  and  steam  pressure  should  pre- 
viously be  brought  as  nearly  as  possible  to  the  same  point  as  at 
the  start.  If  the  water  level  is  not  the  same  as  at  the  start, 
a  correction  should  be  made  by  computation,  and  not  by  operat- 
ing the  pump  after  the  test  is  completed. 

The  two  methods  given  above  for  starting  and  stopping  the 
test  are  taken  from  the  A.  S.  M.  E.  Code  for  conducting  steam 
boiler  trials.  When  the  alternate  method  is  used,  several  precau- 
tions regarding  the  observations  are  necessary.  The  time  of 
starting  and  stopping  should  be  noted  when  the  smallest  amount 
of  fuel  is  on  the  grate,  and  when  it  is  in  the  most  burned- out  con- 
dition, i.  e. ,  just  before  firing  fresh  coal  after  cleaning,  and  when 
the  water  level  is  in  its  most  quiet  condition  and  the  least  raised 
by  ebullition.  This  condition  of  fire  and  of  water  level  can  be 
duplicated  immediately  after  cleaning  the  fire,  but  there  is  no  cer- 
tainty of  duplication  of  any  condition  when  there  is  a  bright  fire 


FUEL  TESTS  WITH  ILLINOIS  COALS  25 

and  consequent  rapid  steaming.  If  the  water  level  is  noted  at 
the  starting  of  the  test  when  it  is  raised  by  a  bright  fire,  and  at 
the  end  of  a  test  when  it  is  depressed  by  the  stoppage  of  violent 
ebullition  or  of  rapid  circulation  due  to  the  cooling  of  the  fire,  the 
boiler  will  be  credited  with  more  water  than  was  really  evapo- 
rated. As  such  a  fall  in  water  level  is  easily  produced  by  open- 
ing fire  doors  and  checking  draft,  it  should  be  guarded  against 
especially  when  using  bituminous  or  flaming  coals.  The  greatest 
care  should  also  be  taken  that  the  bed  of  coal  at  the  end  does  not 
contain  more  waste  material,  which  belongs  to  the  ash,  than  it 
did  at  the  beginning. 

COMPUTATION  OF  RESULTS 

On  account  of  the  variations  in  the  types  of  boilers  and  fur- 
naces, no  specific  directions  can  be  given  for  the  measurement  of 
grate  surface,  height  of  furnace  and  other  furnace  proportions. 
The  heating  surface  should  be  computed  from  the  surface  of 
shells,  tubes  and  fire-boxes  in  contact  with  fire  or  hot  gases.  The 
outside  diameter  of  water  tubes  and  the  inside  diameter  of  fire 
tubes  should  be  used  in  this  computation.  All  surfaces  below  the 
mean  water  level  which  have  water  on  one  side  and  products  of 
combustion  on  the  other  are  to  be  considered  as  water- heating 
surface,  and  all  surfaces  above  the  mean  water  level  which  have 
steam  on  one  side  and  products  of  combustion  on  the  other  are  to 
be  considered  as  superheating  surface. 

The  following  directions  show  how  some  of  the  results  to  be 
derived  from  a  boiler  trial  may  be  obtained.  The  calculation  of 
other  items  is  self-evident. 

Item  26,  the  moisture  in  the  coal,   should  be  obtained  by  the 
chemist  by  drying  the  sample  collected  during  the  test,  for  one 
hour  in  a  sand  or  air  bath  at  a  temperature  between  240°  and 
280°  F.     Sometimes  the  moisture  is  obtained  by  drying  a  known 
quantity  of  the  coal  above  the  boiler;  however,  if  this  method  is 
used,  it  should  be  so  stated  in  the  report.     The  first  method  is 
always  to  be  preferred.  (See  Section  VI,  page  48). 
Item  27=Item  25  X  (100— Item  26) 
Item  30=Item  27X(100-Item  42)-(Item  28Xltem  44) 

As  this  is  dependent  upon  the  ultimate  analysis  of  the  coal, 
which  is  not  always  available,  the  following  may  be  used: 
Item  30=Item  27-Item  28 


OF  THE 

UNIVERSITY 


26  ILLINOIS    ENGINEERING    EXPERIMENT    STATION 

The  latter,  however,  is  in  error,  due  to  the  unaccounted- for 
ash  passing  over  the  bridge  wall. 

Item  51=Item  50 -5- (100— Item  42) 

or     =Item  50-Kltem  27— (Item  28Xltem  45)] 
in  which  the  former  depends  again  upon  the  ultimate  analysis  of 
the  coal. 

Items  52  and  53—14,600  0+62,000(11—^-) +4,000  S, 

o 

in  which  C,  H,  O  and  S  refer  to  the  proportions  of  carbon,  hydro- 
gen, oxygen  and  sulphur  respectively,  as  determined  by  the  ulti- 
mate analysis. 

H— 1146.6— 0.48  (T— 212) 


Item  54=1 00  X 
or       =100  X 


L 

Ibs.  of  moisture  separated 


Ibs.  of  steam-fibs,  of  moisture  separated 


in  which  H=total  heat  and  Lr=latent  heat  per  pound  of  steam  at 
the  pressure  in  the  steam  pipe,  and  T=temperature  of  the  throt- 
tled and  superheated  steam  in  the  calorimeter.  The  first  formula 
applies  to  throttling  and  the  second  to  separating  calorimeters. 

Item  55  should  be  taken  as  the  difference  between  the  read- 
ing of  the  thermometer  for  superheated  steam  and  the  readings 
of  the  same  thermometer  for  saturated  steam  at  the  same  pres- 
sure as  determined  by  a  special  experiment  and  not  by  reference 
to  the  steam  tables. 

Item  5tS=100— Item  54 

For  the  exact  determination  of  the  factor  of  correction  for 
quality  of  steam  we  have  the  following: 

For  wet  steam,  F=Q-hP(^ — =r-),  and 

±1 — Ji 

For  superheated  steam,  F=l+^—  ^,  in  which 

±1 — Ji 

F  =  factor  of  correction 

Q  =  quality  of  steam 

P  =  per  cent  of  moisture  in  steam 

K  =  degrees  of  superheating  in  steam 

H  =  total  heat  of  the  steam  due  to  the  steam  pressure 

Ti=  total  heat  in  the  water  at  the  temperature  due  to  the 

steam  pressure 

Ji=  total  heat  in  the  feed  water  due  to  the  temperature 
Item  59  =  Item  57  X  Item  56 


FUEL  TESTS  WITH  ILLINOIS  COALS  27 

TT  _  "U 

Item  60=;r—  -7,,  in  which  H  and  h  are  respectively  the  total 
i 


heat  in  the  steam  of  the  average  observed  pressure  and  in  water 
of  the  average  observed  temperature  of  the  feed.  This  item  may 
usually  be  obtained  directly  from  steam  tables  giving  the  factors 
for  different  pressures  and  feed  water  temperatures. 

