To Cornell University My Alma Mater This Bcok Is Dedicated COPYRIGHT, 192O O. F. HUNZIKER Fred Klein Co. Printers Chicago THE BUTTER INDUSTRY PREPARED FOR THE USE OF Creameries, Dairy Students and Pure Food Departments By OTTO F. HUNZIKER, B. S. A., M. S. A. tt Author of "Condensed Milk and Milk Powder" Formerly Professor of Dairy Husbandry, Purdue University Now Manager Manufacturing Department and Director Research Laboratory Blue Valley Creamery Co. Chicago Published by the Author LaGrange, Illinois 1920 Preface THE PURPOSE of this book is to acquaint the buttermaker with facts and methods that will assist him in the economical manufacture of butter of attractive flavor, good body, uniform color and superior keeping quality; to place before the teacher and student of buttermaking the newer knowl- edge of the science and art of butter manufacture; to bring the investigator and research worker in close touch with the real problems of the butter industry; and to point out to those in charge of food control the possibilities and limitations of composition and prop- erties of commercial butter. This book deals with the several phases of the but- ter industry, from the care and handling of the milk and cream on the farm to the table of the consumer, with special emphasis of the causes and practical pre- vention of the multitude of butter defects. It represents the author's best knowledge on the subject, derived from practical experience in com- mercial buttermaking, from scientific investigation and research of the problems of economy of manufacture and of production of quality, from the most authentic experimental data of other investigators throughout the dairy world, and from a profound study of the several sciences intimately related to buttermaking. O. F. HUNZIKER. Chicago, Feb. i, 1920. 574322 Acknowledgment In presenting the information contained in this volume to ^he Dairy World^ the author desires to express his sincere appreciation of the facilities provided and opportunities accorded him by the Blue Valley Creamery Company ', which made possible the revelation of new scientific truths of acknowledged value to the butter industry y and which greatly added to the comprehensiveness of this work. THE BUTTER INDUSTRY 9 CONTENTS Chapter I HISTORY AND DEVELOPMENT OF BUTTER INDUSTRY Early history — Later development — Influence of centrifugal cream sepa- rator— Influence of Babcock test — Influence of other inventions — In- fluence of dairy research, instruction and control — Influence of cream- ery promoter — Annual butter production in U. S. and in foreign countries — Number of creameries in U. S Pages 15-30 Chapter II CREAMERY ORGANIZATION, CONSTRUCTION AND EQUIP- MENT Creamery organizations — Mutual co-operative creamery asso. — Joint stock company with co-operative features — Proprietary creamery — Creamery corporation — Location of factory — Water supply — Sewage disposal — Type of building — Drainage and drains — Light — Ventilation — Store room — Cold room — Heating — Insulation of ammonia, brine, steam and water lines Pages 31-46 Chapter III BUYING MILK AND CREAM Systems of securing milk and cream — Direct deliveries — Cream routes — Skimming stations — Cream stations — Route and station shortages — Independent cream buyer — Farmers' co-operative marketing associa- tions— Direct shipper system — Concentration points — Management of patron Pages 31-60 Chapter IV CARE OF MILK AND CREAM ON THE FARM Healthy cows and attendants — Proper feed and water — Cleanliness — Clean- liness of separator bowl — How to wash the separator — Care of cream after separation — How to cool cream — Age of cream — Protection of cream in transit Pages 60-67 Chapter V SEPARATION OF MILK Purpose — Principle of separation — Methods of separation — Gravity separa- tion— Centrifugal separation — Theory of centrifugal separation — Con- struction of separator — Separator frame — Bowl and spindle — Skim- milk outlet— Cream outlet — Proportion of skim milk and cream — Supply tankj float and discharge pans — Driving mechanism — Power separators — Hand separators — Systems of oiling — Power require- ments— Capacity of separator — Conditions affecting skimming effi- ciency— Conditions affecting richness of cream — Advantages of cen- trifugal separation over gravity creaming Pages 68-118 10 THE BUTTER INDUSTRY Chapter VI RECEIVING MILK AND CREAM Grading of cream — Development — Methods of grading — Grading by taste and smell — Apparatus needed — Operation of grading — Classification of grades — Sampling milk and cream — Single samples — Composite sam- ples— Care of samples — Sampling frozen cream — Amount of cream sample — Weighing milk and cream — "Dumping" milk and cream — Can washing — Can washing equipment — Size and construction of cans — Rusty and damaged cans Pages 118-148 Chapter VII NEUTRALIZATION OF SOUR CREAM Definition — Object — Importance of correct neutralization — How to neutral- ize— Adoption of standard of acidity — Testing correctly for acidity — Choice of neutralizer — Preparation, strength and amount of neutral- izer — Affinity of lime for curd — Summary of action of lime in sour cream — Adding lime mix in proper manner — Effect of per cent acid in cream on accuracy of neutralization — Effect of per cent casein — Effect of amount of carbon dioxide in cream — Effect of time and temperature on acid reduction — Effect of neutralization on composi- tion of butter — Specific directions for neutralizing cream with lime — Neutralizing tables Pages 148-180 Chapter VIII PASTEURIZATION ' Definition— Objects — Improvement of flavor — Uniformity of quality — Dis- truction of disease germs — Improvement of keeping quality — Economic advantages— Essentials for successful pasteurization — Methods — Flash or continuous pasteurization — Flash pasteurizers — Regenerative heat- ers and coolers — Operation of flash pasteurizers — Temperature con- • trol — Cooling cream from flash pasteurizer — Vat or holding pasteuri- zation— Construction and operation of vat pasteurizers — Temperature and time of exposure — Cooling cream in vat pasteurizer — Flash and holding process combined — Cleaning and care of pasteurizers — Ad- vantages and disadvantages of flash and vat processes. Effect of pasteurization on flavor and texture of butter — Effect of pasteuriza- tion on exhaustiveness of churning — Blowing cream — Effect of blowing on flavor and keeping quality of butter Pages 180-224 Chapter IX CREAM RIPENING AND STARTERS Definition of cream ripening — Purpose — Effect on flavor and aroma — Effect on uniformity of quality — Effect on exhaustiveness of churn- ing— Effect on keeping quality — Natural ripening — Artificial ripening — Temperature — Ripening vats — Advantages of glass enameled vats — Time required for ripening — Proper acidity of ripened cream — Over- ripened cream — Methods to determine desired degree of acidity — Starter ripening vs. cream ripening — Starters — Natural and commer- cial starters — Directions for preparation of startoline — Directions for making commercial starter from whole milk, skim milk, condensed milk — Milk powder — Equipment for starter making — Acidity in starter — Amount of starter — Scoring starters Pages 224-265 THE BUTTER INDUSTRY 11 Chapter X CHURNING Object — Philosophy of churning — Milk and cream an emulsion — Surface tension — Absorption — Viscosity — Why cream thickens in churn — Why butter "breaks" suddenly — Solidification and coalescence of fat globules — Conditions affecting churnability of cream — Size of fat globules — Chemical properties of butterfat — Viscosity of cream — Churning temperature — Time of holding at churning temperature — Richness of cream — Acidity of cream — Nature and amount of agita- tion— Speed of churn — Amount of cream in churn — Preparation of chum — Sticky churns — Straining the cream — Addition of butter color — Gas in churn — When to stop the churn — Clnirning difficulties. Pages 265-310 Chapter XI WASHING, SALTING AND WORKING Purpose — Drawing-off buttermilk — Addition of water — Temperature of wash water — Effect on moisture content of butter — Overchurning in washwater — Regulating temperature of washwater — Purity of wash- water — Salting — Purpose — Amount of salt — Methods of salting — Dry salting — Wet salting — Brine salting — Types of salt — Quality and bac- teriological and chemical purity of salt — Solubility of butter salts — Condition of salt as affected by storage — Effect of salt on keeping quality, disease germs and moisture content of butter — Working — Purpose — Butterworkers — Overloading the churn — Manner and amount of working — Effect of working on body, color and moisture content of butter — Effect of working on flavor and keeping quality of butter Pages 310-363 Chapter XII PACKING BUTTER Variety of packages — Preparation of tubs, boxes, cubes and firkins — Prepa- ration of liners, circles and wrappers — Tin cans — Packing tubs, boxes, cubes and tins — Butter prints— Packing farm butter — Packing for par- cel post shipments — Packing for exhibits and scoring contests — Loss of moisture in packing — Cost of packing — Packing butter for U. S. Navy Pages 363-394 Chapter XIII THE OVERRUN Definition — Importance — Theoretical overrun— Actual overrun — Condi- tions affecting actual overrun — Composition of butter — Accuracy of weights and tests of cream — Mechanical losses — Examples of overruns in whole milk creamery and in farm separator creamery — Unavoidable discrepancies in weights and tests that affect overrun Pages 394-412 12 THE BUTTER INDUSTRY Chapter XIV MARKETS AND MARKETING Importance — Essentials in successful marketing — Marketing dairy butter — Selling creamery butter localfy — Selling to wholesale produce trade — Track sales — Delivered sales — Commission sales — Contract sales — Speculating in futures — Butter exchanges — The call — Butter quota- tions— Inspection and grading — Butter rules of N. Y. Mercantile Ex- change— Butter rules of Chicago Butter and Egg Board — Distribu- tion— Per capita consumption of butter in U. S. and abroad — Exports and Imports Pages 412-447 Chapter XV BUTTER STORAGE Time and duration — Distribution of commercial stocks of butter — Short held and long "held — Storage conditions — Air, light and heat — Humid- ity— Temperature — Shrinkage in storage — Deterioration in quality — Summary of effect of cold storage on quality of butter. .Pages 447-459 Chapter XVI BUTTER SCORING Definition — The score card — Valuation of defects — Ethics of butter scor- ing—Method and accuracy of scoring — Value of educational butter scoring contests Pages 459-466 Chapter XVII BUTTER DEFECTS Classification — Description — Causes and prevention of the following de- fects in flavor and aroma, body and texture, color — Defects in flavor and aroma: Flat, stale, sour, curdy, cheesy, unclean, cowy and barny, feedy and weedy, musty and smothered, garlic, moldy, yeasty, bitter, • oily, metallic, fishy, tallowy, storage, rancid, woody, scorched, coarse — Defects in body and texture: weak, greasy, salvy, crumbly, mealy, leaky, gritty — Defects in color: too high, too light, bleached, dull, mottled and wavy, white specks, yellow specks, green specks. Pages 459-530 Chapter XVIII COMPOSITION AND PROPERTIES OF BUTTER, MILK, CREAM, SKIMMILK AND BUTTERMILK Butter — Butterfat — Soluble, volatile, insoluble and non-volatile fats — Melting point — Physical structure — Water — Moisture control — Factory directions — Relation of moisture to quality — Curd — Salt — Lactose — Acid — Ash — Milk — Cream — Skimmilk — Buttermilk — Whey — Composi- tion of Ash and Separator Slime Pages 530-558 THE; BUTTER INDUSTRY 13 Chapter XIX HEALTHFULNESS, FOOD VALUE AND BIOLOGICAL PROPERTIES Sanitary purity and healthfulness — Freedom from germs of disease — Di- gestibility—Caloric value— Biological properties— Fat-Soluble A— Food value of diverse foods Pages 558-573 Chapter XX DEFINITIONS AND STANDARDS Butter — Moisture ruling — Fat standard — Butter standards in various coun- tries— Milk — Skimmilk — Cream — Buttermilk — Legal standards by states Pages 573-579 Chapter XXI WHEY BUTTER, RENOVATED BUTTER AND LADLES Whey butter — Manufacture — Wisconsin law — Renovated butter — Defini- tion— History — Output in U. S. — Manufacture — Packing — Markets — Definitions and laws — Ladles Pages 579-588 Chapter XXII STANDARDIZATION, TESTS AND CHEMICAL ANALYSES OF MILK, CREAM, SKIMMILK, BUTTERMILK AND BUTTER Standardization of milk and cream for butter fat — Eight examples- -Test- ing milk and cream for acid — Factory tests — Determination of specific gravity in milk, cream, skim milk and buttermilk — Weight per gallon of cream of varying richness — Determination of total solids in milk, cream, skim milk and buttermilk — Total solids tables — Testing milk and cream for butterfat — The Babcock test — The Gerber test — Stand- ard glassware, scales and weights — Testing skim milk, buttermilk and whey — Butter moisture tests — Butter salt tests — Butter fat tests — Determination of curd, lactose, acid and ash in butter — The Mojonnier test — Detection of renovated butter and oleomargarine — Bacteriolog- ical analyses of butter, milk and cream — Table of Atomic weights — Table of weights and measures Pages 588-665 ERRATA. — Page 301, Footnote, "coal-tar dies" should read "coal-tar dyes." For other typographical errors that may have escaped the proof- reader, the reader's kind indulgence is respectfully solicited. THE BUTTER INDUSTRY CHAPTER I. HISTORY AND DEVELOPMENT OF BUTTER -INDUSTRY. Early History. — The art of buttermaking dates back to times immemorial and reference to the use of butter as an article of food and for medical and cosmetic purposes may be found chronicled long before the Christian Era. Benno Martiny,1 in his treatise "Die Milch" and later in his interesting volume concerning the history of the churn, entitled, "Kirne und Girbe," offers a multitude of quotations on buttermaking by the An- cients as far back as 2000 B. C. He makes reference to the Indians of Asia, the Hebrews, the Arabs, the Egyptians, the Greeks, the Romans, the Teutons, etc., as well as to the his- tory of later centuries. While the word butter appears in the Scriptures on many occasions and as far back as the book of Genesis 18:8 "And he (Abraham) took butter, and milk and the calf which he had dressed and set it before them" etc., one of the first refer- ences to the making of butter is perhaps that by Solomon in Proverbs 30:33, "Surely the churning of milk bringeth forth butter." In the history of Ancient Greece we find that the Greeks knew how to make butter from milk. Herodot and Hippocrates state that the Thracians made butter from cows' milk. Among the Romans who made great strides in agricul- tural development, cheese appears more popular than butter; however, Plinius refers in several instances to butyrum (butter) as an addition to bread. The oldest equipment for buttermaking was constructed of earthenware. Originally the milk was placed in earthen ves- sels and beaten with the hands until the butter granules formed. Later a wooden stirring stick terminating at its lower end in 1 Benno Martiny, Die Milch, ihr Wesen und ihre Verwertungr. Vo. I, 1871. 16 HISTORY AND DEVELOPMENT a butt was used. This arrangement was subsequently changed to a stick carrying a querl consisting of several radial spokes. These were the prototypes of our dash churns in which the dasher terminates in a cross or in a perforated round board or perforated tin cone, fitting closely into the vertical churn. It is evident, therefore, that the two systems of butter-making by stirring or swinging the milk and by beating or dashing it with a dasher, are of very ancient origin. Concerning the early history of the uses of butter Hay- ward1 reports the following: "In early times butter was employed in many ways. The Hindoos used it for the greatest and holiest sacrifices in their worship. The Greeks and Romans did not use butter as a food, but as the standard remedy for injuries to the skin. The soot of burned butter was regarded as a specific remedy for sore eyes. The Romans also used it as an ointment to enrich the skin and as a dressing for the hair. In the time of Alexan- der I. certain of the Macedonians annointed themselves with milk oil; and Galen records that in many cold regions people used butter in the bath. Historians speak of butter used as a remedy for wounded elephants, .and within a century butter was used in large quantities in Scotland and North England for smearing sheep, also as oil for lamps. Besides being applied externally, it was used internally for various troubles. In Spain, as late as the seventeenth century, butter was to be found in the medicine shops fcr external use only. In the middle of the previous century "A medicinal and economic treatment of butter" sets forth in derail the value and use of butter as a remedy. In rural districts in Germany at the present time fresh, unsalted butter is much used as a cooling salve for burns. "Aside from its use ;is a food, a cosmetic, and a medicine, the use or possession of butter was long regarded as indicating wealth, and so served to distinguish the rich from the common people. Evidences of this still exist. In both Chilas and Darel a practice exists of storing- up butter in the ground. Butter so stored is left a number of years, and, to insure its not being 1 Hayward, Facts Concerning the History, Etc. of Butter, U. S. Dept. Agr., B. A. I. Circular No. 56, 1904. HISTORY AND DEVELOPMENT 17 disturbed, a tree may be planted over it. Under these condi- tions it turns deep red and is highly prized. The owner's wealth is computed by the quantity of butter he has stored up in this manner. "Butter was enjoyed as a food by comparatively few people in. its early history; thofo 5^ Skim Mi %Fat 03 3 i & u Z& *~ 1* fe 1 51 4.1 30. .02 51 4.1 31. .04 48 4.1 50.5 .11 2 48 4.4 25. .02 46 4.4 26. .05 45 4.4 28. .10 3 51 3.4 34. .02 51 3.4 34. .05 46 3.4 38. .09 4 50 3.4 24. .01 50 3.4 25. .04 50 3.4 38. .12 5 50 4.2 27. .03 50 4.2 30. .05 50 4.2 40. .20 6 50 4.4 23.5 .04 50 4.4 24. .07 50 4.4 25. .12 7 50 4.0 30. .02 50 4.0 31. .05 48 4.0 34. .09 8 50 4.2 25. .02 51 4.2 27. .06 48 4.2 40. .14 Average . .022 1 1 -051 |.12 SKIMMING EFFICIENCY OF THE SEPARATOR 97 The relative effect of different temperatures of the milk at the time of separation on the per cent of fat left in the skim milk from various makes of hand separators is shown in table 8. Similar results were obtained by Eckles and Wayman1 and by Guthrie.2 At a temperature below 70 degrees F. most separators began to clog, due to the excessive viscosity and the tendency of the milk and cream to churn. Control of Temperature of milk. — On the farm the simplest way to have the milk at the right temperature for separation, is to separate immediately after each milking. This practice does away with the bother of artificially heating of the milk before separating, for which the average farm is not properly equipped and which would be necessary, especially in winter, if the milk were held over for separation from the previous milking or previous day. In the factory, however, where the milk arrives already cooled, special provision is required to heat the milk to the proper temperature (95 to 100 degrees F.) before it passes into the separator. This is most easily accomplished by the use of a continuous milk heater similar to a flash pasteurizer. In some creameries which receive whole milk, the milk is heated to pasteurizing temperature preparatory to separation. This has the advantage of pasteurizing not only the cream but also the skim milk. From the stand point of skimming efficiency, however, nothing is gained by this practice. The fat lost in the skim milk by separating the milk at temperatures of 145 to 185 degrees F. is practically equal to that lost when sepa- rating at 95 to 100 degrees F. Experience has further shown that the separator is more prone to clog with milk at pasteuriz- ing temperature and has to be taken apart oftener for cleans- ing. This hot milk deposits more separator slime. Additional disadvantages of pasteurizing the milk before separation, in- stead of pasteurizing the cream are, the greater cost of the pasteurizing equipment and the greater expense of heating. 1 Eckles & Wayman. — Factors Affecting the Per Cent of Fat in Cream from Farm Separators. Missouri Bulletin No. 94, 1911. 2 Guthrie.— Variations in the Tests for Fat in Cream and in Skimmed Milk. Cornell Bulletin No. 360, 1915. 98 SKIMMING EFFICIENCY OF THE SEPARATOR The skim milk can be pasteurized more economically sepa- rately by the use of exhaust steam. In order to accomplish ex- haustive skimming of cold milk heated to the desired temper- ature for separation, the milk must be held at that temperature for a reasonable length of time so as to give the fat globules a chance to warm and expand and thereby to regain their buoyancy. In some factories the milk is heated without the use of a special heater, but by turning steam direct into the milk. Experience has shown this to be a very undesirable practice. At best, much of the steam used condenses in the milk, dilut- ing the milk and the skim milk. Then, again, the steam is often associated with impurities, such as cylinder oil from the engine, boiler compounds used in the boiler, scales from the inside of the steam pipes, etc. The turning of steam direct into the milk has also been found to be injurious to the quality of the finished product causing both the cream and the butter to take on an oily flavor. Effect of Position of Cream or Skim Milk Screw on the Skimming Efficiency of the Separator. — As already explained, the purpose of the cream screw, or skim milk screw, is to reg- ulate the ratio of cream to skim milk and to control the rich- ness of the cream. Most makes of separators permit of a rather wide range of fat content in cream, without sacrificing their skimming efficiency. Some machines, however, when they are so adjusted as to produce cream testing below 18 per cent fat or above 50 per cent fat, skim less completely. In the case of some machines, especially those with relatively narrow bowls, there is a tendency for the bowl to clog, when attempts are made to produce cream testing 50 per cent fat or more. Generally speaking, it is safe to state that the machines now on the market have reached such a degree of perfection that they can be depended on to do close skimming when set to produce cream containing not less than 18 per cent fat, nor more than 50 per cent fat. This range of richness is sufficient to embrace cream of any richness commercially advantageous. Effect of Smoothness of Running on the Skimming Effi- ciency of the Separator. — The separator cannot be expected to do efficient work unless it runs smoothly. When the bowl re- volves smoothly and without jarring, the skim milk and cream SKIMMING EFFICIENCY OF THE SEPARATOR 99 separated by the centrifugal force thus generated, escape from the machine separately. If the machine trembles and jars, a portion of the cream and skim milk may again become mixed by the vibration of the bowl, causing a relatively large amount of fat to escape with the skim milk and thus reducing the skimming efficiency of the separator. This fact is shown in the following 'table which summarizes the results of experi- ments conducted by Hunziker, with smoothly running and trembling machines. Table 9. — Relative Skimming Efficiency of a Balanced and Unbalanced Separator. Balanced Unbalanced Cream Per cent Fat Skim Milk Per cent Fat Cream Per cent Fat Skim Milk Per cent Fat 42. .03 25. .15 28. .025 30. .17 28. .02 31. .18 28. .035 28. .16 28. .03 28. .155 32. .03 30. .19 Average .03 .17 The trembling of the bowl may be due to any one or more of the following conditions : Shaky foundation, machine not setting level, spindle sprung, internal Contrivances of bowl damaged or not properly placed or incomplete, worn-out bear- ings, loose bushings, excessive speed. The separator should rest on a solid foundation. For farm separators a solid plank floor is adequate, for factory machines a concrete, brick or stone base is preferable. The foundation must be level, though the newer machines with self-balancing bowls minimize the undesirable effect of machines not setting quite level. The separator, while it should be fastened securely to its foundation, should not be screwed down too rigidly for smooth running. A certain amount of "give", or "resonance" is necessary in order to insure smooth running. For this pur- pose it is advisable to place rubber cushions between the sep- 100 SKIMMING EFFICIENCY OF THE SEPARATOR arator base and its foundation. The spindle must be true, the bearings and bushings intact and the internal contrivances of the bowl must be undamaged and in their respective places. The bearings must be fed with oil continuously, must be pro- tected against dust and other material increasing friction, and the bowl and internal contrivances must be handled with care, to prevent damage which would cause to throw the machine out of balance. Effect of Cleanliness of Separator on Skimming Efficiency. — Milk, even in its best condition, contains a certain amount of impurities such as dirt, dust and other foreign matter gain- ing access to it during its production. This, together with par- ticles of viscous nitrogenous matter naturally present in milk, Table 10.— Showing the Effect of Clean and Unclean Separa- tors on the Per Cent of Fat in the Skim Milk. Machines Cleaned After Each Separation Per cent Fat in Skim Milk Machines Cleaned Once per Day Per cent Fat in S'kim Milk .03 .02 .03 .03 .03 .03 .02 .02 .04 .02 .03 .02 .02 .31 .03 .15 .11 .72 .03. .06 .06 .03 .04 .02 .02 .04 .05 .03 .02 .03 .05 .26 .02 .23 .02 .12 .02 .03 .02 .02 .05 .02 .02 .02 .03 .07 Average .... 034 .10 SKIMMING EFFICIENCY OF THE: SEPARATOR 101 collects in the separator bowl, forming the so-called separator slime. It is deposited largely on the walls of the bowl and between the internal contrivances. This slime also impedes the free passage of the milk and cream within the bowl, thereby reducing the diameter, centrifugal force and capacity of the bowl, lowering its skimming efficiency and causing excessive loss of fat. This loss is greatest with milk in poor physical condition. The results of experiments1 with clean and unclean separators are shown in Table 10. Guthrie2 found that, within reasonable limits, deposits of separator slime in the bowl do not materially interfere with the skimming efficiency of the machine. He concludes that only when the bowl fills up with separator slime to the extent of clogging the passages, does the efficiency of separation suffer. In his tests, Guthrie used from 240 to 320 pounds of milk only per test. He does not state the rated capacity of the sepa- rator. It is probable, therefore, that in these experiments the amount of milk used was too small and the amount of sepa- rator slime centrifuged out too limited to materially affect the diameter of the bowl and the centrifugal force. In commercial separation of the milk, where the separator often is in continuous operation for several hours, the accumu- lation of separator slime is frequently very great and this in turn is bound to seriously diminish the skimming efficiency of the machine. Effect of Condition of Milk on Skimming Efficiency of the Separator. — Milk in poor mechanical and physical condition, such as milk containing a relatively large amount of impurities, or milk, which is old and partly sour or curdy, tends to lower the skimming efficiency, largely because it augments the am- ount of separator slime which collects in the bowl; this in turn impedes the free passage of milk and cream and causes exces- sive loss of fat. If the milk is curdy the danger of incomplete separation is augmented by the fact that each particle of curd locks up a small amount of fat, and the curd passing into the skim milk 1 Hunziker.— The Hand Separator and the Gravity Systems of Creaming. Purdue Bulletin No. 116, 1906. 2 Guthrie.— Variations in the Tests for Fat in Cream and Skimmed Milk. Cornell Bulletin No. 360, 1915. 102 CONDITIONS AFFECTING RICHNESS OF CREAM - on account of its greater specific gravity, carries this fat with it. If it is necessary to run curdy milk through the separator, the milk should be poured from one can to another, or stirred, sufficiently to break up the curd as finely as possible. Milk in poor condition is very prone to cause the bowl to clog. If such milk must be separated it is advisable to slightly underfeed the separator. CONDITIONS AFFECTING THE RICHNESS OF CREAM. It is desirable and important, for more reasons than one, that means and methods be used whereby the per cent of fat in cream can be properly controlled. The creamery, in order to utilize its cream satisfactorily and economically, for sale or for manufacture, requires cream of suitable richness for each specific commercial purpose. For buttermaking, cream testing 30 to 35 per cent fat is most desirable. Such cream makes pos- sible easy handling, it minimizes injury to the fat during pas- teurization, and permits of the use of a liberal amount of starter without excessive dilution. Excessively low testing cream sours and spoils more readily than richer cream, so that by the time it reaches the creamery, thin cream is often in a con- dition unfit to be made into good butter. In this sour and curdy condition accurate sampling and testing is rendered diffi- cult, if it is at all possible. Thin cream is undesirable further, because it diminishes the amount of skim milk available for the feeding of calves and pigs on the farm ; it increases the cost of transportation of every pound of butter fat so shipped or hauled ; it makes impractical the use of a reasonable amount of starter in the creamery, and starter is essential for the de- velopment of a pleasing high flavor of butter ; it does not churn out exhaustively and yields an excessive amount of but- termilk, augmenting the loss of fat and thereby reducing the churn yield. Excessively rich cream, such as cream testing above 45 per cent fat is also undesirable from the farmer's and the cream- ery's standpoint. Such cream tends to clog the separator; it CONDITIONS AFFECTING RICHNESS OF CREAM . 103 renders the emptying of the cans exceedingly difficult, espe- cially during cold weather ; it makes difficult accurate sampling and thereby tends to yield incorrect tests; and it contains too small an amount of milk solids to properly protect the fat globules against mutilation and injury during pasteurization and churning. It is desirable to produce somewhat richer cream in summer than in winter to prevent excessive fermentation in summer and difficult handling in winter. When a more exact per cent of fat is desired, as is the case of cream sold as sweet cream direct to the consumer, or used in the manufacture of ice cream, the definite richness is usually most conveniently secured by standardization of the cream after separation. The knowledge and control of conditions which regulate the richness of the cream produced on the farm, is of unques- tionable importance. The cream test reported by the creamery to its patrons is one of the guiding factors which sways the cream producer for or against the reporting creamery. There is no one factor, except possibly open dishonesty, that is so potent of disorganizing and demoralizing the cream supply territory of a creamery, as a repetition of changes in the re- ported cream tests of successive deliveries of cream from the same patron. This fact is largely due to the usual ignorance on the part of the average cream patron of the numerous con- ditions under his own control and not under the control of the creamery, which may cause the richness of the cream and, therefore, the test to vary and yet, when the tests do vary the producer is tempted to accuse the creamery of reporting incor- rect tests and being unfair in its dealings. In some cases these accusations are justified, but in the great majority of instances the variations in the tests are due to variations in the richness of the cream caused by irregular- ities incident to the operation of the farm separator. The fol- lowing are the chief factors controlling the richness of the cream : 1. Position of cream screw or skim milk screw 2. Richness of milk 104 CONDITIONS AFFECTING RICHNESS OF CREAM 3. Speed of separator 4. Rate of inflow 5. Temperature of milk 6. Amount of water or skim milk used to flush the bowl 7. Cleanliness of separator bowl. Effect of Cream Screw or Skim Milk Screw on Richness of Cream. — The relation of the position of the cream screw and skim milk screw to the proportion of cream to skim milk and to the richness of the cream has been previously discussed. Fundamentally, any change in the separator which will alter the relative amounts of skim milk and cream will influence the per cent of fat in the cream. These (Jevices, the skim milk screw and the cream screw are very sensitive adjustments. Only a slight turn (J turn) of the screw is sufficient to bring about a very appreciable change in the per cent of fat of the cream. Effect of Richness of Milk on Richness of Cream. — The richness of the milk separated, directly influences the richness of the cream,; in fact the per cent of fat in the cream stands in direct proportion to the per cent of fat in the milk separated. With the cream screw set to deliver a certain definite rich- ness of cream and all other conditions normal, the separator will deliver a definite ratio of skim milk to cream. This ratio varies with the adjustment of the cream screw or skim milk screw. For illustration, it is assumed that this ratio of skim milk to cream be 85 to 15, that is, that of each 100 pounds of milk separated, the separator discharges 85 pounds of skim milk and 15 pounds of cream. If all conditions are the same this ratio of skim milk to cream remains constant. Changes in the richness of the milk cannot alter it, no matter how rich or how poor the milk, each 100 pounds of milk will yield 85 pounds of skim milk and 15 pounds of cream. But since prac- tically all of the fat goes into the cream, the cream from the separation of rich milk contains more fat than that from poor milk. This fact is graphically illustrated in Fig. 12. CONDITIONS AmcTiNG RICHNESS OF CREAM 105 3*/M/( CWrA/m .3 LB& OF FAT /OOifa OF6X/1JIIC OWTZm 6LK.QFF7ST Tig. 12 Table 11. -^Showing Effect of Richness of Milk on Richness of Cream.1 Experi- ment No. Milk Time of Separa- tion Min. Cream Skim Milk Lbs. Fat % Fat Lbs. | Fat Lbs. % Fat Lbs. Lbs. Fat % Fat Lbs. Milk Testing 3% Fat I. . 50 3 1 5 7 625 19 1 18 45 12 054 II III. ... 50 50 3 3 1.5 1.5 7 7 6.5 6.5 20.5 20.5 1.33 1.33 46 46 .03 .04 .013 .018 Aver. . 50 3 1.5 7 6.42 20 1.28 46 .06 .028 Milk Testing 4.5% Fat I 50 4.5 2.25 7 6.25 34 2.12 45.5 .02 .01 II 50 4.5 2.25 7 6.5 32 2.08 44.8 .1 .05 III. ... 50 4.5 2.25 7 6.25 31.5 1.96 44.7 .05 .02 Aver. . 50 4.5 2.25 7 6.3 32.5 2.05 45 .06 | .03 Milk Testing 6% Fat I 50 6 3 7 6.5 40.7 2.65 44 .12 .052 II 50 6 3 7 6.5 40 2.6 44 .10 .044 III. ... 50 6 3 7 6.5 36 2.34 44 .2 .088 Aver. . 50 6 3 7 6.5 39 | 2.53 44 .14 .061 The above illustration shows that with a ratio of skim milk to cream, of 85 to 15 and all other conditions remaining con- 1 Hunziker.— -Why Cream Tests Vary. Purdue Bulletin No. 150, 1911 and 1915. 106 CONDITIONS AFFECTING RICHNESS OF CREAM slant, three per cent milk produces 20 per cent cream, four and one-half per . cent milk produces 30 per cent cream and six per cent milk produces 40 per cent cream. The correct- ness of this rule is further demonstrated by results of sepa- rator experiments conducted by the Purdue University Agri- cultural Experiment Station, as summarized in table 11. Similar results were also obtained by Eckles and Wayman1 and by Guthrie.2 It is further interesting to note that the difference in the rich- ness of cream from milk of different per cents of fat increases as the ratio of skim milk to cream becomes wider. This rule is shown in the following figures. Table 12. — Relation of Richness of Cream to Ratio of Skim Milk to Cream. Ratio of Skim Milk to Cream Per Cent Fat in Cream from Difference in Per Cent Fat in Cream 3 Per Cent Milk 6 Per Cent Milk 80 to 20 85 to 15 90 to 10 - 15 20 30 30 40 60 15 20 30 The per cent of fat in the milk separated does not appreciably affect the skimming efficiency, the per cent of fat found in the skim milk from rich and poor milk being practically the same. Effect of Speed of Separator on Richness of Cream.— The higher the speed of the separator the higher the per cent of fat in the cream. This rule applies in the case of most separators and under most conditions. The influence of the speed on the richness of the cream is largely due to the direct effect of the speed on the ratio of skim milk to cream. The higher the speed the greater the centrifugal force and the more rapidly will the skim milk leave the bowl. An increase in speed therefore increases the capacity of the skim milk dis- charge. This, means less milk for the cream .outlet and con- sequently richer cream. A decrease in the speed lessens the 1 Eckles and Wayman. — Factors Affecting the Per Cent of Fat in Cream from Farm Separators. Missouri Bulletin 94, 1911. 2 Guthrie. — Variations in the Tests for Fat in Cream and in Skimmed Milk. Cornell Bulletin 360, 1915. CONDITIONS AFFECTING RICHNESS OF 107 centrifugal force, retards the escape of the skim milk, reduces the capacity of the skim milk outlet and more milk has to be discharged through the cream outlet. The cream, therefore, is thinner. In the following table are summarized results of ex- periments1 showing the effect of the speed of the separator on the richness of the cream. Table 13. — Effect of Speed of Separator on Richness of Cream. Experi- ment No. Time of Separation Mift Cream Skim Milk Lbs. Fat % Fat Lbs. Lbs. Fat % Fat Lbs. Low Speed 1 9 9.5 11 1.05 40.3 2.8 1.1 II 9 95 10 95 396 29 1 15 Ill 9 9.7 11 5 1 12 398 25 1 Average 9 96 108 1 04 399 273 1 08 Normal Speed I 55 5.2 41 5 2.17 44.8 04 .02 11 7 47 45 2 12 448 07 .03 III 7 5.1 40 2.04 44.5 .07 .03 Average . 6.5 5 42.2 2.11 44.7 .06 .03 High Speed I 6 33 655 21 46.5 .01 II 65 35 595 208 45.9 .03 .01 Ill 65 3.1 65 202 46.6 .06 .03 Average 633 33 627 207 46.3 .03 .01 These facts apply with all separators and under all con- ditions where the skim milk and cream exits are so adjusted that the skim milk outlet is farther from; the center of the bowl than the cream outlet. This is the case with most separators and under most conditions. Additional factors which may enter into the causes of richer cream, as the result of higher speed, are the reduced relative friction in the skim milk outlet, due to the larger volume of skim milk discharged and the increased relative friction in the cream outlet due to the greater viscosity of the richer cream. Further- more, the more complete separation in the case of high speed may in part at least be conducive of richer cream. 1 Hunziker.— Why Cream Tests Vary. Purdue Bulletin No. 150, 1911. 108 CONDITIONS AFFECTING RICHNESS OF CREAM SPEED L0W SPEED £.o$5 in SKinmtK H/6H3PEED Pl8T- 13 However, the effect of the speed of the separator varies to some extent with the richness of the cream for which the sep- arator is set. When set for rich cream there is a greater difference in the per cent of fat of the resulting cream between high speed and low speed than when set for thin cream. This is due to the fact that when the machine is adjusted to produce rich cream, the relative difference between the distance of the skim milk and cream outlets from the center of the bowl is proportionately greater, the proportion of skim milk discharged is larger, less milk is left to pass out with the cream, the cream is richer and the influence of the speed is greater than when the separator is set for thin cream. When set for thin cream the relative dif- ference between the distance of the skim milk and cream outlets from the center is smaller, the effect of the speed on the capacity of the skim milk and cream discharge is more nearly equalized, causing less variation in the richness of the cream due to changes in speed. In separators, or under conditions, causing the cream outlet to be located farther from the center than the skim milk outlet, a high speed will even yield less skim milk, more cream and thinner cream than a low speed. This is the case with the Simplex separator, for instance, when adjusted to produce thin CONDITIONS AFFECTING RICHNESS OF CRSAM 109 cream, as shown in Table 14, representing results obtained by Eckles and Wayman.1 Table 14. — Effect of Speed. Simplex Separator No. 2 (1540). Full speed 50 revolutions of cran'k per minute. Three-fourths speed 37 revolutions of crank per minute. Half speed 25 revolutions of crank per minute. Temperature uniformly 90°. o""1 b ^g 4* L I* 2 03 |gd 03 *•"* 3 CCQ 5*4 = 1 *i 0 3 £ Speed 5 L. 5^ If s« S*M 3 i! Sg £ I" 1" h Full Speed 3.126 16.684 19.810 1—5.33 31.3 .02 5.0 31.3 .03 17 Three-fourths Speed. 3.200 16.522 19.722 1—5.16 30.2 .06 5.0 30.1 .06 Half Speed 3.128 16.532 19.660 1—5.29 29.0 .31 5.0 28.9 .32 Full Speed 2.448 17.490 19.938 1—7.14 39.6 .03 5.1 39.8 .03 18 Three-fourths Speed. 2.708 16.896 19.604 il-<5.23 35.4 .06 5.1 35.6 .05 Half Speed . ... 3.052 16.576 19.628 1—5.43 30.0 .20 5.1 29.8 .23 Full Speed 4.238 15.645 19.883 1—3.69 21.4 .03 4.9 21.4 .03 19 Three-fourths Speed. 3.863 15.975 19.838 1—4.13 23.2 .07 4.9 23.1 .07 Half Speed 3.206 16.433 19.639 1—5.11 26.8 .25 4.9 26.8 .25 Full Speed 4.365 15.723 20.088 1—3.59 20.6 .03 4.8 20.6 .03 20 Three-fourths Speed. 3.975 15.969 19.944 1—4.03 22.2 .05 4.8 22.2 .06 Half Speed 2.868 16.826 19.694 1—5.85 28.0 .36 4.8 28.2 .36 The above table shows that, while with rich cream the ratio of skim milk to cream and the per cent of fat in the cream de- creased as the speed was reduced, with cream low in fat the 1 Eckles and Wayman. — Factors Affecting the Per Cent of Fat In Cream from Farm Separators. Missouri Bulletin No. 94, 1911. 110 CONDITIONS AFFECTING RICHNESS OF CREAM reverse was the case. As the speed was reduced the ratio of skim milk to cream and the per cent of fat in cream increased. These differences are due to the relative position of the skim milk and cream outlets. Effect of Rate of Inflow on the Richness of the Cream.— The rate of inflow exerts a marked influence on the richness of the cream as shown in the table below. Table 15. — Effect of Rate of Inflow on Richness of Cream. Experi- ment No. Milk Time of Separa- tion Min. Cream Skim Milk Lbs. Fat % Fat Lbs. Lbs. Fat % Fat Lbs. Lbs. Fat % Fat Lbs. Small Inflow I 50 43 215 11 286 70 202 46.7 .05 .02 II . .. 50 44 22 11 3 12 68 212 46.4 .12 .06 III. ... 50 4.8 2.4 12 3.42 71.5 2.44 46.3 .08 .04 Aver. . . 50 4.5 2.25 11JS 3.13 70 2.19 46.5 .08 .04 Normal Inflow 1 50 43 215 7 5 5 | 37.5 206 44.2 1 .04 II 50 4.4 2.2 7 5.37 | 40 2.15 44.1 .05 .02 III. ... 50 3.8 2.4 7 4.37 | 58.5 2.55 45.5 .03 .01 Aver. . . 50 4.5 2.25 7 5.08 | 44.3 2.25 44.6 .06 .02 Large Inflow I 50 43 2 15 6 45 23 5 106 451 25 .11 II 50 4.4 2.2 Q 775 26.5 205 42.1 77 .11 Ill 50 4.8 2.4 6 4.86 51.7 2.51 44.7 .05 .02 Aver. . . 50 4.5 2.25 6 5.70 32.8 1.87 44 .19 .08 The results in table 15 show that the richness of the cream increases as the rate of inflow decreases and vice versa. This is due to the fact that when the rate of 'inflow increases the capacity of the cream outlet increases proportionately greater than the capacity of the skim milk outlet, while a decrease in the inflow causes a greater decrease in the capacity of the cream outlet than in that of the skim milk outlet. The average re- sults of experiments with a small, normal and large inflow as tabulated above show the following proportion of cream to skim milk, Table 16. CONDITIONS AFFECTING RICHNESS OF CREAM 111 IHfLOW. 30OIBS SMALL 1/1FLOW *,**.&* Pig-. 14 Table 16.— Effect of Rate of Inflow on Ratio of Skim Milk to Cream. Rate of Inflow Cream Skim Milk Ratio of Cream to Skim Milk Lbs. % Lbs. % 50 Ibs. in 11 Minutes 3.13 6.26 46.5 | 93 1 : 14.86 50 Ibs. in 7 Minutes. 5.08 10.16 44.6 89.2 1: 8.78 50 Ibs. in 6 Minutes. 5.70 11.40 44.0 88.0 1; 7.72 It was formerly assumed that the skim miilk discharge was constant and was not influenced by the rate of inflow and that all the additional milk of an increased inflow would escape through the cream discharge. The above experimental results show this to be erroneous. The skim milk discharge increased very materially with the increase in the rate of inflow as shown in Table 16 and in the following summary:1 1 Hunziker.— Why Cream Tests Vary. Purdue Agr. Expt. Station. Bull, No. 150, 1911. 112 CONDITIONS AFFECTING RICHNESS OF CREAM Skim milk discharged per minute Ollldll IIJIIUW Normal inflow 11 44.6 t.£o puunus 6 37 pounds L/arge inflow . . . 7 44.0 7 33 pounds 6 Effect of Temperature of Milk on Richness of Cream. — The temperature of the milk influences the richness of the cream yielded by the separator to a marked degree. Table 17.— -Showing Effect of Temperature of Milk on Richness of Cream.1 Experi- ment No. Time of Separa- tion Min. Milk Cream Skim Milk Lbs. Fat % Fat Lbs. Lbs. Fat % Fat Lbs. Lbs. Fat % Fat Lbs. Normal Temperature— 90 to 95° F. I 7 50 3.8 1.9 9 17.5 1.58 41 .03 .01 11 . . 5 31.5 41 1 29 4.5 28 1 26 27 .03 .01 Ill 8 50 4 2 9.7 20.5 2 40.9 .02 .01 IV 8.5 50 4 2 10.1 20 2.02 39.8 .01 V 7.5 50 4 2 10.1 20 2.02 40.3 .01 Aver. . . 7.2 46.3 3.98 1.84 8.68 21.2 1.78 37.8 .02 .01 Low Temperature — 50 to 60° F. I . .. 9 50 38 1 9 2 325 65 48 1.50 .72 II . 7 32 41 1.31 1.5 43 .65 28.5 2.10 .63 III. .... 7.5 50 4 2 7.2 27 1.94 43.6 .05 .02 IV 7.5 50 4 2 7.3 28 2.04 44.3 .03 .01 V. ..... 7.5 50 4 2 7.2 28 2.02 44.1 .05 .02 Aver. . . 7.6 46.4 3.98 1.84 5.04 31.7 1.46 41.7 .75 .28 The experimental results summarized in the above table show that cold milk yields richer cream than warm milk. The cream from the cold milk averaged 31.7 per cent fat, while the cream from milk separated at 90 to 95 degrees F. averaged 21.2 per cent fat. The difference would probably have been con- siderably greater, had it not been for the excessive loss of fat in the skim milk from the cold milk, which reduced the amount of fat supplying the cream discharge. The cream from the cold milk is thicker and more viscous than that from the warm milk. This greater viscosity renders HHunziker, Why Cream Tests Vary, Purdue Bulletin 150, 1911. CONDITIONS AFFECTING RICHNESS OF CREAM 113 it more sluggish in its escape from the bowl, it passes off more slowly, thereby decreasing the capacity of the cream outlet, and more of the milk is forced through the skim milk outlet. EFFtlCTSFTlEMIPSl OTM/LKS0T /00/t effFA/i COMTA/flS JL0JS M SMflfllLK .3 - 33.?* Pig1. 15 The fact that the cold milk has a higher specific gravity than the warm milk may cause the skim milk to escape with slightly more force, thus further increasing the capacity of the skim milk outlet. It is not improbable, also, that the warm milk is sufficiently more fluid than the cold milk to increase the rate of inflow and thereby increase the relative volume of the cream discharge in greater proportion than the skim milk discharge. The results above recorded, however, fail to show a uniform in- crease in the rate of inflow of the warm milk; in fact in two out of five experiments the opposite was the case. In the case of some separators the bowl commences to clog when cold milk is passed through the machine. When this happens the cream from the cold milk is usually thinner than that from the warm milk. A part of the butterfat in the bowl, churns into a roll of butter and only a small amount of cream is discharged and this cream is very low in butterfat. This phe- nomenon is shown in table 18. 114 CONDITIONS AFFECTING RICHNESS OF CREAM Table 18. — Effect of Low Temperature of Milk on Richness of Cream when Bowl Clogs.1 Temper- ature Time of Milk Cream Skim Milk Separa tion Min. Lbs. Fat % Fat Lbs. Lbs. Fat % Fat Lbs. Lbs. Fat % Fat Lbs. 95° R... 50° F.... .4 7 32 30 4.1 4.1 1.31 1.23 4.5 1.5 26 12 1.17 .18 26 25 .03 3.6 .01 .90 As already stated in chapter on "Effect of Temperature of Milk on the Skimming Efficiency of the Separator," as far as the farm separator is concerned, the milk is in the best condition for separation in every respect, immediately after each milking. In the factory, facilities for heating the milk to and holding it at 90 degrees F. or over should be provided. Effect of Amount of Water or Skim Milk used to Flush the Bowl on Richness of Cream. — While this is strictly a minor fac- tor in the control of the richness of the cream, it should be understood that the indiscriminate flushing of the bowl may dilute the cream unnecessarily. It is very desirable that the bowl be properly flushed after each separation. This removes most of the remnants of milk and cream, and loosens the separator slime in the bowl, making subsequent washing more easy. In order to accomplish this, all that is necessary is to run water into the bowl until the dis- charge spout appears watery. Table 19.— Effect of Amount of Water Used to Flush the Bowl on the Richness of the Cream.1 Amount Water Used to Flush Bowl Twice the Experi- Same as Till Cream Arnt. Needed ment None Capacity Discharge for Watery No. of Bowl was Watery Cream Dis- charge Fat % Fat % Fat % Fat % I 32 32 31 29 II 30 30 29 28 III. 58 56 51 48 IV 31 31 30 29 Average. . . 37.8 37.3 35 33.5 1 Hunziker, Why Cream Tests Vary, Purdue Bulletin 150, 1911. ADVANTAGES OF CENTRIFUGAL SEPARATOR 115 Effect of Slime in Bowl of Separator on Richness of Cream. — Experiments conducted by Guthrie and Supplee1 show that deposits of slime in the bowl do not have any appreciable effect on the richness of the cream so long as the slime does not clog the passages. Advantages of Centrifugal Separator over Gravity Creaming. The operation of the centrifugal separator has undisputed advantages over the gravity systems of creaming. The chief of these are: 1. Greater skimming efficiency. 2. Richer cream. 3. Better quality of cream and skim milk 4. More uniform richness of cream Greater Skimming Efficiency. — The centrifugal separator is the most efficient apparatus available for the separation of milk. Below table shows the relative skimming efficiency as secured experimentally.2 Table 20. — Per cent of Fat in Cream and Skim Milk of the Four Different Systems of Creaming under Most Favorable Conditions. Hand Separator Deep-Setting Shallow Pan Water-Dilution S'kim | Skim Skim Skim Milk Cream Milk Milk Cream Milk Milk Cream Milk Milk Cream Milk Lbs. % % Lbs. % % Lbs. % % Lbs. % % Fat Fat Fat Fat Fat Fat Fat Fat 31 33. .01 20 32. .2 50 30. .55 64 22. .70 31 29. .03 30 29. .15 50 26. .40 64 21.5 .68 40 34. .01 27 27. .16 52 31. .38 60 25. .70 34 30. .02 30 30. .18 48 32. .42 60 26. .60 35 32. .02 28 32. .18 50 26. .46 56 25.5 .74 34 33. .03 26 26. .15 50 27. .44 56 24. .68 46 33. .01 28 24.5 .17 52 25. .48 60 31. .72 38 30. .02 25 28. .15 50 32. .02 30 25.5 .18 38 30. .02 30 28. .18 38 28. .02 38 33. .02 Average .02 .17 .44 .68 A glance at the above table reveals the superiority of the and Supplee, Variations in the Tests for Fat in Cream and Skim Milk, Cornell Bulletin 360, 1915. 2 Hunziker, The Hand Separator and the Gravity Systems of Creaming, Pur- due Bulletin 116, 1906. 116 ADVANTAGES OF CENTRIFUGAL SEPARATOR centrifugal separator over the gravity systems of creaming Even in the deep-setting system,, which causes the least loss of fat in the skim milk of any of the gravity systems, the loss of fat is 8.5 times as great as that incurred with the centrifugal separa- tor; the shallow pan and water dilution system lost 22 and 34 times, respectively, as much fat in the skim milk as the cen- trifugal separator. The loss of butter fat with the gravity system of creaming would probably have been even greater, had an attempt been made to secure a richer cream. For buttermaking, cream con- taining from 30 to 35 per cent fat is most suitable. It is difficult, even under the best conditions, with the gravity systems, to produce cream testing 30 per cent fat, it is practically impos- sible to do so without a material increase in the per cent of fat lost in the skim milk. Expressed in pounds of butter lost in the skim milk of one cow in one year, the loss assumes an importance which no pro- gressive dairyman can afford to ignore. It is obvious that even at very moderate butter prices, the centrifugal separator in the skimming of the milk of a herd of 5 to 10 cows would save enough butterfat in less than two years to pay for itself, as shown in table 21. These figures are based on the assumption that each 100 pounds of milk yields 87 pounds of skim milk, that a 20 per cent overrun is secured and that butter sells at 50 cents per pound. Table 21. — Loss Incurred by the Four Systems of Creaming at 50 Cents per Pound of Butter in One Year. Cows Milk Value of Butter Lost by the Use of Different Methods of Creaming No. Pounds Hand Separator $ Deep Setting Method $ Shallow Pan Method $ Water Dilution Method $ 1 5 10 5,000 25,000 50,000 .52 2.60 5.20 4.44 22.19 44.37 11.48 57.40 114.80 17.75 88.74 177.48 Better Quality and Richer Cream. — The centrifugal separa- tor makes it possible for the creamery and for the dairy farmer ADVANTAGES OF CENTRIFUGAL SEPARATOR 117 to secure a pure, sweet and wholesome cream which can be made into a first class butter. In the whole milk creamery, where the btittermaker has exclusive control over the cream as soon as it leaves the separator, conditions are most ideal and the verdict of the butter markets of this country is proof of the fact that our best butter comes from the whole-milk creameries. The cream that arrives at our gathered cream plants, as a general rule does not grade high enough to make "Extras." This fact is one of the main drawbacks of the gathered cream plant. While much of this cream is hand separator cream, the fault cannot be attributed to the separator. It is obvious that just as good cream can be produced by the use of the hand separator as with the factory machine. The fault lies not with the use, but with the abuse of the separator. When proper at- tention is given to cleanliness in the operation of the separator and the handling of the cream, to prompt cooling and to frequent delivery, the resulting cream is bound to be in proper condition to make good butter. Not so, however, where the cream is separated by gravity. The gravity cream, is to-day considered the scum of the raw material which the creameries receive. Creameries which practice systematic grading are generally forced to place gravity cream in their lowest grade and many creameries pay several cents less for such cream than for separator cream. There are many reasons for the inferiority of gravity cream : It is usually old because time is required for setting. It is always relatively low in butter fat and this, together with its age, causes it under average conditions to be of very poor quality by the time it reaches the creamery. Its dilution deprives the buttermaker of the opportunity to improve it by the addition of starter. This thin cream yields a relatively large amount of buttermilk which in turn means heavy loss of fat. This loss is increased also by the fact that this thin cream, especially when pasteurized, does not churn out exhaustively and finally the cream, owing to its thinness and its usual contamination with undesirable ferments, deteriorates rapidly, yielding a low grade of butter. 118 RECEIVING MILK AND CREAM CHAPTER VI. RECEIVING MILK AND CREAM. When the milk or cream is received by the creamery, or cream station and before it enters the manufacturing process, it is graded, weighed, sampled and "dumped" and the cans are washed, rinsed, steamed and dried and retagged preparatory to returning. Grading of Cream, Importance. — iFrom the standpoint of improving the quality of cream received by the creamery the use of an efficient system of cream grading is all important. Until recent years the cream grading has received very little attention by our creameries. Little, if any grading was done and the same price was paid for good and poor cream. This has resulted in a general depreciation of the quality of the cream furnished by the farmer, there was no material inducement to the farmer to make a special effort in the care of the cream on the farm. Unless his personal pride and decency prompted him to produce a clean, sanitary and properly cooled cream, he was all too ready to follow the line of the least resistance and pay no attention to the quality of the cream he furnished. In fact, the failure of the creamery to grade cream put a premium on shiftless and careless handling of cream on the farm and on the receipt of poor cream in the factory. In consequence of this disregard for quality of raw material, much of the butter annually reaching the market was of un- satisfactory quality, the keeping property of much of this but- ter was inferior, causing it to come out of storage in deteriorated condition, large quantities of butter had to be sold under market quotations, inviting keen competition by foreign butter and but- ter substitutes and rendering the establishment of a reputation for American butter in foreign countries exceedingly slow and difficult. Development of Cream Grading. — Within the last five to ten years, the pure food wave that has swept the country awaken- ing the public to a keener appreciation of the value of whole- some food products of good quality, the realization on the RECEIVING MILK AND CREAM 119 part of the creamerymen of the necessity of supplying the market with bettter butter in order to dispose of it at a satisfactory mar- gin, and the efforts of the dairy educational forces to introduce practical methods for the systematic grading of cream, have been mighty factors in focusing the attention of the creamerymen on improving their cream supply by cream grading and quality- paying. The earlier efforts at cream grading were largely abortive. In isolated cases some concerns had the courage and determina- tion to grade and pay on the basis of grade only. But the great majority of creameries, while acknowledging the fundamental correctness of cream grading, lacked the courage to undertake it. Their intentions foundered on the rock of competition in the cream supply territory. They lacked confidence in each other to stand by mutual agreements to start grading and quality-pay- ing. They were fearful of losing patrons and of working into the hands of their competitors. Gentlemen's agreements, drafted in sectional and national conferences of creamerymen to grade cream- proved futile. Attempts to place legislative measures on the statute books, requiring the grading of cream proved uncon- stitutional, and Government inspection of the creameries for the purpose of compelling nation-wide cream grading did not ma- terialize because of the enormity of the proposed undertaking. While most of these proposed and apparently ideal plans failed to materialize and were automatically abandoned, one after another, the constant agitation of the subject did not fail to have its good effect. While it became clear to all practical creamerymen that the industry was not ripe as yet for an organized state- or nation-wide plan of cream grading by mutual agreement between creameries, farsighted creamerymen realized that this complex and difficult matter was a problem to be solved independently by each individual creamery and that it was to the unquestioned advantage of each individual concern to in- troduce cream grading in their own plants. Today most of the really progressive creameries, large and small, are grading their cream and many of these creameries pay the farmer on the basis of quality. Those who have taken this 120 RECEIVING MIIgggggogggg iQ iO O "5 iO O iO iO O iO O O iO O O iO O O iO O O iO O O iO O O iO O iO iO O O iO O iO iO O iO iO O iO iO O to iO O iO iO O ' Vja'aa'&a's&aa'^ lOiO OiOOO » rHC^CNCO^T^iOiOCON-^OOOOOSOOrH iN?5cN" 00 00 OS* OS O O r-I r-I (N CO* CO* TH Tl* io' IO CO* t^ t^ 00 00 OS OS O O rH (N IN CO CO •* •*' io' IO co' t^ t» 00 i-HrHrHrHrHrHrHrHrHrHrHrHrHrHrHrHrHrHCO CO CO t> t 00 00 O5 OS O O i- r IN (N CO CO rj rj U5 iO co co t> t 00 00 00 OS OS O O ^ <-l O O i- r IN (N CO CO rj rj U5 iO co co t> t 00 00 00 OS OS O O rHrHrHrHrHrHrHrHrHl_|l_|l_|l_|r-li-H^li-li-Hr-l>-lr-l(N(N( MN OO'rHC t t oo 0 o o o o o r- r- o o « co w rj Tf 10 10 co co co i> t oo oo o o » o o --i <-< " rH r-J .H (N (N CO CO CO -^' •* Tf >O if) CO CD' CO t-' t^ 00 00 00 O5 O> O O O -I i-<° (N (N* -' N.' 00 00 00 <3> O5 OS r-l i-l i-l ^-1 .-H ^H ^H rH p-t ,-1 r-( r-l rH rH r-l ^H rH r-l rH rH rH i-H ^-1 r-( f-l rH 'H^ »OiOOO»OOOiOiOO"5>OOO»O'OO>O»OOO'OOO»O'OO«O>OOO1OOO»O>OO'O'OOO»O'OO'OiOOO'OO OOOOi^'^'^C^C^C^C^COCOMTf<^^iO O I ^ t»" t^ 00 00* (»' <» OS OS O5 O O O O r-I r-I rH r-i ej N o' "?' CO* CO co' co' co' l> t> t>I t>.' 00 00* 00 00 oo' OS* OS OS OS O O O O CO r-i ^-5 TH p O «O CD CD CO CO CO CO co b- b» t> t- t> t> oo 00 00 (N (N (N M (N o "0 CO CO CD CO CO CO CO M (N OSO'-iNTjO>-iCOCD^O5O'-iCI 5rH3SSSS5«NNNc»ooo> OO»O»OOO>O»OiOOOOiOiO'OOO»O»O'OOOO»OiO»OOOO»O»OOOO"5iO'OOOO«O"5OOO'OUHOOO OiOtOOOOOOiOiOiOOOOOiOiOiOOOOiOiOiOOOOO' ISSSSSSSfc oo»c»c>o>o< OOOOiO» OOOOOOOOOOOO' OOOOOOOOOOOOOOOOOOO»O»O"5»O« OOOOO»O»OiO»0'OiOiO»O>O»OOOOOOOOOOO< O O 0 10 »0 10 »0 10 iQ O O O OO O *O >O«> « IQ »O O OOO O O O «O «P «O «O «O «> O O O O O O «O i OO»O»C»O»OOOOOO»OiOiO»OOOOOO'OiO»O»OOOOOO"3»O>O' '^C^COTtOU5iOOOO»O»O»O>OOOO»O»O'O'OOOO> O«O"3iCOOO»OiOOOO»OiOiOOOO'O»OOOOi 0^^00^0000^0 1C .0000^000^ O'O'OOOiOiCOO'C'OOOOiOOO'C'O! •o a w )cocoeococococococo'«*f^T»<'»jf<»f«ti-*Tj magnesium oxide has an alkalinity equivalent in strength to approximately 116 to 120% of pure calcium lime. (3) Lime has a marked affinity for casein. The absorption of lime By the casein and the reduction of the casein acid are greater than the absorption of lime by the serum and the reduc- tion of the lactic acid. (4) When neutralization is carried to the neutral point, the distribution of the neutralizing action in the components of cream — the serum, curd and fat — is similar with sodium hydrate as it is with lime water. (5) The acid test of the cream determines the total acidity of the cream, including both the casein acid and the lactic acid, It yields, therefore, the correct per cent of acid. (6) The deficiency of the neutralizing action of the lime is due to physical and mechanical combination between portions of insoluble lime and the curd. The fact that from 16 to 20% of the lime does not react in the cream must be attributed to the, great affinity of the lime for casein, particles of lime adhering and becoming permanently attached to particles of free casein. In this condition the lime so held is unable to exert its full neu- tralizing action. Adding Lime Mix in Proper Manner. — It is not enough to use the right strength and amount of lime. The lime mix must NEUTRALIZATION OF SOUR CREAM 173 be handled in the proper manner, after it is made up and before it is added, otherwise it cannot accomplish that for which it is used. Lime settles to the bottom quickly, hence it must be stirred thoroughly before use. It must be strained and diluted with an equal volume of water before it is poured into the cream and it must be sprinkled over the entire surface of the cream while the cream is in agitation. Sediment of limy curd in the bottom of the forewarmer or vat is a fairly conclusive proof that the lime mix was not added as it should have been. In order to secure maximum reaction between the alkalinity of the lime and the acid in the cream, the neutralizer must be distributed thinly and uniformly throughout the entire batch of cream. This is possible only when the lime mix is reasonably diluted before it is poured into the vat, and when it is added, not in one place, but over the entire vat, in the form of a small stream, or a spray, and while the cream in the vat is vigorously agitated. If the full strength of undiluted lime mix is "dumped" into the vat all in one place, there is very intense action on the curd, a portion of the lime mechanically combines with the curd and fat, and will drop to the bottom of the vat in the form of lumps. In this case the lime so fixed, fails to yield its full alkalinity to the serum of the cream and the acid reduction falls short of that calculated even when an excess of 16 to 20% of lime is used, and accurate results from such procedure need not be expected. This lack of proper distribution of the neutralizer in the cream has the further disadvantage of causing excessive loss of fat, the lumps of limy curd in the bottom of the vat being high in fat content. To avoid this, the lime mix should be diluted with an equal volume of water and its uniform distribution is facilitated by spraying it over the vigorously agitated cream, from a flower sprinkling can. Checking Results by Retesting. — Finally, if the operator is to do continuously accurate and reliable work, he must check his work by retesting the cream for acid, after he has given the neutralizer the proper time and condition for full action. 174 NEUTRALIZATION OF SOUR CREAM Other Factors That Cause Irregularities of Results of Neu- tralization.— The complexity of the physical and chemical make-up of cream, its susceptibility to a variety of changes in composition, which are largely beyond the control of the cream- ery, together with irregularities in the preparation and use of the neutralizer which are largely due to the personal factor of the operator, naturally invite frequent fluctuations in the results of neutralization, and interfere more or less with the desired uniformity and accuracy of the results. Notwithstanding these facts, the use of a systematic process of neutralization makes possible the removal of excess acid and the reduction of the acidity to the desired point, within the limits of not to exceed .05 per cent acid above or below that desired. It en- ables the creamery to secure the full benefit of neutralization without danger of overneutralization and its detrimental effect on the quality of the finished product. The dominating factors which cause fluctuations in the re- duction of the acidity of the cream by neutralization are the original per cent acid in the cream before neutralization, the per cent casein in the cream, the amount of carbondioxide in the cream, the strength, dilution and distribution of the lime mix when added, the temperature of the cream and the time allowed for neutralization. Effect of Original Per Cent Acid in Cream Before Neutral- ization on Accuracy of Acid Reduction. — It has been shown that in the neutralization of cream of average acidity (testing about .60 to .80 per cent acid), a portion of the lime (from about 16 to 20 per cent) does not react and that, therefore, lime suffi- cient in amount, or in strength to be equivalent in alkalinity to 16 to 20 per cent in excess of that required to theoretically reduce the acidity to the desired point must be added. It was further shown that this loss of reaction of a portion of the lime is due to the fact that a part of the solid particles of lime mechanically combines with the solid particles of casein, rendering the alka- linity of the lime so held inaccessible to the acid in the cream. The amount of lime not reacting is, therefore, fairly con- stant and does not vary greatly with the acidity of the cream. It is not proportional with the original per cent acid present in the cream. Hence in very high-acid cream, the 16 to 20 per NEUTRALIZATION OF SOUR CREAM 175 cent excess lime added will tend to reduce the acidity of the cream slightly below the calculated point, while in cream of relatively low original acidity, the point to which the acidity drops will tend to be slightly above the calculated point. Effect of Per Cent Casein in Cream on Accuracy of Acid Reduction. — Since the fact, that a portion of the lime does not react, is due to the mechanical tying-up of a portion of the lime with the casein, the amount of lime not reacting must of necessity vary with the per cent casein in the cream, and this in turn is largely controlled by the fat content of the cream. Generally speaking, the ratio of solids not fat to water in cream is the same as that in milk, hence the more fat, and therefore, the less water cream contains, the lower is the per cent of solids not fat in cream, and the per cent curd, being a non-fatty con- stituent is also reduced correspondingly. The following Anal- ysis of Cream, by Richmond,1 illustrates this point clearly. Table 34. — Composition of Cream, Thick Cream % Thm Cream % Water 3937 63.94 Fat . 5609 29.29 Sugar 229 347 Protein 1 57 276 Ash .38 54 99.70 100.00 The above analysis shows that cream testing 56. per cent fat contained only 1.57 per cent protein, while cream testing 3(7. per cent fat contained 2.76 per cent protein. The smaller curd content of rich cream, therefore, ties up less lime than the larger curd content of thin cream. In the case of rich cream, the proportion of lime not reacting with the lactic acid is less than in thin cream. Hence the acidity in rich cream is reduced to a slightly lower point than that in thin cream, when the calculated amount of lime used is the same for both, rich and thin cream. 1 Richmond Dairy Chemistry, Second Edition, 1914, p. 266. 176 NEUTRALIZATION OF SOUR CREAM Effect of Amount of Carbondioxide in Cream, on Accuracy of Acid Reduction. — When determining the acidity present in cream before neutralization by titration with sodium hydrox- ide, the results show not only the lactic acid and the casein acid present, but also the carbondioxide that cream may contain. But the carbondioxide escapes during pasteurization, being ex- pelled by heat; it, therefore, does not claim the alkalinity of the lime added, and allows this alkalinity to further reduce the lactic acid and casein acid of the cream. The carbondioxide content of cream is very variable. It is largely the result of fermentation. In fresh and only moder- ately sour cream it is very slight, while in highly acid cream and especially in yeasty cream, it may be relatively great. Hence, the addition of the amount of lime calculated to reduce the acidity to a given point when based on the original acid test of the cream before neutralization will, in the case of high acid and fermented cream, drop the acidity to a sligthly lower point than that calculated. This irregularity is somewhat mini- mized by the heating of the cream in the forewarmer, which expels a portion of the carbondioxide present before the cream is tested for its original acidity, and the higher the temperature to which the cream is heated in the forewarmer, the more of the carbondioxide is liberated. This fact, however, should not be interpreted to mean that it is desirable to heat the sour cream excessively before neutralization. Such a practice would in part forfeit the benefits of neutralization, causing, especially in the case of thin, sour cream,, the formation of an abnormal curd, with excessive loss of fat and the danger of white specks in the butter. The temperature of the cream before neutral- ization, either in the forewarmer or in the pasteurizing vat, should not be raised above 90 degrees F., if these defects are to be avoided in a dependable manner by neutralization. Effect of Time and Temperature on Accuracy of Acid Reduction. — The neutralizing action of the lime is Comparatively slow, it is not instantaneous. The acid test of the cream, made immediately after neutralization, does not show the full neu- tralizing power of the lime. The per cent acid found in the cream at that time is higher than the calculated per cent acid NEUTRALIZATION OF SOUR CREAM 177 to which the cream is to be reduced. Time is required for com- plete action. Creameries that add their neutralizer by guess and then calculate from the per cent acid found in the cream immediately after neutralization the additional amount of lime needed to reduce the acidity to the desired point, will fail to secure uniform results and may, under certain conditions, un- knowingly overneutralize the cream. Proper dilution and distribution of the lime greatly hasten the action of the lime and the heat of pasteurization assists in completing it. The following table may serve to show the rate at which neutralization progresses from the time the lime mixt properly diluted, is added to the cream, when the temperature of the cream at the time of neutralization averages about 90 degrees F. Table 35. — Showing Progressive Reduction of Acidity in Cream After the Addition of the Neutralizer. Per Cent Acid in Cream After Pasteur- Number of Batches Immediately ization and of Cream Before After Cooling; 2 to 3 Neutralization Neutralization Hrs. After Neutralization Averages of 139 batches.. .658 .295 .251 Averages of 114 batches.. .755 .291 .243 Averages of 175 batches.. .729 .369 .270 Averages of 181 batches.. .740 .362 .275 Averages of 97 batches.. .553 .303 .256 Averages of 133 batches.. .653 .363 .256 Averages of 96 batches. . .485 .300 .244 Averages of 228 batches.. .517 .281 .247 Averages of 76 batches.. .524 .298 .268 Averages of 93 batches . . .594 .335 .271 Averages of 140 batches.. .611 .343 .249 Averages of 1472 batches. .620 .322 .257 Effect of Neutralization on the Composition of Butter. — The composition of butter made from neutralized cream does not appreciably differ from that made of unneutralized cream. The curd content of butter tends to be slightly reduced as the 178 NEUTRALIZATION OF SOUR CREAM result of neutralization. Ramsay1 found the following differ- ences in curd content. Butter Made From Per cent Curd Unneutralized Cream 1.28 Cream treated with Sodium Bicarbonates 87 Cream treated with Calcium Carbonate 72 The above analyses show a rather unusually high per cent of curd in butter made from both, neutralized and unneutral- ized cream. When butter is washed properly the curd content generally averages several tenths per cent lower. However, they are valuable because they show the relative reduction of curd content due to neutralization. The decrease in the curd content may be explained by the fact that the neutralizer causes the precipitated curd to be firmer, more grainy and to separate more completely from the serum. This is especially the case with lime-neutralized cream, but even sodium-neutralized cream has a firmer curd than un- neutralized cream. In this firmer condition more of the curd passes into the buttermilk and less is taken up by the butter. AJ similar difference is noted between butter made from sour and sweet cream. In sweet cream, the curd is present in a more colloid condition which sticks to the butter particles and causes such butter to have a higher curd content than sour cream butter. The butter made from lime-neutralized cream contains slightly more calcium than butter made from untreated cream. Wichmann1 found a slight increase in the calcium oxide of the salt-free ash of neutralized cream butter, as well as in the butter itself, and he claims that when the calcium oxide content of butter exceeds .025 per cent, there is strong indication that such butter was made from limed cream, provided that the salt added to the butter did not contain calcium salts. The slight increase in the calcium oxide of lime-neutralized butter is in all prob- ability due to the calcium attached to the curd. As shown in previous paragraphs, the calcium content of the curd increased 1 Ramsay. Note on Neutralization of Cream in Butter Manufacture and the Effect on the Butter Produced. New South Wales Dept. Agr., Science Bulletin No. 16, 1915. DIRECTIONS FOR NEUTRALIZING CREAM 179 about fivefold when lime was added to the cream. Wich- mann's results, however, are marred by the fact that his experi- ments seem to have lacked a systematic and accurate method of neutralizing. The lime was apparently added by guess and the acid test was taken immediately after neutralization, so that the full neutralizing action was not determined. It is doubtful that butter made from lime-neutralized cream contains enough more calcium oxide to reliably detect neutralization by chemical anal- ysis. In fact such butter might, under certain conditions, con- tain no more or even less lime oxide than butter made from un- treated cream, depending on the completeness of the removal of the buttermilk, which in turn largely depends on the size of the butter granules when the churn is stopped and on the thoroughness of washing the butter. SPECIFIC DIRECTIONS FOR NEUTRALIZING CREAM WITH LIME HYDRATE. 1. Secure hydrated lime that is relatively free from carbonates. If the hydrated lime is a calcium lime (containing but little, not over five per cent magnesium oxide), make up a lime mix or milk of lime by using 2.4 pounds of the dry hydrated lime for every gallon of mix. 2. If the hydrated lime is a magnesium lime, containing not less than 30 to 35 per cent magnesium oxide, make up a lime mix or milk of lime by using 2 pounds of the dry hydrated lime for every gallon of mix. 3. Magnesium lime is more satisfactory than calcium lime. 4. For making up lime mix in small quantities use a ten- gallon can, add 24 pounds of calcium lime or preferably 20 pounds of magnesium lime, fill half full of water, stir until the emulsion is complete, then fill the can full with water and stir again. This now represents the milk of lime, or lime mix, or lime neutralizer. Use the neutralizing tables for determining the correct quantity of this neutralizer required to reduce the acidity in the cream to .25 per cent. 180 DIRECTIONS FOR NEUTRALIZING CREAM 5. For making up larger quantities of lime neutralizer, use a circular tank with agitator, similar to a starter can. A tank with an operating capacity of say 100 gallons may be found most convenient. Mark the level at which the tank contains 100 gallons. This is readily done by pouring ten 10-gallon cans full of water into it and punching a small hole into the side of the tank at a point level with the surface of the water. 6. Withdraw half of the water and weigh into the tank 200 pounds of dry hydrated magnesium lime or 240 pounds of dry hydrated calcium lime, revolve the agitator until all lumps have disappeared and a homogeneous emulsion is secured. Fill up the tank with water to the 100 gallon mark and stir again. A lime mix tank equipped with mechanical agitator which is operated by belt or motor power is much preferable to one with a hand agitator, as .it obviates the laborious work of hand stirring and insures more complete homogenousness of the mix. 7. Now mix the milk of lime in the lime tank thoroughly, giving the agitator at least 15 vigorous turns in the case a hand agitator is used. Then measure out with a gallon measure graduated to half pints the required amount of neutralizer, as indicated in the neutralizing table. 8. Strain it through a cheese cloth into a garden sprinkling pot, add an equal amount of water and sprinkle the neutralizer over the cream in all parts of the vat. 9. Keep the cream agitated while the neutralizer is being added. 10. Always make sure that the quantity of cream and the test of the original acid present are correct, that the milk of lime has been properly mixed before removing the required amount from the lime mix tank and that the neutralizer is prop- erly diluted before it is added to the cream. " ';"' 11. It is advisable to not heat the cream much above 90 degrees F. before the neutralizer is added. PASTEURIZATION 181 CHAPTER VIII. PASTEURIZATION. Definition. — As applied to buttermaking, pasteurization may be denned as the process of heating1 milk or cream to a tem- perature capable of destroying the great majority of bacteria and other ferments contained therein and of cooling quickly to the ripening or churning temperature. In proper pasteurization the milk or cream is heated to 145 degrees F. and held at that temperature for at least twenty minutes or it is heated to from 176 to 185 degrees F. and cooled without holding. Proper pasteurization may also embrace any modification of the above relations of temperature to time of ex- posure that is equivalent in germ-killing efficiency to the above processes and has otherwise no injurious effect on the flavor and texture of butter. If the cream is to be ripened subse- quently, it is cooled after pasteurization to about 65 degrees F. If the ripening process is dispensed with the cream is cooled after pasteurization to the churning temperature which will gen- erally vary from 45 degrees F. to 60 degrees F., according to locality and season of year. Objects of Pasteurization. — Pasteurization does not make possible the manufacture of fancy butter from a poor grade of cream, but it does help the creamery to minimize the injurious effect of contamination of milk and cream with diverse types of germ life and ferments injurious to the quality of the butter and possibly dangerous to the health and life of the consumer. Proper pasteurization, therefore, improves the quality, and keep- ing properties of butter and makes the product safe for consump- tion. Briefly, the chief objects of pasteurization of cream for but- termaking are: Improvement of flavor of butter, better keeping quality, more uniform flavor and quality, destruction of germs of human and animal diseases, increase of economic efficiency of dairy industry. Improvement of Flavor. — Proper pasteurization improves the flavor of butter, partly, because it destroys the great major- ity of ferments present in the cream, some of which are prone to decompose one or more of the ingredients of butter, produc- 182 PASTEURIZATION ing objectionable flavors and odors and partly, because the pas- teurizing heat removes from the cream gases and volatile and soluble substances which possess undesirable odors. Experimental results conducted at various experiment sta- tions in this country and abroad have conclusively demonstrated that efficient pasteurization destroys over 99 per cent of the micro-organisms present in the cream. The type of micro-organ- ism most damaging to the quality of butter is the liquefying bacteria — those which attack the proteins and fat, — and certain species of yeast and molds. Bacteriological analyses of cream before and after pasteurization show that the per cent decrease of these undesirable germs is practically the same as that of the lactic acid bacteria. Pasteurization expels from the cream, vapors and gases, espe- cially carbondioxide gas, which carry with them objectionable volatile substances which may have been absorbed mechanically or which have developed in the cream due to bacterial action. This expulsion is further facilitated by the reduced viscosity of the hot pasteurized cream. Gases are less soluble and more volatile at high temperatures, therefore they escape more read- ily from pasteurized cream. In raw cream they tend to go in solution, they remain in the cream and may be carried into the butter. Soluble decomposition products, such as may be present in cream that has yielded to fermentation, are more easily expel- led from the cream and butter made from pasteurized cream than from raw cream. The clusters of fat globules break up, and offer a greater surface for the liberation of these biprod- ucts. Some of these products as well as the curd, that harbor faulty odors, are precipitated more completely by pasteurization and in this condition pass off in the buttermilk. The curd con- tracts and squeezes out soluble substances, so that part of the curd which subsequently does become a part of the butter is freer from these undesirable, soluble bi-products. Improves Keeping Quality. — Since certain species of bac- teria, yeast and molds that may be present in the cream, cause deterioration of the butter in storage, the elimination of these PASTEURIZATION 183 micro-organisms retards such deterioration and improves the keeping quality of the butter. High temperature pasteurization also destroys the activity of enzymes, some of which are capable of decomposing one or more of the constituents of butter, shorten- ing its life. The destruction of their activity, therefore, furnishes additional protection against deterioration of butter with age. At best the great bulk of butter is several weeks old before it reaches the pantry of the consumer, and during this time it is often exposed to unfavorable temperature conditions which stimulate bacterial and enzyme action. Large quantities of but- ter are also stored for a considerable length of time for the pur- pose of holding it over from summer, the time of surplus, till winter, the period of usual shortage. It is, therefore, of great economic importance that the butter have sufficient keeping properties to successfully withstand the deteriorating influences of age. Produces Greater Uniformity of Quality. — Uniformity of flavor and quality are essential requisites for the successful marketing of butter. The consumer demands that the butter on his table be of uniform quality. With intelligent pasteurization the fermentations in the cream and butter can be more readily controlled, thus insuring greater uniformity of the resulting flavor of the butter of different churnings. Instead of being constantly and entirely at the mercy of the conditions to which the cream is exposed on the farm and in transportation, the buttermaker, by means of efficient pasteurization, is able to modify the variable bacterial flora in cream, eliminating un- desirable ferments and thereby producing a butter of greater uniformity in flavor and quality. Where it is desired to ripen the cream, pasteurization assists in confining the ripening process to the fermentations which are desired and to the exclusion of fermentations of known inju- rious effect. Destroys Disease Germs. — Pasteurization, when* properly executed, also frees the cream, buttermilk and butter from germs of human and animal diseases, thus making the butter safer for human consumption, raising the standard of safety and whole- someness of the product in the eyes of the public and protect- 184 PASTEURIZATION ing the livestock interests of the country against the spread of infectious diseases among young stock and hogs fed on skim milk and buttermilk returned to the farm. Increases Economic Efficiency of Dairy Industry. — For the reasons above indicated, pasteurization has distinct economic value. Through improving the flavor and keeping quality of butter, pasteurization stimulates the appetite and demand for butter; it assists the creamery in securing a satisfactory price for its product and protects it against heavy losses caused by the development of costly defects of butter made from contam- inated raw cream. The increased demand for the improved product, accompanied by better prices, and the elimination of serious loss due to specific butter defects, in turn, enable the creamery to offer to the farmer maximum prices for his butter fat, to increase his profits and thereby to stimulate the produc- tion of milk and cream, and indirectly to improve the fertility of the soil. Through destruction of disease germs pasteurization safe- guards the physical welfare of the consumer and minimizes the danger of heavy losses of livestock due to epizootics resulting from the feeding of infected cream-cry bi-products to farm animals. The improved quality of butter made from pasteurized cream and the guarantee which such butter offers the consumer, as a product wholesome and free from germs of disease, are the most forceful weapons the dairy industry possesses in its never-end- ing struggle against competition with foreign butter and butter substitutes at home, and in its efforts to establish permanent and satisfactory markets abroad. Essential Conditions for Successful Pasteurization, — Many butter buyers are looking upon butter made from pasteurized cream with disfavor, claiming that such butter lacks the desired flavor, open grain and "live" body of raw cream butter. And it is a fact that some butter made from pasteurized cream has marked defects in flavor and in body. In the great majority of these PASTEURIZATION 1&5 cases the cause, however, lies in the improper and faulty appli- cation of pasteurization. These criticisms should not be inter- pretated as a condemnation of the principle of pasteurization, they refer only to the faulty use of a beneficial process. Butter made from properly pasteurized cream does not harbor these defects and is not subject to these criticisms. In order to apply the process of pasteurization so as to ac- complish its helpful objects and to guard against undesirable results, the creamery must use efficient equipment of adequate capacity and kept in sanitary condition, it must have a sufficient and constant supply of heating and cooling media for rapid heat- ing and cooling and for effective temperature control and, above all, the process must be supervised by a competent operator whose experience, knowledge and judgment enable him to prop- erly prepare the cream for, and to conduct, the process in an intelligent and efficient manner. Methods of Pasteurization. — There are in use at the present time fundamentally three methods of pasteurizing cream for buttermaking. These are the flash or continuous method, the vat or holding method and the combined flash and holding method. In the flash or continuous process of pasteurization the cream flows through the pasteurizer in a continuous stream, is heated from 176 to 185 degrees F. and then immediately cooled to the ripening temperature, or the churning temperature. In the vat or holding method of pasteurization the cream is heated in a vat with agitator to a temperature of about 145 degrees F., then held at that temperature for twenty to thirty minutes and cooled to the ripening or churning temperature. * » In the combined flash and holding method of pasteurization the cream flows through a continuous pasteurizer, is heated to a temperature ranging from about 150 to 170 degrees F. and is held in a vat at the above or at 'lower temperatures for from ten to thirty minutes, after which it is cooled to the ripening or churning temperature. 186 PASTEURIZATION FLASH OR CONTINUOUS METHOD OF PASTEUR- IZATION. Flash Pasteurizers. — The following is a list of some of the more popular flash or continuous pasteurizers and coolers now in use in American creameries: f Jensen old style r ~, . . . , \ Jensen sanitary Stationary jacketed -L ^ Peerless Simplex centrifugal (^Eclipse Continuous pasteurizers drum with revolv-: ing agitator Regenerative with revolving drum Revolving discs Jensen sanitary pas- teurizer, regenera- tor and cooler Progress regenera- tive Simplex regenerative f Farrington •s Farrington Jr. ^Miller Tyson Fig*. 22. Jensen flash pasteurizer Courtesy J. G. Cherry Co. Tig. 23. Peerless flash pasteurizer Courtesy J. G. Cherry Co. PASTEURIZATION 187 Principal Features of Diferent Types of Flash Pasteur- izers.— The flash, or continuous pasteurizers are principally of three types. 1. Those consisting of a hollow drum, equipped with a revolving agitator and surrounded by a heating jacket. 