Acute lethality data for Ontario's organic chemical manufacturing sector effluents covering the period from October 1989 to March 1990

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STOPPING
WATER POLLUTION "7"
AT ITS SOURCE

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Municipal/Industrial Strateay tor Abatement

ACUTE LETHALITY DATA
FOR ONTARIO'S ORGANIC
CHEMICAL MANUFACTURING SECTOR
EFFLUENTS COVERING THE PERIOD FROM
OCTOBER 1989 TO MARCH 1990

@ Environment
Ontario

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ISBN 0-7729-8788-2

ACUTE LETHALITY DATA FOR ONTARIO’S
ORGANIC CHEMICAL MANUFACTURING SECTOR
EFFLUENTS COVERING THE PERIOD FROM
OCTOBER 1989 TO MARCH 1990

Report prepared by:
J.T. Lee, C.S. Logan, M.C. Mueller, D.G. Poirier
G.F. Westlake
Aquatic Toxicity Unit
Limnology Section
Water Resources Branch
Ontario Ministry of the Environment

SEPTEMBER 1991

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RECYCLABLE

Cette publication technique
n’est disponible qu’en anglais.

Copyright: Queen’s Printer for Ontario, 1991
This publication may be reproduced for non-commercial purposes
with appropriate attribution.

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Contents

page
AKZO Chemical Ltd., Sarnia

trout 1

Daphnia 7
Amoco Canada Petroleum Canada Ltd., Sarnia

trout 13

Daphnia 17
B.F. Goodrich Canada Inc., Thorold

trout 21

Daphnia 31
BASF Canada Inc., Sarnia

trout 41

Daphnia 49
BASF Fibres Inc., Arnprior

trout 57

Daphnia 59
BTL Specialty Resins, Belleville

trout 61

Daphnia Th.
Canadian Oxy Chemicals Ltd., Fort Erie

trout 93

Daphnia 97
Celanese Canada Inc., Millhaven

trout 101

Daphnia 125
Chinook Chemicals Company, Sombra

trout 149

Daphnia 157

Cornwall Chemicals Ltd., Cornwall
trout 165
Daphnia 175

Contents

Courtaulds Fibres Canada, Cornwall
trout
Daphnia

Dow Chemical Canada Inc., Sarnia
trout
Daphnia

Du Pont Canada Inc., Corunna
trout
Daphnia

Du Pont Canada Inc., Kingston
trout
Daphnia

Du Pont Canada Inc., Maitland
trout
Daphnia

Du Pont Canada Inc., Whitby
trout
Daphnia

Esso Chemical Canada, Sarnia
trout
Daphnia

Ethyl Canada Inc., Corunna
trout
Daphnia

GE Plastics Canada Ltd., Coburg
trout
Daphnia

Guardsman Products Ltd., Cornwall
trout
Daphnia

Morbern Inc., Cornwall
trout
Daphnia

page

183
231

281
339

397
413

425
441

459
471

485
489 .

493
507

521
529

537
547

557
559

561
565

Contents

Novacor Chemicals Ltd., Mooretown
trout
Daphnia

Polysar Ltd., Sarnia
trout
Daphnia

Rohm & Haas Canada Inc., Scarborough
trout
Daphnia

Stepan Canada Inc., Longford Mills
trout
Daphnia

Uniroyal Chemical Ltd., Elmira
trout
Daphnia

page

569
577

585
631

681
689

697
705

713
745

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conne

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SUMMARY

Under the MISA program, the Organic Chemical Manufacturing Sector was required to
monitor its discharges (both process and cooling waters) for acute lethality to trout and
to Daphnia magna by conducting laboratory toxicity tests. This requirement was based
on provisions of the Ontario Environmental Protection Act which allowed the Ministry to
write regulations requesting persons responsible for sources of contaminants to monitor,
record and report to the Ministry. Specific details on the toxicity testing requirements may
be found in the General Effluent Monitoring Regulation (Ontario Regulation 695/88) and
the Effluent Monitoring Regulation For The Organic Chemical Manufacturing Sector
(Ontario Regulation 209/89). For the purposes of these regulations, organic chemical
manufacturing refers to the manufacture of chemicals based on carbon and the plants,
within this industry, can be grouped into three classes of products; organic chemicals,
plastics, and synthetic fibres. An overview of this sector in Ontario is described in the
publication "The Development Document For The Effluent Monitoring Regulation For The
Organic Chemical Manufacturing Sector. Env. Ontario 1989". Information collected under
the MISA effluent monitoring program will be used toward the development of compliance
limits for effluent acute toxicity. The following data report presents the toxicity results of
this monitoring along with the results of audit samples that were tested at the Ministry’s
laboratory in Rexdale. In addition, toxicity tests of some intake waters were also submitted
by industry and these have been included in this report.

The data collected during the first six months of monitoring indicate the majority of
organic chemical manufactures’ effluents were not acutely lethal. Over 80 % of the
samples tested for trout toxicity and 60 % of the samples tested for Daphnia toxicity were
determined to have been non-lethal by standard testing methods. Most of the samples
that were determined to have been acutely lethal to trout and/or Daphnia were collected
from sites at the following six companies: Cornwall Chemicals Ltd. (Cornwall), Courtaulds
Fibres Canada (Cornwall), Du Pont Canada Inc. (Kingston), Du Pont Canada
Inc.(Maitland), GE Plastics Canada Ltd. and Uniroyal Chemical Ltd. (Elmira). All these
companies reported that one or more of their discharges were acutely lethal the majority
of the time when sampled. The Figures 1 to 9 present selected toxicity data (LC50s) for
trout and Daphnia. The plots are for those discharges that had some toxicity to both
animals. Note that low values of LC50 mean high acute toxicity.

In general, toxicity tests are used as a rapid technique to assess the potential impact of
complex effluents on the aquatic environment. In acute lethality toxicity testing, aquatic
organisms are exposed to undiluted effluent, and several effluent dilutions, for a fixed
period of time. Trout tests use a 96 hour exposure regime while Daphnia tests run for 48
hours. In both tests, the number of organisms which have died would be the measured
parameter. The LC50 or the estimated concentration of effluent that causes 50 % mortality
is generally used as the quantitative measure of toxicity. Non-lethal effluents are
considered less likely to produce adverse impacts in the environment after dilution.

The Organic Chemical Manufacturing Sector Regulation required dischargers to collect
information on their operations, and monitoring data from their effluents, and to provide
this information to the Ministry. The timing of toxicity sampling was arranged to coincide
with chemical characterization, also required under this regulation. The frequency of
sampling was monthly for both toxicity test procedures on process effluents with the
exception that if tests over three consecutive months showed insignificant mortalities with
trout then in subsequent months a single concentration test may be used. For cooling
water effluent, the required frequency of sampling and testing was quarterly. All acute
lethality testing was conducted according to Ministry protocols (Protocol To Determine
The Acute Lethality Of Liquid Effluents To Fish. Env. Ontario July 1983 and Daphnia
magna Acute Lethality Toxicity Test Protocol. Env.Ontario April 1988).

The Organic Chemical Manufacturing Sector effluent acute toxicity monitoring originated
sample results submitted for 58 sampling locations at a total of 27 companies. For the first
six months of monitoring, starting in October 1989 and ending March 1990, 572 trout and
Daphnia toxicity test results were submitted by the companies, and 54 audit tests were
conducted by the Aquatic Toxicity Unit of Environment Ontario. BASF Canada Inc.
(Arnprior), Du Pont Canada Inc. (Whitby), Guardsman Products (Cornwall), Morbern
Chemicals (Cornwall), and Rohm and Haas Canada Inc. (Scarborough) were all brought
under monitoring through regulation amendments after the initial promulgation date.
Therefore, there were limited samples to review for these companies. BASF Canada Inc.
(Sarnia), Courtaulds Fibres Canada (Cornwall), Du Pont Canada Inc. (Corunna and
Maitland) and Esso Chemical Canada Ltd. (Sarnia) voluntarily submitted test results for
tests conducted on intake water samples.

Of the 308 samples that were tested for acute toxicity to trout, 248 (80.5 %) were not
acutely lethal. The effluent samples collected from 10 (37 %) companies were consistently
non-acutely lethal. All the samples collected from cooling water discharges or from intake
supplies were non-acutely lethal to trout. Companies included in this category are : AKZO
Chemicals Ltd. (Sarnia), BASF Canada Inc.(Sarnia), Celanese Canada Inc. (Millhaven), Du
Pont (Whitby), Esso Chemical Canada (Sarnia), Ethyl Canada Inc. (Corunna), Morbern
Inc. (Cornwall), Novacor Chemicals Ltd. (Mooretown), Rohm & Haas Canada Inc.
(Morrisburg) and Stepan Canada Inc. (Longford Mills). An additional 27 samples, 8.8 %
of total, resulted in LC50s > 100 %. Many of these tests had only one fish die during the
tests and might be interpreted as being not acutely lethal. Nine companies had one or
more test result with a LC50 > 100 %. This category included the following companies :
Amoco Canada Petroleum Canada Ltd. (Sarnia), B.F.Goodrich Canada Inc.( Thorold),
BTL Specialty Resins (Belleville), Canadian Oxy Chemicals Ltd. (Fort Erie), Chinook
Chemicals Company (Sombra), Dow Chemical Inc. (Sarnia), Du Pont Canada
Inc.(Corunna), Du Pont Canada Inc.(Maitland) and Uniroyal Chemical Ltd. (Elmira).

Thirty-three samples, 10.7 % of the total number of samples tested, were determined to

have been acutely-lethal to trout (96 hour LC50 <100 %). All the lethal samples were
collected from 5 companies (19 % of total companies). This category included the
following companies: Cornwall Chemicals Limited (Cornwall), Courtaulds Fibres Canada
(Cornwall), Du Pont Canada Inc. (Kingston), GE Plastics Canada Ltd. (Coburg) and
Polysar Ltd. (Sarnia). Polysar Ltd. had only one lethal effluent sample during the first six
months of monitoring, while the other plants’ process effluents were lethal the majority of
the time when sampled. The most lethal samples were sampled from Courtaulds Fibres
Canada (Cornwall), where the 96 hour LC50s ranged from 1 % to 61 %.

Of the 328 samples tested for acute toxicity to Daphnia magna, 198 samples (60.4 %)
were determined to have been non-acutely lethal. The effluents from AKZO Chemicals
Ltd., B.F.Goodrich Canada Inc., BASF Canada Inc., Canadian Oxy Chemicals Ltd., and
Novacor Chemicals Ltd. were not acutely lethal to Daphnia. An additional 69 samples
(21.2 %) had 48 h LC50s >100 %. Many of these samples had only one neonate die
during the test, and might be interpreted as being not acutely lethal. Fourteen samples
elicited an unusual toxicity response, in which the effluent became more toxic when it was
diluted.

Fifty-one of the 328 samples (15.5 %) were acutely toxic to Daphnia, generating 48 h
LC50s <100 %. All the lethal samples were from ten companies, and 36 of 51 toxic
samples were from four companies (Courtaulds Fibres Canada, Cornwall Chemicals Ltd.,
and Du Pont Canada Inc. plants in Kingston and Maitland). The effluents from Courtaulds
Fibres Canada process outfalls #100 and #300 were consistently among the most toxic
in this sector. The LC50 values for these outfalls range from 0.9 % to 7.6 % effluent. The
cause of toxicity is partially due to the extremes in pH found at these outfalls. Process
effluent #100 consistently has a pH < 2, and process effluent # 300 consistently has a
p> 2!

For several of the toxic samples, a quick review of the matching analytical chemistry
monitoring data has revealed some probable causes of the observed acute toxicity.
Where this was possible, a brief explanation to the probable causes of toxicity has been
described below. However for some effluent samples, which were consistently lethal, such
as the effluents from Uniroyal, and Dupont Kingston, the causes of toxicity were not as
conclusive, and will need the complete year of monitoring data before an assessment can
be made. It is clear that Courtaulds Fibres effluent toxicity is associated with the effluents
extreme pH conditions, and a mixture of several other toxic contaminants. One effluent
was consistently measured to have a pH reading of 1.4, and another discharge was
measured at 11.8. Water exhibiting a pH in the range between 6.5 and 8.5 is normally
considered of good quality for fish health. In addition to the extreme pH conditions of
Courtaulds effluent samples, which alone could have accounted for the observed
mortalities, the bioassay fish were challenged also by high concentrations of sulphide,
zinc, lead, nickel and mercury. These contaminants were consistently measured in
Courtaulds’ effluent at lethal or sublethal concentrations. Cornwall Chemical’s process

effluent samples were consistently lethal to both trout and Daphnia. On the days where
the effluent was lethal, high concentrations of sulphide and carbon tetrachloride were
measured. Sulphide and carbon tetrachloride concentrations reached as high as 15 ppm
and 20 ppm respectively. It is probable the hydrogen sulphide and carbon tetrachloride
content in the effluent contributed to the observed lethality. Of all the intake water samples
tested, only one source proved lethal. The Dupont Maitland intake samples for the months
of November, January and February were determined to have been lethal to Daphnia
and/or trout. The lethality is believed to have been caused by the high residual chlorine
content. This is consistent with Dupont’s practice of chlorinating their intake water prior
to use. Dupont Maitland discharge water was also determined to have been lethal for the
October and November samples. The effluent toxicity was due in part to the elevated
levels of copper, zinc and ammonia. The combined process effluent samples from GE
Plastics, Coburg were found to have been consistently lethal to test fish and not lethal to
the Daphnia magna. High concentrations of cyanide and ammonia were measured in the
effluent when lethality occurred, and could be considered as contributing factors to
toxicity. Daphnia, like invertebrates in general, are less sensitive to ammonia and cyanide.
This would account for the different observed effects between the two test species.

In general, the reporting of toxicity data by the industries went smoothly. The quality of
the toxicity results and presentation has been good. Where the Ministry requested
industry for data resubmission to correct data entry errors and/or for additional
information, the companies complied favourably. Where Ministry audit samples were
collected and tested, the results were consistent with results submitted by industry. The
following portion of this report presents the acute lethality data as submitted by industry,
grouped by company. A summary of each company’s results precedes each grouping
of individual results. The comment fields on individual Toxicity Test Reports were entered
by the industry’s laboratory performing the tests, and should not be expected to be
consistent across samples and do not represent the views of the Ministry.

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COMPANY : AKZO Chemicals Ltd., Sarnia

(28690006)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

The data for three trout bioassays, conducted on cooling
water samples collected between October 1989 and March
1990, were provided by AKZO Chemicals Ltd. All three
cooling water samples were determined to have been
non-acutely lethal to test fish. An additional audit sample
collected in December from the cooling water effluent was
tested by the O.M.E. laboratory and was determined to have
been non-acutely lethal.

OT cooling water

03890235 sampled: 10/28/89 non-lethal
95% fid. Limits: 0.0 - 0.0 %
comments:

05890121 sampled: 11/22/89 non-lethal
95% fid. limits: 00 = 0.0 %
comments:

01890285 sampled: 12/07/89 non-lethal
95% fad. limits: 0.0 - 0.0 %
comments: MISA audit sample.

05900028 sampled: 02/07/90 non-lethal
S5af1d. limits: 070 — 0.0 "3
comments:

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COMPANY : AKZO Chemicals Ltd., Sarnia
(28690006)
SECTOR: Organic Chemical
REGION: Southwest
SUMMARY

Data for three Daphnia magna acute lethality toxicity
tests conducted on samples of once through cooling water
collected between October 1989 and March 1990 were

submitted by AKZO Chemica

ls Ltd. of Sarnia.

Two samples

were not acutely lethal to Daphnia, and one sample had one

animal die in the 100% concentration during the test.

One

sample of this effluent was tested in the Ministry
It was not acutely lethal to

laboratory in December.
Daphnia.

OT cooling water

03890235 sampled: 10/28/89 non-lethal
95% fid. limits: 0-0) = 0.10 5
comments:

05890121 sampled: 11/22/89 non-lethal
95% fid. limits: 0.0 - O0 SF
comments:

02890285 sampled: 12/07/89 non-lethal
95% £fid. limits: 0.0 - 0-0 %
comments: MISA Audit

05900028 sampled: 02/07/90 non-lethal
95% Fides limits: 0.0 - 0.0 %
comments:

OT cooling water
storm water
storm water
rain gauge

intake water

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COMPANY : Amoco Canada Petroleum Canada Ltd., Sarnia

(104330204)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

The data for two trout bioassays, conducted on storm water
samples collected between October 1989 and March 1990, were
provided by Amoco Canada Petroleum Canada Limited. One
storm water sample had a 96 hour LC50 > 100 %, while the
other sample was determined to have been non-acutely lethal
to test fish.