Item  61  =  Item  59  X  Item  60 

Item  62  =  Item  59^-  Item  2 

Item  63  =  Item  61-*-  Item  2 

Item  64  =  Item  63-^  Item'  7 

Item  65  =  Item  63-^34.5 

This  is  held  to  be  equivalent  to  30  pounds  of  water  evaporat- 
ed from  100°  F.  into  dry  steam  at  70  pounds  gage  pressure.  The 
former  equals  33,317  B.  T.  U.  per  hour  and  the  latter  33,305 
B.  T.  U.  per  hour. 

Item  66.  —  This  item  should  give  besides  the  rated  horse- 
power the  basis  (square  feet  of  heating  surface)  upon  which  this 
rating  is  made. 

Item  67  =  Item  65^-  Item  66 

The  necessary  computations  for  economic  results  and  effi- 
ciency, items  68  to  73,  are  indicated  in  the  form  of  report. 

IV     REPORT  OF  BOILER  TESTS  WITH  ILLINOIS  COALS 

The  following  tables  contain  a  summary  of  the  results  of 
boiler  tests  made  by  the  department  of  Mechanical  Engineering 
at  the  University  of  Illinois.  For  the  most  part  these  tests  have 
been  made,  as  stated  in  the  introduction,  for  purposes  of  instruc- 
tion in  the  method  of  boiler  testing,  although  a  considerable  num- 
ber were  made  for  investigational  purposes  or  as  thesis  work. 
As  a  rule,  they  have  been  conducted  under  the  direct  supervision 
of  a  member  of  the  instructional  staff  of  the  department,  but  at 
times  when  experiments  were  being  made  with  special  applian- 
ces, the  representative  of  the  company  interested  was  present  to 
take  charge  of  the  test. 

COALS  TESTED 

The  coals  used  in  these  tests  were  mostly  those  purchased 
under  the  yearly  contracts  of  the  University.  In  a  few  cases, 
special  coals  were  purchased,  while  other  tests  were  made  on 


28  ILLINOIS    ENGINEEBING    EXPERIMENT    STATION 

coals  sent  to  the  University  by  various  coal  companies  and  manu- 
facturing concerns  to  determine  the  evaporative  efficiency  or 
their  behavior  on  various  kinds  of  stokers. 

35  coals  were  tested,  representing  14  counties  of  Illinois. 
These  are  given  in  the  list  below  together  with  the  commercial 
size  of  the  coal. 

County  Town  Commercial  Size 

\  Christian Pana Lump 

2  Christian Pana Slack 

3  Christian Pana Srceenings 

4  Coles Paradise Lump 

5  Gallatin Junction Pea 

6  Macon Niantic Nut 

7  Macoupin Mt-  Olive Lump 

8  Madison Glen  Carbon Lump 

9  Marion Odin Lump 

10  Marion Odin Pea 

11  Marion - Odin Slack 

12  McLean. Bloomington Lump 

13  McLean Coif  ax Lump 

14  Menard Athens Lump 

15  Perry Du  Quoin Lump 

16  Perry Du  Quoin Pea 

17  Perry Du  Quoin Slack 

18  sangamon Barclay Pea 

19  Sangamon Dawson Pea 

20  Sangamon Divernon - Lump 

21  Sangamon Lowder Slack 

22  Sangamon ...  Ridgely Pea 

V3  Sangamon Riverton Pea 

24  Sangamon Sringfleld Pea 

25  Sangamon Lump 

26  Shelby Moweaqua Lump 

27  Vermilion Catlin Screenings 

2£  Vermilion Fairmount Screenings 

29  Vermilion Muncie Slack 

30  Vermilion Oakwood Lump 

31  Vermilion Oakwood  Pea 

32  Vermilion Oakwood Screenings 

33  Williamson Carterville Washed  Pea 

34  Williamson Herrin New  Kentucky  Pea 

35  Williamson Herrin New  Kentucky  Screenings 

BOILERS  TESTED 

The  tests  were  made  at  the  power  plants  of  the  University 
and  the  neighboring  towns,  under  water-tube  and  fire-tube  boilers 
of  the  following  types: 

Stirling  water-tube  boiler 2  settings 

National  water-tube  boiler 2  settings 

Heine  water-tube  boiler 1  setting 

Babcock  &  Wilcox  water-tube  boiler 8  settings 

Horizontal  tubular  boiler 11  settings 

The  settings  of  these  boilers  include  the  following: 

1  Murphy  smokeless  furnace 

2  Roney  automatic  stokers 

2     Green  chain  grate  stokers 


PARRCANDBD™KS]      FUEL  TESTS  WITH  ILLINOIS  COALS  29 

1     Babcock  &  Wilcox  chain  grate 
1     Brightman  stoker 

The  remainder  of  the  furnaces  were  hand-fired  with  plain  or 
rocking  grates. 

RESULTS  OF   TESTS 

The  results  of  these  tests  are  shown  in  Tables  III  and  IV,  ar- 
ranged according  to  the  counties  in  which  the  coal  was  mined. 
Table  III  gives  the  conditions  of  temperature,  pressure,  heating 
surface  and  grate  area  under  which  the  tests  were  made,  and 
Table  IV  gives  a  few  of  the  most  important  results.  In  some 
cases  the  heat  value  of  the  coals  used  was  not  obtained  and  sev- 
eral of  the  columns  dependent  upon  it  are  left  vacant.  The  head- 
ings of  the  tables  are  self-explanatory.  Where  a  series  of  tests 
was  made  with  the  same  coals  under  like  conditions,  the  average 
of  the  series  is  reported  together  with  the  number  of  tests  in  the 
series.  Where  the  coal  and  steam  have  been  assumed  moisture 
free  and  when  the  moisture  in  the  coal  was  obtained  by  drying  a 
known  amount  above  the  boiler,  indications  have  been  made  in  the 
tables . 

In  the  computation  of  results,  the  usual  correction  for  qual- 
ity of  steam  by  proportional  weights  of  steam  and  water  was  used. 
The  combustible  was  computed  from  the  weights  of  coal  and  ash 
and  not  from  the  ultimate  analysis  of  the  coal,  and  it  is,  therefore, 
in  slight  error  to  the  extent  of  the  ash  which  passed  over  the 
bridge  wall.  The  basis  for  the  rating  of  the  boilers  varied  from 
10  to  15  square  feet  of  heating  surface  per  horse-power  according 
to  the  different  types  of  boilers  used.  The  B.  T.  U.  of  the  coal, 
given  in  the  table,  were  obtained  from  an  analysis  of  the  sample 

taken  during  the  test. 