2. Those consisting of two hollow drums, the smaller rotating inside the larger one and with the heating or cooling medium circulating in the inner drum and in the jacket surrounding the outer drum, while the cream passes in a thin film between the heating surfaces of the two drums. The latter are frequently of the regenerative type. 3. Those consisting of compartments equipped with revolving discs which heat the cream while it flows through the compartment. This type of pasteurizers usually, though not always, contains also compartments for cool- ing the heated cream. Some creameries use two flash pasteurizers, connected tan- dem fashion, in the place of one. The machines are frequently installed at different elevations. In the lower machine the cream is heated to about 135 degrees F. and in the upper machine to about 180 degrees F. The cream flows from the lower to the upper machine and these pasteurizers may be so connected that the first or lower machine is heated by the exhaust steam of the upper or second machine, or each machine may be heated with direct steam in which case they are generally installed side by side on the same level. This double system of flash pasteur- ization, when properly operated, helps to insure thoroughness of heating. All of the flash pasteurizers with closed drums have the power of elevating the cream, making unnecessary the use of pumps to convey the pasteurized cream over the coolers or into the vats. Some of the flash pasteurizers do part cooling of the heated cream, while the remainder are heaters only and require sepa- rate coolers. For this purpose surface coil coolers are most generally installed. Frequently the surface cooler is done away with and internal tube coolers or other coolers are used, or the heated cream may flow direct from the flash pasteurizer into the ripening vat where it is cooled by the revolving coil. 188 PASTEURIZATION Regenerative Heaters and Coolers. — Some of the heaters and coolers are arranged on what is known as the regenerative principle. The inflowing cold cream is heated by the hot cream passing from the pasteurizer, and the outflowing hot cream is cooled by the cold cream flowing to the pasteurizer. The hot and cold cream tend to equalize their re- spective temperatures by passing in counter- current directions, M a n u f a c turers of these coolers claim that the regenerative principle effects a sav- ing of heat and cold amounting to 25 to 35 per cent of the fuel needed. Construction of Flash Pasteurizers. — Most of the contin- uous pasteurizers are constructed of copper with heavily tinned heating surface. Some of these pasteurizers are lined with Ger- man silver. From the standpoint of heat conductivity there is little choice between the two metals. Their efficiency is prac- tically equally high. The German silver has the advantage of preserving the brightness of its surface. In the copper-lined machine the tin coating soon wears off. This, however, is no serious objection as long as the copper surface is kept bright and no verdigris is permitted to form. The details of construction and of power transmission vary somewhat with the different types and makes of flash pasteur- izers. Their descriptions are usually furnished by the respective manufacturers of the machines. In the installation of flash pasteurizers the directions for the same, which accompany the machines, should be carefully Tig. 24. Simplex regeneration pasteurizer Courtesy D. H. Burrell & Co. PASTEURIZATION 189 followed. The cream connections, especially those for the heat- ed cream, should be of such type as to reduce the friction of the cream and consequently the mutilation of the fat globules, to the minimum. Sharp bends should be eliminated as much as possible, and where they are unavoidable, they should be equipped with rounded sanitary couplings in preference to T's Fig-. 25 Fig1. 26 Jensen universal pasteurizer Courtesy Jensen Creamery Machinery Co. and crosses. The entire system should be composed of stand- ard sanitary pipes, valves and fittings. The straight pipes should be equipped with sanitary unions at intervals of 6 to 8 feet, so as to facilitate their dissembling, cleaning and reas- sembling. Operation of Flash Pasteurizers. — In the case of sweet cream, such as is available in wholemilk creameries, the cream needs no special preparation for pasteurization. It is run through the pasteurizer direct from the receiving vat. When cream arrives at the creamery in thick, lumpy or sour condition or is otherwise in unsatisfactory physical con- dition, as is the case in many of the gathered cream creameries, it is not only desirable but very necessary to warm it to about 90 degrees F. and agitate it until it is uniform in consistency and reasonably smooth. This is best done by the use of a forewarmer. The usual type of forewarmer is a plain, tinned gal- 190 PASTEURIZATION vanized iron or tinned copper vat equipped with a revolving copper coil or disc, through which hot water is circulated to raise the temperature of the cream. The forewarmer should be preferably of "low-down" construction so as to facilitate the "dumping" of the cans. If the cream consists of part sweet and part sour cream or if the acidity of different lots of cream in the forewarmer differs materially, it is advisable to hold it in the forewarmer for about thirty minutes or longer, to make the entire batch uniform in acidity. If this is not done a tough, rubbery curd is prone to form in the pasteurizer, which clogs the machine and the strain- ers and causes excessive loss of fat in the buttermilk. The formation of this curd is due to the fact that the acid in the sour cream acts intensely on the curd in the less sour or sweet cream in the presence of pasteurizing heat. This can be avoided by holding the mixed cream in the forewarmer long enough to allow the acid in the sour cream to act on the curd, in the sweet cream at about 90 degrees F. At this temperature this action is less intense and the curd precipitates in the usual and normal way. Tig. 27. Parringrton Junior pasteurizer Courtesy Creamery Package Mfg. Co, PASTEURIZATION 191 If the mixed cream is neutralized in the forewarmer, as is done in most creameries receiving sour cream, the danger of abnormal curd formation is removed, and it is not necessary to hold the cream in the forewarmer after neutralization. In case the cream is neutralized it is desirable to use two or more fore- warmers of suitable capacity, usually holding 250 to 300 gal- lons, so that, while one forewarmer is being filled, the cream in the other may be neutralized and passed through the pasteur- izer. The use of numerous forewarmers has the advantage of speeding up the work, increasing the capacity of the plant and assisting the continuity of operation of the pasteurizer. Thin, sour cream is prone to suffer more intense curdling action, to cause more difficulty in the pasteurizer and to produce greater loss of fat in the buttermilk, than cream of reason- able richness, testing 30 to 35 per cent fat, and averaging about 33 per cent fat. Excessively rich cream, while desirable from the standpoint of economizing vat and churn space, is objection- able, because it is deficient in milk solids not fat, which are necessary to protect the fat globules against mutilation in the pasteurizer. Such cream, when pasteurized is apt to yield but- ter with a greasy or salvy body and an oily flavor, which may later develop into other and more damaging off-flavors, such as metallic and fishy flavor. It is advisable to standardize all cream in the forewarmer for fat to about 33 per cent fat, and for acid to about .25 per cent acid. Dilution of the cream with water, such as occurs when the cream cans and the vats are rinsed with water, or when the standardizing of rich cream is done with water, should be avoided, because such dilution lowers the per cent of non-fatty constituents in the cream. The cans should be freed from the remnants of cream by inverting them over a steam jet, (see paragraph on Can Washing, Chapter IV,) and the standardizing of rich cream for fat should be done with sweet milk or skim milk or redissolved skim milk powder. For stand- ardizing the acidity, see Chapter VII on Neutralization of Sour Cream. The flash pasteurizer should be set high enough to make unnecessary excessive elevation of the cream by the pasteur- izer. The greater the elevation to which the pasteurizer must 192 PASTEURIZATION raise the cream, the faster must be the speed of the pasteur- izer. This high speed tends to cause the liquid fat globules at the high pasteurizing temperature to become distorted, dis- turbing the thin surface layer of adsorbed concentrated serum, which protects them, and exposing a larger surface of the fat to objectionable influences, such as the oxidizing action of light, air, heat and metals. Excessive speed therefore may, under certain conditions, result in serious butter defects. For tfre same reason it is undesirable also to try to force more cream through the pasteurizer than its rated capacity. The amount of cream the pasteurizer is capable of taking care of depends on the speed of the agitator. The higher the speed of the agitator the more cream can be made to pass through the machine in a given length of time. The flash pasteurizers are usually furnished with specific directions as to capacity per hour and speed of agitator or revolving drum, needed to yield the rated capacity. It is unwise to force more cream through the machine than the rated capacity and speed call for, by speeding up the agitator. If faster work is desired, the instal- lation of a larger machine, or an additional machine, will accomplish the purpose without injury to the butter fat. Forc- ing the machine, aside from its unfavorable effect on the fat globules, also usually diminishes the pasteurizing efficiency. Temperature Control. — In all flash or continuous pasteur- izers the regulation of the temperature needs constant atten- tion in order to make possible uniform heating of all the cream that flows through the pasteurizer. Unless the operator supervises the operation of the pasteurizer from start to finish, reliable results need not and should not be expected. The ease of temperature control varies widely with different makes of machines, as well as with such ever-varying factors as temperature of the cream in the forewarmer, mechanical con- dition of the cream,, uniformity of cream inflow, uniformity of steam supply and uniformity of speed of cream pump and pasteurizer. In order to make possible and to facilitate temperature con- trol, the cream in the forewarmer must have a constant tenv perature, preferably about 90 degrees F., the cream pump feed- PASTEURIZATION 193 ing the pasteurizer must run at a uniform speed, the cream supply pipe must be equipped with a suitable valve regulat- ing the inflow, preferably an automatic regulator such as a float- ing ball device, the steam pressure must be uniform and the pasteurizer must run at a uniform speed. In order to make possible a uniform supply of cream, the cream must also be in satisfactory mechanical condition, it must have a smooth body. An Au"fom Keith, < Boston, Mass. i [Boston butter culture Elov Ericsson, ( Ericsson's but- Commercial St. Paul, Minn. \ ter culture starter cultures '"Chris. Hansen, Little Falls, < N. Y. Lactic ferment Elov Ericsson, J Ericsson's but- St. Paul, Minn. ( ter culture Dry cultures ^ Park Davis & , Co., < Flavorone Detroit, Mich. Eli Lilly, Indianapolis, Ind. Lactic acid culture Mother Starter or Startoline. — In order to revive the desir- able germs in the commercial starter culture and to avoid the. addition of the often malodorous and stale medium of the com- mercial culture direct to the milk which becomes the starter, it has been found necessary to inoculate the commercial culture into a small amount of milk and make several propagations STARTERS 255 (usually two to three) before the culture is transferred to the regular starter milk. This is called the startoline or mother starter. In order to keep the starter in uniformly active and pure condition it is necessary to propagate several jars (4 to 6) of mother starter continuously from day to day, as the conditions which are essential to preserve the starter can be more readily controlled in the case of the mother starter in small jars than in the ''big" starter in the vat or starter can. In the successful propagation of startoline. cleanliness in all operations, good quality of properly pasteurized milk or skim milk, protection from contamination after inoculation, and proper control of temperature are of the greatest importance. Use the best milk or skim milk available; be sure that it has been thoroughly heated to at least 180 degrees F. or higher and held at that temperature at least thirty minutes. Use only jars and other apparatus such as thermometers, spoons, dip- pers, etc. that are perfectly clean and as nearly sterile as is possible to make and keep them under reasonably sanitary factory conditions. Do not touch with the fingers the commer- cial culture nor the startoline but transfer it direct from the original bottle into the jar containing the pasteurized and cooled milk. Keep the startoline jars closed, so as to guard against contamination from the dust in the air. Maintain a uniform temperature of about 65 to 75 degrees F. according to season of year. During the hot season use the lower and during the cold season the higher temperature. Good mother starter demands systematic work and scrupu- lous attention to details and in order to make this possible and to economize time, some suitable equipment should be pro- vided which is available and used for this purpose only. The following simple and inexpensive equipment has been found most serviceable for the preparation of mother starter: Equipment for Preparation of Mother Starter. 1. One galvanized iron box for sterilizing quart jars, dip- pers, thermometers, spoons, etc., size preferably 13 inches long, 8J inches wide, 8J inches deep. 256 STARTERS 2. Twelve, one quart fruit jars with lids. 3. One insulated box, metal lined, with drain hole and in- sulated cover, size preferably 15 inches long, 10 in. wide, 10 in. deep. 4. One dairy thermometer with holder. 5. One dessert spoon. 6. One long handled one pint dipper with lip. Fig-. 36. Electric incubator for the preparation of startoline Courtesy Mojonnier Bros. Co. For creameries operating on a large scale, special incubators and other equipment, manufactured and placed on the market, with detailed directions for installation and use by reliable milk products equipment manufacturing firms greatly facilitate the work and enhance uniformity of results. First Propagation. — Fill a clean and properly scalded quart jar two-thirds full of milk or skim milk. Pasteurize at 180° F. or above and hold for not less than 30 minutes. Time may be saved by heating the milk before the jar is rilled, then fill the jar with the hot milk and set it in hot water at 180° F. for 30 minutes. STARTERS 257 Or the startoline milk may be taken from the milk pasteurizer, held and cooled in the starter vat or starter can. Cool to 70° F. and pour the contents of the bottle containing the commercial starter culture into it, stir thoroughly and let stand at a tem- perature of 80° F., or according to special directions furnished by the manufacturer of the starter culture, until sour and curdled. This usually requires about 24 hours. The seal of the bottle containing the starter culture should not be broken until just before the culture is used. Second Propagation. — Wash six one-quart fruit jars and lids thoroughly clean, rinse them and submerge them in boiling hot water, temperature 200° F. or above, in the galvanized iron box. Pull the six quart jars out of the hot water box, scald the clean dipper by dipping it into the hot water in the galvanized iron box and fill the still hot fruit jars two-thirds full with pasteurized milk from the starter vat, and cool to 75° F. or lower according to season. Take the lids out of the hot water box and place them on the jars. Now open the jar containing the first propagation. With the dessert spoon skim off the top inch, having first dipped the spoon into the boiling-hot water. Place the lid on this jar again and shake thoroughly to break up the curd and until the con- tents are smooth. Again scald the spoon in the hot water and transfer one spoonful of the startoline of the first propagation into each of the six quart jars containing the pasteurized and cooled milk for the second propagation. Seal these jars, and hold them in the insulated box at about 75° F. until sour and curdled. Third Propagation. — The next day again prepare and scald six one-quart jars as directed under the "second propagation." Fill them with freshly pasteurized milk from the starter vat; cool to about 75° F. or below, according to season. Take their lids out of the hot water box and place them on the filled jars. Now line up the six mother starter jars of the second propagation. Open one at a time, dip the spoon in scalding-hot water and remove the top inch of milk from each jar, dipping the spoon into hot water after skimming each jar. Seal these 258 STARTERS jars again with their respective covers and shake each jar until contents are smooth. Then taste the mother starter of each jar, using1 the spoon and always dipping the spoon in hot water for each jar. Select the jar the contents of which have the cleanest and best flavor and transfer with the scalded spoon, one spoonful of its contents into each of the six jars containing the freshly pas- teurized startoline milk. Seal the jars of the third propagation and place them in the insulated box. In hot weather it may be advisable to pour enough tap water (temperature 50 to 60° F.) into the insulated box to- have the jars stand in about two inches, of water. This will help to control the temperature. Close the insulated box. The next morning, examine the jars without removing their lids. If the milk in them is coagulated, place the jars im- mediately into the cold room, or preferably into ice water until ready to use. If the milk shows no signs of coagulation, raise the temperature to at least 75° F. and hold until coagulated; then set in cold water until ready to use. If after a few hours at 75° a satisfactory coagulum does not form, reject the contents of the jar. Succeeding Propagations. — The succeeding propagations are made in exactly the same manner as directed for the third propagation. All the mother starter that is of good quality and that is not used for inoculation into jars is then utilized for the inoculation of the "big" starter in the starter vat or starter can. The amount of mother starter used to inoculate fresh mother starter milk in the jars, and the temperature at which the mother starter is held, should be such that in 12 to 18 hours a nice, smooth and soft coagulum forms on the jars, without the ap- pearance of wheyed-off water. The better, purer and more active the startoline, the less startoline need be used. One dessert spoonful per jar is ample in the case of good startoline. If the holding of the jars at 75° F. causes the curd the next morning to be too firm and possibly to whey-off and to be too high in acid, STARTERS 259 the temperature should be lowered until a temperature is found that will control the fermentation sufficiently to prevent over- ripening and yet to produce the desired coagulum. The acid in good active startoline usually is .8 to .9 per cent. It is not prac- tical, nor feasible, to prescribe an exact temperature that would apply everywhere, and at all times of the year. The operator must use his own judgment and be guided by his results from day to day. The directions above given for the preparation and propaga- tion of mother starter, accompanied by proper modifications of temperature at which the jars are incubated, according to weather and factory conditions, will yield a uniformly good quality of startoline and the results can be depended on from day to day. By the above method, propagations from one and the same culture can be carried on almost indefinitely and the startoline often improves in quality and activity as the number of transfers increases. If the directions on sterilizing all apparatus are con- scientiously followed, the. startoline will have no gas holes. If the temperature is adjusted and controlled properly, there will always be active acid production and good body. Without these precautions, neither the startoline nor the starter can be depended on to be of good quality from day to day, and the startoline has to be renewed often by a new commercial culture. Directions for Making Commercial Starter. Good quality of milk, sterility of all utensils and proper temperature control are all important The absence of any one of these essentials ultimately means poor starter. Good Quality of Milk. — Good quality of milk is all essential for good starter of a sharp, clean acid, such as is desired for the best results, although efficient pasteurization will assist in minimizing defects of the raw material. However, a really good starter cannot be made unless the milk which is used is clean and fresh. Fresh, sweet whole milk purchased direct from dairy farms on which a high standard of sanitary production prevails, generally yields the most satisfactory starter, both as to quality and economy of manufacture. Skim milk, if of good quality, is also suitable for this purpose, but often proves somewhat 260 STARTERS more expensive. Condensed milk and milk powder, though serviceable in the absence of whole milk and skim milk, are not as satisfactory media for starter making. Under favorable conditions they may yield reasonably satisfactory results, but quite often their use conveys to butter a distinct off-flavor. Skim milk powder deteriorates with age, it should therefore, be reason- ably fresh when used. Whole Milk from Fanners. — 'The best quality of starter milk is usually secured where the milk is delivered or shipped direct by the farmer to the factory. Every effort should be made to arrange for such milk supply direct from the farmer. Upon arrival the milk should be graded for quality and tested for fat and with the lactometer. Milk that has an un- clean flavor, or that tests more than 2% acid, or that shows a lactometer reading of less than 29 points at 60° F. should not be accepted for starter milk. Special attention should be given the cans returned to the farmers. These cans must be free from rust. They must be washed, rinsed, steamed and dried properly, so that they are perfectly clean, dry and sweet-smelling. The farmer should not be allowed to take back buttermilk in the cans in which he furnishes the milk for starter making. If he wants buttermilk, he should use a separate set of cans for it. The cans for the sweet milk must be returned to him empty, clean and dry. Skim Milk or Whole Milk from Milk Products Factories.— Milk or skim milk purchased from ice cream plants or other milk products factories is usually of poor quality, it is often high in acid and frequently contains undesirable off-flavors. If secured from these sources, each can should be carefully in- spected and it should be clearly understood by the party sel- ling, that milk that is stale, high in acid, off in flavor, or con- tains preservatives, or extraneous water, will be rejected. The milk must be delivered in cans that are free from rust and clean. If the factory from which this milk is purchased furnishes the cans, the plant should be visited to make sure that the cans are in satisfactory condition when they are filled with the milk or skim milk, STARTERS 261 Milk, and skim milk purchased in this manner, should be tested with the lactometer. At 60° F. normal whole milk varies between 29 and 35 lactometer degrees, and normal skim milk varies between 36 and 38 lactometer degrees. If whole milk drops below 29 and skim milk drops below 36 lactometer degrees it may reasonably be suspected that they have been watered. If whole milk rises above 35 lactometer degrees it has been skim- med. If skim milk rises above 38 lactometer degrees it has been adulterated with some foreign substance, other than water. Condensed Milk. — If condensed milk is to be used, purchase plain condensed bulk milk, skimmed. Ask for a concentration of four to one. Dilute with three gallons of water for each gallon of condensed milk. Pour the water into the starter vat first, start the coils without heat and add the condensed milk. Mix well, and pasteurize as usual. If the condensery is not in position to furnish condensed milk with a concentration of 4:1, secure what they can furnish, and ask them for the ratio of concentration and dilute as follows for milk with different con- centrations : Gallons Concentration Gallons Water Condensed Milk 4 :1 3 1 3|:1 2f 1 3i:l 2\ 1 3J:1 2i 1 3 :1 2 1 Skim Milk Powder. — Dissolve at the rate of one pound of powder to nine pounds of water. Attach two small wooden slats, similar to lath, to the coil on its periphery on opposite sides. The slats should be long enough to reach from one end of the coil to the other. They will help to beat up the lumps and to mix and dissolve the powder. These slats are best fastened to the coil by means of "U" bolts. There are some vats on the market, originally intended for use in preparing the mix in ice cream factories, the coil of which is equipped with metal slats, running lengthwise. These vats are ideal for this purpose. Then pour the water, cold or luke warm, into the vat, and add the skim milk powder. Avoid pour- 262 STARTERS ing the powder over the sides of the vat and on the coil as it tends to stick and cake upon heating. Start revolving the coil and turn the heat on. Pasteurize as usual. Preparation of Starter Milk. — Heat the milk, skim milk, or the diluted condensed milk, or the dissolved skim milk powder to 180° F. or higher, hold for one hour and cool to 75° F. or lower, according to season. Keep covers down while cooling. Now add the startoline. Two quarts of good startoline is suf- ficient for 200 gallons of milk. If the startoline is not in good active condition, larger quantities are necessary. Agitate with coil, cover down, for ten minutes. In hot weather, it may be advisable to allow a small stream of water to run through the coil in the vat or through the jacket in the starter can, over night, in order to prevent the temperature from rising too high. In this case the valve in the water pipe should be open just a "crack." The next morning, examine the starter. With a properly scalded dipper, dip out some and test for acidity. If a nice smooth coagulum has formed and the acidity is about .8% or slightly over, cool at once to 50° F. or below and draw the starter off, adding it to the cream as needed. If the starter is not needed for several hours, but the starter vat or can must be vacated for the preparation of the next batch, draw the starter off into clean, steamed and dried shipping cans and set them in the cooler, so as to avoid further fermentation. When the vat is empty, rinse it, wash it clean with wash- ing powder and hot water, rinse, and steam thoroughly with cover down. Fill with new batch of starter milk, pasteurize at 180° F. or above, hold for one hour, cool to about 75° F. or lower, according to season and add startoline as directed for previ- ous day. A good starter has an acidity of about .8 to .9%, it is clean, fairly sharp and has a smooth, soft curd that shakes down readily and that is free from gas holes. Equipment for Making Commercial Starter: Where only a small amount of starter is needed, the milk may be heated in ten gallon milk cans by setting the cans in a vat containing boiling hot water. For larger quantities of starter milk special equipment is desirable. The circular starter STARTERS 263 can, with the insulated water jacket on the outside and the re- volving agitator on the inside, has been found very convenient for this purpose and is in general use in many creameries. The chief objection to these starter cans is that the agitation of the relatively great volume of milk is not sufficient at the periphery to keep the milk from baking onto the heating surface. This makes thorough cleaning exceedingly difficult and laborious and it invites the application of agents which remove the tin as well as the remnants of milk from the copper lining. For creameries with a large make the circular starter can is too small. They generally use standard cream ripening vats with disc or coil agitator and with cover, as their receptacle for starter making. Easy con- trol of temperature is es- sential. As a whole, copper- lined starter cans or starter- vats are objectionable. The tin coating on the copper soon wears off, exposing the copper surface This invites action of the acid in the starter on the copper, yield- ing metallic salts which are distinctly injurious to the quality of the cream and butter, enhancing decomposition which jeeopardizes the flavor and keeping quality of the butter, and leading to the development of such butter defects as metallic flavor, tallowy flavor, fishy flavor, etc. If tinned, copper-lined starter cans and vats are used, they should be retinned as soon as they show any considerable area of exposed copper. The use of glass-enameled starter vats cannot be too highly recom- mended as the most suitable equipment for starter making. Fig*. 37. Trunion starter can Courtesy Creamery Package Mfg. Co. 264 STARTERS Pigf. 38. Glass-enameled starter tank Courtesy Elyria Enameled Products Co. The Proper Degree of Ripeness. — At the time when the starter milk begins to be sour to the taste, but has not reached the coagulating point, it usually has a peculiarly disagreeable odor and flavor. This is explained to be due to the activity of other micro-organisms aside from the lactic acid species in- oculated. Later, when the acid is more pronounced and the milk is at the point of curdling, this disagreeable flavor and aroma generally disappear, the lactic acid species of bacteria having gained the ascendancy, holding the other species in check. If the starter were therefore used in the early stage of acid development and before the battle of species for the survival of the fittest had been decided in favor of the lactic acid organisms, the starter would fail to lend to the cream and the resulting butter the flavor for which it is used. It is important, therefore, to permit the starter to develop until the maximum number and activity of lactic acid bacteria are secured, which is the case usually at the point when the milk commences to curdle. STARTERS 265 On the other hand, it is equally undesirable to carry the souring process too far. After the casein is coagulated the lactic acid bacteria seem to lose their maximum efficiency as acid producers, they weaken, become inactive or degenerate and permit other species to gain the ascendancy. The starter loses its fine flavor and its snap, yeasty fermentations and casein- digesting changes set in, which make the starter unfit and un- safe for use. It is generally conceded that .80 to .90 per cent acid represents the maximum acidity to which it is safe to allow starter to ripen when ordinary commercial cultures of lactic acid bacteria are used. This does not necessarily hold good with cultures of Bacillus bulgaricus. This organism is capable of developing a much higher acid without degenerating and without depreciating the aroma and flavor of the cream. Bacil- lus bulgaricus has not as yet been thoroughly tried out in con- nection with cream ripening and its desirability as a starter organism is as yet undetermined. Amount of Starter to Use. — For directions concerning the proper amount of starter to add to cream the reader is referred to the chapter on Cream Ripening. Scoring the Starter. — In order to express the quality of the starter, aside from the per cent of acid it contains, in more con- crete terms, it is desirable to use a figure scale, or score card. This is especially desirable for the use of the student and for experimental data. The following score card is recommended for this purpose : STARTER SCORE CARD Name, Date, Score Description Perfect] Actual Aroma . . Flavor .... Body 20 40 20 20 Clean, pronounced, pleasant, no taints Clean, pronounced, snappy, free from .yeasty, cheesy, curdy and other off-flavors Smooth, soft, creamy, no gas holes, no whey .8 to .9% acid Acid Total 100 266 CHURNING CHAPTER X. CHURNING. Object of Churning. — The object of churning is to separate the butterfat from the caseous and serous parts of the milk or cream, to make butter. This is accomplished by the formation of butter granules. Philosophy of Churning. — The formation of butter granules is brought about by the crystallization or solidification of the fat in the fat globules and by coalescence of the wholly or partly solidified fat globules into butter granules. Milk and Cream an Emulsion. — In freshly drawn milk the fat is present in the form of minute globules of liquid fat. These fat globules are emulsified in a watery mixture of hydrated col- loid— the skim milk. An emulsion, in this case, is a mixture of two liquids which are insoluble in each other, where one is suspended in the other in the form of minute globules. Milk then represents an emulsion of fat-in-skim milk, the fat rep- resenting the divided or dispersed phase, and the skim milk the continuous or dispersing phase of the emulsion. As long as this emulsion remains intact, there can be no formation of butter granules. Butter does not form. The establishment of this emulsion of fat-in-skim milk is the direct result of the process of milk secretion. When milk is secreted, nature places the fat, \vhich is liberated by the metabolic activity of the cells which line the alveoli, into the skim milk in the form of very finely divided particles. Fischer and Hooker1 who made an extensive study of fatty secretions and fatty emulsions, considering the phenomena of milk secretion from the standpoint of the pathologist, speak of the secretion of butterfat as a fatty degeneration of the cells in the alveoli. "The originally cubical cells wrhich make up the alveoli of an active mammary gland become richer in water and filled with granules (cloudy swelling), while the fat in the cells runs together into more readily visible droplets (fatty degeneration). When this process of cloudy swelling with fat 1 Martin H. Fischer and Marion O. Hooker, Fats and Fatty Degeneration, 1917. CHURNING 267 Fat Globules in Milk, Cream, Skimmilk and Buttermilk Magnification 740. Pig-. 39. Milk fig. 40. Cream Fig*. 41. Skim milk FIff. 42. Buttermilk coalescence becomes sufficiently great, the cell bursts and a fluid mixture of hydrated colloid (meaning the skim milk), con- taining the fat globules, results. This is milk." It is obvious from the above discussion that the fine divi- sion and uniform distribution of the fat in the milk, or the fat- in-skim milk emulsion, is the handiwork of nature. In this finely divided state the fat is most accessible to the digestive juices, facilitating digestion by the young, who depend on milk as their exclusive food and whose delicate digestive or- gans are not prepared to deal with solid masses of fat. 268 CHURNING Permanency of Fat-in-Skimmilk Emulsion. — This emul- sion, established by the secretion of the milk, is fairly per- manent. The question here consistently arises: What causes these fat globules to remain divided, what hinders them from running together like oil? Earlier investigators claimed that each fat globule was surrounded by a definite membrane. This was a mere assump- tion which proved erroneous. The presence of such a membrane has never been satisfactorily established. Later study failed to demonstrate .its existence and yielded substantial evidence that such a membrane does not exist. The only envelope that sur- rounds the fat globules in milk is the skim milk in which they are suspended. The forces that make it possible for the minute fat globules to retain their identity as single units and that prevent them from running together, are the difference in the surface tension be- tween the fat globules and the skim milk, adsorption and the viscosity of the milk. Surface Tension. — The fat globules stay apart, they retain 'their individuality, they do not run together, primarily because of the law of surface tension. By surface tension is under- stood the attraction which the molecules of one and the same substance have for each other. The molecules which are located in the surface of a liquid, are attracted toward the interior of the liquid by the molecules situated there, but there is no similar attraction towards the exterior, because the molecules in the interior of a liquid* are subject to .attraction from all sides. The tension thus produced on the surface by this molecular at- traction towards the interior is called the surface tension. It obviously conveys to the surface the tendency to become re- duced to the smallest possible dimensions. Hence, if a liquid is placed in a position, where it is not affected by gravity, the form of the liquid changes until it assumes the smallest possible surface for a given volume. And this is the sphere. In the case of milk, in the secretion of which nature has placed the fat in finely divided particles, the fat possesses a greater surface tension than the surrounding skim milk. The minute, CHURNING 269 units of fat, therefore, retain their identity and individuality and, because of the surface tension, they are present in the form of round globules. Adsorption and Viscosity. — The ability of the fat globules in milk and cream, to retain their individuality is further assisted by the law of adsorption and by the viscosity of the milk. By adsorption, in the sense here used, is meant the some- what greater concentration in the surface layer of the fat globules of the skim milk; than the concentration of the 're- mainder of the surrounding skim milk. This concentration of the skim milk on the surface layer of the fat globules assists in maintaining their internal cohesion and in diminishing the power of adhesion between fat globules. It tends to convey to the individual fat globules greater stability. Finally, the permanency of the emulsion of the fat globules in milk is enhanced by the natural viscosity of the skim milk, caused by the presence of such colloids as albumen and casein, and of milk sugar. Effect of Cream Separation. — When cream is separated these phenomena do not materially change, they remain funda- mentally the same. Cream still represents an emulsion of fat- in-skim milk. The composition of the non-fatty serum in cream is similar to that of milk and the difference in the surface ten- sion between the fat globules and the cream serum remains the same. There is merely a larger aggregation of fat globules in a smaller volume of skim milk. Effect of Cooling of Cream. — When cream is cooled, pre- paratory to churning, the fat in the fat globules wholly or partly solidifies. This enhances the internal power of cohesion in the fat globules and increases the power of adhesion between fat, globules, offsetting and completely overcoming the effect of the surface tension of the fat globules. If cream were not cooled sufficiently to partly or wholly solidify the fat, the churning would result in a finer division of the fat globules. Effect of Agitation in Churn. — When this cooled cream, with the partly, or wholly solidified fat globules is subsequently subjected to the agitation and concussion generated in the re- 270 CHURNING volving churn, the increased power of adhesion enables the partly or wholly solidified fat globules to unite, forming butter granules. Increase in Size of Butter Granules. — This union of fat globules and formation of butter granules proceeds in geometric progression. While it commences as soon as the churn starts revolving, the process of uniting at first is slow and the change is imperceptible. The minute size of the fat globules retards their opportunity for collision with and adhesion to one-another and the butter granules resulting from these early adhesions are microscopic in size. The average fat globule measures about 3/1000 of one millimeter or about 1/10,000 of one inch in diam- eter. The sum of two fat globules forming one butter granule, therefore, also is extremely small. But, as the churning process progresses, the butter granules form more rapidly and grow in size more rapidly. The larger they grow the more rapidly they increase in size with each successive adhesion. Why Cream Thickens in the Churn. — As the churning process proceeds, the cream begins to thicken and continues to thicken, until it assumes marked rigidity, practically assuming maintenance of form. This thickening is due in part to the increased size of the still microscopic or semi-microscopic but- ter granules. These larger granules offer more internal friction and hold the serum in a mash-like emulsion. Up to a certain point, the larger these microscopic granules the thicker and more rigid the cream. The thickening of the cream during the early part of the churning process is also due, in a large measure, to the profuse incorporation of air in this viscous, cold cream. The cream whips. The air so incorporated and the rigid character of the cream which the minutely divided air helps to bring about, have a very marked retarding effect on the churning process, greatly minimizing the concussion to which the fat globules are subjected, and making it difficult for them to find each other and to strike each other with sufficient force to coalesce to one CHURNING 271 another. If it were not for the obstructing presence in the cream of this air, cream would churn more rapidly. It is obvious that in a vacuum, or under reduced pressure, the churning- process would occupy much less time. Since it is during the churning process and not during the working process, that the bulk of the air found in the finished butter, is incorporated, and since the presence of air in butter represents an active agent of butter-deterioration, churning in vacuo, aside from grealy reducing the churning period and in- creasing the capacity of the creamery, would tend to exert a markedly favorable effect on the keeping quality of the butter. Under certain conditions, which render cream excessively viscous, such as is the case in cream from stripper cows, or very cold /cream, or cream that has undergone ropy-milk fermen- tation, the churning process is very much prolonged and fre- quently it does not reach the breaking point at all, because of the air-holding and whipping properties of the abnormal viscosity of such cream. For this same reason, any agency, or condition that reduces the viscosity, hastens the churning pro- cess. Thus, sour cream churns more quickly than sweet cream, the acid destroying the viscosity and the whipping power of the cream. Cream from cows which have been in milk for a short time only churns more rapidly than cream from stripper cows, because the former is more fluid and less viscous. At a high churning temperature, provided that the temperature remains below the melting point of fat, cream churns quicker than at a low temperature, because a rise in the temperature increases the fluidity of the cream. In this stiff and rigid cream the emulsion of fat-in-skim milk is still intact. Why Butter "Breaks" Suddenly. — As the butter granules become larger in size in the thickened cream, a point is reached, where the surface of the butter granules becomes so small in proportion to their cubic contents, that the fat-in-skim milk emulsion can no longer be sustained, the emulsion is broken. 272 CHURNING The skim milk (now called buttermilk), in excess of that por- tion that is incorporated in, or adheres to, the surface of the butter granules, recedes and "wheys off," the butter granules separate out, and the butter "breaks." This point is reached after the majority of the butter granules have outgrown their original microscopic size and have become large enough to be readily visible to the naked eye. Pig. 43. Water droplets in butter, magnification 740 With the "breaking" of the butter, the emulsion changes from a fat-in-skim milk emulsion as represented by the cream, to a buttermilk-in-fat emulsion, as is represented by the butter. The fat globules cease to exist as units. Butter is a mass of butterfat into which have been emulsified small divided units, or droplets, of buttermilk. Butter represents an emulsion in which the fat is the continuous phase and the hydrated colloid or buttermilk the divided or dispersed phase. While, under normal conditions of churning, the churning process occupies from about 40 to 60 minutes, the actual "break- ing"of butter happens with almost instantaneous suddenness. CHURNING 273 The reason for this is obvious. As previously explained, the increase in the size of the butter granules during- the early stages of the churning process is slow, due to the small initial size of the fat globules and to the obstructing foam. Numerous pro- gressive steps of adhesion between fat globules and later be- tween butter granules are necessary before the breaking point is reached. This requires time, and yet, during all this time there is no visible sign of butter formation. Just before the breaking point the contents of the churn are still cream. But the butter granules, though still invisible to the naked eye, have reached the maximum size at which their reduced surfaces are still capable of sustaining their emulsion with the skim milk in the form of cream. One more union between each two of these relatively large butter granules, causing the granules to be twice of this already relatively large size, may break the emulsion, the resulting granules being too large and their surfaces too small to still sustain their emulsion in the skim milk of the cream. The result is that the skim milk immediately breaks away from the butter granules and the butter "breaks," and we have masses of butter granules on the one hand and buttermilk on the other. The suddenness of the "breaking of the butter is further intensified by the fact, that the relatively large size of the still emulsified butter granules in the cream just before the breaking point, facilitates the coalescence, or adhesion, of these granules in the cream. The larger the granules before the breaking point, the more easily they find each other, the more readily they col- lide, and the accelerated force of impact between these larger granules increases their power of adhesion. When they collide they stick together. Simultaneous with the break of the tension of the fat-in-skim milk emulsion, much of the incorporated air also is liberated, further quickening the breaking of the emulsion. Hence, when this critical point is reached, one or a few more revolutions of the churn suddenly transforms the emulsion of cream into solid butter and fluid buttermilk. The butter "breaks" abruptly. The foregoing discussion makes it clear that the churning process resolves itself into a change from a fat-in-skim milk 274 CHURNING emulsion, such as exists in milk and cream, into a buttermilk-in- fat emulsion, such as exists in butter. This transformation of emulsions, or of cream into butter, is brought about funda- mentally by solidification of the fat globules and by subsequent coalescence of the solidified fat globules, forming butter granules, and by progresive adhesion or uniting of the butter granules. Solidification. — The solidification of the fat globules is caused by low temperature and concussion. The solidifying point of butterfat, like the melting point, is not constant. It varies particularly with the chemical compost tion of the butterfat. Thus the fats of the harder glycerides, such as the myristin, stearin and palmitin, have a higher solidifying point than the fats of the softer glycerides, such as the fats of the volatile fatty acids and the olein. Hence the solidifying point fluctuates according to the relative proportion of these several fats in the mixed fat. At the temperature of the animal body, 98° to 100° F., but- terfat is liquid. At ordinary temperatures (room temperature) butterfat contains both solid and liquid elements. By lowering the temperature, fractional crystallization of the butterfat is ef- fected, the harder glycerides crystallizing first. As the tem- perature drops, more of the softer glycerides begin to crystallize. The extreme range of the solidifying point of the mixed butter- fat lies between about 15.5 degrees C. to 30 degrees C. (60 to 80 degrees F.) Under normal conditions the range of tem- perature is confined to much narrower limits, not falling below about 18 degrees C. nor exceeding 24 degrees C. (65 to 75 degrees F.) and averaging about 21 degrees C. (70 degrees F.). In order for the fat globules to form butter granules, it is necessary therefore, to lower the temperature of the cream suf- ficiently to insure solidification of the fat in the fat globules. The reason why the churning temperature of the cream must be dropped below the minimum temperature at which the mixed fat solidifies, must be attributed in part at least to the fact, that mere solidification, while it causes the cream to churn, does not necessarily give the butter granules the desired firmness. Lower temperatures are needed to render the butter granules sufficiently CHURNING 275 firm to insure exhaustive churning and to produce butter with good body, and free from leakiness and excessive moisture. Recent experiments by Hunziker and Hosman have revealed the fact that mixed butterfat has more than one solidifying point. It appears that even in the cooling of the cream the mixed but- terfat does not solidify all at one temperature, but that fractional solidification takes place, the high melting-point fats solidifying first. These findings further explain why it is necessary to cool the cream to a temperature materially below that of the solidifying point of the mixed butterfat, if a firm bodied butter is to be secured. The temperature must be low enough to also cause the solidification of the lower-melting point fats, particularly the olein. In fact it is at this point, it is in the cream vat, that the body of the butter is determined. If the cream has never been exposed to a temperature low enough to solidify all the butterfat, the butter tends to have a weak and slushy body that does not stand up well under unfavorable temperature conditions. In a warm room it is prone to soften quickly, because some of its fat constituents have not been properly solidified, they still are in fluid, or semi-fluid, condition and cause the butter to become soft and lose its shape even at temperatures below the melting-point of butter. On the other hand, if the cream, at least once between the processes of pasteurization and of churning, has been cooled sufficiently to completely solidify all the butterfat, the butter made from such cream will have a good body that will hold up well, even under unfavorable temperature conditions. In this case the butter has to be warmed to near the melting point, before it will show signs of appreciable softening. And even a considerable rise in the churning temperature of such cream above that desired will not materially reduce the firmness and standing-up properties of the butter made therefrom. Aside from the churning temperature the solidification of the fat globules is enhanced by subjecting them to vigorous con- cussion. The agitation which the cream receives in the churn, furnishes this concussion and therefore further hastens the solidi- fication of the fat globules. 276 CHURNING Coalescence. — Coalescence is the second necessary factor for the formation of butter granules By coalescence is meant the uniting and adhering together of the fat globules and butter granules. The power of the fat globules to coalesce is largely determined by the extent of solidification and the amount of con- cussion. It is also affected by the size of the fat globules, by adsorption and by the viscosity of the cream. In liquid form the fat globules cannot coalesce to the extent of forming butter granules. In warm cream set at rest they may run together, "oiling off" and forming a continuous layer of oil. In cream at any temperature not low enough to cause solidifica- tion or partial solidification of the fat, when subjected to agita- tion such as is produced in the revolving churn, the fat globules, instead of coalescing tend to diminish in size, due to the effect of their surface tension, adsorption and the viscosity of the cream. For this reason cream does not churn out, and but- ter granules do not form when the temperature is too high to effect at least partial solidification. On the other hand, coalescence and the formation of butter granules is greatly delayed, if not made impossible, when the degree of solidification has been carried so far, as to cause the fat globules and the small butter granules to be very hard. In this case the adhesive property, or stickiness, of the fat globules and of the initial butter granules is greatly reduced, the impres- sion which they suffer when they collide is very slight, the surface of contact is therefore too small and the individual globules and granules are too firm to readily adhere to each other when they collide. For this reason, cream that is churned at an ex- tremely low temperature, or that has been held at a very low temperature for a long time before churning, or the fat of which has a relatively high melting point, churns with great difficulty. In order to give the fat globules an opportunity to coalesce they must be subjected to concussion. This is obviously produced by the operation of the churn. The more vigorous the concussion, other things being equal, the greater their power to coalesce and the more rapidly is the churning completed. Other conditions being the same, the time required for the butter granules to form is determined by the size of the fat CHURNING 277 globules and by the viscosity of the cream. The larger the fat globules the more rapid the formation of the butter granules1. The effect of the concussion and the ease of coalescence are intensified in the case of the large globules, because they strike each other and the sides of the churn oftener and with greater force than do the small globules. The viscosity of the cream diminishes the force of the con- cussion. It obstructs the frequency of the collisions between globules and detracts from the force of the impact when they do collide, lessening their power of adhesion. Conditions which Affect the Churnability of Cream and the Mechanical Firmness of Butter. — The ease with which cream churns is dependent on many and varying factors, some of these factors have to do with the initial character of the cream as it arrives at the factory, while others refer to conditions of the proc- ess of manufacture. To the former group may be classed the size of the fat globules, the chemical composition of the butterfat and the viscosity of the cream. The second group includes such factors as temperature of cream, degree of ripeness, richness of cream, nature of agitation, fullness of churn, speed of churn. The following schematic classification may serve to illustrate the numerous factors which enter into the churnability of cream, and to clarify their logical relation to each other : 1 Hunziker, Mills and Spitzer, Purdue Bulletin No. 159, 1912, p. 325. 278 CHURNING Classification of Essential Conditions Influencing the Churnability of Cream I Chemical [Breed composi- J Period of tion of 1 lactation butterfat [Feed Temperature f Churning temperature of butter- 4 Credi- cott Mittle- sted Credi- cott Keist Mittle- sted 1 none 12 93 93 93 93^ 93^ 9$y2 93^ 2 2.20 12 93 93 93 93 93 94 93^ 3 4.44 12 92 92 92 91 91 91 91 4, 6.66 12 88^ 88^ 88^ 88 l/s 88 87 87*4 5 7.17 12 87^ 87^ 87^ 89' 89 88^ 8814 6 none 30 94^' 94^ 94^ 94 94 94 94 7 2.92 30 91 90^ 9034 91 90^ 90J4 9oy3 8 6.13 30 89 91 90 90 90 90^ 90^4 9 7.81 30 89 90^ 8934 88 88 87 87% 10 8.57 30 89^ 89^ 85 85 84 84% The above ten lots of butter were made from the same churning. Lots 1 to 5 were worked 12 revolutions, lots 6 to 10, inclusive, were worked 30 revolutions. These findings, then, give evidence of the fact that while a small amount of salt may and does retard the action of some un- desirable microbes, such as certain molds and yeast, and at the same time permit the activity of desirable bacteria, such as the lactic acid speries and, therefore, has a tendency to improve the keeping quality of butter, the opposite effect may be expected with heavily salted butter. But the effect of salt on the keeping quality of butter, is also governed and modified to a very appreciable extent, by the temperature at which butter is stored. Bacteria, in order to thrive on the food they find in butter, must have that food in liquid form. When the serum of butter, containing the curd 1 Hunziker, Mills and Spitzer, Moisture Control of Butter. Purdue Bulletin 160, 1912. SAI/TING THE BUTTER 341 and sugar, is frozen, bacteria cease to be able to utilize it and their activity stops. When butter is stored at or above the freezing point of water the liquid portion in both salted and unsalted butter is in solution. In salted butter liquid brine has a retarding influence on some of them, while in unsalted butter ' their development is unhindered. It is obvious there- fore that at ordinary temperatures the unsalted butter will spoil more readily than the salted butter, a fact which is amply borne out in the commercial manufacture and handling of butter. But not so when butter is stored at the cold storage tem- perature generally used in this country, i. e. — 6 to — 10° F. At such low temperatures the moisture in unsalted butter is frozen solid, a fact which makes further bacterial development impossible. In heavily salted butter on the other hand, the freezing point of the brine is very near the storage tempera- ture. The brine therefore remains in solution for a relatively long period of time and the micro-organisms which are capable to resist the concentrated brine are able to continue their work. That the brine in heavily salted butter remains in solution for some time, if it freezes at all after the butter has been placed in cold storage, is clearly shown in the paragraph relating to "The Effect of Salt on the Moisture Content of Butter.'1 Unsalted and lightly salted butter lost practically no moisture in cold storage, while heavily salted butter lost from one to three and one-half per cent moisture. Similar results are re- ported by Washburn.1 These findings are in no way contradic- tory to those obtained by the investigators previously quoted who reported that salted butter kept better than unsalted but- ter, because of the differences in the temperature at which their butter was stored. The earlier impression among buttermakers and also quoted in some of the text books was that salt covers up the bad flavors in butter, and it used to be recommended that but- ter of inferior quality should be salted heavily in order to hide the undesirable flavors. Our latest findings on this point do not bear out this assumption. On the contrary, experience has 1 Washburn. Influence of Salt on Storage Butter, Journal of Dairy Science, Vol 1, No. 2, 1917. 342 SALTING THE BUTTER shown, that heavy salting rather intensifies than minimizes the effect of poor quality. Such butter usually takes on a disagree- able, coarse flavor particularly objectionable to the consumer. In fact the bulk of evidence goes to show that butter made from second grade cream is of better flavor and sells to better advan- tage when it is not salted at all. For this reason many of the most progressive creameries, whose daily make is sufficiently large to justify them to churn the different grades of cream separately, put their second grade cream into unsalted butter, for which they can realize a better price than if they salted it, and frequently their second grade unsalted butter brings as good a price as their first grade salted butter. Leaving out of consideration the preference of the con- suming public, one of the most important disadvantages of un- salted butter, as related to quality, lies in the fact that unsalted butter molds very much more readily than salted butter. Mold development usually makes its appearance within less than two weeks of manufacture. Since this is the period before the but- ter reaches cold storage, and during which the temperature to which the butter is exposed, is generally considerably above 32° F., mold growth makes rapid progress. In the absence of salt there is nothing to inhibit it, and if the unsalted butter happens to be made from cream that is high in acid when churned, the moldiness is further intensified. Molds flourish in an acid medium. Salt brine, on the other hand, retards mold growth. Salted butter, therefore, is not so prone to arrive on the market in moldy condition. Effect of Salt on Possible Germs of Disease That May be Found in Butter. — This applies only to butter made from raw cream, as it is generally conceded that proper pasteurization of the cream eliminates the germs of infectious diseases from butter. Data on the effect of salt on the virulence of patho- genic bacteria, are not numerous and such data as are available are confined to the bacillus of tuberculosis. Schroeder and Cotton,1 as the result of experiments with infected butter, conclude that living bacilli of tuberculosis will retain their infectious properties for at least 160 days in salted butter when 1 Schroeder and Cotton, The Relation of the Tubercle Bacillus to Public Health, U. S. Dept. Agr., B. A. I. Circular 153, p. 38. SALTING THE: BUTTKR 343 kept without ice in cellar. Mohler, Washburn and Doane1 re- port as follows: "No dependence should be placed upon the action of the salt that is added to butter as an agent in the destruction of Bacillus tuberculosis. It has been shown that the effect of salt as commonly used in the manufacture of but- ter, is very slight at best. Most of the samples used were salted with the usual amount. Yet the butter contained its virulence for 6 months." These facts emphasize that the heavy salting of butter, as usually practiced on the dairy farm where butter is made, is not an adequate substitute for pasteurization and that pasteur- ization is indispensible as a guarantee of freedom from disease germs. Effect of Salt on Moisture Content of Butter. — Before the salt is added to butter, butter represents an emulsion of water- in-fat, in which the water is present in very small drop- lets, of relatively uniform size and even distribution. The addition of salt causes this emulsion to be disturbed. The salt, owing to its great affinity for water, draws many of the water droplets together into larger droplets and drops and even larger aggregates. There is a marked decrease in the number of small droplets and an increase in the number 'of large droplets. And there is an unmistakable tendency for water to run out of the butter, causing a decrease in the per- centage of moisture. In butter made from cream that was not sufficiently cooled, nor held at the low temperature long enough to thoroughly chill and harden the fat before churning, the salting invariably produces a leaky body. In this case the mechanical-condition of the fat is such that the formation of the water-in-fat emul- sion, resulting during the churning process, is incomplete. While it is sufficiently complete to prevent unsalted butter from being leaky (unsalted butter never is really leaky) it is not suffi- ciently complete to withstand the emulsion-disturbing influ- ence of the salt. It yields to the salting-out process and be- comes leaky. At best the salt tends to decrease the moisture content of 1 Mohler, Washburn and Doane. Virility of Bacillus Tuberculosis, U. S. A. I. 26, Annual Report, 1909. 344 SALTING THE BUTTER butter to some extent, and in the case of butter made from insufficiently chilled cream this decrease may be very great. This does not necessarily mean, however, that the finished prod- uct is lower in moisture in the case of salted butter than in the case of unsalted butter. The expulsion of moisture by the salt occurs during the first few revolutions of the workers. As the working continues, especially with the churn doors closed, brine is reincorporated and the moisture content again in- creases. Salted butter, at the conclusion of the working process may, therefore, contain as much water as unsalted butter, the salt replacing a corresponding portion of the fat and not of the water, causing salted butter to be lower in butterfat than un- salted butter. This fact is demonstrated in the following table:1 Table 53. — Showing Effect of Amount of Salt on Moisture and Fat Content of Butter When the Butter is Worked With the Churn Gates Closed. Lot No. Ounces of Salt per Lb. Fat Revolu- tions Worked Chemical Composition of Butter in Per Cent Salt Fat Moisture Curd Ash April, 1907 (before storage) worked 12 revolutions 1 none 12 .02 84.58 14.05 .63 .20 ' 2 2A 12 2.20 83.00 14.07 .60 .19 3 WA 12 4.44 81.22 14.00 .t50 .19 4 2K 12 6.66 77.70 14.78 .61 .18 5 W 12 7.17 77.31 14.75 .60 .20 Average 4.10 80.76 14.33 .61 .19 When butter is placed i ncold storage the loss of moisture in salted butter is very much greater than that in unsalted but- ter, as shown in experimental data1 in Table 54. As shown in Table 54, the loss of moisture of but- ter in cold storage is greatest in heavily salted butter, while it is very slight in lightly salted butter. While unsalted but- ter lost no moisture in eight months storage at — 6° F., lightly salted butter lost .42 per cent and heavily salted butter as high as 3.08 per cent. Similar results were obtained in exper- 1 Hunziker, Mills and Spitzer. Moisture Control of Butter, Purdue Bulletin 160, 1912, p. 399. SAI/UNG THE BUTTER 345 iments conducted by Rahn, Brown and Smith.1 This loss of moisture in storage was formerly attributed to evaporation, and such is in fact the case to a limited extent with butter, stored at ordinary temperature. In commercial cold storage, however, moisture does not evaporate to any noticeable extent. Table 54. — Showing Loss of Moisture in Butter in Cold Storage. Per Cent Salt Per Cent Moisture Fresh Stored 8 Months at -6° F. Decrease of Per Cent Salt none 2.20 4.48 6.66 7.17 14.05 14.07 14.00 14.78 14.75 14.20 13.65 13.01 11.70 11.83 '.42 .99 3.08 2.92 If here the loss of moisture were due to evaporation, this de- crease of moisture would necessarily have to be accompanied by a material increase in the per cent of salt. This is not the case, as shown in the results of Hunziker, Mills and Spitzer in table 55. The loss of moisture in butter in storage is apparently due to leakage, caused partly by the precipitation and contrac- tion of the casein, rendering the buttermilk less viscous and giving the butter a more open texture, and partly to the fact that in heavily salted butter the brine is so concentrated that its freezing point is near that of the cold storage temperature. This leaves the moisture in butter in liquid form during a con- siderable part of its storage period and gives it an opportunity to leak out. In the case of unsalted and lightly salted butter the moisture freezes at the usual cold storage temperature, pre- venting further leakage. In butter stored at ordinary temperatures and not far below the freezing point of water, the leakage of moisture in both salted and unsalted butter would be more nearly the same. 1Rahn, Brown and Smith, Keeping Qualities of Butter, Michigan Technical Bulletin 2, 1909. 346 WORKING THE BUTTER Table 55.— Salt Content in Fresh and Stored Butter,1 Lot No. Ounces of Salt Added per Pound of Fat Fresh Butter After 8 Months Cold Storage Per Cent Moisture Per Cent Salt Per Cent Moisture Per Cent Salt 1 2 3 4 5 none 2/3 iy2 V/4 3K 14.05 14.07 14.00 14.78 14.75 .02 2.20 4.44 6.66 7.17 14.20 13.65 13.01 11.70 11.83 .02 2.01 4.48 5.57 7:07 Average per cent salt.. 4.10 3.83 WORKING THE BUTTER Purpose. — The fundamental purpose of working- the butter is to completely dissolve, uniformly distribute and properly in- corporate the salt, to accomplish as complete as possible a fusion between brine and water in butter, and to bring the granules of butter together into a compact mass for convenient handling and packing. Incidentally the working process fur- ther serves to expel buttermilk and to control the moisture content of butter. The working is an important -part of butter manufacture, it is a science which requires knowledge, and it is above all an art that demands experience and judgment on the part of the operator, if uniformly satisfactory results are to be obtained. Butter Workers. — There is a great variety of butter workers on the market, in principle they are conveniently di- vided into two classes, namely those which are independent of the churn, and in the use of which the butter is taken out of the churn, and those which are a part of the churn, known as the combined churns and workers. To the first group belong all the handworkers such as are generally used in farm buttermaking and the mechanical table workers which were formerly used in American creameries and are still used to a considerable extent in European creameries. These independent butter workers consist of a bowl, tray or table on which the butter is placed and where it is worked with ladles, or with a lever, or by one or more revolving cor- 1 Hunziker. Mills and Spitzer, Moisture Control of Butter. Purdue Bulletin 160, 1912. WORKING THE BUTTER 347 rugated rollers. In the case of the large table workers, both the table and rollers revolve. When only small quantities of butter are handled, these workers may serve the purpose fairly well, but at best they are a very crude apparatus, their opera- tion requires much labor, is time consuming, lacks uniformity of results as to distribution of salt and moisture, makes the control of temperature of the butter impossible, renders the protection of the butter from flies in summer and diverse im- purities difficult, and exposes the butter excessively to light. Even for the farm dairy the combined churn and worker is greatly preferable and such workers are now available, adapted for use in dairies with a small make. Pig*. 55. Hand butter worker Courtesy Creamery Package Mfg. Co. For creamery use, the independent worker is practically out of the question and the combined churn and worker is the only really satisfactory equipment. The combined churn and workers are of two types. In one type the butterworkers, con- sisting of one, two or four rollers, according to the make of the churn, are permanently installed in the churn, running lengthwise, either near the periphery of the churn barrel or through the center of the churn. The workers revolve on steel shafts with bearings in each end of the churn, and with the gear attachment at one end on the outside of the churn. To this type of combined churns and workers belong the Disbrow, Dual, Perfection, Victor, Wizard, etc. In the other type of com- bined churns and workers one end of the churn is open and the butter workers are on a separate truck outside of the churn. When ready for working, the truck is moved up to the open end of the churn, the workers are pushed into the churn, and the driving gear located outside of the churn is slipped in place. The Simplex churn is a representative of this type of churn, 348 WORKING THS BUTTER On the interior of the combined churns and workers one or more shelves are fastened to the sides of the churn; as the churn revolves these shelves carry the butter and some of the water up and drop them over the workers. In churns containing one worker only, as is the case with the Perfection churn, the roller works against a shelf, the butter being worked while passing between the roller and shelf. Pig-. 56. One-roll workers perfection fig. 57. Two-roll workers' Disbrow chum churn Courtesy J. G. Cherry Co. Courtesy Davis- Watkins Dairymen's Mfg. Co. In churns containing one or more sets of two rollers each, roller works against roller, the butter being worked while pass- ing between the rollers. To churns of this arrangement belong the Disbrow, Dual, Simplex, Victor (4 rollers) and Wizard. The Dual churn is equipped with an idler, a small, loose roller on each side of the main workers. These idler rollers assist in guiding the butter towards the workers and prevent it from dropping down outside of the workers. In some churns (Dis- brow and Victor) the workers travel with the drum of the churn, while in other churns (Dual, Perfection, Simplex and Wizard) the worker or workers are stationary and revolve only on their own axis. In all churns excepting the Wizard, the churn revolves while the workers are rotating. In the Wizard the churn makes one turn, dropping the butter on the workers, then it auto- matically stops and the workers start rotating. When the but- ter has gone through the workers, the churn again revolves and the operation is repeated. WORKING THE BUTTER 349 In order for the churn workers and shelves to perform their work properly, to work all the butter alike, to distribute the moisture and salt evenly and produce uniformity of color in the butter, they must be correctly set, must be taut and free from excessive slack. The distance between workers and be- tween worker and shelf must be the same over their entire Fig1. 58. Two-roll workers with Fig*. 59. Four-roll workers Victor idlers, Dual churn churn Courtesy Creamery Package Mfg. Co. Courtesy Creamery Package Mfg. Co. length, the workers must be so set that, when in operation, the ridges of one worker meet the grooves of the opposite worker, and there must be sufficient freedom from slack or looseness to insure permanency of this correct position of the workers while in operation. Improperly set, maladjusted, loose and slipping workers cause uneven working and this in turn almost invariably causes mottles. Looseness or slipping of the workers is always due to a faulty mechanical condition of the churn. It is caused either by the rollershaft having worked loose in the end of the worker, or by the rollershaft slipping in the gear wheel due to a worn key, or to an excessively worn condition of the cogs in the gear wheels. It is a part of the buttermaker's duty to see to it that the churn and workers are constantly kept in proper mechanical repair. Overloading the Churn. — The author's observation among creameries has been that it is one of the common tendencies of the buttermaker to overload the churn. Similar experience is related by Professor F. W. Bouska,1 butter expert for the American Association of Creamery Butter Manufacturers. The 1 Eouska, Elgin Dairy Report, 1914, 350 WORKING THE BUTTER amount of butter which any given churn will properly work, is dependent on a variety of factors: Churns in which the butter is brought up on the workers in several installments (Simplex) with each revolution of the churn, can take care of more butter, without overloading the workers, than churns in which the butter is deposited on the workers in one mass. Workers that are deeply corrugated and are placed a considerable distance apart, will work more butter than workers with shallow corrugations and which are set close together. In the case of too great a space between workers, however, it is difficult to work small churnings satis- factorily. High-speed workers will handle more butter than low-speed workers. Too low a speed of the workers makes moisture control difficult and tends toward leaky butter. In the case of hard butter, a slow speed causes excessive expulsion of water. Excessive speed of the workers causes rapid incorpora- tion of moisture and makes expulsion of water more difficult. Wide workers can take care of more butter than narrow workers, in the latter case the butter is prone to fall over the workers and to miss being worked. Soft butter increases, while hard butter decreases, the capacity of the workers. Overloading the churn often causes the butter to be crowded toward the ends of the churn. More butter being loaded on the workers than they are able to work through, causes the butter to pile up ; it presses against the ends of the churn. The uneven surface of the ends, magnified by the projecting bolt heads and the sunk-in spy glasses, makes part of the butter stick to the ends and to be carried around by the revolving drum without going through the workers, all the butter does not get the same amount of working, there is uneveness of moisture, salt and brine distribution, and the butter usually becomes mottled. In order to avoid the objectionable consequences of this con- dition, the buttermaker may stop the churn and turn the but- ter which piled up at the ends toward the center. This prac- tice minimizes the resulting defects, but it is laborious, time- consuming and fails to remove the cause of the trouble. The tendency of the butter to crowd toward the ends of WORKING THE BUTTER 351 the churn is not always due to there being more butter in the churn than its rated capacity under normal conditions can properly take care of. Frequently it is caused by the fact that, when renewing the workers, a larger diameter worker is fur- nished and installed. Since the distance between the centers of the worker shafts remains the same, regardless of size of worker, the installation of the larger diameter workers leaves less space between workers, so that the butter of a churning of normal size cannot all go through the workers and the effect is obviously the same as if the churn with workers of proper size had been overloaded. When replacing old churn rollers by new ones, great care should, therefore, be taken that the new workers are of the proper size. Of late years manufacturers of churns that contain more than one worker, have endeavored to overcome the tendency of the butter to crowd toward the ends, by installing at the top and bottom in the center of the churn, a so-called "center- board." The centerboard is a heavy cypress board, about 24 to 36 inches long, running lengthwise, with one edge lying against the churn drum and the other edge pointing radially toward the center. This board is braced on its sides by heavy wooden braces. The evident purpose of these centerboards is to give the butter more contact and therefore more stability to stay in the center (between churn ends) and thereby offset the adhesion at the ends which otherwise pulls the butter away from the center. The center board also helps to hold the butter over the workers and to prevent it from dropping over the outside of the workers without, being worked. Practical experience shows that the centerboards do effectively help to prevent the crowding of the butter toward the ends. But, if the churn is really overloaded, so that the butter cannot all pass through the workers, a portion of it is bound to escape the workers and if it cannot crowd toward the ends it must inevitably fall off the workers over their whole length. One of the most fundamental causes of the tendency in American creameries to overload the workers, lies in the fact that the listed working capacity of the majority of combined churns and workers on the market and in use is greatly over- 352 WORKING THE BUTTER rated. The working capacity of these churns is far 'below their churning capacity. The reason for this absence of proper pro- portion between churning and working capacity is obvious. Most of these churns were designed some twenty to thirty years ago and the design, from the standpoint of working capacity, is the same now as it was then. But in those early and formative days of the creamery industry the creameries received and churned a much thinner cream than they do now. Twenty or more years ago the cream separated on the farm averaged around 20 to 25 per cent fat. During the last score of years the cream- eries, the dairy schools and the dairy press, all have pointed out to the farmer the advantages of separating a richer cream and urged him relentlessly to produce and ship cream with a high per cent of fat. This campaign for richer cream, together with the abandonment of gravity creaming and the universal adop- tion of the farm cream separator, had their desired effect. Today many creameries receive cream testing as high as 50 per cent fat and the average cream when churned probably contains not less than 33 per cent fat. It is obvious that combined churns and workers, designed for a working capacity of 20 to 25 per cent cream, have their workers overloaded when operated to the limit of their rated churning capacity, with cream that tests 33 per cent fat. The overloading of the workers, whatever its cause may be, is bound to result in incomplete and uneven working, lack of uniformity of salt and moisture, inadequate fusion of brine and water and consequent streakiness and mottles. Manner and Amount of Working. — After the wash water is drained from the churn, the churn is given one revolution to bring the butter on top, in front of the churn doors. A deep trench is then dug in the butter, running the entire length of the churn. The salt is placed into this trench, care being taken that the salt is distributed uniformly in all parts of the trench, otherwise there is prone to be a variation in color in butter from different parts of the churn. After salting, the trench is closed and the worker started. Some butter makers prefer to work the butter a few revolutions (3 to 6) before salting, either in the presence or absence of extraneous water, claiming that WORKING THTC BUTTER 353 they can more readily control the moisture. Each individual butter maker has his own method which he believes to operate most satisfactorily. The amount of draining which the butter receives before salting, the method of salting and the draining incident to the working process, largely regulate the per cent of moisture which the finished product of one and the same churning will contain. The extent of draining and working that will yield the desired result as to per cent of moisture and body of butter, must be governed by type of churn and by the me- chanical character of the butter in the churn. Inasmuch as the mechanical character of the butter must determine how much working any given churning in any given churn requires and can stand, and since the mechanical character of the butter varies with many conditions, (such as locality, season of year, richness, acidity and temperature of cream, size of butter granules, fullness of churn, etc.) it is impossible to prescribe any set method that would prove satisfactory under all conditions. The working should be continued until the butter has a com- pact, tough and waxy body, consistent with the desired moisture content. Butter has been worked enough when it breaks with a ragged edge upon passing a laddie through it quickly. Butter not worked sufficiently usually has a loose body, with the grain not packed together properly. Such butter is often leaky and lacks compactness. Butter overworked shows a tallowy or salvy texture in the case of very firm butter and a greasy texture in the case of very soft butter. See also "Moisture Control." Effect of Working on Body and Color of Butter.-^Properly worked butter* has a tough, waxy body, is free from leakiness, greasiness and tallowiness and has a live, bright color, which is uniform throughout the package. When a plug of such butter is pulled out of the tub and is broken, the break presents an uneven surface similar to that of a piece of iron, showing that the grain is still intact. Working has the effect of whitening the color of the salted butter. This is due to the reduction of the size of the water droplets in butter during progressive working. In unsalted but- ter the water droplets are present in the form of innumerable 354 WORKING THE BUTTER Size of Water Droplets in Unsalted Butter During Working Process Magnified 740 times Fig1. 60. Worked six revolutions, no mottles Fig1. 61. Worked 12 revolutions, no mottles Fig-. 63. Worked 26 revolutions Worked 66 revolutions, no mottles WORKING THE BUTTER 355 Size of Water Droplets in Salted Butter During Working Process Magnified 740 times Tig. 66. Worked six revolutions, mottled Pig". 67. Worked 12 revolutions, mottled worked 18 revolutions, mottled Tig. 69. Worked 26 revolutions, slightly mottled Pig- Worked 34 revolutions, no mottles PifiT. 