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1911 


iBsued  May  9,  1011. 


United  States  Department  of  Agriculture, 

BUREAU  OF  SOILS— CIECULAR  No.  26. 

Milton  Whitney,  Chief. 


EXAMINATION  OF  SOIL  SAMPLES. 

Several  hundred  letters  are  received  annually  by  the  Bureau  of 
Soils  asking  for  more  or  less  specific  information  regarding  samples 
of  soils  sent  in  for  examination.  A  review  of  this  correspondence 
shows  that,  while  all  of  the  States  and  Territories  are  represented, 
about  half  of  the  requests  come  from  New  York,  Pennsylvania, 
Texas,  Virginia,  California,  Illinois,  Maryland,  New  Jersey,  Wash- 
ington, and  Florida,  in  about  the  order  named. 

It  appears  that  in  about  one-third  of  the  cases  submitted  for  an 
opinion  the  requests  are  for  advice  as  to  crop  adaptation,  about  one- 
third  for  information  regarding  fertilizer  requirements,  and  one- 
third  for  a  definite  chemical  examination  to  determine  the  amount  of 
some  one  or  more  of  the  mineral  elements — including  potash,  phos- 
phoric acid,  calcium,  and  magnesium — of  nitrates,  of  alkali,  and  of 
the  lime  requirement.  About  1  per  cent  of  the  requests  are  for  spe- 
cific information  requiring  a  special  laboratory  examination  for  the 
purpose  of  determining  harmful  constituents,  usually  suspected  to 
be  of  organic  nature. 

In  the  event  that  the  examinations  show  obscure  conditions,  and 
especially  if  they  indicate  the  presence  of  deleterious  substances  of 
organic  nature,  and  with  all  samples  submitted  for  the  specific  pur- 
pose of  determining  harmful  organic  constituents  suspected  of  caus- 
ing abnormally  low  yields  a  long  and  often  tedious  investigation  is 
required,  based  upon  the  methods  described  in  part  in  Bureau  of 
Soils  Bulletin  74. 

In  very  few  cases  is  it  considered  necessary  or  advisable  to  make  a 
chemical  analysis  by  any  one  of  the  well-known  acid  digestion 
methods,  as  the  result  of  such  an  examination  appears  to  throw  little 
light  upon  the  adaptation  of  crops  to  soils;  and  as  far  as  yield  is  con- 

80517°— Cir.  26— 11 


I 


cerned  there  are  many  contributing  factors  not  shown  by  the  analysis 
which  affect  this  as  much  or  more  than  the  relative  proportions  of  the 
mineral  constituents.  This  matter  is  treated  more  fully  in  Bureau  of 
Soils  Bulletins  55  and  57  and  Farmers'  Bulletin  257. 

When  a  sample  is  sent  to  the  bureau  for  advice  as  to  crop  adapta- 
tion a  determination  is  made,  so  far  as  can  be  done  from  a  small  sam- 
ple, of  the  nature  of  the  material,  to  identify  the  soil  series  to  which 
it  belongs.  If  the  exact  locality  from  which  the  sample  is  taken  is 
given  and  information  is  furnished  regarding  the  deeper  subsoil, 
the  drainage,  elevation,  slope,  location  along  streams  or  in  the  up- 
lands, the  occurrence  of  hardpan,  subsurface  gravel  or  rock  layers,  or 
other  information  bearing  upon  the  origin  and  mode  of  formation  of 
the  material,  an  examination  of  the  soil  and  subsoil  samples  by  the 
aid  of  the  keys  given  in  Bureau  of  Soils  Bulletin  78  will  usually  de- 
termine the  soil  series  to  which  it  belongs.  This  gives  at  once  the 
main  characteristics  of  the  soil  and  its  crop  adaptation  under  certain 
physical  and  topographical  conditions  which  will  be  referred  to  later. 