Storm Water

03900087 sampled: 02/07/90 LE503, S100, «3%
95% fid. limits: 0.0 - 0.0 %
comments: LC50 >100

03900190 sampled: 03/12/90 non-lethal
95% Lid. Limits: 0.0 - DONS

comments: Non lethal
Emergency Overflow
Emergency Overflow
Storm Water
Batch Discharge Effluent

Batch Discharge Effluent

13

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COMPANY : Amoco Canada Petroleum Canada Ltd., Sarnia

(104330204)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

The monitoring regulation did not come into force until
February 1990 for Amoco Canada Petroleum Ltd. of Sarnia.
This company has submitted data for two Daphnia magna acute
lethality toxicity tests conducted on samples of effluent
from storm water outfall #100. Both samples were not
acutely lethal to Daphnia.

Storm Water

03900087 sampled: 02/07/90 non-lethal
95% fid.. Limites! 0.0 - 050 %
comments: Non lethal

03900190 sampled: 03/12/90 non-lethal
95% fid: limits: 0.0 - 0:05

comments: Non lethal
Emergency Overflow
Emergency Overflow
storm Water
Batch Discharge Effluent

Batch Discharge Effluent

47

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COMPANY : BF: Goodrich Canada Inc., Thorold

(370304)
SECTOR: Organic Chemical
REGION: West Central

SUMMARY

The data for six trout bioassays, conducted on combined
effluent samples collected between October 1989 and March
1990, were provided by B.F.Goodrich Canada Incorporated.
All six combined effluent samples were determined to have
been non-acutely lethal to test fish. An additional audit
sample collected from this combined discharge in November
was tested by the O.M.E. laboratory and was also determined
to have been non-acutely lethal.

combined effluent

08890442 sampled: 10/18/89 non-lethal
952 fid. limits: 0.0 - 0.0 3%
comments:

08890472 sampled: 11/16/89 non-lethal
95% fid.. Limits: 0.0 - 0.0 %
comments:

01890277 sampled: 11/29/89 non-lethal
95%) fad. Lamaiits': 0.0 - 0.0 %
comments: MISA audit sample.

08890512 sampled: 12/19/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

08900061 sampled: 01/24/90 LESo0%s) S100 F
95% fid. limits: 0.0 - 0.0 %
comments:

08900101 sampled: 02/12/90 non-lethal
953. fid limits: 0.0 - 0.0 %
comments:

08900211 sampled: 03/12/90 non-lethal
95% £1di. limits: 0.0 - 0.0 &

comments:

2A

B.F. Goodrich Canada Inc. (continued)

waste site
rain gauge

intake water

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COMPANY : B.F. Goodrich Canada Inc., Thorold

(370304)
SECTOR: Organic Chemical
REGION: West Central

SUMMARY

Data for six Daphnia magna acute lethality toxicity
tests conducted on samples of combined effluent collected
between October 1989 and March 1990 have been submitted by
B.F. Goodrich Canada Inc. of Thorold. Two samples were not
acutely lethal to Daphnia and four other samples have LC50s
greater than 100%. One sample of combined effluent was
tested in the Ministry laboratory in November. This sample
had one mortality in the 100% test concentration.

combined effluent

08890444 sampled: 10/18/89 LESOs S100 +
95% fid. limits: 0.0 - 0.0 %
comments:
08890474 sampled: 11/16/89 non-lethal
95% fid. limits: 0.0 - 0:30 “%
comments:
02890277 sampled: 11/22/89 non-lethal
95% £id. lamits: 0.0 - ONO. S
comments: MISA Audit/high conductivity
08890511 sampled: 12/19/89 LeS0:) S100 5
95% fid. limits: 0.0 - OS O7S
comments:
08900062 sampled: 01/24/90 LEso0e) S100 %
95% fid. limits: 0.0 - 0.50%
comments:
08900102 sampled: 02/12/90 LES50: | >100 4
9S$efid.t limits: 0.0 - 0.0 %
comments:
08900212 sampled: 03/12/90 non-lethal
95% fid.. limits: 0.0 - 0. 0S
comments:

31

B.F. Goodrich Canada Inc. (continued)

waste site
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intake water

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COMPANY : BASF Canada Inc., Sarnia

(740407)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

The data for six trout bioassays, conducted on cooling
water and intake water samples collected between October
1989 and March 1990, were provided by BASF Canada
Incorporated. Cooling water samples from both discharge
locations, control points 0100 and 0200, were non-acutely
lethal to test fish. Intake water samples were also
determined to have been non-acutely lethal.

OT cooling water

05890108 sampled: 11/15/89 non-lethal
95% fid. Limits: 0.0 - 0.0 %
comments:

05900033 sampled: 02/13/90 non-lethal
95% fid. limits: 0.0 - 0.0 +
comments:

OT cooling water

05890107 sampled: 11/15/89 non-lethal
95% tid. Jamits: 0.0 - 0.0 %
comments: D

05900034 sampled: 02/13/90 non-lethal
95% f1d. limits: 0.0 - OcO0FS
comments:

rain gauge

intake water

05890106 sampled: 11/15/89 non-lethal
953 t1d. limits: 0.0 - Os Os
comments:

05900031 sampled: 02/13/90 non-lethal
95%, id. (limits: 0.0 - 0.0 %
comments:

41

BASF Canada Inc. (continued)

42

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COMPANY : BASF Canada Inc., Sarnia

(740407)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

Data for six Daphnia magna acute lethality toxicity tests
conducted on samples of intake water and once through
cooling water (outfalls #100 and 200) collected between
October 1989 and March 1990 have been submitted by BASF
Canada Inc. of Sarnia. Samples from the intake water and
once through cooling water #100 were all not acutely lethal
to Daphnia. One sample from once through cooling water
#200 was nonlethal and the other sample had an LC50 greater
than 100%.

OT cooling water

05890108 sampled: 11/15/89 non-lethal
95% fad. limits: 0.0 - 0.0 %
comments:

05900033 sampled: 02/13/90 non-lethal
95% fid. limits: 0.0 = 0.0 %
comments:

OT cooling water

05890107 sampled: 11/15/89 non-lethal
95% fid. J1imits: 0.0 - 0.0 %
comments:

05900034 sampled: 02/13/90 HES0: + >100 - >
95% id. lamits: 0.0 - 0.0 %

comments:
rain gauge

intake water

05890106 sampled: 11/15/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05900031 sampled: 02/13/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

49

BASF Canada Inc. (continued)

50

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COMPANY : BASF Fibres Inc., Arnprior

(740209)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

Acute toxicity monitoring requirement for BASF Fibres
Incorporated was initiated July 31, 1990 therefore no acute
toxicity results have been submitted for the period between
October 1989 and March 1990.

57

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COMPANY : BASF Fibres Inc., Arnprior

(740209)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

Toxicity monitoring for BASF Fibres Inc. of Arnprior
was initiated on July 31, 1990 therefore no data for samples
have been submitted for the period October 1989 to March 1990.

59

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COMPANY : BTL Specialty Resins, Bellville

(1860006)

(now with Bellville Plant)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

The data for twelve trout bioassays, conducted on combined
effluent samples collected between October 1989 and March
1990, were provided by BTL Specialty Resins. All six
samples collected from the combined effluent discharge,
control point 0100, were determined to have been
non-acutely lethal to test fish. One sample from the
combined effluent discharge, control point 0200, had a 96
hour LC50 > 100 %, while the remaining five samples from
this source were determined to have been non-acutely
lethal. An audit sample collected in January from control
point 0100 was tested by O.M.E. laboratory and was
determined to have been non-acutely lethal. An audit sample
collected in January from control point 0200 had a 96 hour
LC50 > 100 %. BTL ceased operation on March 31, 1990 and
site decommissioning is currently underway.

combined effluent

03890214 sampled: 10/10/89 non-lethal
95% fid. Limits: 0.0 - 0.0 %
comments: Non lethal

03890252 sampled: 11/08/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal

03890353 sampled: 12/12/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal

03900023 sampled: 01/09/90 non-lethal
95% fid. Tlinits: 0.0 - 0.0 %
comments: Non-lethal

01900007 sampled: 01/23/90 non-lethal
95%-f 1d. 7limits: 0.0 - 0.0 %
comments: MISA audit sample.

03900100 sampled: 02/06/90 non-lethal
95% fid.. limits: 0.0 - 0207 %
comments: Single Concentration Test

03900202 sampled: 03/13/90 non-lethal
953. fia limaes': 0.0 - 0.0 %

comments: Single concentration test; non-lethal
61

BTL Specialty Resins (continued)

combined effluent

03890215 sampled: 10/10/89 non-lethal
95% id: Limits: 0.0 - 0.0 %
comments: Non lethal
03890251 sampled: 11/08/89 non-lethal
95% fid. Limits: 0.0 - DONS
comments: Non-lethal
03890354 sampled: 12/12/89: non-lethal
95% fid. limits: 0::0:, = 0.0 %
comments: Non-lethal
03900024 sampled: 01/09/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal
01900008 sampled: 01/23/90 LCS50:, 2100: %
95% fid. limits: 0.0 - 0.0 %
comments: MISA audit sample.
03900101 sampled: 02/06/90 ÉCS50: >100 %
95% fid. limits: 0.0 = 0.0 %
comments: Single Concentration Test
03900203 sampled: 03/13/90 non-lethal
95% fid. limits: 0.0 - 0.0 %

comments: Single concentration test; non-lethal

rain gauge

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COMPANY : BTL Specialty Resins, Bellville

(1860006)

(now with Bellville Plant)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

Results from twelve Daphnia magna acute lethality
toxicity tests conducted on samples of combined effluent
(outfalls #100 and 200) collected between October 1989 and
March 1990 were submitted by BTL Specialty Resins of
Belleville. Three of six samples from combined effluent
#100 were not acutely lethal to Daphnia. The remaining
three samples had LC50 values greater than 100%. The
sample collected in October had the greatest mortalities in
the middle concentrations of effluent.

Three samples of combined effluent #200 were not
acutely lethal to Daphnia and the remaining three samples
had LC50 values greater than 100%.

One sample from each of these outfalls was tested in
the Ministry laboratory in January. The sample from
combined effluent #100 had one mortality in the 100% test
solution, and the sample from combined effluent #200 was
not acutely lethal to Daphnia.

BTL ceased operation on March 31, 1990 and site decommissioning
is currently underway.

combined effluent

03890214 sampled: 10/10/89 LC50: >1002 %
95% £id. limits: 0.0 - 0:05
comments: LC50 >100%

03890252 sampled: 11/08/89 LCS0: ~>100.7%
95% fid. limits: OO! = OOS
comments: Non-lethal

03890353 sampled: 12/12/89 non-lethal
95% fid. limits: 0.0 - 00
comments: Non-lethal

03900023 sampled: 01/09/90 EC5SO's >100 &%
95% fid. limits: 0.0 - 0.0 %
comments: LC50 >100

02900007 sampled: 01/23/90 LC50: >100). %
95% fid. limits: 0.0 - ©). 0%
comments: MISA Audit

03900100 sampled: 02/06/90 non-lethal
95% fid. limits: 0.0 - 0.0 %

comments: Non-lethal

TT.

BTL Specialty Resins (continued)
03900202 sampled: 03/13/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non lethal

combined effluent

03890215 sampled: 10/10/89 non-lethal
95% fid. limits: 0.0 = 0.0 %
comments: Non-lethal

03890251 sampled: 11/08/89 LESOS02S100
95% fid. ‘limits: 0.0 - 0.0 %
comments: LC50 >100

03890354 sampled: 12/12/89 non-lethal
95% id “limits: 0.0 - OO &
comments: Non-lethal

03900024 sampled: 01/09/90 LC50: >100
95% fid. limits: 0.0 - O'S0 8S
comments: LC50 >100

02900008 sampled: 01/23/90 non-lethal
95% fid. limits: 0.0 - 0:0 "+
comments: MISA Audit

03900101 sampled: 02/06/90 LC50: 5100
95% fid. limits: 0.0 - 0.0 %
comments: LC50 >100

03900203 sampled: 03/13/90 non-lethal
95% fid. limits: 0.0 - 0.0 %

comments: Non lethal
rain gauge

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COMPANY : Canadian Oxy Chemicals Ltd., Fort Erie

(1590009)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

The data for two trout bioassays, conducted on two cooling
water samples collected between October 1989 and March
1990, were provided by Canadian Oxy Chemicals Limited. One
cooling water sample had a 96 hour LC50 > 100 %, while the
second sample was determined to have been non-acutely
lethal to test fish. An audit sample collected in November
from the cooling water discharge was tested by O.M.E.
laboratory and was determined to have been non-acutely
lethal.

OT cooling water

03890310 sampled: 11/27/89 LESOs, S100 <3
95% fid. limits: O40 = 0.0 %
comments: LC50 >100%
01890276 sampled: 11/29/89 non-lethal
95% fid. limits: 0.0 = 0.0%
comments: MISA audit sample.
03900110 sampled: 02/12/90 non-lethal
95% fad: limits: 0.0 - 0.0 %

comments: Single Concentration Test - Non Lethal
rain gauge

intake water

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COMPANY : Canadian Oxy Chemicals Ltd., Fort Erie

(1590009)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

Results of two Daphnia magna acute lethality toxicity
tests conducted on samples of once through cooling water
collected between October 1989 and March 1990 were
submitted by Canadian Oxy Chemicals Ltd. of Fort Erie.
Both samples were not acutely lethal to Daphnia. One
sample tested in the Ministry laboratory in November was
also not acutely lethal to Daphnia.

OT cooling water

03890310 sampled: 11/27/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal

02890276 sampled: 11/29/89 non-lethal
95% fid. limits: 0.0 - 00%
comments: MISA Audit

03900110 sampled: 02/12/90 non-lethal
95% fid. limits: 0.0 - 0.0 %

comments: Single Concentration Test
rain gauge

intake water

97

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eluydeg vSIW

COMPANY : Celanese Canada Inc., Millhaven

(1730001)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

The data for eighteen trout bioassays, conducted on
combined effluent samples collected between October 1989

and March 1990, were provided by Celanese Canada

Incorporated. All six combined effluent samples collected
from control point 0100 were determined to have been
non-acutely lethal to test fish. An audit sample collected
from control point 0100 in December was tested by O.M.E.

laboratory and it too was determined to have been
non-acutely lethal. Five combined effluent samples

collected from control point 0200 were determined to have
been non-acutely lethal. One sample from this discharge had
a 96 hour LC50 > 100 %. An audit sample collected from
control point 0200 in December was determined to have been
non-acutely lethal. All six combined effluent samples
collected from control point 0300 were determined to have
been non-acutely lethal. An audit sample collected in
December from this discharge was also determined to have

been non-acutely lethal by the O.M.E. laboratory.

combined effluent

06890944 sampled: 10/01/89 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT
06891047 sampled: 11/06/89 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT
06891173 sampled: 12/04/89 non-lethal

95% (£10. .Limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT
01890288 sampled: 12/11/89 non-lethal

95% fid., Limits: 0.0 - 0.0 %

comments: MISA audit sample.
06900097 sampled: 01/16/90 non-lethal

95% fid. limits: 0.0 - 00%

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT
06900224 sampled: 02/05/90 non-lethal

95%. £10. Limits’: 0.0 — 0 «DT

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT

101

OBSERVED

OBSERVED

OBSERVED

OBSERVED

OBSERVED

Celanese Canada Inc. (continued)
06900335 sampled: 03/04/90 non-lethal
95% fid. limits: 0.0: = 020.25
comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED

combined effluent

06890946 sampled: 10/01/89 non-lethal

95% “fra. limits: 0.0 - 0.0%

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
06891045 sampled: 11/06/89 non-lethal

95% fid. limits: OO 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
06891171 sampled: 12/04/89 E50 S100?