71. Worked 66 revolutions, no mottles 356 WORKING THS BUTTER and exceedingly small units which give the butter an opaque whitish color. These droplets remain in this condition during the process of working. Working therefore has no noticeable effect on the color of unsalted butter. But not so in the case of salted butter. . When butter is salted many of these small water droplets run together, forming fewer but larger units or drops. This causes the opaque whitish appearance to vanish and to be replaced by a clear, more trans- lucent and more deeply yellow color, approaching more nearly the natural color of pure butterfat. As the working process proceeds these large droplets are gradually divided again into smaller droplets and as this division and increase of number of small water droplets progresses, the color of the butter begins to lose some of its clear, translucent, bright yellowness. By continu- ing the working process to the point where the water droplets are reduced to their original very small size which they presented before salting, the color of the butter can be returned to the opaque whiteness of the unsalted butter. This can only be done, however, by greatly overworking the butter. The above phenomenon also explains why different portions of butter from one and the same churning show different shades of yellow, when all the butter in the churn does not receive an equal amount of working, as may be the case when the workers slip or are overloaded. Insufficiently worked butter has a loose, open and often a leaky body. A plug of such butter drawn from the tub or cube usually shows lack of compactness and sometimes marked crumbliness. In the case of salted butter, such butter is often gritty, due to the presence of undissolved salt and it usually is streaked or mottled in color, due to the incomplete fusion of brine and water and the consequent uneven size and distribution of the water and brine droplets. While still in the churn, such butter generally has a loose body, being profusely perforated with water pockets which are plainly visible when the butter is cut with the ladle. Unsalted butter, while it may be crumbly and may lack the plasticity of properly worked butter, is compact and free from excessive leakiness, even when very insufficiently worked, and such butter does not become streaky nor mottled WORKING THE BUTTER 357 in color, because the water droplets which it contains are very minute and there is a permanent absence of large droplets. Overworked butter usually has a poor body and defective grain, severely criticized on the market. Overworking injures the grain of the butter. If butter is overworked while soft, the body is prone to be greasy ; if overworked when hard it tends to be salvy in texture. A plug of such butter pulled from the tub breaks with a smooth surface, similar as if it were cut with a knife and showing that the grain has lost its identity. Over- worked butter also has a dull, lifeless color, similar to oleomar- garine and which is not attractive to the buyer. Such butter seldom stands up \vell on the market under unfavorable tem- perature conditions and its flavor and keeping quality may be impaired. Frequently butter of this description contains exces- sive moisture. Butter with a firm body will stand much more working without injury to its body than butter that is soft. Effect of Working on Moisture Control of Butter under diverse Conditions. — The working is an important part of the process of buttermaking as a means to regulate the moisture content of butter. In fact, the expulsion or retainance of mois- ture largely depends on the method employed for working. The smaller the granules when the churn is stopped, the larger the amount of moisture they hold. Churning butter to large granules or lumps tends to expel moisture, unless such overchurning is due to very soft butter, in which case the butter may hold abnormally much moisture. If the churning process is stopped at the proper time, that is when the butter has gath- ered in the form of granules of the size of small corn kernels, butter contains more than sixteen per cent moisture immedi- ately after the buttermilk has been drawn off, and immediately after washing it still contains an excess of moisture. The sub- sequent salting and working removes this excess moisture. If the butter granules are round, smooth and firm as is usually the case in fall, winter and early spring, and especially in the case of thin cream, the excess of moisture escapes very rapidly and there is a strong tendency toward too great escape of moisture, a low moisture in the finished butter and a correspondingly low overrun. The excessive expulsion of moisture can be minimized by 358 WORKING THE; BUTTER draining less thoroughly and working with the churn gates closed, and it can be entirely prevented by working the butter in the presence of a small amount of water. The water so used should be of practically the same temperature as the butter. Table 56. — Showing Amount of Moisture in Butter After Draw- ing-off Buttermilk, After Washing and in Finished Butter When Butter Granules Are of the Size of Whe-at Kernels.1 No. Size of Per Cent Moisture of Churning Granules Inches After Drawing Buttermilk After Drawing Washwater Finished Butter 1 A 23.64 19.87 15.48 2 A 30.66 26.66 13.12 3 A 21.77 19.20 14.45 4 A 25.00 19.66 14.59 5 A 19.83 19.07 13.84 6 A 21.28 19.57 13.86 7 A 24.04 18.58 14.15 8 A 22.55 18.63 14.78 9 A 22.33 17.65 15.00 10 A 21.70 16.94 15.80 Averages . . . | 23.28 19.58 14.51 When the butter granules are very hard, so that consider- able working may be necessary in order to bring the moisture content up to the maximum allowed by law (less than sixteen per cent), there is always more or less danger of injury to the grain of butter. If the butter granules are soft, flaky, irregular and have a ragged surface, as is usually the case in late spring and early summer, when most of the cows have freshened and have access to abundance of succulent pasture, which conditions yield fat globules of large average size, and butterfat with a relatively low melting point, the excess moisture does not escape so rea- dily, and there is danger of excessive moisture in the finished butter. This is due to the fact that cream with predominatingly large fat globules and butterfat with a low melting point, pro- duce a soft butter. This soft butter is more miscible with water 1 Hunziker, Mills and Spitzer, Moisture Control of Butter. Purdue Bulletin 160, 1912. WORKING TH£ BUTTER 359 than hard butter and when the churn is stopped, the moisture is incorporated in the butter granules in the form of very fine drops which are expelled with difficulty. Whenever the butter maker has difficulty to keep the moisture down, the butter should be drained very thoroughly before working and should be worked with the churn doors ajar. It is then advisable to work the but- ter four to five revolutions before the salt is added and to drain again. During the working the churn should be stopped after every two to three revolutions, allowing it to swing freely, with the churn doors ajar and down, permitting the free moisture to escape readily. In cases of extreme difficulty of keeping the moisture within the limits of the law, it may be necessary to delay the working after the salt has been added, for a consider- able time. This gives the salt an opportunity to assist in the expulsion of moisture. Owing to its great affinity for water it draws the minute drops of water out of the butter and gathers them in larger drops which, upon subsequent working, are more easily expelled. It occasionally happens that, owing to the extreme natural softness of the butterfat, or to faulty handling of the cream before churning, or to too high a churning temperature, no amount of working will reduce the moisture content to or below the maximum legal limit. In such butter the moisture has formed so intimate a mixture with the fat, and moisture incor- poration is so complete, that additional working, even to the extent of injuring the grain of the butter, fails to expel water. The only practical way to bring the moisture content of such butter within the limits of the law, is to set the butter in the cold room and allow it to harden over night. The next day it is then cut up into small pieces and worked again with the churn doors ajar and in a similar manner as above described. Unless its moisture content is very greatly in excess and the incor- porated moisture is present in the form of abnormally fine drops, this second working will remove sufficient moisture to meet the requirements of the law. If it still contains over sixteen per cent moisture, more moisture may be expelled by putting the butter back into the cold room and working it again the next day. The hardening of the butter in the cold changes its mechanical make- up and makes it more granular. Some of the minute water par- 360 WORKING THE; BUTTER tides gather into large drops which can be expelled when the butter is worked again. It is obvious that this repeated work- ing does not improve the body of the butter and should be avoided as much as possible. The buttermaker should bear in mind that when the but- ter has been washed, it contains excessive moisture, part of which must be expelled, and that moisture control is not so much a matter of incorporating additional moisture into but- ter, as it is a matter of properly regulating the expulsion of moisture. The control of the expulsion of moisture can be greatly facilitated by proper handling of the cream as to churn- ing temperature, according to the character of the butterfat and this in turn is a problem which requires constant observation and intelligent adjustment of the process in accordance with pre- vailing conditions. See also "Moisture Control." Effect of Working on the Flavor and Keeping Quality of Butter. — Generally speaking, the less the butter is worked and the more nearly the grain of the butter is preserved,' the better will be the flavor and keeping quality of the finished product. There is an unmistakable tendency in American creameries to work their butter too much and thereby to impair its body, and possibly its flavor and keeping quality. This tendency is chiefly the result of one or both of the following two practices : In order to hasten the process of manufacture the butter is worked immediately after the salt has been added. The salt is given no time to dissolve before working. This requires con- siderable working, especially when the usually large amount of salt is incorporated, in order to insure complete solution of the salt and to avoid grittiness and in order to distribute the salt evenly and to fuse the water and brine completely so as to avoid waviness and mottles. For this reason some of the very badly mottled butter has an exceptionally good flavor. This is not due to the presence of the mottles, but it is the result of the same condition which tends to bring about the mottles, usually under- working, or the absence of overworking. In some European creameries where a special effort is made to produce quality, the butter is not worked for several hours after the salt has been added. The salt thus has an opportunity to largely go in solution WORKING THE: BUTTER 361 before working and but little working is needed to complete the solution and distribution of the salt. The same reason, why under- worked butter is of better quality than much-worked butter, also accounts in part for the fact that unsalted butter is often of better quality and keeps better than salted butter. Such butter does not require working in order to insure solution of the salt and to avoid mottles. It therefore is often not worked as much as salted butter and has a better body and better grain. The second reason for the tendency of overworking butter is the common practice of trying to incorporate the maximum amount of moisture which the law permits. In late spring and early summer, when the butter is relatively soft and naturally takes up water readily, there usually is no need of excessive working in order to incorporate moisture, and if the buttermaker understands his business, he need not overwork the butter to the extent of injuring its body or flavor. But not so when the butter comes firm and tends to be low in moisture as is the case in fall, winter and early spring. Under these conditions the butter often requires a comparatively large amount of working in order to contain the maximum amount of moisture allowed by law. This is true especially in the states where much cot- tonseed meal and similar fodder producing hard and crumbly but- ter, are fed. Butter made from such cream, when worked in the usual way, and just enough to insure proper compactness; usually does not contain much over 13.5 per cent moisture and the additional moisture can only be incorporated by additional working and this is often done at the expense of body, flavor and keeping quality. From the point of view of the quality of American butter this additional working or overworking is objectionable and it is a debatable question if, in the long run, the loss in price and prestige due to sacrifice in quality, is not greater than the increased returns due to larger overrun. If in winter, when butter naturally conies in the form of smooth, round and firm granules, the creamery insists on incorporating the maximum amount of moisture permitted by law, it would seem preferable to churn at a sufficiently higher temperature to make the butter come somewhat less firm, thereby increasing its ability to naturally hold moisture and making unnecessary excessive working. In this case great care should be exercised 362 WORKING THE BUTTER to chill the cream sufficiently long so as to guard against a slushy and leaky body of the butter. The exact channels through which overworking of butter deteriorates its flavor and tends to cause such off-flavors as oily, metallic and fishy flavors, are not as yet well understood. Rogers1 shows experimentally that overworking increases the amount of air present in butter and that the presence of air, in combination with other influences, enhances oxidation of the non-fatty constituents of butter. He further states that the development of a fishy flavor is hastened and made more cer- tain by overworking, which increases the air and the oxidizing surface and that fishy flavor may be produced with reasonable certainty by overworking the butter made from sour cream. Rogers' conclusions on this point have not been fully borne out by the work of Hunziker. While overworking certainly does not improve the quality of butter, it fails to produce the distinct defects indicated by Rogers with any degree of regu- larity. Nor does it necessarily increase the air content of but- ter. The incorporation of air in butter begins as soon as the cream is subjected to agitation in the churn and up to a certain 'point it increases, greatly retarding the completion of the churning process. In fact the amount of air incorporated in the interior and on the surface of the still microscopic butter granules is so great, that it is difficult to make satisfactory micro- scopic examinations of these granules. After the granules have reached a sufficient size to "break" the fat-in-skimmilk emulsion and to establish a buttermilk-in-fat emulsion which is butter, much of this air is released and the completion of the churn- ing process is facilitated. And from this point on, any further churning and subsequent working appears to effect an expulsion of a portion of the air locked up in the butter, rather than an incorporation of additional air. There is a vast difference between' the overworking of but- ter that results from manipulating it with a spatula in small amounts as described by Rogers, and by working it in the com- bined churn and worker. While it is quite conceivable how, by special effort, air may be beaten into soft butter with a spatula, it is much less obvious that the squeezing which the butter 1 Rogers, Fishy Flavor in Butter, U. S. Dept Agr., B.A.I. Circular 146, 1909. WORKING THE BUTTER 363 receives in the commercial combined churn and worker incor- porates air and the probability of actual air expulsion in this case is by no means remote. However, it is unquestionably a fact, that any air perma- nently present in the butter, becomes very finely divided and emulsified by overworking and in this form a much larger area of the butter becomes exposed to this air, so that, even without the actual incorporation of additional air, the injurious effect of the air present is greatly magnified. The fact that overworking gives the butter a whiter color is not necessarily due to the incorporation of additional air as Rogers concluded, but it is invariably caused by the reduction of the size of the water droplets as shown by Hunziker and Hosman. Unsalted butter is always whitef than salted butter, both, before working and during any part of the working proc- ess. Microscopic examinations of butter during all stages of the working process, by Hunziker and Hosman, conclusively show, that in unsalted butter the water droplets are exceedingly minute while in salted butter they are relatively large, espe- cially during the early stages of the working process. And, again, the whitening effect due to working takes place even when the butter is submerged in water during the working process, eliminating any possibility of incorporation of additional air. It is also not improbable, though not experimentally proven, that the destruction of the grain of the butter, as is the case in overworking, tends to lessen the resistance of the fat to such oxidizing agencies as air, metallic salts, etc. and therefore hastens its deterioration. When the butter has been worked enough, the workers are stopped and the churn is given another revolution or two in order to deposit the butter on top of the workers from where it can be easily removed and transferred to the tubs or cubes, or other receptacles. Before removing the butter from the churn it should be accurately tested for moisture content, so that if the moisture is excessive, or deficient, it may be corrected by further working. For directions on controlling moisture see also chapter on Com- position of Butter — Moisture Control — Chapter XVIII. , and for directions on moisture tests see Chapter XXII. 364 PACKING BUTTER CHAPTER XII. PACKING BUTTER. Variety of Packages. — Butter is packed and placed upon the market in a great variety of receptacles and forms, varying wide- ly in shape, style and material, such as tubs, boxes, cubes, fir- kins, tin cans, crocks, pails, prints, rolls and individual molds, and varying in weight from one-fourth pound bars up to 110 pound firkins. The standard Danish firkin weighs 50 kilograms, or 110.23 pounds net. The great bulk of the American butter that is put up for the wholesale produce trade in the large mar- kets is packed in tubs, boxes and cubes, while the local trade and retail stores prefer much of their butter in the finished package, the print. Export butter is put up in tubs and cubes, and butter intended for the tropics and much of the butter furnished the United States Navy, is packed in hermetically sealed tin cans. Farm butter is packed in crocks, small fibre boxes, small tubs and pails, rolls, special molds and prints. In many foreign countries the firkin is the predominating package, though much foreign butter is also packed in boxes and prints. Tubs. — Butter tubs are usually constructed of spruce or white ash. They range in size from ten pounds to 63 pounds net. While no particular size has been adopted officially as the standard size tub, the 60 to 63 pound tub is by far the most popular and is used for the great bulk of American tub butter. The war situation threatened a shortage of white ash and especially of spruce. For a time the creameries had difficulty in locating and contracting for a sufficient supply of tubs and prices soared to an unprecedented level. A campaign was start- ed to invite and urge the creamerymen to break away from the butter tub and use boxes or cubes instead. The effort failed and the tub prevailed in spite of all handicaps. The reason for this persistence and tenacity with which creameries stick to the tub is not limited by mere custom and usage. There is no question that, all things considered, the 60 to 63 pound tub is the most satisfactory form of package in which to handle butter in bulk. The mechanical handling at the creamery, in transit, at the market end and in cold storage is by far easier and more prac- PACKING BUTTER 365 tical than any other package of butter of equal capacity. With the possible exception of the firkin, which is not used in this country, and of the tin can which is too expensive a package for domestic use, the butter tub withstands better the abuse and rough handling it is necessarily subjected to in its journey from the creamery to the market, and arrives at its destination in better condition than other butter receptacles. Unlike cubes and boxes it has no nailed sides, ends, bottoms and tops to tear loose, the butter in it does not become soiled, because the tub is tight and dust-proof, which is often not the case with the boxes used for bulk butter. The tub strips easily and quickly, the package does not have to be destroyed in order to get the butter out. Its disadvan- tages are that it does not pack quite as closely as square boxes, requiring somewhat more space in transit and in storage, and that tubbed butter does not cut as satisfactorily for putting up prints as does cube butter. "Smaller size tubs are used upon special request, to fill spe- cial orders and for special occasions, such as for scoring contest butter, etc. Butter tubs are lined with parchment liners and circles which protect the butter from woody odor, impurities, and contamination with mold and prevent it from sticking to the wood, so that the butter slips out of the inverted tub readily when "stripped." Butter tubs should be constructed of the best quality of sound wood, and they should be stored in a dry, clean place in the creamery. They should be well put together, tight, and free from cracked staves. Tubs made from lumber that was felled while the sap was still running, or that has been lying- in stagnant ponds, tend to give rise to woody odor and molds in butter. Their wood is prone to give butter an objectionable woody flavor. Often it is partly decayed and porous, in which condition it may harbor mold spores which contaminate the butter. Exposure of the tubs to dampness and to unclean sur- roundings in the creamery is an additional source of moldy but- ter. When stored in a damp room the tubs frequently become spotted inside and out with mold growth. The liners also may become the source of moldy butter, unless made of a good 366 PACKING BUTTER quality of parchment, kept in a clean, dry place and properly treated before use. Preparation of Tubs and Liners. — All butter tubs should be properly treated before being packed, in order to remove the woody odor which is prone to be absorbed by the butter, to free them from mold spores with which they are always more or less contaminated, to make them airtight to hinder the growth of molds after packing, and to prevent excessive loss of weight due to leakage of brine. Moldy butter in the great majority of cases is the direct result of lack of attention to the proper treatment of tubs and liners. Since salt has properties antagonistic to the growth of molds, the soaking of the tubs in a saturated solution of hot salt brine is a very common and fairly effective method of treatment. This is best done by immersing the tubs in a long vat containing the hot brine. The tubs should be nested so as to retain their shape, otherwise they are prone to warp out of shape. The tubs should be set to soak on the day before they are needed. If they are not clean or show signs of mold spots, they should be thoroughly scrubbed with a brush and hot water containing some alkali, before soaking. Steaming for 5 to 10 minutes is an additional safeguard against mold. The addition to the water or brine in which the tubs are soaked, of formalde- hyde, sodium hypochlorite, boric acid and other disinfectants has also been recommended to guard against mold. Formaldehyde lends the butter an objectionable flavor and odor, if used in other than exceedingly dilute solutions. A safe proportion that still is antagonistic to mold growth is a dilu- tion of 1 part of formaldehyde in 400 parts of water, or about J ounce formaldehyde in one gallon of water. Hypochlorite of soda also should be used with caution, be- cause of its tendency to bleach butter. It may be used at the rate of two tablespoons hypochlorite in four gallons of water. Boric acid has no known injurious effect on butter. It is best used in the form of a .5 per cent solution or about 2/3 ounce in one gallon of water. It should be clearly understood that all these disinfectants and antiseptics are injurious to health when consumed with PACKING BUTTER 367 food, and their presence in butter is in violation of the Federal Pure Food Act of 1906. Their use for treatment of tubs and liners may be justifiable as a means to stamp out an epidemic of mold in butter, but their continued use cannot be recommended and in any event the tubs after treatment should be rinsed with clean water or distilled water before packing. Within the past decade the practice of brine-soaking the tubs has been superseded in a great many creameries by the more efficient treatment of paraffining them. The tubs should be paraffined whenever facilities permit. Proper paraffining obvi- ates the temptation of using antiseptics as far as the tub as a source of mold in butter is concerned. When butter is packed in paraffined tubs, it is unnecessary to soak the tubs in water or brine, in fact it is preferable not to, because the unsoaked tubs present a much more attractive ap- pearance. The old practice of soaking butter tubs in water prior to packing had for its purpose to load the wood with suf- ficient wajter to minimize the absorption by the tub of moisture contained in the butter, which caused a considerable shrink- age in net weight. A properly paraffined tub is impervious to water and therefore is incapable of taking up moisture from the butter. If the tubs are not soaked in water the creamery should always put the tare on the tub. The unsoaked tub weighs from 1 to 2 pounds less than the soaked tub. Without determination of the tare weight, this difference will be lost to the creamery. Soaking in water or brine before paraffining is desirable, however, in the case of tubs the staves and bottoms of which have shrunk to the point where a tight tub can not be secured and in order to hold the tub together. Before paraffining, the tubs should be steamed out thorough- ly until they are hot and dry. This opens the pores and permits the hot paraffine to penetrate. If they are paraffined while wet the paraffine will not penetrate, it merely sticks to the surface and is prone to peel off. If they are cold the paraffine cools before it has an opportunity to fill the pores, it fails to spread, in a thin, smooth and uniform layer and tends to crack. The paraffine should be applied in such a way that it will coat the inside of the tub in the form of a thin film, filling the 368 PACKING BUTTER pores and cracks. The paraffine may be applied with a brush or by pouring a small amount into the tub and rotating the tub until the entire surface is covered, or it may be sprayed into the tub under pressure. The brush method is somewhat crude and tends to produce an uneven coating owing to rapid cooling of the paraffine. In order to secure satisfactory results and avoid a rough and uneven coating of paraffine, the paraffine must be heated to the proper temperature. Rogers1 found that at a temperature of 250 to 260 degrees F. the paraffine can be applied most satis- factorily. The paraffine may be heated over an oil stove or gas burner, but a more convenient arrangement, devised by Rogers, consists of a large pail or small tank equipped with a steam coil connected with the steam line of the creamery, and a drip is provided extending through the bottom of the tank and permitting the condensed steam in the coil to escape. A small amount of the hot paraffine is dipped from the tank into the tub, the tub is rotated so that the paraffine covers its entire inside surface. Then the tub is inverted on a galvanized iron drip tray in order to pour out, and reclaim any excess paraffine in the tub. Such an outfit can be constructed at small cost and is very serviceable, especially in small creameries. There are now on the market also patented paraffiners which both steam and paraffine the tub. The paraffine is heated by a steam heated jacket. The tub is inverted over the paraffin- er and steamed and sprayed with paraffine under pressure. These machines operate very fast, coating the tub with a smooth layer of uniform thickness and economizing the paraffine. These paraffiners are rapidly replacing the dipper and brush method. Aside from protecting butter against mold contamination and mold growth the paraffining of tubs is advisable in order to minimize loss in weight due to leakage of moisture and to give the tub a neater appearance. Rogers1 found the following loss of moisture in 12 paraffined and 12 unparaffined tubs of butter on the eighth day after packing: 1 Rogers, Prevention of Molds in Butter Tubs, U. S. Dept. Agr. B. A. I. Bull. 89. 1906. PACKING BUTTER 369 Paraffined tubs Pounds of butter 757y4 756 Unparaffined tubs Pounds of butter 759 When packed 8 days later Shrinkage When paraffine of the proper temperature is used, from two to three ounces are required per tub. The labor cost of paraffin- ing is no greater than that of preparing a saturated brine solution. Tig. 72. Tub Parafflner Courtesy Creamery Package Mfg. Co. It is advisable to paraffine tubs and to clean covers as shortly before they are needed as the routine of the factory permits, and to stack them, inverted, in a clean place, so as to prevent unnecessary soiling and recontamination. Paraffined tubs should always be lined with parchment liners and circles, the same as the tubs prepared in the ordinary way. Unlined paraffined tubs strip with difficulty, the butter sticks to the comparatively rough surface of the paraffine. This is a serious objection at the market end. Preparation of Parchment Liners and Circles. — The best quality of parchment liners only should be purchased. Inferior parchment invites excessive leakage of moisture and may injure the flavor of the butter. In the summer season, when the butter is often exposed to temperature conditions that cause it to-be soft and therefore to yield readily to the knocks to which the tub is subjected in transit, there is always a tendency for 370 PACKING BUTTER moisture to be pounded out. Evaporation at the higher tem- perature is also most rapid. It is advisable, therefore, to use extra heavy liners in summer. The liners should be of ample size so they will abundantly lap on the side, fold under at the bottom and lap over at the top. The circles should be large enough to cover the entire bottom of the tub. There is a tendency on the part of supply houses to furnish liners and circles that are of inadequate dimen- sions, unless the desired dimensions are specifically demanded. The stock of parchment liners and circles should be kept in a clean, dry room, protected against dust, dirt and dampness. They should not be stored in the creamery cold room which is almost always damp. Immediately before use they should be thoroughly soaked in hot saturated brine. The brine should be of such strength that a deposit of undissolved salt forms in the receptacle, it should be supersaturated, and its temperature should be raised to the boiling point. The circles and liners should be soaked in this hot brine for at least 5 minutes. Such treatment is a three-fold protection against mold development. The heat destroys mold spores that may adhere to the parchment, the soaking frees the parchment from much of .its glucose content and glucose is an ideal food for bacteria, and the brine adhering to the parch- ment helps to inhibit the growth of mold germs that may be in or on the butter. This treatment should be given parchment liners and cir- cles used for packing unsalted butter as well as salted butter. The unsalted butter, because of the readiness with which it be- comes moldy, needs these precautions more urgently than the salted butter. The fact that the brine-treated liner conveys some salt to the surface of the butter needs no serious consider- ation. The very small amount of salt thus imparted to butter is not noticeable and does not remove such butter from the class of unsalted butter. The lining of the tubs should be done with care. The bot- tom circle should be so placed as to cover the entire bottom of the tub, and the line should be strung around the periphery of the tub uniformly and neatly, and iri such a manner as to cause one inch of the liner to project above the top of the tub. PACKING BUTTER 371 The tub covers should also receive some attention. They often contain cinders, soot and dust, which they usually gather in transit to the creamery and in the creamery stock room. These impurities, when the cover is fastened to the packed tub, drop on the salt which is generally sprinkled on the top circle and they soil both the salt and the circle, give the pack- age, when opened by the prospective buyer, an unsightly ap- pearance and convey an unfavorable impression. If the tub happens to be subjected to very rough handling, they even may work into the butter. It is important, therefore, that the tub covers be thoroughly cleaned before they are fastened to the tub. This can readily be done by turning them bottomside up and turning the water hose on them until they are freed from all foreign matter. Boxes and Cubes. — Some of the Eastern markets require the butter to be packed in square wooden boxes, holding about 50 pounds of butter. These boxes should be constructed of good sound wood, with bottoms, sides and tops at least one-half inch, and ends at least % inch thick, properly assembled and nailed with 4 penny cement-coated wire nails. They should be paraffined and otherwise treated in the same manner as the tubs and carefully lined with parchment paper. In the Pacific Coast markets, both for domestic and for export trade, the cube is the standard butter package. The San Francisco Wholesale Dairy Produce Exchange issued offi- cial regulations concerning the size, shape and preparation of the cube, which went in force Feb. 1, 1916, as follows : "In order to grade as 'extras' butter must be packed in cubes as follows : The materials of the sides, tops and bottoms shall be one-half inch in thickness and the ends % inch in thickness. Lumber to be surfaced on both sides, and corners of cubes nosed and rounded. Inside dimensions shall be 12%xl2j4xl3^2 inches and the cubes shall be packed to a uniform weight of 69 pounds net at churn and marked 68 pounds on each end of each cube, as the shrinkage from creamery to market is about one pound. The cubes shall be paraffined on the inside and lined with parchment paper." 372 PACKING BUTTER Firkins. — Firkins are not used in this country for packing butter except on very rare occasions. They are a popular but- ter package in European countries especially for export and storage butter (Datierbutter). Firkins (Drittel) hold 50 kilo- grams or 110.23 pounds of butter. These barrels are 55 cm. (22 inches) in height and their diameter in the center and at the ends is 34 and 41 cm. (13.6 and 16.4 inches) respectively. Before packing they are steamed, soaked in cold water, brine or sal soda solution, for one day, then rinsed out with hot water and again with cold water after which salt is rubbed into the staves on the inside. The bottom is then covered with a thin layer of salt, and the firkin is lined with parchment. After packing, the top of the butter is beveled off toward the sides and covered with a layer of salt. The object of having the surface of the butter highest in the center and tapering toward the sides is to permit the brine to run into the space between the butter and the side of the barrel when the butter, upon standing, has receded from the sides of the barrel ; this shuts out the air and assists in protecting the butter against mold, etc. Tin Cans. — Butter intended for the tropics and South Amer- ica and some butter supplied the U. S. Government is packed in hermetically sealed tin cans. Exporting houses buying their butter from American creameries and supplying the tropics buy the butter in tubs and repack it into tin cans, which are subse- quently hermetically sealed. These cans hold from J4 to 5 kilograms, the metric system being used as the basis of weights. They are packed into cases and in order to prevent shaking and damage to the cans, the interstices between the cans and the sides of the case are filled in with some cheap, light packing ma- terial such as rice hulls, shavings, excelsior, corrugated paper, etc. The object of the use of a non-absorptive and hermetically sealed package is to prevent leakage of water and oil and to improve the keeping quality of the butter, exposed to unfavor- able temperature conditions, by excluding the air. Experiments conducted by Rogers1 show that sterile butter so packed and 1 Rogers, "Canned Butter." U. S. Dept. of Agriculture, B. A. I. Bulletin 57, 1904. PACKING BUTTER 373 held for one hundred days at 23° C. showed no increase in acid- ity. From these results Rogers concludes that the causal rela- tion of physical agents such as heat and moisture to changes of the butter is excluded. In the case of non-sterile canned butter examination showed a marked change in the texture and flavor. The changes were gradual; when about 25 days old, a distinct off-flavor was noticed which increased in intensity, un- til, at two hundred and ninety-seven days in one case and at two hundred and fifty-one days in another, there was a disagree- able, fishy flavor and a strong penetrating odor. There was also a correspondingly slow increase in the acidity. Micro-organ- isms which consisted almost entirely of lactic acid bacteria, a comparatively small number of Torula yeasts and a few lique- fying bacteria decreased rapidly until there were present only a few spore-forming liquefying, bacteria. Owing to this marked decrease in germ life, Rogers attributes the increase in acidity and the off-flavor to the probable action of fat-splitting enzymes. Weigmann1 in a very extensive investigation studied the keeping quality of butter made by different processes and sealed in tin cans, samples of which were placed on board of German men-of-war and which were returned and examined at intervals of six, twelve and eighteen months. These results demonstrated that there is a great variation in the keeping quality of different lots of butter and that while prolonged storage under unfavor- able temperature conditions tended to intensify the deterioration of the butter, a few of the samples packed in tin cans returned in excellent condition even after eighteen months' travel. While Weigmann's results were not conclusive and while his funda- mental aim was to determine that process of manufacture which would produce the best keeping butter, the data secured demon- strated that under certain ideal conditions of manufacture, butter packed in tin cans has remarkable keeping quality. In the canning of butter the tin plate used should be coated with shellac or enamel to protect the can against the action of the acids and the brine of the butter and to guard the butter against rapid deterioration as the result of such action. While tin itself is an inert metal that does not yield to the action of 1 Weigmann, "Versuche zur Bereitung von Dauerbutter" Milchwirtschaft- liches Zentralblatt, Vol. 44. Nos. 23 and 24, 1915. 374 PACKING BUTTER acids and brine, iron is quickly corroded by these agents. The tin plate of the butter cans is sheet iron with a thin coating of tin. This tin coating is not always entirely impervious and sooner or later the acids and the brine will attack the iron un- derneath, unless the tin plate is heavily shellaced. Iron salts thus formed are disastrous to the quality of the butter. Of late years, and particularly as the result of the shortage of tin plate, cans constructed of aluminum are also being used for pack- ing butter. Packing tubs, boxes, cubes and tins. — After the packages have been properly treated and lined, they are ready for the butter. They are now conveniently arranged in a row in front of the churn and the butter is transferred into them from the churn. Since the distribution of salt and moisture in the butter is seldom entirely uniform in all parts of the churn, butter from the same part of the churn should be distributed into the different tubs, boxes or cubes, so that all packages receive1 butter from all parts of the churn. The butter should not be transferred with the naked hand. The skin of the perspiring operator should not touch the butter, he should either wear cotton gloves or rubber gloves, or use ladles, or both. Before using the ladles and packers they should be thoroughly washed and steamed in order to prevent unnecessary contamination of the butter with germ life, then they should be soaked in cold water to prevent the butter from sticking to them. The gloves should be clean and sweet-smelling, and when taken off they should be placed in brine. It is important that the butter in the tub be packed very solidly, avoiding air pockets, especially between the butter and the sides of the -package, which admit air and favor mold growth. Pockets in the body of the butter are undesirable also because these pockets collect the brine, cause uneven distribu- tion of the moisture, uneven color, and give the butter a leaky appearance. The package should be filled completely full and finished neatly on the surface. This is best done by filling the tub or box above the edge of the wood, tamping thoroughly with the packer and cutting off the surplus with a taut wire or a sharp piece of wood — wood is preferable. The border of the PACKING BUTTSR 375 liner, which should project ajbout one inch, is then neatly folded over toward the center and the butter is covered with the top circle, preferably of cloth, on which is strewn a handful of clean, dry salt. The tub cover is then fastened down with 3 to 5 tin fasteners, or in case of the box the lid is nailed down firmly. The package is weighed and marked with the net, tare and gross weight and the churning number, and is placed in the refrigera- tor until ready for shipment. The cold room should be clean, dry, and cold enough to chill and harden the butter before ship- ping. When ready to ship, the address of the consignee is sten- cilled or plainly written on the tub cover. The numbering of each churning and the placing of the churning number on the tub, is an important precautionary meas- ure. It tells the receiver which tubs belong to the same churn- ing and therefore contain the same kind of butter. The receiver is able thereby to supply his customers with butter of uniform quality, salt and color. In case the butter develops defects the receiver, when reporting to the creamery, is in a position to re- fer to the respective churning number as marked on the tub and the creamery then is able to investigate the conditions under which that particular churning was made. If the buttermaker keeps a full and systematic churn record, as he should, the num- bering of the churnings gives him an opportunity to prevent recurrence of the reported defect. Butter Prints. — Formerly butter was retailed direct in bulk packages, such as tubs, boxes and cubes. At the present time the trend is toward individual or consumer's packages in the form of one, two and five pound rolls, and one-quarter, one-half, one, two and five pound prints. Much of the butter that goes to the wholesale trade in bulk packages, is printed by the wholesale receiver, commission man, jobber, or butter cutter before it reaches the retail store. In most of these cases the wholesale dealer packs the butter under his own brand, for which he estab- lishes a special trade. In other cases the retailer uses his own special brand and furnishes the wrappers and cartons to the creamery. Some wholesalers handle prints put up by the cream- ery under the creamery's brand, in which case they pay about one cent more per pound than in bulk. Most of the butter which 376 PACKING BUTTER the creamery sells direct to the retail store is sold in prints. During the fall and winter, when the output is at ebbtide, many creameries print all their butter. The individual or consumer's packages are two pound prints or rolls, one pound prints, one-half pound prints and bars and one-quarter pound prints. The predominating consumer's pack- Fig-. 74. Friday Box Fig-. 73. Friday Printer Courtesy J. G. Cherry Co. age is the one pound print of the following standard dimensions : 2y2 x 2^ x 4^i inches, wrapped in parchment, or wax paper, or both and slipped into a carton. Some creameries wrap an additional paper around the carton and seal it at both ends. Considerable quantities of butter are sold in one-half pound and one-quarter pound prints wrapped in the same manner as the one pound prints and varying in shape from a flat slab to a so-called hotel bar. In New England, efforts are made to establish a one pound print having twice the width, half the depth and the same length as the standard one pound print. Within the last few years the practice of putting the one pound prints up in the form of four one-quarter pound bars, PACKING BUTTER 377 each wrapped separately in parchment paper, has found much favor as a means to accommodate the consumer and increase sales. In accordance with the Federal Pure Food laws all individual or consumer's packages must be marked in plain and legible letters with the net weight of the contents. Packages weighing one pound or over must have the net weight indicated in terms of pounds, packages weighing less than one pound must have their net weight indicated in terms of ounces. A law passed by the New York State Legislature in 1912 provides for the following tolerances in the weight of print butter : "The maximum variation allowed on a pound print to be three-eighths of an ounce on an individual print, provided that the average error of twelve prints, taken at random, shall not be over one-fourth of an ounce per pound. The maximum varia- tion allowed on two-pound prints to be one-half ounce, provided that the shortage on twelve prints, taken at random, be not more than three-eighths of an ounce for two pounds. "Prints that are not of one pound or two pounds must be marked in letters at least three-eighths of an inch in height, giving the correct weight in terms of ounces, or pounds and ounces." Methods of Printing. — The printing of butter is done in various ways. Some creameries transfer their butter from the churn to a table from which it is printed while soft, by the use of one-pound hand molds, or by the use of a mold sunk into the table and worked with a hand lever. In some European* cream- eries the soft butter, coming from the churn or worker, is placed on an automatic, revolving printing table. This table is equip- ped with several molds. The butter is piled into these molds, which pass under a mechanical plunger that tamps it into the mold, then under a stationary knife that removes the surplus butter, after which the finished print is released. Most of the American creameries pack the butter from the churn into spe- cially made crates, boxes or1 cubes, set it in the cooler over night to permit the butter to harden and then cut it into prints by means of wire cutters. To this type of printers belong the 3/8 BACKING Friday, the Low, the Simpson, the Miller printers, and others. For cutting tub butter a machine that utilizes all the culls is most practical. For this purpose the American Butter Cutter is used very generally. When printers of the type of the Friday printers are used, it is advisable to line the boxes with parchment before packing. This keeps the surface of the butter cleaner, it protects it against the injurious effect of contact with the iron parts of the cubes, it minimizes the amount of scraps that have to be disposed vof at a loss. It is desirable also to cover each Friday cube, after packing, with a properly fitting cover. Pigf. 75. C. P. Miller Hydraulic Cutter for Frozen or Otherwise Very Firm Butter Courtesy L. C. Sharp Mfg. Co. The cutting of the butter should be done with clean taut wires, free from rust. Piano steel wire is used for this purpose. For the good of the flavor of the prints, tinned wire only should be used. Any butter adhering to the bare steel wire soon causes it to rust and the action on the metal gives the butter a very disagreeable, puckery, metallic flavor. The mechanical operation of the butter printer should be performed in such a manner as to insure prints with square corners and straight, sharp edges. The handling of the prints should not be done with bare hands. It can readily be done with ladles or sticks. The operator who cuts the butter and places it on the wrapping table, and the person who puts the first wrapper around the print, should wear clean gloves, prefer- ably freshly laundered, white cotton gloves. The printing should be done in a clean, cool room, screened from flies, and properly ventilated. PACKING BUTTER 379 In order to insure correct weights, each print should be passed over an accurate scale. No matter how accurately the wires of the cutter are set, they yield to the resistance of the butter and are apt to stretch. The weighing of each print is the only reliable guarantee against short weights and overweights. Unsalted butter is slightly lighter than salted butter, so that prints of unsalted butter must be very slightly larger than those of salted butter in order to weigh the same. The wrapping is done either by cheap help, boys or girls, or by wrapping machines, which wrap the butter, place it in cartons, and wrap and seal the cartons with great rapidity and precision. The first wrapper should be a parchment wrapper. This should be treated in a similar manner as the tub liners. For maximum convenience a wooden box about 20 inches long and with an inside width slightly greater than the width of the one pound parchment wrapper may be used. This box may be installed in a convenient place in the print room, it should' have an overflow and be connected with the steam and water line. While the print room is in operation this box is kept full of boiling hot brine, containing enough salt, so that there is always a visible deposit of undissolved salt in the bottom. A little steam should run into this brine continually, so as to keep the brine at boiling heat. For suspending the parchment wrappers in the brine, wooden clamps of sufficient length may be used. A bunch of wrappers is fastened into the clamps, the clamps are placed across the box and the wrappers swing and soak in the brine. In this manner all but the top inch of the wrappers is soaked. It is not desirable to wet the entire wrapper because the sheets then stick to one another and delay the work of wrapping. The wrappers should be soaked in the boiling hot brine for at least 5 minutes and the brine should be renewed at least once each day. The same treatment may be given wrappers" used for unsalted butter. High grade parchment wrappers, properly parchmented and free from all kinds of specks, are the most economical. Parch- ment wrappers frequently contain very minute specks of metallic lustre. Microchemical examination of these specks shows that 380 PACKING BUTTER they consist of copper or of some alloy containing copper such as brass or german silver. These metal specks are acted upon by the salt and acid in the butter. Gradually a green spot or circle forms on the wrapper and on the butter at the point of contact, showing verdigris, giving the butter an unsightly and suspicions appearance, and actually rendering it unwholesome. Fig*. 76. Unit of Peters Package Machinery This machine forms and lines the carton, folds the wrapper and closes the carton, and wraps and labels the carton. Courtesy Peters Machinery Co. Such butter is usually rejected by the consumer. With pro- longed age the action of these metallic specks bleaches the entire print and gives it a rank tallowy flavor and odor. Parchment wrappers used for butter should be free from these metallic impurities. The second wrapper is a wax paper. It consists of paper coated on both sides with a thin film of paraffine, the paper having been passed through a paraffine bath. The wax paper wrapper furnishes additional protection against evaporation and against the deteriorating action of air. Experimental trials and commercial experience have demonstrated that butter actually does keep better, especially is the flavor on the outside of the print preserved, by the double wrapper. PACKING BUTTER 381 The wrapped print is slipped into a carton. If the carton is the final enclosure, it is usually of high quality stock, paraf- fined, and bears the name and trade mark of the creamery. Creameries placing a special wrapper on the outside of the carton, generally use a cheaper grade, plain carton, and have their name and trade mark placed on this outside wrapper. Occasionally also printed matter with information for the con- sumer concerning the quality of the butter, also premium labels, etc., are slipped into the carton. Packing in Boxes. — The prints, wrapped and placed in cartons, are packed into wooden or fibre boxes, usually holding from 10 to 50 one pound prints. Some of the larger creameries have their name and trade mark stencilled or burnt onto the ends of the box. This adds to the attractiveness of the package and advertises the brand. Of recent years, carton or fibre boxes have come into extensive use for packing and shipping prints. The chief virtue of the fibre boxes lies in their relative cheapness, averaging at least five cents less per box. They are used to good advantage for local shipments of print butter and especially during the cold season. For long distance shipments of print butter and particularly during the hot summer season, corrugated fibre boxes and similar paper boxes are less suitable. Under these conditions the boxes often become soaked with the brine of the butter and thus suffer seriously in transit. The reason for this is that corrugated fibre boxes are not as rigid as wooden boxes; in summer, due to the heat, the butter is soft and the rough handling to which these boxes are subjected, causes this soft butter to become mutilated ; this in turn results in the expulsion of a portion of the brine of the butter, which soaks through the carton of these boxes. Grocery stores often also object to the fibre boxes, because these boxes are not as serviceable and convenient to use in the store and on the delivery wagon as wooden boxes. Most of the wooden boxes for print butter are made of poplar, hemlock or spruce. The majority of these are bought in the knock-down shape and . are made up in the creamery. Four-penny cement-coated wire nails are best suited for assem- bling the sides, ends, bottom and top. The most perfect boxes 382 PACKING BUTTER are tongued and grooved, but their greater expense causes their use to be limited. The usual weight -of the lumber used for wooden boxes is one-half inch for the sides, top and bottom and three-fourths inch for the ends. For large creameries the assembling of the boxes by the use of nailing machines is most economical. Of late, wire-bound boxes have come into use for packing and shipping prints. These boxes, while they are light, are stronger than the nailed boxes, their initial cost is slightly lower and the expense of assembling them is smaller, requiring less labor and fewer and smaller nails. Wire-bound boxes have the further advantage that they are practically burglar proof, avoiding loss of prints due to removal in transit. The correct size of boxes for standard size one pound prints is 13 x 13 x 10 inches for 50 pound boxes. Too little attention has been paid by many creameries to the quality and neatness of these shipping boxes and to the manner of packing itself. Poor material, shiftless nailing and the use of second hand boxes should be avoided. The boxes should be of the proper size, so that they can be filled full with prints. The packing of 10 prints into a thirty pound box and filling in with diverse refuse material, such as paper, straw, etc., is a poor policy which often results in mutilation of the prints and unsightly appearance. Too large boxes also involve exces- sive expense of transportation. Most boxes see rough handling in transit and unless they are strongly constructed and properly packed they are apt to reach their destination in damaged con- dition. This is especially the case with long-distance shipments and with export shipments. ' Advantage of Selling in Consumer's Packages. — It is obvious that the expense of the package and of packing is greater in the case of prints than in the case of tubs, boxes or cubes. The difference in cost, including package and labor, averages from one-half to one and one-half cent. This extra expense is borne by the consumer; print butter averages usually about one cent more than tub butter, at the sales end. The consumer's package has several distinct advantages. The butter when sealed in the consumer's package at the creamery or in the wholesale deal- er's establishment, is effectively protected against further agencies PACKING BUTTER 383 of contamination and deterioration. The package is opened only by the consumer; and usually reaches him therefore in more satisfactory condition. The individual package is the most con- venient form for distribution through the retailer's stores and for use by the consumer. The butter is protected against agen- cies of deterioration such as light, air and rapid changes in temperature, after it reaches the consumer. Butter bearing the trade mark of the manufacturer or dealer, as is the case with butter sold in the individual package, serves as an effective advertising means. If the butter is of uniformly acceptable quality, the consumer soon becomes familiar with that particular brand and will assume the habit of calling for that brand. In the case of occasional batches of low grade butter it is advisable to use either a plain wrapper or a special brand reserved for second grade butter only, in order not to jeopardize the reputa- tion of the established brand. Packing Farm Butter. — Butter made on the farm is put on the market in diverse packages. Butter that goes to the country store is usually packed in crocks, but considerable butter reaches the store also in the form of rolls. Crocks have the advantage that they protect the butter against abrupt temperature changes. If the crock is well glazed on the inside, it is fairly sanitary. Poorly glazed crocks are porous. The pores fill with grease and curd which are not removed by ordinary methods of washing and which cause the crock to become foul-smelling and to serve as a constant source of contamination with agencies detrimental to the quality of the butter. The crock is objectionable also because of its weight and its frailty. Some farm butter is put up in rolls weighing 1, 2 or 5 pounds and usually wrapped in parchment. Fancy or individual molds are also quite popular. The tendency, however, is to print the butter into standard size one pound prints and put them on the market wrapped in parchment and packed in cartons. The standard size print is, all things considered, probably the most desirable type of package for farm butter, especially when sold direct to residences, etc. The farmer who sells butter, in prints, wrapped in parchments and cartons bearing his name and trade mark is in a position to create a permanent call for it, provided 384 PACKING BUTTER that the butter is of good quality and uniform flavor, salt, and color, while butter sold in crocks, carton boxes, pails, etc., loses its identity when it leaves the farm and before it reaches the consumer. In the choice of cartons for the prints, paper cartons should be given preference over wooden cartons. Wooden car- tons such as are frequently used, lend the butter a woody flavor which is objectionable. Packing for Parcel Post Shipments. — Farm butter or cream- ery butter, to be shipped by parcel post, is best put up in pound prints, wrapped in water-proof parchment and sealed in paraf- fined cartons. The cartons are best inserted into corrugated pasteboard containers suitable for accommodating the different amounts to be shipped, and wrapped with good wrapping paper. Brand1 of the U. S.. Department of Agriculture, Office of Markets, conducted an extensive study of the possibilities and limitations of shipping butter by parcel post. This investigation showed that under ordinary weather conditions practically no difficulty was experienced. The chief problem in shipping butter by parcel post is to prevent the butter from melting, mere softening did not prove injurious. While the difficulty is somewhat greater in summer than in winter, the fact that mail cars must be heated in winter, does not entirely remove the danger of overheating the butter during cold weather. Brand points out, however, that the regulations of the Post Office Department on this subject are of such a nature that it is possible to obviate this trouble to a considerable extent in cold weather by marking butter parcels as follows : "Perishable — Keep away from heating apparatus/' He further offers the suggestions that over ordinary dis- tances and under average conditions butter wrapped as above directed, can be shipped without deterioration ; that it should always be chilled before shipment and chilled again immediately upon receipt by the consumer ; that it should be dispatched with, attention to the mail schedule so that it will be on the road as short a time as possible, and that shipments preferably should be timed to make the greater part of their journey at night, when temperatures are materially lower than during the day. One of the obstacles that has retarded the development of 1 Brand, "Marketing by Parcel Post." U. S. Dept. of Agriculture, Farmers' Bulletin 611, 1914, pp. 16 to 21. PACKING BUTTER 385 parcel post shipment of farm butter and similar farm produce has been the unfortunate tendency of some farmers to ask prices far above those current in their own rural localities and higher than those charged by fancy retail stores of the cities for butter of the same grade. It is obvious that the consumer will refuse to look to the parcel post service as a practical and desirable means to secure his butter, as long as he is unable to buy it through this channel at prices that are no higher than those which he is charged at the store. Packing Butter for Exhibits and Scoring Contests. — When preparing butter for exhibits and scoring contests neatness, attractiveness and protection against high temperature are of chief importance. For exhibits proper, butter may be used for diverse designs, representing certain objects, or it may be put up in neat commercial packages, attractively grouped and arranged. For scoring contests, where the chief object is score on the quality basis, the twenty pound white ash tub is the most suitable pack- age. It is large enough for all practical purposes of scoring and sampling for analysis, and it is small enough to avoid unneces- sary sacrifice of butter and excessive transportation charges. Scoring contest butter is usually not returned to the maker after the contest. In most cases it is sold and the returns are used towards defraying the expense of the scoring, in which case the entire package is lost to the creamery. In other instances the returns sre pro-rated among the contestants according to the pounds of butter entered, in many cases the creamery gets something back for its butter, though the price received for the butter after scoring, is usually very low, due to the damaged condition of the goods. The twenty pound tub is desirable also because it can be conveniently packed into a sixty pound tub for shipment. In putting up the scoring contest butter a perfect tub should be selected. This should be treated in the usual way, steamed, paraffined and neatly lined with brine-soaked parchment circles and liners. The butter should be packed into it very firmly with sterile and cooled ladles and packers and in a clean, cool room. The packing should be finished in the neatest possible way. After cutting the surplus butter off the top so as to leave a 386 PACKING BUTTER perfectly level and smooth surface, the liner extending one inch above the edge of the tub is carefully folded over the butter with clean hands, a clean cloth circle is placed on top and on this is sprinkled a little clean dry salt, evenly distributed. After the lid is put on the tub, the outside of the tub should be sand- papered until it is perfectly smooth and clean. Then the Hd is neatly fastened down to the tub with three to five standard fasteners. The twenty pound tub is then dropped into a sixty pound tub and clean paper, clean shavings, excelsior, sawdust or other insulating material, is solidly packed between the inside and outside tub, bottom, sides and top. It is advisable to place the 60 pound tub and the packing material into the creamery cold room several days before use, so as to thoroughly chill them. The lid is then fastened to the sixty pound tub, it is tagged with the name and address of the maker and the addressee. Then it is best set into the cold room for twenty-four hours before ship- ping, in order to harden the butter. Butter put up as above directed will reach its destination at any reasonable distance in good and attractive condition. The cold packing around the inside tub furnishes a splendid insula- tion, guarding against rapid warming up, which would prove detrimental to the delicate flavor of the butter and disadvan- tageous to the buttermaker's chances of success in the contest. Some buttermakers fill the space between the two tubs with crushed ice. This is unsatisfactory because it detracts from the neatness of the exhibition tub. Also the ice generally melts in transit and if the tub is put in cold storage before scoring, as is usually the case, the water between the two tubs will freeze into a solid mass, converting the entire package into one insep- arable unit. The only means to get the inside tub out in such a case is to chop off the staves of the outside tub with an ax. If the butter judge has to attend to the unpacking himself these difficulties may have an unfavorable, though entirely uncon- scious, effect on the score of the troublesome tub. Aside from these objections melted ice is a good conductor of heat and therefore makes very poor insulation, while sawdust, paper, wood shavings, etc., hold cold very efficiently. PACKING BUTTER 387 Loss of Moisture in Packing. — When butter is packed into tubs and boxes some moisture is lost, as a certain amount of water is thereby pounded out of the butter. A small additional loss of moisture further occurs in the cutting and printing of the butter. The average loss of moisture due to packing of 619 different churnings of butter at the Purdue University Creamery is shown in the following table : 1 Table 58. — Showing Difference of Moisture Content Between Churn and Box Samples — Averages Grouped According to Season of Year. Year Loss of Moisture Due to Packing from Churn to Friday Box April, May and June % Moisture July, August and September % Moisture October, November and December % Moisture January, February and March % Moisture 1907-8 1908-9 1909-10 1910-11 .27 .50 .52 .49 .57 .89 .61 .44 .40 1.04 .61 1.04 1.45 .82 .90 1.58 Averages .44 .63 .77 1.18 The least difference between the churn and box samples was shown in April, May and June. The difference increased grad- ually and was highest in January, February and March, when it averaged over 1 per cent. This gradual increase of the loss of moisture, due to pack- ing, from early summer to spring is interesting. It suggests that it is the result of the increasing firmness of the butter during the same time. The winter butter is firmer than the summer butter, more pounding is required in packing firm butter than in the case of soft butter. The loss of moisture by packing varies considerably with individual churnings. It depends on how well the moisture is incorporated. Leaky butter may lose several per cent, of mois- 1 These figures represent the differences between the churn samples and the tub or box samples. In every case the churn samples contained more moisture than the tub or box samples. 1 Hunziker, Mills & Spitzer, Moisture Control of Butter, Purdue Bulletin, 160, 1912. 388 PACKING BUTTER ture during packing. Under all normal conditions the butter- : maker may expect a loss of at least 4 per cent moisture due to packing from the churn into the tub or box. Table 59. — Moisture Content of Butter Before and After Print- ing with Friday Printer. The Samples Were Taken from Friday Cubes in the Cooler and Again from Prints of the Same Cubes after Wrapping. The Weight of All Prints Was One Pound, Each. Each Lot of Butter Represents a Different Churning. Percent Moisture Lots of Before Printing After Printing Butter Average A B Average A B Average Loss 1 15.8 15.9 15.85 15.4 15.9 15.65 .20 2 15.3 15.3 15.30 14.8 14.8 14.80 .50 3 15.8 15.9 15.85 15.9 15.9 15.90 + .05 4 15.4 15.1 15.25 15.4 15.4 15.40 + .15 5 15.6 15.7 15.65 15.7 15.5 15.60 .05 6 15.1 15.1 15.10 15.4 15.2 15.30 + .20 7 15.9 15.9 15.90 15.8 15.9 15.85 .05 8 15.7 15.8 15.75 15.7 15.7 15.70 .05 9 15.7 15.9 15.80 15.6 15.7 15.65 .15 10 15.3 15.3 15.30 15.3 15.1 15.20 .10 Average 15.58 15.51 .07 The loss of moisture that occurs during the process of printing obviously depends, aside from the completeness of moisture incorporation, on the method of printing employed and the firmness of the butter. Butter that is printed direct from the churn with the hand mold, while it is still soft, is not prone to lose much moisture. Butter that is packed in cubes or crates, which are subsequently placed in the cold room over night and then printed by simply cutting it with wires, as is the case with the Friday printer, also suffers but very little loss of moisture. This is readily shown by the following analyses of butter before and after printing: In the case of tub butter that has been allowed to harden and is subsequently stripped and printed by the use of the Amer- PACKING BUTTER 389 ican Butter Cutter, the loss is obviously considerably greater, amounting to several tenths per cent. In this case the butter is not only cut, but considerably mutilated while it passes through the cutter, as shown in the following table which represents eighteen different lots of tub butter bought on the open market : Table 60. — Moisture Content of Butter Before and After Run- ning it Through the American Printer. The Samples Were Taken from the Stripped Tubs Before Cutting and Again from the Prints Made from the Butter Percent Moisture Tub Numbers From Tubs From Prints Loss 1 15.3 15.2 .10 2 14.3 14.0 .30 3 14.9 14.8 .10 4 16.1 15.9 .20 5 16.0 15.6 .40 6 16.0 15.6 .40 7 14.9 14.6 .30 8 15.2 14.7 .50 9 14.6 14.5 .10 10 16.2 15.9 .30 11 15.9 15.9 .00 12 15.8 15.4 .40 13 15.4 15.3 .10 14 15.4 15.2 .20 15 15.3 15.0 .30 16 15.4 15.1 .30 17 15.9 15.6 .30 18 15.1 14.9 .20 Average 15.43 15.18 .25 Cost of Packing. — The cost of packing butter varies largely with the cost of the package and the expense of labor. Prints are a more expensive package than tubs, boxes and cubes. The quality of wrappers, cartons and shipping boxes used and the elaborateness of the design on them further influence the expense of the package. The quantity in which the package is bought also affects its cost. In car load lots larger rebates, both in the price of the package and in the freight rates, may be secured. 390 PACKING BUTTER This difference naturally operates in favor of the large creamery and against the small creamery with limited operating capital. The use of machines for printing, wrapping and sealing the butter and for mailing the boxes reduces the help needed for labor. In the large creamery this work can be done by the cheapest kind of help, by young boys and girls, for there is enough work to be done to furnish steady employment for this kind of help. In the small creamery where the printing and wrapping occupies only a part of one person's time, the creamery usually cannot secure special cheap help for this work and it is done by the more High-priced help, the buttermaker or his helper. The cost of putting up one-half pound prints in separate cartons is about one-third higher per pound and the cost of putting up one-quarter pound prints in separate cartons is about twice as high per pound of butter as the cost of putting up one pound prints. The cost of putting up one-half pound prints and one-quarter pound prints in one pound cartons is about one-fifth and one-fourth, respectively, higher than the cost of putting up one pound prints. Cost of Packing Butter in Tins. — Two sizes of tins for packing butter are accepted as standard tins by the United States Navy, the net 5 pound tin and the net 6 pound 6 ounce tin. The 5 pound tins are packed in boxes holding 16 tins, the 6 pound 6 ounce tins are packed in boxes holding 12 tins. In May, 1918, the cost of the package (5 pound tins), including tins, boxes, corrugated paper liners and strap iron, was about $2.44 per 1000 tins or about 3 cents per pound of butter. To this should be added the cost of nails and labels which amounts to less than .05 of one cent. The labor, when large quantities of butter are tinned, is but very slightly more than that of printing and wrapping butter, but for average conditions it should be placed at one-half to three-quarters of one cent per pound. This then, would make the total cost of packing butter in tins about 3 1 cents per pound. It is customary for the manufacturers of tin cans to loan to the creamery a sealing machine, for closing the cans after they are packed. The rental basis is usually about $25 per year PACKING BUTTER FOR U. S. NAVY 391 plus the freight on the machine both ways and plus an insur- ance premium of about $3.50 per year on the value of the machine. These prices and terms are naturally subject to changes. They prevailed in the spring of 1918. GENERAL DIRECTIONS FOR PACKING BUTTER FOR THE UNITED STATES NAVY. Tinned and Tub or Cube Butter— Quality. "Shall be fresh butter, made from fresh pasteurized cream (held at a temperature of 145° F. for 25 minutes, or at 176° F. for an instant), none of which shall at any time contain more than 0.27 per cent of acid, calculated as lactic acid, for butter scoring 94, or 0.234 per cent for butter scoring 95 (or more acid in 50 c. c. of cream than will be neutralized by 15 c. c. of N/10 alkali solution for butter scoring 94, or 13 c. c. for butter scoring 95) ; nor shall the cream contain more than 35 per cent butter fat. "Shall be strictly of the highest grade of creamery butter, at least two-thirds of which must score not less than 95 and the rest not less than 94 when made. "Moisture in the finished product at time of packing must not exceed 13*/2 per cent for tinned butter and 14 per cent for tub or cube butter. There must be no preservative used other than common salt, and that shall be at a rate giving not less than 2y2 per cent or more than 3^4 per cent salt in the finished product at time of packing. Inspection and Tests. "The ingredients, manufacture, sanitation, packing, boxing, marking, and shipping of the butter shall be subject to inspec- tion by Government inspectors, who shall have full authority to reject any package or lot of milk, cream, or finished butter, and to enforce compliance with the requirements of these speci- fications as well as to demand first-class work in every particular. "The Government inspector shall make all the necessary tests to determine that the acid in the milk or cream and the salt and moisture contents in the butter are within the limits specified. 392 PACKING BUTTER FOR U. S. NAVY "At the option of the Bureau of Supplies and Accounts, the contractor or his agents may, however, be required to make all the tests necessary to determine that the acid in the milk or cream and the salt and water contents of the butter are within the limits specified, and all such tests made by the contractor or his agents shall be subject to supervision, verification, and approval by Government inspectors. Containers — Tinned Butter. "Tins. — Tins to be made of prime coke plate weighing not less than 90 pounds per box of 112 sheets, size 14 inches by 20 inches. Side seams to be of either lock or lap type and soldered on out- side only. Top and bottom ends to be lined with sanitary lining compound of suitable gasket before being double-seamed on. "Tops and bottoms to be completely covered on the inside and outside with processed lacquer so that there will be no un- tinned edges exposed on the inside of the can. Inside and outside of cans, tops, bottoms and sides, except necessary margin for soldering side seams, to be lacquered before plate is manufac- tured into the finished container, with processed lacquer, which is to be baked on at a temperature of approximately 380° F. The unlacquered margin of side seam to be covered with air- drying lacquer after can is finished. "Two sizes of tins will be acceptable, viz., tins containing 5 pounds net weight, as used heretofore, and standard No. 10 sanitary type tins containing approximately 6 pounds 6 ounces. "The tins must be packed completely full, leaving no air space. Net weight only to be paid for. "Packing. — The butter must be packed in thoroughly clean tins, and the tins fully sealed and marked immediately as di- rected, the creamery where the butter is made, the butter to be packed within two hours after the time of churning. "Sealing. — Each tin must be hermetically sealed by mechan- ical process, without the use of solder. "Cases. — The cases shall be made of well-seasoned lumber, planed on outside; tops, bottoms, and sides to be not less than full y2 inch and ends not less than full ^f inch thick when finished. To be securely nailed and strapped with J^-inch flat PACKING BUTTER FOR U. S. NAVY 393 iron. On each case shall be plainly stenciled or stamped the actual net weight of butter contained therein, the score, name of contractor, brand (optional with contractor), number of con- tract, and date of packing; cases shall be free from all other marks, except such as may be placed thereon by the Government inspector. Five-pound tins are to be packed 16 to the case, and No. 10 tins 12 to the case. Each tin must be plainly marked " pounds net .... butter," name of contractor, and date of packing, and shall be carefully wrapped in paper and packed in sawdust; the cases shall be completely filled with sawdust. Suitable corrugated paper liners and paper fillers may be used in lieu of sawdust, in which case it will not be necessary to wrap each tin in paper, but all motion of tins must be prevented if this style of packing is used. Containers — Tub Butter. "Tubs. — The butter must be put up in regular, sound, first quality white-ash tubs, provided with sound covers and five sound hoops, two at the bottom, one at the center, and two near the top ; tubs to hold from 60 to 65 pounds net weight each. The tubs must be soaked in the usual manner, properly steamed, and immediately coated on the inside with paraffine having a tem- perature of not less than 240° F. when applied. They must then be lined with parchment paper (side lining, bottom and top cir- cles), which must first have been sterilized and then soaked in a clean brine solution for at least 30 minutes immediately pre- ceding the time at which they are used. "Packing. — The parchment lining must overlap the bottom and the top edges of the butter at least half an inch. The butter must be packed immediately after it is made, and each tub must be packed solid throughout and completely filled. A cloth circle must be placed on top of the parchment circle of each tub and covered with a thin layer of salt. The tub covers must be se- curely* fastened by two strips of substantial flat iron not less than y2 inch in width securely fastened to the sides of the tub and brought over the cover at right angles. "By means of a suitable rubber stamp and stamp ink each tub must be plainly marked on the cover and side with the net weight of the butter it contains, the name of the contractor, with 394 THE OVERRUN or without brand, number of contract, and the date of packing, and shall be free from all other marks, except such as may be placed thereon by the Government inspector. Net weight only to be paid for. "The letters in the rubber stamp must not be less than % inch square. Marking by means of stencil and blacking will not be permitted. Containers — Cube Butter. "Cases. — Cases to be cubical or rectangular in shape and to have a capacity of from 56 to 66 pounds; to be made of first quality white spruce or Pacific coast spruce or clear poplar lum- ber, cut true to gauge and planed on both sides; tops, bot- toms, and sides to be not less than J/£ inch thick, and ends not less than % inch thick when finished; to be well nailed with cement-coated nails, and strapped with J^-inch flat iron or strong wire; otherwise to conform to all applicable require- ments of the specifications for containers for tub butter above, which include paraffin coating and parchment paper lining." CHAPTER. XIII. THE OVERRUN. Definition. — By the overrun is understood the difference between the pounds of butterfat churned and the pounds of butter made. The overrun is made possible by the fact that, in addition to butterfat, butter contains non-fatty constituents, such as moisture, salt, curd and small amounts of lactose, acid and ash. Importance. — The overrun is the financial "vitamine" of the creamery business. Under the present system of creamery oper- ation there is no margin left between the purchase price of the butterfat and the sales price of the butter, on which the creamery can do business. In fact, in a great many instances the cost per pound of butterfat is greater than the price received per pound of butter. The creamery must, therefore, depend on the overrun to pay for the cost of manufacture and sale of the butter and to make a reasonable profit. If it were not for the overrun the creamery could not do business on the present method of THE: OVERRUN 395 paying the patrons for butterfat. The overrun, therefore, log- ically and rightfully belongs to the creamery. If the dairy farmer makes butter on the farm, the overrun he makes compensates him for his trouble, time, labor and expense involved in making and selling the butter. The Theoretical Overrun. — The theoretical overrun is a ''pencil" overrun. It aims to indicate the maximum amount of butter that could be legitimately made from a given amount of butterfat, if all conditions of butter manufacture could be con- trolled with mathematical accuracy. The theoretical overrun shows, for example that, if there were no mechanical losses and if butter contained exactly 80 per cent of fat, the maximum amount of butter that could be made 100 from 100 pounds of fat would be -57— X 100 = 125 pounds and • . oU that, therefore, the maximum legitimate overrun is limited to 125 — 100 — 25 per cent. In the commercial operation of the cream, however, it is a mechanical impossibility to establish the degree of accuracy that is assumed in the calculation of the theoretical overrun. No such standard of accuracy can be attained. For this reason the figures resulting from calculation of the theoretical overrun cannot serve as an acceptable standard for overrun. They fail to take into consideration the true possibilities and limitations of the overrun and they are prone to prove confusing and misleading. At best they can serve only as an approximate and arbitrary illustration for the elementary information of the layman. The Actual Overrun. — The actual overrun shows the differ- ence between the actual amount of butter churned out and the amount of butterfat bought and paid for. It is affected by a multitude of factors, which control, directly or indirectly, the determination of the amount of butterfat bought and churned and the amount of butter made. Conditions Influencing the Overrun. — As previously stated, the overrun is made possible by the fact that butter contains, in addition to the butterfat, water, curd, salt and ash. The larger the sum total of these non-fatty constituents, the smaller 396 THS OVERRUN the amount of fat that is required to make one pound of butter, the more butter can be made from a given amount of fat, and the larger, therefore, will be the overrun., Consequently, the composition of the butter is the fundamental factor that con- trols the overrun. Other factors which influence the overrun are the accuracy of weights and tests of cream, butterfat shortages of cream routes and cream stations, the number and amount of mechanical losses of butterfat, such as loss of fat in the skim milk, in the buttermilk and through factory leaks, and accuracy of weights and tests of butter. Effect of Composition of Butter on Overrun. — Of the non- fatty constituents of butter, that control the overrun, the moist- ure, salt and curd are the only ingredients that need be consid- ered and the relative amount of which is large enough and is sufficiently variable to materially affect the overrun. The other non-fatty constituents, the ash, milk sugar and acid, all together total less than .5 of one per cent, they are practically constant and are not materially affected by the process of manu- facture under all normal conditions. Moisture. — The moisture exerts the greatest influence of the non-fatty constituents, on the overrun. It is present in larger amounts than all the other non-fatty constituents com- bined and it is the most variable. Its maximum limit in the United States is fixed by a ruling of the Internal Revenue De- partment below 16 per cent. According to this ruling butter con- taining 16 per cent moisture or over is no longer legal butter, but is classed as adulterated butter. Under all reasonable conditions of manufacture and of raw material, the moisture content of butter will not exceed 16 per cent. There are times and conditions, however, when but- ter has an inherent tendency to naturally hold more moisture. This is especially the case in early summer when the cows are turned from dry feed to succulent pasture, and on account of their ravenous appetite for green feed they consume a great abundance of it. This causes the butterfat to have a low melt- ing point and to be abnormally soft. In this soft condition it mixes readily with water and has the power to retain relatively large quantities of it. With intelligent control of the churn- ing temperature and careful adjustment of the process of work- THE OVERRUN 397 ing, the buttermaker can, without much difficulty, hold the moisture content of his butter below the maximum limit of 16 per cent, even under these abnormal conditions of raw mate- rial. There are other times and conditions when the butter has properties that cause it to take up and hold much less moisture than 16 per cent. This is usually the case in winter, when the cows are well advanced in their period of lactation and receive largely only dry feed. These conditions are conducive of rel- atively small size fat globules and fat of a relatively high melt- ing point, causing the fat to be very firm, in which condition it refuses to readily mix with and hold water. The tendency then is for butter to be low in moisture and the overrun to be corre- spondingly low. But here again, with the proper adjustment of the churning temperature and with the intelligent manipula- tion of the butter in the churn, the buttermaker can, without great difficulty, hold the moisture content of his butter close to the 16 per cent limit and thereby maintain a satisfactory overrun. These facts also explain why the buttermaker on the farm and the buttermakers in many small local creameries, who lack the knowledge, skill and equipment necessary to regulate the per cent moisture in butter, and who often pay no attention at all to moisture content, are unable to secure a satisfactory over- run in winter, and frequently exceed the 16 per cent moisture limit in summer. Since the overrun represents one of the all-essential factors in successful butter manufacture, and since, in the face of the keen competition and of the narrow margin of profit, the very life of the creamery depends on the overrun, it is the butter- maker's undisputed duty to hold the moisture content of his butter as close to the maximum limit permitted by law as possi- ble, consistent with maintenance of quality and making due allowance always for unavoidable variations. If the buttermaker adjusts his process in such a manner as to work to a moisture content of 15.5 per cent, he should experience no serious difficulty to stay within the requirements of the law, and at the same time to secure the maximum overrun that may be expected of him. other factors being under control. 398 THE OVERRUN Salt. — The salt represents the next largest non-fatty con- stituent of butter. The salt content of butter ranges from no salt to about 4.5 per cent salt, averaging about 3 per cent. It is obvious that the more salt butter contains, other factors being equal, the larger will be the overrun. Unsalted butter, therefore, yields a much lower overrun than salted but- ter, unless the legal moisture limit is exceeded or an abnormal amount of curd is incorporated in the unsalted butter, both of which practices are unlawful and would unfavorably affect the keeping quality of the resulting butter. The difference in overrun between unsalted butter and butter containing about 3 per cent salt is approximately 4.5 per cent. With the price of butter at 40 cents, the sale of un- salted butter at the same price would cause the creamery to sacrifice 1.8 cents on every pound of butter manufactured. In other words, unsalted butter would have to be sold at a price approximately 1.8 cents higher than salted butter in order to secure the same returns for butterfat sold in the form of unsalted butter as that sold in the form of salted butter. Curd. — The curd content of butter is not generally consid- ered a factor of consequence from the standpoint of overrun. In properly made butter the curd content is small, averaging about .7 of one per cent, and it is fairly constant. If butter were not washed at all it would not exceed 1.5 per cent curd and would average around 1 to 1.25 per cent. In properly washed butter it is practically always below 1 per cent. In calculating the overrun, the curd is usually figured to be 1 per cent, allow- ing it to also represent the remaining traces of other non-fatty constituents, the ash, milk sugar and acid. Efforts are made occasionally, however, to increase the over- run by incorporating in butter, extraneous additional curd, in the form of wet or dry casein, or skim milk powder. In such cases the extraneous curd is added to the butter in the churn with the salt and it is worked in during the regular process of working. If the curd is so added, in form of starter, the increase of the curd content in the butter is very slight and barely perceptible by analysis, and there is no appreciable increase in the overrun. THE: OVERRUN 399 If the curd is added to the butter in the form of dry casein, or skim milk powder, then the increase of the per cent curd found in such butter is very marked and is limited only by the amount of these products added. The curd content of the butter thus may be from 5 to 10 per cent or more and the increase in the over- run may amount as high as 15 per cent or more. In the case of skim milk powder a considerable amount of milk sugar is also retained in butter with the added curd, making the overrun still higher. Furthermore, the increased curd content of such butter augments the moisture-holding properties of the butter and un- less efforts are made to hold the per cent moisture in such butter to or below 16 per cent, the moisture content may far exceed this limit, causing a still greater overrun. The practice of working extraneous curd into butter in any manner is a pernicious practice. It is in violation of the law which forbids the incorporation in butter of any substance other than the fat of milk or cream and small portions of such other milk constituents as naturally enter into butter in the process of manufacture, with or without salt and with or with- out harmless coloring matter. Extraneous curd incorporation further is a positive detriment to the butter industry, because it causes rapid deterioration, injures the keeping quality and thereby displeases the consumer, reduces sales, depresses the price and invites the consumption of butter substitutes. Accuracy of Weights and Tests of Cream. — Since the over- run is calculated on the basis of butterfat actually bought and paid for, it is necessarily immediately influenced by the accu- racy of the weights and tests of milk and cream, upon the basis of which the amount of the butterfat is calculated. The overrun cannot be correct, be it high or low, if the weights and tests are not correct. Weights of milk or cream that are in ex- cess of the correct weights received and tests higher than the correct tests, are bound to lower the overrun and if the error is considerable and continuous, it spells ruin to the creamery. Where the milk or cream is sampled, weighed and tested at the creamery, as is the case with most cooperative cream- eries and with creameries operating on the direct shipper sys- tem, inaccuracies of this sort are not very frequent and their 400 THE OVERRUN recurrence can be readily avoided. But when the cream is weighed and sampled on the route wagon, as is the case with the cream route system, or where the cream is weighed, sampled and tested at the cream station, or where the creamery accepts the weights and tests of the independent cream buyer, control is far more difficult and the creamery often surfers great losses of butterfat, which compel it to pay for more butterfat than it actually received and this in turn is bound to greatly depress the overrun. If the error in weights and tests is in the other direction, if the weights are short of the actual amount of milk or cream received and if the recorded tests are lower than correct tests would be, then the creamery is receiving more butterfat than it is paying for and the overrun is correspondingly high. Ab- normally high overruns, therefore, are not infrequently due to low weights or low tests, or both. Occasional accidental errors in weights and tests may rea- sonably be expected. They generally work no great hardship, neither on the creamery nor on the farmer, and in the long run usually balance each other. Persistent and continued inaccuracies, all in one direction, on the other hand, suggest either systematic carelessness and inefficiency, or intentional wrongdoing. If due to inefficiency, then the equipment or the method is at fault, and the overrun can only be made to return to what it should be by a systematic effort to locate the trouble. The route, station or platform scales should be examined to make sure that they swing freely, operate correctly, and weigh accurately. Scales that "stick" or do not "break" sharply are very often the cause of a low overrun, registering more milk or cream than the creamery actually received. The milk or cream, and especially the cream on the route wagon and at the cream station, must be thoroughly mixed before the sample is taken. Sudden drops in the overrun in winter are not infre- quently due to an unsatisfactory mechanical condition of the cream at the time the sample is taken. Frozen cream should be treated in accordance with directions given in chapter IV, and the cream, after the treatment, should be stirred very thoroughly. Under any condition the cream sampler should under- OVERRUN 401 stand that the top layer in the cans or in other cream con- tainers, is usually richer in butterfat than any other portion of the contents. If the sample is simply taken from the top, it cannot help containing a higher per cent of fat than the re- mainder of the cream, and tests made from such samples are bound to be too high and the overrun low. In the testing1 of the milk or cream it should be definitely ascertained that the glassware used is correct, that the cream test balance has the necessary sensibility and is in satisfactory operating condition, and that the weighing, testing and reading is done with care and according to standard methods. Cream route and cream station shortages of butterfat are most always due to improper and careless sampling, causing the individual samples to be richer in butterfat than the cream from which they are taken. Whether this be due to mere care- lessness on the part of the operator, or willful deception, makes little difference. Creameries who fail to systematically check up the work of their routes and stations, and to hold their operators to account for their delinquencies, are doomed to a disastrously low overrun. Buying cream on the weights and tests of the independent buyer is a practice fundamentally wrong. The independent buyer is largely interested in selling to the creamery the great- est amount of butterfat possible. Therein lies his livelihood" and his profit. He cannot afford to sell more butterfat than he gets paid for and he is usually looking out for that. Unless he masters a strength of character far above the average of his profession, he may yield to temptation to the detriment of the overrun of the creamery that accepts his weights and tests. The creamery cannot afford to buy butterfat on any basis other than that of its own weights and tests. High tests and low overrun are likely to occur also in creameries that hold their samples for several days before test- ing. This is especially the case when the samples are kept in loosely sealed jars, or in a warm room, or both. In this case the incorrectly high tests are due to evaporation of part of the- moisture in the cream sample, increasing the per cent of fat and causing a low overrun. It is advisable to test all cream samples on the day they are taken or received. All samples should be 402 THIS OVERRUN taken and kept in tightly sealed jars, and if they cannot be tested promptly, they should be placed in the cold room until needed. Mechanical Losses of Fat. — Of the mechanical losses of fat in the creamery which materially affect the overrun, the fat lost in the skim milk and the fat lost in the buttermilk are the most important. Skim Milk. — On the basis of average milk, testing about 4 per cent fat and of butter containing 80 per cent fat, every one- tenth per cent fat lost in the skim milk reduces the overrun by about 2.2 per cent. It is obvious, therefore, that whole milk cream- eries cannot hope to secure as large an overrun as gathered cream creameries. The very marked effect of the small amount of fat lost in the skim milk, on the overrun, emphasizes the importance of securing the greatest possible skimming efficiency in the operation of the factory cream separator, so as to reduce the resulting loss to the very minimum. For detailed directions on the factors which influence the skimming efficiency of the cream separator the reader is referred to Chapter V on the "Separation of Milk." Buttermilk. — The exhaustiveness of the churning does not have so great an effect on the overrun as does the exhaustive- ness of skimming, yet it is a factor that must be reckoned with in order to secure maximum overrun. With cream testing about 33 per cent fat and using 10 per cent starter, and with butter containing 80 per cent fat, each one-tenth per cent fat lost in the buttermilk lowers the overrun approximately .23 per cent. It is generally considered that an average buttermilk test of not to exceed .2 per cent fat is not excessive on this basis ; the sacrifice in overrun that may be expected under fairly normal conditions, due to the fat lost in the buttermilk, is about .5 per cent. In a properly operated creamery where the conditions relat- ing to exhaustiveness of churning are carefully watched, the but- termilk seldom exceeds .2 per cent, and frequently drops below .1 per cent. In plants which ignore the importance of the ex- haustiveness of churning and which do not systematically check it up by testing the buttermilk, it is not uncommon to find the OVERRUN 403 buttermilk to test very high, amounting to from .5 to 1 per cent or more, and causing a reduction of the overrun of from 1 to 3 per cent or more. As it is difficult to correctly determine the per cent fat in the buttermilk by the ordinary Babcock test, the results of the test often do not show all the fat present in the buttermilk, so that the operator may think that he is churning exhaustively when in reality he loses much fat. For directions of testing buttermilk see Chapter XXII. Some of the most important factors which control the ex- haustiveness of churning are: Churning temperature, time held at churning temperature, richness of cream, condition of cream, fulness and speed of churn, size of butter granules when churn is stopped, etc. For detailed discussion of these factors the reader is referred to Chapter X on "Conditions Influencing the Churn- ability of Cream," also Chapter VII on " Neutralization" and Chapter VIII on "Pasteurization." Other Mechanical Losses Which Tend to Reduce the Over- run.