If  the  soil  is  found  to  belong  to  the  Hagerstown,  Sassafras,  Hous- 
ton, Norfolk,  Knox,  Marshall,  Dunkirk,  Clyde,  or  other  known 
series,  adaptations  are  advised  on  the  basis  of  the  known  normal 
peculiarities  of  the  series,  as  determined  by  the  soil  surveys.  The 
soil  sample  or  an  aqueous  extract  of  the  same  is  then  tested  by  the 
wire-basket  method,  described  in  Bureau  of  Soils  Circular  18,  or  by 
the  bottle-culture  method  described  in  Bureau  of  Soils  Bulletins  36 
and  70,  using  carbon  black  in  the  soil  extract  to  be  sure  that  there  is 
no  obscure  substance  present  that  will  unfit  the  soil  for  normal  crop 
development. 

A  sample  submitted  for  fertilizer  requirements  is  subjected  to  ex- 
amination by  the  wire-basket  method,  using  a  normally  productive 
soil  from  the  same  series  for  comparison,  adding  to  the  soil  which  is 
to  be  tested  manure,  lime,  and  commercial  fertilizers  in  approximately 
the  same  amounts  as  used  in  field  culture. 

The  requests  for  information  regarding  the  mineral  composition  of 
soils  are  complied  with  through  the  ordinary  analytical  methods 
when  it  appears  that  the  results  may  throw  any  light  upon  peculiar- 
ities of  constitution  or  character  of  the  soil  that  may  influence  its 
crop  production.  Many  of  these  cases,  it  is  believed,  can  more  prop- 
erly and  more  advantageously  be  considered  questions  of  fertilizer 
requirement.  It  is  oft^n  found  that  the  more  expeditious  method  of 
mineralogical  examination  or  analysis  gives  fuller  information  re- 
garding the  mineral  constitution  and  composition  of  the  soil  than 
does  the  chemical  analysis. 

All  soils  sent  in  for  examination  from  arid  regions,  or  generally 
where  the  rainfall  is  less  than  20  inches  per  annum,  are  examined  by 

IClr.  26] 


the  electrolytic  bridge  method,  described  in  Bureau  of  Soils  Bulletin 
61,  for  accumulations  of  alkali  salts,  and  this  is  carried  further,  if 
for  any  reason  it  seems  desirable,  by  an  analysis  of  the  individual 
saline  constituents  in  the  water  extract. 

The  foregoing  is  substantially  the  procedure  of  the  bureau  in  ex- 
aminations of  soil  samples  submitted  by  correspondence. 

It  is  necessary  to  bear  in  mind  that  the  most  thorough  examina- 
tion of  a  soil  may  reveal  nothing  of  a  deleterious  nature  or  nothing 
indicating  that  success  could  not  be  had  with  the  crops  adapted  to 
that  kind  of  material,  and  yet  these  crops  might  fail  if  certain  field 
indications  are  ignored.  Success  is  not  possible  if  the  drainage  con- 
ditions are  not  satisfactory,  if  the  elevation  and  topography  of  the 
farm  are  not  suitable,  if  the  methods  of  cultivation  and  cropping 
are  not  efficient,  and  if  the  market  demands  and  transportation  facil- 
ities are  inadequate.  Some  of  these  factors,  which  leave  nothing  in 
the  sample  that  can  possibly  be  revealed  and  others  which  may  or 
may  not  leave  eifects  that  could  only  be  determined  by  the  most  re- 
fined methods  and  after  exhaustive  research,  are  so  important  and  so 
much  more  easily  determined  through  a  field  examination  that  con- 
siderable space  will  be  given  their  consideration. 

Local  limitations  as  to  yields  of  crops  arise  partly  through  mis- 
control  and  partly  through  misadaptation  of  soils  to  crops.  The 
most  common  fault  in  the  control  of  soils  comes  through  the  method 
and  means  of  cultivation. 