• 

DISCUSSION  OF  RESULTS 

On  account  of  the  wide  variation  of  conditions  obtaining  in 
the  tests  reported,  an  exact  comparison  was  hardly  possible.  A 
general  comparison  of  results  with  different  types  of  boilers  and 
grates  has,  however,  been  attempted.  Such  a  comparison  is 
shown  in  Table  V,  which  contains  the  general  average  of  the  re- 
sults of  all  trials  made  with  the  same  type  of  boiler  and  grate, 
irrespective  of  all  other  conditions.  It  also  shows  the  average  of 


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FUEL  TESTS  WITH  ILLINOIS  COALS 


35 


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36 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


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FUKL  TESTS  WITH  ILLINOIS  COALS 


37 


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38 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


the  results  of  the  ten  highest  tests  together  with  the  single  high- 
est result  obtained.  The  basis  of  comparison  is  the  equivalent 
pounds  of  water  evaporated  from  and  at  212°  F.  per  pound  of  dry 
coal.  The  same  table  also  contains  the  average  of  the  results  of 
six  tests  with  Illinois  coals  made  by  the  Boiler  Division  of  the 
Fuel  Testing  Plant  of  the  United  States  Geological  Survey  at  St. 
Louis.  It  is  interesting  to  note  that  in  these  latter  tests  in  which 
hand -firing  and  plain  grates  were  used,  the  results  obtained  are 
better  than  any  of  the  others  recorded,  including  the  results  of 
tests  in  which  mechanical  stokers  were  used.  This  fact  may  be 
taken  to  indicate  that  the  maximum  efficiency  of  Illinois  coals  is 
rarely  obtained  under  present  average  conditions.  It  is  probable 
that  with  a  closer  study  of  furnace  conditions,  even  these  results 
may  be  improved.  The  general  tests  reported  in  Tables  3  to  5  in- 
clude a  number  of  trials  made  with  special  objects  in  view.  Several 
of  these  trials  are  described  as  follows: 

1.  Tests  of  a  small  horizontal  tubular  boiler  of  40  horse- 
power, to  determine  its  performance  with  varying  rates  of  com- 
bustion. The  results  of  these  tests  are  given  below. 

RESULTS  OF  A  BOILER  TRIAL  SHOWING  EFFECTS  OF  RATE 

OF  COMBUSTION  ON  THE  PERFORMANCE  OF 

HORIZONTAL  TUBULAR  BOILER 


Dry  coal  per  square  foot  of 

grate  surface  per  hour 

6.80 

9.30 

11.00 

12.00 

14.00 

Equivalent  evaporation 

from  and  at  212°  F.  per 

pound  of  dry  coal 

6.20 

6.55 

6.57 

6.37 

5.75 

Horse-power  in  per  cent  of 

rated  capacity  (40) 

52  50 

87.50 

107.50 

115.00 

122.50 

Temperature     of     escaping 

gases 

432.00 

447.00 

501.00 

516.00 

553.00 

The  same  kind  of  coal  was  used  in  all  these  tests,  and  conditions 
remained  nearly  constant.  It  is  evident  that  the  maximum  results 
were  obtained  with  the  boiler  running  at  its  rated  capacity,  with 
the  flue  gas  temperature  about  500°  F.  With  an  increase  in  the 
rate  of  combustion,  the  capacity  and  flue  gas  temperature  increased 
and  the  evaporation  dropped  off. 

2.  Tests  to  determine  the  effect  of  soot  deposits  on  the  evap- 
oration of  a  small  horizontal  tubular  boiler.  These  tests  were  made 
on  the  same  boiler  as  the  preceding  series  and  with  results  as 
follows : 


PABBCANDBDIBKS]      FUEL  TESTS  WITH  ILLINOIS  COALS 


RESULTS  OF  BOILER  TRIALS  MADE  TO  DETERMINE  THE 

EFFECT  OF  SOOT  DEPOSITS  ON  THE  EVAPORATION 

OF  A  HORIZONTAL  TUBULAR  BOILER 


•  First  Series 
(5  days) 
Soot  allowed 
to  remain  on 
tubes 

Second  Series 
(5  days) 
Tubes  cleaned 
each  morning 

Third  Series 
(6  days) 
Soot  allowed  to 
remain  on 
tubes 

Equivalent  evaporation  from  and   at 
212°  F.  per  pound  of  dry  coal 

6.20 

7.04 

6.23 

Dry  coal  per  sq.  ft.  of  grate  surface 
per  hour 

13.40 

9.09 

13.40 

Horse  power  in  per  cent  of  rated 
capacity 

111.00 

99.00 

115.00 

Temperature  of  escaping  gases 

627.00 

546  00 

698.00 

It  is  evident  from  the  results  that  the  effect  of  the  soot  de- 
posit on  the  evaporation  is  not  very  marked.  It  is  interesting  to 
note  that  in  the  first  and  last  series,  in  which  the  soot  was  allowed  to 
remain  on  the  tubes,  the  soot  burned  upon  reaching  a  certain 
thickness,  leaving  but  a  very  thin  layer.  In  all  three  series  the 
conditions  were  held  as  nearly  constant  as  possible,  although  in 
the  second  series  the  load  fluctuated  somewhat  on  the  different 
days. 


40 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


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BBECKKNBIDGE,  1 
PAKB  AND  DIRKS J 


FUEL  TESTS  WITH  ILLINOIS  COALS 


41 


3.  Tests  of  a  water- tube  boiler  with  chain  grate  stoker  to 
determine  the  relative  economy  of  a  6- inch  and  an  8- inch  fuel  bed 
with  various  rates  of  combustion. 

The  results  of  these  tests  are  best  shown  by  the  curves  in 
Fig.  9. 


15  20  25  30  35  40 

DRY   COAL.    PER    SQ.  PT.   or-   GRATEL  SURFACE  ptR  Hrr-Lns. 

FIG.  9     CURVES  SHOWING   THE  RELATIVE  ECONOMY  OF  A  6-iNCH  AND 
8-iNCH  FUEL  BED  IN  A  CHAIN  GRATE  STOKER 

They  show  that  under  the  conditions  of  the  test,  the  8- inch 
fire  was  the  more  efficient,  giving  an  equivalent  evaporation  per 
pound  of  dry  coal  10  per  cent  greater  than  the  6-inch  fire,  when 
operating  at  the  rated  capacity  of  the  boiler.  The  same  coal  was 
used  throughout  this  series.  The  averages  of  the  results  of  these 
tests  are  reported  in  Tables  III  and  IV,  viz.,  Nos.  41,  42,  43  and 
44.  In  Figs.  10,  11  and  12  are  shown  a  few  of  the  characteristic 
results  of  boiler  trials  made  on  water-tube  boilers  with  chain  grate 
stokers.  These  diagrams  are  plotted  from  the  results  of  38 
trials,  and  each  point  on  the  diagram  represents  the  average  of  5 
trials.  It  is  safe  to  assume,  therefore,  that  the  results  represent 
average  conditions. 


42 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


IO5OO 


11000 
MEAT 


11500 

VAV.UE 


12000  12500 

OF  DRY  COAU-B.T.  u. 


FIG. 