— Frequently the low overrun is found to be due to exces- sive foaming of the cream in the vats. The cream foam usually contains a high per cent of fat. It is flushed out of the vats with difficulty only, and often much of it goes into the sewer. Efforts to thoroughly flush this foam out of the vats into the churn require excessive amounts of water, usually warm water. This in turn dilutes the cream and increases the amount of but- termilk, thus augmenting the volume of buttermilk and with it the amount of fat lost. The thinning of the cream in itself causes a higher per cent of fat in the buttermilk. Furthermore, the cream in the churn is thus warmed above the intended churn- ing temperature, by the copious rinsing down of the foam with warm water, which makes for less exhaustive churning. In most cases the excessive foaming of the cream in the vats is due to too high a speed of the coils, whipping air into the cream. This is especially 'the case when the vat is not full and the coil is only partly covered with the cream. Reducing the speed of the coil generally diminishes and often stops the foam- ing entirely. The larger the coil the slower should be its speed. The proper speed for a 24-inch coil is about 35 to 40 revolutions per minute, for a 29-inch coil 28 to 30 revolutions per minute. 404 THE OVERRUN Filling the vat full, so as to submerge the coil, will lessen the foaming. Running the coil with the vat cover down min- imizes the foaming, the slight pressure thus produced in the closed vat helps to keep the foam down. If the cream splashes into the vat from a great height, there is more or less foaming. A large vat gate assists in carrying off the foam with {he cream, when the vat is being emptied. Additional mechanical losses occur now and then by acci- dental spilling of milk and cream, leaks in pumps, pipe lines, cream troughs and churn doors, incomplete draining of milk and cream cans, pipes and troughs. These losses will greatly vary with the degree of carefulness or carelessness of the creamery personnel. . They represent a useless waste, benefitting no one and reducing the overrun. They are avoidable in most cases and can be guarded against by efficient supervision. All of these precautions play an integral part in the systematic maintenance of a satisfactory overrun. Accuracy of Moisture Tests. — Since the per cent of moisture is a fundamental factor determining the overrun, it is important that its determination be correct and reliable. This means care- ful sampling of the butter, a sensitive balance and conscientious operation of the test. For details of testing butter for moisture see Chapter XXII. The butter should be tested at the churn and again the next morning from the cooler. The churn tests are necessary as a guide for the buttermaker, the cooler tests serve as a check of the churn tests. The cooler tests are final and become a mat- ter of record. Accuracy at this point enables the creamery to approach the moisture limit permitted, with reasonable certainty of not violating the 16 per cent ruling, and thereby to secure the max- imum overrun possible. Accuracy of Weights of Butter. — Finally the overrun may be very materially affected by the accuracy of the weights of butter. In the case of the factory overrun the cubes and tubs are weighed prior to packing and again after packing, the dif- ference between the tare and the gross weights gives the net weight of the butter. Accuracy of weighing is necessary in order to insure the correct calculation of the overrun. THE OVERRUN 405 In the case of packing 63-pound tubs, it is customary to allow from 4 to 12 ounces for shrinkage. If the net weight of the butter is say 62 pounds 10 ounces the weight put on the tub is 62 pounds. Instead of weighing the filled tub, the butter may be weighed before it reaches the tub and the weighed butter is then packed into the tub. In this case only the net weight is placed on the tub. The San Francisco Wholesale Dairy Produce Exchange issued regulations demanding that standard cubes be rilled with 69 pounds of butter net and that the cubes be marked 68 pounds. If the butter is printed at the creamery, the accuracy of the net weight put into each print is reflected in the office over- run. Accuracy here is best secured by passing each print over a sensitive butter balance and correcting the weights, if short, or over. Example of Overrun in Whole-Milk Creamery. 10,000 Ibs. of 4% milk are received. 32% cream is separated. Skim milk tests .1% fat. 10% starter is added. Buttermilk tests .2% fat. Butter contains 80% fat. How much butter is made? What is the overrun? What is the per cent overrun? Answer.— Butterfat contained in milk, 4 X^°° • : = 4°° Ibs. fat. 4x 10000 10-n ,. Cream separated from milk, - r^ - = 12^0 Ibs. cream. Skim milk separated from milk, 10000—1250 = 8750 Ibs. skim milk. Fat lost in skim milk, - — J = 8.75 Ibs. fat. Fat remaining in cream, 400 — 8.75 — 391.25 Ibs. fat. Starter added to cream, - ' • ^ •= 125 Ibs. starter. Total pounds of cream churned, 1250 + 125 — 1375 Ibs. cream. 406 THE OVERRUN Approximate pounds of buttermilk made, 1375 — 391 =984 Ibs. buttermilk. 9 y 984 Fat lost in buttermilk, L14gg — = 1.97 Ibs. fat. Fat left for butter, 391.25 — 1.97 = 389.28 Ibs. fat. Butter made, — } XgQ89'28 = 486.6 Ibs. butter. Overrun, 486.6 — 400 = 86.6 Ibs. overrun. Per cent overrun, - - =. 21.65% overrun. In the above example the mechanical losses on the 400 Ibs. of fat were 8.75 + 1.97 — 10.72 Ibs. of fat, the per cent loss was ' = 2.68 per cent of the total fat received. Adding to these losses, the probable fat lost in the form of milk and cream spilled and retained in the pipes, etc., the total mechanical loss of fat may be placed at from 3 to 3.5 per cent of the total fat received. In whole milk creameries a loss of 3 to 3.5 per cent of the total fat re- ceived is generally accepted as a fair average loss under normal con- ditions of operation, though this loss can be considerably reduced by better organization and greater efficiency of operation. If there were no compensating factors, such as undeterminable unrecognized fractions of weights and tests of milk, which, in an effi- ciently operated creamery are bound to function in favor of the creamery, the per cent overrun would be as follows : V 3 Loss of 3% of total fat received = 25 -- IQQ =21.25% overrun. ioc v ? c Loss of 3.5% of total fat received = 25 \^— = 20.625% overrun. . , ;. Example of Overrun in Farm Separator Cream Creamery. 2000 Ibs. of 33% cream are received. 10% starter are added. Buttermilk tests .2 per cent fat. Butter contains 80 per cent fat. How much butter is made? What is the overrun? What is the per cent overrun? THK OVERRUN 407 Answer.— . . ,: ••". ?000 V^ Fat in 2000 Ibs. of cream, J^: ~ = 660 Ibs. fat. 2000 X 10 Starter added to cream, - r-r-r- — = 200 Ibs. starter. '•!'.' /. *..' .. "- 1UU . . Total pounds of cream churned, 2000 + 200 = 2200 Ibs. cream. Buttermilk produced, 2200 — 660 = 1540 Ibs. buttermilk. "7 V - Fat in buttermilk, , nn = 3-08 lbs- fat 1UU Fat left for butter, 660 — 3.08 = 656.92 lbs. fat. Butter made, 10° p' = 821.1 lbs. butter. Overrun made, 821.1 — 660= 161.1 lbs. overrun. Per cent overrun, - ~Z7 - — 24.41% overrun. 7 OR v 1 no Per cent loss of total fat, * — •467% f at- ooU Adding to this loss, the probable fat lost in the form of cream spilled and retained in the pipes, etc., the total mechanical loss of fat may be placed at approximately 1 per cent of the total fat received. In farm separator cream creameries a loss of 1 per cent of the total fat purchased is generally accepted as a fair average loss under nor- mal conditions of operation, though this loss can be considerably re- duced by improved organization and greater efficiency of operation. If there were no compensating factors, such as undeterminable and unrecognized fractions of weights and tests of cream, which, in an efficiently operated creamery are bouricj to function in favor of the creamery, the per cent overrun would be as follows : Loss ©f 1 •% of total fat received yields 25 -- r^ — : =' 23.75% overrun. Unavoidable Discrepancies in Weights and Tests that affect the Overrun. — The foregoing examples of actual overrun differ from the calculations of the theoretical overrun, in that they make allowance for the mechanical losses of fat in the process of manu- facture. But, similar as in the case of the theoretical overrun they are based on the assumption that the pounds of fat received and paid for, are determined with mathematical accuracy that yields absolutely correct results. They make no allowance in the weigh- 40& THE OVERRUN ing of milk and cream for the fractions of pounds that fall be- tween the smallest graduations on the beam of the scales ; they provide no tolerance in the testing of milk and cream for fractions of the per cent of fat that fall between the smallest graduations on the neck of the test bottle; and furthermore, they assume, in the calculation of the money due the farmer, that all fractions of pounds of butterfat, even those of the last decimal are included, making no allowance for the dropping of any fractions. But in practical operation these details do exist, and contrary to the general impression, their occurrence very vitally affects the actual overrun. It is not often that either the empty or the full can weighs exactly to whole or half pounds. In the majority of cases the exact weight is somewhere between the whole and half pound and the operator has to choose between dropping the undeterminable and unrecognized fraction or calling that fraction one whole or one- half pound. Similar limitations of accuracy occur in the testing of milk and cream, and particularly in the case of cream. The smallest division marks on the neck of the standard cream test bottle record one-half per cent and the distance between the graduation marks is very minute, about one thirty-seventh of one inch, making it impractica- ble, if not impossible, to determine and record fractions of less than one-half per cent, and occasionally difficult to even distinguish one- half per cent. But quite often the length of the fat column fails to exactly coincide with the whole per cent or the half per cent marks and the tester has to choose between dropping the uncertain, undeterminable and unrecognized fraction, reading to the next lower line, or calling that fraction a whole or a half per cent. Finally, the pounds of butterfat, as calculated from the pounds of cream and the fat test, often represent an amount with three to four decimals, rendering the computation of the money due the farmer complicated, time-consuming, uneconomical and inviting errors in the results. This has led to the practice on the part of the creameries, of dropping some of these fractions, usually including those of the second decimal. These unreadable and unrecognized fractions in the weights and tests of cream have, in the past, failed to be considered in the treat- OVERRUN 409 ment of the subject of the overrun. They are a fact, however, which the creamery has to deal with. It has no choice in the matter, and collectively they do affect the overrun to a very marked degree in one direction or the other, and to a degree that has not been fully recognized by the industry in the past. Since business cannot be conducted successfully by paying for more than is actually received, the creamery cannot pay for butter- fat it does not receive and no efficiently operated creamery would tolerate such transactions. Every loyal creamery operator will record only as much weight of cream and as much fat in the test as the cream scales and the Babcock Test actually show. And if the exact weight and the exact test involve fractions which cannot be determined by the standard equipment, and which are not recog- nized, he ignores these fractions. A similar practice is in vogue the country over in the purchase of butter and other farm produce. When butter is sold to the pro- duce trade on the open market, the buyer makes remittance for whole pounds only. The butter buyer does not recognize fractions of pounds, nor even half pounds, and he often insists on the scale beam touching the top when weighing. If a tub of butter weighs 63 pounds and 15 ounces, the creamery selling this butter would be entitled to and would receive pay for 63 pounds only. This is an established custom, recognized and accepted by the industry, not- withstanding the objections which have been raised against it recently. When the creamery recognizes, records and pays for half pounds of cream and half per cents of the test, and this should be the practice in every creamery, it is paying the farmer more nearly for the exact amount of the product it receives than is the estab- lished custom of buying butter and other farm produce. It cannot, as an efficiently conducted business, pay for more than it actually receives, hence it must receive the benefit of the doubt in all cases of unavoidable and unreadable fractions of pounds of cream and of per cent fat in the test. It may be argued that equity demands the payment for butterf at on the basis of a "give and take" system as far as these unreadable fractions of weights and tests is concerned, in which case fractions of over one-fourth pound and over three-fourths pound of cream would be recorded as half pounds and whole pounds respectively, 410 THK OVERRUN and all fractions of over one-quarter and three-quarters per cent in the test would be recorded as half per cents and as whole per cents respectively, while all fractions below the quarter and below the three-quarter pounds and per cents would be ignored. By this sys- tem of "give and take," it is claimed by some, these unreadable frac- tions would be taken care of equitably, both to the farmer and to the creamery. From the standpoint of absolute correctness, this system would be more nearly ideal, but it is impracticable in commercial operation. It is too complicated and confusing to be adaptable to the routine of creamery operation; in fact, it is not done. The unreadable frac- tions are either not recognized, or they are recorded as half or whole pounds and per cents respectively. There can be no double method, and since long established custom of the industry accepts, and busi- ness competition demands, the ignoring of the unreadable fractions, these fractions are, in fact, ignored. The gains in overrun which these unreadable and unrecognized fractions effect will naturally vary. Under average conditions they may amount to about 2 to 4%. In creameries in which the general standard of efficiency is low, these gains are more than offset by the mechanical losses. In creameries which maintain a high standard of efficiency, reducing the mechanical losses to the minimum, these gains very appreciably exceed the mechanical losses and result in the production of an overrun slightly higher than the maximum overrun possible on the basis of the calculations of the theo- retical overrun. Other conditions being the same, the increase in the overrun due to the unrecognized fractions varies largely with the amount and richness of each individual shipment of cream ; the smaller the amount of fat contained in each individual shipment of cream, the greater must necessarily be the effect of the undeterminable and unrecognized fractions on the overrun. Hence these gains actually amount to more in the case of creameries whose individual ship- pers, ship largely only in 5-gallon cans than in the case of cream- eries that receive most of their shipments in 8 and 10-gallon cans. The following arbitrary example may serve to illustrate the influence of the unrecognized fractions of weights and tests of cream and of the resulting fat calculations on the overrun: .>" THE OVERRUN 4.11 Example. — Gains, in weighing empty cans and full cans. 5-gallon empty can weighs 12.75 Ibs., marked 13 Ibs. ; gain is .......... . ... . . ...................... ...... .. .25 Ibs. 5-gallon full can weighs 51.75 Ibs., marked 51.5 Ibs.; gain is . . . ........ ........................ ....... ... .25 Ibs. Gain of cream .................... . ........ . ..... 50 Ibs. Net weight of cream recorded is, 51.5 — 13 = 38.5 Ibs. Cream tests 33 per cent fat. 2-2 \s -jo q Fat in 38.5 Ibs. of 33% cream, - ^ ' - 12.705 Ibs. fat. Fat in .5 Ibs. of 33% cream, 7 = .16 Ibs. fat. 1UU For each 100 Ibs. fat, gain in fat is, '^ X 100= 1.259 Ibs. fat. Gain in testing cream. Assuming that the fat column measures between 33 and 33.5%, say 33.25%, the test is read at 33% mark. For each 100 Ibs. of cream the gain is .25 Ibs. fat. OC \> -20 C • Viv For 38.5 Ibs. of cream the gain is, ' *g = .09625 Ibs. fat. ... . * lUU For each 100 Ibs. of fat the gain is, ' = -758 Ibs. fat. Gain in calculation of butterfat. Second decimal is dropped. In case of 12.705 Ibs. of fat .005 Ibs. fat are gained. DOS V 100 For each 100 Ibs. of fat the gain is, ^705 = '°394 lbs' fat Summary of Gains. Gains on weights of cream ............... ....... 1.259 lbs. fat Gains on tests of cream ............ ........... .... .758 lbs. fat Gains on calculations of fat ..... ................. 039 lbs. fat Total gains per 100 lbs. fat received. . ....... .2.056 lbs. fat Total losses (see example of actual overrun in farm separator cream creamery) ..... . .................. .1.000 lbs. fat - Net gains . . .................. ........... .1.056 lbs. fat Possible overrun. Butter contains ..... ............ . ............ 80% fat 100 100 lbs. fat make, -gjj^X 100. .. ............. 125 lbs. butter Less fat ...................... . ............. 100 lbs. Overrun .................................... 25% Gain in overrun due to losses & gains,— * ' - = 1.32% Total possible overrun ............. , ...... 26.32% 412 MARKETING OF BUTTER The above example is suggestive of the possibilities and limi- tations of the actual overrun. Its purpose is not, to indicate what the overrun should be, but to invite the consideration of the overrun from every angle that influences it. This example does not repre- sent any specific case, nor do the gains shown represent maximum possible gains. On the contrary, the unrecognized fractions re- corded here are small, they might in actual operation at times be considerably larger, in which case the increase in the overrun would be correspondingly greater. But this example does show that, pro- vided that the creamery operates on a high standard of efficiency, it is quite possible for the overrun to be slightly above the maximum of the theoretical overrun which, with butter containing 80%i fat, is 25%. In short, the subject of overrun can be consistently considered only in terms of efficiency and it is through efficiency only that any creamery can hope to regulate the overrun. The creamery that expects to reliably regulate its overrun must aim at maximum effi- ciency in those many details that so vitally affect the overrun ; effi- ciency that makes for exhaustiveness of churning and minimum mechanical losses on the one hand, and correct weighing and testing of cream and butter on the other ; efficiency that means the record- ing of every fraction of a pound of cream and every fraction of a per cent of fat in the test, that the standard equipment for weighing and testing enables the operator to determine. This, practical ex- perience and careful experimental study have shown to result in an overrun, in which the unavoidable mechanical losses are largely, or wholly, or occasionally even slightly more than wholly offset by such gains as may accumulate from the un- determinable and unrecognized fractions in weights and tests. CHAPTER XIV. MARKETS AND MARKETING OF BUTTER Importance. — At best the success of all business ultimately depends on its ability to dispose of its products at a satisfactory margin. Successful marketing is an open secret in all lines of business success and the butter business is no exception to this rule. Notwithstanding this fact, the market end of the butter business is a department not infrequently much neglected and often least understood by many producers and manufacturers MARKETING OF BUTTER 413 of butter and causing annually vast sacrifices in the form of un- satisfactory returns to the farmers and creameries of this coun- try. Essentials in Successful Marketing of Butter. Quality. — Quality is the first and all fundamental requisite for successful marketing. Butter must be of such quality that there is a de- mand for it. The consumer is the final judge of quality. The importance of quality is summarized most admirably in an ad- dress on Butter Markets by Mr. N. J. Eschenbrenner1 of the firm of Gude Bros. & Kieffer of New York City before the Dairy students of Cornell University April, 1916, as follows: "In summing up the whole proposition of marketing butter, it is wholly a matter of quality. When good butter is competing against poorer grades, when high flavored, clean butter is com- peting against unclean flavors, when solid, waxy-bodied butter is competing against weak-bodied, when desirable color, salt and style is competing against undesirable color, salt and style and general workmanship, on a basis of price and distribution, the better grades get the preference over the poorer grades and the poorer grades are absorbed only after satisfactory conces- sion has been made in price." While it is true that at times of butter shortage, when the demand exceeds the supply and the market is very brisk, the difference in price between different grades of butter is relatively small, because the average consumer is willing to "put-up" tem- porarily with lower grades in preference to going without but- ter, in the long run quality asserts itself. Under normal market conditions and when the supply is equal to, or greater than the demand, it is the lower grades that suffer. On quality depends the stability and permanency of our butter markets, quality con- trols the consumptive demand of the public, quality determines our ability to successfully meet competition with butter substi- tutes from within, and with imported butter from without our country, quality is the key to the establishment of satisfactory export markets abroad that will take care of our surplus at home, quality decides our ability to pay the farmer, on whose success the prosperity of the entire dairy industry depends, prices sufficiently attractive to induce him to keep on feeding 1 Eschenbrenner — Address on Butter-Markets, New York Produce Review & Am. Creamery, April, 1916. 414 MARKETING OF BUTTER and milking the dairy cow, and to interest himself in better cows, better methods, larger production and greater returns that make for increased prosperity of the producer and his family and better education for his children. Knowledge of Requirements of Different Markets. — The average consumer wants good butter, not always fancy butter, but butter of clean flavor, firm body, even color and medium salt. While butter of the best quality brings the highest price in most markets, there is a vast difference in the demands of the consumers in different markets of the country and in dif- ferent sections of the same market. Hence all wholesalers, commission men and jobbers do not cater to the same class of trade. There is a class of consumers who demand extra fine but- ter and are willing to pay a premium for it. The trade in many sections of the eastern markets is particularly critical. With this class of trade nothing but the best quality will do 'and lower grades are not desired. But there is also another class which considers price rather than quality and which is satisfied with butter that is of fair quality. While the creamery should concentrate its efforts on securing the best possible quality of cream, and on making the best quality of butter from it, under the now prevailing system of receiving cream in many sections of the country and particu- larly in the central west, it is impossible for many creameries to economically produce butter that grades above "extras," and extreme efforts to improve the quality in order to satisfy the most critical trade under such conditions would tend to prove disadvantageous to the financial success of the creamery, the difference in price received for the butter not being sufficient to offset the increased expense of operation and the possible falling- off of the cream supply. The quality of the butter which the creamery can afford to produce under these and similar circum- stances will depend upon the class of trade it must supply. The creamery that has developed a local trade, that is able to sell its butter 24 to 48 hours after manufacture and that dis- tributes it in small quantities, so that the butter is consumed within one week or less of the time of manufacture, may secure top prices for an 89 to 91 point butter by selecting those stores MARKETING OF BUTTER 415 that do not supply a highly critical trade. In trade of this kind many of the customers buy butter largely by the brand, they believe in the brand and if the butter is fairly uniform in quality they are satisfied. Similar markets may be located in the whole- sale trade of the large consuming centers for the surplus butter. There are wholesale dealers in these markets whose specialty lies in catering to the less critical trade and who therefore are in a position to dispose of the creamery shipments of butter of only fair quality to good advantage. It is to the creamery's interest to study the different channels through which the grade of butter which it produces will net the highest price. There are times when it is exceedingly difficult for the creamery to secure a satisfactory price on the wholesale market. During the early summer months when the principal demand in the larger markets is for butter for storage purposes, butter is bought strictly on the quality basis and sour-cream butter is not in demand, except that from creameries which have estab- lished a reputation of knowing how to handle such cream and how to manufacture from it a product of dependable keeping quality. Then again, in August and September, when the jobbers are loaded with May and June butter of good quality, and which they bought at low prices, the fresh midsummer butter is usually of poorer quality than the May and June butter placed in storage, the demand for it is very limited and its sales are often possible only by offering it at prices below those paid for the early summer butter. At the same time midsummer prices of butterfat paid by the creamery are generally higher than prices paid to the farmers for May and June butterfat. This combination of conditions therefore is prone to yield returns un- satisfactory to the creamery. The advantage to the creamery of having direct connection with consumptive channels of dis- tribution, such as local and neighborhood retail stores, is obvious, and the creamery should aim, during unfavorable periods of the wholesale trade in the larger markets, to move its lower grades through these local channels. The creamery which grades its cream and churns the grades separately may succeed in satisfying its more critical trade with the butter from the first grade cream. The butter from the second grade cream may be sold to bakeries and confectioners 416 MARKETING OF BUTTER but it is often preferable to sell the second grade butter under a special brand reserved for that class of butter only ; frequently it is possible to establish a satisfactory trade with acceptable returns with this special brand. Another, often very desirable outlet for the second grade cream is to manufacture it into un- salted butter and sell it to the Jewish trade, ice cream factories and bakeries. It is obvious from the above discussion that, while quality is supreme, the sucessful marketing of butter requires careful investigation and study on the part of the creamery, of the vari- ous market demands, and of the channels of trade by which these demands may best be supplied. The creamery must find and supply that class of trade which has the greatest demand for its butter. Uniformity of Quality. — Having succeeded in finding the most advantageous channels into which to divert the butter, it is very important that the creamery be able to hold these mar- kets, and success at this point in turn will largely depend on the maintenance of uniformity of quantity and quality. The prob- lem of maintaining the quantity of the supply will be discussed under the heading of "Selling Creamery Butter Locally." Uniformity of quality is an inevitable demand which the consumer exacts. In fact it is paramount in importance to qual- ity itself. The public demands butter that is uniform in flavor, salt, color and workmanship. Lack of uniformity makes the consumer suspicious and dissatisfied. He feels that he cannot depend on the product. Large creameries, who are in a position to grade their butter closely, whose churnings do not vary in size and whose process of manufacture is carefully standardized, find little difficulty to supply the class of trade which they cater to, with butter of fairly constant uniformity. Small creameries, with their irregular churnings and often inadequate equipment and system of manufacture, are not so fortunate in this respect. This handicap is responsible for the frequent loss of an other- wise satisfactory local trade and for their difficulty in securing satisfactory returns from the wholesale and commission mar- kets. MARKETING OF BUTTER 417 Standardizing Quality, Transportation and Distribution. — In an effort to overcome this handicap, creameries located in certain sections of the country have united into county and dis- trict associations. The purpose of these cooperative organiza- tions is to improve and standardize the quality and uniformity of their product. They employ a competent inspector whose duty it is to standardize their methods of manufacture and to inspect and grade their butter. Some creameries have gone one step farther in their co- operative effort, shipping cooperatively in carload lots and standardizing their methods of selling and marketing their product through the same distributing agency. The output of the individual small creamery is too small' to ship in carload lots. The average small creamery has to hold its butter for a week or longer before it can ship to advantage and even then it is often difficult for the small creamery to se- cure refrigerator service. The holding of the butter at the cream- ery with the usual inadequate facilities for keeping it cool, and the lack of refrigeration in transit, often cause the butter to ar- rive at the market in deteriorated condition resulting in low returns. Through intelligent cooperation numerous small cream- eries located in fairly close proximity and situated on the same railway line are often able to fill a car once or twice per week and thus are in a position to secure prompt refrigerator service and at reasonably low cost, so that at a reduced expense they are in a position to place their butter on the market fresher and in better condition. The standardization of methods of selling, is another step in the right direction, which is entirely practical with proper co- operation of a sufficient number of creameries and efficient lead- ership. In some instances these cooperative efforts have re- sulted in the establishment and adoption of an association stamp or trade mark. In some states, viz., Michigan, Minnesota, Iowa and Wisconsin, with the assistance of their respective State dairy commissioners, the creameries have established State brands. . . Marketing Dairy Butter. — Dairy butter, or butter made on the farm, is sold either direct to the consumer, to private resi- dences, hotels, restaurants, boarding houses, clubs, etc., who 418 MARKETING OF BUTTER pay for it in weekly or monthly cash payments, or it is sold to the local country store which generally pays the farmer in trade and not in cash. The great bulk of dairy butter goes to the country store. This is a most primitive method of marketing butter which results, in the great majority of cases, to the dis- advantage of the dairyman. Selling Creamery Butter Locally.---Generally speaking the best markets are those nearest home. Selling butter locally, either to the direct consumer at the door of the creamery, by going direct to residences, through, public or municipal markets, by parcel post, or selling to local stores, or shipping direct to retail stores in neighboring towns and cities, has many and distinct ad- vantages. It enables the creamery to reduce the number of middle- men to the minimum or to do without them entirely, thereby netting the creamery the consumer's or retailer's price. It saves transportation charges to distant points, which may amount to from 1 to 2 cents or more per pound of butter. It protects the butter against conditions unfavorable to its quality in transit and reduces the interval between manufacture and consumption, thereby enabling the creamery to supply the consumer with butter of better quality and demanding a better price. It gives the cream- ery a better opportunity to put "up its butter in the final pack- age, the print, and under its own brand, thereby establishing a constant trade for its own butter and usually at satisfactory prices. It protects the creamery against loss by shrinkage. In some instances creameries have succeeded in disposing of part of their regular output through what is known as the club-buying system. Clubs whose members are consumers are organized by a local individual in his community. He buys butter regularly and usually in sufficiently large quantity per shipment, to supply all the members of his club. This is a very effective system of reaching the consumer in distant markets direct, but the amount of butter that the creamery can dispose of through this channel is naturally limited. The chief difficulty encountered by the average small cream- ery in establishing and holding local markets lies in the irregu- larity of the amount of its output throughout the year and the fluctuations in the demand and supply of local markets. MARKETING OF BUTTER 419 If the creamery establishes a local market for all of its out- put during the flush of the season, it invariably is confronted with the difficulty of supplying that market during the time of shortage, or if the local market takes care only of the output during the time of shortage, then in summer, during the heavy make, there is a surplus of butter which must be disposed of on the open market. This surplus is usually increased by the fact that during the early summer months, when butter fat prices are relatively low, considerable cream is churned on the farms and the creamery has to compete against country butter, which is usually offered for sale at prices below creamery butter. At the same time also the consumption of butter in the local markets generally reaches ebb-tide, partly because of a reduction of butter consumption per capita during- the hot weather and partly because many of the consumers leave for cooler climes. In order to equalize these fluctuating conditions of sup- ply and demand some creameries are buying butter on the open market during the time of shortage to take care of their trade, while others store some of their surplus during the time of flush. In the buying of butter to offset the shortage of output, the greatest care should be exercised that the quality of the butter purchased is equal to that of the regular make. The creamery should also make sure that it complies with the laws of the state concerning the labeling of such butter. In many states the law prohibits the sale of butter under the creamery's private brand, unless the brand plainly indicates that the but- ter was not made by that creamery. Instead of stating that the butter is made by the respective creamery, the wrapper should state that the butter is packed and distributed by the respective creamery. The storing of butter in the creamery, in order to take care of its surplus and to hold it over for the time of shortage, is usually not a practical proposition in the case of the small creamery Avith limited cold storage facilities. Unless butter can be kept at a uniform temperature of Zero degrees Fahren- heit or below it will, under average conditions, depreciate in value to the extent to where it can no longer be sold to the regular trade. If the butter is made from a good quality of 420 MARKETING OF BUTTER cream it is best stored in a commercial cold storage plant. If it is made from a poor quality of cream, its storage is a risky adventure under any condition. Furthermore, the storing of butter involves the "tying-up" of operating capital which is often beyond the financial resources of the small creamery. Experience has shown that under average conditions of the small creamery, it is safer to dispose of its surplus as soon as possible after making. If the creamery exercises due caution and foresight in making the proper arrangements for the dispo- sition of its surplus on the open market, there is no need of seri- ous loss and it should at least break even with its surplus, pro- vided that the butter is of a quality acceptable to the market where it is sold. Furthermore, November 1, 1917, by Proclamation of the President of the United States, Federal Rules and Regulations went into effect providing that butter, and other food products held in cold storage longer than 30 days shall be marked, either on the butter itself, or on the container, with the words "Cold Storage" and shall be sold as cold storage goods. Similar regula- tions have also become state laws in several of the States. While this ruling, which is a War measure, remains in effect, the creamery may find considerable difficulty to satisfy its trade dur- ing the period of shortage with butter placed into cold storage during the time of flush. June butter, made from butterfat that is produced by the cows during the prime of their lactation period and that are feeding on nature's choicest feed, succulent pas- ture grass, is acknowledged to be superior in flavor. If man- ufactured in the proper manner, it generally is of fully as good quality when it comes out of storage as fresh winter butter which is made largely from the milk of. stripper cows, and cows receiving dry feed. In fact, it often is of a quality distinctly superior to the fresh winter butter. From the standpoint of quality, therefore, cold storage butter may be fully as desirable and appetizing as fresh winter butter, but the fact that the pack- age bears the words cold storage, makes it less attractive to the average consumer, it arouses his suspicion that he is getting an inferior article. For this reason, under the cold storage ruling, the creamery may experience serious obstacles in its efforts MARKETING OF BUTTER 421 to take care of its regular trade during the time of shortage of fresh butter, by offering- it cold storage goods in the place of fresh butter. The large centralized creameries obviously have the ad- vantage in disposing of their output direct to the retailer. Their output is large enough, so that they can afford to establish distri- buting offices in the large markets. Through these distributing offices they are able to reach the retailer in distant consuming centers in a similar way as in the local and home markets. These distributing offices also serve as a channel through which the trend of the market may be accurately followed, and through which that class of trade may be located that has the greatest demand for the quality of butter the creamery produces. Selling butter to the wholesale produce trade. — The dis- tribution of vast quantities of the butter made, is taken care of by an organization of middlemen intermediary between the shipper and the city retail stores. This organization is known as the wholesale trade. The wholesale produce trade occupies an important position in supplying the shipper with a market for his product and in regulating the quantity and quality of the supply of the retail store, in reducing the cost of transporta- tion by making possible shipments in large units, in maintaining the necessary business relations with the retail stores for or in the place of the shipper, and in making possible prompt pay- ments so as to enable the shipper to pay the farmer for his cream without delay. In other words, the wholesale produce trade performs that function which the shippej — the creamery — with- out branch offices in the distant city markets, is unable to ac- complish. It acts as a clearing house for the shipper and re- tailer alike. Its proximity to the distributing channels enables it to feel the pulse of the market in its and other cities and to regulate the influx and movement of the various grades of but- ter and other commodities on the market. The organization of the wholesale produce trade is established in all cities of appreciable size. According to Weld,1 "a city is large enough to require a separate wholesale trade organization when it can handle goods in car lots for consumption in the city 1 Weld, The Marketing of Farm Products, p. 67, 1916, 422 MARKETING OF BUTTER or for redistribution in nearby towns." The wholesale produce trade is always localized in a certain district of the city. Thus in Chicago, South Water Street represents the wholesale produce district for that city. The wholesale dealers may be divided into two classes, to each of which are attributed certain, more or less definitely defined functions, namely the middlemen who receive goods direct from the shipper and the middlemen who buy direct from the re- ceivers and sell to the retail stores or other outlets. To the first class belong the wholesale receiver, the com- mission man and the broker. The wholesale receiver buys the butter outright and pays the shipper for it upon receipt. He sells the butter to the retail store and also to the jobber. The commission man does not buy the butter, he does not become owner of it, but acts as an agent for the shipper, selling it for him to retail stores, hotels, restaurants, and other outlets and deducting from the gross receipts a commission for his ser- vices, together with freight and cartage charges. The rate of commission usually charged to the butter shipper is 5 per cent of the gross receipts. The broker operates on a similar plan as the commission man, but he usually handles goods in larger quantities and charges a lower rate of commission. To the second class, the middleman who buys from the wholesale receiver and not direct from the shipper, belongs the jobber. He also sells to the retail trade. These middlemen have their organization of solicitors who look after the retail trade and other outlets in their city as well as in other cities. Most of the butter shipped to the wholesale trade is de- sired in bulk packages, usually 60 pound tubs or 50 pound boxes for Eastern markets and 68 pound cubes for the Pacific coast markets. In exceptional cases the shippers put their butter up in the finished package, the print. Most of the wholesale receivers have a brand of their own, on which they have es- tablished some fancy trade, and for which they print fancy butter and sell it under their own carton. Methods of Sales. — Butter shipped to the wholesale trade is sold according to any one of the following four methods : MARKETING OF BUTTER 423 1. Track Sales.— By track sale is understood F. O. B. (free on board) shipping point. By this method the responsibility of the shipper ceases when the butter is placed on the car, or on ship board, at the shipping point. The buyer pays the freight, cartage, assumes the risk of transportation and the price is definitely fixed. From the shipper's, or creamery's point of view this is the most advantageous method of selling butter to the wholesale trade. In order to sell butter under this agree- ment the creamery must previously satisfy the receiver of the uniformity of quality, workmanship, composition and color of butter the creamery is capable of supplying. This is usually done by trial shipments. The receiver agrees to pay a definite price, based on market quotations of the leading markets F. O. B. track. The creamery knows exactly what it is going to get for its butter at the time the butter is shipped and payments are made upon arrival of the goods at the market. 2. Delivered Sales, or F. O. B. Market. — In this method of sale the shipper's responsibility ceases when the butter has reached the market of the buyer. The shipper pays the freight, cartage, and assumes the risk of transportation. The price de- pends on market prices on the date of arrival of the goods at the market. Agreements to buy butter on the above basis are usually also entered into upon receipt of trial shipments rep- resentative of the quality of the average run of butter man- ufjactured by the contracting creamery. While not as ad- vantageous to the creamery as method No. 1, because the price is determined at the market end and because the shipper has to pay the freight and assumes the risk of transportation, this method is by far preferable to the commission sales. Both, in method 1 and in method 2, the butter sells at prices based on market quotations. It is important that prices should not be based on the score of the butter. According to methods 1 and 2 the buyer agrees to pay the price stipulated on the basis of market quotations, as long as he is willing to accept the butter. Should the butter of some shipments not measure up in quality to the trial samples, the buyer will still pay the price agreed upon, but will notify the creamery of the defect, so it may be remedied promptly. ,In case the quality continues to be inferior 424 MARKETING OF BUTTER to that of the trial shipments, the buyer may ask the creamery to find another outlet for its butter, or else negotiate another agreement satisfactory to both parties. 3. Commission Sales. — The shipper pays the freight and cartage, assumes the risk of transportation and the commission man acts as an agent to sell the butter for which service he charges the shipper a commission, usually of 5 per cent, of the gross receipts. This method places the shipper at the mercy of the commission man, it deprives him of all control over the re- turns from his butter and it is a method which generally proves very unsatisfactory and costly to the creamery. While there are many reliable and trustworthy men in the commission business, the temptations which surround the com- mission man to abuse his power at the expense of the shipper are very great, and are rinding many a vulnerable spot among their members. Most commission men not only act as agents for the shippers, but usually do also a receiver's business. On an ad- vancing market they are encouraged to buy outright, while on a declining market they are prone to adhere to the commission business exclusively. Not infrequently they charge the shipper a commission on goods they purchase outright and thus receive a commission on their own purchase. The creamery has no guarantee that the returns reported represent the price at which the butter actually sold. A business that offers such unlimited opportunities for illegitimate gain at the expense of the power- less shipper, naturally attracts an element that is no credit to the profession and that jeopardizes the welfare of the shipper. 4. Contract Sales. — By contract sales is meant the method whereby the shipper enters into a contract with the dealer agree- ing to deliver a certain number of pounds of butter per week at a price based on market quotations. The contracts are usually short-term agreements and are largely, though not always, con- fined to the storage season. Contract sales are usually taken advantage of by large creameries. Small creameries with a lim- ited and often uncertain output are seldom in a position to ne- gotiate such sales and, when consummating them, they are liable to find serious difficulty in fulfilling their agreement. MARKETING OF BUTTER 425 Speculating in Futures. — Buying or selling for future de- livery is not as common in the butter business as on the grain market, though ,it is participated in to a limited extent by the speculative element in most markets. The purpose of buying for future delivery is based on the hope of the buyer to sell at a higher price at the time of delivery, thereby making a profit. The object of selling for future delivery lies in the assumption of the seller that he may be able to buy at a reduced price and thereby reap a profit. It is obvious that buying and selling for future de- livery is purely a speculative transaction which may yield profit- able returns, but which involves the usually high risks char- acteristic of all speculation. Methods of Payment. — As previously stated, dairy butter sold direct to customers or by parcel post, is usually paid for by cash on delivery. In the case of hotels, restaurants, etc., the dairy farmer usually collects weekly or monthly and sometimes at the end of the season. Dairy butter sold to the country store is generally paid for in trade. Creameries selling direct to retail stores make their collec- tions weekly or monthly. In the case of doubtful customers it is advisable to demand remittance with the order or to deliver the butter C. O. D. Payments for shipments to the wholesale trade in distant markets involve more or less delay. If butter is sold on com- mission, usually several weeks elapse before the returns arrive and even in the case of "track sales" and "delivered sales" several days and often one to two weeks are required for the payments to arrive. In the meantime the farmers have to be paid and the supplies and package have to be purchased. This is often too great a financial strain on the creamery whose operating capital is generally exceedingly limited. This difficulty is most commonly taker! care of by permis- sion, on the part of the wholesale receiver or the commission man, to allow the shipper to draw on him to the extent of a large portion of the shipment of butter at the time of shipment. The creamery attaches a draft to the bill of lading and the receiver or commission man settles for the balance upon arrival of the goods or upon their sale, respectively. Banks that pay interest on the balance of the creamery account, invariably discount these 426 MARKETING OF BUTTER drafts. Banks that pay no interest on the creamery balance, fre- quently accept the drafts without discounting. Butter Exchanges. — The butter exchange is a voluntary trade organization of wholesale dealers in butter. In many cases the exchange is not confined to butter alone, but includes other allied commodities, such as cheese, eggs, poultry, etc. Specific examples of produce exchanges of dealers in butter or butter and allied commodities, whose operations are recognized as having the greatest influence upon the marketing of butter in this coun- try, are: The New York Mercantile Exchange, New York City, N. Y. The Chicago Butter and Egg Board, Chicago, Illinois. The San Francisco Wholesale Dairy Produce Exchange, San Francisco, California. The Elgin Board of Trade, Elgin, Illinois. The Boston Chamber of Commerce, Boston, Massachusetts. These produce exchanges are generally incorporated associa- tions. Weld1 enumerates the primary functions of the produce exchange as follows: "1. To provide a convenient market or trading place. 2. To regulate business dealings of members. 3. To provide a system to facilitate the settlement of trade disputes. 4. To establish uniform grades and a system of inspection. 5. To acquire and to disseminate market information." The specific objects and functions of the different exchanges cover a varying range. The charter of the New York Mer- cantile Exchange, for instance, records the following ob- jects of the 'Association : "To provide and regulate a suitable room or rooms for an exchange in the City of New York; to foster trade; to protect it against unjust or unlawful exactions; to reform abuses; to diffuse accurate and reliable information; to settle differences between members ; to promote among them good fellowship and a more enlarged and friendly intercourse; and to make provision for the widows and families of deceased members." The realization of its objects and the safeguarding of its pol- icies is accomplished by the careful supervision of admission of new members. 1Weld, The Marketing of Farm Products, 1916. MARKETING OF BUTTER 427 The "Call."— One of the important features of the butter ex- change is the "Call." Weld defines the "Call" as "a device for making bids and offers, partly to establish market prices or quotations and partly to bring about actual sales." In the larger markets, such as New York, Chicago, etc., the traders assemble each day at a fixed hour (at 10 a. m. in New York and Chicago) for the "Call." The "Call" is usually con- ducted in a room with a raised platform at one end for the chairman, and a blackboard at the back, on which are recorded receipts of the day, general market conditions and the bids and offers made under the call. After the offers for sale made by the traders, including quantity, quality and price, are posted on the blackboard, bids are called for. The bids are also posted. The members of the Exchange appear on the floor and buyers and sellers make public bids on the offers of butter. Often these bids and offers result in sales and these sales show in a public manner the prices at which receivers are willing to sell their butter and the prices at which buyers are willing to purchase it. The bidding under the "Call" affords competitive sellers an, opportunity to sell butter against each other according to the supply. Should there be more demand for butter on any one day at a price above the quotation of the previous day, the quo- tation will be advanced to such a point as buyers are paying for the butter, for the buyers will not stand for any quotation that is lower than the price they are actually paying for butter. The same principle applies to the sellers. Should the sellers be loaded down with butter, it is their privilege to offer it at such prices at which and until the buyers will take hold, and often- times with the market stocked with butter, it is necessary to sell it at prices where the retailers will be able to reduce their selling price to the consumer. In this way the consumer be- comes interested in consuming more butter and the surplus stock becomes disposed of. The actual sales and purchases made under the "Call" are few. According to Eschenbrenner1 they sometimes do not ex- ceed 5 per cent of the daily receipts of butter, the primary object of the "Call" being to feel market conditions rather than make specific sales. The present tendency of the butter trade 1 Eschenbrenner, New York Produce Review, April, 1916. 428 MARKETING OF BUTTER is toward conducting its transactions through the medium of private sales. The great bulk of butter handled by members of the Exchange is not sold under the "Call," but by private deals between buyers and sellers. This situation is largely the result of the increasing differentials of grades and the develop- ment of special markets for special grades, for which butter from special creameries is demanded. The "Call," however, serves in many instances as a convenient means for the seller who has a surplus, to find a buyer and for the buyer in case of shortage of any particular grade of butter to locate a seller of that grade. Considerable trading is also usually done privately between members at the conclusion of the "Call" and before the meeting adjourns. Butter Quotations. — The problem of determining butter quotations is a subject of the greatest importance to the entire butter industry. Butter quotations, in order to be correct, should coincide with the actual market value of the butter. They should therefore be determined by the supply and demand of butter, otherwise they may be conducive of serious disturbances in the normal movement of butter on the market, which disturbance^ are bound to operate against the best interests of the butter business. Limited space does not permit here a detailed discussion of the multitude of agencies through which price quotations are established, but the importance of the subject justifies a brief reference to the prevailing systems of determining butter quo- tations in a few of the leading butter markets of the country. These references are confined here to the New York, Chicago and Elgin quotations. Formerly the New York and Chicago quotations were de- termined by a committee of the New York Mercantile Exchange and the Chicago Butter Board, respectively. These committees, consisting of dealers, being in most intimate touch with the market and with the actual market value of the butter, were as- sumed to be admirably qualified to arrive at just and correct quotations. They met each day at the conclusion of the "Call" behind closed doors. "This same practice obtained abroad and even in Denmark butter quotations decided upon by the Copenhagen merchants MARKETING OF BUTTER 429 are still largely used as a basis of settlement with creameries. But in this country quotations made by price committees of merchants have not been looked upon with favor by govern- ment officials, especially when they did not accurately repre- sent prevailing values, and it was usually found that the tend- ency of most price committees of merchants was to keep the official quotations below prevailing selling values. Several of our trade organizations were thus forced by the government to discontinue the so-called official quotations, but some still con- tinue the practice."1 In 1907 the Mercantile Exchange of New York was sued by the Government on the ground of fraudulent manipulation of quotations, with the result of prohibiting the Exchange from issuing quotations not representing the value of butter based on actual sales by first hand receivers. In a decision rendered by the Supreme Court it was decided that this quotation committee was a combination in restraint of trade and the practice was decided to be illegal. Realizing that the actual sales under the "Call" of the Exchange were too small to justify the basing of quotations on these sales, the Exchange discontinued the issu- ance of official quotations and the determination of price quo- tations was assumed by outside market reporters. Since then the firm of Urner-Barry Company, with the help of a most efficient force of trained market reporters, has as- sumed the responsibility of establishing daily price quotations in New York. After the "Call" each day, having taken into con- sideration the bids and offers under the "Call," the market re- porter makes a canvass of the market, calling on the buyers and sellers and ascertaining the prices at which they are doing busi-* ness through private negotiations; then, at about noon each day he announces the quotations .he will publish in his paper for the various grades of butter. These quotations are accepted as the settling basis for the day and these are the quotations that are sent broadcast throughout the country. In Chicago the quotation committee met a similar fate, the courts prohibiting its functions, unless quotations were made on the basis of actual sales, and the making of butter quotations passed into the hands of outside market reporters. 1 Making Quotations — Comments, The Buttermakers' Discussion Club, New York Produce Review, July 12, 1916. 430 MARKETING OF BUTTER The Elgin Board also changed its method of determining quotations to issuing them on the basis of actual sales made at weekly meetings of the board. In some markets, however, the committee system of issuing quotations still prevails. The chief reason why quotation committees proved unsat- isfactory and which led finally to their discontinuation in Chi- cago and New York was the fact that these committees repre- sented largely only the wholesale receivers. The receiver nat- urally is interested in buying as cheaply as possible and this created a tendency for the establishment of quotations lower than the actual sales value of the butter, with its undesirable results on the market, such as dissatisfaction among retailers who could not understand the great difference between the prices they had to pay and the butter quotations of the commit- tee, it also invited the practice of paying premiums to the ship- per, etc. The exceedingly small sales on the floor of the Exchange did not justify the price determinations on the basis of the actual sales of the Exchange, hence the only logical alternative ap- peared to be for the Exchange to turn the responsibility of mak- ing price quotations over to independent market reporters. In the case of the Elgin quotations the discontinuation of the Elgin board would have meant the discontinuation of Elgin quota- tions, because the Elgin market itself is a negligible quantity, so the only means to save the Elgin quotation was to comply with the order of the courts and issue quotations on actual sales by the board, in order not to deprive the large sections of the country doing business on the Elgin basis, of the Elgin market to which they have become accustomed as a trading basis. It is obvious that the market reporter, assuming the re- sponsibility of making price quotations, is thus vested with vast powers, the abuse of which for his own interests, or through incompetence, would throw the market into a most chaotic con- dition. In the first place, the market reporter must be a man of ability, experience and judgment. He gets his information by going around among the trade and must be able to distinguish between gossip and facts and between fiction and the truth. Aside from the condition of supply and demand he must cope with the difficulties of the influence on the demand for and sup- MARKETING OF BUTTER 431 ply of storage butter, on the market value of fresh goods, and he must above all be a man of superior integrity, honesty and disinterestedness. Inspection and Grading. — Upon its arrival in the wholesale receiver's hands the butter is inspected and graded. Butter deal- ers have agreed to a standard score card with 100 points as the basis for perfection, and giving certain values to flavor and odor, body and texture, color, salt, and package. Most butter exchanges in the larger markets have an offi- cial inspector of butter, whose services are available to the mem- bers of the exchange, for compensation. Butter so inspected is branded with the official stamp of the exchange. The inspector of the New York Mercantile Exchange has a stamp of different shape for each main grade, so as to facilitate the recognition of the grade by the stamp. The great bulk of the butter re- ceived by the wholesale distributors of the larger markets is not subjected to an official inspection by the inspector employed by the wholesale trade organization. Sales, on the negotiation of which official inspection is not requested, are commonly spoken of as being "over-the-trier." The inspection service maintained by the Exchange is largely, if not entirely, for the purpose of in- specting those lots of butter of which inspection is requested by the butter, when purchased under the "Call," as for instance in the case of dispute between the seller and buyer as to grade, or in the case of butter sold to the Government. When, in the opinion or judgment of the buyer the butter he receives does not conform in quality with the grade he pur- chased under the "Call," he has the privilege to apply for the services of the official inspector. If the decision of the inspector is not acceptable to either or both of the contracting parties, an appeal may be made from the decision of the inspector, to the chairman of the Butter Committee, who then appoints three members from that committee to inspect the butter in dispute. They report their results to the Superintendent of the Exchange. The decision of this subcommittee is final. While there are minor variations in the grades and grading of butter on the different markets, as a whole the classification of grades is very similar in the principal markets throughout the country. 432 MARKETING OF BUTTER BUTTER RULES OF THE NEW YORK MERCANTILE EXCHANGE.1 Classifications — Grades and Scores. 1. Butter shall be classified as Creamery, Renovated, La- dles, Packing Stock and Grease Butter. Definitions. — 2. Creamery. — Butter offered under this class- ification shall have been made in a creamery from cream sepa- rated at the creamery or gathered from farmers. 3. Renovated. — Butter offered under this classification shall be such as is made by melting butter, clarifying the fat there- from and rechurning the same with fresh milk, cream or skim- milk, or other similar process. 4. Ladles. — Butter offered under this classification shall be such as is collected in rolls, lumps, or in whole packages and reworked by the dealer or shipper. 5. Packing Stock. — Butter offered under this classifica- tion shall be original farm-made butter in rolls, lumps or other- wise, without additional moisture or salt. 6. Grease Butter shall comprise all classes of butter grad- ing below thirds, or of packing stock grading below No. 3, as hereinafter specified, free from adulteration. Grades. — 7. Creamery. Renovated and Ladles, shall be grad- ed as Extras, Firsts, Seconds and Thirds; and Packing Stock shall be graded as No. 1, No. 2 and No. 3. Definition of Grades. — 8. Grades of Butter must conform to the following requirements. Extras. — 9. Shall be a standard grade of average fancy qual- ity in the season when offered under the various classifications. Ninety per cent, shall conform to the following standard; the balance shall not grade below Firsts : Flavor. — Must be sweet, fresh and clean for the season when offered if Creamery, or sweet, fresh and reasonably clean if Renovated or Ladles. Body. — Must be firm and uniform. Color. — Not higher than natural grass, nor lighter than light straw, but should not be streaked or mottled. Salt. — Medium salted. 1 Secured through courtesy of New York Produce Review and Am. Cream- ery, April, 1919. MARKETING OF BUTTER 433 Package. — Sound, good, uniform and clean. Firsts. — 10. Shall be a grade next below Extras and must be good butter for the season when made and offered, under the various classifications. Ninety per cent, shall conform to the following standard ; the balance shall not grade below Seconds : Flavor. — Must be reasonably sweet, reasonably clean and fresh if Creamery or Renovated, and reasonably sweet if La- dles. . Body. — Must be firm and fairly uniform. Color. — Reasonably uniform, neither very high nor very light. Salt. — May be reasonably high, light or medium. Package. — Sound, good, uniform and clean. Seconds. — 11. Shall be a grade next below Firsts. Flavor. — Must be reasonably good. Body. — If Creamery, must be solid boring. If Ladles or Renovated, must be ninety per cent, solid boring. Color. — Fairly uniform, but may be mottled. Salt. — May be ' high, medium or light. Package. — Good and uniform. Thirds. — 12. Shall be a grade below Seconds and may con- sist of promiscuous lots. Flavor. — May be off-flavored and strong on tops and sides Body. — Not required to draw a full trier. Color. — May be irregular or mottled. Salt. — High, light or irregular. Package. — Any kind of package mentioned at time of sale. 13. (For grades higher than Extras see paragraph No. 25.) No. 1 Packing Stock. — 14. Shall be sweet and sound, packed in large, new, or good uniform second-hand barrels, having a wooden head in each end, or in new tubs, either to be parchment paper-lined. Barrels and tubs to be packed full. No. 2 Packing Stock. — 15. Shall be reasonably sweet and sound, and may be packed in promiscuous or different kinds of barrels, tubs or tierces, without being parchment paper lined, and may be packed in either two-headed or cloth-covered bar- rels. No. 3 Packing Stock. — 16. Shall be a grade below No. 2, and may be off-flavored, or strong; may be packed in any kind or kinds of packages. 434 MARKETING OF BUTTER 17. Charges for inspection of Packing Stock shall be the same as the rules call for on other grades. 18. Mold. — There shall be no grade for butter that shows mold. Known Marks. — 19. Known marks shall comprise such but- ter as is known to the trade under some particular mark or des- ignation and must grade as Extras or better if Creamery or Ren- ovated, and as Firsts or better if Ladles in the season when of- fered unless otherwise specified. Known marks to be offered tin- der the call must previously have been registered in a book kept by the Superintendent for that purpose. If Renovated, the fac- tory district number and statement be registered. Scoring. — 20. The standard official score shall be as follows and shall apply to Creamery Butter only : Flavor 45 points Body 25 points Color 15 points Salt 10 points Style 5 points 100 points 21. Extra Creamery may score either 91, 92 or 93 points at the discretion of the Butter Committee, who shall determine the required score from time to time in such manner that it shall represent an average fancy quality in the season when offered. But butter scoring more than required for Extras shall be de- liverable on a contract for Extras, and may be branded as such at the request of seller, or buyer. Any change in the Standard score required for Extras shall, after authorization by the Butter Com- mittee, be announced by the caller at the opening of the next regular call and posted upon the bulletin board of the Exchange and be effective 24 hours later. 22. The minimum score of Firsts shall, at all times, be 4 points below the score required for Extras. 23. The minimum score of Seconds shall be 5 points below the minimum score required for Firsts. 24. The minimum score of Thirds shall be 7 points below the minimum score required for Seconds. MARKETING OF BUTTER 435 BUTTER RULES OF THE CHICAGO BUTTER AND EGG BOARD.1 Packages to be Used. Creamery, Centralized Creamery or Held Butter: — Tubs — hardwood about sixty (60) pounds standard, White Ash with wood — or satisfactory metal hoops, or boxes of sat- isfactory material; thickness of material shall not be less than 9/16" for sides and ends and 5/16" for tops and bot- toms ; boxes shall have net capacity of not over seventy (70) pounds or less than sixty (60) pounds. All tubs or boxes should be paraffined and lined with parchment paper. Ladles Tubs or boxes. Renovated Tubs or boxes. Packing Stock Any size or style of package. Grease Butter Any size or style of package. Classifications, Grades and Scores. 1. Butter shall be classified as Creamery, Centralized Cream- ery, Held Butter, Renovated, Ladles, Packing Stock and Grease Butter. Definitions. 2. Creamery. Butter offered under this classification must be made in a creamery. The cream shall either be separated at the creamery or hauled direct to the factory from the farms. 3. Centralized Creamery. Butter offered under this classifica- tion must be made in a creamery. Cream used in the man- ufacture of this butter may be gathered direct from the farmers or shipped in from cream stations. 4. Held Butter. Butter offered under this classification shall be butter that has become Cold Storage Butter by virtue of the laws of the United States or of the State in which such butter is sold. 5. Renovated. Butter offered under this classification shall be such as is made by melting butter, clarifying the fat1 therefrom and re-churning the same with fresh milk, cream, or skimmilk, or other similar process. 1 Secured through courtesy of Chicago Dairy Produce, April, 1919. 436 MARKETING OF BUTTER 6. Ladles. Butter offered under this classification shall be such as is collected in rolls, lumps, or in whole packages and re-worked by the dealer or shipper. 7. Packing Stock. Butter offered under this classification shall be original butter without additional moisture or salt, from creamery or dairy (but may be from miscellaneous sources), which has been collected in any quantity and packed in barrels, tubs or other containers. It must be of quality fit for human consumption as food and free from adulteration. 8. Grease Butter. Butter offered under this classification shall consist of all grades of butter below thirds. If Pack- ing Stock, below No. 3, free from adulteration. Grades. 9. Creamery, Centralized Creamery and Held Creamery shall be graded Extras, Standard, First, Seconds, and Thirds; Renovated and Ladles as Firsts and Seconds; and Packing Stock as Number 1, Number 2. and Number 3. 10. Grades of butter must conform to the following require- ments : Extras. 11. Shall be a grade of creamery of average fancy quality in the season when offered under the classifications. Ninety per cent shall conform to the following standard, the bal- ance shall not grade below ninety points: Flavor: Must be sweet, fresh and clean for the season when offered in Creamery, and sweet a,nd clean in Held. Body: Must be firm and uniform. Color: Must be either light straw color, medium or high, but must be uniform and neither streaked, or mottled. Salt: May be defined as light, medium or high, but must not be gritty. Package: New, sound, good, uniform and clean. Standards. 12. Shall be a grade of centralized creamery of average fancy quality in the season when offered. Ninety per cent shall conform to the following standard and the balance shall not grade below eighty-nine points: MARKETING OF BUTTKR 437 Flavor: Must be sweet, fresh and clean, and sweet and clean if Held. Body: Must be firm and uniform. Color: Must be either light straw color, medium, or high, but must be uniform, and neither streaked nor mottled. Salt: May be denned as light, medium or high, but must not be gritty. Package: New, sound, good, uniform and clean. Firsts. 13. Shall be a grade below Extras and must be good butter for the season when made and offered under the classifica- tions. Ninety per cent shall conform to the following stand- ard, the balance shall not grade below eighty-seven score : Flavor: Must be reasonably sweet, reasonably clean, and fresh if Creamery, Centralized Creamery, Renovated, and reasonably sweet and clean if Held. Body: Must be firm and fairly uniform. Color: Reasonably uniform, neither very high nor very light. Salt: May be light, medium or high. Package: New, sound, good, uniform and clean. If Ladles, must be ninety per cent solid boring, color rea- sonably uniform and package sound and clean. Seconds. 14. Shall be a grade below Firsts. Flavor: Must be reasonably good. Body: If Creamery, Centralized Creamery, or Held must be solid boring. If Renovated or Ladles, must be ninety per cent solid boring. Color: Fairly uniform, but may be mottled. Salt: May be light, medium or high. Package: Good and uniform. Thirds. 15. Shall be a grade below seconds and may consist of promis- cuous lots. Flavor: May be off flavored and strong on tops and sides but not rancid. Body: Not required to draw a full trier. Color: May be irregular or mottled. Salt: High, light or irregular. Package: Any kind of package men- tioned at the time of sale. No. 1 Packing Stock. 16. Shall be original butter without additional moisture or salt, sweet and sound, packed in barrels, or in tubs or boxes, to be parchment paper-lined ; packages to be packed full. 438 MARKETING OF BUTTER No. 2 Packing Stock. 17. Shall be original butter without additional moisture or salt, sweet and sound, may be packed in different kinds of bar- rels, tierces, pails, tubs or boxes; may be without paper lining. No. 3 Packing Stock. 18. Shall be a grade or quality above Grease butter and packed in any kind or all kinds of packages. Scoring. 19. The standard official score for salted butter shall be as fol- lows: Flavor 45 points Body 25 points Color 15 points Salt 10 points Style 5 points 20. The standard official score for unsalted creamery butter shall be as follows : Flavor 45 points Body 30 points Color 15 points Style 10 points Extras. 21. Shall consist of a grade of butter scoring ninety-two points or better. Standards. 22. Standards shall consist of the highest grade of Centralized Creamery made during the season when offered and shall score ninety points or better. Firsts. 23. The minimum score of Creamery Firsts shall at all times be four points below the score required for Extras. Seconds. 24. The minimum score of Creamery Seconds shall be four points below the minimum score required for Firsts. Thirds. 25. The minimum score of Creamery Thirds shall be five points below the minimum score for Seconds. MARKETING OF BUTTER 439 Distribution. — The distribution of butter to the retail trade on the large markets is a class of work which is the business of the jobber. The jobber buys from the wholesale receiver, com- mission merchant or broker and sells to retail stores, hotels, res- taurants, steamship companies, Pullman car companies and other retail outlets. The jobbers are also frequently termed re- tailers because they sell to the retail stores. Jobbers who have no established place of business but load the goods they buy from the wholesale receivers on their wagons and peddle them among .the retail stores, are called "wagon men." In reality the jobbers are not the only middlemen who dis- tribute the butter to the retail men. Many of the wholesale re- ceivers and of the commission men also sell to the retail trade. While some of the butter is sold from the wagon direct to the hotel and restaurant trade, and through other similar di- rect outlets, the great bulk of the butter reaches the consumer through the medium of the grocery store. The houses selling to the retail trade have in their employ a force of salesmen canvassing the city. They call on the grocery trade at regular intervals, such as once per week, soliciting their business. The houses selling to the retail stores are very numerous in the large markets and competition is usually very keen, so that constant soliciting is indispensable in order to hold the trade. As previously stated, the butter passes through the hands of several middlemen, first the railroad, then the wholesale receiver, or the commission man, then the jobber and finally the retail store. When the wholesaler sells direct to the retailer the job- ber drops out of the chain of steps through which the butter moves in its passage from the creamery to the consumer. Occa- sionally the broker also enters into the chain of agencies through which butter passes. The broker handles large quantities only, he does not take possession of the goods but acts in a similar capacity as the commission man, and his overhead expense is very low. He is therefore able to handle butter at a very low rate of commission, usually not over J of 1 cent per pound. He may represent the buyer or the seller. His services are en- gaged most often when the buyer or seller is located at a great distance from the place where the butter is to be bought or 440 MARKETING o£ BUTTER sold, and the party who is trying to buy or sell is not familiar with prospective customers in the distant market. Frequently the wholesale receivers or the commission men have their butter printed by the so-called ''butter cutters." These men have the equipment for printing butter and receive a small commission for their services. Again, there are firms with chain stores, whose buyers may purchase their entire supply of butter from the wholesale receiver, or the commission man. Finally, there is the speculative buyer of butter. He may be a part of the butter business, the creamery, the wholesale re- ceiver, the commission man, the jobber, etc. But quite often he belongs to a class generally not handling butter as a main business, but largely or wholly only for speculation on the side. Thus, especially during the storage season, when butter prices are at ebbtide, individuals in diverse walks of life, buy butter and put it in storage with the hope of reaping a profit when butter prices are high. This type of speculative buyer represents an ele- ment that does not usually add stability to the butter business. He is interested largely only in temporary private gain, in making a little "easy money." When the market unexpectedly weak- ens, he generally becomes panicky and pours his holdings ou*t on the market, causing a further weakening of prices, which in some cases may result in a slump of the market to the tem- porary detriment of the butter industry This in turn usually discourages this class of butter buyers and often rids the busi- ness of much of the speculative element for several years. Consumption of Butter in the United States and in Other Countries. — According to T. R. Pirtle,1 Statistician United States Dairy Division, there was prior to the World war, a steady increase in the consumption of butter throughout the world, and the countries of small butter production had been importing increasing amounts of butter year by year. Exceptions to this general statement are the United States which has shown a decrease in consumption since 1900, the Netherlands since 1903 and the United Kingdom since 1906. The following figures, secured from Mr. Pirtle's article show the per capita butter consumption by years in the United States and in other countries. 1 Pirtle — The Consumption of Butter in the U. S. and in Other Countries, The Milk Magazine, Vol. IT, No. 6, 1919. MARKETING OF BUTTER 441 Table 61. — Per Capita Annual Consumption of Butter in the United States by Years. All Butter Creamery Butter Year Pounds per Capita Year Pounds per Capita 1850 12.9 14.5 13.3 15.2 18.8 19.6 17.5 16.5 14.0 1890 2.4 5.3 6.3 6.8 8.0 7.3 6.9 7.6 1860 1900 1870 1904 1880 1909 1890 1914 1900 1916 1909 1917 1914 .. 1918 1918 . Table 62. — Per Capita Annual Consumption of Butter by Countries. Country Date Pounds per Capita Australia 1913 256 New Zealand 1914 21 7 Denmark 1914 190 United Kingdom 1906 190 United States 1909 175 Canada .....' 1911 163 Norway 1906 140 Netherlands 1912 11 3 Switzerland France 1906 1906 11.0 80 Italy 1913 25 Argentina %. 1913 1 7(J) Union of South Africa Germany 1916 2.0 (2) (3) Austria (4) Egypt (B) Hawaii O Japan O China .. . : . . (8) 1 Represents consumption of factory butter only. 2 Estimated. 8 It is generally understood that consumption of dairy products in Ger- many is large. Imports of butter in 1911 exceeded 120,000,000 pounds, but no records are available to establish per capita consumption. 4 No record available of total production. Imports in 1913 were 14,000,000 pounds and exports 2.000,000 pounds. 5 Consumption very small. 6 1900 record suggests less than one pound per capita. This was im- proved to about five pounds in 1918. 7 Very little butter is consumed except by the foreign population; how- ever, use is increasing and becoming more general. 8 Butter not used by Chinese except by a small but growing number of wealthier classes. Normal consumption of butter estimated at 2,000,000 pounds per annum. 442 MARKETING OF BUTTER EXPORTS AND IMPORTS. The following table shows the pounds of butter exported from and the pounds of butter imported into the United States from 1852 to 1918, inclusive: Table 63. — Exports and Imports of Butter for the United States 1852-19181 Year ending June 30, Exports pounds. Imports pounds. 1852-1856 2,781,510 6,793,614 21,625,165 2,858,578 5,527,762 39,481,907 17,681,492 16,685,391 12,150,434 23,758,629 14,609,637 6,601,489 7,341,923 12,544,777 6,463,061 5,981,265 3,140,545 4,877,797 6,092,235 .. 3,58b,600 3,693,597 9,850,704 13,487,481 26,835,092 26.194.4152 1,612,671 2,484,819 2,978,951 5,257,975 D D 246,631 202,883 91,224 47,421 321,038 847,351 2,914,234 441,755 780,608 646,320 1,360,245 1,007,826 1,025,668 1,162,253 7,842,022 3,828,227 712,998 523,573 1. 655.467s 1857-1861 1862-1866 1867-1871 1872-1876 1877-1881. 1882-1886. 1887-1891 1892-1896 1897-1901.. . 1902-1906. 1907-1911 1912-1916 By years : 1907.. .. 1908 1909 1910 1911 1912 1913 1914 1915 1916. . 1917 1918. . Exports. — The butter export trade of the United States has so far been very limited in amount and value of butter, con- sidering the vast expanse of this country and the great develop- ment of our dairy industry. The annual butter exports within the last 60 years have varied from two million pounds to thirty- nine million pounds, as compared with over two hundred mil- 1 Annual Report, U. S. Department of Commerce and Labor. These figures represent twelve months, ending June 30. D. Included in other Packing House Products. 2 These figures represent twelve months, ending December 31. MARKETING OF BUTTER 443 lion pounds exported by the little country of Denmark with an area of less than 16,000 square miles and a population of only two and one-half million people. During and since the World war there has been a marked and growing increase in the amount of butter exported by the United States, and the great shortage of butter and other fats in Europe suggests that this increase may continue until the de- pleted stocks of butter on the European continent are again replenished. Jn considering the immediate future of the butter- export trade the fact should not be lost sight of that the neutral dairy countries, such as Denmark, Holland, Sweden and Norway, whose decrease in dairy products during the war was due not so much to decrease in cow population, but to diminished pro- duction per cow because of shortage of dairy feed, are now rapidly approaching normal production again, and are in a posi- tion to export to the butter-poor countries of the European con- tinent. Prior to the war our butter exports to countries of the North American continent went largely to Canada, considerable portions were also shipped to the Central American countries, Bermuda, British Honduras, Mexico, Newfoundland and Labrador. Of the European countries England received the lion's share, while minor portions went also to Scotland, Germany, Denmark, Bel- gium, the Netherlands, Spain, the Azores and Turkey in Europe. The chief exports to Oceania went to Australia and the Philip- pine Islands. Of the South American countries Venezuela re- ceived the largest portion, while British and French Guiana, Colombia, Chile, Peru, Brazil, Bolivia, Argentine and Ecuador were recipients of smaller amounts. In Asia our export trade was confined largely to China, Hongkong and Japan. In Africa, American butter went largely to the Belgian Congo and British West and South Africa. During and since the war large ship- ments of butter have been consigned to the countries of the European continents, 444 MARKETING OF BUTTER » -H (M 00 O 1-1 00 (X) r- 1 »O l> 1— 1 Tt< 1 - t- O5 tO CO 00 • i— 1 O O5 r-H CO s M aJ 05 CO r-H ,-lb, T-t M IO O5 CO O »O • Ci 1 OO 00 to O CO 1^ l^rJH ^00 i-t CO 05 'o co co oo 05; t^" to a I-H !>• CO CO ^s to Q 05 c/i »H r-H C^l S • T-H Tf< S 05 t^ CO CO O5 CO • -4-> 3 w T-H ,— 1 O CO CO O O5 tO r-H f"* CO "^ ^ 1 1—1 *§ CO CO CO t^OO • CO O5 CO tO O • CO •*•» '•4-t CO 1 r-H 05 l^ "* l^ O o" « 1 (d 1 PH O5~ t>- i-H CO CO CO t>- to CO CO ' l^ CO CO "* .' oo" « »^ rjn CO r-H O5 o i— 1 r-H co" 3 1 tO O tO O 00 to T-H tO CO O5 CO CO oq_ >> c ri O5 O CO OJ OO CO CO t^ O5 !>- CO CO O r-l 00 TjH t^ r^ CO •— 1 r-H co" o" to" co" T-" J,^ JO CO CO OO OO CO co" V o 1 ^ 'o 00 ^ CO CO CO tO •4^ -t-1 2! Q COr-H oo CO V 4-» s Q 1> r-H 1> PQ O5 w o oo co co t"» o fe 3 •4-» 05 w OO CO >O CO OO O5 O5 CO 00 r-H O OO CO rr-* 'd tO CO CO O5 t^» CO to ¥U CO •* »O IO r-H O 0 ^ § 1 CO t^ 10 t^ to to co to co cot- to CO* 05 CO 1 § 3 *w c co"co"o"oo"co" 05 CO 00 CO ^H l> t>- CO i— i O5 00 J_, • !>. CO CO r-H o CO r^ PQ o^ i-H entries c 05 Pounds tO O CO to OO O CO O5 OO I— r-H O O OO »O IO r-H Tf l>- O tO r— ( 00 r-l 00 cq_ oo 3,585,600 1 W» •d ^ g 0 13 ^ i-H 05 r— 1 CH "^ OO • 1>» O5 to i-H CO • t^ -HH OO t^. to ' CO O IOCO . r-l r^ 1,162,253 0 O d .t>? *t) Dollars to CO CO CM (M r-H 05 CO CO OCO »0 O^ i"H *O O5CO r-l 1,468,432 4-» r"1 «5 a 6 >> Dollars 00 CO • TfH O5 • TjToT ' to oo" 050 .1-1 T-H ; tO 1 r-r. 05 •a •<*l t^ 00 O5 t— O CO to O CO T*H C<5 to CO 2o> , J5 05 •8 CO O • CO CO • O5 CO • to O • tOCO r-U-- • CO I-H S CO CO t— !>• CO co" o ^ 2 oTof ' 05" iC • to" 2 8, CO IO r-l O5 00"* i- § to S £ co co : toco . CO CO o CO r-H CO* t« «^_ r-H g E »O OO t-~ Tfl r-H t^ IO r-H IO r-H CO CO CO o 2 CO to • CO to O5 tO to • CO O CO £ 03 to to oo co 05 co "* 00 ^> 03 O5 CO • CO to 05 co" t^*" co" "^~ 05 tn T—Tco" • fp £^ K^ & § CO to CO o 0 ex 1 COOO : r-l T-H CO W ,_, r— 1 c *""] I 05 w OO r-H O5 O5 tO tO OOt^OOO r-H CO 0 1 O5 w CO CO • to OO l> COCO • O CO CO CO 'g t^ r-l tO CO r-l 00 t>^ <-< CO tO • 00 CO oo O § 05 00 CO 05 CO CO'* r-H CO {f 1 m u O CO to Oi O5 TJH TJ< ; t^ co fe' 4) £H CO^OO I>- °^ vo PH "^ T~l ^ S co" T^ r— * •Q 03 • • ; O • O3 .J H 0) tu ; • fe • • 1 ^i ;'g-g ; ; \ le 4! ••- S o .2 c ' • «? a c S '. o3 H L« 3 Sj J • '1 ea" O a3 *^ _j CJ 15 IP J_o "3 w ^ W O C/2 *^< "^ £ c HH < £ MARKETING OF BUTTER 445 Quality of Butter Exported.1 — Prior to the European war the great bulk of butter exported by the United States has been of the lower grades. This is due in part to the fact that the surplus butter available for export has consisted of the poorer grades, partly because there is always a large demand in our home markets for our better grades and a disposition of our high class trade to pay higher prices for the best butter than can be obtained in foreign markets, and partly because many foreign markets, including the English markets, do not demand our highest grades, as the poorer classes in many of the larger for- eign cities cannot afford to purchase our best grades. For this class of trade, therefore, an inferior quality of butter is exported. The quality of butter for export, therefore, is largely dependent upon the class of trade and the purpose for which the butter is to be used. The fact is that before the war the export business was al- most wholly on Renovated and Baking butter. Since the be- ginning of the war, however, the export business has been largely on butter scoring 90 to 92 points. While the difference in price for butter between foreign and domestic markets will always remain the governing factor in the quality and quantity of butter exported, it is to be hoped that, with the systematic improvement in the quality of Ameri- can butter, the development of foreign markets for our highest quality of butter may grow more rapidly in the future than it has in the past and that our total exports may assume pro- portions consistent with the vastness of the butter industry at home. Imports. — The annual imports into the United States of foreign butter have averaged very materially less than the ex- ports. The extreme variations of annual imports ranged be- tween 6,821,696 pounds of butter in 1868 and 23,700 pounds in 1899. Since the year 1884 and up to 1909 they amounted to less than one million pounds annually. Beginning with the year 1910 the annual imports exceeded one million pounds. The imports fluctuated largely with the domestic butter quotations and the rate of tariff on foreign butter. During the 1 Information furnished by Prof. R. C. Potts, Specialist in Marketing Dairy Products, U. S. Dept. of Agriculture, 1916. 446 MARKETING OF BUTTER years immediately following the Civil War, when domestic but- ter production was at ebbtide and prices soared high, 40 cents and over, butter imports reached their maximum. From 1885 to 1900 when domestic quotations for butter were relatively low, averaging 23 cents, butter imports reached their minimum figure. After the year 1900 butter quotations steadily rose and the amount of imported butter increased. After the tariff re- vision which went into effect in November, 1913, and which low- ered the tariff on foreign butter from 6 to 2*4 cents per pound, foreign shipments of butter arriving at the Atlantic and Pacific seaports increased very rapidly. This increase would un- doubtedly have continued had it not been for the advent of the European War which diminished the surplus of foreign butter and increased the home demand for butter in the warring and neutral countries abroad, causing an immediate and rapid de- cline of butter imported into the United States from foreign countries. Source of Butter Imports. — The amount and value of but- ter and butter substitutes imported from foreign countries dur- ing the years 1911 to 1915 inclusive is shown in Table 63. Prior to the war and immediately after the tariff revision the chief importing European nations were England and Den- mark. Small consignments also came from Belgium, France, Germany, Greece, Italy, the Netherlands, Norway, Russia in Europe, Spain, and Turkey in Europe.