The  equipment  of  a  farm  for  the  proper  and  efficient  cultivation 
of  any  particular  soil  type  should  be  regulated  by  the  grade  of  soil. 
Soils  ranging  in  grade  from  loams  to  clays  require  for  their  efficient 
control  a  farm  equipment  of  large  teams,  of  heavy  draft  animals,  and 
correspondingly  heavy  tools  and  implements,  with  substantial  and 
commodious  buildings.  A  silt  loam  is  usually  heavier  to  handle  than 
a  loam,  and  a  clay  is  usually  heavier  to  handle  than  a  silt  loam,  and 
provision  should  be  made  accordingly.  On  the  other  hand,  soils 
ranging  from  sand  to  fine  sandy  loams  require  for  their  most  efficient 
control  smaller  teams,  lighter  animals,  and  generally  lighter  tools  and 
implements,  and  less  commodious  buildings.  The  heavier  grades  of 
soil  not  only  offer  more  resistance  in  handling,  but  they  require  deeper 
and  more  thorough  cultivation.  Where  a  sand  may  be  efficiently 
cultivated  to  a  depth  of  4  or  5  inches,  a  silt  loam  or  clay  may  require 
8  or  9  inches  in  depth  of  cultivation. 

The  kind  of  implements  most  efficiently  used  on  the  different  grades 
of  soil  and  particularly  on  some  of  the  different  soil  types  should  be 
adapted  to  the  physical  character  of  the  soil.  A  loose  sand  or  sandy 
loam  should  be  worked  with  implements  that  tend  so  far  as  possible 
to  compact  the  subsoil,  while  a  silt  loam  that  tends  naturally  to  com- 

[Clr.  26] 


h 


pactness  unfavorable  to  crops  should  be  handled  with  implements 
that  tend  to  keep  it  in  the  loosest  possible  condition. 

A  second  condition  of  importance  in  soil  control  is  the  content  and 
character  of  the  organic  matter.  As  a  general  rule  soils  respond  to 
applications  of  organic  matter  whether  in  the  form  of  stable  manure 
or  of  plant  remains;  or,  to  state  it  in  another  yvay,  soils  to  do  their 
best  require  that  a  constant  supply  of  organic  matter  be  fed  to  them, 
and  that  this  organic  matter  be  of  such  character  as  to  be  6asily 
digested  by  the  soil.  No  standard  can  be  fixed  as  to  the  quantity  of 
organic  matter  a  soil  should  contain,  but  it  is  essential  for  its  most 
effective  use  that  it  should  at  all  times  contain  readily  digestible 
organic  matter. 

A  soil  is  most  efficient  when  crops  are  grown  upon  it  in  certain 
order  of  rotation.  It  is  not  to  be  expected  that  a  soil  will  produce 
as  large  a  crop  of  corn  immediately  following  potatoes  as  it  would 
if  the  corn  followed  sod;  nor  is  it  to  be  expected  that  the  soil  will 
produce  as  large  a  crop  of  wheat  following  wheat  as  it  would  if  a 
crop  of  clover  had  intervened  between  the  two  wheat  crops.  The 
general  principle  in  a  rotation  should  be  a  sod  followed  by  com,  then 
by  a  small  grain,  and  then  by  sod  again.  This  is  a  safe  general  guide 
where  such  crops  are  well  adapted  to  a  soil  type,  but  the  soil  types 
differ  so  markedly  in  their  adaptations  and  in  their  peculiarities  that 
no  general  rotation  can  be  expected  to  be  successful  on  all  types  of 
soil;  and  yet,  as  stated  above,  the  soil  will  maintain  its  maximum 
capacity  only  if  crops  are  rotated  in  certain  orders,  depending  upon 
the  soil  material,  the  soil  class,  and  the  crop  adaptations. 

Drainage  is  another  factor  upon  which  the  efficiency  of  the  soil 
depends.  There  is  an  optimum  water  content  for  each  type  and 
grade  of  soil  with  which  the  highest  efficiency  of  the  soil  may  be 
expected.  If  the  soil  is  so  situated  as  to  have  excessive  or  deficient 
drainage,  the  highest  efficiency  of  the  soil  can  not  be  expected  until 
these  conditions  are  alleviated. 