10     CHART  SHOWING  VARIATION  IN    BOILER  PERFORMANCE  WITH 
COALS  OF  DIFFERENT  HEAT  VALUE 


Fig.  10  shows  the  results  of  trials,  in  which  coals  of  highest, 
lowest  and  mean  heat  values  were  used,  plotted  on  a  basis  of  heat 
value.  The  sudden  drop  in  the  equivalent  evaporation  per  pound 
of  dry  coal,  with  coals  of  low  and  medium  heat  value  is  no  doubt 
due  to  the  large  increase  in  the  flue  gas  temperature  with  con- 
stant rate  of  combustion  and  capacity.  With  coals  of  medium  and 
high  heat  value  the  equivalent  evaporation  increases  with  increas- 
ing rate  of  combustion  and  capacity,  the  flue  gas  temperature 
remaining  constant.  It  is  evident  from  the  diagram  that  the  effect 
of  the  heat  value  of  the  coal  is  not  very  marked,  a  large  increase, 
however, -other  conditions  remaining  constant,  causing  an  increase 
in  the  evaporation  per  pound  of  coal,  as  will  be  seen  in  Fig.  12. 


BBECKENBIDGK,  ~| 
PABB  AND  DIBKSJ 


FUEL  TESTS  WITH  ILLINOIS  COALS 


43 


IO  »5  2O 

DRV  COAL  PtR   So  FT 


25         30 
Or  GRATt  SuRrACt 


35 
PER  HR.  -  LBS. 


FIG.  11 


CHART  SHOWING  VARIATION  IN  BOILER  PERFORMANCE  WITH 
VARYING  RATES  OP  COMBUSTION 


In  Fig.  11  the  results  of  a  boiler  trial  are  plotted  on  a  basis 
of  rate  of  combustion.  It  is  evident  from  the  diagram  that  the 
equivalent  evaporation  per  pound  of  dry  coal  increases  with  the 
rate  of  combustion  until  the  capacity  reaches  100  per  cent,  or  the 
rated  capacity,  the  heat  value  of  the  coal  remaining  approxi- 
mately constant,  the  flue  gas  temperature  at  this  point  being  500° 
F.  With  a  further  increase  in  the  rate  of  combustion  the  capacity 
and  flue  gas  temperature  still  increase  but  the  equivalent  evapo- 
ration per  pound  of  coal  decreases.  This  carve,  if  it  may  be  called 
such,  might  be  named  the  characteristic  curve  of  the  boiler,  and 
is  important  because  it  shows  the  rate  of  combustion  above  which 
the  evaporation  per  pound  of  coal  decreases. 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


20  40  60  00 

HORSC-POWER  .     PERCENT 


100  leo  140 

RATED    CAPACITY" 


FIG.  12    CHART  SHOWING  VARIATION  IN  THE  PERFORMANCE 
OF  A  BOILER  WORKING  AT  DIFFERENT  CAPACITIES 

The  effect  of  capacity  on  the  evaporation  is  shown  by  the 
diagram  in  Fig.  12.  It  is  seen  that  here  as  in  the  previous  fig- 
are  the  evaporation  per  pound  of  dry  coal  again  increases  with  an 
increase  in  the  capacity  due  to  an  increased  rate  of  combustion. 
However,  instead  of  attaining  a  maximum  at  100  percent  capacity, 
it  increases,  with  a  further  increase  of  capacity  and  rate  of  com- 
bustion. At  first  sight  this  seems  contradictory  to  the  previous 
diagram,  Fig.  11;  however,  it  is  evident  that  this  increase  is  not 
due  to  this  further  increase  in  the  rate  of  combustion  and  capacity, 
but  is  due  to  the  sudden  increase  in  the  heat  value  of  the  coal 
(about  10  per  cent)  used. 

V  ARRANGEMENTS  FOR  FUTURE  FUEL  TESTS 

In  publishing  this  bulletin  it  has  been  the  desire  to  record  the 
results  of  the  most  important  tests  of  boilers  fired  with  Illinois 


FUEL  TE8TS  WITH  ILLINOIS  COALS  45 

coals,  that  have  been  made  up  to  date.  During  the  year  1906  the 
Engineering  Experiment  Station  at  the  University  purchased 
and  installed  a  plant  designed  especially  for  conducting  a  series 
of  fuel  tests  of  Illinois  coals.  The  plant  consists  of  a  210  H.  P. 
Heine  water- tube  boiler  together  with  a  Green  chain  grate  stoker 
and  a  Sturtevant  economizer  and  induced  draft  fan  and  engine. 
This  boiler  is  a  duplicate  of  the  boilers  used  by  the  United  States 
government  in  the  fuel  tests  in  progress  at  St.  Louis  under  the 
direction  of  the  United  States  Geological  Survey.  It  was  thought 
that  in  this  way  the  fuel  tests  here  at  the  University  would  be  in 
a  measure  comparable  with  the  tests  made  by  the  government  on 
coals  from  all  parts  of  the  United  States. 

The  rapid  growth  of  the  industrial  interests  of  Illinois  de- 
mands a  careful  study  of  the  great  fuel  supply,  and  no 'effort 
should  be  spared  in  the  introduction  and  promulgation  of  improved 
methods  and  processes  in  the  production,  treatment  and  con- 
sumption of  its  coal.  In  the  tests  of  Illinois  coals  which  it  is  now 
proposed  to  make,  less  attention  will  be  paid  to  routine  boiler 
tests,  familiarly  known  as  such,  and  more  attention  will  be  given 
to  a  scientific  study  of  fuel  treatment  before  burning  and  to  a 
study  of  those  furnace  constructions  and  conditions  which  give 
promise  of  maximum  results.  In  order  that  future  tests  may  be  con- 
ducted along  lines  which  will  meet  with  the  general  approval  of 
the  various  interests  of  the  state,  a  Conference  Committee  on 
Fuel  Tests  has  been  appointed  consisting  of  the  members  named 
below  and  representing  the  organizations  indicated: 

H.  Foster  Bain,    Director  State  Geological  Survey,  Urbana, 
111.,  representing  the  State  Geological  Survey; 

A.  Bement,     Consulting  Engineer,  Chicago,     the  Western 
Society  of  Engineers; 

Edwin  H.  Cheney,  President  Fuel  Engineering  Co. ,  Chicago, 
the  Building  Managers'  Association  of  Chicago; 

F.  H.  Clark,  Gen.  Supt.  Motive  Power  Burlington  Road, 
C.  B.  &  Q.  Ry.,  Chicago,  the  Western  Railway  Club; 

Adolph  Mueller,  President  H.  Mueller  Mfg.  Co. ,  Decatur, 
111.,  the  Illinois  Manufacturers'  Association; 

Carl  Scholz,  President  Coal  Valley  Mining  Co.,  Chicago, 
the  Illinois  Coal  Operators'  Association; 

A.  V.  Schroeder,  Decatur   Railway  and   Light  Company, 
Decatur,  111. ,  the  State  Electric  Light  Association; 


46 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


Wm.  L.  Abbot,  Chief  Operating  Engineer,  Chicago  Edison 
Co.,  Chicago,  the  Board  of  Trustees  University  of  Illinois; 


FUEL  TESTS  WITH  ILLINOIS  COALS  47 

L.  P.  Breckenridge,  Director  Engineering  Experiment 
Station,  University  of  Illinois,  Urbana,  111. 

Reference  has  been  made  to  the  government  fuel  tests  at 
St.  Louis.  It  should  be  stated  that  the  work  of  the  boiler  division 
of  these  tests  has  been  carried  on  under  the  direction  of  the 
Director  of  the  Illinois  Engineering  Experiment  Station,  who 
will  also  have  charge  of  the  tests  made  at  the  University  of  Illinois. 
Copies  of  Professional  Paper  No.  48,  containing  a  report  on  the 
operations  of  the  government  coal  testing  plant  at  St.  Louis  may 
be  obtained  upon  application  to  a  member  of  Congress  or  to  the 
Director  of  the  United  States  Geological  Survey,  Washington,  D.C. 