- Since the beginning of the war the imports from the warring and neutral nations have become insignificant, Denmark remaining the principal shipper. Imports from countries of the North American continent are largely confined to Canada. The South American butter comes largely from Argentine. In Asia, Turkey is the principal country from which butter reached our ports. From Oceania, Australia and New Zealand were the chief shippers of imported butter and the small amounts of butter imported from Africa came largely from Egypt, Tripoli and Italian Africa. At the close of the year 1916 importation of foreign butter had ceased almost entirely. BUTTER STORAGE 447 Quality and Effect of Imported Butter on Domestic Butter Markets. — The quality of foreign butter imported into the United States before the war varied naturally with the source of the butter, the grades ranging from 85 to 93 points. Butter from Denmark and from the Argentine Republic usually scored 92 or better. Butter from Siberia was more or less irregular in quality, some of it was very poor. New Zealand and Australian butter also came irregular in quality, some of it however being very fine.1 The tariff reduction and the subsequent large influx of foreign butter depressed price quotations in American markets to a very marked degree. Thus in March, 1914, Elgin quotations dropped to 24 cents, which is an abnormally low figure for March. This price depression on domestic goods was felt most in the Pacific Coast states in 1914, at which time large ship- ments of butter were received from Australia and New Zealand. Prices at that time were depressed from 3 to 5 cents, presum- ably as the result of the influx of foreign butter. Potts2 offers the opinion, however, that the sudden depression in prices was largely for the purpose of curtailing further imports, as there- by the market prices here would be lower than those abroad and therefore discouraging exportation from foreign countries. He further states that prior to the beginning of the European war several New York butter firms were arranging for con- tracts to receive butter from Europe. CHAPTER XV. BUTTER STORAGE. Time and Duration of Storage. — The great bulk of butter goes into storage in May, June and early part of July, though butter may be, and is, stored at any time of the year when the supply and butter prices appear favorable for storage. May, June and the first half of July are the natural storage months of butter in the northern hemisphere, because the freshening of the majority of the cows and succulent condition of the pastures 1 Information furnished by S. C. Thompson, U. S. Dairy Division, Aug- ust, 1916. 2 Potts, Specialist in Marketing Dairy Products, U. S. Dept. of Agricul- ture, 1916. 448 BUTTER STORAGE during these months provide a natural surplus of butter and cause butter prices to be at ebbtide. In times of early draught which causes a shrinkage of the surplus output and a rise in butter prices, the storage season is usually cut short. When the season is blessed with plenty of rainfall, keeping pastures green until late into fall and contin- uing a large make, the storage season is usually greatly ex- tended beyond the months of May, June and July. Under normal conditions the great bulk of butter in storage is taken out of storage within nine months of the time it went in. Only in exceptional cases is butter held in storage over one year, and when this is done it is usually accompanied by a great sacrifice in quality and in price. Not all butter that goes into storage is held till late winter. Considerable- quantities of but- ter are "short held," that is, they are put on the market after one or but a few months of storage. As early as August some of the May or June butter may be sold. Es- pecially in times of early draught and consequent early falling off of the summer make and rapid rise of butter prices, and when the quality of the fresh butter is poor, due to the hot weather, butter dealers often find it advantageous to supply their trade from their May or June butter in storage, which is usually of better quality and which was purchased at a considerably lower price than they would have to pay for the midsummer butter. In the case of an open summer and fall with a con- tinuous large make and only very gradual rise in prices, the tendency is to hold the butter in storage until such time as the demand necessitates and prices warrant its movement. It is obvious that aside from the output of fresh butter, the condition of the market, butter prices and consequently the duration of storage and the amount of the storage holdings, are influenced by the general industrial conditions of the country, exports and imports, and to some extent the sale of butter substitutes. Since the advent of the Federal Storage Ruling.1 2 in Nov- ember, 1917, and January, 1918, and rescinded March, 1919, re- quiring all butter that is held in cold storage over thirty days to 1 Rules and Regulations, Governing the Importation, Manufacture, Stor- age and Distribution of Food Commodities for Domestic Trade, by Act of Congress, approved August 10, 1917, and effective November 1, 1917. 2 Amendments and Additions to the above, Series B, Supplement, effective January 28, 1918. BUTTER STORAGE 449 be marked on each package with the words "Cold Storage/' the volume of butter that is "Short Held" or stored not in excess of thirty days has increased greatly and the practice of "rotating" the butter stored, on a 30 day rotation basis, has become quite prevalent. This does by no means take the place of the "long held" cold storage of butter, but in a limited way it helps the creamery and dealer to bridge over and take care of temporary surplus and shortages and to thus avoid sudden embarrassing extremes of supply and demand. Distribution of Commercial Stocks of Butter. — During the major portion of the "long held" storage season the butter held in cold storage represents close to 50 per cent of the commercial stocks of butter in the country. The remaining stocks of butter are divided between the wholesale dealers, creameries, retail dealers and meat packers. According to statistics furnished by the United States Bureau of Markets,1 the distribution of com- mercial butter stocks July 1, 1918 and July 1, 1917 was as follows : Table 67.— Stocks of Butter on Hand July 1, 1918, with Com- parative Figures for July 1, 1917, by Classes of Business. Class of Business Total stocks reported as on hand July 1, 1918 Comparative Figures — From Firms Reporting for Both 1918 and 1917 Quantity reported as in transit on July 1, 1^1918 1918 stocks 1917 stocks Quantity Per cent of 1917 Total Creameries . . . Pounds 76,143,419 Pounds 71,645,214 102.7 Pounds 69,766,707 Pounds 11,786,536 13,526,964 38,558,001 5,895,423 16,188,809 13,630,918 2,557,891 1,974,222 605,988 370,196 295,905 802,133 12,349,457 37,623,380 5,860,935 14,236,457 12,057,916 2,178,541 1,574,985 478,959 251,732 255,679 588,615 108.7 101.7 133.5 93.0 93.3 91.5 93.2 91.2 59.1 124.2 110.4 11,363,204 37,011,569 4,389,469 15,302,442 12,921,408 2,381,034 1,690,023 525,305 425,869 205,849 533,000 8,986,444 367,537 320,550 1,843,813 1,787,546 56,267 267,192 605 Cold storages Meat Packers Wholesale dealers Wholesale dealers in but- ter, eggs, and cheese. . Other wholesale dealers. . Miscellaneous Bakers Oleomargarine manufac- turers Cheese factories Other miscellaneous .... 200,180 66,407 1 Food Surveys, Bureau of Markets, U. S. Department of Agriculture, Special Issue, Vol. II, No. 3, August 31, 1918. 450 BUTTER STORAGE Amount of Butter Held in Cold Storage. — The amount of butter held in cold storage varies largely with the supply and demand jf fresh butter, length of storage season, market prices of fresh butter, etc. It is naturally greatest during the storage season proper, and lowest just before the storage season opens up again. The peak of storage holdings is generally reached Cold storage: Meat packers 1 10 15 ZO 2 5 30 3 S « ••HEBEi • STOCKS REPORTED (Pounds) CLASS TOTAL 1918 1917 71,645,214 69,756,707 • c ••• 1 ' 1 918 917 Creameries Cold storages Meat Backers Wholesale dealers 12,349,467 11,363,204 37,623,380 37,011,569 5,860,935 4.389,469 14,236,457 15,302.442 Tig. 77. Stocks of Butter Reported for July 1, 1918, and July 1, 1917, by Important Classes of Business Millions 6 8 15,194,481 11,045,055 9.1E4.034 4,291,022 3,832,338 3,204,877 3,065,224 2,826,693 111. Pa. Calif Minn. Nebr. N.J. Conn. Wls. Ohio Mich. Kan. Iowa Colo. 2,038,497 1,961,845 1,896,340 1,495,380 1,493,472 1,374,719 1,352,727 1,208,665 1.153,202 Fig*. 78. Stocks of Butter Reported for tlie Eighteen Most Important States. by September and the bottom early in May. During the years from 1907 to 1916 the percentage of storage holdings of butter reported by the Associated Warehouses averaged six and nine- tenths on May 1, and 100 on September 1, as shown in graphic illustration, Fig. 80. The average holdings on the first of September, for the entire period of 10 years amounted to 64,378,898 pounds. This diagram further shows that more than three-quarters ot the BUTTER STORAGE: 451 holdings in these warehouses are stored during the months of June and July, while most of the distribution is within the months of October and March, inclusive. The fact that, accord- ing to these figures, an average of 6.9 per cent of the holdings remain at the opening of the new storage season, suggests that this proportion of holdings is carried over into the next season. Miscellaneous, 2.6 % STOCKS REPORTED (Pounds) 76.143.419 Creameries 13,526,964 cold storages 38,558,001 Beat peckers 5,895,423 ,. Miscellaneous 1,974,222 Tig. 79. Distribution of Stocks by Important Classes July 1, 1918 The cold storage holdings of creamery butter by months reported to the United States Bureau of Markets by the great majority of warehouses and including all of the more important warehouses in this country, are issued by this bureau for the benefit of the dealers, free, in the form of monthly reports. The cold storage holdings covering the period of October 1, 1916 to December 1, 1919 are recorded in Table 68. Storage Conditions. — In order to justify storage and to have the storing of butter fulfill the purpose for which it is intended. 452 BUTTER STORAGE COLD STORAGE HOLDINGS 0 F CREAMERY BUTTER Compiled from the reports of the associated warehouses. Based on the average holdings of the years 1907 to 1916 inclusive. Per cent 100 90 80 70 GO 50 HO 30 20 10 ll cent 100 90 SO 70 60 50 30 20 10 0 rig-, so BUTTER STORAGE 453 Table 68. — Cold Storage Holdings of Creamery Butter in the United States, Oct. 1, 1916, to Dec. 1, 1919.1 Months Total Holdings Comparison of Holdings Stor- ages ported Butter, Pounds Stor- ages ported Butter, Pounds Butter, Pounds Increase or Decrease Percent 1916 1916 1915 1916 1915-1916 Oct. 1.... 165 91,728,394 133 99,449,607 88,909,646 -10.6 Nov. 1... . 179 82,269,098 142 92,718,649 79,294,074 -14.6 Dec. 1... . 239 60,774,859 189 71,848,767 58,627,236 -18.4 1917 1917 1916 1917 1916-1917 Jan. 1.... 268 45,996,514 227 48,977,322 44,673,639 - 8.8 Feb. 1.... 273 30,281,472 211 31,139,173 29,250,641 - 6.1 Mar. 1.... 286 15,542,532 215 15,032,769 14,582,975 - 3.0 Apr. 1.... 275 6,239,268 214 3,345,717 6,022,216 +80.0 May .... 281 2,586,593 211 1,081,913 2,433,144 + 124.9 June .... 292 8,942,120 217 7,016,731 8,431,140 +20.2 July .... 289 47,612,460 217 53,863,278 , 44,633,595 -17.1 Aug 310 85,540,972 257 102,537,337 81,502,751 -20.5 Sept 335 99,225,394 268 105,836,003 94,644,780 -10.6 Oct 380 104,293,375 332 100,521,573 97,456,876 - 3.0 Nov. 1.... 396 100,114,760 345 85,260,302 93,209,717 + 9.3 Dec. 1.... 385 77,463,551 340 67,291,844 73,133,855 + 8.7 1918 1918 1917 1918 1917-1918 Jan. 1.... 373 47,069,946 324 41,686,684 43,311,258 + 3.9 Feb. 1.... 372 24,780,358 325 30,473,709 23,542,245 -22.7 Mar 386 18,808,303 333 16,952,367 18,168,209 + 7.2 Apr 381 14,607,017 345 6,805,476 14,177,901 + 108.3 May .... 375 10,245,288 341 3,607,119 10,100,054 + 180.0 June 383 13,017,143 353 9,953,184 12,752,296 +28.1 July .... 419 49,389,491 386 49,981,732 47,436,912 - 5.1 Aug 421 87,382,926 380 79,203,492 81,384,643 + 2.8 Sept 420 101,838,897 390 107,776,392 100,503,488 - 6.7 Oct 408 87,105,801 390 104,926,813 86,253,033 -17.8 Nov 409 80,595,375 389 96,663,946 79,670,291 -17.6 Dec 397 65,577,900 372 78,733,939 65,380,993 -17.0 1919 1919 1918 1919 1918-1919 Jan. 1 377 43,210,770 50,725,766 43,140,260 -15.0 Feb. 1.. 364 36,815,793 353 25,964,218 36,563,442 +40.8 Mar 349 24,436,630 338 18,658,019 24,414,104 +30.9 Apr 333 12,233,700 327 14,628,544 12,226,929 -16.4 May .... 330 9,661,244 323 10,157,399 9,634,690 - 5.1 June 344 29,285,220 333 12,749,056 29,190,222 +129.0 July .... 342 87,851,371 325 47,919,035 87,720,486 +83.1 Aug 334 122,771,843 2 89,157,820 123,545,670 '+40.6 Sept 289 129,251,064 2 99,334,448 131,710,210 +32.6 Oct 284 121,674,977 2 87,924,232 121,834,544 +38.6 Nov. 1.... 270 100,285,328 2 80,816,681 100,851,405 +24.8 Dec. 1.... 268 73,440,191 2 65,110,521 73,676,233 + 13.2 1 Monthly Reports of Cold Storage Holdings of Butter, Bureau of Mar- kets, U. S. Department of Agriculture, 1916-1919. s Comparison of total holdings. 454 BUTTER STORAGE: the butter must be protected against agents and conditions which cause it to deteriorate in quality. The chief of the con- ditions injurious to the quality of butter in storage are air. light, heat and moisture. Air, Light and Heat. — Excessive exposure to air causes de- terioration of butter through oxidation, or through bacterial action, or both. This oxidation is greatly intensified in the presence of light, or heat, or both, and bacterial action is enhanced in the presence of heat. Exposure to air is minimized by the use of packages of comparatively large size and by packing in wrappers and containers that have previously been made as near impervious to air as possible. Butter is best stored in packages of the largest possible size consistent with convenient handling. The larger the cubic content of the pack- age, the smaller, relatively, is its surface and the smaller is, therefore, the area of butter which is exposed to the air. For this reason the firkin used in Europe, the 63 pound tub which predominates in the central and eastern United States and the 56 to 68 pound cube used in the Pacific Coast states, furnish more suitable forms of packages, than smaller packages such as one, two, or five pound prints, slabs or rolls. The firkins, tubs and cubes should be properly paraffined and lined with heavy, brine-soaked parchment paper, so as to furnish as nearly herrnetical a seal as possible. These same conditions, large size and imperviousness of package to air, also protect the butter against light. In full containers butter keeps better than in containers only partly filled. This was experimentally demonstrated by Gray and McKay,1 who stored butter in cans and in tubs completely filled and similar containers only partly full. At — 10 degrees F. to +10 degrees F. there was practically no difference in the keeping quality of butter packed in full cans and full tubs, but at 32 degrees F. there was a slight difference in favor of the cans. Humidity of Storage Rooms. — Aside from the oxidizing effect of air, light and heat on the constituents of butter, the deterioration of butter in storage results from the decomposition or cleavage of the non-fatty constituents, especially the proteins 1 Gray and McKay, Investigations in the Manufacture and Storage of Putter, U. S. Dept. of Agriculture, B. A. I. Bulletin 84, 1906. BUTTER STORAGE 455 or curd of butter, as caused by bacterial, enzymic or chemical action hastened in the presence of air, heat and moisture. A damp storage is prone to cause the development of mold. The storage room therefore should be dry. Temperature of Storage. — Heat intensifies every type of butter deterioration in storage. It hastens oxidation, it enhances the action of bacteria and enzymes, it accelerates chemical ac- tion and it favors mold development. Butter that is intended for prolonged storage must be stored at temperatures of zero degrees Fahrenheit or below. At higher temperatures its keeping quality is invariably jeopardized and the poorer the quality, the more rapid will be the deterioration with age. Gray and McKay,1 in a series of experiments, studying the effect of storage temperature on keeping quality of butter, found that at — 10 degrees F. the butter kept better, both while in cold storage and after removal from cold storage, than when stored at higher temperatures. The butter in these experiments was stored at these temperatures for 5 to 8 months. Similar results were obtained by Rogers, Thompson and Keithley,2 who show the following scores of butter stored at temperatures rang- ing from zero degrees F. to 20 degrees F. : Points I ^ost After Storage Kinds of Butter Stored at 0°F. Points Stored at 10° F. Points Stored at 20° F. Points Raw cream butter Cry A 5 0 5.3 5.8 Raw cream butter Cry D 1 7 4 1 3 3 Raw cream butter, all samples Pasteurized ripened cream Cry B 3.2 2 2 4.6 3.0 4.8 5.1 Pasteurized ripened cream, Crv. E 1.7 3.6 4.0 Pasteurized ripened cream, all samples . . . Pasteurized unripened cream, Cry. C Pasteurized unripened cream, Cry. D Pasteurized unripened cream, all samples . 2.0 .6 .4 .5 3.3 1.0 1.0 1.0 4.6 1.5 1.6 1.6 From the above results Rogers and his co-workers conclude that the difference between zero degrees F. and 10 degrees F. 1 Gray and McKay, Investigations in the Manufacture and Storage of Butter, U. S. Dept. of Agriculture, B. A. I. Bulletin 84, 1906. 2 Rogers, Thompson and Keithley, The Manufacture of Butter for Storage, U. S. Dept. of Agriculture, B. A. I. Bulletin 148, 1912. 456 BUTTER STORAGE is sufficient to warrant the use of the lower temperature, even for butter of the best keeping quality. The author's own experi- ence, both in experimental and commercial storage of butter, is entirely in accord with the above findings and conclusions; in order to insure the best keeping quality for storage butter of any quality, the butter must be kept at a temperature of zero degrees F. or below. In isolated cases creameries have their own cold storage. This is true of many of the larger creameries. The great ma- jority of the creameries of the country, however, lack the neces- sary equipment and facilities for prolonged cold storage and their attempt to use their own facilities in a great many cases proves disappointing in its results. By far the largest portion of the storage butter is stored in the cold rooms of large commer- cial cold storage houses, whose exclusive business is the storage of perishable goods. Shrinkage of Butter in Cold Storage. — Under normal con- ditions the shrinkage in the weight of butter put in cold storage in tubs or cubes is not very great. The main shrinkage usually takes place before the butter reaches the cold storage, while the butter is held in the creamery cool room and in transportation, and after storage when the butter is put up in prints. The loss in weight between the package at the churn and the arrival at the cold storage, varies considerably with the workmanship of the butter, the completeness of moisture incorporation, the treat- ment of tubs and liners, the time that elapses between packing and storing and the amount of salt .butter contains. Butter that has a leaky body, as is usually the case with butter that is churned at too high a churning temperature, or that is made from cream that was not held long enough at the churning temperature, or butter that is not worked sufficiently to close up the water pockets, is prone to show maximum shrink- age due to loss of water or brine. Butter packed in unparaf- fined tubs will shrink more than butter packed in paraffined tubs. A thin, poor liner permits of greater shrinkage of but- ter than a heavy liner of good quality. The longer the butter is held at ordinary cool room temperature and the greater the distance of transportation before the butter reaches cold storage, the more it will sacrifice in weight. Salted butter will lose more BUTTER STORAGE 457 weight than imsalted butter and heavily salted butter will shrink more than lightly salted butter. Even after the butter is in cold storage this shrinkage in the case of heavily salted butter will continue, resulting in very appreciable loss of weight by the end of the storage period. Light salted and unsalted butter, on the other hand, do not suffer material loss in cold storage. Deterioration of Quality of Butter in Storage. — Butter of good quality, intelligently manufactured and properly packed, will generally withstand noticeable deterioration under ordinary commercial conditions and without regular cold storage for about a month. After that time it tends to depreciate, and unless of exceptional keeping quality, it will gradually develop specific defects, such as rancidity, fishy flavor, etc. In regular cold stor- age good butter may retain the character of fresh butter foi; several months. However, age is the arch enemy of quality, and prolonged storage even at commercial cold storage tempera- tures, gradually develops in the great bulk of butter so stored the characteristic storage flavor. The changes and the causes of these changes which take place in butter in storage are exceedingly complex and as yet far from being thoroughly understood. These changes affect both the flavor and the texture of butter, varying in kind and extent with the character and quality of the butter while fresh and the temperature and 'period of storage. The flavor changes often are very marked, the butter loses the characteristic flavors and aroma of fresh butter and devel- ops a variety of off-flavors, the specific flavor and its intensity in each particular case depending probably on specific combina- tions of conditions. Only in rare cases can the flavor defect be traced direct to one specific cause. A certain combination of factors may yield a specific flavor defect, the absence from this combination of one factor may fail to produce the same defect and may cause an entirely different defect, although all other factors and conditions responsible for the original defect may be present. Thus butter may develop a fishy flavor under certain apparent conditions. Yet when an effort is made to produce fishy butter by subjecting butter to these conditions, fishiness often fails to result and in its place usually some other flavor develops, such as oily flavor or metallic flavor, etc. 458 BUTTER STORAGE These facts emphasize the probability that there are many factors which are instrumental in the production of a specific flavor defect through their joint action, while each separate fac- tor, though necessary for the combination that produces the defect, is by itself alone incapable of so doing. As a concrete example of this may be quoted the case of tallowy butter the specific causes of which have been determined with certainty.1 Oxygen carriers and catalizing agents, such as certain metals and their salts, especially copper and copper salts, are capable of making butter tallowy. These agents are present in average butter to a very small extent and in butter containing a normal per cent acid and kept in cold storage they fail to produce the tallowy flavor. If this butter is made from over-neutralized cream, or is wrapped in parchment which was not entirely freed from the ammonia used for the neutralizing of the sulphuric acid used in the parchmenting process, the butter so wrapped may become tallowy very rapidly, especially when it is exposed to room temperature. In this case the alkali, which alone does not make butter tallowy, is a necessary part of the combination, in which copper may be the fundamental cause of the tallowy flavor. The texture of the butter usually shows marked changes only after prolonged cold storage. The grain of the butter gradually breaks down giving such butter a more or less crumbly and pasty consistency. Summary of the Effect of Cold Storage on the Quality of Butter. Summing up the most important phases of our present knowledge of the effect of storage of butter on its quality the following points are emphasized : 1. Age tends to deteriorate the flavor of butter. The rapidity and intensity of this deterioration, other factors being the same, is influenced largely by the temperature of storage. At the usual temperature of commercial cold storage, — 6 to — 10° F. the changes in flavor are usually very gradual. 2. The most predominating flavor defect which butter de- velops in cold storage is the flavor known as cold storage flavor. In the case of butter that was of good quality when it went x Hunziker and Hosman, Tallowy Butter, Its Causes and Prevention, Journal of Dairy Science, Vol. I., No. 4, 1917. BUTTER STORAGE 459 into storage, the development of the storage flavors may be very slight. Butter of poor quality usually shows very great de- terioration in- storage, the flavor defects may be numerous and often one flavor may succeed another as storage progresses. An oily flavor may develop into a metallic flavor and this in turn may give way to fishy flavor, etc. 3. The quality of the cream from which the butter is made, largely governs the keeping quality of the butter in storage. Butter made from a poor quality of cream cannot be expected to withstand rapid and intense deterioration in storage. 4. The analysable chemical changes which butter undergoes in storage, are very slight, even in butter which has yielded to most pronounced flavor changes. The exact changes, and the constituents of the butter which are changed, that are respon- sible for the development of specific flavor defects have not been determined in the great majority of cases. It is assumed with reasonable certainty however, that rancidity and tallowiness are due to cleavage of the butterfat, rancidity through bacterial or enzymic action or both, and tallowiness through chemical action. The characteristic flavor of cold storage butter and its derivations such as oily, metallic and fishy flavors, are generally assumed to result from the decomposition of the non-fatty con- stituents of butter. 5. The most active agents bringing about deterioration of butter in cold storage appear to be cream with a high acid con- tent, the presence in cream and butter of metals, such as cop- per and iron, and their salts, the air incorporated in the butter and bacteria and enzymes ; though the influence of microorgan- isms is considered of indirect rather than of direct nature. 6. In order to insure, with reasonable certainty, butter of good keeping quality, and minimum deterioration in commer- cial cold storage, the butter should be made from cream of good quality and low acidity, transported in cans that are free from rust, and handled in vats, pasteurizers and conduits properly tinned and the surfaces of which are kept bright and free from accumulations of oxidized or dissolved metal, the pasteurization should be thorough and preferably by the flash process at 176° F. or over, or the holding process at 145° F. for 30 minutes, the 460 BUTTER SCORING butter should be worked in the normal way, avoiding over- churning and overworking and excessive incorporation of air, all equipment and rooms in the factory in which the cream and butter is handled and exposed should be kept clean, the butter should be packed and stored under approved conditions and should reach the cold storage with the least possible delay after manufacture. CHAPTER XVI. BUTTER SCORING. Definition. — The scoring or judging of butter refers to the examination of butter for flavor and aroma, body and texture, color, salt and package. Purpose. — The primary object of scoring butter is to de- termine its quality and market value. The bulk of the butter that reaches the wholesale receivers, jobbers and commission men is scored and most of this butter is sold "over the trier" and paid for on the basis of the grade to which its score entitles it. Butter intended for storage usually is, and always should be, most carefully scored in order to ascertain its fitness for storage. Butter showing a weak body and tendency toward an oily, metallic or fishy flavor is unsafe to go into storage. Such butter is prone to become fishy or develop other storage flavors with age. Careful scoring before permitting its entrance into cold storage may save the owner from heavy loss at the end of the storage period. At butter scoring contests such as are held at County, State and National fairs and shows, the careful scoring of the butter judges and their criticisms and instructions, are often of great help to the buttermaker in his efforts to eliminate butter defects and to improve upon his methods of manufacture. The butter should be scored not only by the buyer and the educational judge but by the buttermaker himself. He should have accurate knowledge of the quality of butter that leaves his factory and he can secure this knowledge only by carefully scoring each churning. This scoring should not be done at the churn, however, for the quality of the fresh butter at the churn BUTTER SCORING 461 is seldom a reliable index to the quality of the butter when it is one or two weeks old. Most butter when perfectly fresh is palatable. Serious defects generally develop and "show up" with age. The Score Card. — The national score card adopted and used by the officials and butter men in all parts of the country is that contained in the rulings of the New York Mercantile Exchange and quoted in the chapter on "Markets and Marketing." Valuation of Butter Defects. — The prices paid for butter sold on the open market, are based fundamentally on the estab- lished classes of market grades, the chief of which are: "Extras," "Firsts," "Seconds" and "Thirds," and in commercial scoring the deductions for defects are generally so made as to place the butter into its respective grade. The exact scores for each grade vary somewhat with the condition of the market and the season of the year as determined by the Butter Committee of the Exchange. Thus the New York Mercantile Exchange rules provide that extras may score either 91, 92 or 93 points, as the minimum, at the discretion of the Butter Committee, who shall determine the required score from time to time in such manner that it shall represent an average fancy quality in the season when offered. But butter scoring more than required for "Extras" shall be deliverable on a contract for "Extras," etc. See rules of New York Mercantile Exchange. The minimum scores, for the several grades are as follows, with Extras at 91, 92 or 93 points: Extras at 91 92 93 Firsts ...87 88 89 Seconds 82 83 84 Thirds 75 76 77 In discussing the figure valuation of butter defects it will be assumed here that "Extras" require a minimum score of 92 points. "Extras." — In order for butter to score "Extras," it must have a clean and pleasant flavor and aroma and it must be free from, any undesirable off-flavors. Its color, salt and body must be perfect. Such butter would merit a flavor score of 37 and a total score of 92. Butter with a specially delicate flavor and 462 BUTTER SCORING creamy texture, showing excellent quality of cream, may be given a flavor score of 38, 39, 40 or 41 points, or higher, or a total of 93, 94, 95 or 96 or higher, according to the pronouncedness of these desirable qualities. "Firsts." — -Butter which is of clean flavor but lacks the char- acteristic delicacy of aroma, and is perfect in body, color and salt, is considered a good "Firsts," meriting a flavor score of 35 to 36 points, or a total score of about 90 to 91 points. Butter with a slightly acid flavor and aroma, or that shows traces of weedy flavor or other slight flavor defects might still be classed as a "Firsts," with a flavor score of 33 to 34 points and a total score of 88 to 89 points, provided that it is perfect in body, color and salt. "Seconds." — Butter that shows slight rancidity, fishiness, oily or metallic flavor, garlic flavor, or yeasty flavor, is classed as a "Seconds," with a flavor score of 28 to 32 inclusive, and a total score of 83 to 87 inclusive, the exact score varying with the intensity of the defect. . "Thirds." — Butter with a strongly rancid, tallowy, fishy, or other intense off-flavor is scored as "Thirds." Butter with a leaky texture or leaky or crumbly body would not be accepted as an "Extras." These defects would cut its score on body such texture from 1 to 3 points. If of clean flavor and perfect color, such butter might score a good "Firsts." Butter that is pronouncedly mottled is cut from 3 to 5 points on color. If otherwise of good quality and clean flavor it would be classed as a "Firsts." Butter that is gritty and excessively salty may be cut from ^2 to 2 points on salt according to the intensity of the defect. Such butter usually has a coarse flavor. If it shows no distinct off-flavor, it may be classed as a "Firsts." In rare cases only is butter scored down on package, but it should be understood that the neatness and cleanliness of the package makes a favorable impression on the judge, while an untidy and soiled package tends to condemn the goods. Method of Scoring. — The scoring of butter is most conven- iently done by the use of a butter trier. A plug of butter is removed from the package by boring from top to bottom of BUTTER SCORING 463 the tub or cube, or from end to end in the case of the print. First the aroma is observed by passing the trier under the nose. Then the butter is tasted for flavor and salt by cutting with a clean knife or spatula, a small piece off the plug. Then the plug is examined for uniformity of color. The texture and body are examined for leakiness, crumbliness, stickiness and weak body. In the case of crumbly and sticky butter it is difficult to secure a solid plug, the plug is ragged and irregular and butter sticks to the back of the trier. In the case of leaky butter the brine runs freely, and in large drops, from the butter. A weak body refers to butter with a poor grain; when the plug is broken the surface at the break resembles that of a tallow candle and the butter gives the impression of salviness. The color of such butter generally lacks brightness and life, it is dull. The Ethics of Butter Scoring. — It must be obvious to all who are interested in the dignity and standard of excellence of the butter industry that the sanitary and ethical aspect of butter scoring demands, that this work be done in a neat, cleanly and careful manner, and yet so many so-called butter judges ignore the most primitive dictates of decency in the scoring of butter. They do this work in slovenly manner, they pay no attention to the cleanliness of their hands, they fail to wipe the trier clean before it is inserted in the butter, they try to ascertain the aroma by rubbing their nose into and wiping it on the butter, they determine the flavor by digging their teeth into a plug, and then replace this mutilated and desecrated butter into the package which is later offered for sale and consumption. Such performances are an insult to the dignity of the butter industry and a depredation to this most valuable and wholesome of food, butter. Nor do such practices denote expertness on the part of the judge. The flavor and aroma of butter are of delicate nature, their correct impression on the senses demands subtle and delicate handling. Pressing one's nose into the butter destroys the delicacy of flavor and aroma and dulls the senses. There is room for much improvement, especially in the cellars of the wholesale produce, in the ethics of butter scoring as now done, and this improvement will assist in convincing the laymen of the wholesomeness and superiot virtues of butter as a food which the dairy interests claim for their product. 464 BUTTER SCORING The necessary equipment for performing the examination and scoring of butter in an approved manner, consists of a nickel-, tin- or silver-plated butter trier, a knife or spatula and clean cheese cloth or clean soft paper, such as tissue paper. Before commencing the work of examining the butter, the scorer should thoroughly wash his hands with soap and water. The trier should be wiped dry and clean. When the plug on the trier is examined for aroma, it should be passed under the nose without touching the nose. For tasting the butter a small piece of butter is removed from the plug with the knife or spatula. The uniformity or color can be seen without mutila- tion of the plug. Examination for leakiness and body and texture is best made by pressing the plug with clean thumb. When the examination is completed, the plug is neatly re- placed in the bore of the package by carefully returning the trier in the bore and withdrawing the empty trier. The surface of the package at the place of the returned plug is then evened up and smoothed over, not with the fingers, but with the trier, and the circle or wrapper is again repjaced neatly. The trier and spatula are then wiped clean, not with the bare hands, but with the cheese cloth or paper, before the next package is examined. Accuracy of Butter Scoring. — It is said that expert butter judges are born and not made. This is true to a limited ex- tent. Expertness requires, above all things, a keen sense of taste and smell. Individuals deprived of an accurate sense of taste and smell lack the fundamental attributes that make for expertness in butter scoring. However, most persons possess these senses to a sufficient degree to be able to distinguish good butter from bad butter, and with a little practice they soon acquire the power to differentiate between the more pronounced flavors and odors. Aside from the natural and acquired ability to detect flavor and aroma, the butter judge needs knowledge, experience and judgment in determining and deciding on the correct valuation in terms of figure scores, of the flavors found in the butter, and these attributes are largely a matter of practice. Finally the butter judge must be a man of character, not given to superficial work and "bluff verdicts," BUTTER SCORING 465 he must be conscientious, careful and able to decide for himself and, after deciding, to stand by his convictions. When more than one judge does the scoring, as is generally the case at educational butter scoring contests and county, state and national fairs, also in scoring experimental butter, each judge should work entirely independent of the other judges, there should be no expression of opinion, no comparison of notes, while the scoring is in progress and until each of the judges has com- pleted his work, otherwise the personal judgment of the individ- ual judge is jeopardized and is liable to be materially, though unknowingly, influenced, and this occurs usually to the detri- ment of the accuracy and fairness of the final score. After each judge has completed his scoring, then the judges may compare notes and rescore, for their own satisfaction, packages on which the scores of the different judges show considerable diversion. The average of the individually determined scores of the several judges promises results of maximum accuracy, a'nd freedom from disturbing influences, of the final score awarded to each package. The Value of Educational Butter Scoring Contests.— With due allowance to the actual service these contests are often capa- ble of rendering, the judge through his criticisms giving the but- termaker valuable information that makes for improvement, it must be admitted that the lasting results of educational butter- scoring contests and the concrete usable information they offer, are often very meager and in a great many cases they do not justify the expense incurred. There are many reasons for this. The average butter judge is not a practical buttermaker. He lacks the full knowledge of the real problems which confront the buttermaker and he therefore falls short in his appreciation of the significance of these problems. In fact, even assuming that he is a capable judge of butter, which is by no means always the case, he has very little to offer to and a great deal to learn from the man whose butter he is scoring. Some of the informa- tion which he endeavors to convey to the buttermaker through his letter of criticisms is either not well founded or does not apply, and much of the remainder of the information given has long been a part of the buttermaker's knowledge , but local conditions, lack of sufficient energy, or other conditions, 466 BUTTER SCORING have hindered him from putting this knowledge "across" in his factory. Again, the basis upon which the butter is scored at most of the scoring contests puts a premium on a very mistaken standard of excellence, that not only has no real commercial val- ue, but is a positive detriment to the success of the butter in- dustry. The ideal used as the basis for scoring has been that of butter with a highly developed butter flavor, and in their efforts to successfully compete, the buttermakers so ripened their cream and handled their butter as to cause it to possess as high a flavor as possible on the day of the contest. Elsewhere in this volume it is conclusively shown that butter so made has very poor keeping quality. It has reached the very limit of changes it is capable of undergoing, without actually deteriorating in flavor and any further changes, which it is bound to suffer with age, will cause it to develop off-flavors. The butter with high flavor which wins top scores and honors at these contests, therefore, has the ear-marks of butter that does not keep well and that, by the time it reaches the table of the consumer, may be anything but "prize butter." Since the consumer is the final judge of the value of butter, the butter must have such keeping property that it is able to withstand agencies of deterioration until it is consumed, and it is essential to the success of the butter industry that the buttermaker concentrate his knowledge and energy in this direction, rather than to manufacture butter that is a prize win- ner tomorrow and that "goes to pieces" thereafter. In some of the states the management of scoring contests, appreciating the significance of these facts, is effectively cor- recting this weakness, by either holding all contest butter for several weeks before the contest, or by rescoring a second time after an interval of several weeks. The results of scoring contests following this practice are bound to be fruitful of much real good, from the standpoint of assisting the butter- maker in his efforts to improve the commercial value of his butter. Finally, the conducting of educational butter scoring con- tests has much educational value in an indirect way. It is an BUTTER DEFECTS 467 effective means to bring the buttermakers together, where they can discuss their problems and difficulties, where they have an opportunity to hear lectures and see demonstrations that give them new information, and where they can come in close touch with the dairy schools and their staffs. CHAPTER XVII. BUTTER DEFECTS. THEIR CAUSES AND PREVENTION. Classification of Defects. — This discussion is confined to the most important butter defects which are considered individually under the following few headings : flavor and aroma, body and texture, color and appearance. DEFECTS IN FLAVOR AND AROMA. Flat Flavor. — Butter termed flat in flavor lacks the delicate flavor and aroma characteristic of "Extras" and fancy butter. Its flavor lacks life. Such butter usually sells as "Firsts" on the market, provided that it has no serious defect otherwise. The flat flavor is usually due to washing excessively in cold water. Cold wash water has the power to absorb the flavor- producing volatile oils of the butter when in granular form. Excessive washing and prolonged exposure of the butter to the cold wash water, therefore, tend to leave the butter with- out much flavor, or flat. Occasionally butter is criticised as being flat in flavor simply because it is low in salt. The use ctf more salt brings out the flavor more pronouncedly. Butter made from sweet cream which was not subjected to the ripening process and to which no starter was added, is generally very mild in flavor and may be termed flat by those who desire a high-flavored butter. Stale Flavor. — The staleness and lifelessness of butter, termed stale, is usually due to the advanced state of the period of lactation. It is an off-flavor which is characteristic of butter made in winter when the cows are approaching the end of their lactation period. The cause here, as in flat-flavored butter, lies in the partial absence of the flavor-producing volatile and solu- ble fats, oils and acids. As the period of lactation advances, the 46S BUTTER per cent of the flavor-producing elements decreases and is lowest at the time the cows are ready to go dry. Observant butter- makers know from experience that, when all their cream comes from stripper cows, their butter always has more or less of this stale flavor, and that the addition of but a few cans of cream or milk from fresh cows will make a wonderful improvement in the flavor of their butter. At the beginning of the period of lactation when the cows are fresh, as is generally the case in early summer, the milk contains the maximum per cent of volatile and soluble fats and acids and the stale flavor is entirely absent in butter made from such milk or cream. While the use of a good active starter generally assists in minimizing the stale flavor, it seldom will overcome it entirely, because the natural flavoring principles in the milk and cream which are necessary in order to secure the full benefit of the starter, are lacking or are present in insufficient quantities in cream from stripper cows. Stale butter seldom grades " Extras." The stale flavor is frequently attributed also to old cream, or cream having been held too long before churning. In most cases of cream that has been held for a long time, however, the staleness is expressed by more specific off-flavors, resulting from fermentation, or absorption of odors from environment, and it is doubtful if the so-called stale flavor of butter can conclusively be traced to old cream. Sour, Curdy and Cheesy Flavor and Aroma. — This defect is characteristic of much of the butter that is made from high-acid cream, such as gathered cream and cream shipped long distances. The sourness is noticeable particularly in the odor or aroma of the butter. If otherwise perfect such butter usually scores a poor "Firsts" or a good "Seconds." It is rejected by the critical trade and is unfit for storage as it tends to deteriorate rapidly. The sour flavor and aroma are usually largely due to cream that arrives at the creamery in very sour condition. It may be avoided by neutralizing the cream and thorough washing out of the buttermilk. Frequently sour butter is the direct result of overripening the cream, or starter, or both, and of leaving too much buttermilk in the butter. Attempts to produce high- flavored butter by only slightly washing the butter and causing BUTTER DEFECTS 469 it to have a milky brine tend toward the development of a sour flavor and aroma. High buttermilk content, overripe cream and starter and similar agencies are responsible also for curdy and cheesy flavors which often accompany the sour flavor, or take its place. They are due directly to the curd content of the butter. This class of flavor defects is characteristic of hot weather butter and especially of butter made from sour, farm separator cream dur- ing the summer season. It will appear as long as the creamery accepts a poor quality of cream, but may be minimized by neutralization, pasteurization, the use of a good quality of starter and expulsion of buttermilk by thorough washing. Unclean Flavor. — This is a rather general term and yet it represents, in the vocabulary of the butter judge, a definite flavor condition of the butter. Butter with an unclean flavor lacks the clean, delicate, pleasant, aromatic butter flavor. Its taste suggests the use of unsanitary utensils and methods of handling the cream, such as unclean strainers, especially cloth strainers ; foul smelling cans, especially cans that are not washed clean, or that contain dirty wash water due to incomplete rinsing, or that were not thoroughly steamed and dried after washing 'and rinsing; unclean farm separators, as the result of not removing all remnants of milk, cream and separator slime after each separation, or not washing the separator after each separation; unclean and leaky vats, pipes and conveyors, churns and pack- ers; and unclean milk and cream and polluted wash water. The unclean flavor is imparted to butter in two ways, by direct incorporation in milk, cream and butter, of decayed rem- nants of milk with foul smelling odors and indirectly by the contamination of the product, through these channels, with pu- trefactive bacteria, yeast and molds, thriving in decaying rem- nants of milk and developing products of putrefaction in the cream and butter. Unclean flavor in butter can be prevented by using clean utensils for the production and handling of milk and cream on the farm, returning to the farmer clean, sterile and dry cream cans, and keeping the equipment in the creamery in sanitary condition. 470 BUTTER Cowy and Barny Flavor. — Butter with a cowy flavor sug- gests contamination with manure and stable air. This flavor oc- casionally is very pronounced, especially in some species of dairy butter, in which case the butter usually scores a poor "Seconds," The cowy flavor may be due to milking cows whose udders and flanks are plastered with manure, the handling and exposure of milk and cream in unventilated stables, and not removing the ani- mal heat from the milk or cream promptly. The milk and cream which produce butter with a cowy or barny flavor are generally contaminated with large numbers of Bacillus coli communis and Bacillus coli aerogenes. These or- ganisms are the natural inhabitants of the colon, or large in- testine of the animal, and are therefore found abundantly in the manure. The abundant presence of these bacilli in milk and cream is rather conclusive evidence of the pollution of milk and cream with excreta from the cow. When milk and cream so con- taminated are not promptly cooled these germs multiply rapidly and intensify the barny odors in the butter. For details see Chapter IV on Care of Milk and Cream on the Farm. Musty and Smothered Flavor. — This butter defect is gener- ally .caused by lack of prompt cooling and aeration of the cream on the farm. The sealing up of the warm cream in the shipping can without giving it any opportunity to give off its animal heat is generally believed to cause a musty, smothered flavor. The stor- ing of the cream in damp and poorly ventilated cellars with a stagnant atmosphere is another probable cause of musty flavored butter. The cause of musty flavor frequently also lies in the feeding of moldy, musty and decayed foods, such as moldy hay, moldy silage and musty grain. Feed and Weed Flavors. — To this group of butter flavors be- long a variety of flavors characteristic of the feeds to which the cows have access. Many of these flavors are not very pronounced and therefore not seriously objectionable, but others are very marked and in some instances greatly depreciate the market value of butter. Since the feed flavors are usually traceable direct to the charac- teristic feeds producing them, or to excessive feeding of certain types of feeds, or to microorganisms with which certain feeds are BUTTER DEFECTS 471 associated, their prevention must of necessity lie -with the pro- ducer of milk and cream. The flavors due to weeds such as gar- lic, rag weed, etc., can be guarded against only by eradication of these weeds from the pasture. See "Garlic Flavor." Roots, such as turnips, are best fed after milking in order to give the feed time to pass through and out of the cow several hours before the succeeding milking. Feed flavors caused by frozen, decayed and moldy feed are prevented by eliminating from the ration all feed not in good, sound condition. Sour, moldy silage, frozen and decayed roots and tops of roots, damp, moldy and poorly cured hay, damp and musty straw, etc., should not be fed to dairy cows. While most of the feed flavors are inherent in the milk and cream which contain them and therefore follow these products into the butter and while their appearance in the butter is beyond the control of the great majority of creameries, many of these flavors, not including the garlic flavor, and rag weed flavor, are greatly minimized by pasteurization and aeration of the cream. Pasteurization assists in driving and expelling from the product volatile flavors, odors, and gases and thus helps to lessen the in- tensity of these flavors in the finished butter. Garlic or Wild Onion Flavor. — When the wild onion flavor has once impregnated the milk or cream, it is very difficult to keep this objectionable flavor out of the butter, and butter made from such milk or cream usually grades a poor "Seconds." It may be improved materially, however, by blowing air through the milk or cream while hot and by prolonged pasteurization at a high temperature. Ayres and Johnson1 demonstrated that milk and cream can be freed from the wild onion flavor entirely by ade- quate blowing, while these raw materials are hot. These investi- gators contrived a blowing equipment for blowing milk and cream on a small scale, with which they were able to entirely remove the onion flavor from milk heated to 145° F for five minutes. For cream they recommend a somewhat longer period of blowing and a temperature of 160° F. Their work was done with sweet cream testing 30% fat. It is probable that for richer cream and for cream that is sour, the apparatus devised would have to be modi- 1 Ayres and Johnson, Removal of Garlic Flavor from Milk and Cream, U. S. Dept. of Agr., B. A. T. Farmers' Bulletin 608, 1914. 472 BUTTER fied somewhat to prevent clogging and to insure more complete aeration. The usual equipment and method employed for this purpose in the creamery are quite inadequate for complete re- moval of garlic flavor in sour cream. They fail to furnish the volume of air necessary for successful results. • Because of the difficulty of even minimizing the garlic flavor in butter made from garlic-flavored milk or cream, and the im- possibility, under practical commercial conditions, of removing this flavor from the once tainted product, entirely, every effort should be made to keep this flavor out of the milk on the farm. There are two ways to accomplish this, namely, to prevent the cows, so far as possible, from obtaining garlic and secondly to manage the herd on garlic pasture in such a manner as to have it suffer the least harmful effect.1 Garlic makes a growth much earlier in the spring than pasture grasses, and therefore is usually most troublesome when cows are first turned to pasture and when grass is not plentiful. In many cases garlic is localized in the pasture and these places should be fenced off and used for pasturing stock other than milk producing cows. When the garlic is scattered about the fields it is impos- sible to do so, and the dairyman who would not have the flavor of the milk of his cows impaired must so manage his herd as to overcome the difficulty. The unpleasant odor and flavor are strongest in milk from cows that have just eaten the garlic. If, three or four hours before milking, the cows are placed in a garlic-free field, the trouble will be reduced to a minimum. If such a field is not available, they may be brought to the stable yard and fed on silage or hay and allowed to remain out of doors until the regular milking time. This practice the dairyman can usually follow without serious inconvenience. The trouble caused by garlic is not liable to last long, as the weed is usually cropped off by the cows within a few days after they are turned to pasture, and as soon as the grass becomes plen- tiful they will eat that in preference. However in years when the season opens slowly so that the pastures fail to satisfy the cows with an abundance of grass for a considerable period of time, garlic-flavored cream may occur for 1 Hoard's Dairyman, November 18, 1918. BUTTER DEFECTS 473 many weeks. In the fall also there is a tendency in some sec- tions for this flavor again to appear. The complete eradication of the garlic plant is the most satis- factory method of avoiding trouble and is practicable on thejpr- dinary dairy farm. Those interested in such eradication should write to the Department of Agriculture, Washington, D. C, for Farmers' Bulletin 610, entitled, "Wild Onion; Methods of Eradi- cation", and Farmers' Bulletin 608, which gives directions for re- moving the garlic flavor of milk. MOLDY BUTTER The genuine moldy flavor of butter is usually due to the pres- ence and growth in cream and butter of certain species of molds. Frequently storage butter, that has reached an advanced stage of deterioration, develops a very marked disagreeable moldy odor and flavor. Causes of Mold Spots on Butter. — The greatest objection of moldy butter, however, does not lie in its objectionable flavor, but rather in the appearance on and in the butter of mold specks and spots which render it unsightly and cause much loss to the creamery'and the butter dealer. This butter fault is especially prevalent in summer and usually shows up in the course of a few days after manufacture. Whole- sale receivers practically every summer complain of moldy butter. They find the butter to be spotted with mold specks of a greenish- brown to black color. These specks are located largely on the surface of the butter, especially in the lower sections of the butter tub. In aggravated cases the mold specks penetrate the butter to a considerable depth and frequently they permeate the entire tub. Even if butter scored an "Extras" in all other points, moldy butter would be classed as a "Seconds" and would be sold by the dealers as such at a great sacrifice in price. The difficulty and trouble of removing all traces of mold from moldy butter is great and expensive. Much butter is wasted, new tubs and liners have to be supplied, and much labor is required. Upon storage at not very low temperature butter occasionally be- comes completely coated with a matting of molds. The fila- ments often grow so long that the surface is actually bearded. 474 BUTTER Unsalted butter is much more prone to become moldy than salted butter, the salt exerting a considerable retarding, if not in- hibiting, effect on mold growth. In fact, it is frequently very difficult to prevent unsalted butter from showing moldiness, in spite of the' observance of otherwise successful and effective precautions. There are numerous classes and species of molds that are capa- ble of developing mold spots on butter, such as Penicilium, Tri- chosporium, Streptothrix, Cladosporium oidium. Griepenberg1 who examined storage butter, found that most of the molds in butter belonged to the genera Penicilium and Trichosporium and that of these, Penicilium cruslaceum and Trichosporium collae were the most common species. Penicilium glaucum and oidium lactis are also known to be very common molds of butter. Most of these organisms thrive on the caseous matter of the butter and some are also capable of splitting the butterfat. According to Thorn and Shaw,2 mold in butter usually takes three forms : "1. Orange-yellow (red) areas with a submerged growth of mycelium, which are produced by Oidium lactis. Cannot develop in butter containing 2.5% of salt. 2. Smudged or dirty-green areas, either entirely submerged or with some surface growth. These are produced by species Alternaria and Cladosporium. Cannot develop in butter con- taining 2.5% salt. 3. Green surface colonies, which are produced by Penicilium, or more rarely, Aspergillus, either upon the butter, causing de- composition, or upon the container or wrapping, injuring the appearance of the sample in the market." The natural channels through which butter becomes contam- inated are infection of milk and cream on the farm, and con- tamination of cream or butter in the factory, from the air in ill- ventilated plants, from unclean vats, pipes, churns and packing equipment, from impure starters and impure washwater, and from mold-infected material used for packing, such as parchment wrappers and liners, and butter tubs and boxes. 1 Griepenberg1, Fleischmann, Lehrbuch der Milchwirtschaft, p. 324, 1915. 2 Thorn and Shaw. Moldiness in Butter. Jour. Agr. Research. Vol. Ill, No. 4, 1915. BUTTER DEFECTS 475 Proper pasteurization materially minimizes the tendency of butter to become moldy. It is destructive to the majority of the species of molds usually found in the cream.1 Pasteurization therefore limits the problem of preventing moldy butter very largely to precautions against recontamination of cream and but- ter after the cream leaves the pasteurizer and confines it to the sanitary condition of the air, vats, pipes, pumps, churns, wash- water and packing equipment and material. Moldy butter has in some instances also been traced to con- taminated salt. The most probable cause of the salt as a source of moldy butter lies in the contamination of the salt in the creamery after the barrel is opened. In many creameries the salt is kept in a room none too clean and in an atmosphere none too pure. If the barrel is left open the surface of the salt is prone to become contaminated with germ life of the air and may become the carrier of mold. The salt barrels should be stored in a clean place and a properly fitting cover should be provided for rem- nant barrels. Such barrels should be covered immediately after each removal of salt. Prevention of Mold in Butter. — Moldiness in butter may best be prevented by observing the following precautions : 1. Pasteurize all cream, skimmilk and starter used. In vat pasteurization heat to at least 145° F. and hold not less than 30 minutes. In flash pasteurization heat to 180 to 185° F. When using the holding process draw a pailful of cream from the gate of the vat as soon as the temperature of the cream reaches 145° F. and pour it back into the vat. This will insure proper heating of the cream located in the gate and nipple. 2. Use pure starter only. If the starter is contaminated reject it. 3. Thoroughly wash, flush and steam all vats, pipes, con- duits and pumps daily. 4. Rinse the churns daily with one batch of hot water containing some good washing- powder and then with clean hot water. The water must have a temperature of 180° F. or over. Use thermometer to make sure. Lime the churns at regular 1 Thorn and Ayres — Effect of Pasteurization on Mold Spores. Jour. Agr. Research, Vol. VI, No. 4, 1916. 476 BUTTER intervals, preferably once per week, or whenever they show signs of staleness. Churns that have been lying idle should always be limed and receive a special cleaning and scalding before they are pressed into service again. The churn is the most difficult piece of equipment to keep clean and sweet, and it represents one of the most dangerous sources of moldy butter. 5. Do not wash packing equipment, such as packers, ladles, cubes and tubs, in dirty water. Rinse them thoroughly with scalding hot water after washing and store them in a clean, dry atmosphere. 6. Wash the butter thoroughly to remove as much as pos- sible of the curd of the buttermilk. Curd is a necessary food for molds to grow on. Use pure wash water. Have the wash water tested bacteriologically at reasonable intervals and if it contains molds pasteurize or filter it. If a wash water storage tank is used it should be kept clean and free from slimy material by frequent scrubbing out. 7. Keep the salt in a clean, dry place. Do not break the seal of the barrels until necessary. Keep remnant barrels covered. 8. Do not store cubes, tubs and parchment liners and wrappers in a damp room. Keep them in a clean, dry at- mosphere and keep the parchment wrappers and liners in their original package until used. 9. Properly paraffin all tubs and boxes. Heat them over the steam jet until they are "piping" hot before paraffining and use boiling paraffin only. Do the paraffining as short a time as possible before the tubs are used and keep them inverted in a clean place after paraffining and before use. 10. Soak parchment wrappers, liners and circles from 5 to 10 minutes in boiling hot saturated brine before use, both for salted and for unsalted butter. 11. Incorporate the moisture in the butter properly. Wet, leaky butter assists in the spread of mold colonies. 12. Pack the butter solidly, avoiding air pockets, espe- cially between the butter and the sides of the tub. Air favors mold growth, BUTTER DEFECTS 477 13. Store the butter in a clean, dry room and keep the temperature as low as possible. Molds grow best in a moist atmosphere and at a temperature around 50 to 60° F. 14. Make the butter from cream of low acidity (.3% acid or below). Molds prefer an acid medium for growth. 15. Keep the air in the creamery well ventilated and the sewers and floors well scrubbed. A stagnant, impure atmo- sphere is often pregnant with mold spores. 16. Spray the walls, ceilings and floors of butter storage rooms with formaldehyde, at reasonable intervals. Do not per- mit the appearance of mold specks on walls and ceilings. For additional directions for the treatment of liners and wrappers see Chapter XII on ''Packing Butter." Yeasty Flavor and Foamy Cream. — This flavor is the re- sult of a yeast fermentation of the cream. It is most preva- lent in summer, particularly during the hottest summer weather, when both, the days and the nights are hot and when the cream is exposed to the summer heat for a considerable length of time. Yeasty flavored butter seldom scores better than a "Sec- ond." It represents a very objectionable flavor defect which no now-known process of manufacture is capable of entirely removing. Nor does it disappear while the butter is held in cold storage. This flavor stays in butter until the butter is consumed. Yeasty cream, therefore, should be culled out at the cream- ery by rigid grading, and churned separately, if it is accepted at all. The adoption and practice of an efficient system of cream grading and paying on the basis of quality is the creamery's most effective immediate weapon to minimize receipts of yeasty cream, accompanied by a systematic effort to acquaint the farmer with the fact that the reason why he received a lower price was that the cream was yeasty, and by instructions of how to best avoid the recurrence of this defect. The fundamental cause of yeasty and foamy cream lies in the presence in cream of yeast cells. Most, if not all, cream contains some yeast cells, but at moderate or low temperatures they fail to gain the ascendency and therefore do not develop a yeasty flavor in the cream nor cause the cream to foam. 478 BUTTER DEFECTS Yeast cells require a relatively high temperature, approach- ing that of the animal body, for their greatest development. When on the farm, or in transit, or both, the cream is exposed sufficiently long to summer heat, so that the cream itself be- comes warm, the development of the yeast cells becomes very pronounced and very intense. Often it is accompanied by vio- lent gas production, frequently causing the lids of the cans to blow off and the cream to foam over. In this condition the cream gives off a very decided and objectionable yeasty flavor similar to baker's yeast, that follows the product into the fin- ished butter. If the cream is cooled promptly and properly on the farm when it leaves the separator and is kept cool until shipped, it usually reaches the creamery before it has a chance to become yeasty and foamy. On the other hand, if the cream is not cooled on the farm, the yeast cells become active at once and when this fermentation has once commenced, it goes on rapidly and is stopped with difficulty only. It is obvious also that the number of yeast cells present in the cream to start with, has a great deal to do with the rapid- ity and extent to which this defect develops. Contamination of the cream through such channels as impure water, unclean utensils, unclean separators and cans, should be avoided as much as possible, and the cream producer should be instructed to pay close attention to the following precautions : Prevention of Yeasty and Foamy Cream. 1. Wash and scald all milk utensils, such as strainers, pails, dippers, cans, etc., after each use. 2. Wash and scald all parts of the cream separator that come in contact with milk and cream, after each use. 3. Cool the cream as soon as it leaves the separator to as low a temperature as possible, preferably below 60° F. 4. Use a cream cooling tank and keep the cream in cold water until it leaves the farm. 5. Protect the cream cans in transit from summer heat by covering them with wet blankets. 6. Do not allow the cans to stand on the station platform exposed to the sun in hot weather- BUTTER DEFECTS 479 7. Deliver or ship the cream often. In the case of the cream station system of receiving cream, cream that may have arrived at the cream station in good condi- tion, frequently is yeasty and foams over by the time it reaches the central creamery. In this case the yeasty defect is largely due to faulty handling of the cream at the cream station. In order to avoid this the cream, after it has been trans- ferred to the shipping cans, should be set in cold water or in a cold room and held there until shipping time. If, during hot weather, cream arrives at the creamery at a time too late for "dumping" on the same day, the cans should be rolled into the cooler, in order to prevent the development of foamy cream over night. Bitter Flavor. — The bitter flavor of butter is a defect, which is confined largely to dairy butter. Its occurrence in creamery butter is comparatively rare. The bitter flavor is either present in the milk at the time it is drawn or it develops in the milk or cream after milking. In either case it passes also into the butter. There are individual cows when in poor physical condition, or when they have reached an advanced state of their period of lactation, usually after the sixth month, that yield milk that has a bitter taste. In many of these cases of bitter milk, the milk is abnormal also in other respects. Often the milk is very viscous and produces cream that refuses to churn out; the but- ter usually has a poor texture and is greasy. In some instances this bitter milk does not curdle in the natural way. The exact cause of this condition has not been satisfactorily determined. Weigmann1 suggests the probability that the peptonizing of the milk proteids may yield bitter-tasting albumoses and peptones, but he also mentions the possibility of the presence in such milk of special bitter substances. Whether these lower forms of milk proteids, the albumoses and peptones, are the result of abnormal physiological action of the cows and are therefore inherent in such milk, or whether they are due to bacterial ac- tion by udder microorganisms, is also a matter not experi- mentally determined. According to Weigmann certain species of the coli and aerogenes groups of bacteria, also Bacterium 1 Weigmann— My kologie der Milch, 1911, p. 132. 480 BUTTER Zopfii and Bacterium lactis innocuum, are capable of making- milk bitter. Jensen1 reports Streptococcus casei amari as a cause of bitter milk. Harrison2 discovered a lactose-fermenting yeast, which he gave the name Torula amara, that produced a bitter flavor in milk and cheese made in Canada. This organism produced an intense bitter flavor in 14 hours. His investigation showed that this yeast grows on the leaves of maple trees and contaminated the milk by being blown from maple trees into the milk cans which stood under these trees on the farms. It was necessary to steam these cans very thoroughly in order to destroy this germ. Conn, Burri, Duggeli, Freudenreich. Govini and others3 report numerous peptonizing microorgan- isms which are capable of rendering milk and butter bitter. Bitter milk and butter frequently also are the result of cer- tain feeds and weeds to which the cows have access, among these we find lupines, rag weed, beet tops, rye pasture (ex- cessive), raw potatoes, and especially many classes of decayed and moldy feed stuffs, and moldy bedding, moldy oat and barley straw. Butter may also derive its bitter flavor from the use of chemically impure salt, especially salt containing relatively large amounts of magnesium salts or calcium chloride, or both. Butter made from sour cream that has been overneutralized, or improperly neutralized, especially when lime is used as a neutralizer, is prone to show a bitter, limy, or so-called neutral- ized flavor. For proper neutralization which will reliably pre- vent bitterness from this source see Chapter VII on Neutral- ization. Oily Flavor. — Causes of Oily Flavor. — Oily flavor of but- ter is a frequent occurrence in creameries receiving sour cream, pasteurizing at a high temperature and cooling by turning the cream over a surface cooler. Butter which has an oily flavor gives the impression of having, and generally does have, in- ferior keeping quality. Experience has shown that such but- ter, when in storage often, though not always, develops other and more objectionable flavor defects, such as metallic flavor 1 Orla Jensen. Die Bakteriologie der Milchwirtschaft, p. 82. 2 Harrison. Landwirtschaftliches Jahrbuch der Schweiz 14, 1900. 3Weigmann. Die Mykologie der Milch, 1911. BUTTER DEFECTS 481 and fishy flavor. The oily flavor is more prevalent in butter made in summer than in winter. Oily butter is not suitable for storage. It usually scores a " Seconds." The specific reactions which produce oily-flavored butter are not well understood, but it is known from practical ex- perience that high temperature pasteurization and the use of a surface cooler for cooling the hot pasteurized cream, are prone to produce an oily flavor in butter. This is especially the case with cream that is excessively sour at the time of pasteuriza- tion. The pasteurization of very rich cream and of cream that has been much diluted with water also tends to make butter oily. Overworking of the butter under certain conditions has a similar effect. The oily flavor has also been attributed by some investi- gators to bacterial action. Jensen1 isolated an organism be- longing to the group of sour milk bacteria, which was capable, aside from curdling the milk into a solid clot in 24 hours, to produce an unpleasant odor and taste resembling that of ma- chine oil. The oily flavor was transmitted from the cream in which it developed to the butter. Others2 claim that oily but- ter is due to the action of microorganisms that decompose the fat, such as Oidium lactis, yeasts and liquefying bacteria. To what extent specific microorganisms are directly responsible for the oily flavor in butter is uncertain, but it is quite possible that they assist in bringing about such combinations of condi- tions as are conducive to the development of oiliness and there- by may become indirectly responsible for this defect. The oily flavor of butter occassionably may be due to causes other than those pertaining to the process of manu- facture. It has at times been found to be caused by the print- er's ink on the butter carton. In this case the oily flavor is usually especially pronounced on the surface of the print while the interior of the butter may be practically free from this defect. In the case of cartons with heavy, solid coloring, that are inclined to transmit to the butter an oily flavor, the danger can be greatly minimized, if not entirely prevented, by allowing 1 Russell— Outlines of Dairy Bacteriology, 1902, p. 158. * Marshall — Microbiology, 1911, p. 343. 482 BUTTER DEFECTS the cartons to dry out, either by aging them or by aerating them in a warm room, preferably with the aid of forced air cir- culation, or both. It is advisable to store all printed cartons in a dry room and preferably in a moderately warm atmosphere. This hastens the aging and drying of the ink and the expulsion of ink odors detrimental to the flavor of the butter. Prevention of Oily Flavor. — In consideration of the above observations concerning the causes of oily flavor in butter, at- tention to the following points may serve to overcome this de- fect or to avoid its recurrence : 1. Do not flash pasteurize cream that is high in acid. If the cream cannot be secured in sweet condition, standardize its acidity to about .25% acid before pasteurization. If this is not possible, use the vat or holding process of pasteurization. 2. Do not dilute cream with water. Instead of rinsing the cream cans with water to reclaim the remnants of cream they contain, blow these remnants of cream out of the cans with steam, inverting the cans over steam jets. 3. Use as little water as possible when rinsing cream and foam out of forewarmers and vats. It would be preferable to use skimmilk instead of water for this purpose. If the cream is too rich, containing above about 33% fat, dilute it with sweet milk, skimmilk, condensed milk or dissolved skimmilk powder. This adds solids not fat to the cream and assists in protecting the fat globules against mutilation during pasteurization. Stand- ardize all cream to about 33% fat before the cream is pas- teurized. 4. Do not run the flash pasteurizer at excessive speed. Use a machine of such capacity that crowding it is unnecessary. 5. Do not expose the hot cream, while cooling, excessive- ly to air and light. In the place of a surface coil cooler, use a cooler which protects the hot cream against these agents. If no such cooler is available run the cream from the flash pas- teurizer direct into the vats and do all the cooling in the vats, preferably with the covers partly down. 6. Do not overwork the butter. Regulate its moisture con- tent by proper adjustment of the churning temperature, rather than by an effort to reincorporate water into too firm butter by overworking. BUTTER DIRECTS 483 7. Use butter cartons only that are incapable of transmit- ting to the butter an oily flavor. Metallic Flavor. — By metallic flavor is generally under- stood a semblance in flavor to the astringent, puckery and metallic flavor, characteristic of the taste of metallic salts, such as are formed by iron, copper, zinc, etc., in acid solutions. This flavor defect is not always sharply defined, often be- ing accompanied by other, more or less pronounced off-flavors. Frequently it borders on oiliness, then again it approaches fishi- ness and occasionally it appears to be a nuance of tallowy flavor. Causes of Metallic Flavor. — While direct contact with metals and high acid in cream are undeniably essential and fundamental factors in the production of metallic flavor in but- ter, they do by no means always produce this defect. This fact suggests that the metallic flavor, similar to the fishy flavor in butter, is the result of a combination of condi- tions, of which all the necessary elements are not as yet def- initely known. Slight variations of the factors making up this combination, or slight variations in the extent to which the individual ele- ments of the combination are present, appear to make wide dif- ferences in the exact flavor defect produced. The result may be the characteristic metallic flavor, or it may be an oily flavor, a fishy flavor, or a tallowy flavor, etc. Thus experimental results of the writer show that under the majority of conditions, the presence of traces of such metals as iron or copper or their salts, in butter made from sour cream, causes such butter to develop a metallic or a fishy flavor, while the presence of the same metals, or their salts, in butter in which the acid has been completely neutralized, will produce a tallowy flavor. Since it is evident that traces of metals or metallic salts are an integral part of the combination of conditions that results in metallic flavor in butter, it is obvious that the condition of the utensils and equipment in which the milk and cream are handled and in which butter is manufactured, exerts a far- reaching influence on the production or prevention of metallic flavor. 484 BUTTER Thus the use of rusty utensils on the farm, the holding and shipping of the cream in rusty cans, the use of forewarmers, pasteurizers, coolers, vats, pipes and conduits, etc., in which the copper has become exposed and especially where the cop- per surface is not scoured thoroughly and regularly and is per- mitted to accumulate verdigris, furnishes a logical basis for the development of metallic flavor. Both iron and copper are most active in the presence of acid forming metallic salts. Therefore, this flavor defect occurs most prominently in butter made from cream that reaches the creamery in sour condition and is churned sour. Because of this fact, metallic flavor is generally more prevalent and more pronounced in summer than in winter butter, the cream con- taining more acid during the hot weather than during cold weather, although metallic flavor is by no means confined to summer butter, and may appear at any time of the year. Flash pasteurization, combined with the use of the sur- face coil cooler for cooling the heated cream, further invites metallic flavor, partly because the action of the sour cream in the presence of heat, air and light on the metal surface of the cooler, is intensified, and partly because this method of cool- ing may result in oily butter, which is often a forerunner or preliminary stage of metallic flavor. For similar reasons, rich cream (cream testing over 33% fat), and cream that is excessively diluted with water, tends to cause butter to develop metallic flavor. As explained under "Oily flavor," such cream contains a relatively low per cent of solids not fat and its viscosity is slight. This robs the cream of the protecting influence of the solids not fat, the fat globules are subjected to excessive mutilation during flash pasteurization and yield more readily to the oxidizing influence of heat, air and light, to which they are exposed, while the hot cream runs over the surface cooler. The ripening and holding of the sour cream in the copper vats and similar equipment for a prolonged period of time, such as holding it over night in vats with profusely exposed cop- per, may lend additional impetus to the development of metallic and similar off-flavors in butter, accelerating the action of the acid on the metal, and the oxidizing and catalizing action of BUTTER DEFECTS 485 the metallic salts on the ingredients of the cream and possibly enhancing also bacterial and enzyme action. Furthermore, in most vats several metals are exposed to the cream, so that it is not improbable that this bimetallic submersion in the acid of the cream, gives rise to a slight galvanic current, producing electro- lytic action which naturally hastens the formation of metallic salts. Finally, the churning of cream with a high acid content augments the acid content of the resulting butter and this furnishes an additional essential factor in the combination of conditions which cause metallic flavor. Attempts to attribute the metallic flavor to the presence in the cream of specific bacteria or groups of microorganisms experimentally, have proven abo'rtive. While bacteria, through their power to decompose portions of the ingredients of cream and butter, forming acid and other cleavage products, may assist to a limited extent in the production of metallic flavor, they cannot be considered as the specific cause of this defect. Nor is the fact that the metallic flavor often does not appear in the fresh butter, but develops after a considerable period of storage, necessarily indicative of bacterial origin. A careful study of the available data dealing with the causes of this but- ter defect emphasizes the complexity of the combination of factors and conditions responsible for the metallic flavor and the wide variations in the rapidity with which this defect de- velops. On the basis of the bulk of evidence it appears reason- able to attribute metallic flavor to chemical action. Prevention of Metallic Flavor. — According to our present limited lights on this subject, the most consistent means to prevent metallic flavor in butter is : 1. To use rust-free cream shipping cans and to return to the farmer cans only that are clean and properly rinsed and steamed and thoroughly dried. 2. To keep forewarmers, pasteurizers, coolers, vats, etc., well tinned, to thoroughly scour exposed copper surfaces, keep- ing them bright and free from verdigris, and to flush the entire system each day before use with hot water, thus removing any water it may contain and which may have absorbed metallic salts. 486 BUTTER 3. To protect hot pasteurized cream from air and light by cooling under cover. 4. To avoid excessive dilution of cream with water and to standardize all cream before pasteurization to about 33% fat or below with skim milk or milk, and to about .25% acid by the use of a suitable neutralizer, in the case of sour cream. 5. To not permit the cream to lie in the vats for an abnormal period of time and to churn it at an acidity of about .3% or below. Especially should cream not be held over night in improperly tinned copper vats. Fishy Flavor. — The fishy flavor is a defect especially com- mon with storage butter, though fishiness in fresh butter and butter only one to three weeks old, is by no means a rare occur- rence. Fishiness is a very serious butter fault, objectionable to most consumers and one which greatly depreciates the market value of the product. Fishy butter is shunned on the open mar- ket. It seldom grades above a poor "Seconds." Causes of Fishy Flavor. — Milk, cream and butter may be- come fishy in flavor when kept in close proximity to fish, in which case the dairy product absorbs the odor. The possibility of tainting butter from this source is pretty generally under- stood and recognized. In Great Britain and Ireland the law requires railway companies to provide separate cars for the carriage of fish and butter. Again, the fishy flavor of butter may be due to the cow herself. Weigmann1 reports a case where an individual cow which received the same feed and care as the rest of the herd, persistently produced a fishy milk. The fishy flavor of her milk was so marked that when mixed with the milk of the remainder of the herd, the mixed milk also became intensely fishy in flavor. In another case a cow produced milk with a fishy flavor only during the hot summer weather. This investigator further states that in Schleswig-Holstein, Germany,' the opinion prevails that cows yield fishy milk when they pasture in the marshes which are periodically flooded by the tide and on the grasses of which small crabs and other sea fauna dry and decay. Lew- kowitsch2 also reports that fishy butter is met with in Norway, 1 Weigmann— Mykologie der Milch, 1911, p. 124. 2 Lewkowitsch — Chemical Technology and Analysis of Oils, Fats and Waxes, Vol. II, 1914, p. 798. BUTTER DEFECTS 487 being obtained from cows fed on fishmeal. In contradiction to the above, Weigmann writes that even in the case of intensive feeding of herring meal or whale meal neither the milk nor the butter show signs of fishiness. Harding, Rogers and Smith1 investigated the cause of fishy flavor and odor in milk brought to the New York State Experi- ment Station by a milk dealer. This fishy taint was so pronounced that the milk was of no commercial value, although coming from a dairyman of more than ordinary carefulness in the handling of his herd. They found that the defect was confined to the milk of one cow that was fed on the same feed and received the same care as the other animals in the herd. This cow was apparently in normal condition. Bacteriological study of her milk revealed no microorganisms capable of producing the fishy flavor. Piffard2 suggests that the salt, owing to its ability to absorb odors and flavors of material in close proximity, may occasionally be responsible for fishy butter. This is improbable, the salt has the power to intensify flavors but it does not readily absorb flavors. The same author holds that frequently fishy butter may be due to impure water with objectionable flavor, to which the cows may have access and which he attributes to the devel- opment of diatoms and algae, notably the Oscillaria. These cases of mechanical absorption by milk or butter of the fishy flavor, or of fishy flavor caused by an abnormal condi- tion of the cow or the milk, are comparatively rare. The great majority of causes of fishy-flavored butter on the market is due to causes, deeper seated, more complex and more difficult to prevent. The seriousness of the defect and the difficulty of avoiding it are augmented further by the fact that the fishy flavor of most of the commercial butter does not show up at the churn. In aggravated cases it may develop within the first few weeks after manufacture, but in the great majority of cases it develops while the butter is in cold storage. The earlier studies of fishy flavor in butter and its causes, dealt largely with efforts to discover specific bacteria or other 1 Harding, Rogers and Smith. Notes on Some Dairy Troubles. New York State (Geneva) Agr. Exp. Sta. Bull. 183, 1900. 2 Piffard. Fishy Flavor in Butter. New York Produce Review and Am. Creamery, Vol. 13, No. 20, 1901. 488 BUTTER DEFECTS micro-organisms capable of producing this flavor. O'Callaghan1 attributes fishiness in butter to the mold Oidium lactis. He claims that this organism when grown in conjunction with Bacil- lus acidi lactici in cream produces fishiness invariably. Harrison2 classes the fishy flavor of butter with bitter, putrid and lardy flavors, the causes of which he attributes to the pres- ence and growth of undesirable microorganisms in the cream. Jensen3 found certain species of yeast that give butter a fishy flavor. Klein,4 speaking of oily, fishy and tallowy butter, holds that all these butter defects may well be considered specific forms of rancid butter, resulting from the action of bacteria. Hammer5 isolated from a can of evaporated cream, which had de- veloped a fishy odor, a bacillus of the Proteus group, which he named Bac. ichthyosmius. With this organism he was able to reproduce the fishy odor in milk, cream and evaporated milk. When inoculated into butter, either direct, or into sweet or sour cream, the butter failed to show fishy odor or flavor. The later studies and observations relating to the causes of fishy butter indicate that the direct cause of fishy flavor and odor in commercial butter is attributable to chemical action rather than to bacterial development. Fleischmann6 states that fishy and oily flavor is a butter defect which appears only in butter made from sour cream, that it shows itself as an augmen- tation of an aroma characteristic of this class of butter, carried to the point where it becomes offensive to taste, and that it is caused by certain species of bacteria which develop in the cream during souring and associatively with the lactic acid ferments. Rogers7 found that in all cases where butter became fishy, the butter was made from high acid cream, both in the case of acid produced in the cream by bacteria, and of acid in the form 1 O'Callaghan — "Cause and Remedy of Fishy Flavored Butter." The Agr. Gazette of N. S. Wales, Vol. 12, p. 341, 1901. O'Callaghan — "Butter Classification.' The Agr. Gazette of N. S. Wales, Vol. 18, p. 223, 1907. O'Callaghan' — "That Fishy Flavor." Chicago Dairy Produce, April 25, 1916, p. 8. 2 Harrison — "Defects in Butter." Twenty-seventh Annual Report On- tario Agr. Exp. Sta., p. 79, 1901. 3 Jensen — Die Bakteriologie der Milchwirtschaft, 1913, p. 24. * Klein — Milchwirtschaft, 1914, p. 238. 5 Hammer — Fishiness in Evaporated Milk. Iowa Research Bui., 1917. 6 Fleischmann— Lehrbuch der Milchwirtschaft, 1915, p. 322. 7 Rogers— Fishy Flavor in Butter. U. S. Dept. Agr., B. A. I. Circular 146, 1909. BUTTER DEFECTS 489 of lactic acid and acetic acid added to sweet cream, although cream with high acid did not uniformly develop fishiness. He further states that overworking of butter produced fishiness with a reasonable degree of certainty. He offers the opinion that fishy flavor is caused by a slow, spontaneous, chemical change to which acid is essential and which is favored by the presence of small amounts of oxygen, and that it may be pre- vented with certainty by making butter from sweet cream; also that butter made from pasteurized cream with a starter but without ripening seldom, if ever, becomes fishy. In a subsequent publication, dealing with results on the Manufacture of Butter for Storage, Rogers, Thompson and Keithley1 show still more conclusively the freedom from fishiness in butter made from unripened pasteurized cream, and the ten- dency of butter made from ripened, raw or pasteurized cream to become fishy in storage. Dyer2, as the result of a chemical study of fresh and stored butter, concludes that "the production of off-flavors" so com- monly met with in cold storage butter (and of which the fishy flavor is a very prominent one) is attributable to a chemical change expressed through a slow oxidation progressing in some one or more of the non-fatty substances occurring in buttermilk. The extent of this chemical change is directly proportional to the quantity of acid present in the cream from which the butter was prepared. Dyer further emphasizes that the development of undesirable flavor in butter held in cold storage at a tempera- ture of 0° F. is not dependent upon an oxidation of the fat itself* The writer's experience has been fully in accord with the findings of Rogers and Dyer, to the effect that high acid cream and overworking of butter are conditions favorable to the devel- opment of fishy butter. Fishy butter is very closely related to oily and metallic butter. It appears to be the result of a com- bination of certain factors, one of which is high acidity and another a weak body of butter due to overworking, which destroys the grain and excessively exposes the butter to the action of air. Other factors may embrace the presence in the 1 Rogers, Thompson and Keithley — The Manufacture of Butter for Stor- age, U. S. Dept. Agr., B. A. I. Bulletin 148, 1912. 