95% fid. limits: 0.0 - 0.0 %

comments: 10% MORTALITY IN FULL STRENGTH EFFLUENT
01890286 sampled: 12/11/89 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: MISA audit sample.
06900099 sampled: 01/16/90 non-lethal

95% fid. limits: 0.0 = OO

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
06900226 sampled: 02/05/90 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
06900337 sampled: 03/04/90 non-lethal

95% fid. limits: O70: 7— 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED

combined effluent

06890948 sampled: 10/01/89 non-lethal

954. fide. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
06891049 sampled: 11/06/89 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
06891175 sampled: 12/04/89 non-lethal

95% fid. limits: 0.02 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
01890287 sampled: 12/11/89 non-lethal

95%? fid.. dimes: 0.0 - ONDES

comments: MISA audit sample.
102

Celanese Canada

06900101 sampled:
95% fid. limits:

comments: NO MORTALITY OR

06900228 sampled:
95% fid. limits:

comments: NO MORTALITY OR

06900339 sampled:
95% fid. limits:

comments: NO MORTALITY OR

process effluent
emergency overflow
storm water

rain gauge

intake water

Inc. (continued)

non-lethal
OS OT
SUBLETHAL IMPAIRMENT OBSERVED

non-lethal
OO °3
SUBLETHAL IMPAIRMENT OBSERVED

non-lethal

0.0 %
SUBLETHAL IMPAIRMENT OBSERVED

103

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Millhaven

COMPANY : Celanese Canada Inc.,
(1730001)
SECTOR: Organic Chemical
REGION: Southeast
SUMMARY

Results for eighteen Daphnia magna acute lethality

toxicity tests conducted on samples collected from three

combined effluent outfalls between October 1989 and March
1990 were submitted by Celanese Canada Inc. of Millhaven.
The six samples from combined effluent #100 were not

acutely lethal to Daphnia.

Five samples from combined

effluent #200 were not acutely lethal to Daphnia and a
sixth sample had one mortality in the 100% effluent

concentration.

were also nonlethal to Daphnia.
Tests conducted in the Ministry laboratory in December

on samples of effluent for all three outfalls indicated

that the effluents were nonlethal at this time.

combined effluent

06890945 sampled: 10/01/89
95% fid. limits: 0.0 -
comments: NO MORTALITY OR

06891048 sampled: 11/06/89
95% fid. limits: 0.0 -
comments: NO MORTALITY OR

06891174 sampled: 12/04/89
95% t1d- limits: 0.0 -
comments: NO MORTALITY OR

02890288 sampled: 12/11/89
95% fid. limits: 0.0
comments: MISA Audit

06900098 sampled: 01/16/90
95% -fid:. limits: 0.0
comments: NO MORTALITY OR

06900225 sampled: 02/05/90
95% fid. limits: 0.0 -
comments: NO MORTALITY OR

06900336 sampled: 03/04/90
953efiide waimaresis O0 =
comments: NO MORTALITY OR

non-lethal
0.0 &
IMMOBILITY OBSERVED

non-lethal
0.05%
IMMOBILITY OBSERVED

non-lethal
0.0 %
IMMOBILITY OBSERVED

non-lethal
OO &

non-lethal
0.0 %
IMMOBILITY OBSERVED

non-lethal
OW 0's
IMMOBILITY OBSERVED

non-lethal

0.0 %
IMMOBILITY OBSERVED

125

IN

IN

IN

IN

IN

IN

48

48

48

48

48

48

All six samples from combined effluent #300

HRS

HRS

HRS

HRS

HRS

HRS

Celanese Canada Inc. (continued)
combined effluent

06890947 sampled: 10/01/89 LeCSO 2100 8%

95% fid. limits: 0.0 - 0.0 %

comments: 10% MORTALITY IN FULL STRENGTH EFFLUENT
06891046 sampled: 11/06/89 non-lethal

95% fid. limits: (BJ ES 0.0 %

comments: NO MORTALITY OR IMMOBILITY OBSERVED
06891172 sampled: 12/04/89 non-lethal

95% fid. limits: 0.0" = 0.0 %

comments: NO MORTALITY OR IMMOBILITY OBSERVED
02890286 sampled: 12/11/89 non-lethal

95% fid. limits: O0 0.0 %

comments: MISA Audit
06900100 sampled: 01/16/90 non-lethal

95014. Limits: OO 00 4

comments: NO MORTALITY OR IMMOBILITY OBSERVED
06900227 sampled: 02/05/90 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR IMMOBILITY OBSERVED
06900338 sampled: 03/04/90 non-lethal

953"f1d. Limits’ 0% Or— 0.0 %

comments: NO MORTALITY OR IMMOBILITY OBSERVED

combined effluent

06891050 sampled: 11/06/89
95% fid. limits: 0.0 -
comments: NO MORTALITY OR

06891176 sampled: 12/04/89
95% fid: limits: 0.0 -
comments: NO MORTALITY OR

02890287 sampled: 12/11/89
95% fid. limits: 0.0 -
comments: MISA Audit

06900102 sampled: 01/16/90
95%) £10)... limits: 02:0" =
comments: NO MORTALITY OR

06900229 sampled: 02/05/90
95% fad: Limits: 0.0 -
comments: NO MORTALITY OR

non-lethal
0.0 +
IMMOBILITY OBSERVED

non-lethal
0.0 %
IMMOBILITY OBSERVED

non-lethal
0.0 +

non-lethal
0.0 %%
IMMOBILITY OBSERVED

non-lethal
020 uz
IMMOBILITY OBSERVED
126

IN

IN

IN

IN

IN

IN

IN

IN

IN

48

48

48

48

48

48

48

48

48

HRS

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HRS

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HRS

HRS

HRS

HRS

Celanese Canada Inc. (continued)
06900340 sampled: 03/04/90 non-lethal
95% fid., Limits: 0.0 — 0.10 3
comments: NO MORTALITY OR IMMOBILITY OBSERVED IN 48 HRS
process effluent
emergency overflow
storm water

rain gauge

intake water

P27

gel

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COMPANY : Chinook Chemicals Company, Sombra

(5600002)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

The data for six trout bioassays, conducted on combined
effluent samples collected between October 1989 and March
1990, were provided by Chinook Chemicals Company. Five of
six combined effluent samples were determined to have been
non-acutely lethal to test fish. The remaining sample
produced a 96 hour LC50 of >100 %.

combined effluent

03890220 sampled: 10/17/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal

03890289 sampled: 11/21/89 LC50: >100 %
95% fid. Limits: 0.0 - 0.0 %

comments: Non lethal

03890379 sampled: 12/19/89 non-lethal
95% fid. Limits: 0.0 - O20 %
comments: Non-lethal

03900065 sampled: 01/23/90 non-lethal

95% fF1d: limits: 0.0 - 0.0 %

comments: Single Concentration Test
03900131 sampled: 02/20/90 non-lethal

95% fid. limits: 00 — 0.0 %

comments: Single Concentration Test--Non-lethal
03900221 sampled: 03/20/90 non-lethal

953 £1d).,-limits: 0.0 — 0.0 %

comments: Single Concentration Test; Non-lethal
emergency overflow
rain gauge

intake water

149

Chinook Chemicals Company (continued)

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COMPANY: Chinook Chemicals Company, Sombra

(5600002)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

Results for six Daphnia magna acute lethality toxicity
tests conducted on samples of combined effluent collected
between October 1989 and March 1990 were submitted by
Chinook Chemicals Company of Sombra. The toxicity of the
effluent samples was variable. Three samples were not
acutely lethal to Daphnia, two samples had LC50s greater
than 100%, and one sample had an LC50 of 17.1%.

combined effluent

03890220 sampled: 10/17/89 LCSOss >100 .+
95% £1d. limits: 0.0 - 0.0 %
comments: Non-lethal

03890289 sampled: 11/21/89 non-lethal
95% fid. limits: 00 = 0.0 %
comments: Non-lethal

03890379 sampled: 12/19/89 LESC: 3 1er A0 es
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comments: Lethal

03900065 sampled: 01/23/90 LCSOs “S100° +
95% fid. limits: 0.0 - 0.0 %
comments: LC50 >100

03900131 sampled: 02/20/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non lethal

03900221 sampled: 03/20/90 non-lethal

95% Lid. limits: 0.0 - OZOLE
comments: Non lethal

emergency overflow
rain gauge

intake water

157

Chinook Chemicals Company (continued)

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COMPANY : Cornwall Chemicals Limited, Cornwall

(33050006)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

The data for seven trout bioassays, conducted on process
effluent samples collected between October 1989 and March
1990, were provided by Cornwall Chemicals Limited. Four of
the samples, collected from control point 0100, were
determined to have been acutely lethal to test fish.
Statistically, the percentage effluent required to kill 50
% of the test fish by the end of the four days exposure
were 57.0 % (October), 80.6 % (December), 16.7 % (January),
and 84.4 % (February). The remaining three samples were
determined to have been non-acutely lethal to test fish.

process effluent

06890964 sampled: 10/02/89 LC50: SOS

95% id. 1imits: 65.01 = 50.10%

comments: pH DECREASED IN 50&65% CONC. DURING 72896 HRS
06891053 sampled: 11/06/89 non-lethal

95% fid. Limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
06891181 sampled: 12/05/89 LC50: 80.6 %

953 fd). Jimits: 6533.0) <= 100.0: 3

comments: 100% MORTALITY IN FULL STRENGTH EFFLUENT
06900028 ‘sampled: 01/08/90 LC50: Gt 7b:

95% f14. lames: l'ONG TA 2s

comments: 70% MORTALITY IN 20% CONCENTRATION.
06900025 sampled: 01/08/90 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
06900220 sampled: 02/05/90 LC50: 84.4 %

95% fid. limits: 0.0 - 0.0 %

comments: 90% MORTALITY IN FULL STRENGTH EFFLUENT
06900343 sampled: 03/05/90 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED

165

Cornwall Chemicals Limited (continued)
rain gauge

intake water

166

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COMPANY : Cornwall Chemicals Limited, Cornwall

(33050006)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

Results for six Daphnia magna acute lethality toxicity
tests conducted on samples of process effluent collected
between October 1989 and March 1990 were submitted by
Cornwall Chemicals Limited of Sarnia. All six samples were
toxic to Daphnia with LC50 values ranging between 14 and
61% effluent.

process effluent

06890965 sampled: 10/02/89 ÉESO!: 39.40 4%

95% fid. limits: 202, 0F— 250510 2s

comments: 100% MORTALITY IN 50% CONCENTRATION
06891054 sampled: 11/06/89 LC50: 9373 €

95% fid. Limits: Diet = 178278). -%

comments: 60% MORTALITY IN FULL STRENGTH EFFLUENT
06891182 sampled: 12/05/89 LE50's 14,09 %

95% fid. limits: LVOSO— =20R0) 2%

comments: 100% MORTALITY IN 20% CONCENTRATION
06900028 sampled: 01/08/90 LC50: lé 7e

95% fid. limits: 1422 = 19:63

comments: 70 % MORTALITY IN 20 % CONCENTRATION
06900221 sampled: 02/05/90 LC50: 33.80%

95% fid. limits: 2995 <5 38.5 %

comments: 100% MORTALITY IN 50% TEST CONCENTRATION
06900344 sampled: 03/05/90 LESO:s 29.47%

95%. f4d., limits: 2545..= 33.9: 4%

comments: 60% MORTALITY IN 30% TEST CONCENTRATION
rain gauge

intake water

LED

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COMPANY : Courtaulds Fibres Canada, Cornwall

(1900000)

(now with Cornwall Plant)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

The data for thirty-eight trout bioassays, conducted on
effluent samples collected between October 1989 and March
1990, were provided by Courtaulds Fibres Canada. All twelve
samples of process effluent collected from control point
0100 and 0300 were determined to have been acutely lethal
to test fish. For samples collected from 0100,
statistically, the percentage effluent required to kill 50
% of the test fish by the end of the four days exposure
WEGeH 6s St ts 3:05, 03.091 57/4120, 4, 1.0.5 sand 2:05, For
samples collected from 0300, statistically, the percentage
effluent required to kill 50 % of the test fish by the end
of the four days exposure were 61.0 %, 8.8 %, 12.0 %, 14.1
%, 18.4 % and 12.6 %. All the samples collected from the
four combined effluent discharges were determined to have
been non-acutely lethal to test fish except for one sample.
The Ministry audit sample,collected in November from
combined effluent 0700, had a 96 hour LC50 of 53.0 %. Both
intake water samples were determined to have been
non-acutely lethal.

process effluent

03890221 sampled: 10/18/89 LC50: 6.673%
95% fia. Limits: 4.7 — 8.5 % slope: 5.5
comments:

01890269 sampled: 11/21/89 LC50: Dis 7 3S
95% fid. Jimits: 21 3,6
comments: MISA audit sample.

03890296 sampled: 11/22/89 ÉC50;: 3,10) 5%
953 £10. TIMIES: 1.9 - 4.6 % slope 3) 4
comments:

03890384 sampled: 12/19/89 LC50: 3.9 %
95% fid. limits: 2.6 - 5.26 1% Slopes Sia
comments:

03900041 sampled: 01/16/90 LC50: 12.0 %
95% fid. limits: 9.1 - 15.7 % slope: 549
comments:

03900162 sampled: 02/27/90 EC50)s 1.10,
95% fad. Jamas OO; As = 1.9 % slope Peel
comments:

183

Courtaulds Fibres Canada (continued)

03900228 sampled: 03/20/90 ECS Ol: 210
95% fid. limits: 1.2 = 3.1 % slope:
comments: Lethal

pr 200

03890227 sampled: 10/18/89 LC50: 25% 3
95% fid. limits: 18.8 = 33.9 % slope:
comments:

process effluent

03890222 sampled: 10/18/89 LC50': 61.0
95% fid. limits: 40.0 =~ 65.0" +
comments:

01890270 sampled: 11/21/89 LC50': Ses
95% fid. Wimies' 2 1 5.0 +
comments: MISA audit sample.

03890297 sampled: 11/22/89 LC50: 8.8
95% f£1id. limits: 6.8 = 11.4 % slope:
comments:

03890385 sampled: 12/19/89 LC50: 120
95% fid. limits: 9.1 = 15:7 % slope:
comments:

03900042 sampled: 01/16/90 LC50 V4.5 1
95% fid. limits: L0.0 — "20.0 %
comments: Lethal

03900163 sampled: 02/27/90 LC50 18.4
95% fid. limits: 13.7 - 24.6 % slope
comments:

03900229 sampled: 03/20/90 LC50 12.6
95% fid. “Limits: 9.4 —- “16.9 % slope
comments: Lethal

combined effluent

03890223 sampled: 10/18/89 non-lethal
95% fid. limits: 0.0 - 0.0%
comments: Non-lethal

03890298 sampled: 11/22/89 non-lethal
95% fid. limits: 0.0 - O0
comments: Non lethal

184

Courtaulds Fibres Canada (continued)

03890386 sampled: 12/19/89 non-lethal
95%, £2d.. limits: 0.0 = 0.0 %
comments: Non-lethal

03900043 sampled: 01/16/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal

03900164 sampled: 02/27/90 non-lethal
95% fid. limits: 0.0 - 0.0 3
comments: Single Concentration Test--Non-lethal

03900230 sampled: 03/20/90 non-lethal
95% fid,. Limits: 0.0 - 0.0 %

comments: Single Concentration Test; Non lethal

combined effluent

03890224 sampled: 10/18/89 non-lethal
95% £10. Limits: 0.0 - 0.0 %
comments: Non-lethal

03890299 sampled: 11/22/89 non-lethal
95% fid. limits: 0.0 - DONS
comments: Non lethal

03890387 sampled: 12/19/89 non-lethal
9535 fla limits: 0.0 = 0.0 %
comments: Non-lethal

03900044 sampled: 01/16/90 LES Oise > LOUE
95% £1d. limits: 0.0 - 0.0 %
comments: Single Concentration Test

03900165 sampled: 02/27/90 non-lethal
95% rad; Limits’ 0.0 - OL OMS
comments: Non-lethal

03900231 sampled: 03/20/90 non-lethal
95%, tid limits: 0.0 - 0.0 %

comments: Non lethal

combined effluent

03890225 sampled: 10/18/89 non-lethal
95% fid. limits: 0.0 - OOS
comments: Non-lethal

01890273 sampled: 11/21/89 EES O's 5301s
95% fid. limits: 36 B Hs WOeAas

comments: MISA audit sample.
185

Courtaulds Fibres Canada (continued)

03890300
95% fid. limits:
comments: Non lethal

sampled: 11/22/89
0.0 —

03890388
95% fid. limits:
comments: Non-lehtal

sampled: 12/19/89
0.0

03900045
95% fid. limits:
comments: Non-lethal

sampled: 01/16/90
OO x=

03900166
95% fid. limits:

sampled: 02/27/90
0.0 =

comments: Single Concentration Test--Non-lethal

non-lethal
0.0 %

non-lethal
0.0 %

non-lethal
0.0 %

non-lethal
0.0 %

non-lethal

03900232 sampled: 03/20/90
95% fid. limits: 0.0 = 0.0 %
comments: Single Concentration Test; Non lethal

combined effluent

03890226 sampled: 10/18/89 non-lethal
95%. F1d.linits: 0.0 - 0.0 %
comments: Non-lethal

03890301 sampled: 11/22/89
95% fid. limits: 0.0 - OÙ
comments: Non lethal

03890389 sampled: 12/19/89
95% fid. limits:
comments: Non-lethal

non-lethal
0.0 = 0.0 %

03900046 sampled: 01/16/90 non-lethal
95% fid. limits: 0.0 - 0.07
comments: Non-lethal

03900167 sampled: 02/27/90 non-lethal
95% fid. limits: 0.0 = 05:0. °%
comments: Single Concentration Test--NOn-lethal

03900233 sampled: 03/20/90 non-lethal

95% fid. limits: 0.0 = 0.0 3
comments: Single Concentration Test; Non lethal

186

Courtaulds Fibres Canada (continued)
rain gauge

intake water

03890302 sampled: 11/22/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non lethal

03890390 sampled: 12/19/89 non-lethal
95% fid. limits: 0.0 - 0.0 3

comments: Non-lethal

187

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COMPANY : Courtaulds Fibres Canada, Cornwall

(1900000)

(now with Cornwall Plant)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

Results for thirty-eight Daphnia magna acute lethality
toxicity tests conducted on effluent samples collected
between October 1989 and March 1990 were submitted by
Courtaulds Fibres Canada of Cornwall. The samples from the
various outfall points of this plant were either very
toxic, or had low levels of acute toxicity. One sample of
intake water collected in December was nonlethal, and one
sample of storm water collected in October had an LC50 of
8.8%.