It  is  not  the  intention  of  this  bulletin  to  discuss  the  subject  of 
fuel  testing.  A  future  bulletin  will  take  up  that  subject  and  will 
also  describe  in  full  the  plant  provided  for  such  tests  at  this 
University.  Attention  is  called,  however,  to  the  facilities  now  of- 
fered for  this  important  work.  It  is  hoped  that  mine  owners  and 
manufacturers  will  find  it  advantageous  to  cooperate  with  the  En- 
gineering Experiment  Station  in  the  proposed  tests.  The  Station 
Staff  will  always  be  glad  to  receive  such  suggestions  concerning 
this  work  as  those  interested  may  desire  to  offer. 

VI    CHEMICAL  ANALYSIS  AND  HEAT  VALUES  OF 
ILLINOIS  COALS 

By  S.  W.  PARR,  Professor  of  Applied  Chemistry 

The  accompanying  results  of  chemical  analyses  of  Illinois  coals 
may  be  divided  into  three  classes:  first,  those  which  were  directly 
connected  with  the  boiler  tests  conducted  by  the  department  of 
Mechanical  Engineering,  and  which  are  listed  in  a  separate  table, 
covering  such  work  from  the  year  189 1  to  1905;  second,  in  connec- 
tion with  thesis  work  by  Mr.  F.  C.  Koch  in  1901,  there  were 
assembled  by  him  the  results  of  all  analyses  of  Illinois  coals  which 
had  been  made  by  the  department  of  Chemistry  previous  to  that 
date.  These  results  were  published  together  with  his  own  work 
in  a  bulletin  through  the  courtesy  of  Secretary  Ross  of  the  Bureau 
of  Labor  Statistics  in  the  report  of  that  Bureau  in  1902.  They 
are  designated  in  the  tables  by  the  letters  B.  L.  S.  The  third 
series  of  results  comprises  the  work  on  one  hundred  fifty 
samples  of  Illinois  coal  collected  in  1904  and  published  in  a 
separate  bulletin  in  connection  with  the  exhibit  of  mines  and  min- 


48  ILLINOIS    ENGINEERING    EXPERIMENT    STATION 

erals  at  the  St.  Louis  Exposition.  These  results  are  designated 
in  the  tables  by  S.  W.  P.  The  sum  total  of  data  which  has  thus 
resulted,  while  of  a  somewhat  desultory  nature,  constitutes  a  very 
considerable  contribution  to  our  knowledge  of  the  constituents  of 
Illinois  coals.  It  is  to  be  noted  that  the  processes  employed  in 
connection  with  this  series  were  confined  almost  exclusively  to  the 
method  of  proximate  analysis.  In  the  future  the  more  exacting 
demands  of  modern  methods  will  require  extended  data  such  as 
are  furnished  by  both  proximate  and  ultimate  analysis,  including 
of  course  the  determination  of  calorific  units.  It  may  be  well  there- 
fore, at  the  present  time,  to  assemble  the  information  obtainable 
up  to  the  present  date,  compiling  it  as  in  the  accompanying  tables, 
and  also  to  discuss  briefly  some  of  the  terms  which  are  used  in 
connection  with  the  chemical  work  on  coals.  The  chemist  employs 
terms  and  processes  which  are  also  used  by  the  engineer,  but  it 
does  not  always  follow  that  their  use  of  terms  is  in  accord. 

Moisture. — Moisture  in  coal  is  constantly  undergoing  a  change 
as  to  quantity.  The  percentage  contained  at  the  time  of  break- 
ing out  the  coal  from  the  vein  is  greater  than  at  any  subsequent 
stage  of  its  history,  unless  possibly  it  be  under  the  conditions  of 
rain  or  snow  or  drenching  with  the  hose.  Some  of  this  moisture 
which  is  normally  contained  in  the  coal  is  lost  when  the  coal  is 
exposed  to  the  air,  being  in  this  respect  like  water  which  has  been 
poured  upon  the  coal.  But  there  remains  moisture  in  the  coal 
after  air- dry  ing  and  which  is  removed  only  at  the  temperature  of 
boiling  water.  This  moisture  is  described  as  hygroscopic.  If  now 
the  chemist  works  upon  a  sample  which  is  overcharged  with  mois- 
ture, as  is  the  condition  when  the  sample  is  freshly  mined,  it  will 
be  constantly  losing  in  weight  and  modifying  his  results.  Simi- 
larly, if  he  works  upon  a  sample  which  has  been  completely  dried 
in  the  oven,  it  will  have  great  avidity  for  moisture  and  be  con- 
stantly gaining  in  weight  throughout  his  work.  He,  therefore,  pro- 
ceeds in  his  determinations,  as  a  rule,  with  the  coal  in  that  condi- 
tion which  is  least  affected  by  external  conditions,  viz.,  in  the  air- 
dry  state  with  the  normal  amount  of  hygroscopic  moisture  pre- 
sent, but  without  the  excess  of  water,  which  might  be  termed 
water  of  saturation. 

Therefore,  we  have  three  distinctly  different  conditions:  first, 
the  wet  coal;  second,  the  air-dry  coal;  and  third,  the  oven-dry 
state.  The  engineer,  however,  not  having  to  do  with  the  condi- 


TE8T8  WITH  ILLINOIS  COALS  49 

tions  under  which  the  chemist  works,  recognizes  only  the  two 
phases,  either  the  wet  or  dry,  and  by  this  latter  term  he  means 
the  oven-dry  state.  The  failure  on  the  part  of  the  engineer  and  the 
chemist  to  recognize  these  terms  often  leads  to  misinterpretation 
of  results.  The  chemists,  therefore,  should  agree  to  such  use  of 
terms  relating  to  water  as  have  become  firmly  established  in  en- 
gineering literature:  viz.,  that  dry  coal  refers  to  moisture  free 
coal  or  to  the  oven- dry  state,  and  second,  that  wet  coal  refers  to 
the  condition  as  received  or  previous  to  any  process  of  air-drying, 
and  that  it  is  one  or  the  other  of  these  conditions  that  is  of  inter- 
est to  the  engineer,  regardless  of  how  important  it  may  be  to  the 
chemist  to  proceed  upon  the  basis  of  the  air-dry  condition. 