2 Dyer — Progressive Oxidation in Cold Storage Butter. Jour. Agr. Re- search, Vol. VI, No. 24, 1916. 490 BUTTER DEFECTS eream and butter of metallic salts, such as iron and copper lac- tates, which act as oxidizers and catalizers, and the presence in the cream and butter of diverse ferments and their products. Prevention of Fishy Flavor. — In order to minimize the danger of butter going fishy before, during and after cold storage, attention to the following phases of manufacture is recom- mended : 1. Secure as fresh, sweet and unfermented cream as pos- sible. Systematically grade the cream for quality and churn first and second grade separately. 2. Use only non-rusty cans that are thoroughly cleaned, rinsed, steamed and dried before they are returned to the farmer. 3. Keep the copper surfaces in forewarmers, pasteurizers, coolers and vats well tinned, do not permit exposed copper sur- feces to become coated with verdigris, wash all forewarmers, pumps, pasteurizers, coolers, vats and conduits thoroughly each day and flush them out again with hot water immediately before use the next day. 4. If the cream arrives at the creamery sour, neutralize it to about .25% acid. 5. Do not dilute cream with water. If cream is too rich, standardize it to about 33% fat by the addition of sweet milk or sweet skimmilk. 6. Pasteurize all cream, but do not run the heated cream over an open surface cooler. Protect it against excessive ex- posure to the air and light. 7. Churn the cream with an acidity of .3% or below. 8. Do not overwork the butter. Tallowy Flavor. — This butter defect refers to butter which has a distinct taste and odor of spoiled tallow. Tallowy butter is usually, but not always, bleached in color, and may be en- tirely white. Very old tallowy butter may change to a pinkish brown color. Tallowiness is a defect which renders butter utterly unfit for the market. Butter may, and frequently does develop a tallowy flavor and odor and a bleached color within a few weeks of the date of manufacture, though this defect usually requires from three BUTTER DEFECTS 491 to six weeks to become pronounced under commercial condi- tions of handling butter. Tallowiness is not a usual cold stor- age defect of butter. In commercial cold storage, butter seldom goes tallowy. This defect develops primarily in butter lying in stores and exposed to rather high temperatures (room tem- perature). Tallowiness is more prevalent in print butter than in tub butter. The tallowy flavor and the bleaching start on the surface of the butter and gradually work into its interior. But- ter may have turned very tallowy and perfectly white on its surface, while the core of the package may still have the nor- mal yellow color, and be free from the tallowy flavor. Causes of Tallowy Flavor. — Tallowiness, similar to ran- cidity, is due to a decomposition of the butterfat. These two flavor defects often occur in the same piece of butter and have frequently been confused, or considered synonymous. This con- fusion is unfortunate, inasmuch as it has led to misleading in- terpretations of experimental results, rendering difficult the establishment of their true causes and hindering efforts in- tended toward their prevention. A careful study of the causes of tallowy butter shows that, unlike rancidity, which is the result of hydrolysis of the fats, tallowiness is due to oxidation. On the basis of our present knowledge1 relating to tallowy butter, the causes and prevention of this defect may consist- ently be summarized as follows: 1. Oxidation the Cause of Tallowy Butter. — The butter defect known as tallowy odor and flavor is the result of a process of oxidation. The oxidizing action may, or may not, be on the fat, according to agencies and conditions favoring the oxidation, as outlined in succeeding paragraphs. 2. Exposure to Air, Light and Heat. — Air readily brings about oxidation of the fat in butter, and this oxidation is greatly intensified in the presence of light and heat. Butter so exposed is prone to rapidly develop a tallowy flavor. This fact is well known to the layman. Tallowiness, caused through these channels, is comparatively rare, because the great bulk of commercial butter is guarded against these agents. The wrap- a Hunziker and Hosman, Tallowy Butter, Its Causes and Prevention. Journal of Dairy Science, Vol. I., No. 4. 1917. 492 BUTTER pers and cartons of print butter and the liners and paraffined tubs and cubes of bulk butter, protect the butter against exces- sive exposure to air and light. While the butter remains in the creamery, it is usually kept at a temperature considerably be- low that at which heat alone is capable of producing tallow- mess. Butter intended for immediate consumption (within one to three weeks) does not become tallowy, even at ordinary ice box temperature, such as it is exposed to in the store and in the home, unless it contains other agents that cause tallow- iness. The bulk of the butter going to the tropics is packed in hermetically sealed tin cans, excluding the air and light and thereby greatly minimizing the action of heat. Butter intended for prolonged storage, rarely develops tallowiness, because the low temperature of commercial cold storage sufficiently retards the action of air and light. Although under present commercial conditions of manufacture and handling of butter, air, light and heat are improbable causes of tallowiness, their importance should not be ignored and every effort should be made to pro- tect butter against these agents. To run the hot pasteurized cream over a surface coil cooler} located near windows with transparent panes or with open sash, where it is exposed to the direct sunlight, and possibly to air currents; to keep the pasteurizing vats open during the entire process of heating, holding and cooling; to work butter on an open table near the window, and to expose the butter in the print room and later in storage excessively to air, light and heat, are dangerous practices, which jeopardize quality and may readily lead to tallowy flavor in butter. 3. Presence in Cream and Butter of Metals and Metallic Salts. — Oxidizing agents, such as metals and their salts, are capable of turning butter tallowy in a very short time. These agents act as oxygen carriers or catalizers. Iron and copper and their salts, also the alloys of copper, such as brass and German silver, belong to this class. The copper, copper salts, and the alloys of copper are the most active metals, metallic salts and alloys that enter into the problem in commercial butter- making. Iron oxide also has specific catalytic action which aids the oxidation process, while in the case of iron bases and BUTTER DEFECTS 493 salts the action is relatively slight. Nickel and tin are practi- cally negative in this respect and do not produce tallowy flavor in butter. Most of the equipment used in the handling of cream and the manufacture of butter is constructed of iron or copper, usu- ally originally coated with tin. When this tin coating wears' off, as it always does to a greater or less extent, the iron or copper becomes exposed, and often the exposed iron is permitted to rust and the exposed copper allowed to become coated with verdigris. In this condition, these metals are most active, con- siderable portions being dissolved by the acid in the cream and thereby not only act in the cream, but also find their way into the butter, jeopardizing its quality and inviting the development of tallowy flavor. This danger can best be minimized, if not entirely avoided, by furnishing the farmer with bright and non-rusty cans and by preventing the cans from rusting, by systematic and thor- ough washing, rinsing, steaming and drying; keeping weigh cans, forewarmers, pasteurizers, coolers, pumps and pipes and conduits well tinned, thoroughly cleaning and steaming them after each day's use and flushing them with hot water each morning- before circulating the cream, so as to remove any remnants of water of the previous day which may be pregnant with metallic salts; removing the rust from all parts of the packing and printing equipment and using wrappers and liners only which are free from metallic specks. Water used for washing butter should be free, or nearly so, from iron. 4. Presence in Butter of Excess Lactose. — The presence in butter, in excess, of specific compounds which are themselves readily oxidized may yield tallowy flavor, as one of their oxida- tion products. To these compounds belong lactose, glucose and glycerol. Danger from these products need be considered only, however, when the cream or butter is subjected to alkaline con- dition, as shown in the succeeding paragraph. When butter is made under proper conditions, and containing a normal amount of acid, the presence of lactose and similar compounds has no injurious effect on its flavor and does not, in itself, con- stitute a cause of tallowy butter. In fact, the addition of lac- 494 BUTTER DEFECTS tose to butter, when in normal acid condition, may have a slight preservative effect, improving its keeping quality. 5. Neutralization. — The presence of an unnatural alkaline condition of the butter, or of the cream from which the butter is made, accelerates any oxidizing action by rendering the compounds capable of oxidation, more susceptible to oxidation. Over-neutralization with any alkali very greatly intensifies the oxidizing action of all the foregoing agents and hastens the development of tallowiness. This can be permanently pre- vented only by careful standardization of the entire operation of neutralization, including the testing of cream for acid, the prep- aration of the neutralizer and its addition to the cream. Guess work in neutralization is one of the most potent causes of tal- lowy butter. The butter should further be protected against direct contact with alkalies, by the complete removal from churns, cubes and diverse packing equipment, of all traces of alkaline wash water, and by the use of parchment wrappers that are free from alkali, such as ammonia, which is used to neutralize the sulphuric acid employed in the parchmenting process. Storage Flavor. — Where butter is held for any considerable length of time in storage, it gradually surrenders some of its delicate flavor and aroma which is characteristic of good fresh butter, and develops a peculiar flavor known to the butterman as the storage flavor. In butter of good quality this change takes place very slowly and is for a long time hardly perceptible. Rogers1 reports that, in examining some millions of pounds of butter made and stored for the U. S. Navy Dept., sweet cream butter, almost without exception, kept through several months' cold storage with only slight changes in flavor. In butter of in- ferior quality the storage flavor generally develops rapidly. Other conditions being the same, the rapidity with which the storage flavor develops depends largely on the temperature of storage and on the time and temperature at which the butter is held before it enters cold storage. The lower the tempera- 1 Rogers, Factors Influencing Changes In Storage Butter. Address at the Third International Congress of Refrigeration, Washington-Chicago, 1913. BUTTER DEFECTS 495 ture of cold storage and the shorter the time that elapses be- tween manufacture and cold storage, the longer will the butter generally retain the desired aroma and flavor of fresh butter. The exact cause of this flavor and the nature of the decom- position products responsible for it have not been conclusively demonstrated. Experimental data suggest that this flavor is principally due to spontaneous chemical changes, in which oxidation plays an important part and that this oxidation is accelerated by the presence of catalyzers in the form of metallic salts. Butter made from a poor quality of cream, such as cream that has yielded excessively to fermentation and that is of high acidity, develops storage flavor and its derivatives most rapidly. It is not improbable also that the storage flavor represents a forerunner, or early stage, of other off-flavors which under favor- able conditions may supersede it in the form of metallic flavor, or fishy flavor, etc. Rancid Flavor. — Rancidity is fa very common and Well known butter defect. The rancid or strong flavor is a charac- teristic infirmity of old butter. When present to a pronounced extent in butter, such butter is no longer salable as "eating" butter and generally has to be disposed of as packing stock at a great sacrifice in price. Cause of Rancid Flavor. — Rancidity is a flavor and odor de- fect that is due to decomposition of the butterfat. It is char- acteristic not only of spoiled butter or butterfat, but is a common decomposition product of all fats and oils, animal and vegetable. The chemistry of the reactions yielding rancid flavor and odor is not well understood, though it has been the subject of ex- tensive investigations for many years. In the case of butter, rancidity, and especially the initial phase of rancidity, appears to be due to hydrolysis of the butter fat, which splits the glycerides of the fats into free fatty acids and glycerol. This hydrolysis is in all probability due very largely to bacterial and mold action, since the casein and lac- tose contained in butter furnish the food elements necessary for the bacteria to thrive on. The hydrolysis of the fat leading to rancidity, however, is not necessarily dependent on micro-organisms. It may be 496 BUTTER DEFECTS brought about in pure butter fat and other fats which do not contain bacterial life, by enzymic action in the presence of mois- ture. Air, light and heat, and the presence of catalizers, such as acids and alkalies, favor the development of rancidity. In the case of butter, however, it is conceded by the best authorities that bacteria and molds are the chief factors that hydrolize the fats, making the butter rancid. Jensen1 and Kirch- ner2 demonstrated that certain species of micro-organisms, very commonly present in butter, are capable of hydrolizing the fat in butter to a very marked degree and of producing butter with an intense rancid odor and flavor. The chief of these organisms are Oidium lactis, Cladosporium butyri, Bacillus fluorescence liquefaciens and Bacillus prodigiosus. Lewkowitsch3 suggests the possibility that even in the case of rancidity produced by these micro-organisms, the hydrolysis may be due to enzymes produced by them rather than by their direct action on the fat. It is generally accepted that in butter the rancid flavor and odor are due to the presence of the free fatty acids resulting from hydrolysis, and it is well known that especially the volatile fatty acids, such as butyric, etc., have a pungent odor that resembles the rancid odor and flavor of butter. The free fatty acids re- sulting from fat hydrolysis are expressed as, and determined by, the acid value of the fat. The acid value would therefore ap- pear to be a logical and correct measure of the degree of ran- cidity of the butter. And in a great many cases rancid butter is accompanied by a high acid value, as Jensen has shown. However, there is a vast volume of experimental data on record which shows that quite often butter may have intense rancidity while the acid value of the fat from this butter shows no appreciable increase over the acid value in fat from the same butter when fresh, and instances are also recorded where a relatively high acid value was not accompanied by a pro- nounced rancid character of the butter. In fact the fat of per- fectly fresh butter shows a considerable acid value. It is therefore quite probable that even in the case of butter, 1 Jensen — Ueber das Ranzig-werden der Butter, Laridw. Jahrb. d. Schweiz. 1901. 2 Kirchner — Berichte d. deutsch. botan. Gesellschaft, 1888, p. 101. 8 Le-wkowitsch — Chemical Technology and Analysis of Oils, Fats and Waxes, Vol. I ,p. 53 ,1914. BUTTER DEFECTS 497 hydrolysis is only the initial phase of rancidity and that either the free fatty acids, or the glycerol, or both, undergo further de- composition yielding products which produce and intensify ran- cidity in butter, and this further decomposition must of neces- ity be an oxidation. In the case of the saturated fatty acids, the action would be only very slight and if at all, it would probably be of enzymic nature. The unsaturated fatty acids, of which the oleic acid is representative, yield more readily to oxidation. They may be oxidized forming fatty acids of higher molecular weight, such as acids of the hydroxy series. Or they may be broken down to acids of lower molecular weight, forming various fatty acids such as pelarg-omc, azelaic acid, etc., which may produce or intensify the rancid odor and flavor. Also aldehydes formed by the breaking down of oleic acid may play a part in the pro- duction of rancidity ; this possibility, however, Lewkowitsch does not consider probable. That the oxidation of the free fatty acids plays a considerable role in the production of rancid butter, is therefore very probable, and is emphasized by the fact that exposure of the butter to air, especially in the absence of re- frigeration, and in the presence of light which intensifies oxida- tion, greatly hastens the development of rancidity. Allen2 also holds that oxygen and light play a considerable part in the chain of factors instrumental in the production of rancidity. Again it is possible that the free glyverol, resulting from the hydrolysis of the fats, and which in itself is neutral, odorless and tasteless, may yield to oxidation, forming acids and alde- hydes, many of which have a very pungent odor resembling ran- cidity. Browne1 attributes the pungent, irritating odor which all rancid fats give off, especially on being warmed, to the de- composition (oxidation) of free glycerol, forming acrolein. He found a decrease in the percentage of glycerol of all fats when they become rancid, the decrease being proportional to the ran- cidity of the samples. Furthermore, the lactose of butter, upon oxidation, may assist in the development of products, similar to those result- 1 Allen, Commercial Organic Analysis, Vol. II, 1912, p. 313. 8 Browne, A Contribution to the Chemistry of Butterfat, Jour. Amer. Chem. Soc. Vol. 21. 1898. 498 BUTTER ing from the oxidation of glycerol and thereby constitute a fac- tor tending toward the production, modification or intensification of -the rancid odor and taste. The small amount of lactose nat- urally present in commercial butter, however, must of necessity limit the power of this butter constituent as an important agent in this respect. < In the presence of our now available information concern- ing the reactions responsible for rancidity in butter, as briefly outlined in the foregoing paragraphs, the following summary may serve to bring out the most important facts and proba- bilities. 1. The initial stage of rancidity in butter lies in the hydro- lysis of the butterfat. This produces free fatty acids which, when present in considerable amounts, produce a strong rancid taste and odor. 2. The hydrolysis of the butterfat is brought about by bacterial and mold action, or by enzyme action, assisted by cat- alizers such as acids and alkalies, and in the presence of water and exposure to temperatures higher than those of commercial refrigeration of butter. 3. The rancidity of butter may be greatly intensified by the oxidation of the free fatty acids, or of the free glycerol, or both. The action is greatly hastened by exposure of the butter to air. light and heat. 4. Lactose, upon oxidation, may also assist in the forma- tion of products yielding rancidity. 5. The curd in butter assists in the development of ran- cid flavor insofar as it furnishes desirable nutrients for the ran- cidity-producing organisms to thrive on. Butter with a high curd content, other factors being the same, therefore is more prone to become rancid than butter with a low curd content. It should be understood that rancidity is the result of pro- gressive changes in butter and that most butter, if kept long enough, will ultimately become rancid with age. However, the development of rancidity and the postponement of this common butter defect may be controlled with a reasonable degree of suc- cess, by so handling the cream in its production and the butter in its manufacture and storage, as to minimize, if not eliminate BUTTER DIRECTS 499 entirely, the agencies which are known to contribute towards the appearance of rancid flavor and odor in butter. Attention to the following points will assist towards the prevention of rancidity in butter. Prevention of Rancid Flavor. — 1. Elimination ; of bacteria and mold from butter. The fresher and sweeter the cream and the greater its freedom from objectionable bacteria and mold and from their products, and the freer the butter from curd, the* better will such butter withstand decomposition which results in rancidity. 2. Proper pasteurization of the cream and thorough washr ing of the butter with pure water greatly lessens the tendency of butter to become rancid. Pasteurization destroys the germs capable of producing rancid butter. Thorough washing removes much of the curd and therefore reduces the necessary foq4 available for rancidity-producing microorganisms. Farm-made butter usually develops rancid flavor and odor very rapidly, because it is made from raw cream teeming with germlife and usually contains excessive buttermilk. Storage butter made dur- ing a pasteurization experiment under the direction of the author1 did not develop rancidity when made from pasteurized cream; raw cream butter when made from ungraded gathered cream almost invariably became rancid, while raw cream butter made from selected gathered cream did not show much rancidity in storage. This emphasizes both, the value of pasteurization and the importance of careful grading of cream. The housewife in many European countries, who purchases a year's supply of cook- ing butter (Schmelzbutter) melts and boils it until the curd, water and other non-fatty constituents have settled out and the fat has become clear. This fat is stored in a cool place (the cellar) in crocks, covered writh parchment, and keeps almost in- definitely (until used up) without showing signs of rancidity. These illustrations emphasize that rancidity can be greatly de- layed by removing germ life and the food on which micro- organisms thrive. Efficient pasteurization, and thorough wash- 1 Hunziker, Spitzer and Mills, Pasteurization of Sour, Farm-Skimmed Cream, Produce Bulletin 208, 1918. 500 BUTTER ing of butter accomplish this to a large extent, provided that recontamination of cream and butter is avoided by sanitary con- ditions of vats, churns and packing equipment and proper treat- ment of tubs, cubes, liners and wrappers. 3. Protection of the butter against air, light and heat, and the absence in it of catalizers, such as metallic salts, high acid, or alkali, will minimize the action of rancidity-producing agencies which may be present in butter. Churn the cream at a low acidity, do not overneutralize and put the butter in the sealed package, and refrigerate it, as promptly as possible after manu- facture. Woody Flavor. — This is not a very common flavor defect of butter, though "epidemics" of woody-flavored butter have occurred, causing serious objection on the market. The most common cause of butter with a woody flavor is probably the churn. New churns that have not been properly" treated before use, may impart to butter a woody flavor. Churns also that are in unclean condition, or the wood of which has become decayed, may become infested with certain species of microorganisms, especially molds, that are capable of giving the butter a woody taste. Such conditions are especially liable to happen with churns that are not in daily use, giving the micro- organisms an opportunity to work into the cracks between the staves and also into the pores of the wood, where they are diffi- cult to be reached, dislodged or destroyed, and where they form a continuous source of contamination of succeeding batches of cream and butter. A case of this type, resulting in woody-flav- ored butter, was noted and investigated at Purdue University1. The churn that produced the woody flavor was used only once per week. Investigation showed that the woody flavor was due to a mold lodged in the cracks of an apparently clean churn. This mold produced the same intense woody flavor when inocu- lated and propagated in sterile milk. For treatment and disin- fection of churns see "Preparation of Churn," Chapter X. Salt, packed in barrels of decayed and infected wood, is also known to be capable of transmitting to butter a woody flavor. 1 Hunziker and Switzer. Results not published, 1916. BUTTER DEFECTS 501 Butter packages, such as tubs, cubes and cartons made of wood which naturally harbors an intensive woody odor, always lend butter a woody flavor. Hence, pine tubs, boxes and cartons are entirely unsuited for packing butter, while spruce, white ash, hemlock, etc., well cured and dried and when properly soaked before use, are generally free from this objection. However, even spruce and white ash tubs may give butter in storage a pronounced woody flavor. In such cases the woodi- ness is usually confined to the surface of the butter at the bot- tom and side, the interior remaining free from it. The flavor at or near the outside, however, is frequently intensely woody and pound prints cut from the outer portions of such butter may be practically ruined from the standpoint of the market. When butter is stored in tubs made from well seasoned, sound lumber of white ash or spruce, and when they are prop- erly treated before packing, the danger from woodiness is very remote. But when the tubs are made up of a poor grade of lumber, and especially of pithy stayes, or lumber that is green and has not been well seasoned and dried, or lumber felled while still in sap, the woody odor is very intense and there is great danger of woody flavor in butter. This danger can be minimized, if not entirely overcome, by soaking the tubs over night in brine, preferably hot brine, and by drying and heating them thoroughly over a steam jet before paraffining, so that the paraffine will soak well into the wood, forming a uniform and complete coating that will permanently stick and not peel off. For further directions see "Preparation of Butter Tubs," Chapter XII. Cooked or Scorched Flavor. — As the name implies, this flavor is the result of exposure of the product to heat. It does not often appear in raw cream butter, but is a frequent defect of butter made from pasteurized cream. It is generally due to heating to excessively high temperature or to prolonged exposure to the heat, or improper application of the process of pasteur- ization. It is probably the direct cause of the action of heat on the caseous matter of the cream. Most of the butter made from pasteurized cream has a slight pasteurized, or cooked flavor when fresh. This slight cooked 502 BUTTER DEFECTS flavor, however, disappears in a short time. Only a strong cooked flavor is permanent in butter and is therefore objection- able. Crowding the pasteurizer and the consequent use of too much steam pressure is a common cause of cooked flavor. When pasteurizing under such conditions, the caseous matter in the cream that comes in direct contact with the overheated heating surface becomes scorched and bakes on to the heating surface. The scorching of the cream on the overheated coil of the pasteurizer is also very often the cause of the scorched flavor. When butter made from raw cream has a cooked flavor, the cause usually lies in overheating the coil in the forewarmer, by forcing steam through it excessively. In this case the coil usu- ally becomes heavily coated with a layer of burnt cream. It is advisable to heat the coil in the forewarmer with hot water instead of steam, in order to avoid the cooked flavor .in butter. The cooked flavor is occasionally confused with the oily flavor, which is also a frequent characteristic of butter made from improperly pasteurized cream, as explained under "Oily Flavor." The two flavor defects have nothing in com- mon, neither in their origin, nor in their relation to the market value of the butter. The oily flavor is a serious butter defect which is generally indicative of poor keeping quality. The cooked flavor is not seriously objectionable, nor does its pres- ence unfavorably reflect on the keeping quality of the butter. Coarse Flavor. — This is a rather indefinite and general ex- pression of butter flavor. It refers to butter that lacks the char- acteristic delicacy of flavor of good butter, though the butter may have no specific "off-flavor." Butter with a coarse flavor is usually the result of high acid cream, or overripened cream or overripened starter and excessive salt. The combination of high acid and high salt seems to be particularly favorable for the production of this so-called coarse flavor, and the presence of undissolved salt crystals further intensifies this defect. Butter, the flavor of which is termed coarse, is generally not looked upon with favor on the open market. If it shows no other specific defect it usually grades as a poor "Firsts." Its keep- ing quality is considered questionable, if not unreliable. BUTTER DEFECTS 503 DEFECTS IN BODY AND TEXTURE. Properly made butter has a firm body and a waxy texture. The body and texture of the butter are controlled by the char- acter.of the butter fat and the churning temperature primarily, and by the conditions incident to the churning, washing, salt- ing and working of the butter. The character of the butter fat is largely determined by its chemical composition and the size of the fat globules, factors which in turn are controlled by breed, period of lactation and feed of the cows, as explained fully in the chapter on the "Conditions which Affect the Churn- ability of Cream," Chapter X. Weak-Bodied Butter. — Such butter lacks a firm, solid body that will stand up well under unfavorable temperature conditions. It softens quickly upon exposure to temperatures of about 65° F. and above. It also is prone to show excessive leakiness. But- ter with a weak body is usually the result of too high a churn- ing temperature, or not holding the cream at the churning tem- perature long enough before churning. It may be due also to overworking, especially when excessively soft. The fundamental cause of a weak body generally lies in the fact that the cream from which the weak-bodied butter is made was never sufficiently cooled to adequately chill and harden all the butterfat, especially those fats that have a relatively low solidifying point. The butter from such cream then contains a mixture of fats, all of which have not been congealed and some of which are still in a liquid or semi-liquid state. Under these conditions the mixed fat, representing the butter, lacks firm- ness, it is "weak," and its mechanical stability readily collapses when the butter is exposed to room temperature, or to higher temperatures, though these temperatures may be considerably below the melting point (90—99° F.) of mixed butterfat. For the same reason a weak bodied butter results when the cream, though it may have been cooled to the proper tempera- ture, is not held at that temperature long enough to enable the fat to actually partake of the low temperature. The defect is further intensified when this weak-bodied but- ter is excessively worked in this soft condition. The proper temperature to which cream must be cooled, in 504 BUTTER DEFECTS order to prevent the weak body varies considerably with such factors as breed of cows, period of lactation and feed ; the relation of these factors to the churning temperature and to the firmness of the butter is fully explained in Chapter X- " Churning." For the assistance of the buttermaker the prevention of weak-bodied butter may best be summarized as follows: 1. Thoroughly chill the cream and hold it at the low tem- perature not less than two to three hours before churning. 2. Do not guess at the churning temperature but determine it accurately with a correct thermometer. 3. When deciding what the churning temperature should be, be guided by the firmness or softness of the previous churn- ing and by the time required to complete the churning process. 4. Other conditions being the same, have the cream at that churning temperature at which the butter will break in about 40 to 50 minutes. 5. Butter that breaks in 20 to 25 minutes is prone to have a weak body. The cream from which it was made either was not cooled low enough or not held long enough at the low temperature. 6. Cool the cream, according to conditions, to temperatures within the range of about 45° to 53° F. in summer and about 54° to 60° F. in winter. This refers to cream churned in the middle western states. 7. In case the butter comes exceedingly soft, let it rest, in granular condition, in cold water or ice water until it has hardened, so it can be handled and worked without serious danger of becoming greasy. 8. Do not overwork soft butter. 9. Points 7 and 8 do not prevent weak body, at this stage the weak body is already an accomplished fact. But they may help to minimize the unfavorable consequences of the defect. Greasy Body. — Butter becomes greasy when worked ex- cessively while in very soft condition, due either to too high churning temperature of the cream, too rich cream, or holding the butter in the churn too long before working, allowing it to warm up, or working it on a table worker in a warm room. Greasiness can be avoided by so governing the churning tern- BUTTER DEFECTS 505 perature, the period of holding the cream at that temperature and the temperature of the wash water, as to make the butter have a firm body when it is worked. The butter should be churned to small granules and preferably washed with water a few degrees colder than the temperature of the buttermilk. The danger of greasiness is especially great when churning cream rich in fat, such as cream testing 35 per cent, fat or over. Thin cream may be churned at considerably higher temperatures without danger of yielding a greasy butter, than rich cream. Rich cream should be churned at a relatively low temperature and should be held at that temperature at least three hours be- fore the churning process commences. Greasiness may be due also to allowing the butter to be- come very soft before it is worked as frequently happens in summer in a warm churn room where the butter is held unduly long in the churn or is worked on an open worker. For the above reasons greasiness is a very common defect of farm dairy butter, where facilities for cooling the cream and for working the butter in a cool room are usually lacking during the summer season. Salvy Body. — Salvy butter is butter in which the grain has been destroyed to the extent to where the granules have com- pletely lost their identity. This defect is prone to appear in butter that is overworked when in a very firm condition, espe- cially when the working is done in the absence of water. In exceptional cases the salvy body is due to conditions independ- ent of the working process, and may occur as the result of abnormal churning conditions. In winter when, owing to the advanced stage of the period of lactation of the great majbrity of the cows, and also owing to the character of the feed ration, the cream is very viscous and contains relatively small fat glob- ules, the cream churns with difficulty. If this cream happens to be very thin and has been exposed for a long time to a low temperature, as is frequently the case with hand separator cream, the solidification of the fat globules may have reached such a stage that these globules are so firm that they coalesce with great difficulty. This prolongs the churning process and frequently from one to three hours are required to make the butter "break" and to form large enough granules for conveni- 506 BUTTER DEFECTS ent handling. This abnormally prolonged agitation causes these firm globules and small firm granules to grind against each other and to strike the sides of the churn until they completely lose their identity, destroying the grain and giving the butter a salvy body and texture. Such butter is also prone to be abnormally high in moisture. A raise in the churning temperature of cream of this character sufficient to make the butter come reasonably soft, will shorten the time required for churning and avoid the production of butter that is salvy. Crumbly Body. — The brittle and crumbly texture of butter is characteristic of butter made in late fall, winter and early spring. Most creameries are troubled with this defect to some extent during the winter season. While its consequences are not fatal, the buyer demands a waxy body that permits of draw- ing a smooth plug with the trier and the consumer criticises butter that refuses to spread on account of its brittleness. The hotel and restaurant trade particularly objects to crumbly but- ter, because they find it very difficult to cut it into neat slabs and cubes ready for the table. Crumbly butter refuses to respond to knife or wire. On a weak market, crumbly butter often sells at a sacrifice. Causes of Crumbly Body. — There are two fundamental causes of crumbly butter, neither of which is under the control of the butter maker, namely, the cow and the feed. In winter the great majority of the cows are well advanced in their period of lactation. Cream from stripper cows contains predominat- ingly very minute fat globules. The small fat globules do not bind, together readily when the cream churns, they are firm and persist in retaining their individuality. They do not yield so readily to the forces which overcome the surface tension. They remain intact and are prone to form small, smooth-surface, round, firm, shot-like granules, which do not pack readily and which lend the butter a short-grain and loose body of consid- erable firmness. This fact was conclusively demonstrated by the author1 in experiments to determine the effect of the size of the fat globules on the moisture content of butter. In these experiments milk was separated in such a manner, as to produce 1Hunziker, Mills and Spitzer, "Moisture Control of Butter." I. Factors not under Control of the Buttermaker. Purdue Bulletin 159, 1912. BUTTER DEFECTS 507 churnings of cream in which the small globules, and churnings in which the large globules, respectively, predominated. The large-globule cream churned quickly and yielded a soft, pliable butter that packed readily. The small-globule cream, on the other hand, churned slowly, produced small, round, smooth and hard granules which did not pack readily and which made a very firm, crumbly and brittle butter, from which it was impos- sible to draw a solid plug. The second fundamental cause of the tendency of winter butter to be crumbly lies in the feed the cows receive during the winter season. Dry feed and most of the common concen- trates always increase the firmness of butter. If the winter ration contains hay or corn fodder and liberal quantities of such concentrates as cottonseed meal, bran, etc., the butter fat in the cream will contain a relatively small percentage of the fats with low melting point, such as olein, and a relatively high per- centage of the fats with high melting point, such as stearin, palmitin, myristin, etc., and the resulting butter will, therefore, be firm and tend to be crumbly. Potatoes, beets and beet tops, apples and cornsilage also produce high melting fats conducive of firm and crumbly butter. Prevention of 'Crumbly Body. — It is obvious from the above discussion that the fundamental causes of crumbly butter may be eliminated entirely by a change to winter dairying whereby the cows are so bred that most of them freshen in the fall, yield- ing milk in which the large globules predominate; and by the addition to the feed ration of such feeds as have a tendency to produce butter fat of a lower melting point, such as linseed meal, glutenfeed, etc. The dairy man who makes butter on the farm has the fac- tors of period of lactation and feed largely under his control and, therefore, is in a position to avoid crumbly butter by the intel- ligent adjustment of these factors. The average creamery which draws its cream supply from a large number of farms which are often scattered over a wide area, cannot hope for relief from crumbly butter by any efforts to remove these fundamental causes, and must, therefore, aim to minimize their effect by modifications in the process of manufacture. The only means available to the creamery to prevent crum- 508 BUTTER DEFECTS bly butter is to churn, wash and work at temperatures suffi- ciently high to secure a reasonably soft butter that binds and compacts readily and makes the butter pliable. Churn at a tem- perature that will insure the formation of moderately soft, flaky granules, instead of small, round, hard granules, then wash the butter with wash water of the same temperature as that of the buttermilk, or possibly a degree or two higher, especially in a cold churn room, and work it sufficiently to secure a waxy, tough texture. The crumbly body of butter is frequently also attributed to frozen cream. There is no evidence on record that the freezing of cream has any appreciable influence on the body of the butter, but it is quite possible, that improper methods of thawing of frozen cream, causing it to "oil off," may intensify the tendency of winter butter to be crumbly. See also Chapter VI on the "Handling of Frozen Cream." Faulty pasteurization, in which the cream is permitted to "oil off," as may be caused by the use of excessively high tem- peratures, or by allowing the cream, while hot, to lie in the vat undisturbed and without agitation, will intensify the crumbly butter defect for the same reason as is the case with faulty handling of frozen cream. The crumbliness of brittle butter is augmented by exposure of such butter to very low temperatures. Butter that is inclined toward brittleness and that is intended for the critical hotel trade, should, therefore, be held in a room at a moderate temperature, so that, at the time of delivery, it is not excessively firm and will lend itself more readily to the slab cutter. Such hotels might also advantageously be cautioned not to expose this butter to abnormally low temperatures before cutting.1 Mealy Body. — 'Mealy butter is butter that lacks the smooth, velvety texture of well-made butter. It is a defect that is critic- ized by the buyer, and when the mealiness is very pronounced, it is seriously objected to. Causes of Mealy Body. — In the great majority of cases mealy butter is due to a hardened condition of the particles of casein, resulting from excessive exposure to heat in the pres- ence of high acid, as is the case when heating sour cream to too 1 It is advisable to work butter that is inclined to be crumbly very thor- oughly, even to the extent of slight overworking. BUTTER DEFECTS 509 high a temperature, heating too slowly, holding at pasteurizing temperature too long, or not cooling rapidly enough. The acid in sour cream changes the casein to casein lactate, and precipitates it into very fine flakes, or particles of curd. Van Slyke and Hart1 found that the casein is changed to casein lac- tate, when the amount of lactic acid in cream exceeds .5 per cent. In sweet cream the casein is largely in the form of calcium casein and some free casein. When this sour cream is heated for a prolonged period of time, as is often the case in the holding process of pasteurization, these particles of curd contract, expel much of their moisture, become firm and dry and give both the cream and the resulting butter a mealy texture. The mealiness is noticeable in the hot cream, and in the cream after cooling, quite as much as in the butter. Mealy cream always makes a mealy butter. Mealiness of this type does not occur in sweet or slightly sour cream, because in such cream the casein is present in its original and unchanged form. It has not been acted upon by the acid, it has not been precipitated. However, acid alone does not make cream and butter mealy. The particles of curd in the raw sour cream are soft. It is only in the presence of very high heat or upon prolonged exposure to heat, that sour cream be- comes mealy and makes mealy butter. Mealiness resulting from the above causes can be avoided by shortening the time required to heat the cream to the pas- teurizing temperature, by not exceeding 145° F. in the holding process, by holding for 30 minutes only and by cooling rapidly. Under proper conditions, such as adequate steam supply, ample size of steam and water pipes leading to the vat pasteurizer and adequate heating surface, the heating to 145° F. can usually be done in about 15 minutes. Experience has shown that, where the temperature can be raised to 145° F. in 15 minutes, there is very little danger of the cream and butter becoming mealy. If the time required to heat to 145° F. exceeds 30 minutes it is more difficult, and under certain conditions impossible, to avoid mealiness. Mealy butter is also almost invariably produced from sour * Van Slyke & Hart, "The Proteids of Butter in Relation to Mottled Butter/* New York State (Geneva) Agr. Bxpt Station Bull. 263, 1905. 5 10 B UTTER cream that is aerated by blowing cold air through it, while the cream is being heated. This is largely due to the longer time required for raising the temperature to 145° F. The blowing of the cream with cold air, as ordinarily practiced in our creameries, prolongs the period of heating from 10 to 15 minutes, which is sufficient to excessively harden the particles of curd and to make cream and butter mealy, when the condition of the cream is such as to favor mealiness. t When persistent trouble from mealiness is experienced and when it is desired to blow the cream, the danger from mealiness may best be avoided by blowing the cream while cold, or with hot air after the temperature of 145° F. has been reached. Blow- ing the cold cream, however, is less effective from the standpoint of the purpose for which the blowing is done, i. e., to remove objectionable flavors and odors. The volatile substances respon- sible for these flavors and odors are expelled more readily from hot cream than from cold cream. . The reduction of the acid in the cream by neutralization does not prevent mealiness. In fact practical experience has demonstrated that the excessive use of lime hydrate in sour cream tends to intensify rather than minimize mealiness. A further cause of mealiness of this type lies in the improper use of lime in the process of neutralization. When neutraliza- tion is done in an approved manner and as directed in Chapter VII, the danger of mealiness is removed. Another type of mealiness of butter is that which is due to a peculiar granular condition of the butterfat, similar to that of renovated butter. In this case the mealy body of the butter is not due to the grainy condition of the cream, but to granu- lated fat. This type of mealiness is not confined to butter made from sour pasteurized cream, it may occur as well in sweet cream butter. It appears whenever the cream is subjected to condi- tions that will cause it to "oil off." When this cream with the "oiled-off" or "run-together" butter oil is subsequently cooled and the fat hardens, the fat granulates and refuses to return to its original mechanical condition, and the granulated fat gives the butter a mealy consistency. This species of mealiness does not appear in the cream while hot; it becomes noticeable only after cooling and in the finished BUTTER DEFECTS 511 butter. It is caused either by faulty pasteurization or by im- proper handling of frozen cream. If, during the process of pasteurization the hot cream is allowed to repose in a vat without agitation, as may be the case with flash pasteurized cream that is not run over a continuous cooler, or with vat pasteurized cream with the coil at rest during the holding period, there is a tendency for the butter fat to run together, "oil-off" and gather in the form of butter oil on the surface of the cream. When the cream is subsequently cooled this butter oil crystallizes or granulates^ giving the butter a mealy body. This can best be avoided by guarding against excessively high temperatures of pasteurization and by keeping the cream thoroughly agitated while hot and until it has been cooled to a temperature at which the butterfat congeals, i. e., about 70° F. or below. The experience of many creameries has been that in winter, when some of the cream arrives at the factory in frozen condi- tion, butter is prone to be mealy, and the mealy condition of such butter has therefore been attributed to frozen cream. A careful study by the author of this phenomenon has shown that frozen cream, as such, does not produce mealiness, but that frozen cream may and does become the cause of mealiness in- directly by improper handling of this cream. For further details see Chapter IV "Receiving Milk and Cream." Finally, experience has shown that mealiness resulting from either of the two fundamental causes, the curd precipitation and the "oiling-off" of the fat, is characteristic more especially of the use of the holding process of pasteurization than the flash process. In the flash process the cream is heated and cooled quickly, not giving the particles of curd sufficient time to con- tract and harden excessively, and the cream is subjected to continuous agitation until it is cooled, thus largely preventing the "oiling-off" of the fat. Butter resulting from the flash process usually has a clearer and smoother body and is more completely free from mealiness than butter made from cream pasteurized by the holding process. Summary of Prevention of Mealiness. — In brief, then, the mealy body of butter can be avoided by : 512 BUTTER 1. So regulating the temperature of pasteurization and the period of exposure to pasteurizing temperature, as to avoid the excessive contraction of the curd in the sour cream. Heat rap- idly, do not exceed 145° F. in the case of the holding process, limit the time of holding to 30 minutes and cool rapidly. Do not blow the cream. 2. Preventing the cream from "oiling-off." Keep the coil in the vat revolving during heating, holding, and until the cream is cooled to 70° F. or below. Do not heat the frozen cream to a temperature higher than 95° F. and hold it at that temperature until it has become fluid. Leaky Body. — This defect is characteristic of salted butter only. Unsalted butter seldom, if ever, shows real leakiness. In leaky butter much of the water present is incompletely incor- porated in the fat and oozes out profusely when such butter is handled, cut, packed, shipped and stored. When bored with the trier, brine runs freely from the plug, and when the plug is squeezed, there is further escape of moisture. Leaky butter, owing to the ready escape of moisture, gen- erally suffers excessive loss in weight between the churn and the market, as well as in storage. Leaky butter usually also has an objectionable briny flavor suggesting excessively high salt content, although the actual percentage of salt it contains may not be high and may even be below the average. The briny flavor in this case is due to the direct appeal to the palate of free brine. For these several reasons leaky butter is not looked up- on with favor by the buyer. Causes of Leaky Butter. — Because the leaky body is large- ly confined to salted butter only, this defect has been attributed to faulty methods of salting and working, and the popular im- pression prevails that such is the case. Within relatively nar- row limitations leakiness may be intensified or minimized by the processes of washing, salting and working, but the funda- mental cause of leakiness lies prior to these processes, it has to do with the treatment the cream receives preparatory to the churning process. Leakiness is due to incompleteness and consequent in- stability of the emulsion of buttermilk (or water) in fat, and this BUTTER DEFECTS 513 emulsion occurs during the churning process. The complete- ness and permanency of the water-in-fat emulsion is depend- ent on the relative mechanical firmness of the fat at the time of churning. If the butterfat in the cream in the churn has previously been thoroughly chilled by cooling to, or below, the proper churning temperature and by holding it at that temperature for the necessary length of time, leaky butter is not likely to result. Butterfat in this condition yields an emulsion of water-in-fat that is relatively stable. The finely divided water droplets are firmly held in this compact fat. When salt is added to and worked into butter made from incompletely chilled cream, the loosely held emulsion of water- in-fat is disturbed and partly broken. The emulsion yields to the salting-out process. The water droplets are not firmly enough locked up in the body of the butter to resist the attraction of the salt. The salt draws them together into drops and larger aggregates; which leak freely from the butter. Even when efforts are made on the part of the buttermaker to harden this butter in the churn, either by churning the cream with ice or by holding the butter for a considerable length of time in ice water, a really good body can not be recovered. The defect may be somewhat minimized by these remedial prac- tices but the damage has already been done, and the butter will have a distinctly weak body that will not stand up well under adverse temperature conditions, and that is prone to be leaky. If cream has been cooled to a point where the fat becomes thoroughly chilled, as it should be, churning at a temperature slightly too high does not produce leakiness, the fat is still of good firmness, because it does not respond to temperature changes rapidly, being a poor conductor of heat and cold. This leaky butter defect appears largely, though not wholly, only in the spring and early summer. This is the time when, due to the freshening of the cows and the change from dry feed to succulent pasture, the melting and solidifying points of the butterfat drop rapidly. The average buttermaker fails to fully appreciate this rapid change in the character of the butterfat he receives in the spring, and he often does not respond quickly enough to this change 514 BUTTER with an adequate lowering of the churning temperature. There- fore the tendency of spring and early summer butter to be leaky. The incomplete chilling of the cream in early summer is in many cases the result of an insufficient supply of cooling medium and inadequate vat capacity to handle the great volume of cream that arrives during the flush. Leaky butter may result at any other time of the year, whenever the temperature of the cream before churning is not low enough and the period of holding at this temperature is not long enough to thoroughly chill the fat. Rich cream is more apt to make a leaky body than thin cream, unless the rich cream is churned at a lower temperature. If the cream of different churnings varies in per cent fat con- siderably, it is more difficult to have successive churnings of butter of good body and free from leakiness. The standard- ization of each churning for fat greatly assists the buttermaker in- his efforts to produce a perfect body, with reasonable regularity. The tendency toward leakiness is intensified also by any agency that is prone to mutilate or tear apart the body of the butter. Churns that tear the butter during the working process are more apt to yield a leaky butter than churns, the workers of which squeeze it. The tearing and chopping of the butter during the working disturb the texture and tend to liberate some of the otherwise firmly held water droplets. Summary on Prevention of Leaky Butter. — When the butter- maker is troubled with leaky butter he should pay attention to the following phases of manufacture: 1. Standardize each churning to a uniform percentage of fat, preferably between 30 and 33 per cent. 2. Thoroughly chill the fat in the cream by cooling the cream to a temperature low enough and holding it at this tem- perature long enough to secure firm butter granules. Unless cooling facilities permit the cooling of the cream to far below the desired churning temperature, the cream should be held at the temperature cooled to for not less than two hours, and preferably three hours. 3. Work the butter until visible water pockets have disap- peared and the butter has a compact, solid, tough, waxy body. BUTTER DE^CTS 515 This is possible only with butter made from cream that has been thoroughly chilled before churning. Gritty Body. — This defect is due to the presence in butter of undissolved salt crystals. Grittiness is highly objectionable to the consumer, it conveys the impression of excessive salt, and gives the butter a seemingly strong salty and coarse flavor. In properly salted butter all the salt is present in complete solu- tion. The more complete the solution and distribution of the salt, the more salt butter will stand without tasting objection- ably salty. The usual factors which enter into the presence or absence of grittiness of butter are, moisture content, temperature of but- ter, amount of working, amount and temperature of salt added and size and shape of salt crystals. As shown in "Composition of Butter," Chapter XVIII, 100 pounds of water at ordinary temperature is capable of dissolving and holding in solution 35.94 pounds of salt, so that, theoret- ically, butter containing say 15 per cent moisture is capable 15 x 35 94 of holding in solution r-r^-1 — 5.39 per cent salt. Owing 1UU to the very fine division of a part of the moisture in butter, the salt added to butter is incapable of gaining access to and of utilizing all the moisture present in butter during the brief time during which butter is worked. In reality, butter containing 16 per cent moisture, makes possible the complete solution of not to exceed about 4.5 to 5 per cent of salt, although this same amount of water, if freed from the other butter constitutents is, in fact, capable of dissolving salt equivalent to a salt content in butter, of 5.75 per cent. Butter containing more than this amount of salt, therefore, is prone to be gritty. All conditions which tend towards a low moisture content invite the production of gritty btitter, unless the amount of salt added is reduced correspond- ingly. Insufficient working of the butter is another very common cause of gritty butter. When butter is of normal texture it should be worked until the salt is dissolved and all signs of grittiness have disappeared. Finally the size and shape of the salt crystals may become responsible for grittiness. The use of very coarse salt and espe- 516 BUTTER cially if such crystals are of cube shape, retards solution, while reasonably fine crystals enhance solution. Too fine salt also is undesirable because it tends to paste and cake in the butter and thereby hinders ready solution and even distribution. Salt of the proper degree of fineness will pass through a sieve with 28 to 30 meshes to the inch. DEFECTS IN COLOR. As previously stated, the color of butter must be of the intensity desired by the market where it is sold. According to Palmer1 the natural yellow color of cream and butter is derived from two classes of yellow pigment, the carotin and xanthophyll, which accompany the green chlorophyll of plants. These yellow pigments, particularly the carotin, are found in the blood of the cow and it is in this way the carotin passes from the feed to the milk gland where it associates itself with the milkfat. Palmer classifies the following feeds with reference to their carotin content and consequent property to make yellow cream and butter as shown below. This classifica- tion explains why cows fed on green pasture, as is the case in early summer, produce a deep yellow butter, while in winter High Color Low Color Carotin-Rich Feeds. Carotin-Poor Feeds. Green pasture grass, especially A11 ha>T that has lost its green when fresh in the spring or color in curinS' such as most - .j timothy and clover hay. Dry corn fodder (corn stover). Hay, cured with a large part of A1f corn silage> except when its original green color, such very new. as most western-cured alfalfa Straw, all kinds. hay. Corn, both yellow and white. All soiling crops. Wheat ~ . , t All so-called mill by-products, Green corn fodder. , , , , such as wheat bran, brewers Very new corn silage. grains> cottonseed meal, lin- Carrots, and other yellow roots seed meal, natural gluten- and tubers. feed, etc, 1 Palmer— The Yellow Color in Cream and Butter. Missouri Circular 74, BUTTER DEFECTS 517 when they receive largely dry fodder and grain by-products, the butter has a very light yellow and often an almost white color. It is well known that the Channel Island breeds, the Jersey and Guernsey, are capable of yielding a much more yellow butter than the Holsteins and Ayrshires. This is explained by Palmer to be due largely to the fact that some breeds (Jerseys and Guernseys) make use of more feed carotin than others (Hoi- steins and Ayrshires). It is also a matter of common knowledge that the natural color of butter varies with the period of lactation. Palmer states that no breed difference in color exists immediately after parturition, the colostrum milk of all cows being very highly colored due to a relatively large amount of carotin in the milk- fat. As the period of lactation advances the intensity of the color decreases. In the case of the Jerseys and Guernseys the color does not diminish as rapidly and not to so great a degree as in the case of the Holsteins and Ayrshires, so that even in winter when most of the cows approach the end of the period of lactation and when the carotin content of the feed ration is low, the Channel Island breeds are 'still producing a light yellow butter, while the butter of the Holsteins and Ayrshires is almost white. This is explained to be due to the fact that the Channel Island breeds are storing up a reserve of carotin in their body fat in summer when the succulent pasture supplies them with an abundance of carotin and on which they draw in fall and winter when the feed is largely devoid of this coloring pigment, while the Holsteins and Ayrshires are unable to do this to the same extent. In order to satisfy the demand of the butter market and to maintain uniformity of color at a time of the year when, espe- cially in Holstein and Ayrshire localities, the natural color of butter is practically white, artificial butter color is added. Too High Color. — As previously stated the trend of the best butter trade is toward a light, straw-colored butter. In these markets, therefore, butter with a deep golden yellow color is not desired. While, in winter, when the natural color of butter is very light, the buttermaker is in a position to meet these demands by modifying the amount of artificial color added, in early sum- 518 BUTTER DEFECTS mer, when most of the cows freshen and have access to green pasture, the butter is often so intensely yellow, without any addition of artificial butter color, that it is criticized as being too high in color. This is especially true with butter produced in localities where the Jerseys and Guernseys predominate. In the great majority of complaints by the trade, too high color is due to carelessness or accident on the part of the butter- maker. In this case it is caused either by incorrect calcula- tion of the amount of butterfat in the churning on which he bases the amount of artificial butter color to add, or careless measuring of the butter color, or not modifying the proportion of butter color used in accordance with a sudden change in the natural color of the cream, especially in the spring of the year, or a change to a new brand of stronger butter color, or butter color from the bottom of the drum which may contain an ac- cumulation or concentration of the coloring principle due to settling. The prevention of these difficulties is obvious. The butter- maker should constantly bear in mind that the trade objects to uneven and excessive coloring in butter and that it expresses its objection in discounting the value of the butter to the detri- ment of the net returns to the creamery. It does not pay to overcolor butter. Too Light Color. — This is a shortcoming for which butter is seldom criticized and only in very isolated markets which insist on a high-colored butter throughout the year. The excessively light color is usually due to the season of the year and occurs only during the winter months when the cows are receiving dry feed only and no artificial butter color is added to the cream. It can readily be remedied by the addition of the proper amount of artificial butter color. In some instances the lack of yellowness may be due to the bleaching of the color of the butter after the butter is made and packed. This is usually due to an oxidizing action taking place in the butter, either on the butterfat itself or on other ingredients which butter may contain. See "Tallowy Butter." The bleaching of butter may also be the result of holding butter in water. In hotels and restaurants where the butter is BUTTER DEFECTS 519 cut into small slabs for table use, these slabs are generally dropped from the butter cutter into ice water. In the case of salted butter, if these slabs are permitted to remain in this water for any considerable length of time, portions of the surface begin to bleach, giving the butter a mottled appearance. Con- tinued exposure will bleach .the entire surface, the mottles be- come very indistinct, but the color on the surface of the slabs is much lighter. This type of bleaching can be readily and entirely avoided, as demonstrated by the work of Hunziker1, by dropping the slabs of salted butter into a solution of 25 per cent brine instead of water. In this case there is but one kind of liquid present and that is brine, brine in the butter and brine surrounding it, no interchange of liquids takes place and there is no bleaching. If the slabs consist of unsalted butter they do not bleach when dropped into water, because here again there is but one liquid and that is water, water in the butter and water surround- ing it, there is no cause for interchange of liquids and there is no change in the color of trie slabs. See also "Mottled Butter." Excessive working of salted butter also has a marked whitening effect on the butter. This is due to the fact that in normally-worked butter the average size of the water drop- lets is relatively large and this lends the salted butter a relatively clear, deep yellow color. Overworking causes a finer division of these water droplets and this in turn produces a lighter and more opaque appearance, more nearly like that of unsalted butter, in which the water droplets always average much smaller in size. Dull Color. — Much of the butter made in some creameries has a dull and lifeless color. This is usually the result of at- tempts to incorporate a high per cent of moisture, and overwork- ing. When, in an effort to incorporate moisture, the butter is overworked to the extent to where the grain of the butter is destroyed, the fat granules lose their bright lustre. The large amount of moisture held by the fat in very minute droplets and very complete emulsion, together with the very firxe division of the air in the butter, also resulting from overworking, hides the 1 Hunziker — Defects in the Coloring of Butter. Address American Asso- ciation of Creamery Butter Manufacturers, Chicago, February 18, 1919. 520 BUTTER DEFECTS bright yellow color and gives the butter a dull and lifeless appearance. It is obvious that this defect can readily be avoided by in- corporating a normal amount of moisture and not overworking the butter. The difficulty of incorporating the desired amount of moisture in butter that is naturally very firm and dry, and does not readily take up and hold moisture, in order to secure a reasonable overrun, may best be overcome by raising the churn- ing temperature sufficiently to give the butter a somewhat less firm body. Mottled and Wavy Butter. General Description. — Uneven- ness in the color of butter is shown in the butter in the form of streaks, waves and mottles. Streakiness or waviness refers to butter in which the unevenness in color shows in the form of layers or waves of different shades of yellow, the color in the layer or wave itself, however, may be perfectly uniform. In the case of mottles the butter is dappled with spots of lighter and deeper shades of yellow throughout its body. Unevenness in color, and especially 'mottles, in butter, are a serious defect from the standpoint of its market value. This defect has nothing to do with the quality of the butter, mottled butter is just as good and just as wholesome as butter that is not mottled. But while the criticism of the trade is a superficial one, the objection is no less real. Butter that is otherwise perfect and might score a good "Extras," if it is mottled, clears as a "Seconds" and is sold on that basis by the dealer. Causes and Prevention of Mottles. — Extensive experiments by Hunziker and Homan1 have shown that the causes of mottles are due to the following factors : 1. Mottles are caused by an uneven distribution of the water droplets in butter. 2. The white, opaque dapples in mottled butter are caused by the presence, or localization of innumerable very small water drop- lets. The small size, high curvature and large number of these drop- lets bend, refract and deflect the rays of light to such an extent that they render the butter opaque and give it a whitish appear- ance.2 1 Hunziker & Hosman. A Study of the Causes of Mottles in Butter. Blue Valley Research Lab., Chicago 1918 and 1919. Journal Dairy Science, Vol. Ill, No. 2, 1920. 2 The opacity is further intensified by the difference in the refractive in- dex between butterfat and water. BUTTER DEFECTS 521 3. The clearer and deeper yellow blotches in mottled butter are caused by absence, or the relatively small number of the very small droplets or by the presence of a larger number of large droplets, or both. Both, the absence of any water droplets and the presence of relatively large droplets and aggregates of drops, minimize the refraction and deflection of the rays of light, permitting the rays to enter sufficiently to give the butter a clearer and more translucent body and revealing more of the natural golden yellow color characteristic of butterfat. 4. The reason why unsalted butter always has an opaque whit- ish color, and never is mottled, lies in the fact that in unsalted but- ter, regardless of the amount of working, the water is always pres- ent in the form of exceedingly minute and innumerable water drop- lets of uniform size and distribution, giving the entire body of but- ter a uniform opaque whitish appearance. The permanency of this uniform white appearance is due to the absence in unsalted butter of agents capable of breaking this fine emulsion of water-in-fat. 5. The reason why salted butter always has a clearer and deeper yellow color than unsalted butter, lies in the fact that the salt, due to its action on the curd and to its great affinity for water, draws the more loosely held small droplets together into larger aggregates, it makes the emulsion of water-in-fat less complete, it diminishes the refraction and deflection of the rays of light and makes the butter more translucent. 6. Salted butter at the churn is never mottled, because, even in insufficiently worked butter the distribution of the large droplets at the conclusion of the working process is sufficiently complete to hide the localized sections of the very minute droplets. 7. Salted butter, when insufficiently or unevenly worked, in- variably becomes mottled upon standing, because in such butter the fusion and the emulsification of brine and water are incomplete. Owing to the difference in concentration, and to osmosis be- tween brine and water, interchange and migration of brine and water takes place in the butter at rest. This causes the more loosely held, larger water droplets to run together into larger aggregates and the portions of butter containing these fewer but larger droplets show themselves as and represent the clearer, more translucent and deeper yellow blotches of mottled butter. 522 BUTTKR Size of Water Droplets in Light and Dark Portions of Mottled Butter. Magnified 740 times. Fig. 82. Dark portions BUTTER DEFECTS 523 The running-together of the larger droplets simultaneously also uncovers the localized sections of innumerable very small droplets which, at the conclusion of the working process, were hidden by the larger droplets. And the appearance of these aggregates of very small droplets brings to view the opaque, dense, whitish dapples of mottled butter. 8. The reason why salted butter, when sufficiently and evenly worked, does not show mottles upon standing lies in the fact, that in such butter the large droplets resulting from the action of the salt, have been redivided and remulsified in the butter and the fusion of brine and water has become relatively complete. Hence there is practically only one kind of liquid in this butter and that is brine. There is no difference in concentration, there is no cause for osmosis, and there is no interchange and migration of liquids. And the permanency of the emulsion is further strength- ened by the more minute division of the droplets in properly and evenly worked butter. 9. Streaky or wavy butter is caused by uneven working of dif- ferent portions of butter of one and the same churning, either due to a faulty condition of the workers or an overloaded churn. Those portions of the churning which receive the most working have the lightest color, because the more the butter is worked, the smaller become the water droplets and the smaller the water droplets, the more opaque and the whiter is the butter. 10. Streaky or wavy butter may also result when the distribu- tion of the salt over the entire length of the churn is very uneven. In this case the butter that received the most salt will have larger water droplets and will therefore have a clearer, more translucent and more yellow color than that part of the butter that received the least amount of salt. Practical directions for the prevention of waves and mottles in butter: 1. Keep churn and workers constantly in good me- chanical repair. — Make sure that the workers are correctly set, properly adjusted and that they are free from slack and do not slip. The distance between workers, in the case of churns with two or more workers, and between worker and shelf in the one- worker churn, should be the same over the entire length of the churn. Uneven distance causes uneven working. An uneven distance between work- ers is due to the fact that either one or more of the workers are crooked, the worker shafts are out of line, the shaft has worn a 524 BUTTER DEFECTS large hole in the end of the worker, the bearings in which the worker shafts run are worn, the worker shafts themselves are worn, the distance between centers of the worker shaft bearings in one end of the churn is not the same as that in the other end of the churn, the periphery of the workers has become badly dam- aged in places, or the shelves are not of the same width over their whole length, do not lie straight, have become damaged, or are loose and wobbly. In churns with more than one worker, the workers must be so set that, when in operation, the ridges of one worker meet the grooves of the opposite worker. If they are so set that ridges meet ridges and grooves meet grooves, the working is very uneven, invit- ing mottles. The workers must be taut, and free from excessive slack and from slipping. Slack and slipping workers won't stay set right and therefore cause uneven working and mottles. Slack and slipping is due either to the worker shafts having worn loose in the ends of the workers, the worker shafts slipping in the gear wheels due to a worn key or worn shaft, or to excessive wear of or damage to the cogs of the gear wheels. The buttermaker who would make butter uniformly free from mottles and waviness must keep close watch of the mechanical con- dition of his churns and keep the churns and workers in a constant state of good mechanical repair. 2. Do Not Overload the Workers. — An overloaded churn needs more revolutions with the workers in gear than a churn not overloaded. But at best such working is prone to lack of uniformity. When the workers are overloaded all of the butter cannot go through the workers with each churn revolution. Some of the butter will fall off over the outside of the workers, and therefore fails to be worked, as fully explained in Chapter XL, "Working." 3. The Butter must be worked sufficiently for complete so- lution of the salt and distribution of the brine. — The process of working is the only means whereby the extraneous water and the brine can be evenly distributed throughout the mass of butter. If this complete solution of salt and distribution of brine is not accom- plished during the process of working, it will never be accomplished, and such butter, upon standing, is bound to become mottled. It is only during the process of working that the brine is capable of pene- BUTTER DEFECTS 525 trating the fine emulsion of the native water in butter, and that the brine itself is capable of becoming sufficiently fused with the water and emulsified with the protein and fat particles of the butter to preclude interchange of the brine and water after working. If the salt crystals are not completely dissolved by the working process, the migration of the free liquid in the butter at rest, is intensified by the affinity of the salt for water and the dapples or mottles appear more quickly and more conspicuously. Fig-. 82A. Fissures in salted butter, showing migration of water Magnified 110 times So far as the process of working is concerned, therefore, in order to prevent mottles,- the butter must be worked sufficiently to dissolve the salt completely, to cause a very thorough fusion of the brine and the water and to produce a sufficient emulsion of the brine, fat and protein of butter to hold it. The degree of fineness of the salt, or the size of the salt crys- tals, influences its solubility. Too coarse salt requires more water and more time for the complete solution of each crystal. Too fine salt tends to cake or paste the crystals together, again hindering ready solution. .See also Chapter XL, "Salting.'' Briefly, then, mottles and waves can be prevented by the use of churns in which the workers and shelves are set correctly and are in 526 BUTTER perfect mechanical condition, by avoiding the overloading of the workers, by the proper use and even distribution in the churn of readily soluble salt, and by adjusting the working process according to the mechanical firmness of the butter in such a manner, as to insure complete solution of the salt, even distribution and complete fusion of brine and water and producing a butter in which the free brine and water have been sufficiently emulsified, to give the butter a close, tough, waxy texture, free from visible water pockets. White Specks in Butter. — Butter occasionally is permeated with a multitude of small white specks. This condition is due to the incorporation of small pieces of coagulated casein. The defect is easily preventable and should not occur when proper attention is given to the handling of the starter and the cream. Its most common cause is overripe starter, overripe cream and cream that has been allowed to dry on the surface due to lack of stirring dur- ing the ripening process. If the starter is added before it is over- ripe and has formed a firm curd, or if the coagulum is thoroughly broken up by stirring or pouring and the starter is strained into the cream, if the cream is properly stirred during the ripening process so as to prevent its drying on the surface, if it is not overripened, and is strained into the churn, there is usually no danger of white specks in butter. Cream and starter should never be allowed to enter the churn unless they are run through a fine strainer. The occasional appearance of white specks in butter may be due to the cream strainer in the churn becoming clogged and flowing over, or to emptying the accumulated material caught in the strainer, into the churn, either through accident or through ignorance. Yellow Specks in Butter. — This is a very rare defect and yet occasionally it occurs and causes trouble. When these specks are of an orange shade, they are usually due to sediment in the but- ter color used. If the butter color contains such sediment it should be allowed to settle and only the clear oil on top should be used. These yellow specks occur most generally only when the supply of butter color in the drum or other receptacle is nearly exhausted, so that the very bottom strata of the color in the drum are drawn on. In this case it is advisable to discard the remnant of butter color and draw from a new drum. BUTTER DEFECTS 527 Frequently the yellow specks are of a different nature and are due to other causes. There occasionally appear yellow spots in the butter that are of an oily, translucent nature. In this case they are generally due to accidental exposure of that particular portion of butter to some object warm enough to cause partial melting and, when recongealed, the butter in that spot looks deep yellow like clear butterfat. This defe'ct may occur when the operator uses a packer that was soaked in hot water immediately before use and failed to cool it. The warm butter packer melts a small portion of the butter which it touches, resulting in yellow specks showing up in the but- ter when examined over the trier, or when cut. The buttermaker frequently argues that the butter packs more easily when a warm packer is used. All tools, packers and ladles should be chilled in cold water or cold brine, before they are used in the packing of butter. Occasionally prints of butter are found that are completely jacketed in a layer of this same translucent, clear, deep yellow, oily- looking butter. This is caused when unsalted butter is stored in a warm room for a considerable length of time. In this case the surface layer becomes very soft, evaporates most of its moisture and expels a portion of its protein content. When rehardened, a surface layer, varying in thickness according to the temperature ex- posed to and the duration of the exposure, of very sharply defined, almost pure butterfat, is produced and this is of very translucent deep yellow color, while the remainder of the print retains its nat- ural opaque white color. Chemical analysis shows that the moisture content of this outer layer of yellow butter may be no higher than one per cent. This defect is greatly minimized in its intensity and the evaporation retarded when the butter, in addition to the parch- ment wrapper, is enclosed in a wax paper and packed in a carton. Salted butter exposed to similar conditions is not subject to this defect. This is probably due to the fact that the loss of moisture due to evaporation is more evenly distributed throughout the body of the print. As the moisture on and near the surface evaporates, salt crystals form which draw more moisture from the interior of the butter. It is obvious that the storing of butter in a warm room is ob- jectionable at best, and store-keepers should be urged not to keep 528 BUTTER DEFECTS more butter on the open shelves of their stores than they may rea- sonably expect to dispose of each day, or preferably to reserve a compartment in their refrigerator for all the butter they carry in stock. Tig. 83. Unsaltecl butter held at room temperature for 3O days, showing- d.eep yellow border at periphery due to evaporation of moisture, while interior retained its original color; moisture in surface layer was 1 per cent, in interior 16 per cent. Green Spots in Butter. — Green spots occasionally appear on the surface or in the interior of butter, other than those described under "moldy butter." This green coloration, especially when found on the surface, usually shows up in the form of small circles or rings, which grow larger with age. Microchemical examination of these green spots by Hunziker and Hosman1 showed these spots to contain traces of copper. When they appear on the surface of print butter they can generally be traced to the presence in the parchment wrapper of very minute specks with metallic lustre. These specks in the wrapper have been found, by the authors, to consist of copper or an alloy containing copper, such as German silver, or brass. Further investigation has revealed that the parchment paper manufacturers are experiencing considerable difficulties to keep 1 Hunziker ahd Hosman, Blue Valley Research Laboratory, 1917-1919. Re- sults not published. BUTTER DEFECTS 529 filings of these metals out of their paper pulp and that, in order to guard against their appearance in the paper, the manufacturers are employing diverse devices, such as magnets, etc., in the process of manufacture. The original source of these minute specks of metallic lustre in the parchment paper lies in the rags which constitute a portion of the raw material from which parchment paper is manufactured. In spite of the manufacturers' efforts to eliminate them, metal but- tons and buckles of discarded overalls and of similar rags occa- sionally escape detection, pass into the process with the rags and are thus ground into fine particles or filings which later appear in the finished parchment paper. Whenever particles of these metal filings become incorporated in the parchment wrapper and the butter is wrapped in such wrap- pers, the salt and acid in the butter attack the copper contained in these minute specks, forming verdigris. This in turn starts the formation of a small green circle on the butter and on the wrapper, where the metal speck is located. The green circle grows as the butter ages and the action con- tinues. Around the green coloration there is often also white, bleached butter with an intense tallowy odor. This oxidation, un- der favorable conditions, may ultimately involve the entire print, causing the whole package to be greenish white and tallowy. In other cases the green coloration may occur in the interior of the butter. In this case it is also due to particles of copper or an alloy containing copper, but the source of the copper lies in the manufacturing process. It is especially prone to occur when the strainer over the forewarmer or over the pasteurizing vat sags and scrapes the revolving coil, or when accidentally a can cover or other obstruction drops into the bottom of the forewarmer and becomes wedged in between the forewarmer and the revolving coil. In such instances and other similar cases, particles of the copper of the coil and possibly of the strainer are filed off into the cream and are later worked into the butter. The metal particles may be very small and hardly perceptible to the naked eye, but their corro- sion by the salt and acid of the butter is inevitable, causing the appearance of green verdigris in the interior of the butter. It is obvious that this defect is highly objectionable, verdigris is poisonous and the green coloration is offensive. It can be easily 530 COMPOSITION AND PROPERTIES otf BUTTER avoided by using wrappers that are free from metallic specks and by avoiding- any carelessness in the creamery, that causes the in- corporation in butter of metallic elements. The copper coils should never be permitted to scrape against any metal, and if any material or instrument is used to clean the coil or vat lining, that causes vio- lent friction on the copper surfaces, the greatest care should be exer- cised to flush such surfaces thoroughly so as to remove every ves- tige of metallic material before cream is again permitted to enter the vat. Chapter XVIII. COMPOSITION AND PROPERTIES OF BUTTER, MILK, CREAM, SKIM MILK AND BUTTERMILK. Butter. Butter is a mixture of butterfat, small amounts of the non- fatty constituents of milk, cream and water, and it may contain added salt and coloring matter. It is an emulsion of diluted buttermilk-in-fat. It is composed chiefly of butterfat, water, curd and salt in the case of salted butter, and butterfat. water and curd in the case of unsalted butter. The remaining non-fatty constituents, are the ash, lactose and acid. The percentage composition varies considerably with the character of the cream and the method of manufacture. The average composition of butter, made in different localities, dur- ing the several seasons of the year and under diverse methods of manufacture would approximate the following figures : Salted Butter Unsalted Butter Butterfat .82.5% 84.0 Water 13.8 14.5 Salt 2.5 0.0 Curd 6 .85 Ash 1 .20 Lactose 25 .3 Acid .15 .15 Total .x 100.00 100.00 Thompson, Shaw and Norton1, in a study of the normal composition of creamery butter, analyzed 695 samples of dif- 1 Thompson, Shaw and Norton, The Normal Composition of American Creamery Butter, U. S. Dept. Agr., B. A. I. Bulletin 149, 1912. COMPOSITION AND PROPERTIES OF BUTTER 531 ferent churnings of butter from California, Iowa, Michigan, Minnesota, North Dakota, Pennsylvania, Texas and Wisconsin, and found the maximum, minimum and average percentages of butterfat, water, salt and curd to range as follows : Table 71. — Maximum, Minimum and Average Percentages of Butterfat, Water, Salt and Curd1 in American Creamery Butter. Butter. 695 Samples of Butter Fat Water Salt Curd Average 82.41 13.90 2.5°1 U8 Maximum 87.39 20.65 5.98 3.42 Minimum 73.49 10.13 .68 .12 A study of these figures shows a most unusual range be- tween maximum and minimum percentages of the several butter constituents, while the average percentage appears quite normal. The wide range of percentage composition may be due in part, at least, to the fact that over two-thirds of the samples an- alyzed represent butter from the very heart of the co-operative and small local creamery, the states of Minnesota, Wisconsin and Iowa. The average buttermaker in these creameries is more of an all around creameryman than an expert buttermaker. His knowledge of the art and science of moisture control is limited and the percentage composition of his butter is prone to lack in uniformity. Analyses of butter from the larger creameries, whose butter- makers are strictly churnmen, and whose skill in moisture con- trol is more highly developed, would undoubtedly show a much more uniform percentage composition, with a slightly higher average water and salt content and a slightly lower fat and curd content. The Butterfat. — The butterfat is the chief constituent of butter. It normally varies between about 80 and 85 per cent, averaging about 82^ per cent. Abnormal cases occasionally show variations within much wider limits. In rare cases butter has been found to contain as high as 90 per cent fat and as low as 72 per cent fat. 1 The term "curd" as used here includes, in addition to the nitrogenous constituents, the ash and lactose. 532 COMPOSITION AND PROPERTIES OF BUTTER Normal variations in the percentage of butterfat in butter are due to its natural mechanical firmness which determines its power to absorb and hold water and by the process of manu- facture. The mechanical firmness of the butterfat is dependent on such factors as season of year, which largely controls the period of lactation and the character of the feed, and on locality which determines the breed of cows and, in part, the character of their feed. Butterfat is the fat of milk, milk fat is a natural compound of several different fats which vary in their properties. The chief of these fats are the olein, palmitin, myristin, stearin, laurin, butyrin, caproin, caprylin and caprin. These fats are present in the form of a chemical combination of glycerol (glycerin), as the base, and of one or more fatty acids, such as oleic, palmitic, myristic, stearic,-lauric, butyric, capronic, caprylic and capric acids. These fats are spoken of as the glycerides. The proportion in which these glycerides, or fats, are present in the mixed milk fat varies according to breed, period of lactation and feed of the cows, hence analyses of milk fat derived from different sources are somewhat at variance. Richmond1 shows the follow- ing composition of milk fat: Table 72. Composition of Milk Fat. Fats (Glycerides) Fats (Glycerides) Per Cent Fatty Acids of These Glycerides Per Cent Glvcerol of These Glycerides Per Cent Butyrin . . 