Sixteen of seventeen samples from combined effluents
#500, 600 and 800 were either not acutely lethal to Daphnia
(29% of samples) or had less than 4 test animals die during
any one test. One sample from combined effluent #600
collected in January was acutely lethal to Daphnia, with an
LC50 = 60.9%.

The samples from combined effluent #700 were more
variable than all the others from this plant. Three
samples were nonlethal, one sample had an LC50 > 100%, and
two samples had Lc50 values of 87.1 and 93.3%.

Samples from process effluents #100 and #300 are
consistently acutely toxic. All twelve samples from these
outfalls had LC50s < 8% effluent, and 11 of 12 samples had
LC50s < 4%. Much of the toxicity from these outfalls can be
attributed to the extremes in pH of the effluents. The acid
sewer (#100) effluent consistently has pH values of 2, and
the alkal sewer (#300) effluent consistently has pH > 11.5.
At these pH levels Daphnia are killed within the first hour
of exposure to 100% effluent concentrations.

Audit samples for combined effluents #100, 300, 500,
600, 700, and 800 were tested in the Ministry laboratory in
November. The results were consisent with those submitted
by the company.

process effluent

03890221 sampled: 10/18/89 LC50: Oh IF
O53. £1d% * limits’ 1.4 - 2.5 % slope: Sith
comments:

02890269 sampled: 11/21/89 LCSO: 00: St: OF Pat
S5S° £1 al) limits: 0.0 - ODOM

comments: MISA Audit/ low pH, rapidly lethal

2:31

Courtaulds Fibres Canada (continued)

03890296 sampled: 11/22/89 LC50:

95% fid. limits: 1.0 1.8 % slope:
comments:

03890384 sampled: 12/19/89 LC50:
95%sfid< iLimats: Les = 2.3 % slope:
comments:

03900041 sampled: 01/16/90 LC50:

95% fid. “limits: 5.8 - 9.8 + slope:
comments: Lethal

03900162 sampled: 02/27/90 LCSO!

95% £10. limits: 2.8 = 4.7 % slope:
comments:

03900228 sampled: 03/20/90 LC50:

95% fid.tWlimits: 1 lor 2.1 % slope:
comments:
pr 200

03890227 sampled: 10/18/89 LC50:

95% fid. limits: 6:7» =1 , 141.45 Saslope:
comments:
process effluent

03890222 sampled: 10/18/89 LC50:

95% tid. linits: RE 2.2 % slope:
comments:

02890270 sampled: 11/21/89 LC50:

95%, fid., damits: 0.5 = 7.8 %
comments: MISA Audit/high pH, low oxygen,

03890297 sampled: 11/22/89 LC50:

95% fid.. limits: 2.4 - 3.7 % slope:
comments:

03890385 sampled: 12/19/89 LC50:

95% fid. Mimits: 0.7 — 1.6 + ‘slope:
comments:

03900042 sampled: 01/16/90 LC50:

95% Fid.+-Linies: 0.4 - 1.56% (slopes
comments: Lethal

03900163 sampled: 02/27/90 LC50:

952 Lid.) Jamies: 1.5) = 33.0 %

comments:

1.74 %
4.7

2.0 %
rapidly leth.

3.0 %

Courtaulds Fibres Canada (continued)

03900229 sampled: 03/20/90 LC50: PROMS) Hi
953 fia: limits: 2.0 - 3.4 % slope: 641
comments:

combined effluent

03890223 sampled: 10/18/89 non-lethal
95% ride. damits: 0.0 - 0.0 %
comments: Non-lethal
02890272 sampled: 11/21/89 LE50: >100: oF
Os seid iiimastsic 0.0 - 01.0)-%
comments: MISA Audit
03890298 sampled: 11/22/89 non-lethal
95% fid. Limits: 0.0 - 0.0 %
comments: Non-lethal
03890386 sampled: 12/19/89 non-lethal
95% fid. limits: 0.0 - OS OS
comments: Non-lethal
03900043 sampled: 01/16/90 L503 © \SlLOORat
95% fid. limits: 0.0 - OO
comments: LC50 >100
03900164 sampled: 02/27/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal
03900230 sampled: 03/20/90 LE502' ci >100 8 4%
95% fid. Limits: 0.0 - O0

comments: LC50 >100

combined effluent

03890224 sampled: 10/18/89 non-lethal
953 fd. limits: On 0) = 0.0 %
comments: Non-lethal
02890268 sampled: 11/21/89 LE503) | .>1008 <%
95% -f£id. Limits: 0.0 - O0
comments: MISA Audit/several floaters in 100% & 60%
03890299 sampled: 11/22/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal
03890387 sampled: 12/19/89 LE50s 5) >100Kas
95% fid. limits: 0.0 - 0.0 %

comments: LC50 >100
233

Courtaulds Fibres Canada (continued)

03900044 sampled: 01/16/90 LCS50: 60.9 %
95% fid. ‘limits: 35.49 f= $103.0 -% Oslope: 220
comments: Lethal

03900165 sampled: 02/27/90 LC50: >100 2%

95% fid. limits: 0.0 - 0.0 %
comments: LC50>100

03900231 sampled: 03/20/90 LESO: S100 (4%

95% fid. limits: 0.0 - 0.0 -%

comments: LC50 >100

combined effluent

03890225 sampled: 10/18/89 non-lethal
95% fid. limits: 0.0 — 0.0 %
comments: Non-lethal

02890273 sampled: 11/21/89 LC50: 64.5 %
95% fid. limits: 51.9 7=9 «80.1 -F
comments: MISA Audit/

03890300 sampled: 11/22/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal

03900045 sampled: 01/16/90 LC50: 93.39
95% fid. limits: 66.2 °=-131.3"4Vsillope: 3.56
comments: lethal

03900166 sampled: 02/27/90 non-lethal
95% fid. limits: 0.0 0.0 %
comments: Non-lethal

03900232 sampled: 03/20/90 LESO0:v>100. 2%
95% fid. limits: 0.0 - ON O7

comments: LC50 >100

combined effluent

03890226 sampled: 10/18/89 LE50¢* \S10008%
95% fid. limits: 0.0 - O0... 0"
comments: Non-lethal

02890271 sampled: 11/21/89 non-lethal
95% fid. limits: 0.0 - 0.10" S
comments: MISA Audit

03890301 sampled: 11/22/89 LCSOSL \S100bms
95% fid. limits: 0.0 - 00%

comments: LC50>100
234

Courtaulds Fibres Canada (continued)

03890389 sampled: 12/19/89 non-lethal
95%, £id. Jaimi'ts!: 0.0 - 0.0 %
comments: Non-lethal
03900046 sampled: 01/16/90 ECS = STOO RE
95% fid. limits: 0.0 - 070 #3
comments: LC50 > 100
03900167 sampled: 02/27/90 LE50: « 2100. .%
95% tid limits: 0.0 - 0.06%
comments: LC50 >100
03900233 sampled: 03/20/90 LC50 >100 %
952) fad. limits: 0.0 - 0.0) 3
comments: LC50 >100
rain gauge
intake water
03890302 sampled: 11/22/89 non-lethal
95% fid. limits: 0.0 - 10/10) 8%
comments: Non-lethal
03890390 sampled: 12/19/89 LES50: ">100 ¢
95% id. limits: 0.0 - 0.0 3%

comments: LC50 >100

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COMPANY : Dow Chemical Canada Inc., Sarnia

(910109)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

The data for forty-three trout bioassays, conducted on
process effluent, combined effluent and once through
cooling water effluent samples collected between October
1989 and March 1990, were provided by Dow Chemical Canada
Incorporated. All six samples collected from combined
effluent control point 0200 were determined to have been
non-acutely lethal to test fish. One audit sample collected
in March and tested by the O.M.E. laboratory was also
non-acutely lethal. All six samples from combined effluent
control point 0500 were also non-acutely lethal. An audit
sample collected in March was also non-acutely lethal. All
six samples from combined effluent control point 0600 were
non-acutely lethal. The audit sample collected in March was
similiarily determined as non-acutely lethal. All six
samples collected from combined effluent 0700 were
determined to have been non-acutely lethal. The audit
sample collected in March was also non-acutely lethal. Five
of six samples from the combined effluent control point
0900 were determined to have been non-acutely lethal while
the remaining had a 96 hour LC50 > 100 %. The audit sample
collected in March was non-acutely lethal. All twelve once
through cooling water samples from control point 0300 and
1000 were non-acutely lethal. The two audit samples for the
two OTCW discharges were also non-acutely lethal. Four of
five process effluent samples collected from control point
2100 were determined to have been non-lethal. The remaining
sample and the audit sample collected in March had a 96
hour? -bC50s: > LOOL't.

intake water

combined effluent

03890206 sampled: 10/10/89 non-lethal
95% -fid. Aimits!: 100.10 —-100..10 &
comments:

03890256 sampled: 11/13/89 non-lethal
95% tfad. limits: 0.0 - 0.0 %
comments: Non lethal

03890359 sampled: 12/13/89 non-lethal
953 £10. lamits: 0.0 - 0.0 %

comments: Non lethal

281

Dow Chemical Canada Inc. (continued)

03900018 sampled: 01/09/90 non-lethal
95%. fid. limits: 0.0 - 0.0 %
comments: Non-lethal

03900111 sampled: 02/13/90 non-lethal
95% fid...limits: 07:0, = OF OS
comments: Single Concentration Test

01900028 sampled: 03/04/90 non-lethal
95% fid. limits: 020 = 0.0 %
comments: MISA Audit

03900209 sampled: 03/19/90 non-lethal
95% fid..limits: 0.0 - 00, %

comments: Single Concentration Test; Non-lethal

OT cooling water

03890203
95% fid.
comments:

sampled:
limits:

10/10/89
0.0 -

03890261
95% fid.
comments:

sampled:
limits:
Don Lethal

11/13/89
0.0 -

03900016
95% fid.
comments:

sampled:
LIimiEs:
LC50 >100

01/09/90
0.0 -

01900027
95% fid.
comments:

sampled:
limits:
MISA Audit

03/04/90
0.0 -

03900210
95% fid.
comments:

sampled:
Jinies:
Single

03/19/90
0.0 -

combined effluent

03890207 sampled: 10/10/89
95% fid. limits: 0.0 -
comments:

03890257 sampled: 11/13/89
95% fid. limits: 0.0 -
comments: Non lethal

03890360 sampled: 12/13/89
95% fid. limits: 00
comments: Non lethal

non-lethal
OO -%

non-lethal
OS OF es

LCS0: >1'00 “3
0.0 %

non-lethal
0.0 %

non-lethal
0.0 %

Concentration Test; Non-lethal

non-lethal
0.0,,%

non-lethal
0-053

non-lethal
OO) #3

282

Dow Chemical Canada Inc.

03900015 sampled: 01/09/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal

03900112 sampled: 02/13/90 non-lethal
95% fia... limits: 0.0 - O50 +s

comments:

Single Concentration Test

01900029 sampled: 03/04/90 non-lethal
95% fid. Limits: 0. 0%= D 00
comments: MISA Audit

03900211 sampled: 03/19/90 non-lethal
95% fid. Limits: O0 0.0 %

comments: Single Concentration Test; Non-lethal

combined effluent

03890209 sampled: 10/10/89 non-lethal
95% fid. limits: 100.0, = 10007 &
comments:

03890258 sampled: 11/13/89 non-lethal
95% fid. limits: 0, 0,-= 0.0 %
comments: Non lethal

03890356 sampled: 12/13/89 non-lethal
95% f£id. limits: OO. = 0.0 %
comments: Non lethal

03900013 sampled: 01/09/90 non-lethal
95% fid. limits: 0.0 = 0.0"
comments: Non-lethal

03900113 sampled: 02/13/90 non-lethal
95% fad. (limits: 0.0 - 0.0 %

comments:

Single concentration test - Non lethal

01900031 sampled: 03/05/90 non-lethal
95% £10. limits: 050" = 0.0 %
comments: MISA Audit

03900212 sampled: 03/19/90 non-lethal
95% fidi; Limits: O50n— 0.0 %

comments:

Single Concentration Test; Non-lethal

283

(continued)

Dow Chemical Canada Inc. (continued)
combined effluent
03890205 sampled: 10/10/89 non-lethal

95% fid. Dimes: ,. 100.00= 1007003
comments:

03890259 sampled: 11/13/89 non-lethal
95% EI1d. limites: 0:0:= 0.0 %
comments: Non lethal

03890358 sampled: 12/13/89 non-lethal
95% fid. limits: 0.0 - Où ONE
comments: Non lethal

03900014 sampled: 01/09/90 non-lethal
95% fid. limits: 0...07 = O50) Fs
comments: Non-lethal

03900114 sampled: 02/13/90 non-lethal
95% «Eid. limits: 0.0 - 0.0 %
comments: Single Concentration Test

01900030 sampled: 03/05/90 non-lethal
95% fid. limits: 030 .- 050 %%
comments: MISA Audit

03900213 sampled: 03/19/90 non-lethal
95% fid. limits: O30 = 0.0 %

comments: Single Concentration Test; Non-lethal
combined effluent
03890202 sampled: 10/10/89 non-lethal

95% fid. limits: 100.0 = .1.0.0).:0) 3
comments: Non lethal

03890260 sampled: 11/13/89 non-lethal
95% fid. limits: 0.0 - 0. 0.,.%
comments: Non lethal

03890361 sampled: 12/13/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non lethal

03900012 sampled: 01/09/90 LCS0* 12100 %
95% fid. limits: 0.0 - 0.40) 83
comments: LC50 >100

03900115 sampled: 02/13/90 non-lethal
95% fad. Jamies: 0.0 - O10! 4%

comments: Single Concentration test
284

Dow Chemical Canada

Ene.

01900032 sampled: 03/05/90 non-lethal
95%) fd. imacts: 0.0 = 0.0 %
comments: MISA Audit
03900214 sampled: 03/19/90 non-lethal
95% fid. Lamits: 0.0 - 0.0 %
comments: Single Concentration Test; Non-lethal

OT cooling water

03890204 sampled: 10/10/89 non-lethal
952 wid. Aimitss MODO = 10040 AZ
comments:

03890262 sampled: 11/13/89 non-lethal
95% fid. Limits: 0.0 - O20: %
comments: Non lethal

03900017 sampled: 01/09/90 non-lethal
95% fid. limits: 0.0 - 050 %
comments: Non-lethal

01900035 sampled: 03/12/90 non-lethal
95% fid. limits: 0.0 - 0.0 -%
comments: MISA Audit

03900215 sampled: 03/19/90 non-lethal
95% f1d. limits: 0.0 - 0.0 %

(continued)

comments: Single Concentration Test; non-lethal

intake water

process

process

process

process

process

process

process

effluent
effluent
effluent
effluent
effluent
effluent

effluent

285

Dow Chemical Canada Inc. (continued)
process effluent

process effluent

03890274 sampled: 11/16/89 non-lethal
95% fid. limits: 0.08- 0. 0F
comments: Non lethal
03890357 sampled: 12/13/89 LCSO!: 100) —s
95% fid. limits: 0.0" = OO
comments: LC50 >100%
03900011 sampled: 01/09/90 non-lethal
95% fid., limits: 0.0 - OO
comments: Non-lethal
03900116 sampled: 02/13/90 non-lethal
95% fid: limits: 0.0 - 00%
comments: Non lethal
01900034 sampled: 03/14/90 LCSO0: Loot 3%
95% fid. limits: 0.0 - 0.0 %
comments: MISA Audit
03900216 sampled: 03/19/90 non-lethal
95% f£3'd); limites: 0.0 - 0.0 -%

comments: Non-lethal
waste site
total plant
steam plant
north pump house
south pump house

rain gauge

286

282

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COMPANY : Dow Chemical Canada Inc., Sarnia

(910109)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

Data for forty-three Daphnia magna acute lethality
toxicity tests conducted on samples of effluent collected
between October 1989 and March 1990 were submitted by Dow
Chemical Canada Inc. of Sarnia. Overall, the samples
tested for Dow Chemical had little or no acute toxicity to
Daphnia. In all test results submitted there were never
more than three neonates dead in any one concentration of
effluent and in most cases less than two animals died
during the test.