The  presence  of  certain  weeds,  and  in  general  an  abundance  of 
weeds,  lowers  the  efficiency  of  the  soil  for  all  cultivated  crops,  and 
weeds  are  often  indicators  of  soil  conditions  which  make  the  soil 
poorly  adapted  to  certain  crops. 

These  factors  of  miscontrol  do  not  leave  as  a  rule  sufficient  evi- 
dence in  the  soil  to  be  determined  by  a  laboratoi*y  examination  of  a 
sample,  and  where  failure  to  maintain  the  soil  in  its  highest  state  of 
efficiency  results  through  such  mismanagement,  it  is  the  part  of  the 
expert  farmer  or  soil  scientist,  skilled  in  handling  soil  material  in 
the  field,  rather  than  that  of  the  soil  chemist,  confined  to  laboratory 
examination,  to  determine  the  cause  of  failure  and  the  remedial 
measures. 

(Clr.  26] 


Failure  to  maintain  a  high  degree  of  efficiency  of  the  soil  for  any 
particular  crop  is  very  often  seen  in  the  misadaptation  of  soil  mate- 
rial or  the  use  of  a  soil  series  which  does  not  function  properly  for 
the  crop  grown.  As  an  illustration,  it  is  not  to  be  expected  that 
soils  of  the  Portsmouth,  Volusia,  and  Susquehanna  series  will  pro- 
duce under  normal  conditions  of  cultivation  satisfactory  crops  of 
wheat,  and  with  other  series  there  are  degrees  of  adaptation  from 
which  it  is  possible  to  eliminate  many  soils  from  consideration  for 
commercial  wheat  production. 

In  the  matter  of  class  of  material,  also,  the  sands  and  up  to  and 
including  the  fine  sandy  loams  are  generally  unsuited  to  wheat  pro- 
duction, while  the  heavier  members  of  the  series  may  be  admirably 
adapted  to  this  crop.  This  illustration  holds  for  most  soils  and  for 
most  crops,  and  it  is  not  to  be  expected  that  equal  success  will  be 
attained  by  the  indiscriminate  use  of  soils  for  any  or  all  crops. 

The  structure  of  a  soil  and  subsoil  and  often  of  the  deep  subsoil 
affect  the  adaptation  to  crops  without  imparting  to  the  soil  sample 
evidences  of  the  unfavorable  conditions  which  exist.  Such  condi- 
tions can  only  be  determined  by  a  field  examination. 

In  many  instances  the  depth  to  the  subsoil  determines  the  charac- 
ter, grade,  or  yield  of  crops,  particularly  in  highly  specialized  indus- 
tries. For  example,  in  the  production  of  the  Sumatra  leaf  tobacco 
on  the  Norfolk  fine  sandy  loam  in  Florida,  a  soil  of  medium  depth 
of  6  or  8  inches  gives  by  far  the  better  quality,  and  where  the  sub- 
soil is  found  closer  to  the  surface  or  considerably  deeper  equally 
good  results  are  not  to  be  expected. 

Topography  and  elevation  play  an  important  part  in  the  adapta- 
tion of  certain  crops,  sometimes  limiting  sharply  the  kinds  and  at 
other  times  the  quality  or  the  yield. 

The  color  of  the  soil  is  often  a  safe  guide  in  the  adaptation  of  soils, 
indicating  as  it  does  not  only  material  differences  in  constitution, 
but  also  the  general  nature  of  the  processes  taking  place  in  the  soil. 

The  presence  of  concretionary  formations,  either  as  graved  or  as 
more  or  less  continuous  layers  of  hardpan,  influence  the  adaptation 
and  frequently  the  yield,  acting  in  such  a  way  as  to  leave  no  sensible 
effect  upon  the  sample  submitted  for  examination,  and  requiring  a 
field  investigation  rather  than  a  laboratory  analysis. 