385 343 1.17 Caproin , 360 325 .86 Caprylin .55 .51 .10 Caprin 1.90 1.77 .31 Laurin 7.40 6.94 1.07 Stearin 1.80 1.72 .19 Myristin 20.2 19.14 2.53 Palmitin 25.7 24.48 2.91 Olein 35.0 33.60 3.93 Total 100.0 1 Richmond, Dairy Chemistry. COMPOSITION AND PROPERTIES OF BUTTER 533 Soluble or Volatile Fats and Insoluble or Non- Volatile Fats. —The milk fats are spoken of as soluble or volatile and insoluble or non-volatile fats. In reality none of the fats are soluble or volatile, but the fatty acids of some of the fats or glycerides, when, as the result of the decomposition of the respective glyc- erides, they become separated from their base, the glycerol, be- come soluble and volatile. Some of the fatty acids are wholly soluble and volatile, to these belong the butyric acid and the caproic acid ; others are only partly soluble and volatile, to them belong the caprylic, capric and lauric acids; still others are entirely insoluble and non-volatile, to these belong the oleic, palmitic, myristic and stearic acids. Of the total milk fat about 8 to 12 per cent yield volatile and soluble fatty acids, while the remainder of 88 to 92 per cent are insoluble and non-volatiles It is generally accepted, though by no means fully experi- mentally proven, that the volatile fatty acids, of which the butyrin is the most important, give the dairy products their characteristic odor and flavor and that they derive from the feed of the cows the characteristic feed flavors. Storch holds that it is the slimy, nitrogenous film which he claims surrounds each fat globule, that contains and is responsible for the char- acteristic flavor and aroma of butter. Melting Point of Milk Fats. — The melting point of the mixed milk fat ranges between about 90 and 99 degrees F. and the solidi- fying point ranges betwen 65 and 75 degrees F. Fleischmann1 gives the melting point at 31 to 36 degrees C. (87.8-96.8 degrees F.) and the solidifying point at 19-24 degrees C. (65-75 de- grees F.). The several fats or glycerides of which the milk fat is composed, differ from one another largely in their melting points and in their solidifying points, and since the melting point and the solidifying point of the fat control the mechanical firm- ness or softness of butter, this fact is of the greatest importance in the art of buttermaking. The melting points of the several more important fats contained in milk are as follows : iFleischmnnn — Das Buch der Milchwirtschaft, 1901. 534 COMPOSITION AND PROPERTIES OF BUTTER Table 73. Tri-butyrin —60 to —70° C. or —76 to —94° F. Olein 5° C. or 41° F. Myristin 54° C. or 129° F. Palmitin 61° C. or 142° F. Stearin 65.5° C. or 150° F. Both the butyrin and the olein have melting points much lower than the other insoluble fats. A material increase in the proportion of butyrin or olein, or both, therefore suggests a lowering of the melting point of the mixed fat and vice versa. This fact has been amply demonstrated by Eckles1 and by Hun- ziker2. Exceptions to these facts are not infrequent, however, and they must be largely attributed to the fact that the volatile acids in such cases were made up of unusually high proportions of the less common constituents, such as caprylic, capric and lauric acids, whose melting points are 16.5, 31.3 and 43.6 de- grees C., respectively, as suggested by Eckles, or that the rela- tive proportion of the glycerides of the individual soluble and insoluble acids exclusive of oleic, must have exerted a dominant influence, as suggested by Hunziker. Again, Lewkowitsch3 points out that the melting point of a mixture of fats cannot be predicted from the melting points of the fats themselves ; and Twitchell4 shows the interesting fact that a mixture of palmitic and stearic acids lowers the solidifying points of each other to a greater extent than a mixture of either of these two acids with oleic acid. Barring these exceptions, and for all practical purposes, the fact remains that a high percentage of butyrin, or of olein, or of both, causes the mixed butterfat to have a relatively low melting point, while a low percentage of butyrin, or of olein, or of both, causes the mixed butterfat to have a relatively high melting point. Therefore, in early summer, when, because of the freshening of the majority of the cows, the per cent of bu- tyrin is relatively high, and because of the cows gorging them- 1 Eckles and Palmer — Influence of Plane of Nutrition of the Cow Upon the Composition and Properties of Milk and Butterfat. Missouri Research Bulle- tin 24. 1916. 2 Hunziker, Mills and Spitzer — Moisture Control of Butter, Factors not under Control of the Buttermaker. Purdue Bulletin 159, 1912. 3 Lewkowitsch — Chemical Technology and Analysis of Oils, Fat and Waxes, Vol. I, 1909. * Twitchell— Journal Ind. Eng. Chem., Vol. VI, p. 564, 1914; also Analyst, Vol. XXXIX, p. 448, 1914. COMPOSITION AND PROPERTIES OF BUTTER 535 selves with succulent pasture grass, the per cent olein is also high, often amounting to about 50 per cent of the total fat, the melting point of the mixed fat is relatively low and the butter made from this butterfat is relatively soft. Physical Structure of Butterfat. — In freshly drawn milk and cream the butterfat consists of miscroscopic, liquid fat globules. These fat globules are present in the form of a fairly permanent emulsion in the skim milk which consists of water in which are dissolved the milk sugar, albumen and part of the milk ash, and which contains in suspension the casein. The casein is of colloid nature and the skim milk may logically be considered an emulsion of hydrated colloid. Milk and cream, then, are a fat-in-hydrated colloid emulsion, or a fat-in-skimmilk emulsion. The fact that the butterfat globules remain as independent units, and that they form this emulsion, is due to the fact that nature produces them in this fine state of division in the first place. Fisher and Hooker very interestingly show that the secretion of butterfat is the result of fatty degeneration of the cells in the alveoli of the mammary gland or udder. In this fatty degenera- tion the cells break down, liberating the minute fat globules in a fat-in-hydrated colloid emulsion, in which they retain their individuality because of the forces of surface tension, adsorption and viscosity, as explained under "Philosophy of Churning," Chapter X. Size of Fat Globules. — As previously stated the butterfat, or milk fat, is present in milk and cream in the form of very minute fat globules. These fat globules vary in size from about one micromillimeter to about 17.4 micromillimeters ; they average about from three to five micromillimeters in diameter. One micromillimeter, or one micron represents about one twenty- five tousandth of one inch. The size of the fat globules is controlled by breed and period of lactation of the cows, and it is influenced by temporary indisposition of the cows and abrupt changes in feed. The Channel Island breeds, the Jerseys and Guernseys, produce milk in which the fat globules average nearly three times as large in diameter as those in the milk from the Hoi- steins and Ayrshires. At the beginning of the period of lactation the fat globules are largest. As the period of lactation advances the average 536 COMPOSITION AND PROPERTIES OF BUTTER size of the fat globules gradually decreases and is smallest shortly before the cows go dry. See also Chapter X on Churning. The relative size of the fat globules exerts a marked in- fluence on the mechanical firmness of the butterfat and butter, and, therefore, on the moisture content of the resulting butter. Butter made from relatively large fat globules is much softer, churns much easier and more rapidly and contains more moist- ure than butter made from relatively small globules. This is RELATIVE SIZE OF THE SMALLEST AND LARGEST GLOBULES OBSERVED Pig'. 84 Volume — .5236 cubic microns Volume — 2758.32 cubic microns Diameter — 1 micron Diameter — 17.4 microns clearly shown by the results of Hunziker1, who, by centrifugal separation, produced different lots of cream from the same milk, containing average large globules (54.24 cubic microns) and average small globules (20.72 cubic microns). Sixteen churnings were made from each type of cream. The churning conditions, as to temperature of cream, time held, amount of cream, richness of cream, acidity of cream, etc., were the same for all churnings. The results are shown in the following table : The small-globule cream churned with difficulty, the butter required over twice as much time to "break" as the large-globule cream, and it formed round, hard, smooth granules, which did not pack read- ily, and made a very firm and crumbly butter. The large-globule 1 Hunziker, Mills and Spitzer, Purdue Bulletin 159, 1912. COMPOSITION AND PROPERTIES OF BUTTER 537 Table 74. — Effect of Size of Average Fat Globules on Per Cent Moisture in Butter Experiment Number Large — Globule Cream. Average Volume of Globules 54.249 Cubic Microns Small — Globule Cream. Average Volume of Globules 20.724 Cubic Microns Churning Number Moisture in Butter Percent Churning Number Moisture in Butter Percent 1 1 3 19.38 20.19 2 4 17.70 17.75 2 5 7 26.62 26.28 6 8 21.24 19.20 3 9 11 21.70 21.40 10 12 16.21 17.72 4 13 15 19.05 18.54 14 16 16.03 15.47 5 17 19 19.76 17.61 18 20 15.69 16.28 6 21 23 20.41 20.61 22 24 1-7.01 16.28 7 25 27 23.06 20.00 26 28 17.20 17.50 8 29 31 18.50 19.95 30 32 18.14 17.17 Average 20.82 17.29 cream churned rapidly, formed soft, irregular, ragged-edged flakes, which packed readily and made a rather soft-bodied but- ter. The milk from which the two kinds of cream were produced came from cows of the same breed, of as nearly the same age and the same stage of the period of lactation as possible. These results suggested that the difference in the firmness of the butter may have been due to a difference in chemical composition of the fat, between the large and the small fat globules. Lemus1 and Kluseman2 claim that such a difference does exist. Lemus found more volatile acid and less olein in the small fat globules than in the large ones. Kluseman states that 1 Lemus, Diss. Leipzig, 1902. •Kluseman, Diss. Leipzig, 1893. 538 COMPOSITION AND PROPERTIES OF BUTTER the large fat globules contain more of both the volatile acids and the olein than the small fat globules. On the other hand, Siedel and Shaw and Eckles found no difference in the chemical com- position of the large and small fat globules of the same milk. Hunziker's results agree with the findings of the last four in- vestigators as shown in the Table 75. These findings suggest that the softer butter with the higher moisture content, resulting from the large-globule cream is not due to a lower melting point of the fat in these globules, but is largely due to physical or mechanical influences. The forces overcoming the surface tension are greater in the larger globules, causing them to lose their equilibrium and to collapse more readily, and yielding a butter with a softer body which is more miscible with water and which retains water more read- ily than the firmer butter, which results from the smaller fat globules. Table 75. — Chemical Composition of Butter Fat from Cream with Large Average Globules and from Cream with Small Average Globules. Large and Small-Globule Butter Reichert- Meissl Number Iodine Number Saponi- fication Number Melting Point Soluble Acids % Insoluble Acids % Refrac- tive Index Large 3034 28.92 232 2 339 607 88.90 42.2 Large Small 30.35 3020 28.90 2950 231.6 231 3 34.1 33 7 6.00 609 88.50 89.15 42.0 42.0 Small 30.30 29.30 231.6 34.0 5.98 89.00 41.7 Average large globules 30.34 28.91 231.9 34.0 6.04 88.70 42.1 Average small globules 30.25 29.40 231.4 33.9 6.04 89.08 41.9 The Water, Moisture Control. — The water in butter rep- resents quantitatively the largest non-fatty constituent of butter. Under normal conditions of manufacture the water content in finished butter ranges about from 12 to 16 per cent. In very abnormal cases butter has been found to contain less than ten COMPOSITION AND PROPERTIES OF BUTTER 539 per cent and over 20 per cent water, but butter can be made to contain considerably less than 10 per cent and very much more than 20 per cent water. The water content of butter averages about 14 per cent. The water content of butter after washing and draining, but before working and salting, and while the butter is still in granular form, under normal conditions of churning, firmness of butter and size of granules, generally averages above 16 per cent, but it varies considerably with the firmness of the butter and size of the butter granules. Other factors being the same, soft butter granules have a higher water content than firm and hard granules. In the case of normal firmness and very fine granules, similar in size to small rice kernels, the water content of butter before work- ing and salting averages around 20 to 24 per cent. In the form of small corn kernels butter averages around 17 to 18 per cent water and in still larger form, such as in lumps, the water content may drop below 16 per cent, always provided, how- ever, that the butter is of normal firmness at the time it "breaks." If the large granules or lumps are excessively soft, such as is the case when the churning temperature was too high in proportion to the melting point of the fat, then such lumps usually show a high water content. In such cases both the soft- ness of the butter and the over-churning are the direct result of the high churning temperature which causes the butter to "break" and gather so rapidly that excessive massing takes place before the churn is stopped. In unsalted butter and in properly worked, salted butter, the water is present largely in the form of microscopic droplets, varying widely in size and ranging in diameter from less than one micron (one twenty-five thousandth of one inch) to over 15 microns (three five thousandths of one inch). In butter prior to working and in much of the salted butter there are present also considerable quantities of water in the form of large drops and water aggregates larger than drops. As previously stated with relation to the physical structure of butterfat and the philosophy of churning, butter represents an emulsion of hydrated colloid-in-fat, that is, it is an emulsion of buttermilk-in-fat. When the butter is worked, a portion of 540 COMPOSITION AND PROPERTIES OF BUTTER the buttermilk, that which adheres to the surfaces of the butter granules, is removed and replaced by the water and when the butter is salted and worked a portion of the "remaining butter- milk and water is replaced by or fuses with, the brine, or both. When the butter is worked, most of the free water is ex- pelled, while the firmly held and finely emulsified microscopic droplets in the interior of the butter granules remain in the butter. For this reason, during the first stages of the working process the water content of butter decreases, and under normal conditions drops to about 13 per cent or slightly lower. As the working process progresses, the butter loses its granular state and becomes less friable and more plastic. When this state is reached further working causes the butter to "pick up" water from the churn and the water content increases again. The amount of water which the butter now assimilates and the extent to which the water content increases, depends on the mechanical condition of the butter, as determined by the melting point of the butterfat, the temperature of the cream and the washwater, and on the amount of water there is in the churn. The amount of water present in the churn obviously is largely governed by the extent of draining, with the churn doors ajar before and during the working process. If the churn is stopped with the doors ajar and down after every few revolutions of the churn, and the butter is allowed to drain completely each time, so that all the free water escapes, further working decreases the water content of the butter. But even when working with the churn doors closed, so that free water remains in the churn, a point is gradually reached when further working no longer materially increases the water content of the butter. A point of saturation has then been reached that does not permit of additional incorporation of water. The time when this point is reached depends largely on the mechanical firmness of the butter and the temperature of the water in the churn. The softer the butter and the warmer the water, the greater the amount of water that can be in- corporated before the point of saturation is reached. Conditions that tend to disturb the emulsion of buttermilk-, water-, or brine-in-fat, reduce the amount of water that is capable COMPOSITION AND PROPERTIES OF BUTTER 541 of remaining in butter in the form of very finely divided drop- lets, unaided by working. In sweet-cream, unsalted butter, the fine state of division of the water droplets present in butter before working remains practically intact and is not materially affected by working. In sour-cream butter the lactic acid present has a tendency to slightly lower the permanency of the emulsion by its action on the nitrogenous constituents of the buttermilk and such butter may be expected to show a slightly smaller number of very small droplets and a slightly larger number of larger droplets. The difference, however, is very slight. In salted butter the effect of the salting-out influence of the emulsion is very marked and during the early stages of the working process salted butter shows a marked decrease in the number of small droplets and a decided increase in the number of the larger droplets. In this condition the water in butter is not permanently fixed, the emulsion is incomplete and the but- ter is leaky. This butter, therefore, has to be worked until the body is sufficiently plastic to permit, by means of the working process, the redivision and re-emulsification of the water droplets until the size of these droplets is again reduced nearly to the point that prevailed before the salting and working commenced, other- wise this butter remains permanently leaky. It may be logically considered, therefore, that the water in butter is present in two forms; namely, in the form of very finely divided droplets, as originally emulsified and locked up in the granules during the churning process, and in the form of larger droplets, drops and aggregates of drops of free moisture, which is loosely held in the interstices between the butter gran- ules and a part of which adheres to their surface. The control of moisture in butter, then, resolves itself into the retaining in the butter of the first form of water, the finely divided and thoroughly emulsified droplets originally present, and the dividing and emulsifying into the butter of a portion of the free water; and the ease with which the moisture content is controlled depends on the control by the buttermaker over the mechanical firmness of the butter and the temperature of the cream and wash water. 542 COMPOSITION AND PROPERTIES OF BUTTER .• The natural firmness of the butter varies with locality and season of year, but the actual firmness can- be controlled readily by the proper adjustment of the churning temperature, and the proper adjustment and control of the churning temperature is the foundation of satisfactory moisture control. When, in the spring, the butterfat becomes softer, the churning temperature must be lowered sufficiently to maintain the desired firmness of the butter. In the fall, when the natural change in the character of the butterfat tends towards a firmer butter, the churning tem- perature must be raised sufficiently to offset this change. The extent to which the butter is drained before, or during the work- ing process, or both, will further influence the control of its moisture content. In the case of unsalted butter, moisture control is largely a matter of giving the free water an opportunity to escape, since, under average conditions, the amount of water present in its original, finely divided and thoroughly emulsified form, repre- sents a very large portion of the total per cent of water that legal butter is permitted to contain. In unsalted butter the tendency naturally is toward a high moisture content. In the case of salted butter the salt, owing to its great affinity for water, causes a large number of the very small droplets to run together into drops and to escape as free water. Moisture control, here, therefore, has to do with the re-division, re-emulsification and reincorporation of a sufficient amount of the free water, in order to bring the per cent moisture back to that desired, and this is accomplished by proper working. Moisture Control. — Factory Directions. — Owing to the many and ever-changing factors which influence the property of the butter to retain or take up and hold water, such as type of churn, character of butterfat, churning temperature, etc., it is, as yet, not possible to reduce the art of moisture control to a mathemat- ical, exact science, whereby a given formula may be depended upon to produce the desired results. Moisture control is an art, the success of which demands local experience and judgment on the part of the buttermaker, quite as much as scientific knowl- edge. For this reason, the specific method that should be used for best results, must be left to the judgement of the buttermaker, who, operating his churns daily, is familiar with his local condi- COMPOSITION AND PROPERTIES OF BUTTER 543 tions and is in the best position to know how to go about under his particular conditions. Attempts to reduce moisture control to a fixed method, by reducing the moisture content of butter by means of preliminary draining and working to a figure below the percentage desired, then testing for per cent moisture and adding the mathematically calculated correct amount of water to increase the moisture con- tent to the desired per centage in the finished butter, have not proven entirely successful. In the absence of the availability of a more specifically exact method, the following procedure is recommended : 1. Have the churning temperature of the cream sufficiently low to complete the churning process in 40 to 60 minutes and to produce butter of a good firm body. Do not overload the churn and run the churn at about 30 revolutions per minute. 2. Hold the cream at the churning temperature not less than two hours. 3. Wash with water at a temperature the same, or nearly the same, as the temperature of the buttermilk, drain well and give the churn a revolution or two to bring the butter up on the shelves. 4. If the butter happens to be unexpectedly soft, use wash water several degrees colder than the buttermilk. This condi- tion, however, tends toward a leaky body. 5. If the butter happens to be excessively firm, use wash water a few degrees warmer than the temperature of the but- termilk. 6. Trench the butter, distribute the salt uniformly over the entire trench, wet the salt with a small amount of water and close the trench. In the case of a tendency toward excessive moisture, omit wetting of the salt. 7. Give the butter from 12 to 20 revolutions in a four-roll churn, or 25 to 35 revolutions in a two-roll or one-roll churn, according to needs, and test for moisture. 8. If previous experience has shown that there is a tendency for butter to take up excessive moisture, stop the workers after every few revolutions of the churn and allow the butter to drain, with churn doors down and ajar and the churn swinging freely. 544 COMPOSITION AND PROPERTIES OF BUTTER 9. If previous experience has shown that there is a tendency for butter to be low in moisture, work with the churn doors closed. 10. If the moisture test taken at the churn (see paragraph 7) is high, allow the butter to set for a few minutes, then give the churn another revolution with the workers in gear and again let drain with the churn doors down and ajar. Repeat this until the test shows that excessive moisture is no longer present. 11. If the excess moisture refuses to be expelled by follow- ing directions in paragraph 10, remove the butter to the cooler in tubs or other containers, allow it to harden overnight. The next morning strip the tubs, cut the butter into small pieces with wire, and rework as in paragraph 10. This will usually bring the moisture' down to the desired point. 12. If. after following directions in paragraph 11, the mois- ture is still excessive, put the butter in the cooler again and repeat the reworking next day. 13. If the moisture test (see paragraph 7) is slightly too low, give the butter a few more revolutions with the churn gates closed and test again. 14. If the moisture test (see paragraph 7) is considerably too low, calculate the amount of water needed to raise it to the desired point and add the calculated amount of water at a temperature a few degrees higher than the temperature of the buttermilk and work again with the churn doors closed until the desired per cent moisture has been reached. Calculate the amount of water needed by multiplying the difference between the test secured and the test desired by one ond one-fourth times the pounds of fat in the churn and divide by 100. Example : Test desired 15.9 per cent Test secured 13.5 per cent Difference 2.4 per cent Fat in churn 800 Ibs. 2.4 X 1.25 X 800 — 24 Ibs. water to be added. 1UU 15. It will be found, in following the above suggestions, that the results may fall short of those desired under many conditions, in which case they need modification to suit condi- tions. COMPOSITION AND PROPERTIES OP BUTTER 545 For instance, in churns in which the free water in the churn precedes the butter in its movement toward and through the workers, increase in moisture content may be found exceed- ingly difficult. Under these conditions great care should be taken not to drain and especially not to work the butter ex- cessively before salting. Continued working and draining before salting also renders complete solution of the salt difficult be- cause it may cause such a reduction of the moisture in butter, that not enough water is left to readily dissolve the salt and these conditions make the assimilation of free water difficult, in spite of overworking. The author's purpose of submitting these very inexact sug- gestions is merely to place before the buttermaker, especially if he be a beginner, some concrete idea of the principles involved and their practical application, which may assist him in working out his own method of moisture control that will best suit his local conditions and equipment. Relation of per cent moisture to quality of butter. — Within reasonable limits, not exceeding about 16 per cent, the moisture content of butter has no marked effect on its quality. Butter con- taining 16 per cent moisture, other conditions being the same, may have as good quality and may keep as well, as butter con- taining only 12 per cent moisture. Generally speaking, however, excessive moisture does not improve the quality of the butter, and it may give rise to butter of very inferior quality, develop- ing such off-flavors as oiliness and fishiness. This is not neces- sarily due so much to the actual amount of water present, but rather to the process of manufacture that was responsible for the high water content. Whenever the high per cent of water is the result of over- working the butter, quality is sacrificed. The breaking down of the grain and the emulsification of air in butter, which are inevitable incidents to such moisture incorporation, are antag- onistic to good flavor and keeping quality. They invite oxidation and other channels of decomposition. This is especially the case with butter made from sour cream. Butter made in summer readily holds 16 per cent water without overworking. Such butter is entirely normal, its grain 546 COMPOSITION AND PROPERTIES OF BUTTER has suffered no mutilation. It may therefore be of just as good flavor and keeping quality as butter containing much less water. In fact, if the low-moisture butter required excessive working in order to reduce the water content, the high-moisture butter may be superior. On the other hand, high-moisture butter made in winter is often very inferior to low-moisture butter, because overworking was necessary in order to hold up the moisture content. In winter, when the butterfat is naturally firm and the butter tends to be low in moisture, it may be preferable, from the standpoint of quality, if the buttermaker insists on incor- porating the maximum water permitted by law, to raise the churning temperature sufficiently to make the butter "come" in very slightly softer condition, rendering it more miscible with water and thereby making unnecessary excessive working, rather than to mutilate the body of very firm butter by overworking, always providing, however, that the slightly less firm butter is not overworked. The buttermaker should clearly understand that the less firm the butter, the greater the danger of over- working. Soft butter does not stand much working without injury to its grain. It also usually tends to have a leaky body. The Curd. — The curd represents the nitrogenous constitu- ents of butter. It is generally thought of as the casein (casein lactate) derived from the buttermilk. This impression may be somewhat erroneous, as it appears that there are other nitrog- enous substances in butter with properties differing somewhat from those of casein and casein lactate. Storch1 separated from butter a nitrogenous substance which formed a slimy precipitate in acetic acid, quite different from the usual white, cheeselike, lumpy or flocculent precipitate formed by the casein. This slimy precipitate was insoluble in weak ammonia, and in a 2 per cent solution of sodium hydroxide, while the casein dissolves exceed- ingly readily in these solutions. According to Storch, this nitrogenous substance corresponds completely with a protein associated with the fat globules. He claims that on the basis of its insolubility in the above alkalies, this slimy substance 1 Storch — 36 Bericht des Koenigl. Veterinar- und Landbauhochschule- Laboratoriums, Kopenhagen, Denmark. COMPOSITION AND PROPERTIES OF BUTTER 547 constituted a little over 60 per cent of the protein, or curd, in butter, while the remainder of about 40 per cent is casein. Storch's findings and conclusions may assist in the explana- tion why, even when the churning process is stopped while the butter granules are still exceedingly minute, and when this butter is subsequently very thoroughly washed with repeated washings, so that the butter drains perfectly clear, it is not possible to reduce the curd content, as determined by the Kjel- dahl method, to any appreciable extent below about .4 per cent. This slimy protein substance does not wash out. The curd content of butter is determined and expressed in one or the other of two entirely different ways and yielding results in per cent curd, that differ from one another. One way is to determine the nitrogen content of butter, and by multiply- ing the results by the factor 6.38, expressing it as per cent protein. This represents the true curd content. The other way is to determine the per cent curd by difference, by deducting the sum of the per cent of fat, moisture and salt from 100. In this case the per cent curd so obtained embraces, aside from the protein, also the traces of ash, acid and lactose contained in butter. This is termed the physiological curd. In the case of the true curd of butter, the percentage of curd usually fluctuates between about .5 per cent and one per cent, averaging about from .6 to .7 per cent, provided that the butter is washed in a normal manner. Butter made from sweet cream, and unsalted butter, has a slightly higher curd content than butter made from ripened cream and butter that was salted. Butter that is only very slightly washed contains more curd than butter in the manu- facture of which the churn is stopped when the granules are still very small and which are washed thoroughly. Butter that is not washed at all usually contains from about 1 to 1.5 per cent curd. In case of expressing the curd content as physiological curd, the percentage of curd averages from .5 to .6 per cent higher than the true curd. The Salt. — The salt is the one constituent of butter strictly foreign to the natural composition of butter, unsalted butter con- 548 COMPOSITION AND PROPERTIES OF BUTTER taining only very minute traces of sodium chloride as a part of its mineral content. Being added to the butter, the amount of salt which butter may contain is controlled exclusively by the buttermaker. The great bulk of all butter manufactured in the United States is salted butter, and most of the foreign butter intended for export trade is also salted butter. Salted butter contains from about 1 to 5 per cent of salt. Most of the salted butter on the market averages from about 2.5 to 4.0 per, cent salt, and the great bulk contains between 3 and 3.5 per cent salt. For the best interests of the butter industry, excessive salt- ing should be avoided and the per cent salt should be held down to below 4 per cent. The consumer's objection to excessively salted butter is clearly expressed by the San Francisco Wholesale Dairy Produce which issued a ruling that after February, 1, 1916, the salt con- tent of all butter coming into San Francisco shall be three per cent. They further state that practically all the butter that had been coming into San Francisco recently (prior to February 1, 1916) contained a much higher per cent of salt and that one of the chief complaints on all butter was that butter contained too much salt. See also Chapter XI on Salting. The Lactose, C12 H22 Olt + H2O.~ Normal butter contains from about .20 to .45 per cent of lactose, or milk sugar. The lactose is the sugar of milk which is present in solution in the milk, cream and buttermilk, and a portion of which the butter- granules, in their process of forming, pick up and lock up. The per cent lactose in butter obviously varies somewhat according to the extent of washing and removal of buttermilk. The more thorough the. washing, the less lactose the butter will contain. In instances where skimmilk powder is added to the butter in the churn, such as is done in some creameries for the purpose of incorporating extraneous curd in the butter, the lac- tose content of the butter also increases. In experiments with skimmilk powder, conducted by Hunziker and Hosman,1 butter contained as high as 1.26 per cent lactose. 1 Hunziker and Hosman — A Study of the Composition of Butter. Blue Valley. Research Laboratory, 1917. COMPOSITION AND PROPERTIES OF BUTTER 549 The lactose content of butter decreases slightly in storage, partly because of the probable conversion of small portions of the lactose, through bacterial, or through chemical action, into lactic acid, glycolic acid and other acids, and partly due to loss of water or brine by leakage. The lactose is one of the unstable and readily fermentable constituents of butter, it rapidly yields to bacterial action, split- ting up into simpler compounds, of which lactic acid is a very prominent one, but not necessarily the only one. Under certain conditions lactose also readily yields to chemical decomposition detrimental to the market value of the butter. Being itself a powerful reducing agent, it invites and accelerates oxidation in butter, especially in a weakly alkaline condition. In butter made from over-neutralized cream, the lactose may give rise to most disastrous butter defects, such as bleached and tallowy butter, as demonstrated by Hunziker and Hosman.1 In butter with a decided acid reaction, on the other hand, lactose appears to have no deteriorating action, on the contrary, it tends to exert a slight, but distinct preservative influence. It is for this reason that some butter manufacturers purposely add lactose to their butter. The Acid. — Fresh butter contains from about .1 to .35 per cent acid, presumably largely, but generally not exclusively, lactic acid. In a similar manner, as in the case of curd and ash of butter, the acid is derived from the cream o'f which it is a natural constituent. Therefore, sweet cream butter contains less acid than ripened-cream butter, and butter made from sour cream that has been neutralized contains less acid than butter from unneutralized sour cream. Butter made from pasteurized cream contains less acid than butter made from raw cream. This is especially the case with the flash process, or high tem- perature pasteurization, as shown by Hunziker, Spitzer and Mills2 in Table 77. The decrease of the acidity of butter, due to pasteurization of the cream is in all probability due to the presence, in the raw 1 Hunziker & Hosman — Tallowy Butter, Blue Valley Research Laboratory, also Journal of Dairy Science, Vol. I, No. 4, 1917. 2 Hunziker, Spitzer and Mills — Pasteurization of Sour, Farm-Skimmed Cream for Butter Making. Purdue Bulletin 203, 1917. 550 COMPOSITION AND PROPERTIES OF BUTTER cream, of carbon dioxide and other volatile acids which are ex- pelled by the heat of pasteurization, and the higher the tem- perature of pasteurization the more readily do these volatile acids escape. It has been noticed also by the author and others that the reduction of acid due to pasteurization is much greater in the case of cream that had undergone considerable fermenta- tion before pasteurization, than in cream that is comparatively fresh and unfermented. Table 77.— Per Cent Acid in Butter Made from Different Por- tions of the Same Cream Before and After Pasteuriza- at 145° F. 20 Minutes, 165° F. Flash and 185° F. Flash. Per Cent Acid in Butter. Raw Cream Butter Pasteurized Cream Butter. 145° F. 20 Minutes 165° F. Flash 185° F. Flash Fresh butter .3260 .2448 .2250 .2034 In storage the acidity of the butter increases slightly, - due to the breaking down of a portion of the milk sugar as shown in the following results by Hunziker, Spitzer and Mills,1 and Table 78.— Showing Relation of Per Cent. Lactose and Per Cent. Acid in Fresh and Stored Butter Made from Raw and Pasteurized Cream — Averages of 44 Churnings. Lactose Acidity Age of butter decrease per increase cream months per in 3 cent. in 3 cent. months months Raw fresh .339 .3073 Raw 1 month .367 .3613 Raw 3 months 336 .063 4073 .1000 145 degrees F. 20 minutes fresh 398 2565 145 degrees F. 20 minutes 1 month 360 2745 145 degrees P. 20 minutes 165 degrees P. flash 3 months fresh .353 .388 .045 .2835 2295 .027 165 degrees F. flash 165 degrees F. flash 185 degrees F. flash 185 degrees F. flash 185 degrees F. flash 1 month 3 months fresh 1 month 3 months .343 .315 .389 .360 .350 .073 .039 .2543 .2655 .2093 .2295 .2655 .036 .056 x Hunziker, Spitzer and Mills— Pasteurization of Sour, Farm-Skimmed Cream for Butter Making. Purdue Bulletin 203, 1917. COMPOSITION AND PROPERTIES OF BUTTER 551 probably also as the result of partial cleavage of the proteins and fats. It was formerly believed that the acidity was favorable to the keeping quality of butter, and that ripened cream butter would keep better than sweet cream butter. The great bulk of experimental data on the relation of acidity to keeping quality, and the experience in the commercial manufacture of butter, have amply demonstrated that such is not the case. It is now conceded by the best authorities on the subject, that the acid content of butter, is one of the active agents, which, in com- bination with other factors, hastens decomposition, leading to the development of specific flavor defects, and shortening the life of good butter. The Ash. — The Ash, or mineral matter, is present in butter in very small amounts only, ranging from about .09 to .20 per cent. It very rarely exceeds .14 per cent and it averages about .12 per cent. It is derived from the ash of milk and cream and therefore has a similar composition as the ash of milk, which is as follows: Table 79. — Composition of Ash in Butter from Sour Cream, Butter Not Washed but Thoroughly Worked.1 Potassium Oxide 19.329 per cent Sodium Oxide 7.714 " " Calcium Oxide 23.092 " " Magnesium Oxide 3.287 " " Iron Oxide (Ferric) and Sulphuric Acid 288 " " Phosphoric Acid (Anhydride) 44.273 " " Chlorine . 2.604 " " 100.587 Less Oxygen Equivalent to Chlorine 587 " 100.000 ' 1 Fleischmann — Lehrbuch der Milchwirtschaft, 1901. 552 COMPOSITION AND PROPERTIES OF MILK COMPOSITION OF MILK. Table 80. — Average, Maximum and Minimum Composition of Cow's Milk. Average Composition by Different Max- Min- Investigators of Milk imum per ct. imum per ct. Far- rington & Woll1 per ct. Van Slyke2 5552 an- alyses per cent Eckles3 per ct. Bab- cock4 per cent Fleisch- mann5 per cent Water 90.0 82.0 87.4 87.1 87.1 87.17 87.75 Fat 7.8 2.3 3.7 3.9 3.9 3.69 3.40 Casein 1 Albumin ' J 4.6 2.5 3Z 2.5 .7 3.4 3.02 .53 2.80 .70 Milk sugar 6.0 3.5 5.0 5.1 4.75 4.88 4.60 Ash * .9 .6 .7. .7 .75 .71 .75 Total Solids 12.6 12.9 12.80 12.83 12.25 Solids, not fat 8.9 9.0 8.90 9.14 8.85 Specific gravity at 60° F. 1.02^—1.034; average 1.032. Specific heat, at 61-62.6° F. .9406— .9523. (Chanoz and'Vaillant.) At 57-61° F. .9457, at 81° F. .9351 (Fleischmann.5) Freezing point —.54 to —.57° C. Average —.555° C. (31° F.) (Grim- mer.6) Table 81. — Average Composition of Cow's Milk, by Major Breeds. Percentage of Fat in Total Solids.3 Breeds Fat Per Cent Total Solids Per Cent Solid not Fat Per Cent Parts of Fat in 100 Parts of Total Solids Holstein 345 1229 884 28 Ayrshire 385 1298 913 296 Guernsey 498 1420 922 350 Tersev. . 5 14 1490 976 345 Brown Swiss. . 3.91 13.28 9.37 29.4 1 Farrington and Woll, Testing Milk and Its Products, 1908. 8 Van Slyke. Modern Methods of Testing Milk and Its Products. 1916. « Eckles, Dairy Cattle and Milk Production, 1911. *Babcock, Wing Milk and Its Products, 1909. 6 Fleischmann, Das Buch der Milchwirtschaft, 1901. • Grimmer, Chemie und Physiologic der Milch, 1910. COMPOSITION AND PROPERTIES OF MII.K 553 Table 82. — Composition of Ash in Normal Cow's Milk.1 Mineral Constituents In Milk In Ash Per Cent In Milk Per Cent Potassium oxide (potash) 25 02 175 Sodium oxide (soda). 1001 070 Calcium oxide (lime) 2001 140 Magnesium oxide (magnesia) . . 242 017 Iron oxide (ferric) 13 001 Sulphur trioxide 3 84 A?7 Phosphoric pentoxide 2429 170 Chlorine. 1428 100 Total ash 100.00 .700 Table 83.— Composition of Colostrum Milk.2 Time After Calving Specific Gravity Water % Fat % Casein % Albumin % Sugar % Ash % Total Solids % Immediately . . 1.068 73.07 3.54 2.65 16.56 3.00 1.18 26.93 After 10 hours. 1.046 78.77 4.66 4.28 9.32 1.42 1.55 21.23 After 24 hours. 1.043 80.63 4.75 4.50 6.25 2.85 1.02 19.37 After 48 hours. 1.042 85.81 4.21 3.25 2.31 3.46 .96 14.19 After 72 hours. 1.035 86.64 4.08 3.33 1.03 4.10 .82 13.36 Table 84. — Composition of Ash in Colostrum Milk.3 Potassium oxide ........... .................. 7.23 per Sodium oxide ____ .............. .... ........... 5.72 " Calcium oxide ...:.. ____ > ..................... 34.85 " Magnesium oxide ............................ 2.06 " Iron oxide (ferric) . . . . ................ ____ _____ .52 " Phosphoric acid (anhydride) ................... 41.43 " Sulphuric acid ....... . . . .............. * ........ 16 " Chlorine . , 11.25 " cent Less oxygen equivalent to chlorine 103.22 3.22 100.00 1 Leach — Food Inspection and Analysis, 1914. 2 Engling-Leach — Food Inspection and Analysis, 1914. 8 Fleischmann — Lehrbuch der Milchwirtschaft, 1901. 554 COMPOSITION AND PROPERTIES OF Table 85. — Composition of Mammalian Milks. Kind of Milk Analyst or Author No. of Analyses «§£ •3 > ccO f £ Total Solids % * 1 c 3^ | •1^ o 1 Albumin % II 1 Lactose % | £ 1 WOMAN— Minimum.. Maximum . Average . . . cowT Minimum . . Maximum . Average . . . GOAT— Minimum. . Maximum . Average . . . EWE— Minimum. . Maximum . Average . . . BUFFALO— Minimum. . Maximum . Average. . . Koenig* 1.027 1.032 L0348 1.0285 1.0290 1.0340 1.0320 81.09 91.40 87.41 88.13 89.47 82.0 90.0 87.4 87.1 87.17 82.02 90.16 85.71 85.80 87.11 74.47 87.02 80.82 78.70 83.00 81.56 84.23 82.69 82.93 81.67 8.60 18.91 12.59 11.87 10.53 10.00 18.00 12.60 12.90 12.83 9.84 17.98 14.29 14.20 12.89 12.98 25.53 19.18 21.30 17.00 15.77 18.44 17.31 17.07 18.33 1.43 6.83 3.87 2.24 3.02 2.3 7.8 3.7 3.9 3.69 3.10 7.55 4.78 4.50 4.45 2.81 9.80 6.86 8.94 5.30 6.69 9.19 7.87 7.46 9.02 .50 4.32 2.29 2.41 1.89 2.5 4.6 3.2 3.2 3.55 3.22 5.05 4.29 5.00 3.67 4.42 7.46 6.52 6.34 6.30 3.99 7.78 5.88 4.59 3.99 .18 1.96 1.03 1.96 .95 .32 2.36 1.26 .45 .94 3.88 8.34 6.21 i37 3.5 6.0 5.0 5.1 4.88 3.26 5.77 4.66 4.00 4.09 2.76 7.95 4.91 5.02 4.60 4.16 5.18 4.52 421 .12 1.90 .31 .25 .32 .60 .90 .70 .70 .71 .39 1.06 .76 .70 .72 .13 1.72 .89 1.00 .80 .72 .85 .76 .86 .86 I « Grimmer2 « Farrington &Woll3 « Van Slyke4 Babcock5 200 1 1 5552 2.5 3.02 2.44 3.94 3.20 3.80 2.00 3.59 5.69 4.97 '70 .53 .78 2.01 1.09 1.20 1.67 .83 1.77 1.55 Koenig* 1.0280 1.0360 1.0305 1.0320 1.0313 1.0298 1.0385 1.0341 .0377 .0369 .0310 .0336 .0323 1.0339 « Fleischmann6 .... Scheurlen2 .... '266 Avg. Koenig1 . % « Sartori2 "32 2500 Avg. Fleischmann6 .... Szentkiralyi2 . . 4.60 1.70 a u Fleischmann6 .... Rimini2 "2 3.63 .73 5.06 1 Koenig — Chemie der Menschl. Nahrungs- und Genussmittel. Compiled by Leach. 2 Grimmer — Chemie und Physiologic der Milch, 1910. 8 Farrington and Woll — Testing Milk and Its Products, 1908. *Van Slyke— Modern Methods of Testing Milk and Its Products, 1916. B Babcock-Wing — Milk and Its Products, 1909. 6 Fleischmann — Das Buch der Milchwirtschaft, 1901. 7 Richmond — Dairy Chemistry, 1914. COMPOSITION AND PROPERTIES OF CREAM 555 Table 85.— (Continued.)* Kind of Milk Analyst or Author o'! 6 § K< 0 >> fj-^ -*-3 coO r Total Solids % | £ 2 Total Protein % II .9$ 1 o i$ 1 f$ £ 1 Mare Ass .. . Fleischmann* . . . . 1.0310 1.0347 1.0350 1.0330 1.0360 1.0320 90.70 90.78 90.13 88.85 89.64 91.23 89 14 9.30 9.22 9.87 11.15 10.36 8.77 1086 1.20 1.21 .94 .36 1.64 1.15 1 °r8 2.00 1.99 1.65 1.31 2.22 1.50 9S1 5.70 5.67 6.98 4.94 5.99 6.00 6.04 4.80 4.25 3.13 3.11 4.91 1.95 1.33 0.00 .40 .35 .30 .31 .51 .40 .53 .38 1.07 1.05 .91 .51 2.56 .57 .46 .99 .46 Koenig1 47 1.24 .75 Vieth2 Schlossman2 .... .98 .67 .94 .33 1.55 .53 Mule Koenig1 5 Ellenberger2 Aubert & Colby2. Leed» Henry & Well2. . . Koenig1 Sow Avg. 91.59 80.96 84.09 77.00 81.63 69.50 41.11 48.76 69.80 48.67 8.41 19.04 15.91 23.00 18.37 30.50 58.89 51.24 30.20 51.33 1.59 7.06 4.55 9.26 3.33 10.45 45.80 43.71 19.40 43.67 1.64 6.20 7.23 9.72 9.08 15.54 11.19 7.57 9.43 7.11 .... .... Doe Koenig1 4.15 3.12 5.57 5.96 Cat Koenig1 Rabbit Pizzi* 1.0493 Guinea Pig . . Delphin. . Purdie2 Franklain2 Whale Scheibe2 Richmond7 * For references to above table, see previous page. Table 86. — Composition of Cream. Constituents of Cream By Centrifugal Separation By Gravity Creaming Snyder1 % Rich- mond* % Fleisch- mann* % Fleisch- mann8 % Fleisch- mann* % Koenig4 % Water 66.41 25.72 } 3.70 3.54 .63 33.59 7.87 39.37 56.09 2.29 1.57 .38 60.63 4.24 29.6 67.5 1.3 1.5 .1 70.4 2.9 68.5 25.0 2.8 3.3 .4 31.5 6.5 72.9 20.0 3.0 3.6 .5 27.1 7.11 68.82 22.66 3.76 4.23 .53 31.18 8.42 Fat Casein . . Albumin Milk Sugar Ash. Total Solids Solids not Fat . . Specific gravity. — See Standardization of Milk and Cream. Specific heat of cream testing 19.18% fat at 14-16° C. .9833; at 27.5° C. .8443 (Fleischmann).3 1 Snyder — Dairy Chemistry. 2 Richmond — Dairy Chemistry, 1914. * Fleischmann — Lehrbuch der Milchwlrtschaft, 1901. * Leach — Food Inspection and Analysis, 1914. 556 COMPOSITION AND PROPERTIES OF SKIM MILK Table 87. — Composition of Ash in Cream.4 Potassium oxide 28.381 per cent Sodium oxide 8.679 " " Calcium oxide 23.411 Magnesium oxide 3.340 Iron oxide (ferric) 2.915 " " Phosphoric acid (anhydride) 21.735 " " Chlorine . .... 14.895 " " Less oxygen equivalent to chlorine 103.356 3.356 " 'v* 100.000 " " Table 88. — Composition of Skimmilk. Centrifugal Separation Gravity Creaming in Skim Milk VanSlykei % Snyder2 % Rich- mond3 % Fleisch- mann4 % Fleisch- mann4 % Water Fat 90.30 .10 90.25 .20 90.48 .12 90.35 .20 89.85 .75 Casein Albumin . 2.75 .80 | 3.60 3.22 .42 I 4.00 4.03 Milk Sugar 5.25 5.15 4.88 4.70 4.06 Ash .80 .80 .78 .75 .77 Total Solids 9.70 9.75 9.52 9.65 10.15 Specific gravity at 60°F. 1.035 to 1.038; average 1.036. Specific heat at 14 to 16° C. .9388* at 27.5° C. .9455 (Fleisch- mann)4; at 0° C. .940; at 15° C. .943; at 40° C. .952 (Hammer and Johnson)5. xVan Slyke — Modern Methods of Testing Milk and Its Products. 2 Snyder — Dairy Chemistry. "Richmond — Dairy Chemistry, 1914. * Fleischmann — Lehrbuch der Milch wirtschaft. 6 Hammer and Johnson — The Specific Heat of Milk Products. Iowa Re- search Bulletin 14, 1913. COMPOSITION AND PROPERTIES OF BUTTERMILK 557 Table 89: — Composition of Ash in Separator Skim Milk.5 Potassium oxide 31.634 per cent Sodium oxide 10.265 " " Calcium oxide 21.913 Magnesium oxide 3.115 Iron oxide (ferric) 921 " Phosphoric acid (anhydride) 19.478 " Sulphuric acid (anhydride) 1.000 " " Chlorine 15.071 103.397 "• " Less oxygen equivalent to chlorine 3.397 100.000 " " Table 90. — Composition of Buttermilk. Constituents in Buttermilk From Ripened Cream From Sweet Cream Van Slykei % Storch2 % Snyder3 " % Vieth* % Fleisch- mann8 % Storcha % Rich- mond* % Water Fat • 90.6 .1 2.8 .8 4.4 .6 .7 90.93 .31 ^3.37 ' 4.58 .81 90.5 .2 3.3 5.3 .7 90.39 .50 3.60 4.06 .75 .80 91.30 .50 3.50 | 4.00 .70 89.74 1.21 3.28 4.98 .79 90.98 .35 3.51 /4.42 1 .01 .73 Casein Albumin Milk Sugar. . . . Lactic Acid .... Ash Specific gravity of sweet-cream buttermilk 1.033 16. Specific gravity of sour-cream buttermilk 1.03146. Table 91. — Composition of Ash in Buttermilk.5 Potassium oxide 24.53 Sodium oxide 1 1.54 Calcium oxide 19.73 Magnesium oxide 3.56 Iron oxide (Ferric) and Sulphuric acid 47 Phosphoric acid (anhydride) 29.89 Chlorine . . 13.27 per cent Less oxygen equivalent to chlorine 102.99 2.99 100.00 1 Van Slyke — Modern Methods of Test Milk and Its Products. 2 Storch — Richmond's Dairy Chemistry. 3 Snyder — Dairy Chemistry. 4 Vieth — Richmond's Dairy Chemistry. 6 Flelschmann — T.ehrbuch der Milchwirtschaft, 1901. 6 Richmond — Dairy Chemistry, 1914. 558 COMPOSITION AND PROPERTIES OF WHEY Table 92.— Composition of Whey. Constituents of Whey VanSlyke % Fleisch- mann Koenig % Smetham % Vieth from Skim Milk Water Fat. . Casein Albumin . . . Milk Sugar. Ash Total Solids 93.40 .35 .10 .75 4.80 .60 6.60 93.15 .35 1.00 4.90 .60 6.85 93.38 .32 .86 4.79 .65 6.62 93.33 .24 .88 5.06 .49 6.67 93.00 .09 .92 5.45 .52 7.00 Specific gravity 1.025 to 1.028 (Fleischmann1). Specific heat, at 0° C, .0978; at 15° C., .976; at 60° C, .972. Hammer and Johnson.2 Table 93. — Composition of Separator Slime. Richmond3 Fleischmann1 per cent per cent Water 66.24 68.20 Fat . .50 1.44 Protein 22. 25.34 Milk sugar 50 Other organic matter 7.75 Ash 3.01 3.22 Total milk solids 26.01 30.00 Table 94. — Composition of Ash in Separator Slime.1 Potassium oxide 3.155 per cent Sodium oxide 1.325 Calcium oxide 45.025 Magnesium oxide 3.361 Iron oxide (ferric) 1.846 Phosphoric acid (anhydride) 43.976 Chlorine 1.691 100.381 " " Less oxygen equivalent to chlorine 381 " " 100.00 1 Fleischmann — Buch der Milchwirtschaft, 1901. a Hammer and Johnson — The Specific Heat of Milk and Milk Derivatives. Iowa Research Bulletin 14. 1913. 8 Richmond — Dairy Chemistry, 1914. HEAi/THtfui,]smss OF BUTTER f 559 CHAPTER XIX. HEALTHFULNESS, FOOD VALUE AND BIOLOGICAL PROPERTIES OF BUTTER Sanitary Purity and Healthfulness : The degree of free- dom £>f butter from products of decomposition and from micro- organisms harmful to man, must of necessity vary greatly with the purity of the raw material, the milk and cream from which the butter is made and with the process used for manufacture. And these factors in turn are subject to wide variations. Whole milk creameries which receive their milk in fresh condition and have exclusive control over the cream, are in a position to prevent undesirable fermentations that render both cream and butter unpalatable though not necessarily unwhole- some. All creameries receiving cream instead of milk, depend to a large extent on the cream producer for the quality and de- gree of freshness of their raw material. Most gathered-cream creameries receive their cream in more or less sour condition, the degree of acidity varying from sweet cream with no more than .2 per cent acid, to sour cream with an acidity of from .3 to 1.2 per cent and averaging about .5 per cent acid. The acidity of the cream naturally varies with such conditions as location, season of year, facilities and inclination of the producer to cool the cream on the farm, and frequency of delivery or shipment. Cream coming from territory in the southern tier of the dairy belt, where the climate is relatively warm and the temper- ature of the available water on the farm is too high to permit of sufficient cooling to check acid development entirely, will naturally average higher in acidity than cream produced in the northern sections of the dairy belt where the nights are general- ly cool and the available water for cooling the cream is cold. During the hot summer months the cream naturally con- tains a higher per cent of acid than is the case with winter cream. Farmers who have a proper understanding and appreciation of the importance of taking adequate care of their cream, and who are equipped with cooling tanks for the cooling and storing of their cream, are in a position to furnish a much sweeter cream 560 HEAI/TH*UI,NESS OF BUTTER than producers lacking this knowledge, appreciation and equip- ment. Creameries located in territories in which the cow popula- tion is dense, the herds relatively large and the radius of cream supply condensed, are able to receive cream with a lower acidity than creameries that draw their supply from territories with a sparse cow population, where the herds are small and far be- tween and where dairying is merely a side line of general farm- ing. In such territories the volume of cream is too small to permit of shipments or deliveries sufficiently frequent to insure its arrival in sweet condition. Aside from the production of acid in the cream, other fer- mentations may and frequently do set in, which tend to lower the quality of the cream and the flavor, keeping quality and market value of the butter. The great majority of these fer- mentations, while objectionable from the standpoint of the mar- ket value of the butter, are so far as is known, entirely harmless as related to the health of the consumer. In rare cases isolated cans of cream may contain matter of putrefaction. The shipment and acceptance of such cream is unlawful in most states. Such cream is rejected or discarded by the creameries, or confiscated by the health authorities. In the process of manufacture efforts are made to minimize the effect of the conditions which tend to jeopardize the keeping quality of the product. These efforts largely consist in standardizing the acidity of the cream by the use of a neutral- izer, in pasteurization to remove objectionable microorganisms, in using a pure culture starter of lactic acid bacteria to intensi- fy the desirable flavor, and in washing the butter with pure water to eliminate much of the buttermilk. None of these steps in the process of manufacture are ob- jectionable from the standpoint of the health of the consumer. The neutralizer most commonly used is milk of lime which in itself is a necessary food element of man and if it were taken up by the butter in appreciable quantities could do no possible harm. However, analyses have shown that butter made from cream in which the acidity was standardized by the use of lime, contained no appreciable increase in lime content over butter made from cream not so treated. Pasteurization has no noticeable HEAI/THFUI is CO 8 03 H • o >o >to :£« :S§ s o6 oo '8 :S :8 :8 0000000 nnn cream and 88.33 Ibs. skim milk (100—11.67 = 88.33). TESTING MILK AND CREAM FOR ACID 593 The removal of 125 Ibs. of skim milk necessitates the separa- tion of 88.33 : 100= 125 :X, or 141.5 pounds of the 1000 Ibs. of 3.5% milk. EXAMPLE 8. 2000 Ibs. of 32 per cent cream are wanted. How many pounds of skim milk starter and how many pounds of 38 per cent cream must be mixed? 38 32 32 0 6 38 38 : 32 = 2000 : X; X = 1684 Ibs. 38% cream 38 : 6 = 2000 :X; X= 316 Ibs. starter. 2000 Ibs. 32% cream. In order to secure 2000 Ibs. of 32 per cent cream, 1684 Ibs. of 38 per cent cream must be mixed with 316 Ibs. of skim milk starter. TESTING MILK, CREAM AND STARTER FOR ACID The acidity in milk, cream and starter is intimately related to the flavor and keeping quality of the resulting butter. It is impor- tant for the creamery to know the acidity of the milk when it arrives at the factory so as to determine its fitness for manufacture. In the ripening of cream and starter the acidity expresses the degree of ripeness, and in the neutralization of sour cream the acidity must be accurately determined in order to enable the operator to use the correct amount of neutralizer that will reduce the acidity to the desired point. It is important, therefore, that the creamery use sys- tematically a simple, practical and accurate test of milk, cream and starter for acid. Principle of Acid Tests. — Numerous acid tests have been devised for this purpose, all of which are based on the principle of measuring the per cent acid by the amount of alkali needed to reduce a measured volume of the sample to be tested to the neutral point. These tests are devised on the basis that -a given volume of a normal solution of an alkali neutralizes the same volume of a normal solu- tion of an acid. By the term "normal solution" is meant a solution 594 TESTING MII,K AND CREAM FOR ACID which is so prepared that one liter shall contain the hydrogen equiv- alent of the active reagent weighed in grams (Sutton).1 In other words, a normal solution of an acid is a solution which contains in one liter as much of the active reagent, the acid, as is represented by the molecular weight of the acid in grams. In the case of lactic acid (C3H6O3) the molecular weight is 90. A normal solution of an alkali is a solution which contains in one liter as much of the active reagent, the alkali, as is represented by the molecular weight of the alkali in grams. In the case of caustic soda or sodium hydroxide (NaOH) the molecular weight is 40. Since equal amounts of normal solutions of acids and alkalies neutralize each other, 1 c.c. of N Na OH (1 c.c. of a normal solu- tion of caustic soda or sodium hydroxide) neutralizes 1 c.c. of N C3 H6O3 (1 c.c. of a normal solution of lactic acid). The acid contained in milk, cream and starter is largely lactic acid and is always calculated as such. The alkali used for determining the per cent acid is sodium hydroxide (NaOH), commonly known as caustic soda. In order to know when a liquid is alkaline and when it is acid, or when enough alkali has been added to reduce all the acid and render the liquid neutral, a color indicator is used that shows different color reaction in acids and in alkalies. Of the several indi- cators available, that known as phenolphthalein is most commonly and most suitably used in acid tests of milk and cream. In acids, such as sour milk, sour cream and starter, phenolphthalein is color- less similar as water. In alkaline solutions, such as sodium hydrox- ide, phenolphthalein turns to a deep pink color. Hence, when enough sodium hydroxide has been added to milk, cream or starter, to neutralize all the acid, these products turn pink. The moment a permanent faint pink color appears, the test is completed and the number of cubic centimeters of sodium hydroxide needed to produce this permanent faintly pink tint, serves as the basis upon which the per cent acid is calculated. In order to augment the sensitiveness and accuracy of the test, alkaline solutions, much weaker than a normal solution, are used. In most tests the alkaline solution is a tenth normal solution of N sodium hydroxide (^- NaOH). The alkaline solution must be of standard strength, it must be accurate, otherwise the test cannot be dependable in its results. It 1 Farrington & Woll, Testing Milk and Its Products. TESTING MII.K AND CREAM FOR ACID 595 is not feasible for the average creamery which has no chemical laboratory, and no skilled chemist, to weigh out the dry sodium hydroxide and to make up the desired strength solution from it. Attempts to do this work under ordinary creamery conditions almost invariably result in alkaline solutions that are not of standard strength and that yield erroneous tests. The creamery may, however, purchase standard alkaline solu- tion of a strength suitable to be used without further dilution, or it may purchase a concentrated standard alkaline solution which can be diluted in accordance with the directions furnished on the bottle, or it can purchase the chemically pure, dry sodium hydroxide of exact known weight and dissolve the contents of the entire package in the necessary amount of distilled water, or the sodium hydroxide may be purchased in the form of tablets of known strength, which, when dissolved in a given amount of water, produce the desired standard solution. Any of the above enumerated forms of alkali will yield standard alkaline solutions, when purchased from a reliable supply house, when diluted with or dissolved in the correct amount of distilled water, or rain water, or other water free from alkalies or acids, and when care is taken that all of the alkali contained in one and the same purchased container is used and that none of it is spilled. For creameries that are not equipped with a chemical laboratory and that do not have the services of a skilled chemist the purchase and use of sodium hydroxide in any of the forms enumerated above will generally place at their disposal uniformly accurate alkaline solu- tions. For creameries that maintain their own chemical laboratory, the following method, devised by Hunziker and Hosman,1 may as- sist in the further "fool-proofing" of tenth normal alkali solutions : Use a common large stock bottle, a two gallon bottle, such as can be readily purchased from and easily replaced by any drug store. These bottles, when filled to just below the neck, hold 7500 cubic centimeters. Fill them with water to the 7500 c.c. mark and mark the 7500 c.c. level by a scratch on the shoulder of the bottle with a file. Crush in a mortar, or otherwise, sodium sticks and weigh 30 grams of the crushed sticks each into glass tubes. The tubes should i Hunziker and Hosman, A Practical M'ethod for the Preparation of Accu- rate NAOH Solutions for Acid Tests. Blue Valley Research Laboratory 596 TESTING MII^K AND CREAM FOR ACID be constructed of reasonably thin glass, the ordinary test tubes used in the chemical laboratory are very suitable for this purpose. They should have an outside diameter of % inch and should be about 7 inches long, so that they readily slip through the mouth of the two- gallon bottle. Seal these tubes by fusing the glass over the flame. In order to make up a tenth normal solution, all the operator has to do is to drop one of these tubes rilled with dry sodium hydroxide into the two-gallon bottle. The tube breaks as it strikes the bottom of the bottle, releasing the alkali. Now fill the bottle with water to the scratch on the shoulder. Mix thoroughly by placing hand over mouth of bottle and inverting it several times, until the alkali is all dissolved. This is now a tenth normal solution which is ready for use. When the solution has been used up, empty the bottle of the remnant of solution and the broken glass tube, drop into the bottle a fresh tube and again fill up with distilled water and mix. If commercial sodium sticks are used, which are not chemically pure, from 31 to 32 grams are required, according to the extent of impurities present. In this case the sodium hydrate should be care- fully titrated against standard acid, so as to determine the exact amount of sodium hydrate to be weighed into the glass tubes that will yield, in the 7500 c.c. of distilled water, a tenth normal solution. Calculation of Per Cent Acid When a Tenth Normal Solution of Sodium Hydroxide is Used 1 c.c. ^ NaOH neutralizes 1 c.c. ^ C3H6O3. N 1 c.c. of a -r:r lactic acid solution contains .009 grams lactic • i J. \J acid. Hence, in order to find the per cent acid in milk, cream or starter, multiply the cubic centimeters of alkali solution required to neutralize the milk or cream with .009, divide the product by the grams of milk or cream used and multiply by 100. N c.c. alkali solution X .009 X 100 = % lactic acid. grams milk or cream .ME .1 For all practical purposes the measuring of the milk or cream gives sufficiently accurate results to obviate the less practical and TESTING MII^K AND CREAM FOR ACID 597 more time-consuming work of weighing. While the size of the sample may vary, factory experience has shown that 18 grams makes a very practical sample. It represents enough material to insure reasonable accuracy and it obviates complex calculations to determine the per cent acid. In the case of milk the 18 grams are measured with the standard 17.6 c.c. Babcock test pipette. In the case of cream an 18 c.c. or possibly a 9 c.c., pipette is used. The cream pipette must be rinsed with water and the rinsings added to the sample. Example : 7.4 c.c. of tenth normal alkali solution are required to neutralize 18 c.c. of cream to a faint pink color. What is the per cent acid? 7.4 Or, for more rapid calculation, simply divide the c.c. alkaline solution required, by 20. 7-4 ^ — = .37 per cent acid. If instead of an 18 c.c. pipette, a 9 c.c. pipette is used, then only one-half as much alkaline solution, or 3.7 c.c., is required and the per cent acid is calculated as follows: 37 * -009 X 100 = .37% acid. Or the c.c. alkaline solution required is simply divided by 10. -j-=z .37 per cent acid. Phenolphthalein indicator is prepared by dissolving 1 gram dry. phenolphthalein in 100 c.c. of a mixture of one-half alcohol and one- half water. Standard Acid Tests and their Equipment for Factory Use. — The following are practical and satisfactory acid tests, the equipment and chemicals for which can be readily secured from glassware manufacturers and from dairy and creamery supply houses : Mann's Acid Test. — Apparatus needed: 50 c.c. graduated burette with burette stand for measuring the alkaline solution ; a 50 c.c. pipette for measuring the cream, a white cup and stirring rod or teaspoon. N Reagents needed: j^rNaOH (a one-tenth normal solution of 598 TESTING MILK AND CREAM FOR ACID sodium hydroxide) and an alcoholic solution of phenolphthalein. Both of these solutions may be purchased from creamery supply houses or chemical supply houses. Making the Test. — With the 50 c.c. pipette transfer 50 c.c. of the cream into the white cup, rinse pipette with water and add rins- ings to sample in cup. Add one-half c.c. of phenolphthalein solu- tion. Fill the 50 c.c. burette with the tenth normal solution of sodium hydroxide. Run this solution slowly from the burette into the white cup, stirring the cream constantly. Each drop of sodium hydroxide will give the cream a pink color which at first immediately disappears. As more of sodium hydrate solution is added the pink color disappears more gradually until, when the neu- tral point has been reached the pink color of the cream remains con- stant for several minutes. When this point is reached, that is, when upon stirring a faint pink color remains in the cream, enough sodium hydroxide has been added and the test is completed. Now read off on the graduations of the burette the number of c.c. of decinormal alkali solution that was used and multiply this by the factor .018. OOQ ( ' X 100 = .018). This gives the per cent acid in the cream. N Example. — 35 c.c.yjy NaOH are required to neutralize 50 c.c. of cream. What is the per cent acid? 7C v OOQ C ' X 100, or 35 X -018= .63% acid. *)U The detection of the pink color is facilitated by adding a pipette full of water to the cream in the cup before titrating. A Practical Factory Test. — For practical creamery operation the Mann's acid test is modified to the extent of using a 17.6 c.c. pipette for milk or an 18 c.c. pipette for cream instead of a 50 c.c. pipette. Measure 17.6 c.c. or 18 c.c. of the milk or cream to be tested into the white cup. Add 5 drops of phenolphthalein indi- cator and then add tenth normal alkaline solution from the burette until a permanent faintly pink color appears, stirring the milk or cream in the cup with the rod while adding the alkaline solution. Do not add alkali until the sample is deep pink. If not sure that the neutral point has been reached and that enough alkaline solution has been added, pour one drop of phenolphthalein indicator into cup. If the milk or cream turn pink the test is completed, if no pink color TESTING MILK AND CREAM FOR ACID 599 appears, add more alkaline solution from the burette: When the test is completed divide the number of c.c. tenth normal alkaline solution required to produce the pink shade, as indicated on the graduation of the burette, by 20. The result represents per cent acid. ^ N Example. — 12 c.c. -r^ NaOH are needed to neutralize the 18 c.c. of milk or cream. 12 20 = .6 per cent acid. rig-. 85. Nans Alkali Bottle and Burette for Acid Test Courtesy of Louis F. Nafls Farrington Alkaline Tablet Test. — Apparatus Needed. One 100 c.c. graduated glass cylinder with stopper; one 17.6 c.c. Bab- cock pipette; one white cup. Reagents. — Farrington Alkaline tablets. Making the Test. — Dissolve 5 tablets in 97 c.c. wrater in the glass cylinder. As these tablets require about six hours for com- plete solution it is advisable to place the tablets in the water in the cylinder on the evening before the day when the solution is to be 600 TESTING MILK AND CREAM FOR ACID used ; stopper tightly and 'lay the cylinder horizontally. This insures complete solution by the time the tablet solution is needed. When ready for the test, pour with the pipette 17.6 c.c. cream into the white cup and add tablet solution from the cylinder until the cream remains faintly pink. Then read off the number of c.c. of tablet solution used on the graduations of the cylinder. Each c.c. tablet solution represents .01 per cent acid. Example. — 60 c.c. tablet solution are required to neutralize the cream, in the cup. 60 X .01 = .6 per cent acid. The Farrington alkaline tablets are especially convenient because they contain both the alkali and the indicator. They may be purchased from any creamery supply house. They should be kept perfectly dry and in the dark. Otherwise they will weaken and the indicator will bleach out. For maximum accuracy an 18 c.c. pipette should be used for cream. Marshall Acid Test. — Apparatus Needed. One alkaline solu- tion bottle with graduated burette, one 9 c.c. pipette, one white cup, one bottle for indicator. Reagents Needed. — Tenth normal solution of sodium hydro- xide (neutralizer) and phenolphthalein indicator same as in Mann's test. Making the Test. — With the pipette pour 9 c.c. of cream into the white cup ; add a few drops of indicator. Fill neutralizer bottle N with the -Tp solution of sodium hydroxide. Fill the graduated bur- ette by tipping the bottle until the burette is full and run neutralizer from the burette into the cream in the cup until the cream remains slightly pink. The number of c.c. of neutralizer solution used, as indicated on the graduation of the burette, represents per cent acid- ity. Soxhlet-Henkel Acid Test— This test is very similar to the previous tests, but instead of expressing the results in number of cubic centimeters of decinormal alkaline solution required, as is the case in Mann's acid test, or in per cent of acid in the cream as is the case of the Farrington Tablet test and the Marshall Acid test, the Soxhlet-Henkel Acid test gives its results in degrees acid. One degree is equivalent to approximately .045 per cent acid or to 2.5 c.c. decinormal alkaline solution of Mann's acid test using 50 c.c. of cream. In this test a one-fourth normal solution of sodium hydrate is used for neutralizing the acid. DETERMINATION OF SPECIFIC GRAVITY 601 Apparatus Needed. — One Soxhlet-Henkel titration apparatus consisting of one 50 c.c. graduated burette with pinch cock ; one solu- tion bottle with double perforated stopper and equipped with rubber bulb and connection with burette ; one 50 c.c. pipette for measuring cream ; one white cup or porcelain dish ; one 2 c.c. pipette for meas- uring the indicator. Reagents Needed. — One-fourth normal solution of sodium hydrate and an alcoholic solution of phenolphthalein. Making the Test.— With 50 c.c. pipette pour 50 c.c. of the cream to be tested into the white cup. Add 2 c.c. of the phenolphtha- lein indicator. Fill the burette to the top graduation with the alkaline solution from the bottle by pressing the rubber bulb. Then draw from the burette enough of the alkaline solution into the cup until after rotating the cup, or stirring the contents, a faint pink color remains. The number of cubic centimeters of the alkaline solution required, as shown on the graduation of the burette, are termed degrees of acid. Each cubic centimeter of the one-fourth normal alkaline solution represents one degree of acid. This method was later modified by Soxhlet-Henkel to the extent of using 100 c.c. of cream instead of 50 c.c. and increasing the phe- nolphthalein from 2 c.c. to 4 c.c. Here again each cubic centimeter of one-fourth normal alkaline solution required to neutralize the acid in the cream represents one degree of acid. In this case one degree of acid is equivalent to .0225 per cent acid, or 1.25 c.c. of decinormal alkaline solution of Mann's test. In stating the degree of acid by the Soxhlet-Henkel method it is necessary therefore to know whether they refer to the use of 50 c.c. or of 100 c.c. of cream. DETERMINATION OF SPECIFIC GRAVITY OF MILK SKIM MILK, CREAM AND BUTTERMILK Definition. — By the specific gravity of a liquid is meant the weight of a given volume of the liquid, such as milk, skim milk, cream, etc., as compared with the weight of the same volume of water at the same temperature. The specific gravity of water is 1. That is, one cubic centimeter of water weighs one gram. Milk is heavier than water, therefore its specific gravity is greater than that of water. Average milk has a specific gravity of 1.032. The specific gravity is usually determined or calculated at a temperature of 60° F. The specific gravity of liquids is readily determined by means 602 DETERMINATION OF SPECIFIC GRAVITY of instruments called hydrometers. The hydrometer is a floating glass spindle, so constructed that it rests in the liquid to be tested in an upright position. The spindle bears a graduated scale on which the specific gravity, or its equiva- lent at a given temperature (usually 60° F.), can be read at a glance. In order to make the divisions on the scale as far apart as possible and to thereby make the instrument most sensitive and accurate, different hydrometer scales have been devised and are used for different liquids. The hydrometers used for milk are called lactometers, of which there are two types, namely, the Quevenne lactometer and the New York Board of Health lactometer. Quevenne Lactometer. — The Quevenne lactometer is the one most generally used for determining the specific gravity of milk and skim milk. It consists of a spindle with a scale gradu- ated from 15 to 40, a weighted bulb, and usually a thermometer. The scale is divided into 25 equal parts, ranging from 15 to 40. Each divi- sion is called a degree and every fifth division is numbered on the scale. Each division corre- sponds to one point of the third decimal of the specific gravity scale. The Quevenne degrees are converted into specific gravity by adding 1000 and dividing by 1000. .1 Example. — Quevenne Reading is 32. What is the specific gravity? 1000 + 32 1000 = 1.032 specific gravity. The Quevenne lactometer is so constructed that the scale records the correct degree at a temperature of 60° F. At a temperature above 60° F. the reading is corrected by adding one- M< 4-. Board tenth point to the actual reading for each degree of Hcaltn Pigf. 86. Quevenne Lactometer Courtesy F. above 60. At a temperature below 60° F. de- B?osnncor duct one-tenth point for each degree F. below 60. Lactom- DETERMINATION Otf SPECIFIC GRAVITY 603 Example. — Quevenne reading at 65° F. is 33. What is the corrected reading? 33 + -5 = 33.5, corrected Quevenne reading. For the use of the Quevenne lactometer provide a glass or tin cylinder about 10 inches high and one and one-half inches wide. Fill the cylinder with the milk to be tested. The temperature of the milk should be within the limits of 50 to 70° F. Insert the lacto- meter and when it has found its equilibrium, note the point on the scale at the surface of the milk. This represents the Quevenne degrees. The milk should be free from foam. Freshly drawn milk, and skim milk direct from the centrifugal separator will yield too low readings because of the incorporated air. Such milk should be allowed to stand at rest until the air has had a chance to escape. New York Board of Health Lactometer. — This type of lacto- meter has an arbitrary scale, it does not show the specific gravity direct. It was originally constructed for the use of milk inspectors in eastern cities, but its use is now only very limited.- It has a graduation from zero to 120. The zero point is the point to which this lactometer sinks in water. The 100 mark is the point to which the scale sinks in milk of a specific gravity of 1.029 at 60° F., which is assumed to be the lowest^ specific gravity of normal milk, or milk to which no extraneous water has been added. 'The distance between zero and 100 is divided into 100 equal points and the scale is extended beyond the 100 divisions to 120. To convert New York Board of Health lactometer degrees into Quevenne degrees, multiply the B. of H. reading by .29 and to convert Que- venne degrees into B. of H. degrees divide the Quevenne degrees by .29. EXAMPLES. Milk tests 110 B. of H. lactometer degrees at 60° F. What is the Quevenne reading at 60° F. 1 10 X. 29 = 31.9 degrees Quevenne. Milk tests 34 degrees Quevenne lactometer at 60° F. What is the B. of H. reading at 60° F. ? 34 -yg = 117.2 degrees B. of H. lactometer. 604 DETERMINATION OF SPECIFIC GRAVITY Table 101. — Degrees on Quevenne Lactometer Corresponding to Degrees on New York Board of Health Lactometer. Board of Health Degrees Quevenne Degrees Board of Health Degrees Quevenne Degrees Board of Health Degrees Quevenne Degrees 60 17.4 81 23.5 101 29.3 61 17.7 82 23.8 102 29.6 62 18.0 83 24.1 103 29.9 63 18.3 84 24.4 104 30.2 64 18.6 85 24.6 105 30.5 65 18.8 86 24.9 106 30.7 66 19.1 87 25.2 107 31.0 67 19.4 88 25.5 108 31.3 68 19.7 89 25.8 109 31.6 69 20.0 90 26.1 110 31.9 70 20.3 91 26.4 111 32.2 71 20.6 92 26.7 112 32.5 72 20.9 93 27.0 113 32.8 73 21.2 94 27.3 114 33.1 74 21.5 95 27.6 115 • . 33.4 75 21.7 96 • 27.8 116 33.6 76 22.0 97 28.1 117 33.9 77 22.3 98 28.4 118 34.2 78 22.6 99 28.7 119 34.5 79 22.9 100 29.0 120 34.8 80 23.2 • For temperatures above 60° F. add one lactometer degree for every 3° F. above 60. For temperatures below 60° F. deduct one lactometer degree for every 3° F. below 60. The New York Board of Health lactometer is used in a similar manner as the Quevenne lactometer. Specific Gravity of Cream and Buttermilk. — The aerometric or hydrometer method of determining the specific gravity is not gen- erally suitable for cream and buttermilk. The viscosity of the cream and the usual presence of varying amounts of air in cream render the results unreliable. In the case of buttermilk, the chief objection lies in the fact that when this product is fluid enough to afford reason- ably free movement of the lactometer, the curd drops to the bottom rapidly and before a satisfactory reading can be taken; and when the consistency of the buttermilk is such as to prevent the rapid separation of the curd, it is too viscous to permit the hydrometer DETERMINATION OF SPECIFIC GRAVITY 605 to find its equilibrium in a reasonable length of time. It is advisable, therefore, to resort to the gravimetric, or picnometer method of determining the specific gravity in cream and in buttermilk. Gravimetric Determination. — This consists of the filling of a perfectly dry picnometer or other graduated flask of known meas- ure with milk at the standard temperature (60° F., or 15.5° C.) and weighing the flask and contents. The weight of the flask is then deducted from the weight of the flask plus contents and the differ- ence is divided by the weight of an equal volume of water at stand- ard temperature. The result is the specific gravity of the milk. The Westphal balance method furnishes another accurate means of determining the specific gravity. Both the gravimetric method and the Westphal balance method, while accurate when operated by the skillful chemist, require considerable time. Experimental comparisons have demonstrated that for all practical purposes of testing milk and skim milk the Quevenne hydrometer, when accu- rately graduated, yields correct results, and the simplicity and rap- idity of its operation render its use in the determination of specific gravity of milk and skim milk highly advantageous and satisfactory. Weight of One Gallon of Butterfat, Water, Milk, Skim Milk and Cream in Pounds. — In the standardization of milk and cream it is necessary to know the amount of milk and cream by weight in pounds and not by measure in gallons. In American creameries the weight of milk and cream is frequently not definitely known. For the convenience of the operator, therefore, a table is here given showing the weight per gallon of these liquids at a temperature of approximately 60° F. The weight of one gallon of cream obviously varies with its butterfat content. As the cream increases in richness, its specific gravity is lowered and its weight per gallon decreases. The weight of one gallon of cream or any other liquid is determined by multiply- ing the weight of one gallon of water, which is 8.3389, by the spe- cific gravity of the liquid in question. For example, skim milk has an average specific gravity of about 1.036. One gallon of skim milk therefore weighs 1.036 X 8.3389 = 8.6391 Ibs. The specific gravities of cream of different richnesses were cal- culated by the following formula adopted by and secured through the courtesy of Professor E. H. Farrington1 : i Farrington, by correspondence, 1916. 606 DETERMINATION OF SPECIFIC GRAVITY Table 102.— Specific Gravity at 60° F. and Weight in Pounds, of One Gallon, of Butterfat, Water, Milk, Skim Milk and Cream. Kind of Liquid Specific Gravity at 60° F. Weight of one Gallon Pounds Butterfat 0.9300 Water 1.0000 Milk average 1.0320 Skim milk average 1.0360 Cream, 10 per cent fat 1.0243 15 " " " 1.0186 16 " " " 1.0174 17 " " " 1.0163 18 " " " 1.0152 19 " " " 1.0140 20 " " " 1.0129 21 " " " 1.0118 22 " " " 1.0107 23 * " " 1.0096 24 " " " 1.0085 25 " " " 1.0073 26 " " " 1.0062 27 " " " 1.0051 28 " " " 1.0040 29 " rt " 1.0029 30 " " " 1.0017 31 " " " .... 1.0006 32 u " " 0.9995 33 " " " 0.9984 34 " " " 0.9973 35 " " " 0.9963 36 " " - 0.9952 37 " " " 0.9941 38 " " " 0.9930 39 " " " 0.9919 40 " " " 0.9908 41 " " " 0.9897 42 " " " 0.9886 43 " " • " 0.9875 44 " " " 0.9864 45 " " « 0.9854 46 " " " 0.9843 47 " " " 0.9832 48 " " « 0.9821 49 " " " . 0.9811 8.3389 8.6057 8.6391 8.5417 8.4938 8.4843 8.4749 8.4654 8.4560 8.4465 8.4372 8.4278 8.4184 8.4090 8.3997 8.3905 8.3812 8.3719 8.3626 8.3534 8.3443 8.3352 8.3260 8.3168 8.3076 8.2985 8.2894 8.2804 8.2714' 8.2624 8.2534 8.2444 8.2354 8.2265 8.2176 8.2087 8.1998 8.1909 8.1821 DETERMINATION OF SPECIFIC GRAVITY Table 102. — Continued. 607 Kind of Liquid Specific Gravity at 60° F. Weight of one Gallon Pounds 50 " " " 09801 81733 51 " " " 0.9790 8.1646 52 " " " 09780 8.1558 53 " " " 0.9770 8.1470 54 " " " 0.9760 81382 55 " " " .. 09749 8 1294 56 " " " 09738 81207 ry « « ,. 0.9728 8.1121 58 " " " 0.9718 8.1035 59 " " " 0.9707 8.0948 60 " " " 0.9637 8.0861 70 " " " 09595 80007 80 " " " 0.9494 79172 90 " " "... 09396 78353 100 " " " . 0.9300 7.7552 Specific gravity of fat at 15° C., .93. Specific gravity of fat-free serum at 15° C. = 1.036. F = per cent of fat in any cream. 100 — F = per cent of serum. Volume of fat in 100 grams of cream = — c.c. 100-F Volume of serum in the same cream = 1.036 c.c. Volume of 100 grams of cream must equal the sum of the above F , 100-F quantities, or -^ +-T5^-cc. Since volume in cubic centimeters multiplied by the specific gravity equals the weight in grams (F 100-F \ "93"+ 1036 ) X sPecific^ravity of cream =100. By reduction the following formula is obtained : Q •* f 96.348 Specific gravity of cream — 93 » 195 p The values in the Table 102 are theoretical and apply only to cream free from air, in which the specific gravities of fat and 608* DETERMINATION OF TOTAI, SOLIDS serum conform to the above assumptions. The actual weights found in most cases will be somewhat less than the weights given in the table because of the varying amounts of air in the cream. They are calculated on the bases of a temperature of approximately 60° F. Cream at a higher temperature will weigh slightly less and cream at a lower temperature will weigh slightly more. DETERMINATION OF TOTAL SOLIDS IN MILK, SKIM MILK, CREAM AND BUTTERMILK By Means of the Babcock Formula. — For rapid and reason- ably accurate work the total sglids of milk may be determined by the use of the Babcock formula, which is as follows : Total solids — -^ + 1.2 X f. L = Quevenne lactometer reading, f = per cent of fat. Example : Lactometer reading is 32 ; per cent fat is 4. 32 Total solids =-j-+ 1.2 X 4= 12.8 per cent. For the determination of the solids not fat use the formula : -^+.2xf. = per cent solids not fat. or deduct the per cent fat from the per cent total solids. The Babcock formula for the determination of total solids and solids not fat is applicable only to milk and skim milk. For cream and buttermilk the gravimetric method is recommended. See also Table 103, showing per cent total solids in milk and skim milk when per cent fat and lactometer reading are known. Gravimetric Method. — "Heat from three to five grams of milk, skim milk or buttermilk at the temperature of boiling water until it ceases to lose weight, using a tared flat dish of not less than 5 c.c. diameter. If desired, from fifteen to twenty grams of pure, dry sand may be previously placed in the dish. Cool in a desiccator and weigh rapidly to avoid absorption of hygroscopic moisture. In the case of cream use only two to three grams of sample." DETERMINATION OF ToTAI, SOUDS 609 Table 103.— Per Cent Total Solids, When Per Cent Fat and Quevenne Lactometer Reading at 60° F. are Known, Quevenne Lactometer Reading at 60° F. Fat 26 27 28 29 30 31 32 33 34 35 36 per cent Total Total Total Total Total Total Total Total Total Total Total solids solids solids solids solids solids solids solids solids solids solids per per per per per per per per per per per cent cent cent cent cent cent cent cent cent cent cent 0.0 6.50 6.75 7.00 7.25 7.50 7.75 8.00 8.25 8.50 8.75 9.00 0.1 6.62 6.87 7.12 7.37 7.62 7.87 8.12 8.37 8.62 8.87 9.12 0.2 6.74 6.99 7.24 7.49 7.74 7.99 8.24 8.49 8.74 8.99 9.24 0.3 6.86 7.11 7.36 7.61 7.86 8.11 8.36 8.66 8.86 9.11 9.36 0.4 6.98 7.23 7.48 7.73 7.98 8.23 8.48 8.73 8.98 9.23 9.48 0.5 7.10 7.35 7.60 7.85 8.10 8.35 8.60 8.85 9.10 9.35 9.60 0.6 7.22 7.47 7.72 7.97 8.22 8.47 8.72 8.97 9.22 9.47 9.72 0.7 7.34 7.59 7.84 8.09 8.34 8.59 8.84 9.09 9.34 9.59 9.84 0.8 7.46 7.71 7.96 8.21 8.46 8.71 8.96 9.21 9.46 9.71 9.96 0.9 7.58 7.83 8.08 8.33 8.58 8.83 9.08 9.33 9.58 9.83 10.08 .0 7.70 7.95 8.20 8.45 8.70 8.95 9.20 9.45 9.70 9.95 10.20 .1 7.82 8.07 8.32 8.57 8.82 9.07 9.32 9.57 9.82 10.07 10.32 .2 7.94 8.19 8.44 8.69 8.94 9.19 9.44 9.69 9.94 10.19 10.44 .3 8.06 8.31 8.56 8.81 9.06 9.31 9.56 9.81 10.06 10.31 10.56 .4 8.18 843 8.68 8.93 9.18 9.43 9.68 9.93 10.18 10.43 10.68 .5 8.30 8.55 8.80 9.05 9.30 9.55 9.80 10.05 10.30 10.55 10.80 .6 8.42 8.67 8.92 9.17 9.42 9.67 9.92 10.17 10.42 10.67 10.92 .7 8.54 8.79 9.04 9.29 9.54 9.79 10.04 10.29 10.54 10.79 11.04 1.8 8.66 8.91 9.16 9.41 9.66 9.91 10.16 10.41 10.66 10.91 11.17 1.9 8.78 9.03 9.28 9.53 9.78 10.03 10.28 10.53 10.78 11.03 11.29 2.0 8.90 9.15 9.40 9.65 9.90 10.15 10.40 10.66 10.91 11.16 11.41 2.1 9.02 9.27 9.52 9.77 10.02 10.27 10.52 10.78 11.03 11.28 11.53 2.2 9.14 9.39 9.64 9.89 10.14 10.39 10.64 10.90 11.15 11.40 11.65 2.3 9.26 9.51 9.76 10.01 10.26 10.51 10.76 11.02 11.27 11.52 11.77 2.4 9.38 9.63 9.88 10.13 10 38 10.63 10.88 11.14 11.39 11.64 11.89 2.5 9.50 9.75 10.00 10.25 10.50 10.75 11.00 11.26 11.51 11.76 12.01 2.6 9.62 9.87 10.12 10.37 10.62 10.87 11.12 11.38 11.63 11.88 12.13 2.7 9.74 9.99 10.24 10.49 10.74 10.99 11.24 11.50 11.75 12.00 12.25 2.8 9.86 10.11 10.36 10.61 10.86 11.11 11.37 11.62 11.87 12.12 12.37 2.9 9.98 10.23 10.48 10.73 10.98 11.23 11.49 11.74 11.99 12.24 12.49 3.0 10.10 10.35 10.60 10.85 11.10 11.36 11.61 11.86 12.11 12.36 12.61 3.1 10.22 10.47 10.72 10.97 11.23 11.48 11.73 11.98 12.23 12.48 12.74 3.2 10.34 10.59 10.84 11.09 11.35 11.60 11.85 12.10 12.35 12.61 12.86 3.3 10.46 10.71 10.96 11.22 11.47 11.72 11.97 12.22 12.48 12.73 12.98 3.4 10.58 10.83 11.09 11.34 11.59 11.84 12.09 12.34 12.60 12.85 13.10 3.5 10.70 10.95 11.21 11.46 11.71 11.96 12.21 12.46 12.72 12.97 13.22 3.6 10.82 11.08 11.33 11.58 11.83 12.08 12.33 12.58 12.84 13.09 13.34 3.7 10.94 11.20 11.45 11.70 11.95 12.20 12.45 12.70 12.96 13.21 13.46 3.8 11.06 11.32 11.57 11.82 12.07 12.32 12.57 12.82 13.08 13.33 13.58 3.9 11.18 11.44 11.69 11.94 12.19 12.44 12.69 12.94 13.20 13.45 13.70 4.0 11.30 11.56 11.81 12.06 12.31 12.56 12.81 13.06 13.32 13.57 13.83 4.1 11.42 11.68 11.93 12.18 12.43 12.68 12.93 13.18 13.44 13.69 13.95 4.2 11.54 11.80 12.05 12.30 12.55 12.80 13.05 13.31 13.56 13.82 14.07 4.3 11.66 11.92 12.17 12.42 12.67 12.92 13.18 13.43 13.68 13.94 14.19 4.4 11.78 12.04 12.29 12.54 12.79 13.04 13.30 13.55 13.80 14.06 14.31 4.5 11.90 12.16 12.41 12.66 12.91 13.16 13.42 13.67 13.92 14.18 14.43 4.6 12.03 12.28 12.53 12.78 13.03 13.28 13.54 13.79 14.04 14.30 14.55 4.7 12.15 12.40 12.65 12.90 13.15 13.40 13.66 13.91 14.16 14.42 14.67 4.8 12.27 12.52 12.77 13.02 13.27 13.52 13.78 14.03 14.28 14.54 14.79 4.9 12.39 12.64 12.89 13.14 13.39 13.64 13.90 14.15 14.40 14.66 14.91 610 TESTING FOR BUTTERFAT Table 103. — Continued. Quevenne Lactometer Reading at 60° F. Fat 26 27 28 29 30 31 32 33 34 35 36 per Total Total Total Total Total Total Total Total Total Total Total' cent solids solids solids solids solids solids solids solids solids solids solids per per per per per per per per per per per cent cent cent cent cent cent cent cent cent cent cent 5.0 12.51 12.76 13.01 13.26 13.51 13.76 14.02 14.27 14.52 14.78 15.03 5.1 12.63 12.88 13.13 13.38 13.63 13.89 14.14 14.39 14.64 14.90 15.15 5.2 12.75 13.00 13.25 13.50 13.75 14.01 14.26 14.51 14.76 15.02 15.27 5.3 12.87 13.12 13.37 13.62 13.87 14.13 14.38 14.63 14.88 15.14 15.39 5.4 12.99 13.24 13.49 13.74 14.00 14.25 14.50 14.76 15.01 15.26 15.51 5.5 13.11 13.36 13.61 13.86 14.12 14.37 14.62 14.88 15.13 15.38 15.63 5.6 13.23 13.48 13.73 13.99 14.24 14.49 14.75 15.00 15.25 15.50 15.75 5.7 13.35 13.60 13.85 14.11 14.36 14.61 14.87 15.12 15.37 15.62 15.87 5.8 13.47 13.72 13.97 14.23 14.48 14.74 14.99 15.24 15.49 15.74 15.99 5.9 13.59 13.84 14.10 14.35 14.60 14.86 15.11 15.36 15.61 15.86 16.12 6.0 13.71 13.96 14.22 14.47 14.72 14.98 15.23 15.48 15.73 15.98 16.24 6.1 13.83 14.08 14.34 14.59 14.84 15.10 15.35 15.60 15.85 16.10 16.35 6.2 13.95 14.20 14.46 14.71 14.96 15.22 15.47 15.72 15.97 16.22 16.48 6.3 14.07 14.32 14.58 14.83 15.08 15.34 15.59 15.84 16.09 16.34 16.60 6.4 14.19 14.44 14.70 14.96 15.20 15.46 15.71 15.96 16.21 16.46 16.72 6.5 14.31 14.56 14.82 15.08 15.32 15.58 15.83 16.08 16.33 16.58 16.84 6.6 14.43 14.68 14.94 15.20 15.44 15.70 15.95 16.20 16.45 16.70 16.96 6.7 14.55 14.80 15.06 15.32 15.56 15.82 16.07 16.32 16.57 16.82 17.08 6.8 14.67 14.92 15.18 15.44 15.68 15.94 16.19 16.44 16.69 16.94 17.20 6.9 14.79 15.04 15.30 15.56 15.80 16.06 16.31 16.56 16.81 17.06 17.32 TESTING MILK, CREAM, SKIM MILK AND BUTTER- MILK FOR BUTTERFAT Volumetric Methods The Babcock Test Principle of Babcock Test. — The principle of the Babcock test is based on the fact that when sulphuric acid in sufficient strength and amount is added to milk, cream or other dairy product, the acid breaks down the non-fatty constituents without materially affecting the fat. The action of the acid, together with the heat generated, destroys the emulsion of fat-in-milk serum, causing the fat to sep- arate out. The completeness of this separation is facilitated by sub- jecting the mixture of acid and milk to centrifugal force. In order to make possible the ready measurement of this prac- tically pure, separated fat in terms of per cent, the neck of the test bottle, in which the fat appears in the finished test, is graduated. Each one per cent graduation has a capacity of .2 cubic centimeter. The specific gravity of butterfat at about 135 degrees F., which is the temperature at which the test is read, averages .9. The .2 cubic centimeter of butterfat therefore weighs .2 X .9 = .18 grams. In TKSTING FOR BUTTERFAT 611 order to have .18 grams butterfat represent 1 per cent of the milk or cream tested, .18 X 100 or 18 grams of milk or cream must be used. In the case of milk, the sample, for convenience's sake, is measured, instead of weighed into the test bottle. The average specific gravity of milk is 1.032. Hence 18 grams of milk have a 1 8 volume of y-?)T2 or ^>44 cubic centimeters. But when milk is poured from the pipette, approximately .15 c.c. remain in the pipette and fail to be discharged into the test bottle. For this reason a poured from the pipette, approximately .15 c.c. remain in the pipette delivers 18 grams of milk. In the case of cream, the specific gravity varies very greatly with the richness of the cream and the amount of foam it contains, hence the measuring of the cream into the test bottle introduces considerable error. For this reason the cream is weighed, and not measured, into the test bottle, using 18 grams. In the course of the development of the Babcock test for cream, it was found desirable to reduce the charge of cream used for the test from 18 grams to 9 grams, and accordingly the percentage graduation in these cream test bottles was modified to the effect that each 1 per cent of the graduation has a capacity of .1 cubic centimeter which corresponds to .09 grams of butterfat. In the use of these so-called 9 gram cream test bottles, therefore, .09 X 100, or 9 grams of cream are weighed into the test bottle and the graduation again represents per cent. SPECIFICATIONS FOR STANDARD APPARATUS AND CHEMICALS FOR TESTING MILK AND CREAM FOR BUTTERFAT BY THE BABCOCK TEST1 1. Apparatus and Chemicals. Milk Test Bottle. — 8 per cent 18 gram milk test bottle, gradu- ated to 0.1 per cent. Graduation — The total per cent graduation shall be 8. The graduated portion of the neck shall have a length of not less than 63.5 mm. (2y2 inches). The graduation shall repre- sent whole per cent, five-tenths per cent and tenths per cent. The tenths per cent graduations shall not be less than 3 mm. in length ; the five-tenths per cent graduations shall be 1 mm. longer than the 1 Hunziker, Journal of Dairy Science, Vol. I, No. 1, May, 1917. 