It  may  not  be  out  of  place  further  to  indicate  how  results  may 
be  transferred  from  one  basis  to  the  other.  It  is  not  an  uncom- 
mon practice  for  the  chemist  to  report  his  results  on  the  air- dry 
basis,  in  which  case  he  should  also  report  the  amount  of  moisture 
lost  upon  air  drying,  provided  his  sample  comes  to  him  sealed  in 
such  a  way  as  to  make  this  factor  possible.  Suppose,  for  exam- 
ple, that  the  loss  of  moisture  upon  air-drying  is  4  per  cent,  then 
all  his  results  reported  on  fche  air-dry  basis  would  be  changed 
to  the  wet  coal  basis  by  multiplying  each  by  96  per  cent;  not  by 
dividing  by  104  per  cent  as  is  often  erroneously  done.  This  will 
make  small  difference  in  a  constituent  which  has  a  low  percentage 
factor,  but  the  error  is  very  considerable  in  a  factor  like  the  fixed 
carbon  which  is  from  40  to  50  per  cent.  This  may  seem  like  a  sim- 
ple arithmetical  problem  to  mention  in  this  connection,  but  it  is 
one  not  always  correctly  interpreted. 

Conversely,  if  it  is  desired  to  change  factors  to  the  dry  coal 
basis,  each  factor  should  be  divided  by  100  minus  the  percentage 
content  of  water  in  that  condition  from  which  the  transfer  is  be- 
ing made.  For  example,  if  we  are  calculating  this  coal  from  the 
air -dry  state,  supposing  it  to  have  6  per  cent  of  moisture  present, 
each  factor  should  be  divided  by  94  per  cent,  but  it  should  be  noted 
that  if  we  are  calculating  from  the  wet-coal  condition  our  divi- 
sor will  not  be  100  per  cent  minus  the  sum  of  the  two  factors,  6  and 
4,  as  in  the  above  illustration,  but  100  minus  96  per  cent  of  6 
plus  4,  or  90.24.  Here  again  is  a  not  uncommon  place  for  stum- 
bling in  what  might  seem  to 'be  a  simple  arithmetical  problem. 

Volatile  Matter. — When  coal  is  subjected  to  high  temperature 
out  of  contact  with  the  air,  a  considerable  amount  is  driven  off  as 


50  ILLINOIS    ENGINEERING    EXPERIMENT    STATION 

volatile  matter.  This  includes,  also,  of  course,  any  moisture  in 
the  sample,  if  we  start  with  a  portion  which  has  not  been  dried  in 
the  oven.  Now  an  even  greater  discrepancy  in  the  use  of  terms 
has  come  into  use  in  connection  with  this  constituent  than  is  the 
case  with  different  forms  of  water.  One  of  the  oldest  terms  is 
that  of  volatile  carbon.  This  is  both  incorrect  and  meaningless 
because  carbon  is  not  volatile,  and  because  the  constituents  of  this 
material  are  numerous  and  complex.  The  term  that  is  perhaps  most 
frequently  met  designates  this  material  as  volatile  combustible. 
This  again  is  incorrect  and  misleading,  as  this  material  in  the  or- 
dinary bituminous  type  of  coal  has  from  one-third  to  one-half  of  its 
weight  made  up  of  non-combustible  material.  It  is  evident,  there- 
fore, that  the  only  proper  term  among  those  commonly  in  use  for 
this  constituent  is  that  of  volatile  matter.  The  only  restriction  in- 
deed in  connection  with  this  term  is  to  understand,  as  is  the  uni- 
form custom,  that  the  moisture  of  the  coal  is  not  included.  A  word 
may  be  in  place  here  in  connection  with  a  term  which  is  occasion- 
ally met,  and  is  likely  to  be  more  frequently  used  than  formerly. 
This  term  is  intended  to  designate  that  part  of  the  volatile  matter 
which  does  not  burn.  This  constituent  is  sometimes  referred  to 
as  "water  of  composition".  It  is  not  included  in  any  of  the  re- 
suits  listed  in  the  following  tables,  and  hence  its  use  does  not  en- 
ter into  any  of  the  discussions  in  this  bulletin.  It  is  noted  in  this 
connection,  however,  in  order  that  it  may  not  be  confused  with 
any  of  those  terms  which  are  intended  to  designate  the  water  in 
its  ordinary  form  and  which  are  capable  of  being  driven  off  at 
the  temperature  of  boiling  water.  This  property  does  not  belong 
to  the  water  of  composition,  as  this  substance  like  the  other  part 
of  the  volatile  matter,  requires  a  red  heat  for  its  dissociation. 

Fixed  Carbon  and  Ash. — Concerning  these  constituents  there 
is  no  disagreement  as  to  the  use  of  terms  unless  it  be  the  occasion- 
al use  of  the  word  coke.  Coke  in  its  proper  and  technical  sense 
should  apply  to  the  residue  including  the  ash  after  subjecting  the 
coal  to  destructive  distillation.  It  is,  therefore,  not  proper  to 
designate  the  fixed  carbon  as  coke,  though  it  would  be  proper,  of 
course,  to  use  the  term  "coking  carbon"  in  this  connection.  The 
preferable  term  and  the  one  commonly  employed,  however,  for 
this  material  is  that  of  fixed  carbon. 

Methods  of  Analysis. — The  methods  of  analysis  employed  are 
those  in  common  use  and  their  description  is  so  easily  accessible 


BBECKENBIDGE.  1        FTTlrr     TT^qT^^ftl^tf  V£xs*#nTQ    PO  A  T  Q  ^  1 

PARR  AND  DIRKS  J  U  -^    L  ^8  J          »fc*SLl±-ai»4rnN  U    S    L/UAL.S 

that  no  repetition  is  necessary  here.  Reference  may  be  made  to 
the  report  of  the  committee  of  the  American  Chemical  Society  on 
coal  analysis.1 

Calorific  Value. — The  determination  of  heat  units  in  coals  is, 
of  course,  a  necessity  in  connection  with  any  well  conducted  boiler 
test.  Two  systems  of  units  are  employed,  viz. ,  the  kilo  calories 
and  the  British  Thermal  Units,  designated  as  B.  T.  U.  Each  unit 
is  the  measure  of  heat  imparted  to  the  water  by  an  equal  weight 
of  coal.  They  would,  therefore,  be  identical  if  it  were  not  for  the 
fact  that  the  one  is  read  on  the  Centigrade  scale  and  the  other  on 
the  Fahrenheit  scale.  The  transfer,  therefore,  of  calories  per 
kilo  over  to  B.  T.  U.  per  pound  is  effected  by  multiplying  by  the 
ratio  of  9:5  or  1.8. 