All  of  these  subjects  are  treated  in  the  soil  survey  reports  and 
adequate  information  is  supplied  for  such  areas  as  have  been  sur- 
veyed, but  where  misadaptation  of  material  owing  to  the  presence  of 
any  of  th^e  factors  gives  an  insufficient  crop,  the  results  of  labora- 
tory investigations  upon  the  sample,  removed  from  its  place  in  the 
field  and  changed  in  its  physical  conditions  through  packing  and 

[Cir.  26] 


transportation,  do  not  apply.     It  is  only  in  the  absence  of  these 
limiting  conditions  that  such  results  are  of  value. 

It,  thus,  is  essential  to  the  proper  investigation  of  a  sample  of  soil 
by  the  bureau  that  the  purpose  for  which  the  examination  is  required 
be  stated,  and  that  information  be  given  which  will  enable  the  bureau 
to  identify  the  material,  the  agencies  which  have  led  to  its  formation, 
and  those  that  have  influenced  the  present  condition  of  the  soil.  The 
general  purposes  for  which  such  examinations  may  be  requested  may 
be  briefly  stated : 

1.  Adaptation  of  the  soil  for  crop& 

2.  Fertilizer  and  manurial  requirements. 

3.  Alkali  determination. 

4.  Special  chemical  and  mineralogical  examination. 

5.  Investigations  to  reveal  the  presence  of  deleterious  substances  suspected  to 
be  of  organic  nature. 

The  purpose  for  which  the  soil  is  to  be  used  should  be  stated — that 
is,  whether  for  greenhouse,  garden,  or  field  crops,  and  the  kind  of 
crops  it  is  intended  to  grow. 

The  general  topography  and  elevation  of  the  field  should  be  stated 
and  its  relative  position  with  respect  to  surrounding  fields.  If  the 
soil  occurs  as  prairie  or  not,  this  fact  should  be  stated,  together  with 
the  nature  and  species  of  the  native  plants,  whether  weeds,  grass,  or 
trees. 

The  occurrence  of  concretionary  formations  such  as  ferruginous 
or  calcareous  hardpan  or  nodules  will  often  aid  in  the  identification 
of  material  and  in  the  consideration  of  the  problem  of  adaptation 
and  yield.  If  the  soil  is  of  recent  alluvium,  it  should  be  stated 
whether  of  first  bottom  or  of  second  bottom,  and  a  note  should  be 
made  of  the  drainage  conditions.  Any  unusual  phenomena  or  ab- 
normal growth  or  death  of  crop  should  be  stated,  and  general  infor- 
mation as  to  the  crops  previously  grown  and  the  character  and 
efficiency  of  cultivation. 

It  is  advisable  always  to  have  a  sufficiently  large  sample  to  serve 
for  the  different  kinds  of  examinations  that  will  be  required.  For 
this  purpose  there  should  be  submitted  at  least  10  pounds  of  the  top 
soil  taken  down  to  a  change  of  color  or  of  texture  marking  the  sub- 
soil; or  if  tnere  is  no  particular  difference  between  the  soil  and  sub- 
soil, the  sample  should  be  taken  to  a  depth  of  at  least  8  or  9  inches. 
There  should  also  be  submitted  a  sample  of  about  5  pounds  of  the 
subsoil  immediately  underlying;  and  if  there  is  a  gravel  substratum 
below  this,  the  fact  should  be  stated.  Care  should  be  exercised  in 
securing  the  sample  to  select  a  spot  representing  as  accurately  as 
possible  the  conditions  that  are  to  be  investigated.    If  the  examina- 

[Cir.  26] 


tion  is  to  be  for  the  general  characteristics  of  a  field,  it  is  better  to 
make  a  composite  sample  from  8  or  10  different  parts  of  the  field. 
In  all  cases  the  exact  location  of  the  farm  should  be  stated,  giving 
distances  in  miles  and  direction  from  some  post-office,  town,  or  vil- 
lage or  indicating  position  by  land  lines. 

Approved : 

James  Welson, 

Secretary  of  Agriculture. 

Washington,  D.  C,  April  7, 1911. 

tClr.  26] 


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