Four of eight samples from once through cooling water
outfalls #300 and 1000 were not acutely lethal to Daphnia.
The remaining four samples had LC50s > 100%.

Five samples from process effluent #2100 were tested
for toxicity to Daphnia. Three of these were not acutely
lethal to Daphnia and the remaining two had 48 h LC50s >
100%.

Samples from the combined effluent outfalls (#200, 500,
600, 700, and 900) were rarely acutely toxic to Daphnia.
Seventy-seven percent of the samples were nonlethal. The
remaining seven samples had LC50s > 100%. Outfalls #200,
700, and 900 were toxic during the January sampling period,
and outfalls #200 and 500 were toxic during the October
sampling period.

In March, audit tests were conducted by Ministry
Scientists on samples from all outfalls being examined at
Dow Chemical. Once through cooling water #1000 was not
acutely lethal to Daphnia, and OTCW #300 had an LC50 >
100%. Samples of combined effluent from outfalls #200, 500
and 900 were nonlethal, and only one neonate died in each
of the tests with effluents from outfalls #600 and 700.

intake water
combined effluent
03890206 sampled: 10/10/89 non-lethal
95%) -fid.. limits: 100.0 = 100.0 %
comments: Non-lethal
03890256 sampled: 11/13/89 non-lethal

953. Laid. 2amictsis 0.0 - OS 0, 3
comments: Non-lethal

33,9

Dow Chemical Canada

03890359
95% fid.
comments:

sampled:
limits:
Non-lethal

12/13/89
0.0 -

03900018
95% fid.
comments:

sampled:
Limits’:
LC50 >100

01/09/90
0.0 —

03900111
95%.f1d.
comments:

sampled:
limits:
Non-lethal

02/13/90
ese

02900028
95% fid.
comments:

sampled:
limits:
MISA Audit

03/04/90
0.0 -

03900209
95% fid.
comments:

sampled:
limits:
Non lethal

03/19/90
0.0 -

OT cooling water
03890203

95% fid.
comments:

sampled: 10/10/89
limits: 100.0 -
Non-lethal

03890261
95% fid.
comments:

11/43/89
00 —

sampled:
limies:
Non-lethal

03900016
95%... 1d.
comments:

sampled:
limits:
LC50 >100

01/09/90
0.0 -

02900027
95% fid.
comments:

sampled:
limits:
MISA Audit

03/04/90
0.0 -

03900210
95% fid.

sampled:
limits:

03/19/90
0.0 -

Inc: (continued)
non-lethal
OS ONE
LC50: >100,2%
0.0 %

non-lethal
OT OS

non-lethal
0-07

non-lethal
0; Ons

non-lethal
VOUS OT

non-lethal
0.0 %

LC505 = >T100, +

LC50: >100 %

0.0 %

non-lethal
0.0. #

comments: Single Concentration Test: Non lethal

combined effluent

03890207
95% fd.
comments:

sampled: 10/10/89
limits: 100.0. -
16.7% mortality

03890257
95% faa:
comments:

sampled:
limits:
Non-lethal

11/13/89
0.0 -

non-lethal
100.0 °%
@ 6%

non-lethal
0.0 %

340

Dow Chemical Canada Inc.

03890360
95% fid.
comments:

sampled:
limits:
Non-lethal

12/13/89
0.0 -

03900015
95% F1d.
comments:

sampled:
limits:
Non-lethal

01/09/90
0.0 -

03900112
95% fid.
comments:

sampled:
limits:
Non-lethal

02/13/90
0.0 -

02900029
95% fid.
comments:

sampled:
limits:
MISA Audit

03/04/90
0.0 -

03900211
95% fid.
comments:

sampled:
Limits:
Non lethal

03/19/90
0.0 -

combined effluent

03890209 sampled: 10/10/89
95% Lid. Limits: 100.08 =
comments: Non-lethal

03890258
95% fid.
comments:

sampled:
limits:
Non-lethal

11/13/89
0.0 -

03890356
95% fid.
comments:

sampled: 12/13/89
limits: 0.0 -
LC50 >100%.

03900013
95% fid.
comments:

01/09/90
0.0 -

sampled:
limits:
Non-lethal

03900113
95% fid.
comments:

sampled:
limits:
Non-lethal

02/13/90
0.0 -

02900031
953 stad.
comments:

sampled:
limits:
MISA Audit

03/05/90
0.0 -

03900212
95% fad:
comments:

sampled:
VIMÉES:
Non lethal

03/19/90
0.0 -

0.

QO.

0.

0.

QO.

100.

0.

QO.

0.

Of

QO.

0.

341

(continued)

non-lethal
0 %

non-lethal
0 %

non-lethal
0 &

non-lethal

0 %
non-lethal
0 %
non-lethal
0 %
non-lethal
0 +

ECHO: > 100) as
0 %
non-lethal
0 %
non-lethal
0 %
non-lethal
0 %
non-lethal
0 %

Dow Chemical Canada Inc.

combined effluent

03890205
95% fid.
comments:

sampled: 10/10/89
limits: 100.0 —
Non-lethal

03890259
95% fid.
comments:

sampled:
limits:
Non-lethal

11/13/89
0.0 -

03890358
95% f£id.
comments:

sampled:
limits:
Non-lethal

12/13/89
0.0 -

03900014
95% fid.
comments:

sampled:
Limits:
LC50 >100

01/09/90
0.0 -

03900114
95% fid.
comments:

sampled:
limits:
Non-lethal

02/13/90
0.0 -

02900030
95% fid.
comments:

sampled:
limits:
MISA Audit

03/05/90
0.0 -

03900213
95% fid.
comments:

sampled:
limits:
Non lethal

03/19/90
0.0 -

combined effluent
03890202

95% fid.
comments:

sampled: 10/10/89
limits: 200.0 =
Non-lethal.

03890260
95% fid.
comments:

sampled:
limits:
Non-lethal

11/13/89
0.0 -

03890361
95% fid.
comments:

sampled:
limits:
Non-lethal

12/18/89
0.0 =

03900012
95% id:
comments:

sampled:
limits:
LE50% >1L00

01/09/90
0.10. =

03900115
95% fid.
comments:

sampled:
limits:
Non-lethal

02/13/90
0.0 -

(continued)

non-lethal
100.0 %

non-lethal
0.0 %

non-lethal
OO"

LC50: 224100 As

0.0 %

non-lethal
0.0 %

non-lethal
OO"

non-lethal

0.0" $
non-lethal
100.0 %
EC50): >100 #%
O075
non-lethal
OS OURS
LC50: >100 %
0.0 %
non-lethal
0.0 3

342

Dow Chemical Canada Inc. (continued)

02900032 sampled: 03/05/90 non-lethal
95% -fid. Lamits: 0.0 - 0.0 %
comments: MISA Audit/high conductivity

03900214 sampled: 03/19/90 non-lethal
95%. fid. limits: 0.0 - OfF0.
comments: Non lethal

OT cooling water
03890204 sampled: 10/10/89 non-lethal

953) fila. J'IMLES : LOOS0F = LOOE:LO: 4
comments: 16.7% mortality @ 13%

03890262 sampled: non-lethal
95% fid. limits: ONO! %
comments: LC50 >100%

03900017 sampled: non-lethal
95% fid. limits: 0.0 %
comments: Non-lethal

02900035 sampled: non-lethal
95% fid. limits: 00°
comments: MISA Audit

03900215 sampled: non-lethal
95% -fild Limits? OOS
comments: Non lethal

intake water

process
process
process
process
process
process

process

effluent

effluent

effluent

effluent

effluent

effluent

effluent

343

Dow Chemical Canada Inc. (continued)
process effluent

process effluent

03890274 sampled: 11/16/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal
03890357 sampled: 12/13/89 Beso: TOO
95% fid. limits: 0.0 - O0
comments: LC50>100
03900011 sampled: 01/09/90 LES0's3* S100) ¥ +s
95% fid. limits: 0.0 - 0.0 +
comments: LC50 >100
03900116 sampled: 02/13/90 non-lethal
95% fid. limits: 0.0 = 0.05%
comments: Non-lethal
02900034 sampled: 03/12/90 non-lethal
95% tid. Jimiesi: 0.0 - 0.0 %
comments: MISA Audit/high conductivity, low D. ©.
03900216 sampled: 03/19/90 non-lethal
95% fid. limits: 0.0 - 0.0 %

comments: Non lethal
waste site
total plant
steam plant
north pump house
south pump house

rain gauge

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COMPANY :

SECTOR:
REGION:

SUMMARY

The data for thirteen trout bioassays,

Du Pont Canada Inc: ,
(80309)

Corunna

(now with: St. ‘Clair River Site)

Organic Chemical
Southwest

conducted on intake

water and combined effluent samples collected between
October 1989 and March 1990, were provided by Du Pont
Canada Incorporated. All thirteen samples were determined
to have been non-acutely lethal to test fish.

intake water

05890088 sampled: 10/18/89 non-lethal
95% fid. limits: 0. 0u= OO
comments:

05890111 sampled: 11/15/89 non-lethal
95% ifad. limits: 0.0 - 0.0 %
comments:

05890127 sampled: 12/13/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05900008 sampled: 01/10/90 non-lethal
SSI slaimitsis 0.0 — 0.0 %
comments:

05900035 sampled: 02/14/90 non-lethal
95% fid. limits: 0.0 - 0. 012%

comments: 10% Control Mortalities, Valid by Protocol

05900056 sampled: 03/14/90 non-lethal
95% Lida. Aimits: 0.0 - 00: +
comments:

combined effluent

05890089 sampled: 10/18/89 non-lethal
95% fid. > limits: 0.0 - O10) 3
comments:

05890110 sampled: 11/15/89 non-lethal
95% -fid. limits: 0.0 - 0.0 %
comments:

05890126 sampled: 12/13/89 non-lethal
95% fd). Sliamastsi: 0.0 - 0.0. %
comments:

397

Du Pont Canada Inc. (continued)

05900009 sampled: 01/10/90 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments:
05900036 sampled: 02/14/90 LESO: S100 4

95% fid. limits: 0.0 - 0.0 %

comments: 10% Control Mortalities - Valid by Protocol
01900016 sampled: 02/20/90 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments:

05900055 sampled: 03/14/90 non-lethal
95% fid. limies: 0.0 - 0.0 2
comments:

combined effluent

01900017 sampled: 02/20/90 non-lethal
95% fid. limits: 0.0 - 0.0%

comments:

rain gauge

398

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COMPANY : Du Pont Canada Ine., Corunna

(80309)
(now with St. Clair River Site)

SECTOR: Organic Chemical

REGION: Southwest

SUMMARY

Data for twelve Daphnia magna acute lethality toxicity
test conducted on samples of intake water and combined
effluent collected between October 1989 and March 1990 were
submitted by Du Pont Canada Inc. of Corunna. Samples of
intake water and effluent had little or no acute toxic
affects on Daphnia.

Five of six samples of intake water were not acutely
lethal to Daphnia. One sample had an LC50 > 100%.

Fifty percent of the effluent samples were nonlethal,
and the remaining three samples had only one neonate die
during the test.

Tests were conducted in the Ministry laboratory on
samples collected in February from the effluent stream and
from the pellet skimming pond. The combined effluent
sample had an LC50 > 100%. The sample from the pellet
skimming pond generated an unusual toxicity response in
which most of the mortalities occurred in the middle
(diluted) concentrations of effluent.

intake water

05890088 sampled: 10/18/89 EEsO%s | S200 (3%
95% fid. limits: 0.0 — 0.0 %
comments:

05890111 sampled: 11/15/89 non-lethal
95% fid. limits: 0.0 - 0.07
comments:

05890127 sampled: 12/13/89 non-lethal
95%; fid.s limits: 0.0 - 0.0
comments:

05900056 sampled: 03/14/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

combined effluent

05890089 sampled: 10/18/89 EES Or > LOUE
95%) fide Limstes's 0.0 - O10) .%
comments:

413

Du Pont Canada Inc. (continued)

05890110 sampled: 11/15/89 LC50: >100 %
95% fid. limits: 0.0 = OO
comments:

05890126 sampled: 12/13/89 LeEso02 >100) 3
95% fidi Limits’: 0.0 - ORIOL 3
comments:

02900016 sampled: 02/20/90 LC50:1610011"%
95% fid."1Aimits: 0.0 - OR OMS

comments: MISA Audit

05900055 sampled: 03/14/90 non-lethal
95% LÉ T4. MAIMLES: 0.0 - 0.0 %
comments:

combined effluent
02900017 sampled: 02/20/90 LCS0Ë OS 1100 7%
95% “fia ‘Timics: 0.0 - O0 +
comments: MISA Audit/bell-shaped lethality curve

rain gauge

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Polysar Limited

05900013 sampled: 01/15/90
95% fid. limits: 0.0 -
comments:

05900039 sampled: 02/19/90
95% fid. limits: 0.0 -
comments:

05900058 sampled: 03/19/90
95% fid. limits: 0.0 -
comments:

process effluent
storm water
storm water
storm water

rain gauge

intake water

(continued)

non-lethal
0.07%

non-lethal
0.0; 4

non-lethal
0.0 %

589

Polysar Limited (continued)

storm water
OT cooling water

05890097 sampled: 11/06/89

95% fid. limits: 0.0 - 0.

comments:

05900024 sampled: 02/05/90

95% fid. limits: 0.0 - QO.
comments:
Batch

05890091 sampled: 10/30/89
95% fid. limits: 0.0 - 0.
comments:

05890115 sampled: 11/20/89
953. fra. limits: 0.0 - Ol:
comments:

05890134 sampled: 12/18/89
95% fid. limits: 0.0 - Où

comments:

05900017 sampled: 01/15/90

95% fid. limits: 0.0 - (8)

comments:

05900041 sampled: 02/19/90
95% fid. limits: 0.0 - (5
comments:

05900061 sampled: 03/19/90
95% fid. linits: 0.0 - Où
comments:

process effluent

05890086 sampled: 10/16/89
95s fad... Limits: 0.0 - 0.
comments:

05890112 sampled: 11/20/89
95% fid. limits: 007 = 0;

comments:

05890133 sampled: 12/18/89

95% £1d. limits: 0.0 - Oz

comments:
588

non-lethal
0 %

non-lethal

0 %

non-lethal

0 %

non-lethal
0 %

non-lethal
0 %

non-lethal
0 %

non-lethal
0 %

non-lethal

0 %

non-lethal

0 %

non-lethal
0. %

non-lethal
Os

Polysar Limited (continued)

05900060
95% fid.
comments:

sampled:
limits:
emergency overflow
process effluent
process effluent
process effluent
combined effluent
05890087 sampled:
95% fid. limits:
comments:
05890113

95% fid.
comments:

sampled:
limits:

05890131
95% fid.
comments:

sampled:
limits:

05900012
95% fid.
comments:

sampled:
limits:

05900040
95% fid.
comments:

sampled:
Limits’

05900059
95% fid.
comments:

sampled:
Limites:

emergency overflow

storm water

OT cooling water
05890095

95% fid.
comments:

sampled:
limits:

05900022
95% fid.
comments:

sampled:
limits:

03/19/90
0)..0) =

10/16/89
0.0 -

11/20/89
0.0 -

12/18/89
0.0 -

01/15/90
0.0 -

02/19/90
0.0 -

03/19/90
62.0 <

11/06/89
0.0 -

02/05/90
0.0 -

0.

non-lethal
(0)

non-lethal

0.0 %

non-lethal

0.0 %

non-lethal

0.0 %

QO.

0.

QO.