There  are  four  types  of  instruments  in  use  for  measuring  the 
heat  value  of  coals.  The  first  and  most  elaborate  is  the  Mahler 
instrument  which  has  numerous  modifications  as  to  detail,  but 
which  embodies  the  use  of  a  steel  bomb  capable  of  maintaining 
oxygen  from  twenty  to  twenty- five  atmospheres  pressure.  The 
next  in  the  order  of  time  is  the  Fisher  calorimeter  which  burns 
the  sample  of  coal  in  a  small  chamber  supplied  with  oxygen  at  at- 
mospheric pressure.  The  third  type  may  be  designated  as  the  L. 
Thompson  calorimeter,  wherein  the  coal  is  mixed  with  a  chemical 
which  in  itself  supplies  the  oxygen  for  carrying  on  the  combus- 
tion and  in  which  the  gaseous  products  are  allowed  to  bubble  up 
through  the  water,  thus  imparting  their  heat  to  the  liquid.  The 
fourth  type  may  be  designated  as  the  Parr  calorimeter  which  also 
employs  a  chemical  having  its  own  supply  of  oxygen,  but  which 
absorbs  the  gaseous  products,  thus  retaining  all  the  heat  of  the 
reaction  for  more  accurate  measurements  by  the  thermometer.  Of 
the  second  and  third  types,  it  may  be  said  that  owing  either  to  in- 
completeness of  combustion  or  to  loss  of  heat  by  transmission  of 
the  gases,  results  are  obtained  which  are  not  of  sufficient  accuracy 
for  reliable  work.  Results  from  the  Thompson  calorimeter  are 
reported  by  certain  authorities  to  admit  of  variations  amounting 
to  15  per  cent.  The  Mahler  type  of  calorimeter  is  accurate  when 
operated  by  one  thoroughly  familiar  with  such  processes.  The 
Parr  calorimeter  is  the  one  used  in  connection  with  the  analyses 
in  these  tables  of  all  coals  made  since  1900,  and  is  now  the  instru- 


IJour.  Am.  Chem.  Soc.  Vol.  XXI.  p.  1130. 


52 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


ment  most  commonly  used  in  technical  work.     A  brief  description 
of  this  apparatus  follows : 

Pig.  13  shows  the  relative  position  of  parts.  The  can  A.  A. 
for  the  water  has  a  capacity  of  2  litres.  The  insulating  ves- 
sels B.B.  and  C.C.  are  of  indurated  fiber.  The  charge  of  coal  and 
chemical  is  put  in  the  cartridge  D.  Upon  ignition,  the  heat  gen- 
erated is  imparted  to  the  water  and  the  rise  in  temperature  is  in- 
dicated on  the  finely  graduated  thermometer  T.  The  cartridge 
or  bomb  rests  on  the  pivot  F  and  is  made  to  revolve,  and  by  aid 
of  the  small  turbine  wings  attached  effects  a  complete  circula- 
tion of  the  water  and  equalization  of  temperature. 

The  reaction  accompanying  the  combustion  may  be  repre- 
sented by  the  equation: 

56Na2O2  -j-   C25H18O3  =  25   Na2CO3  -f-    18  NaOH   -f   22  Na2O 

Sod.  perox.  Coal  Sod.  carb.  Sod.  hydrate          Sod.  oxide 


FIG.  13 


FUEL  TESTS  WITH  ILLINOIS  COALS  53 

With  certain  substances  such  as  coke,  anthracites,  petrole- 
ums, etc.,  a  more  strongly  or  vigorously  oxidizing  medium  is 
needed  than  exists  in  the  peroxide  alone.  This  may  be  secured 
by  various  additions.  The  most  effective  are:  A  mixture  of  po- 
tassium chlorate  and  nitrate  in  the  proportion  of  1  to  4  and  this 
mixture  used  in  the  ratio  of  1  to  10  of  the  sodium  peroxide;  an- 
other effective  mixture  is  an  addition  of  potassium  persulphate  in 
the  ratio  of  1  to  10  of  the  sodium  peroxide.  Other  substances  fa- 
cilitate the  oxidation,  notably  ammonium  salts  and  certain  organic 
substances,  as  tartaric  or  oxalic  acid,  benzoic  acid,  etc.  In  the 
work  on  Illinois  coals,  while  ordinarily  no  extra  chemical  would 
be  necessary,  still  in  certain  cases,  such  as  extra  slaty  coals  and 
coals  with  excessive  volatile  matter,  and  also  to  guard  against 
variations  in  the  quality  of  the  sodium  peroxide,  a  mixture  as  first 
described  above,  of  chlorate  and  nitrate,  has  uniformly  been 
used  throughout  these  tests. 

Further  extension  of  the  use  of  the  instrument  to  other  types 
of  coal  and  to  petroleum  has  made  it  necessary  to  extend  still  fur- 
ther the  oxidizing  power  of  the  chemicals  employed  beyond  what 
is  afforded  by  the  chlorate  mixture.  In  addition  to  this  the  use 
of  the  residue  for  determining  the  total  carbon  and  sulphur  has 
made  it  highly  desirable  in  such  additional  chemicals  to  avoid  the 
use  of  compounds  containing  carbon  or  sulphur.  To  meet  these 
conditions,  the  so-called  "boro- mixture"  has  been  devised.  It 
consists  of: 

Boric  acid 11  parts 

Potassium  chlorate 4  parts 

Magnesium  powder 1  part 

Its  correction  factor  is  found  by  trial  with  a  pure  chemical  of 
known  heat  value,  such  as  napthalene  or  by  burning  with  a  coal 
whose  heat  value  is  already  accurately  known.  This  mixture  has 
the  further  advantage  of  carrying  on  a  combination  with  material 
so  low  in  carbonaceous  matter  as  to  be  non  burning  by  ordinary 
methods,  such  as  ashes  and  coals  of  very  high  ash  content. 

Still  further  modifications  relate  to  the  bomb  as  shown  in 
Fig.  14,  and  have  to  do  mainly  with  the  avoidance  of  screw 
threads  on  the  interior  of  the  combustion  chamber,  especially  in 
the  upper  part,  where  particles  tend  to  lodge  and  thus  escape 
combustion;  also  in  jacketing  the  lower  part  of  the  chamber  to 
avoid  direct  contact  with  the  water,  thereby  avoiding  rapid 


54 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


cooling  of  the  parts  and  extending  somewhat  the  period  of  high 
temperature,  thus  securing  a  more  perfect  combustion. 


a 


FIG.    14 

Calorific  Values  By  Calculation. — Numerous  methods  for  calcu- 
lating the  calorific  value  of  coal  have  been  proposed,  but  no 
method  can  be  said  to  have  any  value  which  is  not  based  on  a 
knowledge  of  the  percentage  constituents  of  the  total  carbon, 
available  hydrogen  and  sulphur.  Even  under  these  conditions 
the  results  by  calculation  are  not  always  in  agreement  with  the  in- 
dicated results  by  means  of  the  calorimeter,  and  in  any  event,  of 
course,  results  from  proximate  analysis  do  not  furnish  the  neces- 


FUEL  TEST8  WITH  ILLINOIS  COALS  55 

sary  data  for  this  calculation.  When  this  method  is  used  the  Du- 
long  formula  is  considered  the  most  nearly  accurate  and  is  as 
follows: 

Gal.  =  8080  +  34,500  H  +  2250  S 

In  the  results  here  recorded  the  necessary  factors  were  not 
always  available  for  applying  this  formula,  but  it  is  the  one  used 
wherever  calorific  values  by  calculation  are  included. 