612 TESTING FOR BUTTERFAT tenths per cent graduations, projecting 1 mm. to the left ; the whole per cent graduation shall extend at least one-half way around the neck to the right and projecting 2 mm. to the left of the tenths per cent graduations. Each per cent graduation shall be numbered, the number being placed on the left of the scale. The maximum error in the total graduation or in any part there- of shall not exceed the volume of the smallest unit of the graduation. Neck. — The neck shall be cylindrical and of uniform internal diameter throughout. The cylindrical part of the neck shall extend at least 5 mm. below the lowest and above the highest graduation mark. The top of the neck shall be flared to a diameter of not less than 10 mm. Bulb. — The capacity of the bulb up to the junction of the neck shall be not less than 45 cc. The shape of the bulb may be either cylindrical or conical with the smallest diameter at the bottom. If cylindrical, the outside diameter shall be between 34 and 36 mm. ; if conical, the outside diameter of the base shall be between 31 and 33 mm., and the maximum diameter between 35 and 37 mm. The charge of the bottle shall be 18 grams. The total height of the bottle shall be between 150 and 165 mm. and 6j^ inches). Cream Test Bottle 1. — 50 per cent 9 gram short-neck cream test bottle, graduated to 0.5 per cent. Graduation — the total per cent graduation shall be 50. The graduated portion of the neck shall have a length of not less than 63.5 mm. (2T/2 inches). The gradu- ation shall represent 5 per cent, 1 per cent, and 0.5 per cent. The 5 per cent graduations shall extend at least half-way around the neck (to the right). The 0.5 per cent graduations shall be at least 3 mm. in length, and the 1 per cent graduations shall have a length intermediate between the 5 per cent and the 0.5 per cent graduations. Each 5 per cent graduation shall be numbered, the number being placed on the left of the scale. The maximum error in the total graduation or in any part thereof shall not exceed the volume of the smallest unit of the graduation. Neck. — The neck shall be cylindrical and of uniform internal diameter throughout. The cylindrical part of the neck shall extend TESTING FOR BUTT.SRFAT 613 at least 5 mm. below the lowest and above the highest graduation mark. The top of the neck shall be flared to a diameter of not less than 10 mm. Bulb. — The capacity of the bulb up to the junction of the neck shall not be less than 45 cc. The shape of the bulb may be either cylindrical or conical with the smallest diameter at the bottom. If cylindrical, the outside diameter shall be between 34 and 36 mm. ; if conical, the outside diameter of the base shall be between 31 and 33 mm. and the maximum diameter between 35 and 37 mm. The charge of the bottle shall be 9 grams. All bottles shall bear on top of the neck above the graduations, in plainly legible characters, a mark defining the weight of the charge to be used (9 grams). The total height of the bottle shall be between 150 and 165 mm. (5% and 6l/2 inches), same as standard milk test bottles. Cream Test Bottle 2. — 50 per cent 9 gram long-neck-cream test bottle, graduated to 0.5 per cent. The same specifications in every detail -as specified for the 50 per cent 9 gram short-neck bottle shall apply for the long-neck bottle with the exception, however, that the total height of this bottle shall be between 210 and 235 mm. (8% and 9 inches), that the total length of the graduation shall be not less than 120 mm., and that the maximum error in the total gradua- tion or in any part thereof shall not exceed 50 per cent of the volume of the smallest unit of the graduation. Cream Test Bottle 3. — 50 per cent 18 gram long-neck cream test bottle, graduated to 0.5 per cent. The same specifications in every detail as specified for the 50 per cent 9 gram long-neck bottle shall also apply for the 18 gram long-neck bottle, except that the charge of the bottle shall be 18 grams. All bottles shall bear on top of the neck above the graduation, in plainly legible characters, a mark defining the weight of the charge to be used (18 grams). Pipette, capacity 17.6 cc. Total length of pipette not more than 330 mm. (13J4 inches). Outside diameter of suction tube 6 to 8 mm. Length of suction tube, 130 mm. Outside diameter of deliv- ery tube, 4.5 to 5.5 mm. Length of delivery tube, 100 to 120 mm. Distance of graduation mark above bulb, 15 to 45 mm. Nozzle straight. To deliver its contents when filled to the mark with water at 20° C., in five to eight seconds. The maximum error shall not exceed 0.05 cc. Acid measure, capacity 17.5 cc. 614 TESTING FOR BUTTERFAT Cream Testing Scales. — Sensibility reciprocal of 30 mgm., i. e.» the addition of 30 mgm. to the scales, when loaded to capacity, shall cause a deflection of the pointer of at least one division on the gradu- ation. Weights. — 9 gram weights for 9 gram cream test bottles and 18 gram weights for 18 gram cream test bottles, preferably stamped correct by the United States or State Bureau of Stand- ards. Tester. — Standard Babcock test centrifuge and speed in- dicator. Dividers for measuring fat column. Water bath for cream samples, with proper arrangement for regulating and recording temperature of samples. Water bath for test bottles, of sufficient size and with neces- sary equipment to insure proper control of temperature. The fol- lowing dimensions for a twenty-four bottle water bath are recom- mended: Metal box, 14 inches long, 11 inches wide, and S1/^ inches deep and equipped with a bottle basket 9l/2 inches long and 6l/2 inches wide, capacity twenty-four bottles, a steam and water inlet, a drain, a thermometer holder with thermometer. Chemicals. — Commercial sulphuric acid, specific gravity 1.82 to 1.83 ; glymol, or white mineral oil, high grade. OPERATION OF THE BABCOCK TEST Milk Test Milk Samples. — The sampling of milk is fully discussed in Chapter VI on "Receiving Milk and Cream." Preparation of Milk Sample for the Test. — Before testing, the samples should be brought to the proper temperature; this may range from 55 degrees to 70 degrees F. If the samples have been exposed to summer heat or to temperatures near the freezing point, the sample bottles are best set into a tank, sink, or tub and allowed to stand in water at about 60 degrees F. until the temperature of the milk is neither below 55 degrees F. nor above 70 degrees F. If to be transported by mail, express, or otherwise, the sample bottle should be completely full and tightly stoppered and the sam- ples should be preserved as previously directed, see Chapter VI. The contents of each bottle must be thoroughly mixed before TESTING FOR BUTTERFAT 615 pipetting into the test bottle. If the composite sample has received the proper care, as directed in Chapter VI, the gentle shaking of the sample bottle and the pouring of the contents from one bottle to another several times should be sufficient. I--""-"-.-: "-""_-- -' Fig-. 88 Pig-. 89 Fig-. 90 Fig-. 91 Standard Babcock Milk and Cream Test Bottles Courtesy Louis F. Nafis Samples containing lumps of cream or granules of butter cannot be tested properly without extra preparation. They should be heated to at least 110 degrees F., or until all lumps of butterfat have melted and disappeared ; they should then be shaken vigorously and pipetted into the test bottle at once. Even with this precaution it is difficult to transfer to the test bottle a representative portion 616 TESTING FOR BUTTERFAT from such a sample. Avoid incorporation of air bubbles while mixing the sample. Curdy and churned samples are not dependable. Sour and curdy samples should be treated as follows: add one-half teaspoonful of soda lye or potash lye, shake, and let stand until all lumps of curd have disappeared. The sample is then ready for the test. When testing samples to which soda lye or other alkali has been added, the acid should be added slowly and carefully to avoid accidents and to prevent the loss of a portion of the contents of the bottle by exces- sive effervescence. Measuring the Milk Into the Test Bottle. — Use standard milk test bottles and a standard 17.6 cubic centimeter pipette. Measure 17.6 cubic centimeters (representing 18 grams) of the properly prepared sample into the test bottle. In order to do this rapidly, and without spilling, the delivery tube of the standard pipette has been constructed of such diameter, that this tube readily drops into the neck of the standard "8 per cent milk test bottle. Hence drop the delivery tube of the pipette into the neck of the test bottle until the bulb of the pipette rests on the neck of the bottle, then release the milk. Blow the last drop of milk out of the pipette before removing it from the bottle. Mark each bottle with a number corresponding with the number of the respective patron on the sample bottle. The marking is best done with an ordinary lead pencil on the etched shoulder of the test bot- tle^ Or equip the test bottles with metal tags which bear consecu- tive numbers. Slip one tag over the neck of each test bottle. In this case the test bottle number may and usually does differ from the patron's number shown on the sample bottle. It is necessary therefore, to record the test bottle number on the test report blank opposite the respective patron's name or number at the time of rill- ing each test bottle. Adding the Acid. — Use commercial sulphuric acid, specific gravity 1.82 to 1.83. The temperature of the acid should be the same as that of the milk, 55 degrees F. to 70 degrees F. In order to insure the proper temperature of the acid it is advisable to set the acid bottle into the tank containing the milk sample bottles. Add 17.5 cc. of acid to the milk in the test bottle and mix by giving the bottle a rotary motion until the lumps of curd are com- pletely dissolved and the mixture presents a brown-black color. It TESTING FOR BUTTERFAT 617 is advisable to add the acid in about three installments, shaking the bottle after each addition. Attention to this precaution helps to secure clear tests. WhirEng and Adding Water.— Set the test bottles into the Babcock centrifuge. If the test bottles containing the mixture of milk and acid are held over and allowed to become cool, they should be heated by setting in hot water before whirling. Steam turbine and electric driven testers with not less than twenty-four pockets are best adapted for factory use. They are constructed of two general sizes, — those having a twelve-inch diame- ter wheel and those having an eighteen-inch diameter wheel. Table 104. — Correct Speed of Testers of Different Diameters1 Measuring from Pocket Bottom to Opposite Pocket Bottom Diameter of Wheel Revolutions of. Wheel Inches per Minute 10 1,074 12 980 14 909 16 848 18 800 20 759 22 724 24 693 Fill the bottles to the bottom of the neck with hot, soft water; whirl again for two minutes and fill the bottles with hot, soft water to about the 7 per cent mark ; whirl for one minute. The tempera- ture of the water added should be not lower than 140 degrees F. and preferably near that of boiling water (212 degrees F). Reading the Test. — Place the test bottles in a water bath and read after a temperature of 130° F. to 140° F. has been maintained for not less than three minutes. Measure the fat column with a pair of dividers, including the meniscus or curve, both at the bottom and at the top of the fat column. Each subdivision represents .1 per cent ; each main division represents 1 per cent. Record the per- centage of fat thus found on the test sheet. Abnormal Appearance of the Fat Column. — When the test is made properly and in accordance with above directions, the fat Farrington & Woll, Testing Milk and Its Products. 618 TESTING FOR BUTTDRFAT column is clear, translucent, has a golden yellow or amber color and the top and bottom curves are sharply denned. The presence of whitish curd in or immediately below the fat column is the result of excessively cold milk and acid, or the use of too little or too weak acid. The presence of charred matter in the fat column is the result of the use of too much or too strong acid, or too high a temperature of milk or acid, or both, at the time of adding the acid. The appearance of foam on the surface of the fat column is caused by the use of hard water. The carbonates, when acted on by the sulphuric acid, break down, liberating carbon dioxide gas which, rising through the fat column, gathers on its surface in the form of air bubbles. Where soft water, distilled water, or rain water is not available, the water may be softened by boiling it or by the addition to it of a few drops of sulphuric acid before use. All tests which are milky, or foggy, showing the presence of curd or charred matter in or below the fat column, or of which the reading is indistinct or uncertain, should be rejected. Duplicate tests are essential in all work where special accuracy of results is required, such as in official testing and experimental investigations. Cream Test Cream samples. — The taking of cream samples, at the factory, at the cream station and on the cream route is fully discussed in Chapter VI on "Receiving Milk and Cream." Cream samples should be tested as soon as possible and not later than three days after they are taken. Composite samples rep- resenting portions of consecutive deliveries of the same patron are prone to be unreliable. Samples should at all times be kept in non-absorptive containers, sealed air-tight and held in the cold. Immediately before testing, mix the sample until it pours readily and a uniform emulsion is secured. If in good condition shake, pour, stir or blow until properly mixed. If very thick, warm to 85 degrees F. and then mix. In case of lumps of butter, heat the sample to from 100 degrees F. to 120 degrees F. by setting in water bath, mix thoroughly and weigh out at once. For commercial work on a large scale it is advisable to temper all samples to 100 degrees to 120 degrees F. in a water bath previous to mixing. Great care should be exercised to avoid overheating the sample, causing the TESTING FOR BUTTERFAT 619 Fig*. 93. Acid Dipper for Cream Pig*. 94 Cream Pipette '- Lg*. 92 Standard Milk Pipette Pig1. 95 Combined Acid Bottle - Tig. 96 Acid Cylinder 1 Courtesy Louis F. Naf.s. 2 Courtesy Mojonnier Bros. Co. 620 TESTING #OR .-*.*- • creanl to "oil off." This precaution is especially necessary with thin cream. Cream Test Bottles. — Use standard 50 per cent 9-gram short- neck, or standard 50 per cent 9-gram long-neck, or standard 50 per cent 18-gram long-neck cream test bottles. The divisions on each of the three standard cream test bottles represent .5 per cent, 1 per cent and 5 per cent. The 5 per cent divisions bear a figure to the left of the graduation. Cream Test Balances. — Only high-class balances which are in satisfactory operating condition should be used. The reliability of the cream test balance depends in the first place on its sensitiveness and capacity. Experiments conducted with different types of cream testing scales by Hunziker, Spitzer and Ogle1 showed the following results and conclusions : 1. Results of tests of 4623 cream samples made in commercial creameries show that where the one-bottle balances were used, 96.43 per cent of the tests checked with the retests within .5 per cent, while the best performance of the twelve-bottle balance yielded only 80.43 per cent of tests that checked with the retests. 2. Balances with a sensibility reciprocal of .01 to .03 grams produced tests, 98.2 per cent of which checked with the retests, and the average variation between duplicate tests was .119 per cent. 3. Balances with a sensibility reciprocal of .1 gram yielded only 36.1 per cent of tests which checked with the retests, and the average variation between duplicate tests was .993 per cent. 4. The condition, care and manipulation of the cream test bal- ance greatly influence its sensitiveness, reliability and length of use- fulness. 5. The general adoption of standard cream test balances with a sensibility reciprocal of thirty milligrams would materially augment the reliability of cream tests. 6. Preference should be given to small capacity balances. 7. Balances, with a graduated beam which carries a traveling poise are less reliable than those with a beam of equal arms, balanc- ing in the center and requiring the use of separate weights. 8. Balances of simple principle and construction are generally superior under average commercial conditions, retain their sensi- bility reciprocal longer and are more durable than balances of more complex principle and construction. 1 Hunziker, Spitzer and Ogle, Cream Testing Scales, Purdue Bulletin 189, 1916. TESTING FOR BUTTERFAT 621 SPECIFICATIONS AND TOLERANCES FOR STANDARD CREAM TEST BALANCES UNITED STATES BUREAU OF STANDARDS1 Definition. — A cream-test or butterfat-test scale is a scale especially designed and adapted for determining the fat content of cream or butter. Specifications. — 1. All scales shall be provided with a gradu- ated scale or arc divided into at least 10 equal spaces, over which the indicator shall play. 2. The clear interval between the graduations on the graduated scale or arc shall not be less than 0.05 inch. 3. The indicator shall be of such length as to reach to the gradu- ated divisions and shall terminate in a fine point to enable the read- ings to be made with precision. 4. All scales whose weight indications are changed by an amount greater than one-half the tolerance allowed, when set in any position on a surface making an angle of 5 per cent or approximately j degrees with the horizontal, shall be equipped with leveling screws and with a device which will indicate when the scale is level. The scale shall be rebalanced at zero each time its position is altered dur- ing this test. 5. All scales shall be so constructed and adjusted that when the pans are released or disturbed, the pointer will return to its orig- inal position of equilibrium. Sensibility Reciprocal. — The maximum sensibility reciprocal allowable for these scales shall not exceed one-half grain, or approxi- mately 30 milligrams, when the maximum load is placed upon the scale. (The term "sensibility reciprocal" means the weight required to move the position of equilibrium of the beam, pan, pointer, or other indicating device of the scale a definite amount. In scales provided with a pointer and a graduated scale or arc, such as the above, the sensibility reciprocal is the weight required to cause a change in the position of rest of the pointer equal to one division on the graduated scale or arc.) Tolerances. — The tolerance to be allowed in excess or de- ficiency on all cream-test and butterfat-test scales shall not be 1 United States Bureau of Standards, Tolerances and Specifications for Weights and Measures, Proceedings of Tenth Annual Conference on the Weights and Measures of the United States, May 25-28, 1915. 622 TESTING FOR BUTTER? AT greater than one-half grain or approximately 30 milligrams, when the scale is loaded to capacity." Manipulation of Balance. — .1. Level the balance each time be- fore using. 2. Adjust or balance the instrument immediately before weigh- ing and make sure that its beam swings freely and does not "stick." 3. Protect the balance from air currents. If resting on an open bench have the nearest doors and windows closed. The setting of the balance in a box large enough for convenient operation and with the near side open is recommended. 4. Use accurate weights only and be sure that they are clean. 5. Don't release the balance with a jerk so that the pans strike the rest ; release them easily and slowly and handle them gently when they are moved. Careless and rough handling may damage spring bands and dull knife edges. 6. Don't try to use the balance when out of repair. 7. Use painstaking care and reasonable judgment in all opera- tions. SPECIFICATIONS FOR STANDARD NINE AND EIGHTEEN GRAM WEIGHTS 1. Weights shall be made of brass or aluminum. 2. Weights shall have smooth surfaces and no sharp points or corners. 3. Weights shall not be covered with a soft or thick coat of paint or varnish. 4. All weights shall be clearly marked with their nominal value i. e. 9 for nine gram weights and 18 for eighteen gram weights. 5. The tolerance shall be forty milligrams for nine gram weights and fifty milligrams for eighteen gram weights. • Weighing the Cream Into the Test Bottle. — The cream must be weighed into the test bottle, not measured. This is necessary in order to secure the correct amount by weight. Cream varies in weight with its richness and its mechanical condition, and no one measure will hold the correct amount of cream of varying richness. The correct amount of cream by weight is 9 grams or 18 grams, respectively. Set the cream test bottles on the scales and balance the scales accurately. The cream is most readily transferred into the test TESTING FOR BUTTERFAT 623 bottles from the properly mixed sample by means of a 9 or 18 cc. pipette which has a short, wide-bore delivery tube. In this manner spilling is readily avoided and the work is most rapid. If any cream is spilled over the outside of the bottles or on the balance, it should be wiped off immediately and before the weighing is com- pleted. Making the Test. — Three methods of performing the test have been adopted as standard methods; each of which, when properly executed, insures accurate results, but methods II and III are pre- Fig\ 97. Jalco Electric Centrifuge Tig. 98. Facile Steam Turbine Courtesy Jalco Motor Co. Tester Courtesy D. H. Burrell & Co. ferred to method I, as they leave less to the judgment of the oper- ator and therefore are more nearly "fool-proof :" Method I. Add standard commercial sulphuric acid until the mixture of acid and cream, immediately after shaking, resembles in color, coffee with cream in it. Usually about 8 to 12 cc. of acid is required in the case of the 9-gram bottle or 14 to 17 cc. of acid in the case of the 18-gram bottle, the amount needed depend- ing on the temperature of acid and cream and on the richness of the cream. Whirl in Standard Babcock centrifuge at proper speed, five, two and one minutes, respectively, filling the bottles with hot, soft water, temperature 140° F. or above, to the bottom of the neck after the first whirling and to near the top graduation after the second whirling. 624 TESTING FOR BUTTERFAT Method II. Add 9 cc. of water after the cream has been weighed into the test bottle and before the acid is added, then add 17.5 cc. acid and proceed as in previous method. This method is applicable with the 9-gram bottle only. Method III. Add 8 to 12 cc. of acid in the case of the 9-gram bottle or 14 to 17 cc. of acid in the case of the 18-gram bottle, or add acid until the mixture of cream and acid, after shaking, has a choco- late brown color. After the cream and acid have been thoroughly mixed and all lumps have completely disappeared, add a few cubic centimeters (not less than 5 c.c.) of hot, soft water, whirl five min- utes, add hot, soft water to near top of scale and whirl one minute. The proper speed of the centrifuge is 800 revolutions per min- Figf. 99. Babcock Tester Courtesy Davis-Watkins Dairymen's Mfg. Co. ute for an 18-inch diameter wheel and 1000 revolutions per minute for a 12-inch diameter wheel. Reading the Cream Test. — Place the test bottles into the water bath and read after a temperature of 130 to 140 degrees F. has been maintained for not less than three minutes. Just before reading the test and when taking the bottles from the water bath, add a few drops of glymol. The glymol removes the meniscus or curve on top of the fat column, leaving a straight line which is sharply defined and readily seen. Measure the fat column, preferably using dividers, and record the percentage of fat on the test sheet, opposite the test bottle num- ber of the respective patron. TESTING FOR BUTTSRFAT 625 Purpose and Use of Glymol. — Glymol is a high quality of white mineral oil, similar to typewriter oil. It is slightly lighter than butterfat and therefore floats on top of the fat column. The object of using glymol is to remove the meniscus or curve present at the top of the fat column. This curve, owing to refrac- tion of the light, is indistinct and renders correct reading difficult. When a few drops of glymol are placed on top of the fat column, the meniscus disappears and a straight, sharply defined line is formed Fig-. 100. Beading1 Cream Test between the top of the fat and the bottom of the glymol. In this condition the test can be read easily and accurately. For the best results the glymol should be added immediately before reading. The glymol may be conveniently transferred to the test bottle from a pipette, burette, or by squirting from a small oil can. 626 TESTING FOR BUTTERFAT Experienced testers are able to secure correct readings without glymol by reading to the bottom of the upper meniscus, but the use of glymol is urged for maximum accuracy. Glymol should be used in the reading of the cream test only; the milk test should be read without glymol, otherwise the results of the milk tests would be too low. Experimental results by Hun- ziker1 have indicated that in the milk test the meniscus compensates for the loss of residual fat. It therefore must be included in the reading. In the cream test the proportion of residual fat lost is very small and is amply compensated for by the usual impurities in the fat column. Coloring Glymol. — Some operators prefer the use of colored glymol, though equally satisfactory results are obtained with the un- colored glymol. Glymol is best colored with an aniline dye. A dye that is sold under the trade name "oil red" proves highly satisfactory for this purpose. Add 1 gram of oil red to 4 gallons glymol. Abnormal Appearance of Fat Column. — When the cream test has been properly performed the fat column in the neck of the bottle is clear, translucent and free from milky, curdy and charred matter in or below the fat. Any tests in which the fat column is not free from visible impurities, or in which the fat column rests on a layer of non-fatty material, or of which the reading is otherwise indistinct or uncertain, should be rejected. See also abnormal appearance of fat column of milk tests. Testing Skim Milk, Buttermilk and Whey for Butterfat Test Bottles. — For the Babcock test of skim milk, buttermilk and whey use bottles with double necks, which are especially con- structed for this purpose. The graduation of these bottles varies somewhat with the make of bottle. In some bottles the total gradua- tion is .25 per cent and the subdivisions represent .01 per cent. In others the total graduation is .5 per cent and the subdivisions repre- sent .05 per cent. Making the Test. — Measure the properly mixed skim milk into the test bottles with the 17.6 cc. pipette used for milk testing. Add 20 cc. of sulphuric acid. For best results add the acid in several installments and shake until all the lumps of curd have completely disappeared. Whirl in tester for 10 minutes. 1 Hunziker, Indiana Agricultural Experiment Station Annual Report, 1914. TESTING FOR BUTTDRFAT 627 Special attention should be given when the bottles are placed into the tester. Test bottles in which the lower end of the funnel- neck extends perpendicularly along the side of the bulb to the bot- tom of the bottle, should be so placed that the funnel-neck faces the center of the tester, otherwise the fat rises into the funnel-neck. Test bottles in which the lower end of the funnel-neck extends diagonally to the bottom of the bottle should be so placed that the graduated neck faces the center of the tester. This will prevent excessive breakage of this type of bottles. The tester should run perfectly smooth in order to prevent excessive breakage, as these bottles are of very delicate construction. Add distilled water or rain water at a temperature of 140° F. or over to the bottom of the neck of the boftle; whirl 5 minutes! Add hot water to near top of neck, whirl 10 minutes and read. In the case of buttermilk and whey use the same method as described for skim milk. In the case of buttermilk, especially that derived from pasteurized sour cream, the buttermilk should be stirred very thoroughly before sampling. This is necessary, because upon standing the curd precipitates out and settles to the bottom very rapidly, and it is the curd that holds the bulk of the fat con- tained in the buttermilk. The amount of fat contained in skim milk, buttermilk and whey, particularly in the first two liquids, is, or should be, so minute, the fat globules are so small and the construction of the test bottle is so crude, that it is difficult to secure very accurate tests by this method, the proportion of fat actually shown in the test often repre- senting only a very small part of the total fat content of the orig- inal sample. The results of testing skim milk and buttermilk with the standard Babcock test should not be relied upon absolutely for accuracy, but if the tests are carefully made, the results may serve as a convenient guide, showing the operator whether these products contain com- paratively little or much fat. Investigations in which both Babcock tests and chemical fat estimations of skim milk and buttermilk were made, -indicate that the fat content of these products seldom drops below .1 per cent as determined by the chemical estimation. It is reasonable to assume, therefore, that when the Babcock test shows only .05 per cent fat or less, the results are considerably lower than they should be. 628 TESTING FOR BUTTERFAT Bbuska1 recommends that 1 cc. of amyl alcohol be added to the test before centrifuging in order to facilitate the separation of the fat, improve the clearness of the fat column and augment the accur- acy of the test. He found, however, that blank tests made by this method also show a layer in the neck of the test bottle, resembling butterfat, and recommends the advisability of additional experimen- tal work with the use of amyl alcohol. Pig-. 101 Skim Milk Test Bottle - Tig. 102. Wizard Steam Tester « THE GERBER TEST Fig1. 103 Calipers for Beading- - This test* was invented by Dr. N. Gerber, Zurich, Switzerland. It became available for commercial use in Europe shortly after the introduction of the Babcock test in this country and has found wide application, especially in European countries. Apparatus and Chemicals. — -1. Acido-butyrometer. This is a glass bulb, extended at its top into a closed, graduated neck. The graduations represent per cent and tenths per cent. The bottom of 1 Bouska, Report before American Association of Dairy Science, 1918. 2 Courtesy Louis F. Nafls. 8 Courtesy Creamery Package Mfg. Co. * Gerber, Die praktische Milchprufung, 7th edition, 1900. TESTING FOR BUTTERFAT 629 the bulb terminates into a threaded neck into which fits a rubber stopper. 2. Butyrometer stand and water bath. 3. 1.1 cc. pipette for milk. 4. 3 cc. pipette for cream. 5. 10 cc. pipette graduated to .l.cc. 6. 8.2 cc. pipette for diluting cream. 7. 10 cc. bulb pipette for acid, or automatic acid measuring apparatus. 8. 1 cc. pipette for amyl alcohol. 9. Centrifuge. Commercial sulphuric acid, specific gravity 1.82 to 1.825 at 15° C. (59° F.). Pure amyl alcohol, specific gravity .8165 to .818 at 15° C. (59° F.) boiling point 124-130° C., should give a clear solution with an equal volume of strong hydrochloric acid. Operation of Test Milk, Skim Milk, Buttermilk, Whey. — Place the butyrometers in rack or stand. Add 10 c.c. sulphuric acid to each, measure 11 c.c. of properly mixed sample of milk and then 1 cc.'of amyl alcohol into the butyrometers. Insert corks, place thumb over cork and shake until all the curd is dissolved. Completely invert the stand several times to insure thorough mixing. Place the butyrometers into the centrifuge with corks toward the periphery, and whirl two to three minutes, or until the fat column is perfectly clear. Place butyrometers into water bath at 60 to 70° C. (140-158° F.) and read. So adjust the rubber stopper in the bottom of the bulb while reading, that the bottom of the fat column coincides with, the zero graduation. Read to the bottom of the meniscus. Compara- tive tests have demonstrated that this test yields very accurate results. Skim milk and buttermilk should be whirled longer and at maxi- mum attainable speed and .05 per cent must be added to the reading.1 Cream. — Wyssmann and Peter2 recommend dilution of the cream at the rate of one part of cream to four parts of water, mak- 1 Richmond, Dairy Chemistry, 1914. 2Wyssman und Peter, Milchwirtschaft, 1907. 630 TESTING BUTTER ing a dilution of 1 in 5, and requiring the multiplication of the reading by five. This appears to be the most practicable method of cream testing with the Gerber test. Richmond1 recommends the use of a 3 cc. pipette for measuring the cream and the subsequent addition of 8.2 cc. water, and the reading to be interpreted into per cent by the use of a calculated table; claiming accurate results for cream testing not over 32 per cent fat. For richer cream he advises a dilution of equal parts, by weight, of cream and water and then proceeding as with cream test- ing not over 32 per cent fat. Either of the above two methods for cream testing is obviously rather unsuited for use in creameries that purchase their butterfat in the form of cream. The first is undeniably inaccurate and the second, while somewhat more accurate, is too complicated for prac- tical purposes under American conditions. BUTTER Determination of Per Cent Moisture Preparation of Sample. — Official.2 — "If large quantities of but- ter are to be sampled, use a butter trier or sampler. Melt com- pletely the portions thus drawn, 100-500 grams, in a closed vessel at as low a temperature as possible. When softened, cool and, at the same time, shake the mass violently until it is homogeneous and solidified sufficiently to prevent the separation of the water and fat. Then pour a portion into the vessel from which it is to be weighed. The sample should completely or nearly fill the vessel and should be kept in a cool place until analyzed. Moisture. — Official. — "Weigh 1.5 to 2.5 grams of the sample into a flat-bottomed dish, having a surface of at least 20 sq. cm., dry at the temperature of boiling water and weigh at hourly intervals until the weight becomes constant. The use of clean, dry sand or asbestos is admissible." For factory purposes the official method is obviously not well adapted, largely because of its time-consuming element. It is nec- essary to make moisture tests while the butter is still in the churn and here quick work, consistent with reasonable accuracy, is indis- pensable. Creameries whose motto is "Safety First" will also make 1 Richmond, Dairy Chemistry, 1914. 2 Journal of the Association of Official Agricultural Chemists, Vol. II, No. 3, Nov. 15, 1916. TESTING BUTTER 631 moisture tests of the butter in the cooler, so as to be doubly sure that no butter leaves the factory that does not comply with the Federal ruling. Factory Moisture Tests Preparation of Sample. — It is an open and disputable question as to whether the butter sample should be especially prepared, or whether a sample large enough only for immediate weighing should be used. Both methods, if properly executed, are capable of yield- ing practically equally reliable results. Fig*. 104. Aluminum Evaporating1 Dish If the sample is especially prepared, a larger sample and more portions of butter from different parts of the churning or package can be taken. This obviously has the advantage, theoretically at least, of securing a more representative sample, but this advan- tage is often offset by irregularities in the preparation of the sample and by the extra time consumed. However, when it is neces- sary to hold the sample for a considerable length of time before testing, when it is to be transported, either by mail or otherwise, when it is to be tested by more than one party, or when a composite sample is taken from more than one churning or package, special prepara- tion of the sample is indispensable. In all these cases churn samples should be taken with a dry, warm spoon or spatula from both ends and the center of the churn. Tub or box samples should be taken by boring the butter diagonally with a dry trier and removing from different parts of the trier seg- ments for the sample, with a knife or steel spatula. In the case of prints a thin cross section through the center of the entire print may be cut out for the sample. 632 TESTING BUTTER The sample jar should be tightly sealed. In order to prepare the sample the butter is allowed to soften by warming until it has a creamy consistency, in which condition it must be thoroughly shaken. If used immediately, portions of this thickly flowing butter emulsion may be weighed out without rehardening. If not used immediately the sample should be cooled and constantly vigorously shaken while cooling. Brown1 recommends the preparation of the butter sample with- out warming by inserting in the sample jar a rapidly revolving spiral wire, in a similar manner as milk shakes at the soda fountain are emulsified. Taking Samples without Subsequent Preparation. — Where the sample is to be immediately tested after it is taken, quite satis- factory results may be obtained without special preparation. In this case the following method of sampling is recommended : From Churn: Bring butter upon workers, wipe water off door frame, cut top off butter with ladle, so as to have surface smooth and solid, with knife cut three small cones of butter and place in alumi- num dish. Take second sample from the other end of the churn, and place in another aluminum dish. The sample in each aluminum dish should be large enough to weigh approximately ten (10) grams. From Cooler: Run trier diagonally through Friday box or through tub and take portions from the plug at each end and in the center. Do not shake the trier, or the butter, at any stage of the process of sampling, to remove loose moisture. This moisture be- longs to the butter. Bore at least two packages of cooler butter from each churning and make a test of each. The sample in each evaporating dish should be large enough to weigh approximately 10 grams. From Prints: Cut the print into two halves, and cut a slab about one-fourth inch thick from the fresh surface. Quarter this slab and transfer one of the quarters to the aluminum dish. Making the Moisture Test. Equipment: One steel spatula, One butter trier. Aluminum cups of medium size. One balance, sensibility reciprocal .01 gram. 1 Brown, Chemist Beatrice Creamery Co., Lincoln. Neb. TESTING BUTTER 633 One heating arrangement, consisting of an al- cohol or gas burner with tripod and small piece of fine copper wire gauze, or prefer- ably an electric plate, '., . One thermometer registering to 300° F. Weighing: Have balance properly balanced. See that it swings freely. Keep pans perfectly clean. Check balance several times during the day. Check up weights of aluminum cups weekly by re-weighing, in order to detect loss in weight. Before taring aluminum cups, wash them, dry them, and heat them. Do not use dry scouring powders for aluminum cups. If washing powder is used dissolve it first. Weigh to the third decimal point. Handle weights with forceps only and keep them clean. If they show signs of wear, have them replaced by new ones. In the case of the unprepared sample, simply weigh the butter which was transferred direct from churn or package to the tared aluminum dish and record the weight thus obtained. In the case of the prepared sample transfer a small portion, about 10 grams, of the butter in the sample jar to the tared dish, weigh and record weights. The butter is now ready for the evaporation of the mois- ture. Heating: Slowly heat over flame or on hot plate, stirring con- stantly with thermometer. When temperature has risen to 260° F. remove flame. The temperature will usually continue to rise to about 280° F. When it has dropped back to about 240° F. heat again as before. Evaporation of moisture then is complete. Weigh the aluminum cup again and calculate per cent moisture. For heating, use moderate heat. Too large a flame produces so intense a heat that the contents are liable to sputter over and also may become burnt. When using an alcohol flame, have a wire gauze or light steel plate between flame and cup. When using a gas flame, have a thin asbestos board between flame and cup. This helps to give a more uniform heat. When the heating has been done properly, the curd in the bottom of the cup should be slightly brown. A whitish yellow curd indi- cates insufficient heating, which is conducive of too low tests. A dark brown curd suggests overheating, which usually causes too high tests. 634 TESTING BUTTER When done using the thermometer, scrape it off on one side of cup, but do not wipe it off, so as to avoid removing fat from the test, and getting the next test too high. Second Weighing: Weigh cup again and calculate the per cent moisture by deducting the second weighing from the first weigh- ing, dividing the difference by the net weight of the sample (first weighing) and multiplying the result by 100. Example : Butter plus cup 23.463 Cup 12.863 Net weight of butter. . 10.600 First weighing 23.463 Second weighing 21.784 Net loss in weight 1.679 "ffol X 100=rl5-8% moisture. Determination of Per Cent Fat in Butter Volumetric Methods The Volumetric methods of testing butter for fat, which have been devised, are all modifications of the Babcock test. The modi- fications refer almost exclusively to such changes in the type and graduation of the Babcock test bottle as to make the bottle applica- ble for the butter test. In these methods the butter is weighed into the butter test bottle and the per cent fat is read off the graduation on the neck of the bottle. The testing of butter by these methods cannot as yet be consid- ered a complete success and the results have not as a whole been entirely reliable. The chief obstacles with which the operator is confronted in his efforts to determine the per cent of fat in butter by the modified Babcock test are : 1. The reaction of the sulphuric acid used in the test with the salt contained in the butter. The reaction generates hydrochloric acid gas which tends to char the fat and the escape of which causes violent foaming to the extent of forcing a portion of the contents out of the bottle. The danger of charring the fat has been largely overcome by adding water before the addition of the acid and by filling the TESTING BUTTER 635 bottle to the bottom of the neck with water, immediately after the acid has been added and mixed. The danger of violent foaming and expulsion of a portion of the sample is minimized materially, if not entirely prevented, by adding the acid very slowly, in numerous installments and mix- ing thoroughly after each addition. 2. The experimental error in a product containing so high a percentage of the ingredient to be determined as is the case with fat in butter (butter contains 80 or more per cent fat) is naturally proportionally great, and the causes which introduce the experimen- tal error are fixed and cannot be removed. Thus, in estimating fat by volume, it must be assumed that the butterfat has a definite spe- cific gravity, that is, that a given weight occupies a definite volume. This is not the case. Butterfat represents a compound of several fats, varying widely in specific gravity and the proportion in which these different fats are present in the mixed butterfat varies consid- erably with breed, period of lactation and feed, as determined by locality and season of the year. While the variations in the specific gravity of the mixed butterfat are not large, yet, with butter con- taining 80 per cent fat or over, they do affect the volume of the fat column and therefore the accuracy of the reading. This one factor is entirely beyond the control of the operator. Again, the temperature of the fat column when read is another factor introducing experimental error. By the intelligent use of the water bath, the temperature can be controlled within reasonable limits, thus minimizing the effect of this interfering factor to a con- siderable extent. The modified Babcock tests for butter which have been devised are those in the operation of which the Hepburn bottle, the Wagner bottle and the Wright bottle are used. They are briefly described in the following paragraphs. Hepburn1 Test Bottles. Two types of bottles have been designed by Hepburn, namely, the 9 inch, 9 gram, 90 per cent bottle, and the 6 inch, 6 gram, 90 per cent bottle. The 9 inch, 9 gram, 90 per cent bottle. — The graduated por- tion has a capacity of 90 per cent of the sample tested. 90 per 1 Hepburn, A Modified Babcock Method for Determining Fat in Butter. Thesis for Degree of Ph.D., Cornell, 1918. 636 TESTING BUTTER cent of 9 grams is 8.1 grams. Since the specific gravity of butterfat, under test conditions, averages approximately .9, the 8.1 grams of 8 1 butterfat occupy a space of -5- or 9 cc. The volume of the neck, from 0 to 90, therefore, must occupy exactly 9 cc. This volume calls for a test bottle of the following dimensions : Height over all, approximately 8.8 inches. Length of graduated portion of neck, Tig. 105 Pig-. 106 Hepburn Butter Test Bottles Courtesy Louis F. Nans 139 mm. Diameter of graduated portion of neck, 9.07 mm. The graduated portion of neck is divided into 90 divisions. This bottle is applicable for a Babcock centrifuge with a wheel diameter of 18 inches or more. TESTING BUTTER 637 The 6 inch, 6 gram, 90 per cent bottle. — The graduated portion, of the bottle has a capacity of 90 per cent of the sample tested. 90. per cent of 6 grams = 5.4 grams. Since the specific gravity of butterfat, under test conditions, averages approximately .9, the 5.4 5 4 grams of butterfat occupy a space of ~ or 6 cc. The volume of the neck of the test bottle, from 0 to 90, therefore, must be exactly 6 cc. This volume calls for a type of "bottle with the following dimensions : Height over all, approximately 6.5 inches. Length of graduated portion of neck, 93.5 mm. Diameter of graduated por- tion of neck, 9.04 mm. The graduation from 0 to 90 is divided into 90 divisions. This bottle is adapted for Babcock testers with a diameter of less than 18 inches. Scales, sensibility reciprocal .01 grams. Chemicals, commercial sulphuric acid, specific gravity 1.82 to 1.83. Glymol, or high grade white mineral oil. Operation of Test with 9 inch, 9 gram, 90 per cent bottle.—- Transfer, preferably by pouring, 9 grams of the properly prepared, thickly fluid sample of butter into the test bottle previously balanced on the scales. Add 9 cc. of lukewarm water and then 17.5 cc. com- mercial sulphuric acid. Add the acid carefully, in small portions, mixing thoroughly after each addition, until all of the 17.5 cc. has been added. This precaution is necessary in order to avoid exces- sive foaming and loss of sample due to action between acid and salt in the butter. After the contents of the bottle have been thoroughly mixed, add a sufficient amount of water to fill the bottle to the base of the neck. Centrifuge in Babcock tester for five minutes at the usual speed for the same size tester as used for milk and cream. See Table 104. Add hot water to near the top of the graduation and whirl for four min- utes. Transfer bottles to the hot water bath and hold at a tem- perature of 125° to 130° F. for not less than three minutes. Add a few drops of glymol and read at once. The reading gives the per- centage of butterfat direct. Operation of Test with the 6 inch, 6 gram, 90 per cent bottle. — Follow the directions given for the operation of the test with the 9 inch, 9 gram, 90 per cent bottle with the following modifications : Instead of 9 grams, weigh 6 grams of the butter into the test bottle, 638 TESTING BUTTER and instead of 9 cc. add 12 cc. of lukewarm water just before the acid is added. Accuracy of Results. — Hepburn, as the result of a comparison of tests between the two 90 per cent butter test bottles and the official, chemical analysis, and embracing work with 124 separate samples of butter, finds the modified Babcock test, as described above, applicable as a successful commercial method for estimating the percentage of fat in butter. Other Modifications of the Babcock Test. — Earlier attempts to modify the Babcock test, so as to make it suitable for the rapid determination of the fat in butter, resulted in the construction and use of the Wright bottle and the Wagner bottle. In these bottles the graduated portion of the neck has a very narrow diameter and the bulk of the fat is assembled in a bulb which is a part of the graduated neck. Tests with these bottles have proven very uncertain and unrelia- ble, probably largely because even slight temperature changes, during the reading of the test, caused very great expansions or contractions of the fat column in the graduated portion of the neck, due to the relatively large volume of fat affected in the bulb of the neck and to the very narrow diameter of the graduated neck. This intensity of expansion and contraction of the thin fat column that is directly connected with the relatively large volume of fat in the bulb of the neck rests on the same principle as the mercury column in the ther- mometer. For these reasons, therefore, the use of these modi- fied Babcock bottles, equipped with bulbs in the neck of the bottle, is prone to yield entirely erroneous results and cannot be recom- mended for the determination of the percentage of fat in butter. Gravimetric Determination. Indirect Method. — Official. — Dissolve the dry butter, obtained in the moisture determination2 in which no absorbent was used, in absolute ether or petroleum ether, transfer to a weighed Gooch, with the aid of a wash bottle filled with the solvent and wash until free from fat. Dry the Gooch and contents at the temperature of boil- ing water until the weight is constant and determine the fat. Direct Method.— Official.1— From the dry butter, obtained in the determination of moisture,2 either with or without the use of an 1 Journal of the Association of Official Agricultural Chemists, Vol. II, No. 8, November, 1916. a See Determination of Moisture in Butter (Official TESTING BUTTER 639 absorbent, extract the fat with anhydrous, alcohol-free ether, receiv- ing the solution in a weighed flask. Evaporate the ether, dry the extract at the temperature of boiling water and weigh at hourly intervals until the weight is constant. Fat Determination by Kohman Method.1 Kohman recommends the following fat determination in con- nection with the moisture test : "The moisture is determined as usual over a small flame in a tall, rather narrow, lipped aluminum beaker with a capacity of about 100 cc., using a 10 gram sample. After the beaker is weighed to determine the loss of moisture, it is filled with petroleum ether and the contents are stirred with a glass rod to secure a thorough mix- ture. It is then covered with a watch crystal and allowed to stand two or three minutes for the mixture of curd and salt to settle, when the solvent is gently decanted off without disturbing the sedi- ment. The beaker is then filled with fresh solvent. The curd and salt mixture settles rapidly in the fresh solvent and the liquid can be decanted off after a very short time. By gently heating the beaker now, either on a water bath or a hot plate, or directly over a small flame, but not so rapidly as to cause sputtering, the sediment can be completely freed of petroleum ether by evaporation in a very short time. The per cent of fat is then determined by difference upon reweighing the beaker with its contents. The salt is now in ideal condition to be determined by titration, using a solution of such strength that the number of cc. used represents the per cent of salt. Before trying to evaporate the petroleum ether from the mixture of curd and salt, it is well to loosen it from the bottom of the beaker, gently tapping it on the desk in order to lessen the tendency to sput- ter." According to Kohman, this test requires about 15 minutes. Fat Determination by Shaw.2 "In this test for fat, the salt and part of the curd are first re- moved with hot water, the remaining curd is dissolved in dilute sul- phuric acid, the acid solution is removed from the fat, and the latter weighed. 1 Kohman, A Rapid and Accurate Method for Butter Analysis, Suitable for Factory Control Work. Journal of Ind. and Eng. Chemistry, Vol. 11, No. 1, 1919. 2 Shaw, A New Method for Determining Fat and Salt in Butter, Especially Adapted for Use in Creameries. U. S. Dept. of Agriculture, B. A. I. Circular 202, 1912. 640 TESTING BUTTER Apparatus Required. — "A Babcock centrifuge. A special sep- aratory funnel. A balance which is sensitive to 0.01 gram. (A tor- sion balance such as is used in the moisture test will answer if it is in good condition.) An accurate set of metric weights. A 10- cubic centimeter graduated glass cylinder. A 100-cubic centimeter glass beaker. Special Separatory Funnel. — -"This is essentially a separatory funnel with a capillary stem. The capacity of the funnel should be about 75 cubic centimeters and its weight when empty should not exceed 70 grams. The stopper may be dispensed with if desired. It is a convenience in the final weighing, but not a necessity. Special Socket. — "This is a double socket for holding the above funnel while centrifuging, and is made of heavy sheet copper with hangers of steel. Each socket will hold two funnels. The cut shows the construction and dimensions. It differs in no material way from the socket ordinarily used on the Babcock centrifuge, except for the opening in the side. If the dimensions given fail to fit the centrifuge at hand, they may be changed to suit so long as the dimensions of the barrels are not altered. Care must be taken that the capillary stem of the funnel does not project far enough through the hole in the socket to strike against the side of the centrifuge when being whirled. It is best to fit a disk of rubber gasketing to the bottom of the socket. Sampling the Butter. — . NEW* YORK WASHINGTON SAN FRANCISCO CHICAGO ROCHESTER, N. Y. LONDON Leading American Makers of High Grade Optical Products ALLWOOD Milk of Magnesia Lime The Perfect Neutralizer By the use of this material you are assured uniform, reliable and satisfactory neutralization. Its high standard of quality has been proven by continuous use in thousands of creameries. For further particulars, address, ALLWOOD SALES COMPANY MILWAUKEE WISCONSIN THE BUTTER INDUSTRY OlDENGLOWBUTTERCOLOR PURELY VEGETABLE fT'OR the butter maker who is JL more than ordinarily particu- lar there is no substitute for the GOLDEN GLOW. A single trial of this, an old and standard color, will convince you of its excep- tional merit. Original orders of any size will be sent transpor- tation charges paid. The understanding will be that if Golden Glow does not prove exadtly what you have always wished for in the way of a butter color it is to be returned at our ex- pense. On the primary points of quality and economy we invite comparison. It will be a pleasure on request to send a free sample for trial Quality and Economy BOERNER-FRY COMPANY IOWA CITY, IOWA 676 THE BUTTKR INDUSTRY THE BUTTER INDUSTRY 677 The "Simplex" Combined Churn and Butter Worker (Patented) No. 6 Cast Frame Type Showing Butter Worker in Position The only fully Automatic Combined Churn and Butter Worker. Churns the cream, works and delivers the Butter on tray ready to pack. Used in all Dairy Countries of the World. Also "SIMPLEX" Link Blade Cream Separa- tors and Milk Clarifiers, "SIMPLEX" Pas- teurizers, "SIMPLEX" Sanitary Milk Pumps, "FACILE" Babcock Testers and full line of apparatus for Butter and Cheesemaking and handling of milk. D. H. Burrell & Company Little Falls, New York, U. S. A. Sendfor Special Circulars 678 THE BUTTER INDUSTRY The Cedar Rapids manufacturing plant of the J. G. Cherry Company Everything in Equipment And Many Items of Current Supplies for the Modern Buttermaker The line of creamery machinery manufactured by the J. G. Cherry Company includes the well known Dreadnaught Churn Perfection Churn Haugdahl Starter Can Jensen Flash Pasteurizer Peerless Flash Pasteurizer Edwards Culture Can Cherry Ripener Simpson Printer Friday Printer Tubular Coolers Cherry Forewarmer Cherry Moisture Test Our Buttermakers catalog and Hand Book is a safe guide and ever-present help. Ask for it. J.G. CHERRY COMPANY ^RAPIDS IOWA THE: BUTTER INDUSTRY ALTHOUGH a good buttermaker can make good butter with almost any old churn, he can^make much better butter with a modern, efficient machine. The Dual Combined Churn and Butterworker is constructed on the correct mechanical principle, and as a result most prize-winning butter is made in a Dual. The Dual works the butter evenly between the rolls. Other two roll machines do not have the proper spacing between the rolls. The one-roll churn never could properly work butter — it simply mashes it over the edge of a shelf. Headquarters for Dairy Equipment For thirty years we have been serving the dairy industry — have grown with it — and now have the most complete line of dairy machinery and supplies (consisting of over 5,000 different items,) in the world. YOUR INQUIRIES ARE EARNESTLY SOLICITED The Creamery Package Mfg. Company SALES BRANCHES: (Write to nearest one) CHICAGO, 61-67 W. Kinzie St. NEW YORK, 47 W. 34th St. SAN FRANCISCO, 699 flattery St. BUFFALO, 133-137 Swan St. OMAHA, 113-15-17 S. Tenth St. PORTLAND, ORE., 6-8 N. Front St. MINNEAPOLIS, 318-320 Third St.,N. TOLEDO, OHIO, 119 St. Glair St. WATERLOO, IOWA, 406 Sycamore St. KANSAS CITY, 931 W. Eighth St. PHILADELPHIA, 1907 Market St. 680 THE BUTTER INDUSTRY THE REASON FOR. Lie Laval Leadership Every one who has given sound thought or considera- tion to the question, knows that the name DE LAVAL stands today-r- as it has since 1878 — for leadership in quality and There is always a good reason for every lasting success. Years of actual use in the hands of nearly three million users the world over have demonstrated beyond question the su- periority of the De Laval hand and factory size separators. They have met the requirements of every-day use in the best possible Likewise, the other members of the De Laval family — the Clarifiers, Emulsors and special Centrifugal machines of various kinds, have been designed to meet the needs of their users in the most efficient way and for that reason each one of the line stands in the front rank in prestige and reputation. The reason for De Laval leadership is in service ren- dered. The De Laval machines work better, last longer, and produce the greatest possible returns for every dollar in- vested. There is a great deal of satisfaction, as well as extra profit, in owning and using the best machinery and equip- ment and there is no good reason why any responsible farmer or creameryman or ice cream manufacturer should be satisfied with any other style of machine. Make up your mind to know the facts about the history and performance of the machines you are planning to buy. We covet the most rigid investigation and comparison — and will gladly leave the decision to your judgment. The De Laval Separator Co. 165 Broadway, New York 29 E. Madison St., Chicago 61 Beale St., San Francisco! Cal. THE: BUTTER INDUSTRY 681 Progress Can Washer WITH this machine in your plant you are enabled to furnish the producers with clean, sterile and dry milk cans. This service helps to lower your bacteria count to a minimum. Whether you wash a hundred or a thousand cans per day you will find this machine a profitable investment. It is practical. It occupies small floor space and uses very little power. It saves waste, time, labor and money. Write for information. DAVIS-\\^TKINS DAIRYMEN'S MFG.CO. ADDRESS NEAREST OFFICE JERSEY CITY. N. J. NORTH CHICAGO. ILL. ATLANTA. GA. DENVER COLO SAN FRANCISCO. CALIF. LOS ANGELES CALIF. SEATTLE, WASH. THE BUTTE* A Wonderful Churn YOUR buttermaker is a success at his job if you give him the right took to work with. He takes great pride in properly handling efficient machinery. He is just as proud of a pure-bred churn as you are of your pure-bred Jerseys, Holsteins, Packards or Pierce- Arrows, Don't you see how important it is that you give him a modern Disbrow? It is just as rssrnrial to him as a good cook store is to your wife, put up with almost anything CDC, but sac must have a good It's *Vf thing her neighbors see anj ^jmjfr. It makes her finable. She turns out better food for your family by having •OTU her kitchen because of it. Write for a copy free, and there is no obligation. for you. CD it of it all other tools are The Disbrow Omni Book." It i DAMS -\VT\TKINS DAIRYMEN'S MFG.CO. THE BUTTER INDUSTRY 683 Minnetonna Cream Ripener A beautiful machine for the man who wants the right appear* well as efficiency. The two are combined in the Mint to build this marhinr so it wfll give customer satisfaction and honest value for the money invested. The Miniirf <••** Cream Ripener pictured above is with wfcit enameled sheets and tinned copper trimmings. The cover is tinned copper completely finished inside and outside. You can have yours for either motor or belt drive. This machinr will add much to the at- tractiveness of your plant. If you prefer, you can purchase this same efficient cream ri a plain finished steel body. Some folks like the wood Cream Ripener; you can have one of these, which of as much money as the steel or enamel finished machines. As to capacity . we make many sizes from the small one holding 200 gallons up to those Teflusthe Write our nearest office for full n size you are interested in. Your order wfll have our Let us have it quickly. DAMS-WMKINS DAIRYMEN'S MFG.CO. ADDRESS NEAREST OFFICE 684 THE: BUTTER INDUSTRY View of Elyria tanks in the modern plant of the Stroh Products Company, Detroit, Mich. ELYRIA SEAMLESS, ONE-PIECE, GLASS- ENAMELED EQUIPMENT is rapidly coining to be the standard in all modernly equipped dairies and butter-making establishments. This is because it is 100 per cent, efficient. It has the permanence of steel and the cleanliness and sanitation of glass. Without the semblance of crevice or seam for the lodgment of bacteria, with an inside surface of hard, glossy, deep-blue enamel that is as easy to clean as a china bowl, Elyria Equipment is the safest with which to take care of milk and milk products, enabling the Buttermaker to do his work with certainty of economy and absolute sanitation. The Elyria Company is prepared to show that the installation of Elyria-Equipment will, in a compara- tively short time, save more than the original cost of the investment. We shall be glad to send complete literature to any one engaged in the Buttermaking Industry. The Elyria Enameled Products Co. ELYRIA, OHIO, U. S. A. New York Chicago Pittsburgh Los Angeles San Francisco THE: BUTTER INDUSTRY 685 Triple Beam in Agate Bearing above cap Fairbanks No. 10105 Receiving Scale Has Full Capacity Beam and Tare Bar Marked: Upper Bar 200 IBs. x 1 Ib. Main Bar4001bs. x 100 Ibs. Lower Bar 100 Ibs. x % Ib. Fairbanks, Morse & Co. 900 So. Wabash Ave. CHICAGO 686 THE BUTTER INDUSTRY Facts Mold Opinions IN EVERY walk of life opinions are fashioned by facts. Horseless vehicles were deemed unlikely until the automobile came into existence and what was even more recent, much improved cleaners for use in dairies, butter and cheese factories were considered impossible until became a fact. Today the rapidly increasing use of this cleaner and the wide recognition awarded it by leading authorities in every depart- ment of dairying and its allied industries plainly suggests how much it will profit you, provided you utilize these facts. Wherever the facts concern- ing Wyandotte Dairyman's Cleaner and Cleanser are known the opinion is the same — it cleans clean. IN EVERY. PACKAGE ORDER FROM YOUR SUPPLY HOUSE The J. B. Ford Co., Sole Mnfrs., Wyandotte, Mich THE: BUTTKR INDUSTRY 687 For Sterilizing P*HE control of bacteria during every step in the handling of dairy products — beginning at the cow and ending with the consumer — is of such import- ance that easy means of accomplishing it must be within the reach of everyone engaged in handling such products. B-K provides a sterilizer effective in the hands of any butter-maker, cheese maker, or dairy farmer. It is easy to use — does its work quickly — at a low operating cost — requiring no extra labor or equipment for its application. In addition it is economical in actual use and produces a degree of cleanliness not to be obtained without it. B-K provides bacteria control in all kinds of equipment. Being liquid, it flows over and into every spot and corner that milk or cream will touch. As the B-K rinse flows through the equipment it dissolves bacteria and casein sediment alike, leaving a condition of cleanliness difficult to obtain by any other method. Our Laboratories and Service Department have given expert service to B-K users for years. We have had a large experience in the field, under practical conditions, and are prepared to give help in bacteria control to all who need it. Write us for information and free bulletins. General Laboratories 110 So. Dickinson Street Madison, Wisconsin 688 THE BUTTER INDUSTRY SANITARY MllKCAN WILL SERVE YOU LONG AND WELL BUTTER INDUSTRY 689 How To Prevent Streaks and Mottles in Butter Prof. Hunziker asserts that streaks and mottles in butter are caused by: (1) — Incomplete fusion of salt and water in butter. (2) — Faulty mechanical condition of the butter workers. (3) — Overloading of the machine. Not one of these causes but what may be overcome by any buttermaker who takes pride in his product. With Colonial Salt the buttermaker will never be troubled with incomplete fusion. The other two causes are mechanical and can be easily remedied. Flake salt dissolves quicker than cube salt of the same size grain. Colonial salt is the only all flaked Butter Salt on the market. It will produce over-run, color, flavor and body. Try it in your next batch of butter. THE SALT THAT MELTS LIKE SNOW FLAKES AND DISSOLVES LIKE MIST THE COLONIAL SALT CO. AKRON, OHIO CHICAGO BOSTON ATLANTA BUFFALO GLASCOTE SEAMLESS, GLASS -COATED, STEEL EQUIPMENT FOR THE BUTTER INDUSTRY GLASCOTE equipment being seamless, and coated inside with pure white glass, enforces cleanliness and prevents metallic flavors. CREAM RIPENING, PASTEURIZING AND PROCESSING TANKS, STARTER CANS, STORAGE TANKS, ETC., complete in every detail and most efficient. They save floor space and labor and handle your product in the most sanitary, efficient and attractive manner possible. WRITE FOR MILK PRODUCTS BULLETIN The Glass Coating Company New York — Chicago — San Francisco CLEVELAND, OHIO 690 THE BUTTER INDUSTRY The JALCO The Why of the Jalco — Brought up in a creamery, the Jalco is an investment in which you, as a member of the same guild as its designer, can place the utmost confidence. The Jalco is built to fit your current; designed for cream and milk testing exclusively and carries a guarantee that means real machinery devotion. No gears, no rheostats or starting boxes and no hand brakes; just genuine died - in - the - aluminum quality. A postal card brings the information you need from any of the supply houses listed on this page or direct from: THE JAICO MOTOR COMPANY IS SOLD AND RECOMMENDED BY: A. H. Arnold & Bro. J. G. Cherry Company A. H. Barber Creamery Supply Co. Blanke Mfg. & Supply Co. Riley Hauk Supply Co. Hawkeye Supply Co. The Creamery Package Mfg. Company Davis-Watkins Dairymen's Mfg. Co. Bessire & Company N. A. Kennedy Supply Co. John W. Ladd Company Owatonna Creamery Supply Co. Crary Brokerage Company J. S. Biesecker E. B. Adams Company The Central Ohio Supply Co. Cherry-Bassett Company The Dairy Supply Co. Dairymen's Supply & Construction Co. E. F. Mangold Company Standard Milk Machinery Co. West-Hutchison Company Wisner Manufacturing Company W. T. Connelley K. J. Madden E. A. Kaestner UNION CITY. INDIANA. THE BUTTER INDUSTRY 691 Better Cream — Better Prices CREAMERY MEN EVERYWHERE WILL WELCOME THE WONDERFULLY EFFECTIVE NEW Sanitary Cream Cooler CREAM, when first separated, is at its highest value to the butter- maker. Help your creamery patrons to realize the most for their produce and at the same time make more for yourself by being sure the cream is cooled directly after milking. The Sanitary Cream Cooler makes this possible. Creamery managers can well afford to send out coolers, paying for them in the increased price of sweet cream. WRITE FOR PLAN. DESCRIPTION AND QUANTITY PRICES INDEPENDENT SILO CO., St. Paul, Minn. MANUFACTURERS OF Cream and Milk Coolers, Milking Machines, Silos and Tanks The World's Model Paper Mill - Special Papers Best Brand Pure Vegetable Parch- ment Paper. The paper that is better moist than dry. Toughens up like a bladder when wet. Made under sanitary conditions for the absolute purity a paper used in wrapping butter must have. Used to line butter tubs, for lard bags, as carton linings, to protect from contamination. Manu- factured in rolls or cut in regular butter sizes, plain or printed, as well as many special sizes to order. Send for samples. KALAMAZOO VEGETABLE KALAMAZOO. Pure KVP Waxed Paper Used in great .quantities for carton sealers and bread wrappers. Made in many colors, in rolls or cut sizes, plain or printed. Send for samples. The New KVP Bond A multi-purpose bond that takes half-tone cuts in great style! Low Cost. High Quality. Made in all bond weights and a line of colors and white. Samples ready. PARCHMENT COMPANY MICHIGAN 692 THE BUTTER INDUSTRY Vertical -Universal and Ripener Pasteurizer COIL of the Tertical type and entirely sus- pended; shaft of heavy seamless brass; tubing of 2 -inch 16 gauge copper; Twin Coil. UNIFORM tempera- ture throughout Tat during heating or cool- ing. INSULATION— VA- inch and 2-inch Cork Board, depending on size of machine. COVERS — Overlap style with piano hinge,. PACKING BOXES— entirely eliminated from the vat and lo- cated above and out- side the vat. ELIMINATES AIR FROM PRODUCT— It is constantly worked out by the helical coil. Oxidation reduced. FLOOR SPACE— One-half that of hori- POWER — Motor or Belt % to % that re- quired for horizontals Increase your efficiency of Pasteurization and Ripening, by using this machine. It is the Only Real Glass-Lined Pasteurizer or Copper Vat Pasteurizer equipped with a double twin Helical coil but Without Packing Boxes in the ends of the vat. Why suffer with mold, yeast and bacterial recontamination when it can be entirely overcome by using this Vertical-Universal ? Reduce oxidation in your product by clarifying it of gas and air. The vertical twin or double coil con- stantly working from the bottom up, wrings the air and gas out. A longer-keeping product results. JENSEN VERTICAL CONDENSED MILK COOLER Eliminate Crystallization Furnish correct amount of agi- tation to pro- duce a smooth product. Eliminate air and gasses through Rota- tion of Double Helical Coil during cooling process. Prevent Contamination As all packing and stuffing boxes are out- side and above the machine. Specially Built for Cooling Condensed and Evaporated Milk. Ask for Catalogue No. 20-A. B JENSEN CREAMERY MACHINERY COMPANY LONG ISLAND CITY. N. Y. «Hm«»N D.STR.BUTORS- OAKLAND. CALIFORNIA IBLANKE MFG. & SUPPLY co., ST. LOUIS. MO. THE BUTTER INDUSTRY 693 Pasteurizing Unit CONTINUOUS SANITARY Eliminate Seconds . Send for Catalogue No. 24-A WRITE AND LET US TELL YOU HOW IT IS DONE Jensen Pumps Sanitary Durable Efficient ELECTRIC DRIVE COMBINATION Simple in Con- struction ONLY TWO PARTS TO TAKE DOWN AND RE-ASSEMBLE WHEN CLEANING STANDARD U BASE Send for Catalogue No. 21 JENSEN CREAMERY MACHINERY COMPANY LONG ISLAND CITY. N. Y. SOUTHERN DISTRIBUTORS: OAKLAND, CALIFORNIA BLANKE MFG. 8c SUPPLY CO., ST. LOUIS, MO. 694 THE: BUTTER INDUSTRY CORRECT NEUTRALIZATION of sour cream is an important part of the process of modern butter- making. And the choice and use of the right kind of neutralizer is equally essential. Our Special Dairy Lime The Ideal Cream Neutralizer is a lime of the highest quality and has been found the best available and most suitable for this purpose. Ask for prices — address "Industrial Dept." The Kelley Island Lime & Transport Co. World's Largest Producer of Lime and Limsetone Products 11 ACTIVE PLANTS NEAR PRINCIPAL CENTERS General Offices ' Cleveland As NECESSARY As SALT Make good butter — Protect its goodness- Put your brand on it- Get your butter to the consumer as fresh, pure and clean as when it leaves your churn. Protect it from dust and dirt by wrapping it in PATERSON PIONEER PARCHMENT PAPER and put your name on the parchment. That will mean a bigger demand for your butter and higher prices. WRITE FOR FREE BOOK "BETTER BUTTER" EVERY DAIRYMAN SHOULD READ IT The Paterson Parchment Paper JCo. Passaic, New Jersey, U. S. A. THE BUTTER INDUSTRY 695 Get Rid of Excessive Moisture in Your Creamery Is your creamery wet? Does steam con- dense on the walls and water drip from the ceiling? Poor ventilation is the cause. The King System of Ventilation will change the air in your creamery every few min- utes and carry off the moisture. Your creamery is kept sanitary, preserving your equipment and the health of your butter makers. Lengthens the life of your build- ing. Makes the creamery more attractive. Send for Our Book on Creamery Ventilation This book explains the King: System— what it is— why you need it— how we put it in— what it will save you. Kinsr Engineers study each creamery before planning a system. When you order a King: System we assume a responsibility which does not cease until your creamery is properly ventilated. King Ventilating Co. 1219 Cedar St. Owatonna, Minn. On the Jefferson Highway Vtnt lalinz Engineers for Creameries and Farm Buildings KING This shows the way the King Sya. tern carries out excessive moisture through Aerator on the roc f. Unless the vent!- lating system bears this diamond King trade-mark it is not a King System System of Ventilation 696 THE BUTTER INDUSTRY The Lathrop- Paulson Company has Perfected a New Type Can Washer of Super -Success. No Waste, Less Work, Bigger and Better Results. This New L-P Entirely Automatic Machine has Capacity up to 700 Cans and Covers per hour. Practical and efficient in every way. Embodies all the features of our former machines with double their efficiency, at less cost. Aug. 20, 1907. Aug. 20, 1907. Sept. 14, 1909. 22, 1916. 4. 1917. Feb. Dec. Apr. Sept. 4, 1916. 9, 1919. . 864,131 . 864,133 . 934.404 .1,172,808 .1,249,129 . 168,585 . 192,648 Jan. Apr. Aug. Mar. Feb. U. S. PATENTS L918.... 1,252,453 16, 1&18.... 20, 1907 3, 1908 15, 1910.... CANADIAN PATENTS Nov. 11, 1919.... Sept. 9, 1919.... 1,262.679 864,132 880,713 949,121 193,886 192,647 Nov. Dec. Feb. Dec. Nov. Nov. Other U. S. and Foreign Patents Pending 27, 1917. 4, 1917. 12, 1918. 31, 1918. 11. 1919. 25. 1919. .1,247,692 .1,249,130 .1,255,896 .1,289.824 193,885 194,208 NOTABLE IMPROVED FEATURES: Does not require even one man to operate. Machines are END FED, most convenient for disposal of can by milk dumper. Driven by motor or steam turbine of less than one and one-half horse power. Less than one-quarter horse-power consumed in automatic machine drive. Water consumption cut seventy-five per cent. Drying capacity DOUBLED. Fan delivering 1800 cubic feet of dry, sterile, super-heated air per minute. WARM SODA SOLUTION WASH-under pressure of 80 to 100 pounds. CLEAR SCALDING WATER WASH immedi- ately following under pressure of 80 to 100 pounds. THE LATHROP -PAULSON COMPANY art MILK CAN WASHING MACHINE SPECIALISTS and SOLICIT YOUR INQUIRIES and REQUIREMENTS THE LATHROP -PAULSON COMPANY STEAM STERILIZATION under complete con- trol. any amount you desire. Operating at the rate of 700 cans and covers per hour. EACH and EVERY CAN re- ceives THREE to FIVE minutes of bac- teria-destroying sterilization. Insures Clean, Dry, Sterile receptacles for the conveyance of product from producer to manufacturer at lowest possible cost. Machines have the unique feature of handling cans as fast or as slow as desired, depending solely on the speed they are fed to machine, and cannot be crowded beyond capacity. 2459 WEST 48TH STREET CHICAGO, ILLINOIS BUTTER INDUSTRY 697 The Mojonnier Culture Controller is used for the continual propagation and control of pure Lactic Cultures and other bacteriological work. Made in several sizes, — compartments of a few quarts capacity to the larger size holding four two- gallon cans for large dairies in two and three com- partment models. The Mojonnier Composite Sample Bottle with pure Para rubber stopper fastened to bottle by non-kinkable chain. Sold either 4-oz., 8-oz. or 16-oz. sizes. Other specialties for butter-makers and dairies being developed, including a new type butter print scale. A model for ecery requirement. Write for literature. MILK ENGINEERS 739 W. da.ckson Bout. Chicago Branch Offices— New York, St. Louis, and San Francisco 698 THK BUTTER INDUSTRY Naf is Creamery Glassware WILL HELP TOWARD HIGHEST EFFICIENCY IN YOUR TESTING ROOM It is made according to scientific methods and is guaranteed to be Accurate and to give Excellent Service. IMPROVED BUTTER TEST BOTTLE for determining percentage of butter fat in butter Pat. Aug. 18, 1918 Nafis Standard Butter Color Rod contains four standard shades of yellow for matching the color of butter for various markets. Based upon the color formula of the U. S. Bureau of Standards. Approved by butter experts. There is a tremendous weight in the fact that NAFIS GLASSWARE is used by most of the largest creameries in the country, but the strongest proof for you is the proof of your own experience. If your dealer cannot supply you with Nafis Glassware write for our illustrated catalogue and list of our dis- tributors. Nans Automatic Acidity and Salt Testing Outfits LOUIS F. NAFIS, Inc. MANUFACTURERS OF CREAMERY GLASSWARE 542-548 Washington Blvd. CHICAGO THE) BUTTER INDUSTRY 699 Peters Automatic Package Machinery COMPLETE line of machinery which automatically (i) forms, (2) lines, (3) fills, (4) folds, (5) closes, (6) wraps, (7) labels, (8) seals pack- ages of food products, or performs any part of these operations independently. This ingenious, compact machinery effects material economies in labor, time, and floor space. Further, it places packages of food products in the hands of consumers in sub- stantially the same condition in which they left the producer. For years it has been used success- fully by foremost food manufacturers. PETERS MACHINERY COMPANY 209 South La Salle Street CHICAGO 700 THE BUTTER INDUSTRY Pfaudler Glass Enameled Cream Ripener Pfaudler Cream Ripener Prevents Metallic and other "Off Flavors" by providing an absolutely sterile, Glass Lined, container. Provides a method of heating that is well distributed, and readily responsive to the will of the operator. Avoids "pockets" where filth can collect. Is so easily "get-at-a-ble" that the cleaning operation can be safely intrusted to cheap labor. The Method of Heating The jacket is filled with water and an extra pipe attached for use as an expansion chamber. Steam is injected into the water through the Steam Spreader shown in the sketch. The Jacket is provided with a thermometer and the temperature of the water may be regulated at will. Specifications Capacity, 250 gallons. It may, however, be had in any suitable size and in different widths and heights. Brass agitator either tinned or silver plated, mounted in an oil-less bearing. Copper cover. Tight and loose pulley. Prices on application. Showirvj How Water h Jacket Is Heated By Steanv Just Printed, "Pfaudler Dairy Equipment " Write for your copy The PFAUDLER Co. DETROIT ROCHESTER, N. Y. NEW YORK CHICAGO ST. LOUIS SAN FRANCISCO THE BUTTER INDUSTRY 701 Pfaudler Glass Enameled Cream Vat Mr. Hunziker recently said: "It has been conclusively de- monstrated experimentally by the United States Dairy Division and by the writer, and it has been proven in the manufacture of millions upon millions of pounds of butter by the writer, that ex- cessive exposure of the milk, cream or butter to iron or cop- per causes chemical action, which leads to most disastrous and cost- ly butter defects The only really satisfactory material for the construction of fore- warmers and cream vats, is the glass-enameled type Cop- per vats such as have been in use in the past and are still in use, have been found damaging to the quality of butter There is only one substitute for a copper vat that is better than it and that is the glass-enameled vat. Glass-enameled equip- ment is the coming equipment for the creamery." The Illustration The Pfaudler Glass Enameled Receiving Vat shown is six feet long, three feet wide, two and a half feet deep, and has a total height of three and a half feet Capacity 300 gallons. It may, however, be had in other sizes and capacities and may be equipped with an agitator. Prices on application. Just Printed* "Pfoudler Dairy Equipment " Write for your copy The PFAUDLER Co. ROCHESTER, N. Y. NEW YORK DETROIT ST. LOOS CHICAGO SAN FRANCISCO 702 THE BUTTER INDUSTRY Hansen's Lactic Ferment Culture and Danish Butter Color ARE USED ALL OVER THE WORLD WHERE THE FINEST BUTTER IS MADE. Rennet Extract and liquid Cheese Color for factory use. Rennet Tablets and Cheese Color Tablets for cheese making on the farm. Junket Tablets for Cottage Cheese in every home. CHR. HANSEN'S LABORATORY, Inc., Little Falls, N. Y. ' BRANCHES at Milwaukee. Wis. and Philadelphia. Pa. FACTORIES also at Copenhagen. Denmark; Reading. England, and Toronto, Canada. PERFECTION BRAND BUTTER COLOR PURELY VEGETABLE A TOP NOTCH BUTTER COLOR MADE BY The Preservaline Mfg. Co., Brooklyn, New York Rice & Adams Hydraulic Can Washer Produces clean, dry, sterile cans. Cleanses the inside, outside and cover in one operation, leaving the can immaculately clean. No more sour milk trouble when the R & A Hydraulic is used. SEND FOR THE R 6- A CATALOG RICE & ADAMS, INC. 166-182 Chandler Street Buffalo, New York THE BUTTER INDUSTRY 703 Great Western Cream Separator Great Western equipped with electric motor Here is the cream separator that has proved itself a profit maker for 15 years. That's be- cause it gets all the cream from every skimming, day after day- week after week. With the Great Western the milk just naturally runs down hill and out the bottom outlet of the bowl, while the cream, being lighter, comes to the top and goes out the top outlet. The bottom outlet bowl sepa- rates the cream from the milk just as Nature does — and the Great Western is the only disc bowl machine with this desirable bottom outlet bowl feature. Correct Oiling System Low Upkeep The big expense on most separators is for new bearings caused by the milk getting in with the oil, thinning out the oil and thus eating out the bearings. On the Great Western the bottom outlet bowl gives the milk a straight down- ward course. It never runs over and down the sides into the spindle bearings of the pan base. The Great Western is made in six sizes, ranging from 300 to 900 Ibs. capacity per hour. WRITE TODAY FOR COMPLETE DETAILS AND LARGE ILLUSTRATED GREAT WESTERN CATALOG. Rock Island Plow Company Factory and General Offices .. Rock Island, Illinois BRANCHES: Sioux Falls Minneapolis Indianapolis Omaha Kansas City Oklahoma City Dallas 704 THE BUTTER INDUSTRY THERE IS A BEST IN EVERYTHING Miller's Hydraulic Cutter ESPECIALLY ADAPTED FOR CUTTING CONGEALED MATERIAL SUCH AS BUTTER, OLEOMARGARINE, SOAP. VEGETABLE OIL PRODUCTS, ETC., ETC. SOLE MANUFACTURERS L. C. Sharp Manufacturing Company Plattsmouth, Nebraska, U. S. A. THE; BUTTER INDUSTRY 705 Oar Stock of Chemicals and Chemical Apparatus for the Butter and Milk Laboratory is Very Complete AMONG OTHER THINGS WE CAN SUPPLY PROMPTLY:- Autoclavs Counting Plates Petrie Dishes Staining Dishes Incubators for Gas Electric Incubators Cover Glasses and Slides Electric Moisture Ovens Balance and Weights Microscopes Aluminum Dishes Babcock Milk Testers Etc. Correspondence solicited Catalogue on request We will be glad to quote on your laboratory requirements E. H. Sargent & Co. IMPORTERS, MAKERS AND DEALERS IN CHEMICALS AND CHEMICAL APPARATUS OF HIGH GRADE ONLY 1 55- 1 65 E. Superior Street Chicago, Illinois 706 THE: BUTTER INDUSTRY Mr. P. M. Sharpies invented and perfected the first American separator nearly forty years ago. Sharpies machines today are manufactured in the oldest and largest separator factories in America and are the standard machines throughout the world. Sharpies machines are 100% American: Owned by Americans, manufactured by Americans, built by Ameri- can labor of American material and preferred by Americans. Send for special catalogs on any of these machines in which you may be interested: Sharpies Suction-feed Cream Separator; Sharpies Factory Milk Separator; Sharpies Whey Separator; Sharpies Super -Clarifier and Sharpies Emulsifier. The Sharpies Separator Co. WEST CHESTER, PA. BRANCHES: CHICAGO SAN FRANCISCO TORONTO TH£ BUTTER INDUSTRY 707 For Sanitary Service Use They are easy to clean and keep clean. The most sanitary, and the most econom- ically operated milk plants use them ex clusively. They are made of highest quality steel plate, tinned and retinned. All seams are soldered on the inside — perfectly smooth. No crev- ices for milk particles to lodge in and sour. You should see our extra heavy seamless rim cover. Send for Catalog No. 111. Sturges & Burn Mfg. Co. 508 South Green Street Chicago, 111. TORSION BALANCE SCALES THE ACCEPTED STANDARD FOR BUTTER MAKERS Rapid- Sensitive- Accurate No. 1700— Moisture Test Scale. Extensively used for moisture in butter. Percentage of moisture (1 / 10# to 30#) read direct from the beams without calculation. Thousands in daily use. CREAM TEST SCALES BUTTER PRINT SCALES Christian Becker Analytical Balances for Chemical Laboratories. TORSION BALANCE COMPANY Factory— Jersey City, N. J. Main Office— 92 Reade St., New York, N. Y. BRANCHES— 31 West Lake St., Chicago. 111.; 49 California St.. San Francisco, Cal. THE BUTTER INDUSTRY An AuTom^rfic System of Temperature Corrfrol PASTEURIZER Typical application of a TAG Perfect Automatic Temperature Controller and Recording Thermometer attached to a flash pasteurizer — both of which are es- sential for efficient and economical pasteurizing. Simple-Efficient-Self-Paying Improvement of flavor and keeping quality are the two principal advantages of efficient pasteurization but — efficient pasteurization can only be achieved by constantly maintaining a UNIFORM temperature within the pasteurizers. TAG Perfect Temperature Controllers offer a simple and efficient solution because they automatically maintain the exact temperature required — and are self-paying because they not only conserve considerable labor and steam, but also improve the flavor and keeping quality of the butter. TAG Recording Thermometers assure uniformity of results because they accurately record every temperature operation, day or night, thereby promoting efficiency among the workmen in their efforts to pro- duce praiseworthy charts. Catalogs H-42S and H-345 will provide further informa- tion of interest and value. MFG.CO. TEMPERATURE ENGINEERS \J6-68 ThirtyThini St. Brooklyn. N.Y. THE BUTTKR INDUSTRY 709 Precise Weights in Packing Butter E Toledo Predetermined Weight Scale for use in packing butter in tubs is especially de- signed to prevent both underweight and over -allow- ance for shrink- age. In other processes of weighing in the dairy, other types of Toledo Springless Automatic Scales also render rapid, accurate and efficient service. WRITE FOR INFORMATION Largest Automatic Scales Manu- facturers in the World Toledo Scale Company Toledo, Ohio Canadian Factory: Windsor, Ontario BRANCH OFFICES AND SERVICE STATIONS in sixty-nine cities in the United States. , Others in thirty-four foreign countries. 10 THE BUTTER INDUSTRY Ask Yourself These Questions /Will not fine salt dissolve more quickly than coarse salt? Will not the fine salt which dis- solves the quickest distribute the most evenly? Will not the fine salt which dis- solves the quickest and dis- tributes the most evenly be the one best adapted to help you control the moisture content of your butter? Will not this fine salt also be the one least liable to cause mottles or brine pockets in your butter? Scientific tests and practical experience have proven time and again that the Worcester Brand is the quickest dissolving butter salt. Its crystals are very fine in grain and remarkably alike in shape and size. They afford the maximum of surface on which the moisture in your butter can act. Combined with these advantages the peculiarly sweet and pleasant flavor of Worcester Salt makes it 100% efficient. That is why it is the favorite Brand of buttermakers everywhere. They know IT TAKES THE I TO MAKE THE J Worcester Salt Co. LARGEST PRODUCERS OF HIGH GRADE SALT IN THE WORLD New York FACTORIES: Silver Springs, N. Y. Ecorse, Mich. OFFICES: Boston, Philadelphia Chicago, Columbus, Detroit THIS BOOK IS DUE ON THE LAST DATE STAMPED BELOW AN INITIAL FINE OF 25 CENTS WILL BE ASSESSED FOR FAILURE TO RETURN THIS BOOK ON THE DATE DUE. THE PENALTY WILL INCREASE TO SO CENTS ON THE FOURTH DAY AND TO $1.OO ON THE SEVENTH DAY OVERDUE. oqr 21 t938 NOV 25 1932 u 1933 FEB 15 FEB 15 1933 JAN 251939 OCT 18 f9ft 24Nov'5W 131954 UP LD 21-50w-8,-3 UNIVERSITY OF CALIFORNIA LIBRAK