0.

non-lethal
0 %

non-lethal
0 %

non-lethal
0 4

non-lethal
Ors

non-lethal

0.0 %

587

Polysar Limited (continued)

process effluent
combined effluent
05890081

95% fid.
comments:

sampled:
limits:

05890103
95% Lids
comments:

sampled:
limits:

05890123
95% fid.
comments:

sampled:
limits:

05900016
95% fid.
comments:

sampled:
limits:

05900029
95% fid.
comments:

sampled:
limits:

05900068
95% fid.
comments:

sampled:
limits:

combined effluent
05890085

95% fid.
comments:

sampled:
limits:

05890114
95% fid.
comments:

sampled:
limits:

05890132
95% e f£id.
comments:

sampled:
Fimits:

05900014
95%. fid.
comments:

sampled:
limits:

05900038
95% fid.
comments:

sampled:
limits:
Single

10/09/89 non-lethal
008 0.0 %
11/13/89 non-lethal
0 0ù= 0047
12/11/89 non-lethal
0.0 — 0.0 %
01/08/90 non-lethal
0.0 0.0 %
02/12/90 non-lethal
0.0 - 0.0 %
03/26/90 non-lethal
0.0 — 0.0 %
10/16/89 non-lethal
0.0 — 0.5.0 2%
11/20/89 non-lethal
0.0 = 0.013
12/18/89 non-lethal
050 — 0.0 %
01/15/90 non-lethal
0.0 — 0.0 %
02/19/90 LC50: >100
0.0: = 2100.0 5%

Concentration Test - 100% mortality

586

COMPANY : Polysar Limited, Sarnia
(30007)
SECTOR: Organic Chemical
REGION: Southwest
SUMMARY

The data for forty trout bioassays, conducted on process
effluent, batch effluent, combined effluent and once
through cooling water samples collected betweeen October
1989 and March 1990, were provided by Polysar Limited.
Twenty-two of twenty-four samples collected from the four
combined effluent discharge locations (0200, 0400, 0500,
1100) were determined to have been non-acutely lethal to
test fish. The other two combined effluent samples were
determined to have been acutely lethal. Statistically, the
percentage effluent required to kill 50 % of the test fish
by the end of the four days exposure was 3.2 % (control
point 0200 - March). The combined effluent sample (0500)
collected in Febrauary was also lethal, causing 100 %
mortality in non-diluted effluent. All the samples
collected from the locations; OTCW 1400, OTCW 1600, batch
1700 and process effluent 1800 were determined to have been
- non-acutely lethal to test fish.

combined effluent

05890083 sampled: 10/09/89 non-lethal

95% fid. limits: 0.0 - 0.0 %
comments:

05890096 sampled: 11/06/89 non-lethal
95% fid. limits: 0.0 - 0:0 %
comments:

05890122 sampled: 12/04/89 non-lethal
95% id: 1imits: 0.0 - OS OMS
comments:

05900001 sampled: 01/01/90 non-lethal
95% 4f1d. limits’: 0.0 - 0.0 %
comments:

05900023 sampled: 02/05/90 non-lethal
95% fid. limits: 0.0 - 050.23
comments:

05900049 sampled: 03/05/90 LE50 SAN:
9JS$eEId: limits: 0.0 - Oe Os
comments:

585

78

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Novacor Chemicals Ltd. (continued)

578

COMPANY:

SECTOR:
REGION:

SUMMARY

Novacor Chemicals Ltd., Mooretown
(380105)

Organic Chemical

Southwest

Data for six Daphnia magna acute lethality toxicity
tests conducted on samples of combined effluent collected
between October 1989 and March 1990 were submitted by
Novacor Chemicals Ltd. of Mooretown. Due to scheduling
conflicts the December sample was collected on January 3,

1990. All six samples were not acutely lethal to Daphnia.

combined effluent

05890090 sampled:
95% fid. limits:
comments:

05890109 sampled:
95% fid. limits:
comments:

05900002 sampled:
95% fid. limits:
comments:

05900021 sampled:
95% fid. limits:
comments:

05900046 sampled:
95% fid. limits:
comments:

05900064 sampled:
95% fid. limits:
comments:

storm water

emergency overflow

storm water

——_—_—_—_—_—_—_—_—_—_—"—"—"—"—"—"—"—"—"—"—…—"—…—"—…—"—…"…"—"…"—"—"—"…"—"—"—"—"—…"—"…"…"…"…"…"…"—"—"…"—"—"—"—"—"—"———

10/30/89 non-lethal
0:0%= 0.0 %

11/15/89 non-lethal
0.0 - 0.0 %

01/03/90 non-lethal
0.0 = 0.0 %

01/24/90 non-lethal
O30 = OO

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Nos, VSIW

COMPANY: Novacor Chemicals Ltd., Mooretown

(380105)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

The data for five trout bioassays, conducted on combined
effluent discharge samples collected between October 1989
and March 1990, were provided by Novacor Chemicals Limited.
All five combined effluent samples were determined to have
been non-acutely lethal to test fish.

combined effluent

05890090 sampled: 10/30/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05890109 sampled: 11/15/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05900002 sampled: 01/03/90 non-lethal
95% fid. limits: 0.0) = 0.0 %
comments:

05900021 sampled: 01/24/90 non-lethal
95$1f1d. limits: 0.0 - 0.0 %
comments:

05900046 sampled: 02/21/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05900064 sampled: 03/21/90 non-lethal
95% fid. Limits: 0.0 - 0.0 %

comments:
storm water
emergency overflow

storm water

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COMPANY: Morbern Inc., Cornwall

(12580007)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

Morbern Inc. of Cornwall commenced the monitoring
regulations on February 1 1990, and therefore have only
submitted data for two Daphnia magna acute lethality
toxicity tests. Both samples from once through cooling
water outfalls #100 and 200 were not acutely lethal to
Daphnia.

OTCW
06900352 sampled: 03/06/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: UNSEANSONABLE WARM TEMPERATURES TEMP ELEVATED
OTCW
06900350 sampled: 03/06/90 non-lethal
95% fid. limits: O0 0.0 %

comments: UNSEANSONABLE WARM TEMP RESULTED IN ELEVATION

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COMPANY : Morbern Inc., Cornwall

(12580007)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

The data for two trout bioassays, conducted on once through
cooling water samples collected between October 1989 and
March 1990, were provided by Morbern Incorporated. Both
samples of cooling water were determined to have been
non-acutely lethal to test fish. Morbern commenced monitoring
on February 1, 1990.

OTCW
06900349 sampled: 03/06/90 non-lethal
95% fid. limites: 0.0 - 0.0 %
comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED
OTCW
06900351 sampled: 03/06/90 non-lethal
95% fid. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED

561

COMPANY : Guardsman Products Ltd., Cornwall

(122470008)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY
Guardsman Products Ltd. of Cornwall commenced the

monitoring regulations on February 1, 1990, therefore
there is no data for review at this time.

OTCW

OTCW

559

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COMPANY : Guardsman Products Ltd., Cornwall

(122470008)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

The initiation of acute toxicity monitoring by Guardsman
Products Ltd. began on February 1, 1990, therefore no data

has been submitted for the period between October 1989 and March
1990.

SSS
OTCW

OTCW

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GE Plastics Canada Ltd. (continued)

OT cooling water

06891148 sampled: 11/27/89 LC50: 23.45%
95s fide. limites: 1707/1295 "3. slope: 47.5
comments:

06900032 sampled: 01/09/90 ECS50': 370! 3
95% fid. limits: 40.4 = 33.9 %

comments: 100% MORTALITY IN 50% CONCENTRATION.

intake water

548

-—

COMPANY : SE Plastics Canada Ltd., Cobourg
(600007)

SECTOR: Organic Chemical

REGION: Central

SUMMARY

Data for eight Daphnia magna acute lethality toxicity
tests conducted on samples of once through cooling water
and combined effluent were submitted by G.E. Plastics
Canada Ltd. of Cobourg.

The two samples of once through cooling water were
toxic to Daphnia with LC50 values 23.4 and 37%.

The six samples of combined effluent tested by the
company were not acutely lethal to Daphnia.

combined effluent

06890989 sampled: 10/10/89 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments:
06891085 sampled: 11/14/89 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: .
06891273 sampled: 12/12/89 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments:
06900030 sampled: 01/09/90 non-lethal

95% fid. limits: 0.0 - OS OS

comments: NO MORTALITY OR IMMOBILITY OBSERVED IN 48 HRS
06900266 sampled: 02/13/90 non-lethal

95% fid. limits: 0.0 - 0.0 %

comments: NO MORTALITY OR IMMOBILITY OBSERVED IN 48 HRS
06900389 sampled: 03/13/90 non-lethal

95% fid.! Limies? 0.0 - 0.0: 3

comments: UNSEASONABLE WARM TEMP RESULTED IN ELEVATION
storm water

storm water

547

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GE Plastics Canada Ltd. (continued)
storm water
storm water

OT cooling water

06891147 sampled: 11/27/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

06900031 sampled: 01/09/90 non-lethal
95% f£id. limits: 00 050.3

comments: NO MORTALITY OR SUBLETHAL IMPAIRMENT OBSERVED

intake water

538

COMPANY: GE Plastics Canada Ltd., Cobourg

(600007)
SECTOR: Organic Chemical
REGION: Central

SUMMARY

The data for eight trout bioassays, conducted on combined
effluent and once through cooling water samples collected
between October 1989 and March 1990, were provided by GE
Plastics Canada Limited. Five of the six combined

effluent samples were determined to have been acutely
lethal to test fish. Statistically, the percentage effluent
required, to kill .50.% of the, test fish by Ehe end of the
four days exposure were 49.9 % (November), 37.0 %
(December), 80.6 % (January), 28.1 % (February) and 14.1 %
(March). The other two combined effluent samples were
determined to have been non-acutely lethal. Two samples of
once through cooling water were determined to have been
non-acutely lethal.

combined effluent

06890988 sampled: 10/10/89 non-lethal
95% fid. limits: 0.0 - 0.0
comments:
06891084 sampled: 11/14/89 LCESO: 49.9 %
95% fid. limits: 43.7 - 56.9 %
comments:
06891272 sampled: 12/12/89 LE50% 3710" %
95%etid. limits: 33,9 = "40.3
comments:
06900029 sampled: 01/09/90 LESO: 80.6 %
95% fid.slimits: 20070 = 65.0 4
comments: 100% MORTALITY IN FULL STRENGTH EFFLUENT.
06900265 sampled: 02/13/90 LC50% 28-115
95% fid. limits: 24.6 - 32.1 %
comments: 70% MORTALITY IN 30% TEST CONCENTRATION
06900388 sampled: 03/13/90 LESO: LAINE
95% fid. limits: TO 3 17.21%

comments: 90% MORTALITY IN 20% TEST CONCENTRATION

537

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Ethyl Canada Inc. (continued)
process effluent
storm water
storm water
storm water
rain gauge

intake water

530

COMPANY: Ethyl Canada Inc., Corunna
(120006)
SECTOR: Organic Chemical
REGION: Southwest
SUMMARY

Data for six Daphnia magna acute lethality toxicity
tests conducted on samples of combined effluent collected
between October 1989 and March 1990 was submitted by Ethyl
Canada Inc. of Corunna. Two of the six samples were not
acutely lethal to Daphnia. One sample generated an unusual
toxicity response in which the highest mortalities occurred
in the middle concentrations of effluent.

combined effluent

05890084 sampled: 10/10/89 LC50: >100 %

95% fid. limits: 0.0 - OSOME
comments:

05890105 sampled: 11/14/89 LESO: INVALID
95% fid. limits: 0.0 - 0.0 % slope:
comments: ;

05890125 sampled: 12/12/89 Le50%°. >1100.. =
95% fid. limits: 0.0 - 0.0 5
comments:

05900018 sampled: 01/16/90 non-lethal
95% fid. limits: 0.0 - 0.0
comments: Duplicate Tested

05900032 sampled: 02/13/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05900054 sampled: 03/13/90 LC50: >100 %
95% fid. limits: 0.0 - 0.0 %
comments:

process effluent

529

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Ethyl Canada Inc.

storm water
storm water
rain gauge

intake water

(continued)

522

Ethyl Canada Inc., Corunna

COMPANY :
(120006)
SECTOR: ! Organic Chemical
REGION: Southwest
SUMMARY

The data for six trout bioassays, conducted on combined
effluent samples collected between October 1989 to March
1990, were provided by Ethyl Canada Incorporated. All six
samples of combined effluent collected from control point
0100 were determined to have been non-acutely lethal to
test fish.

combined effluent

05890084 sampled: 10/10/89 non-lethal
95% fid. limits: 0.0°=- 0.0 %
comments:

05890105 sampled: 11/14/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05890125 sampled: 12/12/89 non-lethal
95% fid. Jinrts: 0.0 - 0.0 %
comments:

05900018 sampled: 01/16/90 non-lethal
95% fid. limits: OL ON 0.0 %
comments:

05900032 sampled: 02/13/90 non-lethal
95% fid. limits: 0.0 - 0:05
comments:

05900054 sampled: 03/13/90 non-lethal
95% fid. limits: 0.0 - 0.0 %

comments:

process effluent

process effluent

storm water

522

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Esso Chemical Canada (continued)

process effluent

combined effluent

05890092
95% fid.

sampled:
limits:

comments:

05890120
95% fid.

sampled:
limits:

comments:

05890128
95% f£id.

sampled:
limits:

comments:

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95% fid.

sampled:
limits:

comments:

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95% fid.

sampled:
limits:

comments:

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95% fid.

sampled:
limits:

comments:

rain gauge

10/30/89
0.0 -

11/22/89
0.0 -

12/13/89
0.0 -

01/10/90
0.0 -

02/07/90
0.0 -

03/07/90
0.0 -

0.

0.

OF

0.

non-lethal
0 %

non-lethal
0 %

non-lethal
0 %

non-lethal
0 %

LC50:

0.0 %

0.

508

non-lethal
0 %

707

L
COMPANY: Esso Chemical Canada, Sarnia

(70201)

(now with Sarna Chemical Plant)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

Data for thirteen Daphnia magna acute lethality
toxicity tests conducted on samples of intake water and
combined effluent collected between October 1989 and March
1990 were submitted by Esso Chemical Canada of Sarnia. All
six samples of intake water were not acutely lethal to
Daphnia.

Six of seven samples of final effluent were not acutely
lethal to Daphnia. One sample collected in February
appears to have been tested in duplicate. One test
indicated the sample was toxic with a 48 h LC50 = 70.7%,
while the other test was nonlethal.

a

intake water

05890093 sampled: 10/30/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05890119 sampled: 11/22/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05890129 sampled: 12/13/89 non-lethal
95% fid. Limits: 0.0 - 0.0 %
comments:

05900010 sampled: 01/10/90 non-lethal
95% fid. limits: 0.0 - OS ONE
comments:

05900027 sampled: 02/07/90 non-lethal
953. fid. “Limits; 0.0 - 0.0 %
comments:

05900050 sampled: 03/07/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

507

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Esso Chemical Canada (continued)

05890128 sampled: 12/13/89
95% fid. limits: 0.0: =
comments:

05900011 sampled: 01/10/90
95% >fiay limes: 002
comments:

05900025 sampled: 02/07/90
95% fid. limits: 0.0 -
comments:

05900051 sampled: 03/07/90
95% fid. limits: OÙ Où

comments:

rain gauge

QO.

0.

QO.

0.

494

non-lethal
0 %

non-lethal
0%

non-lethal
0 %

non-lethal
0 %

COMPANY : Esso Chemical Canada, Sarnia

(70201)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

The data for twelve trout bioassays, conducted on combined
effluent and intake water samples collected between October
1989 and March 1990, were provided by Esso Chemical Canada.
All six combined effluent (control point 0300) samples and
six intake water samples were determined to have been
non-acutely lethal to test fish.

intake water

05890093 sampled: 10/30/89 non-lethal
95% fid. limits: 0.0; = 0.0 %
comments:

05890119 sampled: 11/22/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05890129 sampled: 12/13/89 non-lethal
95% £id. limits: 0.0 - 0.0 %
comments:

05900010 sampled: 01/10/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05900027 sampled: 02/07/90 non-lethal
95% fid. limits: 0.0 - OO
comments:

05900050 sampled: 03/07/90 non-lethal
95% fid. limits: 0.0 - O20: %
comments:

process effluent

combined effluent

05890092 sampled: 10/30/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05890120 sampled: 11/22/89 non-lethal
SSL ElIMIES): 0.0 - OO
comments:

493

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COMPANY: Du Pont Canada inc., Whitby

(80408)
SECTOR: Organic Chemical
REGION: Central

SUMMARY

Monitoring at the Du Pont Canada Inc. plant in Whitby
did not commence until February 1990, therefore data for
only two Daphnia magna acute lethality tests conducted on
samples of combined effluent were submitted. One sample
was not acutely lethal to Daphnia, and the other had an
C50: > (100%.