56 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


BBECKENBIDGE.  ~| 
PAKB  AND  DIRKS  J 


FUEL  TESTS  WITH  ILLINOIS  COALS 


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66 


ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


TABLE  VIII 
LIST  OF  ILLINOIS  COALS  ANALYZED.   ARRANGED  BY  TOWNS 


Town 

County 

Ref  .  Number 
in  Table  of 
Analyses 

Assumption  . 

Christian 

8-12 

Astoria  

Fulton        

28-30 

Athens                            

Menard  . 

185-188 

Auburn  

Sangamon  

359-255 

Barclay                .... 

Sangamon. 

256-258 

Benton  

Franklin  

27 

Bloomington                ....         

McLean  

110-116 

Braceville 

Grundy 

50-51 

Braidwood  

Will. 

327-328 

Breese 

Clinton 

20-21 

Briar  Bluff  

Henry  

57 

Brighton 

Macoupin 

124 

Bush  

Williamson  

332 

Buxton                                       .       .  . 

Clinton 

22 

Cable  

Mercer  

196-197 

Canton.            .                  ....          .    . 

Fulton  

31-32 

Cantrall 

Sangamon 

259  260 

Carbondale     

Jackson  

62-65 

Cardiff 

Livingston 

95-96 

Carterville  

Williamson  

334-345 

Catlin 

Vermilion 

296-299 

Centralia  

Marion  

145-148 

Colchester. 

McDonough 

109 

Coif  ax  

McLean  

117 

Collinsville 

Madison. 

138-139 

Cuba  

Fulton  

33-36 

Danville. 

Vermilion.     ..  . 

300-310 

Dawson 

Sangamon 

261-264 

Decatur  .  . 

Macon  

118 

Delafleld 

Hamilton  . 

54 

De  Soto  

Jackson  

66-71 

Divernon 

Sangamon 

265 

Donkville  

Madison  

140-141 

Dunfermline   . 

Fulton 

38 

Du  Quoin  

Perry  

210-223 

EdwardsviUe.  .   . 

Madison,             

142-143 

Eldorado 

Saline 

239-243 

Elm  Grove  

Ad  ams  ... 

1-2 

Elmwood 

Peoria 

203-207 

Etherly  ...         

Knox  

76-77 

Fairbury 

Livingston 

97-98 

Fairmount  

Vermilion  

311-313 

Farmington. 

Fulton 

39-42 

Fiatt  

Pulton  

43 

Flatrock             

Crawford             .               

26   ' 

Forest- 

Livingston 

99-100 

French  Village              

St.  Glair  

233-234 

Galatia 

Saline. 

244 

Galva  

Henry  

58 

Gilchrist 

Mercer  .                            .               .... 

198 

Glen  Carbon 

Madison 

144 

Grape  Creek  

Vermilion  

314-316 

Greenview 

Menavd 

189-191 

Greenridge    

Macoupin  

125-126 

Harrisburg  . 

Saline 

245-251 

Herrin  

Williamson  

346-352 

Holies  

Peoria  

208-209 

Ivesdale 

Champaign 

7 

Joliet  

Will  

329-331 

49 

Kangley 

La  Salle 

79-80 

Kewanee  

Henry  

59-61 

Kinmundy 

Marion  ... 

149-150 

Ladd  

Bureau  

3-4 

Lake  Creek  .  .  . 

Williamson.  .  . 

353 

BRECKENBIDGE,  ~] 
PABB  AND  DIBKS  J 


FUEL  TESTS  WITH  ILLINOIS  COALS 


67 


TABLE  VIII    (Concluded) 


Town 

County 

Ref  .  Number 
in  Table  of 
Analyses 

La  Salle  

La  Salle  

81-84 

Lauder                                       

Williamson  ... 

354 

Lincoln.  .        

Logan  

101-106 

Litchfleld                 

Montgomery.        

201-202 

Bureau 

5 

Lowder                           

Sangamon  .     ...        

266 

McLeansboro 

Hamilton 

55 

Marissa      

St.  Clair  

235-238 

Middletown 

Menard  . 

192-193 

Moweaqua  

Shelby              

289-295 

Mt  Carbon 

Jackson. 

72 

Mt  Olive        

Macoupin  .        

127-132 

Mt  Pulasld 

Logan. 

107-108 

Perry 

"24 

Murphysboro 

Jackson. 

73-75 

Niantic  .   .              .  .           

Macon  

119-123 

Norris 

Fulton 

44-45 

Oakwood  

Vermilion  

317-322 

Odin 

Marion  .                                           

151-178 

Oglesby 

La  Salle 

85-88 

Palmyra 

Macoupin.          .          .         

133-135 

Pana  

Christian  

13-19 

Paradise 

Coles                     .... 

25 

Peru 

La  Salle 

89-90 

Petersburg 

Menard.  .                 

194-195 

Perry 

225-226 

Rido-ely 

Sangamon     

267-268 

Sangamon 

269-274 

St  David.,    . 

Fulton  

46-48 

St  John 

Perry 

227-228 

Sandoval  .  .                ...        

Marion  

179-181 

Sherrard 

Mercer 

199-200 

Soperville  .        ...                

Knox  

78 

Sparta 

Randolph  

229-230 

Sangamon 

275 

Springfield 

Sangamon.           

276-283 

Sangamon 

284 

Spring  Valley 

Bureau      

6 

La  Salle 

91-94 

Sugar  C**eek 

Wabash  

326 

Williamson 

355 

Tilden                                                  

Randolph  

231-232 

Toluca 

Marshall                             

182 

Trenton                                 ....        .... 

Clinton  

23-24 

Virden 

Macoupin.          

136-137 

Marshall 

183-184 

Westville 

Vermilion  

323 

S   Westville 

Vermilion 

324-325 

S  Wilmington 

Grundy  

52-53 

68  ILLINOIS    ENGINEERING    EXPERIMENT    STATION 


PUBLICATIONS   OF  THE   ENGINEERING   EXPERIMENT   STATION 


Bulletin  No.  1.  Tests  of  Reinforced  Concrete  Beams,  by  A.  N. 
Talbot.  1904. 

Circular  No.  1.  High-Speed  Tool  Steels,  by  L.  P.  Brecken- 
ridge.  1905. 

Bulletin  No.  2.  Tests  of  High- Speed  Tool  Steels  on  Cast  Iron, 
by  L.  P.  Breckenridge  and  Henry  B.  Dirks.  1905. 

Circular  No.  2.  Drainage  of  Earth  Roads,  by  Ira  O.  Baker. 
1906. 

Bulletin  No.  3.  The  Engineering  Experiment  Station  of  the 
University  of  Illinois,  by  L.  P.  Breckenridge.  1906. 

Bulletin  No.  4.  Tests  of  Reinforced  Concrete  Beams,  Series 
of  1905,  by  A.  N.  Talbot.  1906. 

Bulletin  No.  5.  Resistance  of  Tubes  to  Collapse,  by  A.  P. 
Carman.  1906. 

Bulletin  No.  6.  Holding  Power  of  Railroad  Spikes,  by  R.  I. 
Webber.  1906. 

Bulletin  No.  7.  Fuel  Tests  with  Illinois  Coals,  by  L.  P.  Breck- 
enridge. 1906. 


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