Storm Water

Combined Effluent

03900157 sampled: 02/27/90 non-lethal
95% fid. limits: 0.0, — 0.0 %
comments: Non lethal
03900250 sampled: 03/27/90 LCS0: +100 3
95% fid. limits: 0.0 - 0.0 4
comments: LC50 >100
OTCW
OTCW
OTCW
OTCW

Combined Effluent

489

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COMPANY : Du Pont Canada Inc.,

(80408)
SECTOR: Organic Chemical
REGION: Central

SUMMARY

The data for two trout bioassays, conducted on combined

effluent samples collected between October 1989 and March
1990, were provided by Du Pont Canada Incorporated. Both
samples of combined effluent were determined to have been

non-acutely lethal to test fish.

Storm Water

Combined Effluent

03900157 sampled: 02/27/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: non lethal

03900250 sampled: 03/27/90 non-lethal
95% fid. limits: 0.0 - O OS
comments: non lethal

OTCW
OTCW
OTCW
OTCW

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485

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Du Pont Canada Inc.

combined effluent

(continued)

03890230 sampled: 10/18/89 LCSO;:

95% f£id. LIMTES: AA" 200: Ss Slopes
comments:

02890266 sampled: 11/15/89 LC50:

95% id; limits: 38.4 - 43.9 %
comments: MISA Audit/ high oxygen demand

03890276 sampled: 11/15/89 LCSO:

95% fid. limits: 1344 2346 % slope:
comments:

03890394 sampled: 12/20/89 non-lethal
95% f£id.. Limits: 0.0 - 02°05 °%
comments: Non-lethal

03900050 sampled: 01/17/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non lethal

03900144 sampled: 02/21/90 non-lethal
95%, tid. limits: 0.0 - 0.0 %
comments: Non-lethal

03900236 sampled: 03/21/90 non-lethal
95% fid. limits: O0 = 0:07 2
comments: Non-lethal

emergency overflow

rain gauge

472

5). es
3%

41.0 %

17e 9

6

8

COMPANY : Du Pont Canada Inc., Maitland

(80002)

(now with Maitland Site)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

Data for nine Daphnia magna acute lethality toxicity
tests conducted on samples of intake water and combined
effluent collected between October 1989 and March 1990 were
submitted by Du Pont Canada Inc. of Maitland.

Two of three intake water samples were toxic to
Daphnia, as was an audit sample tested in the Ministry
laboratory in November.

Four of six samples of combined effluent were not
acutely lethal to Daphnia. The samples collected at the
beginning of the monitoring period in October and November
were toxic to Daphnia. LC50s for these sample were 15.1
and 17.9% consecutively. An audit sample tested in the
Ministry laboratory in November was also toxic to Daphnia
with 48 h LC50 = 41.1%.

process effluent

process effluent

combined effluent
combined effluent
storm water

storm water

intake water

03890275 sampled: 11/15/89 ECHO: > S100) TS
95% fid.. limes: O00: = 0.0 %
comments: LC50 >100%
02890265 sampled: 11/15/89 LC50: 15:01=" 30505
95% fad. “Limits: 0.0 - 0.0 %
comments: MISA Audit/immobilization within 24 hrs.
03900051 sampled: 01/17/90 LC50: 307%
95% id. limits: 23.4 - 40.1 % slope: 422
comments: Lethal
03900143 sampled: 02/21/90 non-lethal
953 fid. 1 limitss 0.0 c= 0.0 %

comments: Non-lethal
471

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Du Pont Canada Inc. (continued)

combined effluent

03890230 sampled: 10/18/89 LESO: >100 %
95% f1d. Lames: 0}.0) = 0.0 %
comments:
03890276 sampled: 11/15/89 EES Oss ShLOOw +
95% fid. limits: 0.0 - 0.0 %
comments:
01890266 sampled: 11/15/89 LC50: 7OnLr,ES
955" fid: limits: 57:15. =U08/8 39) Fs
comments: MISA audit sample.
03890394 sampled: 12/20/89 non-lethal
95% fid: limits: 0.0 — 0.0 %
comments: Non-lethal
03900050 sampled: 01/17/90 non-lethal
95% fid. limits: O0 = 0.0 %
comments: Non-lethal
03900144 sampled: 02/21/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: Non-lethal
03900236 sampled: 03/21/90 non-lethal
95% Lid)... limits: 0.0 - 0.0 %

comments: Single Concentration Test; Non lethal
emergency overflow

rain gauge

460

COMPANY : Du Pont Canada inc., Maitland

(80002)
(now with Maitland Site)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY .

The data for nine trout bioassays, conducted on combined
effluent and intake water samples collected between October
1989 and March 1990, were provided by Du Pont Canada
Incorporated. Two of the combined effluent samples were
determined to have been acutely lethal to test fish. Both
sample 96 hour LC50s were >100 %. The Ministry audit
sample, collected in November, 96 hour LC50 was 70.1 %. The
remaining four combined effluent samples were determined to
have been non-acutely lethal to test fish. Two of the
intake water samples were determined to have been
non-acutely lethal while the third, collected in February,
had a 96 hour LC50 >100 %.

process effluent

process effluent

combined effluent
combined effluent
storm water

storm water

intake water

03890275 sampled: 11/15/89 non-lethal
953 id; Jamies: 0.0 - 0.0
comments: Non lethal
03900051 sampled: 01/17/90 non-lethal
95% fid. limits: 0.0 - 0.0 3%
comments: Non Lethal
03900143 sampled: 02/21/90 LCS0:1 >100 3
95% Lid. limits: 0.0 - 0.0 %

comments: LC50 >100

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Du Pont Canada Inc. (continued)

443

Du Pont Canada Inc. (continued)

02900021 sampled: 02/26/90 CSOs HOO? 'S
95% fid.. Jamits: 61.5 = 79.6 %
comments: MISA Audit/high biological oxygen demand
03900234 sampled: 03/20/90 LC50: >100: +
95% fid."imits: 0.0 - 0.0 %

comments: LC50 >100
waste site
process effluent

combined effluent

03890229 sampled: 10/17/89 LeE50: LGR 25kS
95% fid. Mimits: AA = 2156's slopes 5.4
comments:

03890278 sampled: 11/14/89 TE50 MA > 100) os
95% fid. limits: 0.0 - 0.0 3%
comments: Non-lethal

03890393 sampled: 12/19/89 LC50: 8.0 %
95% fid. limits: 5.3 = 12.0 % slope: 2.5
comments:

03900047 sampled: 01/16/90 non-lethal
953 £1d.. Limits: 0.0 - 0.0). %
comments: Non lethal

03900145 sampled: 02/20/90 LC50: SSI
95% fid. limits: 252108 = 500 +
comments:

02900023 sampled: 02/26/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: MISA Audit

03900235 sampled: 03/20/90 LC50: >L00 + -%

95% fid. limits: 0.0" = 00 +

comments: LC50 >100
rain gauge

intake water

442

COMPANY : Du Pont Canada Inc., Kingston

(80101)

(now with Kingston Site)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

Data for twelve Daphnia magna acute lethality toxicity
tests were conducted on samples of combined effluent
collected between October 1989 and March 1990 were
submitted by DuPont Canada Inc. of Kingston. Toxicity was
variable for both outfalls.

All six samples from combined effluent #700 were lethal
to Daphnia. Toxicity ranged from a sample in which only
one animal died, to a sample collected in December with an
LC50 = 12.7%.

Two of six samples from combined effluent pipe #1100
were not acutely lethal to Daphnia. Toxicity in the
remaining 4 samples ranged from the November sample in
which only one animal died in the test, to a sample
collected in December which generated an LC50 = 8.0%.

Audit tests were conducted in the Ministry laboratory
on samples collected in February from both outfalls. The
sample from combined effluent #700 was toxic to Daphnia
with a 48 h LC50 of 70.0%. The sample from combined
effluent #1100 was nonlethal.

process effluent

combined effluent

03890228 sampled: 10/17/89 LCS0: 18.9 %
95% fid. limits: 14.3 - 24.7 % slope: 5. i
comments:

03890277 sampled: 11/14/89 non-lethal
95% fid. limits: 0.0 = 0.0 %
comments: Non-lethal

03890392 sampled: 12/19/89 LC50: 1257165
95% fid. limits: 10.0 — 16.0 % slope: 5.16
comments:

03900048 sampled: 01/16/90 LC50: >100 %

95% fid. limits: 0.0 - 0.0 +
comments: LC50 > 100

03900146 sampled: 02/20/90 LES: 39.3 %
95% fid. limits: 29.9. = 51.4 tuslope: 58
comments:

441

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Du Pont Canada Inc. (continued)
03900234 sampled: 03/20/90 non-lethal
95% fid. dimits: 0.0 - OC ONE
comments: Non lethal
waste site

process effluent

combined effluent

03890229 sampled: 10/17/89 LC50: SAS ONS
95%, tad. limits’: 40.0 = 65.0) %
comments:

03890278 sampled: 11/14/89 non-lethal
954 fd. Vimiltess: 0.0 - O10" 3
comments: Non lethal

03890393 sampled: 12/19/89 LC50: A2 NE à
95% fid. limits: 33.9, 53:7, %,. slopes 6.,1
comments:

03900047 sampled: 01/16/90 non-lethal
95% £id. limits: 0.0 - OL OMS
comments: Non-lethal

03900145 sampled: 02/20/90 LESO: 56.85%
95% f1d.. limits: 476 = 67.7 % Sloper — 8.4
comments:

01900023 sampled: 02/26/90 LESO: 5100 “%
95% £id. limits: 0.0 - 0.0:
comments: MISA Audit

03900235 sampled: 03/20/90 LESO0: M>100 5
95% fid. limits: 0.0 - 0). 0! °%

comments: LC50>100
rain gauge

intake water

COMPANY: Du Pont Canada Inc., Kingston

(80101)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

The data for twelve trout bioassays, conducted on combined
effluent samples collected between October 1989 and March
1990, were provided by Du Pont Canada Incorporated. Three
of the six samples collected from combined effluent
(control point 0700) were determined to have been acutely
lethal to test fish. Statistically, the percentage effluent
to kill 50 % of the test fish by the end of four days
exposure, for each sample, were 81.0 % (October), 64.3 %
(December), and 86.4 % (February). The other three samples
were determined to have been non-acutely lethal.

Three of the six samples collected from the combined
effluent (control point 1100) were determined to have been
acutely lethal to test fish. Statistically, the percentage
effluent to kill 50 % of the test fish by the end of four
days exposure, for each sample, were 51.0 % (October), 42.7
% (December) and 56.8 % (February). One sample 96 hour LC50
was > 100 % and the other two samples were determined to
have been non-acutely lethal. An audit sample collected
from combined effluent (control point 1100) was tested by
O.M.E. laboratory and its 96 hour LC50 was > 100 %.

oe

process effluent

combined effluent

03890228 sampled: 10/17/89 LC50: 81.0 %
95% £1a.. Limits: 65.0 - 100.0 %
comments:

03890277 sampled: 11/14/89 non-lethal
95% f10.- Limits: 0.0 — 0.0 %
comments: Non lethal

03890392 sampled: 12/19/89 LCS50: 64.3 %
95% É1d.e 11mits: 48.6 - 84.9 % slope: 4.3
comments:

03900048 sampled: 01/16/90 non-lethal
953 fid.2limits: 0.0 - 0.0 %
comments: Non-lethal

03900146 sampled: 02/20/90 EC5SO% 86.4 %
95% fid.f limes: 76.1 - 98.1 % slope: 1373
comments:

425

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COMPANY: Polysar Limited, ‘Sarnia

(30007)
SECTOR: Organic Chemical
REGION: Southwest

SUMMARY

Data for forty Daphnia magna acute lethality toxicity
tests conducted on samples of effluent collected between
October 1989 and March 1990 were submitted by Polysar
Limited of Sarnia. The samples generally had little or no
acute toxicity to Daphnia for all eight outfalls being
examined. The exceptions were three samples of combined
effluent from outfalls #200, 500 and 1100 collected in
Febrary or March. These samples were acutely toxic to
Daphnia with LC50s ranging from 2.6 to 59.7%.

The four samples from once through cooling water
outfalls #1400 and 1600 were not acutely lethal to Daphnia.
The six samples from Batch effluent #1700 were not
acutely lethal to Daphnia. Three of six samples of process

effluent #1800 were nonlethal, and three samples had only
one or two neonates die during the duration of the test.
Four samples from combined effluent #200 were not
acutely lethal to Daphnia, and one sample had a 48 h LC50 >
100%. One sample collected in March was very toxic to
Daphnia with an 48 h LC50 = 2.6%. Similarly, three samples
from combined effluent #1100 were nonlethal, two samples
had LC50s > 100% and the March sample was acutely toxic to
Daphnia with an LC50 = 59.7%. Four samples from combined
effluent #500 were nonlethal, and one sample had an LC50 >
100%. The toxic sample in this case was collected in
February and had a 48 h LC50 = 6%. There was no change in
pH, or conductivity in any of the toxic samples to give a
clue as to the cause of their toxicity. Such deviations
from the normal effluent quality may have been caused by a
system failure, or by routine pipe cleaning maintenance.
Five samples from combined effluent #400 were nonlethal and
one sample had two mortalities in the 100% effluent only.

combined effluent

05890083 sampled: 10/09/89 non-lethal
953 Lid— Limits’: 0.0 - OO"
comments:
05890096 sampled: 11/06/89 non-lethal
95s tid limits: 0.0 - O0
comments:
05890122 sampled: 12/04/89 LCS0: >100,. %
FS tmcid “limits: 0.0 - ORO} <%
comments:

631

Polysar Limited (continued)

05900001 sampled: 01/01/90 non-lethal
95% f£id. limits: 0.0 - 0.0 %
comments: Control Mortality <10%

05900023 sampled: 02/05/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05900049 sampled: 03/05/90 LCS50: 226 %
95% Fi1d:"Tlimits: 1.9 - 325%
comments:

process effluent
combined effluent

05890081 sampled: 10/09/89 non-lethal
952° fid. limits: 00" 0.0 %
comments:

05890103 sampled: 11/13/89 non-lethal
95% fid. limits: 0.0 - 0../0"'3
comments:

05890123 sampled: 12/11/89 CSOs: S31 0108s
953° f1d. limits! 0.0 - 0.0 % |
comments: |

05900016 sampled: 01/08/90 non-lethal
95% f£1id.* limits: OO Ov 0"
comments: Duplicate also tested

05900029 sampled: 02/12/90 non-lethal
95% fid: limits: 070" = 0.0 %
comments:

05900068 sampled: 03/26/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

combined effluent

05890085 sampled: 10/16/89 LC50:, >100 3
95% fi: limits: 0.0 - O07
comments:

05890114 sampled: 11/20/89 non-lethal
954 Fid. limites’: 0.0 — OZ ON

comments:

632

Polysar Limited (continued)

05890132 sampled: 12/18/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

05900014 sampled: 01/15/90 non-lethal
95% fid. limits: 0.0 - O0
comments:

05900038 sampled: 02/19/90 LESO's 0.0 - 6. Or = "3
95% fid. limits: 0.0 - OS OS
comments:

05900060 sampled: 03/19/90 non-lethal
952 fa. limits: 0.0 - OL OS

comments:
emergency overflow
process effluent
process effluent
process effluent

combined effluent

05890087 sampled: 10/16/89 non-lethal
95% fid. Limits: 0.0 - Oi:0) 4%
comments:

05890113 sampled: 11/20/89 non-lethal
95% fid. limits: 050= 0.0 3
comments:

05890131 sampled: 12/18/89 LC50!s? S100 4%
95% fid. limits: 0.0 - 060$
comments:

05900012 sampled: 01/15/90 non-lethal
95$#E1d. limits: O0 00)
comments:

05900040 sampled: 02/19/90 non-lethal
95%-fid. Vimitss 0.0 - OOM S
comments:

05900059 sampled: 03/19/90 LC50: 59278
95% fia. limits: SOS =) ONE

comments:

Polysar Limited (continued)
emergency overflow
storm water

OT cooling water

05890095 sampled: 11/06/89 non-lethal
95% fid. limits: 0.0 - 0-04
comments:

05900022 sampled: 02/05/90 non-lethal
95% fald.. limits: 0.0 - 0.0
comments:

storm water
OT cooling water

05890097 sampled: 11/06/89 LC50 >100
95% fid. limits: 0.0 - 0.0 %
comments:

05900024 sampled: 02/05/90 non-lethal
95% fid. limits: 0.0 - OO
comments:

Batch

05890091 sampled: 10/30/89 non-lethal
95% fad. Limits: 0.0 - 0% O.a%
comments:

05890115 sampled: 11/20/89 non-lethal
95% fid. limits: 0.0 - 0'.'O.cs
comments:

05890134 sampled: 12/18/89 non-lethal
95% fids Limits: 0.0 - OO 23
comments:

05900017 sampled: 01/15/90 non-lethal
95% f1d. limits: 0.0 - 0.05%
comments:

05900041 sampled: 02/19/90 non-lethal
95% fid. limits: 0.0 - 0.0 =%
comments:

05900061 sampled: 03/19/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

634

Polysar Limited (continued)

process effluent

05890086 sampled: 10/16/89
95% fid.- Limits: 0.0 -
comments:

05890112 sampled: 11/20/89
95% £10. Limits: DO
comments:

05890133 sampled: 12/18/89
95% fid. limits: Or. 0ù=
comments:

05900013 sampled: 01/15/90
95% fid. limits: 0.0 -
comments: Duplicate Tested

05900039 sampled: 02/19/90
95% fid. limits: 0.0 -
comments:

05900058 sampled: 03/19/90
95% fid. limits: 0.0 -

comments:
process effluent
storm water
storm water
storm water
rain gauge

intake water

LC50: >100
0.0 %

LC50: >100
0.0 %

EC503~" >100
OR OSS

non-lethal
0.0 %

non-lethal
0:0! -%

non-lethal
050: %

635

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« on 19 7

COMPANY: Rohm & Haas Canada Inc., Scarborough

(580001)
SECTOR: Organic Chemical
REGION: Central

SUMMARY

The initiation of acute toxicity monitoring by Rohm & Haas
Canada Incorporated was delayed therefore no data has been
submitted for the period between October 1989 and March
1990:

677

COMPANY: Rohm & Haas Canada Inc., Scarborough

(580001)
SECTOR: Organic Chemical
REGION: Central

SUMMARY

The toxicity monitoring for Rohm and Haas Canada Inc.
of Scarborough has been delayed, therefore no data has been
submitted for the period October 1989 to March 1990.

679

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Ae mm _ — ——— — A —

COMPANY: Rohm and Haas Canada Inc., Morrisburg

(580100)
SECTOR: Organic Chemical
REGION: Southeast

SUMMARY

The data for six trout bioassays, conducted on combined
effluent samples collected between October 1989 and March
1990, were provided by Rohm and Haas Canada Incorporated.
All six combined effluent samples were determined to have
been non-acutely lethal to test fish.

combined effluent

03890233 sampled: 10/25/89 non-lethal
JSSMELd: Dimas: 0.0 - 01.20) %
comments:

03890295 sampled: 11/21/89 non-lethal
95% f1d. Limits: 0.0 - O0
comments: Non lethal

03890391 sampled: 12/19/89 non-lethal
95% £1d. limits: 0.0 - O15 02S
comments: Non-lethal

03900079 sampled: 01/23/90 non-lethal
95% ELA. limits: 0.0 - 0.013
comments: Non-lethal

03900160 sampled: 02/27/90 non-lethal
95% fad. limits: 0.0 - OS OS
comments: Non-lethal

03900227 sampled: 03/20/90 non-lethal
95% fid. alimits: 0.0 - OÙ 015

comments: Single Concentration Test; Non-lethal
process effluent
storm water
rain gauge

intake water

681

e

Rohm and Haas Canada Inc. (continued)

682

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COMPANY :

SECTOR:
REGION:

SUMMARY

Rohm and Haas Canada Inc., Morrisburg
(580100)

Organic Chemical

Southeast

Data for six Daphnia magna acute lethality toxicity
tests conducted on samples of Combined effluent collected
between October 1989 and March 1990 were submitted by Rohm
and Haas Canada Inc. of Morrisburg.

Four samples were not acutely lethal to Daphnia, and
two samples had 48 h LC50s > 100%. One toxic sample
induced an unusual toxic response in which the greatest
number of mortalities occurred in the middle concentrations

of effluent.

combined effluent

03890233 sampled: 10/25/89 LESO0: S100" ¥
953 (fia. Linits: 0.0 - 00%
comments: LC50 >100
03890295 sampled: 11/21/89 LE50: S100 4
95% Lid... lamits': 0.0 - 0.00%
comments: LC50 > 100
03890391 sampled: 12/19/89 non-lethal
OSe f£id. limits: 0.0 - ORO
comments: Non-lethal
03900079 sampled: 01/23/90 non-lethal
OS5t tid. Jaimiltss <« 10.0) — 0.0 %
comments: Non-lethal
03900160 sampled: 02/27/90 non-lethal
95%) fid.= limits: 0.0 - O10 %
comments: Non-lethal
03900227 sampled: 03/20/90 non-lethal
95t fide limits: 0.0 - OO
comments: Non-lethal

process effluent

storm water

689

Rohm and Haas Canada Inc. (continued)
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COMPANY : Stepan Canada Inc., Longford Mills

(140004)
SECTOR: Organic Chemical
REGION: Central

SUMMARY

The data for six trout bioassays, conducted on combined
effluent samples collected between October 1989 and March
1990, were provided by Stepan Canada Incorporated. All six
combined effluent samples were determined to have been
non-acutely lethal to test fish.

combined effluent

08890441 sampled: 10/18/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

08890473 sampled: 11/15/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

08890492 sampled: 12/13/89 non-lethal
95% ELA. limits: 0.0 - OZ OS
comments:

08900031 sampled: 01/17/90 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments:

08900111 sampled: 02/20/90 non-lethal
95% fid. limits: 0.0 - 0.0
comments:

08900221 sampled: 03/21/90 non-lethal
95% f1d. limits: 0.0 - O0! %

comments:
process effluent
emergency overflow
rain gauge

intake water

697

Stepan Canada Inc. (continued)

698

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COMPANY :

SECTOR:
REGION:

SUMMARY

Stepan Canada Inc., Longford Mills
(140004)

Organic Chemical

Central

Data for six Daphnia magna acute lethality toxicity
tests conducted on samples of combined effluent collected
between October 1989 and March 1990 were submitted by
Stepan Canada Inc. of Longford Mills.

Four of the six samples were not acutely lethal to
Daphnia. The remaining two samples induced an unusual
toxic response in which the greatest number of mortalities
occured in the middle concentrations of effluent.

combined effluent

08890443 sampled: 10/18/89 LC50:, >100 +
95% fid. limits: 0.0 - 0:10 +
comments:
08890471 sampled: 11/15/89 non-lethal
95% fid. Limits: 0.0" = DONS
comments:
08890491 sampled: 12/13/89 LEsSos , >1007 5
95tfid. dAaimatsi: OO -= 0.0"
comments:
08900032 sampled: 01/17/90 LCS0¢; |) S100 SE
95% fid. limits: 0.0 - 0.0 %
comments:
08900112 sampled: 02/20/90 non-lethal
95% fid. limits: 0.0 - OO
comments:
08900222 sampled: 03/21/90 non-lethal
95 sa fade limits 0.0 - OO
comments:

process effluent

emergency overflow

705

Stepan Canada Inc. (continued)
rain gauge

intake water

706

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COMPANY : Uniroyal Chemical Ltd., Elmira
(680108)
SECTOR: Organic Chemical
REGION: West Central
SUMMARY

The data for twenty-two trout bioassays, conducted on
combined effluent and once through cooling water samples
collected between October 1989 and March 1990, were
provided by Uniroyal Chemical Limited. Three of six

samples collected from combined effluent 0600 had 96 hour
LC50s of > 100 %. The other three samples were determined
to have been non-acutely lethal. One of six samples
collected from combined effluent 0800 had a 96 hour LC50 of
> 100 %. The other five samples were non-acutely lethal.
Two of six samples collected from the combined effluent
0900 had 96 hour LC50s of > 100 %. The other four samples
were non-acutely lethal.

One of the four cooling water samples had a 96 hour LC50:of
> 100 %, while the remaining were non-acutely lethal. All
Ministry audit testing of samples collected from the four
locations were determined to have been non-acutely lethal
to test fish.

OT cooling water

OT cooling water

01890284 sampled: 12/06/89 non-lethal
95% fide + lamest 0.0 - 0.0 %
comments: MISA audit sample.

03890374 sampled: 12/18/89 ÉC5HO0 >100: -%
95% nid: limits: 0.0 - 0.0 %
comments: LC50 >100

03900035 sampled: 01/15/90 non-lethal
95ÉMÉLd limits: 0.0 - 0.0 %
comments: Non-lethal

03900129 sampled: 02/19/90 non-lethal
95% -fid. limists: 0.0 - 0.08%
comments: Non-lethal

03900218 sampled: 03/19/90 non-lethal
95kMÉid «limits: 0.0 - 0:08
comments: Non lethal

713

Uniroyal Chemical Ltd. (continued)
OT cooling water
combined effluent
rain gauge
combined effluent
03890217 sampled: 10/16/89 non-lethal
95% -fid: limits: 0.0 - OO
comments: Non-lethal
03890286 sampled: 11/20/89 LC50: >100 %
95% fid limits: 0.0 - 050 &
comments: LC50 > 100
01890281 sampled: 12/06/89 non-lethal
95% fid. limits: 0.0 - 0.0 %
comments: MISA audit sample.
03890375 sampled: 12/18/89 non-lethal
952 tid. limits: 0.0 - 0.0 %
comments: Non-lethal
03900036 sampled: 01/15/90 non-lethal
663 fi. limits: 0.0 - 0.0 %
comments: Non-lethal
03900130 sampled: 02/19/90 LCS0:0 >100n7%
95% fid. limits: 0.0 - OF ONS
comments: Single Concentration Test--Lethal
03900217 sampled: 03/19/90 LC50:0 | >10022%
95% id. limits: 00 = 0.0 %
comments: LC50>100
combined effluent
combined effluent
03890218 sampled: 10/16/89 non-lethal
95% E1d. limits: 0.01 0.0 %
comments: Non-lethal
03890287 sampled: 11/20/89 LC50: >1,003 45
95% fid. limits: 0.0 - 0.0 %
comments: LC50 > 100
01890282 sampled: 12/06/89 non-lethal
95% £ id). Amies: O10) >= OMOLE
comments: MISA audit sample.

714

Uniroyal Chemical Ltd. (continued)

03890376 sampled: 12/18/89 non-lethal
95% Lid. limits: 0.0 - 0.0 +
comments: Non-lethal

03900037 sampled: 01/15/90 non-lethal
95% fid. limits: 0.0 - O0
comments: Non-lethal

03900127 sampled: 02/19/90 non-lethal
OStvf£id.. lamrts: 0.0 - 0.0 %
comments: Single Concentration Test; Non-lethal

03900219 sampled: 03/19/90 non-lethal
953) fad. Limits: 010: = OOS

comments: Single Concentration Test; Non lethal

combined effluent

03890219 sampled: 10/16/89 non-lethal
95% £id.s Limits: 0.0 - O20 6%
comments: Non-lethal
03890288 sampled: 11/20/89 LESOs "TOO %
95% fid. limits: 0.0 - OO
comments: LC50 > 100
01890283 sampled: 12/06/89 non-lethal
95% fid. limits: 01,0) = 001
comments: MISA audit sample.
03890377 sampled: 12/18/89 non-lethal
95% fid. limits: 0.0 - OS ONS
comments: Non-lethal
03900038 sampled: 01/15/90 LESC: >LOO! "+
953 Ed. limits: 0.0 - 0.0
comments: LC50 >100
03900128 sampled: 02/19/90 non-lethal
95 t= fad’. M IimÉESs : 0,0 5= DOS
comments: Non-lethal
03900220 sampled: 03/19/90 non-lethal
95% fid. limits: 0.0 - OO

comments: Non lethal

715

Uniroyal Chemical Ltd. (continued)

intake water

7.46

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COMPANY : Uniroyal Chemical Ltd., Elmira

(680108)
SECTOR: Organic Chemical
REGION: West Central

SUMMARY

Data for 24 Daphnia magna acute lethality toxicity
tests conducted on samples of effluent collected between
October 1989 and March 1990 were submitted by Uniroyal
Chemical Ltd. of Elmira.

One sample of once through cooling water was toxic to
Daphnia with a 48 h LC50 = 33.2%. The remaing three
samples submitted by the company had only one neonate die
in the 100% concentration in each test. An audit sample
collected in December was tested in the Ministry laboratory
and was found to be not acutely lethal to Daphnia.

Samples from combined effluent #600 were all toxic to
Daphnia. Two samples had LC50s > 100%, and the remaining
four samples had LC50s between 35.6 and 65.5%. The
Ministry audit sample conducted in December had an LC50
between 60 and 100%.

Three of six samples from combined effluent #900 were
nonlethal and the remaining three samples had LC50s > 100%.
The Ministry audit sample collected in December was not
acutely lethal to Daphnia.

Three of six samples from combined effluent #800 were
not acutely lethal to Daphnia and two samples had LC50s >
100%. The sample collected in November had a 48 h LC50 =
66.3%. The Ministry audit sample collected in December was
nonlethal.

OT cooling water
OT cooling water
02890284 sampled: 12/06/89 non-lethal

95% fid. limits: 0.0 - 0.0 %
comments: MISA Audit

03890374 sampled: 12/18/89 LESOs FSl00 =
95% fid: limits: 0.0 - 0.0 %
comments: Lethal; LC50>100

03900035 sampled: 01/15/90 LE50': BBR2 %
95% fid. limits: 230° —" "47.8 (> slope: 257
comments:

03900129 sampled: 02/19/90 LCS0N 100562
95% f1d. limits: 0.0 - 0.0 %

comments: LC50 >100

745

Uniroyal Chemical

03900218 sampled: 03/19/90
95% fid. limits: 0.0 -
comments: LC50 > 100

OT cooling water
combined effluent
rain gauge

combined effluent

03890217 sampled: 10/16/89
95% fid. limits: 0.0 -
comments: LC50 >100%

03890286 sampled: 11/20/89
95% fid. limits: 0.0 -
comments: LC50 >100%

02890281 sampled: 12/06/89
95% f1d. “himits': 0.0 -
comments: MISA Audit

03890375 sampled: 12/18/89
O54. fads IIMIES: 27.0 -
comments: Lethal

03900036 sampled: 01/15/90
95% fid. limits: 50.3 -
comments:

03900130 sampled: 02/19/90
95% fid. limits; 29.1 -
comments: Lethal

03900217 sampled: 03/19/90
95% fid. limits: 46.2 -
comments: Lethal

combined effluent
combined effluent

03890218 sampled: 10/16/89
DST A IIMIES : 0.0 -
comments: LC50 >100%

03890287 sampled: 11/20/89
Nays Seatols M TIAIMLES: 45.0 -
comments:

Ltd. (continued)
BESOR) \ 1004 ES
0.0 %
LC50 >100%e 1%
0.02
LC50 >100 %
0.0. %
LC50: 60.0
0.0 %
LC50 3516
46.9 % slope
LC50 65:25
85.1 % slope
LC50: BY 7214
48.2 % slope:
LE50); 58.4
T3 80% Slopes:
LC50 >100' 4%
0.0 %
LC50 66.3
OW 45s eslliope:

100.0

is)

Uniroyal Chemical Ltd.

02890282 sampled: 12/06/89
95% fid. limits: 0.0 -
comments: MISA Audit

03890376 sampled: 12/18/89
95% fad... amis: 0.0 -

0.

0.

comments: Lethal; LC50 > 100%

03900037 sampled: 01/15/90
95% fid. limits: 0.0 -
comments: |

03900127 sampled: 02/19/90
95% fid. limits: 0.0 -
comments: Non lethal

03900219 sampled: 03/19/90
95%. Lid. limits: 0.0 -
comments: Non lethal

combined effluent

03890219 sampled: 10/16/89
95% fid. limits: 0.0 -
comments: LC50 >100%

03890288 sampled: 11/20/89
95% fid. limits: 0.0 -
comments: LC50>100

02890283 sampled: 12/06/89
95% fid. limits: 0.0 -
comments: MISA Audit

03890377 sampled: 12/18/89
95% fid. limits: 0.0 -

0.

0.

QO.

0.

QO.

comments: Lethal; LC50 > 100%

03900038 sampled: 01/15/90
95% ide eames: 0.0 -
comments: Non lethal

03900128 sampled: 02/19/90
95% fad... MIMmLES: 0.0 -
comments: Non lethal

03900220 sampled: 03/19/90
JOSÉ. AIMAES: 0.0 -
comments: non lethal

0.

QO.

QO.

747

non-lethal
0 %

LE50i5. . 100
0 %

non-lethal
0 %

non-lethal
Or .3

non-lethal
0 %

Le50 >100

LC950:.. >100

non-lethal

0 %

0): >100

‘or
ie)
o Un

non-lethal
0 %

non-lethal
OMS

non-lethal
0 %

(continued)

oe

oe

Uniroyal Chemical Ltd. (continued)

intake water

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